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HomeMy WebLinkAbout2021-05-03 Analyticals[TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2102508 Report Date: May 03, 2021 16:36 Natural Healing CenterNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 23, 2021 13:40 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com California ELAP Certification # 2438 client.oec.com\reportsClient Connect: Page 1 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix Bin 2094-A 2102508-01 04/23/2021 11:00 04/23/2021 13:40Solid Solid Bin 2094-B 2102508-02 04/23/2021 11:05 04/23/2021 13:40Solid Solid Bin 2094-C 2102508-03 04/23/2021 11:10 04/23/2021 13:40Solid Solid Bin 20340-A 2102508-04 04/23/2021 11:15 04/23/2021 13:40Solid Solid Bin 20340-B 2102508-05 04/23/2021 11:20 04/23/2021 13:40Solid Solid Bin 20340-C 2102508-06 04/23/2021 11:25 04/23/2021 13:40Solid Solid Bin 20158-A 2102508-07 04/23/2021 11:30 04/23/2021 13:40Solid Solid Bin 20158-B 2102508-08 04/23/2021 11:35 04/23/2021 13:40Solid Solid Bin 20158-C 2102508-09 04/23/2021 11:40 04/23/2021 13:40Solid Solid Bin 2088-A 2102508-10 04/23/2021 11:45 04/23/2021 13:40Solid Solid Bin 2088-B 2102508-11 04/23/2021 11:50 04/23/2021 13:40Solid Solid Bin 2088-C 2102508-12 04/23/2021 11:55 04/23/2021 13:40Solid Solid Bin 20376-A 2102508-13 04/23/2021 12:00 04/23/2021 13:40Solid Solid Bin 20376-B 2102508-14 04/23/2021 12:05 04/23/2021 13:40Solid Solid Bin 20376-C 2102508-15 04/23/2021 12:10 04/23/2021 13:40Solid Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 2 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID *** DEFAULT GENERAL METHOD *** Asbestos Bulk PLM-(non-soil& Asphalt)(sub) OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 04/27/2021 07:10B1D0766 STLC Metals by ICP 6010B STLC 04/30/2021 10:33B1D0916 STLC Metals Extraction STLC Metals Extraction 04/28/2021 12:44B1D0838 TCLP Metals by ICP 6010B TCLP 04/30/2021 10:49B1D0919 TCLP Metals Extraction TCLP Metals Extraction 04/28/2021 12:48B1D0839 Total Metals by CVAA Mercury Total EPA 7471A 04/26/2021 09:00B1D0711 Total Metals by ICP 6010B Total 04/26/2021 07:37B1D0734 Volatile Organic Compounds by GC/MS 8260B Full List 04/23/2021 12:11B1D0650 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 04/23/2021 14:16B1D0692 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 3 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.095 B1D0711 04/26/21 14:53mg/kg 1Mercury0.094 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 13:51mg/kg B1D07341Antimony2.4 "7.4 """"Arsenic 1.9 "690 """"Barium 0.97 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "64 """"Chromium 0.48 N-02 "14 """"Cobalt 0.48 "260 """"Copper 0.97 N-02 "2400 """"Lead 0.48 N-01, N-03 "2.0 """"Molybdenum 0.48 "94 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.97 "31 """"Vanadium 1.9 "1300 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.28 B1D0916 05/03/21 12:58mg/L 2Chromium0.10 "1.6 """"Copper 0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B2.0 B1D0919 05/03/21 14:09mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 4 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 14:32mg/kg B1D06921TPH Gasoline (C5-C12)4.9 R-07 """( 39 - 157 )94 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/27/21 15:24mg/kg B1D07661TPH Diesel (C13-C22)10 "97 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )84 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 5 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 17:17mg/kg B1D06501Benzene0.051 ND """ ""Bromobenzene 0.051 ND """ ""Bromochloromethane 0.051 ND """ ""Bromodichloromethane 0.051 ND """ ""Bromoform 0.051 ND """ ""Bromomethane 0.051 ND """ ""n-Butylbenzene 0.051 ND """ ""sec-Butylbenzene 0.051 ND """ ""tert-Butylbenzene 0.051 ND """ ""Carbon tetrachloride 0.051 ND """ ""Chlorobenzene 0.051 ND """ ""Chloroethane 0.051 ND """ ""Chloroform 0.051 ND """ ""Chloromethane 0.051 ND """ ""2-Chlorotoluene 0.051 ND """ ""4-Chlorotoluene 0.051 ND """ ""Dibromochloromethane 0.051 ND """ ""1,2-Dibromo-3-chloropropane 0.051 ND """ ""1,2-Dibromoethane (EDB)0.051 ND """ ""Dibromomethane 0.051 ND """ ""1,2-Dichlorobenzene 0.051 ND """ ""1,3-Dichlorobenzene 0.051 ND """ ""1,4-Dichlorobenzene 0.051 ND """ ""Dichlorodifluoromethane 0.051 ND """ ""1,1-Dichloroethane 0.051 ND """ ""1,2-Dichloroethane 0.051 ND """ ""1,1-Dichloroethene 0.051 ND """ ""cis-1,2-Dichloroethene 0.051 ND """ ""trans-1,2-Dichloroethene 0.051 ND """ ""1,2-Dichloropropane 0.051 ND """ ""1,3-Dichloropropane 0.051 ND """ ""2,2-Dichloropropane 0.051 ND """ ""1,1-Dichloropropene 0.051 ND """ ""cis-1,3-Dichloropropene 0.051 ND """ ""trans-1,3-Dichloropropene 0.051 ND """ ""Ethylbenzene 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 6 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 17:17mg/kg B1D06501Hexachlorobutadiene0.051 ND """ ""4-Isopropyl Toluene 0.051 ND """ ""Isopropylbenzene 0.051 ND """ ""Methylene chloride 0.051 ND """ ""Naphthalene 0.051 ND """ ""n-Propylbenzene 0.051 ND """ ""Styrene 0.051 ND """ ""1,1,1,2-Tetrachloroethane 0.051 ND """ ""1,1,2,2-Tetrachloroethane 0.051 ND """ ""Tetrachloroethene (PCE)0.051 ND """ ""Toluene 0.051 ND """ ""1,2,3-Trichlorobenzene 0.051 ND """ ""1,2,4-Trichlorobenzene 0.051 ND """ ""1,1,1-Trichloroethane 0.051 ND """ ""1,1,2-Trichloroethane 0.051 ND """ ""Trichloroethene (TCE)0.051 ND """ ""Trichlorofluoromethane 0.051 ND """ ""1,2,3-Trichloropropane 0.051 ND """ ""1,2,4-Trimethylbenzene 0.051 ND """ ""1,3,5-Trimethylbenzene 0.051 ND """ ""Vinyl chloride 0.051 ND """ ""Xylenes (total)0.051 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )89 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 7 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:02mg/kg B1D07111Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 13:54mg/kg B1D07341Antimony2.4 "7.6 """"Arsenic 1.9 "220 """"Barium 0.97 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "100 """"Chromium 0.48 N-02, N-03 "15 """"Cobalt 0.48 "61 """"Copper 0.97 "320 """"Lead 0.48 N-02, N-03 "1.6 """"Molybdenum 0.48 "130 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.97 "38 """"Vanadium 1.9 "410 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.29 B1D0916 05/03/21 13:00mg/L 2Chromium0.10 "20 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/03/21 14:26mg/L B1D09191Chromium0.050 "0.31 """"Lead 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 8 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 14:58mg/kg B1D06921TPH Gasoline (C5-C12)4.8 R-07 """( 39 - 157 )99 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M16B1D076604/27/21 15:24mg/kg 1TPH Diesel (C13-C22)10 D-06 "150 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )80 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 9 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 17:45mg/kg B1D06501Benzene0.049 ND """ ""Bromobenzene 0.049 ND """ ""Bromochloromethane 0.049 ND """ ""Bromodichloromethane 0.049 ND """ ""Bromoform 0.049 ND """ ""Bromomethane 0.049 ND """ ""n-Butylbenzene 0.049 ND """ ""sec-Butylbenzene 0.049 ND """ ""tert-Butylbenzene 0.049 ND """ ""Carbon tetrachloride 0.049 ND """ ""Chlorobenzene 0.049 ND """ ""Chloroethane 0.049 ND """ ""Chloroform 0.049 ND """ ""Chloromethane 0.049 ND """ ""2-Chlorotoluene 0.049 ND """ ""4-Chlorotoluene 0.049 ND """ ""Dibromochloromethane 0.049 ND """ ""1,2-Dibromo-3-chloropropane 0.049 ND """ ""1,2-Dibromoethane (EDB)0.049 ND """ ""Dibromomethane 0.049 ND """ ""1,2-Dichlorobenzene 0.049 ND """ ""1,3-Dichlorobenzene 0.049 ND """ ""1,4-Dichlorobenzene 0.049 ND """ ""Dichlorodifluoromethane 0.049 ND """ ""1,1-Dichloroethane 0.049 ND """ ""1,2-Dichloroethane 0.049 ND """ ""1,1-Dichloroethene 0.049 ND """ ""cis-1,2-Dichloroethene 0.049 ND """ ""trans-1,2-Dichloroethene 0.049 ND """ ""1,2-Dichloropropane 0.049 ND """ ""1,3-Dichloropropane 0.049 ND """ ""2,2-Dichloropropane 0.049 ND """ ""1,1-Dichloropropene 0.049 ND """ ""cis-1,3-Dichloropropene 0.049 ND """ ""trans-1,3-Dichloropropene 0.049 ND """ ""Ethylbenzene 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 10 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 17:45mg/kg B1D06501Hexachlorobutadiene0.049 ND """ ""4-Isopropyl Toluene 0.049 ND """ ""Isopropylbenzene 0.049 ND """ ""Methylene chloride 0.049 ND """ ""Naphthalene 0.049 ND """ ""n-Propylbenzene 0.049 ND """ ""Styrene 0.049 ND """ ""1,1,1,2-Tetrachloroethane 0.049 ND """ ""1,1,2,2-Tetrachloroethane 0.049 ND """ ""Tetrachloroethene (PCE)0.049 ND """ ""Toluene 0.049 ND """ ""1,2,3-Trichlorobenzene 0.049 ND """ ""1,2,4-Trichlorobenzene 0.049 ND """ ""1,1,1-Trichloroethane 0.049 ND """ ""1,1,2-Trichloroethane 0.049 ND """ ""Trichloroethene (TCE)0.049 ND """ ""Trichlorofluoromethane 0.049 ND """ ""1,2,3-Trichloropropane 0.049 ND """ ""1,2,4-Trimethylbenzene 0.049 ND """ ""1,3,5-Trimethylbenzene 0.049 ND """ ""Vinyl chloride 0.049 ND """ ""Xylenes (total)0.049 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 11 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-03 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.17 B1D0711 04/26/21 15:04mg/kg 1Mercury0.098 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:05mg/kg B1D07341Antimony2.5 "7.7 """"Arsenic 2.0 "280 """"Barium 1.0 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "52 """"Chromium 0.50 N-02 "10 """"Cobalt 0.50 "79 """"Copper 1.0 "270 """"Lead 0.50 N-02, N-03 "1.1 """"Molybdenum 0.50 "69 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "34 """"Vanadium 2.0 "370 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.24 B1D0916 05/03/21 13:03mg/L 2Chromium0.10 "22 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.11 B1D0919 05/03/21 14:29mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 12 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 15:24mg/kg B1D06921TPH Gasoline (C5-C12)4.8 R-07 """( 39 - 157 )93 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/27/21 15:47mg/kg B1D07661TPH Diesel (C13-C22)10 "220 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )79 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 13 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 18:12mg/kg B1D06501Benzene0.049 ND """ ""Bromobenzene 0.049 ND """ ""Bromochloromethane 0.049 ND """ ""Bromodichloromethane 0.049 ND """ ""Bromoform 0.049 ND """ ""Bromomethane 0.049 ND """ ""n-Butylbenzene 0.049 ND """ ""sec-Butylbenzene 0.049 ND """ ""tert-Butylbenzene 0.049 ND """ ""Carbon tetrachloride 0.049 ND """ ""Chlorobenzene 0.049 ND """ ""Chloroethane 0.049 ND """ ""Chloroform 0.049 ND """ ""Chloromethane 0.049 ND """ ""2-Chlorotoluene 0.049 ND """ ""4-Chlorotoluene 0.049 ND """ ""Dibromochloromethane 0.049 ND """ ""1,2-Dibromo-3-chloropropane 0.049 ND """ ""1,2-Dibromoethane (EDB)0.049 ND """ ""Dibromomethane 0.049 ND """ ""1,2-Dichlorobenzene 0.049 ND """ ""1,3-Dichlorobenzene 0.049 ND """ ""1,4-Dichlorobenzene 0.049 ND """ ""Dichlorodifluoromethane 0.049 ND """ ""1,1-Dichloroethane 0.049 ND """ ""1,2-Dichloroethane 0.049 ND """ ""1,1-Dichloroethene 0.049 ND """ ""cis-1,2-Dichloroethene 0.049 ND """ ""trans-1,2-Dichloroethene 0.049 ND """ ""1,2-Dichloropropane 0.049 ND """ ""1,3-Dichloropropane 0.049 ND """ ""2,2-Dichloropropane 0.049 ND """ ""1,1-Dichloropropene 0.049 ND """ ""cis-1,3-Dichloropropene 0.049 ND """ ""trans-1,3-Dichloropropene 0.049 ND """ ""Ethylbenzene 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 14 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 18:12mg/kg B1D06501Hexachlorobutadiene0.049 ND """ ""4-Isopropyl Toluene 0.049 ND """ ""Isopropylbenzene 0.049 ND """ ""Methylene chloride 0.049 ND """ ""Naphthalene 0.049 ND """ ""n-Propylbenzene 0.049 ND """ ""Styrene 0.049 ND """ ""1,1,1,2-Tetrachloroethane 0.049 ND """ ""1,1,2,2-Tetrachloroethane 0.049 ND """ ""Tetrachloroethene (PCE)0.049 ND """ ""Toluene 0.049 ND """ ""1,2,3-Trichlorobenzene 0.049 ND """ ""1,2,4-Trichlorobenzene 0.049 ND """ ""1,1,1-Trichloroethane 0.049 ND """ ""1,1,2-Trichloroethane 0.049 ND """ ""Trichloroethene (TCE)0.049 ND """ ""Trichlorofluoromethane 0.049 ND """ ""1,2,3-Trichloropropane 0.049 ND """ ""1,2,4-Trimethylbenzene 0.049 ND """ ""1,3,5-Trimethylbenzene 0.049 ND """ ""Vinyl chloride 0.049 ND """ ""Xylenes (total)0.049 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 15 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-04 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.13 B1D0711 04/26/21 15:06mg/kg 1Mercury0.087 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:07mg/kg B1D07341Antimony2.5 "7.3 """"Arsenic 2.0 "230 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "58 """"Chromium 0.49 N-02 "12 """"Cobalt 0.49 "63 """"Copper 0.98 "390 """"Lead 0.49 N-02, N-03 "2.1 """"Molybdenum 0.49 "69 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "35 """"Vanadium 2.0 "530 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.24 B1D0916 05/03/21 13:05mg/L 2Chromium0.10 "14 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.20 B1D0919 05/03/21 14:31mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 16 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 15:50mg/kg B1D06921TPH Gasoline (C5-C12)5.2 R-07 """( 39 - 157 )99 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/27/21 15:47mg/kg B1D07661TPH Diesel (C13-C22)10 "170 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 17 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 18:40mg/kg B1D06501Benzene0.051 ND """ ""Bromobenzene 0.051 ND """ ""Bromochloromethane 0.051 ND """ ""Bromodichloromethane 0.051 ND """ ""Bromoform 0.051 ND """ ""Bromomethane 0.051 ND """ ""n-Butylbenzene 0.051 ND """ ""sec-Butylbenzene 0.051 ND """ ""tert-Butylbenzene 0.051 ND """ ""Carbon tetrachloride 0.051 ND """ ""Chlorobenzene 0.051 ND """ ""Chloroethane 0.051 ND """ ""Chloroform 0.051 ND """ ""Chloromethane 0.051 ND """ ""2-Chlorotoluene 0.051 ND """ ""4-Chlorotoluene 0.051 ND """ ""Dibromochloromethane 0.051 ND """ ""1,2-Dibromo-3-chloropropane 0.051 ND """ ""1,2-Dibromoethane (EDB)0.051 ND """ ""Dibromomethane 0.051 ND """ ""1,2-Dichlorobenzene 0.051 ND """ ""1,3-Dichlorobenzene 0.051 ND """ ""1,4-Dichlorobenzene 0.051 ND """ ""Dichlorodifluoromethane 0.051 ND """ ""1,1-Dichloroethane 0.051 ND """ ""1,2-Dichloroethane 0.051 ND """ ""1,1-Dichloroethene 0.051 ND """ ""cis-1,2-Dichloroethene 0.051 ND """ ""trans-1,2-Dichloroethene 0.051 ND """ ""1,2-Dichloropropane 0.051 ND """ ""1,3-Dichloropropane 0.051 ND """ ""2,2-Dichloropropane 0.051 ND """ ""1,1-Dichloropropene 0.051 ND """ ""cis-1,3-Dichloropropene 0.051 ND """ ""trans-1,3-Dichloropropene 0.051 ND """ ""Ethylbenzene 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 18 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 18:40mg/kg B1D06501Hexachlorobutadiene0.051 ND """ ""4-Isopropyl Toluene 0.051 ND """ ""Isopropylbenzene 0.051 ND """ ""Methylene chloride 0.051 ND """ ""Naphthalene 0.051 ND """ ""n-Propylbenzene 0.051 ND """ ""Styrene 0.051 ND """ ""1,1,1,2-Tetrachloroethane 0.051 ND """ ""1,1,2,2-Tetrachloroethane 0.051 ND """ ""Tetrachloroethene (PCE)0.051 ND """ ""Toluene 0.051 ND """ ""1,2,3-Trichlorobenzene 0.051 ND """ ""1,2,4-Trichlorobenzene 0.051 ND """ ""1,1,1-Trichloroethane 0.051 ND """ ""1,1,2-Trichloroethane 0.051 ND """ ""Trichloroethene (TCE)0.051 ND """ ""Trichlorofluoromethane 0.051 ND """ ""1,2,3-Trichloropropane 0.051 ND """ ""1,2,4-Trimethylbenzene 0.051 ND """ ""1,3,5-Trimethylbenzene 0.051 ND """ ""Vinyl chloride 0.051 ND """ ""Xylenes (total)0.051 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 19 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-05 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.095 B1D0711 04/26/21 15:08mg/kg 1Mercury0.091 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:10mg/kg B1D07341Antimony2.5 "10 """"Arsenic 2.0 "240 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "50 """"Chromium 0.49 N-02 "11 """"Cobalt 0.49 "54 """"Copper 0.98 "800 """"Lead 0.49 N-02, N-03 "0.77 """"Molybdenum 0.49 "79 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "37 """"Vanadium 2.0 "350 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.29 B1D0916 05/03/21 13:08mg/L 2Chromium0.10 "120 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.23 B1D0919 05/03/21 14:34mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 20 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 16:16mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )99 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M37B1D076604/27/21 16:09mg/kg 1TPH Diesel (C13-C22)10 D-06 "280 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 21 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 19:07mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 22 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 19:07mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )91 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 23 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-06 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:10mg/kg B1D07111Mercury0.091 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:13mg/kg B1D07341Antimony2.4 "11 """"Arsenic 2.0 "340 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.24 "50 """"Chromium 0.49 N-02 "14 """"Cobalt 0.49 "230 """"Copper 0.98 "1200 """"Lead 0.49 N-01, N-03 "1.7 """"Molybdenum 0.49 "73 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "32 """"Vanadium 2.0 "1000 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.32 B1D0916 05/03/21 13:11mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.84 B1D0919 05/03/21 14:36mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 24 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 16:42mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )96 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M29B1D076604/27/21 16:09mg/kg 1TPH Diesel (C13-C22)10 D-06 "150 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )83 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 25 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 19:35mg/kg B1D06501Benzene0.050 ND """ ""Bromobenzene 0.050 ND """ ""Bromochloromethane 0.050 ND """ ""Bromodichloromethane 0.050 ND """ ""Bromoform 0.050 ND """ ""Bromomethane 0.050 ND """ ""n-Butylbenzene 0.050 ND """ ""sec-Butylbenzene 0.050 ND """ ""tert-Butylbenzene 0.050 ND """ ""Carbon tetrachloride 0.050 ND """ ""Chlorobenzene 0.050 ND """ ""Chloroethane 0.050 ND """ ""Chloroform 0.050 ND """ ""Chloromethane 0.050 ND """ ""2-Chlorotoluene 0.050 ND """ ""4-Chlorotoluene 0.050 ND """ ""Dibromochloromethane 0.050 ND """ ""1,2-Dibromo-3-chloropropane 0.050 ND """ ""1,2-Dibromoethane (EDB)0.050 ND """ ""Dibromomethane 0.050 ND """ ""1,2-Dichlorobenzene 0.050 ND """ ""1,3-Dichlorobenzene 0.050 ND """ ""1,4-Dichlorobenzene 0.050 ND """ ""Dichlorodifluoromethane 0.050 ND """ ""1,1-Dichloroethane 0.050 ND """ ""1,2-Dichloroethane 0.050 ND """ ""1,1-Dichloroethene 0.050 ND """ ""cis-1,2-Dichloroethene 0.050 ND """ ""trans-1,2-Dichloroethene 0.050 ND """ ""1,2-Dichloropropane 0.050 ND """ ""1,3-Dichloropropane 0.050 ND """ ""2,2-Dichloropropane 0.050 ND """ ""1,1-Dichloropropene 0.050 ND """ ""cis-1,3-Dichloropropene 0.050 ND """ ""trans-1,3-Dichloropropene 0.050 ND """ ""Ethylbenzene 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 26 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 19:35mg/kg B1D06501Hexachlorobutadiene0.050 ND """ ""4-Isopropyl Toluene 0.050 ND """ ""Isopropylbenzene 0.050 ND """ ""Methylene chloride 0.050 ND """ ""Naphthalene 0.050 ND """ ""n-Propylbenzene 0.050 ND """ ""Styrene 0.050 ND """ ""1,1,1,2-Tetrachloroethane 0.050 ND """ ""1,1,2,2-Tetrachloroethane 0.050 ND """ ""Tetrachloroethene (PCE)0.050 ND """ ""Toluene 0.050 ND """ ""1,2,3-Trichlorobenzene 0.050 ND """ ""1,2,4-Trichlorobenzene 0.050 ND """ ""1,1,1-Trichloroethane 0.050 ND """ ""1,1,2-Trichloroethane 0.050 ND """ ""Trichloroethene (TCE)0.050 ND """ ""Trichlorofluoromethane 0.050 ND """ ""1,2,3-Trichloropropane 0.050 ND """ ""1,2,4-Trimethylbenzene 0.050 ND """ ""1,3,5-Trimethylbenzene 0.050 ND """ ""Vinyl chloride 0.050 ND """ ""Xylenes (total)0.050 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 27 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-07 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.11 B1D0711 04/26/21 15:12mg/kg 1Mercury0.092 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP EPA 6010B5.9 B1D0734 04/26/21 14:16mg/kg 1Antimony2.5 "8.5 """"Arsenic 2.0 "260 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "65 """"Chromium 0.49 N-02 "11 """"Cobalt 0.49 "77 """"Copper 0.98 "530 """"Lead 0.49 N-02, N-03 "1.2 """"Molybdenum 0.49 "91 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "34 """"Vanadium 2.0 "780 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.59 B1D0916 05/03/21 13:21mg/L 2Chromium0.10 "17 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.12 B1D0919 05/03/21 14:39mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 28 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 28 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 17:08mg/kg B1D06921TPH Gasoline (C5-C12)5.1 R-07 """( 39 - 157 )98 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M38B1D076604/27/21 16:32mg/kg 1TPH Diesel (C13-C22)10 "150 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 29 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 29 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 20:02mg/kg B1D06501Benzene0.045 ND """ ""Bromobenzene 0.045 ND """ ""Bromochloromethane 0.045 ND """ ""Bromodichloromethane 0.045 ND """ ""Bromoform 0.045 ND """ ""Bromomethane 0.045 ND """ ""n-Butylbenzene 0.045 ND """ ""sec-Butylbenzene 0.045 ND """ ""tert-Butylbenzene 0.045 ND """ ""Carbon tetrachloride 0.045 ND """ ""Chlorobenzene 0.045 ND """ ""Chloroethane 0.045 ND """ ""Chloroform 0.045 ND """ ""Chloromethane 0.045 ND """ ""2-Chlorotoluene 0.045 ND """ ""4-Chlorotoluene 0.045 ND """ ""Dibromochloromethane 0.045 ND """ ""1,2-Dibromo-3-chloropropane 0.045 ND """ ""1,2-Dibromoethane (EDB)0.045 ND """ ""Dibromomethane 0.045 ND """ ""1,2-Dichlorobenzene 0.045 ND """ ""1,3-Dichlorobenzene 0.045 ND """ ""1,4-Dichlorobenzene 0.045 ND """ ""Dichlorodifluoromethane 0.045 ND """ ""1,1-Dichloroethane 0.045 ND """ ""1,2-Dichloroethane 0.045 ND """ ""1,1-Dichloroethene 0.045 ND """ ""cis-1,2-Dichloroethene 0.045 ND """ ""trans-1,2-Dichloroethene 0.045 ND """ ""1,2-Dichloropropane 0.045 ND """ ""1,3-Dichloropropane 0.045 ND """ ""2,2-Dichloropropane 0.045 ND """ ""1,1-Dichloropropene 0.045 ND """ ""cis-1,3-Dichloropropene 0.045 ND """ ""trans-1,3-Dichloropropene 0.045 ND """ ""Ethylbenzene 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 30 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 20:02mg/kg B1D06501Hexachlorobutadiene0.045 ND """ ""4-Isopropyl Toluene 0.045 ND """ ""Isopropylbenzene 0.045 ND """ ""Methylene chloride 0.045 ND """ ""Naphthalene 0.045 ND """ ""n-Propylbenzene 0.045 ND """ ""Styrene 0.045 ND """ ""1,1,1,2-Tetrachloroethane 0.045 ND """ ""1,1,2,2-Tetrachloroethane 0.045 ND """ ""Tetrachloroethene (PCE)0.045 ND """ ""Toluene 0.045 ND """ ""1,2,3-Trichlorobenzene 0.045 ND """ ""1,2,4-Trichlorobenzene 0.045 ND """ ""1,1,1-Trichloroethane 0.045 ND """ ""1,1,2-Trichloroethane 0.045 ND """ ""Trichloroethene (TCE)0.045 ND """ ""Trichlorofluoromethane 0.045 ND """ ""1,2,3-Trichloropropane 0.045 ND """ ""1,2,4-Trimethylbenzene 0.045 ND """ ""1,3,5-Trimethylbenzene 0.045 ND """ ""Vinyl chloride 0.045 ND """ ""Xylenes (total)0.045 """( 74 - 122 )96 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )93 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 31 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-08 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.12 B1D0711 04/26/21 15:14mg/kg 1Mercury0.090 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:19mg/kg B1D07341Antimony2.5 "6.5 """"Arsenic 2.0 "270 """"Barium 0.99 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "86 """"Chromium 0.49 N-02 "25 """"Cobalt 0.49 "60 """"Copper 0.99 "190 """"Lead 0.49 N-02, N-03 "1.0 """"Molybdenum 0.49 "170 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "35 """"Vanadium 2.0 "380 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.34 B1D0916 05/03/21 13:23mg/L 2Chromium0.10 "13 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.29 B1D0919 05/03/21 14:41mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 32 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 17:34mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )89 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M93B1D076604/28/21 15:31mg/kg 4TPH Diesel (C13-C22)40 D-06 "320 """"TPH Motor Oil (C23-C40)200 """( 65 - 136 )84 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 33 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 33 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 20:30mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 34 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 34 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 20:30mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )87 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 35 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 35 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-09 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:16mg/kg B1D07111Mercury0.087 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP EPA 6010B38B1D073404/26/21 14:22mg/kg 1Antimony2.5 "13 """"Arsenic 2.0 "610 """"Barium 0.99 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "63 """"Chromium 0.49 N-02 "19 """"Cobalt 0.49 "78 """"Copper 0.99 "8000 "04/26/21 14:50"100Lead49 N-01, N-03 "1.8 "04/26/21 14:22"1Molybdenum0.49 "110 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "39 """"Vanadium 2.0 "2100 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.27 B1D0916 05/03/21 13:26mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.054 B1D0919 05/03/21 14:44mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 36 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 36 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 18:00mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )97 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M39B1D076604/27/21 16:32mg/kg 1TPH Diesel (C13-C22)10 D-06 "110 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )75 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 37 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 37 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 23:41mg/kg B1D06501Benzene0.052 ND """ ""Bromobenzene 0.052 ND """ ""Bromochloromethane 0.052 ND """ ""Bromodichloromethane 0.052 ND """ ""Bromoform 0.052 ND """ ""Bromomethane 0.052 ND """ ""n-Butylbenzene 0.052 ND """ ""sec-Butylbenzene 0.052 ND """ ""tert-Butylbenzene 0.052 ND """ ""Carbon tetrachloride 0.052 ND """ ""Chlorobenzene 0.052 ND """ ""Chloroethane 0.052 ND """ ""Chloroform 0.052 ND """ ""Chloromethane 0.052 ND """ ""2-Chlorotoluene 0.052 ND """ ""4-Chlorotoluene 0.052 ND """ ""Dibromochloromethane 0.052 ND """ ""1,2-Dibromo-3-chloropropane 0.052 ND """ ""1,2-Dibromoethane (EDB)0.052 ND """ ""Dibromomethane 0.052 ND """ ""1,2-Dichlorobenzene 0.052 ND """ ""1,3-Dichlorobenzene 0.052 ND """ ""1,4-Dichlorobenzene 0.052 ND """ ""Dichlorodifluoromethane 0.052 ND """ ""1,1-Dichloroethane 0.052 ND """ ""1,2-Dichloroethane 0.052 ND """ ""1,1-Dichloroethene 0.052 ND """ ""cis-1,2-Dichloroethene 0.052 ND """ ""trans-1,2-Dichloroethene 0.052 ND """ ""1,2-Dichloropropane 0.052 ND """ ""1,3-Dichloropropane 0.052 ND """ ""2,2-Dichloropropane 0.052 ND """ ""1,1-Dichloropropene 0.052 ND """ ""cis-1,3-Dichloropropene 0.052 ND """ ""trans-1,3-Dichloropropene 0.052 ND """ ""Ethylbenzene 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 38 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 38 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 23:41mg/kg B1D06501Hexachlorobutadiene0.052 ND """ ""4-Isopropyl Toluene 0.052 ND """ ""Isopropylbenzene 0.052 ND """ ""Methylene chloride 0.052 ND """ ""Naphthalene 0.052 ND """ ""n-Propylbenzene 0.052 ND """ ""Styrene 0.052 ND """ ""1,1,1,2-Tetrachloroethane 0.052 ND """ ""1,1,2,2-Tetrachloroethane 0.052 ND """ ""Tetrachloroethene (PCE)0.052 ND """ ""Toluene 0.052 ND """ ""1,2,3-Trichlorobenzene 0.052 ND """ ""1,2,4-Trichlorobenzene 0.052 ND """ ""1,1,1-Trichloroethane 0.052 ND """ ""1,1,2-Trichloroethane 0.052 ND """ ""Trichloroethene (TCE)0.052 ND """ ""Trichlorofluoromethane 0.052 ND """ ""1,2,3-Trichloropropane 0.052 ND """ ""1,2,4-Trimethylbenzene 0.052 ND """ ""1,3,5-Trimethylbenzene 0.052 ND """ ""Vinyl chloride 0.052 ND """ ""Xylenes (total)0.052 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )91 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 39 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 39 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-10 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.19 B1D0711 04/26/21 15:18mg/kg 1Mercury0.088 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:25mg/kg B1D07341Antimony2.5 "9.0 """"Arsenic 2.0 "380 """"Barium 1.0 ND """ ""Beryllium 0.50 "1.3 """"Cadmium 0.25 "44 """"Chromium 0.50 "13 """"Cobalt 0.50 "36 """"Copper 1.0 "360 """"Lead 0.50 N-02, N-03 "0.73 """"Molybdenum 0.50 "71 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "35 """"Vanadium 2.0 "780 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B12B1D091605/03/21 13:28mg/L 2Lead0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.092 B1D0919 05/03/21 14:46mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 40 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 40 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 18:26mg/kg B1D06921TPH Gasoline (C5-C12)4.6 R-07 """( 39 - 157 )98 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M21B1D076604/27/21 16:54mg/kg 1TPH Diesel (C13-C22)10 D-06 "140 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )80 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 41 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 41 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 00:08mg/kg B1D06501Benzene0.052 ND """ ""Bromobenzene 0.052 ND """ ""Bromochloromethane 0.052 ND """ ""Bromodichloromethane 0.052 ND """ ""Bromoform 0.052 ND """ ""Bromomethane 0.052 ND """ ""n-Butylbenzene 0.052 ND """ ""sec-Butylbenzene 0.052 ND """ ""tert-Butylbenzene 0.052 ND """ ""Carbon tetrachloride 0.052 ND """ ""Chlorobenzene 0.052 ND """ ""Chloroethane 0.052 ND """ ""Chloroform 0.052 ND """ ""Chloromethane 0.052 ND """ ""2-Chlorotoluene 0.052 ND """ ""4-Chlorotoluene 0.052 ND """ ""Dibromochloromethane 0.052 ND """ ""1,2-Dibromo-3-chloropropane 0.052 ND """ ""1,2-Dibromoethane (EDB)0.052 ND """ ""Dibromomethane 0.052 ND """ ""1,2-Dichlorobenzene 0.052 ND """ ""1,3-Dichlorobenzene 0.052 ND """ ""1,4-Dichlorobenzene 0.052 ND """ ""Dichlorodifluoromethane 0.052 ND """ ""1,1-Dichloroethane 0.052 ND """ ""1,2-Dichloroethane 0.052 ND """ ""1,1-Dichloroethene 0.052 ND """ ""cis-1,2-Dichloroethene 0.052 ND """ ""trans-1,2-Dichloroethene 0.052 ND """ ""1,2-Dichloropropane 0.052 ND """ ""1,3-Dichloropropane 0.052 ND """ ""2,2-Dichloropropane 0.052 ND """ ""1,1-Dichloropropene 0.052 ND """ ""cis-1,3-Dichloropropene 0.052 ND """ ""trans-1,3-Dichloropropene 0.052 ND """ ""Ethylbenzene 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 42 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 42 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 00:08mg/kg B1D06501Hexachlorobutadiene0.052 ND """ ""4-Isopropyl Toluene 0.052 ND """ ""Isopropylbenzene 0.052 ND """ ""Methylene chloride 0.052 ND """ ""Naphthalene 0.052 ND """ ""n-Propylbenzene 0.052 ND """ ""Styrene 0.052 ND """ ""1,1,1,2-Tetrachloroethane 0.052 ND """ ""1,1,2,2-Tetrachloroethane 0.052 ND """ ""Tetrachloroethene (PCE)0.052 ND """ ""Toluene 0.052 ND """ ""1,2,3-Trichlorobenzene 0.052 ND """ ""1,2,4-Trichlorobenzene 0.052 ND """ ""1,1,1-Trichloroethane 0.052 ND """ ""1,1,2-Trichloroethane 0.052 ND """ ""Trichloroethene (TCE)0.052 ND """ ""Trichlorofluoromethane 0.052 ND """ ""1,2,3-Trichloropropane 0.052 ND """ ""1,2,4-Trimethylbenzene 0.052 ND """ ""1,3,5-Trimethylbenzene 0.052 ND """ ""Vinyl chloride 0.052 ND """ ""Xylenes (total)0.052 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 43 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 43 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508- Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.11 B1D0711 04/26/21 15:20mg/kg 1Mercury0.099 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:28mg/kg B1D07341Antimony2.5 "15 """"Arsenic 2.0 "270 """"Barium 0.98 ND """ ""Beryllium 0.49 "1.4 """"Cadmium 0.25 "130 """"Chromium 0.49 N-02, N-03 "16 """"Cobalt 0.49 "68 """"Copper 0.98 "440 """"Lead 0.49 N-02, N-03 "1.2 """"Molybdenum 0.49 "120 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "38 """"Vanadium 2.0 "1400 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.23 B1D0916 05/03/21 13:31mg/L 2Chromium0.10 "14 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/03/21 14:49mg/L B1D09191Chromium0.050 "0.27 """"Lead 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 44 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 44 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 20:35mg/kg B1D06921TPH Gasoline (C5-C12)4.6 R-07 """( 39 - 157 )97 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M17B1D076604/27/21 16:54mg/kg 1TPH Diesel (C13-C22)10 D-06 "87 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )74 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 45 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 45 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 00:35mg/kg B1D06501Benzene0.045 ND """ ""Bromobenzene 0.045 ND """ ""Bromochloromethane 0.045 ND """ ""Bromodichloromethane 0.045 ND """ ""Bromoform 0.045 ND """ ""Bromomethane 0.045 ND """ ""n-Butylbenzene 0.045 ND """ ""sec-Butylbenzene 0.045 ND """ ""tert-Butylbenzene 0.045 ND """ ""Carbon tetrachloride 0.045 ND """ ""Chlorobenzene 0.045 ND """ ""Chloroethane 0.045 ND """ ""Chloroform 0.045 ND """ ""Chloromethane 0.045 ND """ ""2-Chlorotoluene 0.045 ND """ ""4-Chlorotoluene 0.045 ND """ ""Dibromochloromethane 0.045 ND """ ""1,2-Dibromo-3-chloropropane 0.045 ND """ ""1,2-Dibromoethane (EDB)0.045 ND """ ""Dibromomethane 0.045 ND """ ""1,2-Dichlorobenzene 0.045 ND """ ""1,3-Dichlorobenzene 0.045 ND """ ""1,4-Dichlorobenzene 0.045 ND """ ""Dichlorodifluoromethane 0.045 ND """ ""1,1-Dichloroethane 0.045 ND """ ""1,2-Dichloroethane 0.045 ND """ ""1,1-Dichloroethene 0.045 ND """ ""cis-1,2-Dichloroethene 0.045 ND """ ""trans-1,2-Dichloroethene 0.045 ND """ ""1,2-Dichloropropane 0.045 ND """ ""1,3-Dichloropropane 0.045 ND """ ""2,2-Dichloropropane 0.045 ND """ ""1,1-Dichloropropene 0.045 ND """ ""cis-1,3-Dichloropropene 0.045 ND """ ""trans-1,3-Dichloropropene 0.045 ND """ ""Ethylbenzene 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 46 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 46 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 00:35mg/kg B1D06501Hexachlorobutadiene0.045 ND """ ""4-Isopropyl Toluene 0.045 ND """ ""Isopropylbenzene 0.045 ND """ ""Methylene chloride 0.045 ND """ ""Naphthalene 0.045 ND """ ""n-Propylbenzene 0.045 ND """ ""Styrene 0.045 ND """ ""1,1,1,2-Tetrachloroethane 0.045 ND """ ""1,1,2,2-Tetrachloroethane 0.045 ND """ ""Tetrachloroethene (PCE)0.045 ND """ ""Toluene 0.045 ND """ ""1,2,3-Trichlorobenzene 0.045 ND """ ""1,2,4-Trichlorobenzene 0.045 ND """ ""1,1,1-Trichloroethane 0.045 ND """ ""1,1,2-Trichloroethane 0.045 ND """ ""Trichloroethene (TCE)0.045 ND """ ""Trichlorofluoromethane 0.045 ND """ ""1,2,3-Trichloropropane 0.045 ND """ ""1,2,4-Trimethylbenzene 0.045 ND """ ""1,3,5-Trimethylbenzene 0.045 ND """ ""Vinyl chloride 0.045 ND """ ""Xylenes (total)0.045 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 47 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 47 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-12 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:30mg/kg B1D07111Mercury0.096 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:31mg/kg B1D07341Antimony2.5 "13 """"Arsenic 2.0 "300 """"Barium 0.99 ND """ ""Beryllium 0.49 "19 """"Cadmium 0.25 N-02 "56 """"Chromium 0.49 N-02 "17 """"Cobalt 0.49 "1100 """"Copper 0.99 N-02 "390 """"Lead 0.49 N-02, N-03 "1.1 """"Molybdenum 0.49 "100 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "34 """"Vanadium 2.0 "660 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.088 B1D0916 05/03/21 13:34mg/L 2Cadmium0.050 "0.24 """"Chromium 0.10 "0.69 """"Copper 0.10 "10 """"Lead 0.10 N-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 48 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 48 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.085 B1D0919 05/03/21 14:59mg/L 1Lead0.050 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 21:01mg/kg B1D06921TPH Gasoline (C5-C12)4.8 R-07 """( 39 - 157 )96 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M20B1D076604/27/21 17:17mg/kg 1TPH Diesel (C13-C22)10 D-06 "130 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )78 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 49 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 49 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 01:02mg/kg B1D06501Benzene0.045 ND """ ""Bromobenzene 0.045 ND """ ""Bromochloromethane 0.045 ND """ ""Bromodichloromethane 0.045 ND """ ""Bromoform 0.045 ND """ ""Bromomethane 0.045 ND """ ""n-Butylbenzene 0.045 ND """ ""sec-Butylbenzene 0.045 ND """ ""tert-Butylbenzene 0.045 ND """ ""Carbon tetrachloride 0.045 ND """ ""Chlorobenzene 0.045 ND """ ""Chloroethane 0.045 ND """ ""Chloroform 0.045 ND """ ""Chloromethane 0.045 ND """ ""2-Chlorotoluene 0.045 ND """ ""4-Chlorotoluene 0.045 ND """ ""Dibromochloromethane 0.045 ND """ ""1,2-Dibromo-3-chloropropane 0.045 ND """ ""1,2-Dibromoethane (EDB)0.045 ND """ ""Dibromomethane 0.045 ND """ ""1,2-Dichlorobenzene 0.045 ND """ ""1,3-Dichlorobenzene 0.045 ND """ ""1,4-Dichlorobenzene 0.045 ND """ ""Dichlorodifluoromethane 0.045 ND """ ""1,1-Dichloroethane 0.045 ND """ ""1,2-Dichloroethane 0.045 ND """ ""1,1-Dichloroethene 0.045 ND """ ""cis-1,2-Dichloroethene 0.045 ND """ ""trans-1,2-Dichloroethene 0.045 ND """ ""1,2-Dichloropropane 0.045 ND """ ""1,3-Dichloropropane 0.045 ND """ ""2,2-Dichloropropane 0.045 ND """ ""1,1-Dichloropropene 0.045 ND """ ""cis-1,3-Dichloropropene 0.045 ND """ ""trans-1,3-Dichloropropene 0.045 ND """ ""Ethylbenzene 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 50 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 50 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 01:02mg/kg B1D06501Hexachlorobutadiene0.045 ND """ ""4-Isopropyl Toluene 0.045 ND """ ""Isopropylbenzene 0.045 ND """ ""Methylene chloride 0.045 ND """ ""Naphthalene 0.045 ND """ ""n-Propylbenzene 0.045 ND """ ""Styrene 0.045 ND """ ""1,1,1,2-Tetrachloroethane 0.045 ND """ ""1,1,2,2-Tetrachloroethane 0.045 ND """ ""Tetrachloroethene (PCE)0.045 ND """ ""Toluene 0.045 ND """ ""1,2,3-Trichlorobenzene 0.045 ND """ ""1,2,4-Trichlorobenzene 0.045 ND """ ""1,1,1-Trichloroethane 0.045 ND """ ""1,1,2-Trichloroethane 0.045 ND """ ""Trichloroethene (TCE)0.045 ND """ ""Trichlorofluoromethane 0.045 ND """ ""1,2,3-Trichloropropane 0.045 ND """ ""1,2,4-Trimethylbenzene 0.045 ND """ ""1,3,5-Trimethylbenzene 0.045 ND """ ""Vinyl chloride 0.045 ND """ ""Xylenes (total)0.045 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )98 %Surrogate: Toluene-d8 """( 75 - 121 )88 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 51 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 51 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-13 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:32mg/kg B1D07111Mercury0.091 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:41mg/kg B1D07341Antimony2.5 "7.0 """"Arsenic 2.0 "360 """"Barium 1.0 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "48 """"Chromium 0.50 "10 """"Cobalt 0.50 "620 """"Copper 1.0 N-02 "940 """"Lead 0.50 N-02, N-03 "1.4 """"Molybdenum 0.50 "66 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "34 """"Vanadium 2.0 "610 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B2.4 B1D0916 05/03/21 13:36mg/L 2Copper0.10 "51 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B4.7 B1D0919 05/03/21 15:01mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 52 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 52 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 21:27mg/kg B1D06921TPH Gasoline (C5-C12)5.2 R-07 """( 39 - 157 )92 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M12B1D076604/27/21 17:17mg/kg 1TPH Diesel (C13-C22)10 D-06 "67 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )73 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 53 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 53 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 01:29mg/kg B1D06501Benzene0.050 ND """ ""Bromobenzene 0.050 ND """ ""Bromochloromethane 0.050 ND """ ""Bromodichloromethane 0.050 ND """ ""Bromoform 0.050 ND """ ""Bromomethane 0.050 ND """ ""n-Butylbenzene 0.050 ND """ ""sec-Butylbenzene 0.050 ND """ ""tert-Butylbenzene 0.050 ND """ ""Carbon tetrachloride 0.050 ND """ ""Chlorobenzene 0.050 ND """ ""Chloroethane 0.050 ND """ ""Chloroform 0.050 ND """ ""Chloromethane 0.050 ND """ ""2-Chlorotoluene 0.050 ND """ ""4-Chlorotoluene 0.050 ND """ ""Dibromochloromethane 0.050 ND """ ""1,2-Dibromo-3-chloropropane 0.050 ND """ ""1,2-Dibromoethane (EDB)0.050 ND """ ""Dibromomethane 0.050 ND """ ""1,2-Dichlorobenzene 0.050 ND """ ""1,3-Dichlorobenzene 0.050 ND """ ""1,4-Dichlorobenzene 0.050 ND """ ""Dichlorodifluoromethane 0.050 ND """ ""1,1-Dichloroethane 0.050 ND """ ""1,2-Dichloroethane 0.050 ND """ ""1,1-Dichloroethene 0.050 ND """ ""cis-1,2-Dichloroethene 0.050 ND """ ""trans-1,2-Dichloroethene 0.050 ND """ ""1,2-Dichloropropane 0.050 ND """ ""1,3-Dichloropropane 0.050 ND """ ""2,2-Dichloropropane 0.050 ND """ ""1,1-Dichloropropene 0.050 ND """ ""cis-1,3-Dichloropropene 0.050 ND """ ""trans-1,3-Dichloropropene 0.050 ND """ ""Ethylbenzene 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 54 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 54 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 01:29mg/kg B1D06501Hexachlorobutadiene0.050 ND """ ""4-Isopropyl Toluene 0.050 ND """ ""Isopropylbenzene 0.050 ND """ ""Methylene chloride 0.050 ND """ ""Naphthalene 0.050 ND """ ""n-Propylbenzene 0.050 ND """ ""Styrene 0.050 ND """ ""1,1,1,2-Tetrachloroethane 0.050 ND """ ""1,1,2,2-Tetrachloroethane 0.050 ND """ ""Tetrachloroethene (PCE)0.050 ND """ ""Toluene 0.050 ND """ ""1,2,3-Trichlorobenzene 0.050 ND """ ""1,2,4-Trichlorobenzene 0.050 ND """ ""1,1,1-Trichloroethane 0.050 ND """ ""1,1,2-Trichloroethane 0.050 ND """ ""Trichloroethene (TCE)0.050 ND """ ""Trichlorofluoromethane 0.050 ND """ ""1,2,3-Trichloropropane 0.050 ND """ ""1,2,4-Trimethylbenzene 0.050 ND """ ""1,3,5-Trimethylbenzene 0.050 ND """ ""Vinyl chloride 0.050 ND """ ""Xylenes (total)0.050 """( 74 - 122 )96 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )89 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 55 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 55 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-14 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.20 B1D0711 04/26/21 15:34mg/kg 1Mercury0.097 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:44mg/kg B1D07341Antimony2.5 "6.7 """"Arsenic 2.0 "440 """"Barium 0.99 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "73 """"Chromium 0.50 N-02 "9.4 """"Cobalt 0.50 "57 """"Copper 0.99 "2000 """"Lead 0.50 N-01, N-03 "2.5 """"Molybdenum 0.50 "68 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 0.99 "30 """"Vanadium 2.0 "770 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.23 B1D0916 05/03/21 13:39mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.99 B1D0919 05/03/21 15:04mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 56 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 56 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 21:53mg/kg B1D06921TPH Gasoline (C5-C12)5.1 R-07 """( 39 - 157 )96 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/28/21 15:08mg/kg B1D07661TPH Diesel (C13-C22)10 "64 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )79 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 57 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 57 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 01:57mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 58 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 58 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 01:57mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )91 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 59 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 59 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-15 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:36mg/kg B1D07111Mercury0.094 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:47mg/kg B1D07341Antimony2.4 "5.6 """"Arsenic 1.9 "320 """"Barium 0.97 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "49 """"Chromium 0.48 "10 """"Cobalt 0.48 "41 """"Copper 0.97 "440 """"Lead 0.48 N-02, N-03 "0.80 """"Molybdenum 0.48 "68 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.97 "38 """"Vanadium 1.9 "580 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B40B1D091605/03/21 13:41mg/L 2Lead0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.20 B1D0919 05/03/21 15:06mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 60 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 60 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 22:18mg/kg B1D06921TPH Gasoline (C5-C12)4.6 R-07 """( 39 - 157 )94 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M140B1D076604/28/21 16:38mg/kg 2TPH Diesel (C13-C22)20 D-06 "360 """"TPH Motor Oil (C23-C40)100 """( 65 - 136 )120 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 61 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 61 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 02:24mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 62 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 62 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 02:24mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 63 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 63 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0711 - EPA 7471A Prep[TOC] Batch B1D0711 - EPA 7471A Preparation: EPA 7471A Prep 04/26/21 09:00 Blank (B1D0711-BLK1) [TOC_3]Blank (B1D0711-BLK1)[TOC] Analyzed: 04/26/21 14:37 Mercury mg/kgND0.10 LCS (B1D0711-BS1) [TOC_3]LCS (B1D0711-BS1)[TOC] Analyzed: 04/26/21 14:31 Mercury mg/kg0.803 0.10 0.833 85-11596 LCS Dup (B1D0711-BSD1) [TOC_3]LCS Dup (B1D0711-BSD1)[TOC] Analyzed: 04/26/21 14:33 Mercury mg/kg0.765 0.10 0.833 2085-11592 5 Duplicate (B1D0711-DUP1)Source: 2102489-02 [TOC_3]Duplicate (B1D0711-DUP1)[TOC] Analyzed: 04/26/21 14:45 Mercury mg/kg0.0432 0.099 0.0418 203 Matrix Spike (B1D0711-MS1)Source: 2102489-02 [TOC_3]Matrix Spike (B1D0711-MS1)[TOC] Analyzed: 04/26/21 14:47 Mercury mg/kg0.843 0.090 0.746 0.0418 75-125107 Matrix Spike Dup (B1D0711-MSD1)Source: 2102489-02 [TOC_3]Matrix Spike Dup (B1D0711-MSD1)[TOC] Analyzed: 04/26/21 14:49 Mercury mg/kg0.673 0.087 0.723 0.0418 20 QR-0275-12587 22 Post Spike (B1D0711-PS1)Source: 2102489-02 [TOC_3]Post Spike (B1D0711-PS1)[TOC] Analyzed: 04/26/21 14:51 Mercury ug/L5.23 5.00 0.273 85-11599 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 64 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 64 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0734 - EPA 3050B[TOC] Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Blank (B1D0734-BLK1) [TOC_3]Blank (B1D0734-BLK1)[TOC] Analyzed: 04/26/21 13:29 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1D0734-BS1) [TOC_3]LCS (B1D0734-BS1)[TOC] Analyzed: 04/26/21 13:04 Antimony mg/kg97.0 2.5 100 80-12097 Arsenic "100 2.0 100 80-120100 Barium "93.5 1.0 100 80-12094 Beryllium "99.0 0.50 100 80-12099 Cadmium "99.2 0.25 100 80-12099 Chromium "102 0.50 100 80-120102 Cobalt "100 0.50 100 80-120100 Copper "104 1.0 100 80-120104 Lead "99.4 0.50 100 80-12099 Molybdenum "98.4 0.50 100 80-12098 Nickel "102 0.50 100 80-120102 Selenium "101 2.0 100 80-120101 Silver "5.04 0.50 5.00 80-120101 Thallium "108 1.0 100 80-120108 Vanadium "99.8 2.0 100 80-120100 Zinc "97.0 2.0 100 80-12097 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 65 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 65 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 LCS Dup (B1D0734-BSD1) [TOC_3]LCS Dup (B1D0734-BSD1)[TOC] Analyzed: 04/26/21 13:06 Antimony mg/kg97.8 2.5 100 2080-12098 0.8 Arsenic "101 2.0 100 2080-120101 0.7 Barium "93.6 1.0 100 2080-12094 0.2 Beryllium "98.6 0.50 100 2080-12099 0.4 Cadmium "99.5 0.25 100 2080-120100 0.3 Chromium "103 0.50 100 2080-120103 0.8 Cobalt "101 0.50 100 2080-120101 0.3 Copper "104 1.0 100 2080-120104 0.8 Lead "99.8 0.50 100 2080-120100 0.3 Molybdenum "99.4 0.50 100 2080-12099 0.9 Nickel "102 0.50 100 2080-120102 0.4 Selenium "101 2.0 100 2080-120101 0.1 Silver "5.04 0.50 5.00 2080-120101 0.1 Thallium "108 1.0 100 2080-120108 0.5 Vanadium "100 2.0 100 2080-120100 0.4 Zinc "97.4 2.0 100 2080-12097 0.4 Duplicate (B1D0734-DUP1)Source: 2102489-01 [TOC_3]Duplicate (B1D0734-DUP1)[TOC] Analyzed: 04/26/21 13:35 Antimony mg/kgND2.5 ND 20 Arsenic "5.86 2.0 6.40 209 Barium "87.5 0.99 72.5 2019 Beryllium "0.369 0.49 0.419 2012 Cadmium "ND 0.25 ND 20 Chromium "20.3 0.49 22.2 209 Cobalt "6.53 0.49 6.95 206 Copper "18.4 0.99 21.5 2016 Lead "5.52 0.49 6.10 2010 Molybdenum "1.50 0.49 2.18 20 QR-0437 Nickel "25.9 0.49 30.4 2016 Selenium "ND 2.0 ND 20 Silver "ND 0.49 ND 20 Thallium "ND 0.99 ND 20 Vanadium "18.9 2.0 20.6 209 Zinc "49.7 2.0 53.8 208 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 66 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 66 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Matrix Spike (B1D0734-MS1)Source: 2102489-01 [TOC_3]Matrix Spike (B1D0734-MS1)[TOC] Analyzed: 04/26/21 13:08 Antimony mg/kg30.5 2.5 98.3 ND 10-11631 Arsenic "102 2.0 98.3 6.40 77-12197 Barium "159 0.98 98.3 72.5 30-16988 Beryllium "93.2 0.49 98.3 0.419 86-11194 Cadmium "90.1 0.25 98.3 ND 81-11292 Chromium "124 0.49 98.3 22.2 75-129103 Cobalt "98.3 0.49 98.3 6.95 71-12193 Copper "123 0.98 98.3 21.5 68-135103 Lead "95.5 0.49 98.3 6.10 72-12191 Molybdenum "87.8 0.49 98.3 2.18 70-11287 Nickel "122 0.49 98.3 30.4 73-12193 Selenium "91.6 2.0 98.3 ND 76-11693 Silver "4.59 0.49 4.92 ND 54-13293 Thallium "94.7 0.98 98.3 ND 64-12096 Vanadium "117 2.0 98.3 20.6 78-12498 Zinc "142 2.0 98.3 53.8 50-14389 Matrix Spike Dup (B1D0734-MSD1)Source: 2102489-01 [TOC_3]Matrix Spike Dup (B1D0734-MSD1)[TOC] Analyzed: 04/26/21 13:11 Antimony mg/kg28.7 2.4 97.7 ND 2010-11629 6 Arsenic "99.5 2.0 97.7 6.40 2077-12195 2 Barium "173 0.98 97.7 72.5 2030-169103 9 Beryllium "90.5 0.49 97.7 0.419 2086-11192 3 Cadmium "86.7 0.24 97.7 ND 2081-11289 4 Chromium "120 0.49 97.7 22.2 2075-129100 3 Cobalt "95.5 0.49 97.7 6.95 2071-12191 3 Copper "120 0.98 97.7 21.5 2068-135101 3 Lead "92.4 0.49 97.7 6.10 2072-12188 3 Molybdenum "85.4 0.49 97.7 2.18 2070-11285 3 Nickel "121 0.49 97.7 30.4 2073-12192 1 Selenium "87.5 2.0 97.7 ND 2076-11690 5 Silver "4.44 0.49 4.88 ND 2054-13291 3 Thallium "90.3 0.98 97.7 ND 2064-12092 5 Vanadium "115 2.0 97.7 20.6 2078-12496 2 Zinc "141 2.0 97.7 53.8 2050-14389 0.6 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 67 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 67 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Post Spike (B1D0734-PS1)Source: 2102489-01 [TOC_3]Post Spike (B1D0734-PS1)[TOC] Analyzed: 04/26/21 13:14 Antimony mg/L1.85 2.00 -0.00714 75-12593 Arsenic "2.15 2.00 0.129 75-125101 Barium "3.34 2.00 1.46 75-12594 Beryllium "1.96 2.00 0.00843 75-12597 Cadmium "1.88 2.00 -0.0200 75-12594 Chromium "2.46 2.00 0.448 75-125100 Cobalt "2.05 2.00 0.140 75-12596 Copper "2.56 2.00 0.433 75-125106 Lead "2.01 2.00 0.123 75-12594 Molybdenum "1.97 2.00 0.0438 75-12596 Nickel "2.55 2.00 0.613 75-12597 Selenium "1.96 2.00 -0.0375 75-12598 Silver "0.0965 0.100 -0.00476 75-12596 Thallium "1.98 2.00 -0.0435 75-12599 Vanadium "2.41 2.00 0.416 75-125100 Zinc "2.96 2.00 1.08 75-12594 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 68 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 68 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: STLC Metals by ICP - Quality Control[TOC_1]STLC Metals by IC Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0916 - EPA 3010A Leachate[TOC] Batch B1D0916 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:33 Blank (B1D0916-BLK1) [TOC_3]Blank (B1D0916-BLK1)[TOC] Analyzed: 05/03/21 12:22 Cadmium mg/LND0.025 Chromium "ND 0.050 Copper "ND 0.050 Lead "ND 0.050 LCS (B1D0916-BS1) [TOC_3]LCS (B1D0916-BS1)[TOC] Analyzed: 05/03/21 12:35 Cadmium mg/L9.62 0.025 10.0 80-12096 Chromium "9.56 0.050 10.0 80-12096 Copper "9.66 0.050 10.0 80-12097 Lead "9.70 0.050 10.0 80-12097 LCS Dup (B1D0916-BSD1) [TOC_3]LCS Dup (B1D0916-BSD1)[TOC] Analyzed: 05/03/21 12:37 Cadmium mg/L9.68 0.025 10.0 2080-12097 0.6 Chromium "9.59 0.050 10.0 2080-12096 0.3 Copper "9.70 0.050 10.0 2080-12097 0.4 Lead "9.78 0.050 10.0 2080-12098 0.9 Duplicate (B1D0916-DUP1)Source: 2102467-01 [TOC_3]Duplicate (B1D0916-DUP1)[TOC] Analyzed: 05/03/21 12:53 Cadmium mg/LND0.050 ND 20 Chromium "0.0860 0.10 0.111 20 QR-0425 Copper "1.53 0.10 1.76 2014 Lead "0.773 0.10 0.930 2018 Leach Fluid Blank (B1D0916-LBK1) [TOC_3]Leach Fluid Blank (B1D0916-LBK1)[TOC] Analyzed: 05/03/21 12:25 Cadmium mg/LND0.050 Chromium "ND 0.10 Copper "ND 0.10 Lead "ND 0.10 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 69 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 69 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: TCLP Metals by ICP - Quality Control[TOC_1]TCL Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0919 - EPA 3010A Leachate[TOC] Batch B1D0919 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:49 Blank (B1D0919-BLK1) [TOC_3]Blank (B1D0919-BLK1)[TOC] Analyzed: 05/03/21 13:54 Chromium mg/LND0.050 Lead "ND 0.050 LCS (B1D0919-BS1) [TOC_3]LCS (B1D0919-BS1)[TOC] Analyzed: 05/03/21 14:02 Chromium mg/L9.42 0.050 10.0 80-12094 Lead "9.97 0.050 10.0 80-120100 LCS Dup (B1D0919-BSD1) [TOC_3]LCS Dup (B1D0919-BSD1)[TOC] Analyzed: 05/03/21 14:04 Chromium mg/L9.35 0.050 10.0 2080-12094 0.7 Lead "9.82 0.050 10.0 2080-12098 2 Duplicate (B1D0919-DUP1)Source: 2102508-01 [TOC_3]Duplicate (B1D0919-DUP1)[TOC] Analyzed: 05/03/21 14:11 Chromium mg/LND0.050 ND 20 Lead "1.60 0.050 2.02 20 QR-0424 Leach Fluid Blank (B1D0919-LBK1) [TOC_3]Leach Fluid Blank (B1D0919-LBK1)[TOC] Analyzed: 05/03/21 13:57 Chromium mg/LND0.050 Lead "ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 70 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 70 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0692 - EPA 5035/5030B Solid GC[TOC] Batch B1D0692 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 04/23/21 08:32 Blank (B1D0692-BLK1) [TOC_3]Blank (B1D0692-BLK1)[TOC] Analyzed: 04/23/21 10:26 TPH Gasoline (C5-C12)mg/kgND0.50 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1030.128 LCS (B1D0692-BS1) [TOC_3]LCS (B1D0692-BS1)[TOC] Analyzed: 04/23/21 09:34 TPH Gasoline (C5-C12)mg/kg1.07 0.50 1.00 68-139107 "0.126 39-157Surrogate: 4-Bromofluorobenzene 1160.146 LCS Dup (B1D0692-BSD1) [TOC_3]LCS Dup (B1D0692-BSD1)[TOC] Analyzed: 04/23/21 10:00 TPH Gasoline (C5-C12)mg/kg1.05 0.49 0.988 2068-139106 2 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1210.150 Duplicate (B1D0692-DUP1)Source: 2102433-01RE1 [TOC_3]Duplicate (B1D0692-DUP1)[TOC] Analyzed: 04/23/21 22:44 TPH Gasoline (C5-C12)mg/kgND4.8 ND 20 "1.20 39-157Surrogate: 4-Bromofluorobenzene 981.18 Matrix Spike (B1D0692-MS1)Source: 2102433-01RE1 [TOC_3]Matrix Spike (B1D0692-MS1)[TOC] Analyzed: 04/23/21 23:10 TPH Gasoline (C5-C12)mg/kg8.79 4.9 9.80 ND 10-17190 "1.23 39-157Surrogate: 4-Bromofluorobenzene 1091.34 Matrix Spike Dup (B1D0692-MSD1)Source: 2102433-01RE1 [TOC_3]Matrix Spike Dup (B1D0692-MSD1)[TOC] Analyzed: 04/23/21 23:36 TPH Gasoline (C5-C12)mg/kg8.26 4.4 8.77 ND 2010-17194 6 "1.10 39-157Surrogate: 4-Bromofluorobenzene 1181.29 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 71 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 71 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0766 - EPA 3550C[TOC] Batch B1D0766 - EPA 8015M Preparation: EPA 3550C 04/27/21 07:10 Blank (B1D0766-BLK1) [TOC_3]Blank (B1D0766-BLK1)[TOC] Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "49.8 65-136Surrogate: o-Terphenyl 8441.9 LCS (B1D0766-BS1) [TOC_3]LCS (B1D0766-BS1)[TOC] Analyzed: 04/27/21 13:53 TPH Diesel (C13-C22)mg/kg42010 499 72-11584 TPH Motor Oil (C23-C40)"404 50 499 74-12681 "49.9 65-136Surrogate: o-Terphenyl 8643.0 LCS Dup (B1D0766-BSD1) [TOC_3]LCS Dup (B1D0766-BSD1)[TOC] Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22)mg/kg42010 500 2072-11584 0.2 TPH Motor Oil (C23-C40)"402 50 500 2074-12680 0.5 "50.0 65-136Surrogate: o-Terphenyl 8542.3 Duplicate (B1D0766-DUP1)Source: 2102489-01 [TOC_3]Duplicate (B1D0766-DUP1)[TOC] Analyzed: 04/27/21 15:02 TPH Diesel (C13-C22)mg/kgND9.9 ND 20 TPH Motor Oil (C23-C40)"ND 50 ND 20 "49.6 65-136Surrogate: o-Terphenyl 7838.9 Matrix Spike (B1D0766-MS1)Source: 2102489-01 [TOC_3]Matrix Spike (B1D0766-MS1)[TOC] Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22)mg/kg4309.9 497 ND 46-14786 TPH Motor Oil (C23-C40)"418 50 497 ND 35-17184 "49.7 65-136Surrogate: o-Terphenyl 8140.2 Matrix Spike Dup (B1D0766-MSD1)Source: 2102489-01 [TOC_3]Matrix Spike Dup (B1D0766-MSD1)[TOC] Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22)mg/kg48010 499 ND 2046-14796 11 TPH Motor Oil (C23-C40)"429 50 499 ND 2035-17186 3 "49.9 65-136Surrogate: o-Terphenyl 8944.5 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 72 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 72 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0650 - EPA 5035/5030B MEOH[TOC] Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (B1D0650-BLK1) [TOC_3]Blank (B1D0650-BLK1)[TOC] Analyzed: 04/23/21 16:50 Benzene mg/kgND0.0050 Bromobenzene "ND 0.0050 Bromochloromethane "ND 0.0050 Bromodichloromethane "ND 0.0050 Bromoform "ND 0.0050 Bromomethane "ND 0.0050 n-Butylbenzene "ND 0.0050 sec-Butylbenzene "ND 0.0050 tert-Butylbenzene "ND 0.0050 Carbon tetrachloride "ND 0.0050 Chlorobenzene "ND 0.0050 Chloroethane "ND 0.0050 Chloroform "ND 0.0050 Chloromethane "ND 0.0050 2-Chlorotoluene "ND 0.0050 4-Chlorotoluene "ND 0.0050 Dibromochloromethane "ND 0.0050 1,2-Dibromo-3-chloropropane "ND 0.0050 1,2-Dibromoethane (EDB)"ND 0.0050 Dibromomethane "ND 0.0050 1,2-Dichlorobenzene "ND 0.0050 1,3-Dichlorobenzene "ND 0.0050 1,4-Dichlorobenzene "ND 0.0050 Dichlorodifluoromethane "ND 0.0050 1,1-Dichloroethane "ND 0.0050 1,2-Dichloroethane "ND 0.0050 1,1-Dichloroethene "ND 0.0050 cis-1,2-Dichloroethene "ND 0.0050 trans-1,2-Dichloroethene "ND 0.0050 1,2-Dichloropropane "ND 0.0050 1,3-Dichloropropane "ND 0.0050 2,2-Dichloropropane "ND 0.0050 1,1-Dichloropropene "ND 0.0050 cis-1,3-Dichloropropene "ND 0.0050 trans-1,3-Dichloropropene "ND 0.0050 Ethylbenzene "ND 0.0050 Hexachlorobutadiene "ND 0.0050 4-Isopropyl Toluene "ND 0.0050 Isopropylbenzene "ND 0.0050 Methylene chloride "ND 0.0050 Naphthalene "ND 0.0050 n-Propylbenzene "ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 73 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 73 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (B1D0650-BLK1)Analyzed: 04/23/21 16:50 Styrene mg/kgND0.0050 1,1,1,2-Tetrachloroethane "ND 0.0050 1,1,2,2-Tetrachloroethane "ND 0.0050 Tetrachloroethene (PCE)"ND 0.0050 Toluene "ND 0.0050 1,2,3-Trichlorobenzene "ND 0.0050 1,2,4-Trichlorobenzene "ND 0.0050 1,1,1-Trichloroethane "ND 0.0050 1,1,2-Trichloroethane "ND 0.0050 Trichloroethene (TCE)"ND 0.0050 Trichlorofluoromethane "ND 0.0050 1,2,3-Trichloropropane "ND 0.0050 1,2,4-Trimethylbenzene "ND 0.0050 1,3,5-Trimethylbenzene "ND 0.0050 Vinyl chloride "ND 0.0050 Xylenes (total)"ND 0.0050 "0.0498 74-122Surrogate: Dibromofluoromethane 970.0484 "0.0498 65-128Surrogate: Toluene-d8 960.0479 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 910.0453 LCS (B1D0650-BS1) [TOC_3]LCS (B1D0650-BS1)[TOC] Analyzed: 04/23/21 14:31 Benzene mg/kg0.0389 0.0050 0.0396 70-13198 Bromobenzene "0.0369 0.0050 0.0396 74-13093 Bromochloromethane "0.0351 0.0050 0.0396 64-13389 Bromodichloromethane "0.0368 0.0050 0.0396 69-13793 Bromoform "0.0337 0.0050 0.0396 55-13285 Bromomethane "0.0397 0.0050 0.0396 10-142100 n-Butylbenzene "0.0440 0.0050 0.0396 64-156111 sec-Butylbenzene "0.0465 0.0050 0.0396 75-155117 tert-Butylbenzene "0.0438 0.0050 0.0396 74-144110 Carbon tetrachloride "0.0396 0.0050 0.0396 67-135100 Chlorobenzene "0.0399 0.0050 0.0396 73-134101 Chloroethane "0.0366 0.0050 0.0396 10-16792 Chloroform "0.0371 0.0050 0.0396 69-12494 Chloromethane "0.0286 0.0050 0.0396 34-13672 2-Chlorotoluene "0.0421 0.0050 0.0396 75-135106 4-Chlorotoluene "0.0420 0.0050 0.0396 70-138106 Dibromochloromethane "0.0370 0.0050 0.0396 67-13593 1,2-Dibromo-3-chloropropane "0.0368 0.0050 0.0396 41-14993 1,2-Dibromoethane (EDB)"0.0365 0.0050 0.0396 68-13192 Dibromomethane "0.0322 0.0050 0.0396 61-14081 1,2-Dichlorobenzene "0.0409 0.0050 0.0396 76-136103 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 74 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 74 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS (B1D0650-BS1)Analyzed: 04/23/21 14:31 1,3-Dichlorobenzene mg/kg0.0427 0.0050 0.0396 76-138108 1,4-Dichlorobenzene "0.0410 0.0050 0.0396 72-132104 Dichlorodifluoromethane "0.0196 0.0050 0.0396 10-15550 1,1-Dichloroethane "0.0399 0.0050 0.0396 63-139101 1,2-Dichloroethane "0.0359 0.0050 0.0396 64-12691 1,1-Dichloroethene "0.0435 0.0050 0.0396 52-167110 cis-1,2-Dichloroethene "0.0380 0.0050 0.0396 70-13596 trans-1,2-Dichloroethene "0.0421 0.0050 0.0396 67-147106 1,2-Dichloropropane "0.0368 0.0050 0.0396 68-13193 1,3-Dichloropropane "0.0359 0.0050 0.0396 64-12891 2,2-Dichloropropane "0.0404 0.0050 0.0396 63-154102 1,1-Dichloropropene "0.0386 0.0050 0.0396 68-13897 cis-1,3-Dichloropropene "0.0376 0.0050 0.0396 72-13495 trans-1,3-Dichloropropene "0.0385 0.0050 0.0396 69-13297 Ethylbenzene "0.0404 0.0050 0.0396 68-136102 Hexachlorobutadiene "0.0446 0.0050 0.0396 72-198113 4-Isopropyl Toluene "0.0439 0.0050 0.0396 74-150111 Isopropylbenzene "0.0429 0.0050 0.0396 71-149108 Methylene chloride "0.0402 0.0050 0.0396 51-127102 Naphthalene "0.0436 0.0050 0.0396 57-158110 n-Propylbenzene "0.0435 0.0050 0.0396 70-143110 Styrene "0.0412 0.0050 0.0396 68-138104 1,1,1,2-Tetrachloroethane "0.0373 0.0050 0.0396 76-13094 1,1,2,2-Tetrachloroethane "0.0407 0.0050 0.0396 60-136103 Tetrachloroethene (PCE)"0.0381 0.0050 0.0396 73-13896 Toluene "0.0371 0.0050 0.0396 72-12894 1,2,3-Trichlorobenzene "0.0390 0.0050 0.0396 61-16698 1,2,4-Trichlorobenzene "0.0406 0.0050 0.0396 71-158103 1,1,1-Trichloroethane "0.0389 0.0050 0.0396 71-13598 1,1,2-Trichloroethane "0.0341 0.0050 0.0396 64-13286 Trichloroethene (TCE)"0.0374 0.0050 0.0396 74-13994 Trichlorofluoromethane "0.0379 0.0050 0.0396 30-15696 1,2,3-Trichloropropane "0.0383 0.0050 0.0396 67-12397 1,2,4-Trimethylbenzene "0.0419 0.0050 0.0396 68-134106 1,3,5-Trimethylbenzene "0.0440 0.0050 0.0396 71-140111 Vinyl chloride "0.0352 0.0050 0.0396 43-14489 Xylenes (total)"0.122 0.0050 0.119 69-138102 "0.0495 74-122Surrogate: Dibromofluoromethane 990.0490 "0.0495 65-128Surrogate: Toluene-d8 960.0475 "0.0495 75-121Surrogate: 4-Bromofluorobenzene 960.0476 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 75 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 75 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (B1D0650-BSD1) [TOC_3]LCS Dup (B1D0650-BSD1)[TOC] Analyzed: 04/23/21 14:59 Benzene mg/kg0.0417 0.0050 0.0398 2070-131105 7 Bromobenzene "0.0394 0.0050 0.0398 2074-13099 6 Bromochloromethane "0.0377 0.0050 0.0398 2064-13395 7 Bromodichloromethane "0.0392 0.0050 0.0398 2069-13798 6 Bromoform "0.0363 0.0050 0.0398 2055-13291 8 Bromomethane "0.0416 0.0050 0.0398 2010-142105 5 n-Butylbenzene "0.0475 0.0050 0.0398 2064-156120 8 sec-Butylbenzene "0.0493 0.0050 0.0398 2075-155124 6 tert-Butylbenzene "0.0464 0.0050 0.0398 2074-144117 6 Carbon tetrachloride "0.0418 0.0050 0.0398 2067-135105 5 Chlorobenzene "0.0420 0.0050 0.0398 2073-134106 5 Chloroethane "0.0394 0.0050 0.0398 2010-16799 7 Chloroform "0.0392 0.0050 0.0398 2069-12499 5 Chloromethane "0.0302 0.0050 0.0398 2034-13676 5 2-Chlorotoluene "0.0435 0.0050 0.0398 2075-135109 3 4-Chlorotoluene "0.0431 0.0050 0.0398 2070-138108 3 Dibromochloromethane "0.0397 0.0050 0.0398 2067-135100 7 1,2-Dibromo-3-chloropropane "0.0410 0.0050 0.0398 2041-149103 11 1,2-Dibromoethane (EDB)"0.0388 0.0050 0.0398 2068-13198 6 Dibromomethane "0.0334 0.0050 0.0398 2061-14084 4 1,2-Dichlorobenzene "0.0429 0.0050 0.0398 2076-136108 5 1,3-Dichlorobenzene "0.0444 0.0050 0.0398 2076-138112 4 1,4-Dichlorobenzene "0.0436 0.0050 0.0398 2072-132110 6 Dichlorodifluoromethane "0.0206 0.0050 0.0398 2010-15552 5 1,1-Dichloroethane "0.0424 0.0050 0.0398 2063-139107 6 1,2-Dichloroethane "0.0395 0.0050 0.0398 2064-12699 10 1,1-Dichloroethene "0.0446 0.0050 0.0398 2052-167112 2 cis-1,2-Dichloroethene "0.0413 0.0050 0.0398 2070-135104 8 trans-1,2-Dichloroethene "0.0447 0.0050 0.0398 2067-147112 6 1,2-Dichloropropane "0.0401 0.0050 0.0398 2068-131101 9 1,3-Dichloropropane "0.0383 0.0050 0.0398 2064-12896 6 2,2-Dichloropropane "0.0436 0.0050 0.0398 2063-154110 8 1,1-Dichloropropene "0.0416 0.0050 0.0398 2068-138105 8 cis-1,3-Dichloropropene "0.0407 0.0050 0.0398 2072-134102 8 trans-1,3-Dichloropropene "0.0414 0.0050 0.0398 2069-132104 7 Ethylbenzene "0.0422 0.0050 0.0398 2068-136106 4 Hexachlorobutadiene "0.0478 0.0050 0.0398 2072-198120 7 4-Isopropyl Toluene "0.0465 0.0050 0.0398 2074-150117 6 Isopropylbenzene "0.0461 0.0050 0.0398 2071-149116 7 Methylene chloride "0.0427 0.0050 0.0398 2051-127108 6 Naphthalene "0.0454 0.0050 0.0398 2057-158114 4 n-Propylbenzene "0.0460 0.0050 0.0398 2070-143116 6 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 76 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 76 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (B1D0650-BSD1)Analyzed: 04/23/21 14:59 Styrene mg/kg0.0437 0.0050 0.0398 2068-138110 6 1,1,1,2-Tetrachloroethane "0.0395 0.0050 0.0398 2076-13099 6 1,1,2,2-Tetrachloroethane "0.0415 0.0050 0.0398 2060-136104 2 Tetrachloroethene (PCE)"0.0400 0.0050 0.0398 2073-138100 5 Toluene "0.0399 0.0050 0.0398 2072-128100 7 1,2,3-Trichlorobenzene "0.0432 0.0050 0.0398 2061-166109 10 1,2,4-Trichlorobenzene "0.0439 0.0050 0.0398 2071-158110 8 1,1,1-Trichloroethane "0.0415 0.0050 0.0398 2071-135104 6 1,1,2-Trichloroethane "0.0377 0.0050 0.0398 2064-13295 10 Trichloroethene (TCE)"0.0396 0.0050 0.0398 2074-13999 6 Trichlorofluoromethane "0.0412 0.0050 0.0398 2030-156104 9 1,2,3-Trichloropropane "0.0381 0.0050 0.0398 2067-12396 0.6 1,2,4-Trimethylbenzene "0.0448 0.0050 0.0398 2068-134113 7 1,3,5-Trimethylbenzene "0.0461 0.0050 0.0398 2071-140116 5 Vinyl chloride "0.0371 0.0050 0.0398 2043-14493 5 Xylenes (total)"0.128 0.0050 0.119 2069-138108 5 "0.0497 74-122Surrogate: Dibromofluoromethane 1010.0504 "0.0497 65-128Surrogate: Toluene-d8 960.0476 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 960.0475 Duplicate (B1D0650-DUP1)Source: 2102489-01 [TOC_3]Duplicate (B1D0650-DUP1)[TOC] Analyzed: 04/24/21 03:18 Benzene mg/kgND0.0050 ND 20 Bromobenzene "ND 0.0050 ND 20 Bromochloromethane "ND 0.0050 ND 20 Bromodichloromethane "ND 0.0050 ND 20 Bromoform "ND 0.0050 ND 20 Bromomethane "ND 0.0050 ND 20 n-Butylbenzene "ND 0.0050 ND 20 sec-Butylbenzene "ND 0.0050 ND 20 tert-Butylbenzene "ND 0.0050 ND 20 Carbon tetrachloride "ND 0.0050 ND 20 Chlorobenzene "ND 0.0050 ND 20 Chloroethane "ND 0.0050 ND 20 Chloroform "ND 0.0050 ND 20 Chloromethane "ND 0.0050 ND 20 2-Chlorotoluene "ND 0.0050 ND 20 4-Chlorotoluene "ND 0.0050 ND 20 Dibromochloromethane "ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane "ND 0.0050 ND 20 1,2-Dibromoethane (EDB)"ND 0.0050 ND 20 Dibromomethane "ND 0.0050 ND 20 1,2-Dichlorobenzene "ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 77 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 77 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Duplicate (B1D0650-DUP1)Source: 2102489-01 Analyzed: 04/24/21 03:18 1,3-Dichlorobenzene mg/kgND0.0050 ND 20 1,4-Dichlorobenzene "ND 0.0050 ND 20 Dichlorodifluoromethane "ND 0.0050 ND 20 1,1-Dichloroethane "ND 0.0050 ND 20 1,2-Dichloroethane "ND 0.0050 ND 20 1,1-Dichloroethene "ND 0.0050 ND 20 cis-1,2-Dichloroethene "ND 0.0050 ND 20 trans-1,2-Dichloroethene "ND 0.0050 ND 20 1,2-Dichloropropane "ND 0.0050 ND 20 1,3-Dichloropropane "ND 0.0050 ND 20 2,2-Dichloropropane "ND 0.0050 ND 20 1,1-Dichloropropene "ND 0.0050 ND 20 cis-1,3-Dichloropropene "ND 0.0050 ND 20 trans-1,3-Dichloropropene "ND 0.0050 ND 20 Ethylbenzene "ND 0.0050 ND 20 Hexachlorobutadiene "ND 0.0050 ND 20 4-Isopropyl Toluene "ND 0.0050 ND 20 Isopropylbenzene "ND 0.0050 ND 20 Methylene chloride "ND 0.0050 ND 20 Naphthalene "ND 0.0050 ND 20 n-Propylbenzene "ND 0.0050 ND 20 Styrene "ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane "ND 0.0050 ND 20 1,1,2,2-Tetrachloroethane "ND 0.0050 ND 20 Tetrachloroethene (PCE)"ND 0.0050 ND 20 Toluene "ND 0.0050 ND 20 1,2,3-Trichlorobenzene "ND 0.0050 ND 20 1,2,4-Trichlorobenzene "ND 0.0050 ND 20 1,1,1-Trichloroethane "ND 0.0050 ND 20 1,1,2-Trichloroethane "ND 0.0050 ND 20 Trichloroethene (TCE)"ND 0.0050 ND 20 Trichlorofluoromethane "ND 0.0050 ND 20 1,2,3-Trichloropropane "ND 0.0050 ND 20 1,2,4-Trimethylbenzene "ND 0.0050 ND 20 1,3,5-Trimethylbenzene "ND 0.0050 ND 20 Vinyl chloride "ND 0.0050 ND 20 Xylenes (total)"ND 0.0050 ND 20 "0.0496 74-122Surrogate: Dibromofluoromethane 970.0479 "0.0496 65-128Surrogate: Toluene-d8 980.0485 "0.0496 75-121Surrogate: 4-Bromofluorobenzene 910.0452 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 78 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 78 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (B1D0650-MS1)Source: 2102489-02 [TOC_3]Matrix Spike (B1D0650-MS1)[TOC] Analyzed: 04/24/21 04:12 Benzene mg/kg0.0404 0.0050 0.0402 ND 37-145101 Bromobenzene "0.0359 0.0050 0.0402 ND 29-14789 Bromochloromethane "0.0367 0.0050 0.0402 ND 40-14591 Bromodichloromethane "0.0384 0.0050 0.0402 ND 39-15396 Bromoform "0.0332 0.0050 0.0402 ND 32-14383 Bromomethane "0.0467 0.0050 0.0402 ND 10-141116 n-Butylbenzene "0.0324 0.0050 0.0402 ND 10-16281 sec-Butylbenzene "0.0408 0.0050 0.0402 ND 14-168102 tert-Butylbenzene "0.0388 0.0050 0.0402 ND 21-15997 Carbon tetrachloride "0.0380 0.0050 0.0402 ND 28-14895 Chlorobenzene "0.0384 0.0050 0.0402 ND 32-14896 Chloroethane "0.0502 0.0050 0.0402 ND 11-166125 Chloroform "0.0400 0.0050 0.0402 ND 40-139100 Chloromethane "0.0350 0.0050 0.0402 ND 18-13587 2-Chlorotoluene "0.0362 0.0050 0.0402 ND 25-15190 4-Chlorotoluene "0.0363 0.0050 0.0402 ND 22-15090 Dibromochloromethane "0.0359 0.0050 0.0402 ND 40-14789 1,2-Dibromo-3-chloropropane "0.0390 0.0050 0.0402 ND 25-15897 1,2-Dibromoethane (EDB)"0.0369 0.0050 0.0402 ND 38-14792 Dibromomethane "0.0319 0.0050 0.0402 ND 39-15079 1,2-Dichlorobenzene "0.0362 0.0050 0.0402 ND 24-15490 1,3-Dichlorobenzene "0.0369 0.0050 0.0402 ND 21-15392 1,4-Dichlorobenzene "0.0362 0.0050 0.0402 ND 21-14690 Dichlorodifluoromethane "0.0188 0.0050 0.0402 ND 10-14947 1,1-Dichloroethane "0.0420 0.0050 0.0402 ND 34-151105 1,2-Dichloroethane "0.0400 0.0050 0.0402 ND 40-137100 1,1-Dichloroethene "0.0449 0.0050 0.0402 ND 21-172112 cis-1,2-Dichloroethene "0.0385 0.0050 0.0402 ND 38-14796 trans-1,2-Dichloroethene "0.0409 0.0050 0.0402 ND 30-160102 1,2-Dichloropropane "0.0397 0.0050 0.0402 ND 39-14699 1,3-Dichloropropane "0.0396 0.0050 0.0402 ND 39-14199 2,2-Dichloropropane "0.0280 0.0050 0.0402 ND 26-14970 1,1-Dichloropropene "0.0385 0.0050 0.0402 ND 28-15096 cis-1,3-Dichloropropene "0.0371 0.0050 0.0402 ND 34-14992 trans-1,3-Dichloropropene "0.0384 0.0050 0.0402 ND 36-14396 Ethylbenzene "0.0397 0.0050 0.0402 0.00290 23-15092 Hexachlorobutadiene "0.0313 0.0050 0.0402 ND 10-19278 4-Isopropyl Toluene "0.0385 0.0050 0.0402 0.00290 11-16589 Isopropylbenzene "0.0406 0.0050 0.0402 0.00202 17-16696 Methylene chloride "0.0456 0.0050 0.0402 ND 28-135114 Naphthalene "0.0441 0.0050 0.0402 0.00948 10-17486 n-Propylbenzene "0.0393 0.0050 0.0402 0.00310 16-15690 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 79 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 79 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (B1D0650-MS1)Source: 2102489-02 Analyzed: 04/24/21 04:12 Styrene mg/kg0.0387 0.0050 0.0402 ND 24-15496 1,1,1,2-Tetrachloroethane "0.0367 0.0050 0.0402 ND 38-14991 1,1,2,2-Tetrachloroethane "0.0387 0.0050 0.0402 ND 22-16496 Tetrachloroethene (PCE)"0.0349 0.0050 0.0402 ND 25-15387 Toluene "0.0376 0.0050 0.0402 ND 26-14994 1,2,3-Trichlorobenzene "0.0323 0.0050 0.0402 ND 10-16380 1,2,4-Trichlorobenzene "0.0323 0.0050 0.0402 ND 10-16281 1,1,1-Trichloroethane "0.0387 0.0050 0.0402 ND 34-14996 1,1,2-Trichloroethane "0.0397 0.0050 0.0402 ND 25-17599 Trichloroethene (TCE)"0.0386 0.0050 0.0402 ND 25-17096 Trichlorofluoromethane "0.0487 0.0050 0.0402 ND 19-155121 1,2,3-Trichloropropane "0.0403 0.0050 0.0402 ND 32-165100 1,2,4-Trimethylbenzene "0.0466 0.0050 0.0402 0.0183 15-15070 1,3,5-Trimethylbenzene "0.0413 0.0050 0.0402 0.00496 10-15890 Vinyl chloride "0.0446 0.0050 0.0402 ND 22-148111 Xylenes (total)"0.130 0.0050 0.120 0.0173 22-15393 "0.0502 74-122Surrogate: Dibromofluoromethane 970.0487 "0.0502 65-128Surrogate: Toluene-d8 960.0484 "0.0502 75-121Surrogate: 4-Bromofluorobenzene 940.0474 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 80 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 80 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid STLC Metals by ICP STLC/EPA 6010B OEC, CA-ELAP6010B STLC Cadmium Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Chromium Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Copper Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Lead Water STLC Metals Extraction STLC OEC, InternalSTLC Metals Extraction Solid TCLP Metals by ICP EPA 1311/EPA 6010B OEC, CA-ELAP6010B TCLP Chromium Water EPA 1311/EPA 6010B OEC, CA-ELAP6010B TCLP Lead Water TCLP Metals Extraction EPA 1311 OEC, CA-ELAPTCLP Metals Extraction Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 81 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 81 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample Method Summary (Continued) Laboratory & CertificationMethodAnalysisMatrix Total Metals by CVAA EPA 7471A OEC, CA-ELAPMercury Total EPA 7471A Solid Total Metals by ICP EPA 6010B OEC, CA-ELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP8260B Full List Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 82 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 82 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample Method Summary (Continued) Laboratory & CertificationMethodAnalysisMatrix Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 83 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 83 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-01 Analyte concentration exceeds TTLC. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 84 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 84 of 94 EMSL Analytical, Inc. 464 McCormick Street San Leandro, CA 94577 Tel/Fax: (510) 895-3675 / (510) 895-3680 http://www.EMSL.com / sanleandrolab@emsl.com 092105912EMSL Order: Customer ID:OILF50 Customer PO:2102508 Project ID: Attention:Phone:Shahanaz Parvin (805) 922-4772 Fax:Oilfield Environmental and Compliance (805) 925-3376 Received Date:307 Roemer Way 04/26/2021 8:45 AM Analysis Date:Suite 300 04/26/2021 Collected Date:Santa Maria, CA 93454-1105 04/23/2021 Project:2102508 Test Report: Asbestos Analysis of Bulk Materials via EPA 600/R-93/116 Method using Polarized Light Microscopy Sample Description Appearance % Fibrous % Non-Fibrous Non-Asbestos Asbestos % Type 2102508-16 092105912-0001 None DetectedQuartz Non-fibrous (Other) 50% 50% Tan Non-Fibrous Homogeneous 2102508-17 092105912-0002 None DetectedQuartz Ca Carbonate Non-fibrous (Other) 50% 40% 10% Gray Non-Fibrous Homogeneous Analyst(s) Gavin Lee (2)Cecilia Yu, Laboratory Manager or Other Approved Signatory EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 “Interim Method”) but augmented with procedures outlined in the 1993 (”final”) version of the method. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non-friable organically bound materials present a problem matrix and therefore EMSL recommends gravimetric reduction prior to analysis. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Estimation of uncertainty is available on request. Samples analyzed by EMSL Analytical, Inc San Leandro, CA NVLAP Lab Code 101048-3, WA C884 Initial report from: 04/26/2021 13:36:56 Page 1 of 1ASB_PLM_0008_0001 - 1.78 Printed: 4/26/2021 1:36 PM File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2314.D Operator : EW Acquired : 23 Apr 2021 2:32 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-01@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 14 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2314.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2315.D Operator : EW Acquired : 23 Apr 2021 2:58 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-02@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 15 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOMD2315.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2316.D Operator : EW Acquired : 23 Apr 2021 3:24 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-03@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 16 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2316.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2317.D Operator : EW Acquired : 23 Apr 2021 3:50 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-04@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 17 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2317.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2318.D Operator : EW Acquired : 23 Apr 2021 4:16 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-05@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 18 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2318.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2319.D Operator : EW Acquired : 23 Apr 2021 4:42 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-06@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 19 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2319.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2320.D Operator : EW Acquired : 23 Apr 2021 5:08 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-07@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 20 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2320.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2321.D Operator : EW Acquired : 23 Apr 2021 5:34 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-08@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 21 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOMD2321.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2322.D Operator : EW Acquired : 23 Apr 2021 6:00 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-09@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 22 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2322.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2323.D Operator : EW Acquired : 23 Apr 2021 6:26 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-10@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 23 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2323.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2328.D Operator : EW Acquired : 23 Apr 2021 8:35 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-11@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 28 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2328.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2329.D Operator : EW Acquired : 23 Apr 2021 9:01 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-12@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 29 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOMD2329.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2330.D Operator : EW Acquired : 23 Apr 2021 9:27 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-13@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 30 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2330.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2331.D Operator : EW Acquired : 23 Apr 2021 9:53 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-14@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 31 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2331.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2332.D Operator : EW Acquired : 23 Apr 2021 10:18 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-15@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 32 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2332.D\FID1A Page 85 of 94 Page 86 of 94 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLDYRD(60/ekuijuieihekuijuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 87 of 94 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$3ODVWLF%DJ(06/$QDO\WLFDO,QF6ROLG$R]*ODVV(06/$QDO\WLFDO,QF6ROLG5HFHLSW/RJLQ%\’$5HFHLSW5HYLHZHG%\$00Page 88 of 94 Page 89 of 94 Page 90 of 94 OrderID: 092105912Page 1 Of 1Page 91 of 94 STLC Cr, Cu; TCLP PbSTLC Cr, Pb; TCLP Cr,PbSTLC Cr, Pb; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr; TCLP PbSTLC Pb; TCLP PbPage 92 of 94 STLC Cr, Pb; TCLP Cr,PbSTLC Cr,Cd,Cu,Pb; TCLP PbSTLC Cu, Pb; TCLP PbSTLC Cr; TCLP PbSTLC Pb; TCLP Pbadded all above 6010B STLC & TCLP SP 4/28/2021Page 93 of 94 OrderID: 092105912Page 1 Of 1Page 94 of 94