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2021-05-06 analyticals
[TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2102742 Report Date: May 06, 2021 17:25 Natural Healing CenterNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 05, 2021 08:00 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com California ELAP Certification # 2438 client.oec.com\reportsClient Connect: Page 1 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix NW Corner 2102742-01 05/04/2021 14:30 05/05/2021 08:00Solid Solid NE Corner 2102742-02 05/04/2021 14:35 05/05/2021 08:00Solid Solid SW Corner 2102742-03 05/04/2021 14:40 05/05/2021 08:00Solid Solid SE Corner 2102742-04 05/04/2021 14:45 05/05/2021 08:00Solid Solid Center 2102742-05 05/04/2021 14:50 05/05/2021 08:00Solid Solid [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 05/05/2021 10:31B1E0062 Total Metals by CVAA Mercury Total EPA 7471A 05/05/2021 08:00B1E0098 Total Metals by ICP 6010B Total 05/05/2021 09:08B1E0102 Volatile Organic Compounds by GC/MS 8260B Full List 05/05/2021 09:05B1E0101 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 05/05/2021 06:24B1E0095 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 2 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NW Corner Sampled : 05/04/21 14:30 Lab ID : 2102742-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:11mg/kg B1E00981Mercury0.096 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:33mg/kg B1E01021Antimony2.5 "7.8 """"Arsenic 2.0 "120 """"Barium 0.99 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "44 """"Chromium 0.50 "18 """"Cobalt 0.50 "36 """"Copper 0.99 "16 """"Lead 0.50 ND """ ""Molybdenum 0.50 "71 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 0.99 "43 """"Vanadium 2.0 "68 """"Zinc 2.0 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M19B1E009505/05/21 12:06mg/kg 1TPH Gasoline (C5-C12)4.4 D-04 """( 39 - 157 )109 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M490B1E006205/05/21 19:52mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )89 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 3 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NW Corner Sampled : 05/04/21 14:30 Lab ID : 2102742-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 16:56mg/kg B1E01011000Benzene1.3 ND """ ""Bromobenzene 1.3 ND """ ""Bromochloromethane 1.3 ND """ ""Bromodichloromethane 1.3 ND """ ""Bromoform 1.3 ND """ ""Bromomethane 1.3 ND """ ""n-Butylbenzene 1.3 ND """ ""sec-Butylbenzene 1.3 ND """ ""tert-Butylbenzene 1.3 ND """ ""Carbon tetrachloride 1.3 ND """ ""Chlorobenzene 1.3 ND """ ""Chloroethane 1.3 ND """ ""Chloroform 1.3 ND """ ""Chloromethane 1.3 ND """ ""2-Chlorotoluene 1.3 ND """ ""4-Chlorotoluene 1.3 ND """ ""Dibromochloromethane 1.3 ND """ ""1,2-Dibromo-3-chloropropane 1.3 ND """ ""1,2-Dibromoethane (EDB)1.3 ND """ ""Dibromomethane 1.3 ND """ ""1,2-Dichlorobenzene 1.3 ND """ ""1,3-Dichlorobenzene 1.3 ND """ ""1,4-Dichlorobenzene 1.3 ND """ ""Dichlorodifluoromethane 1.3 ND """ ""1,1-Dichloroethane 1.3 ND """ ""1,2-Dichloroethane 1.3 ND """ ""1,1-Dichloroethene 1.3 ND """ ""cis-1,2-Dichloroethene 1.3 ND """ ""trans-1,2-Dichloroethene 1.3 ND """ ""1,2-Dichloropropane 1.3 ND """ ""1,3-Dichloropropane 1.3 ND """ ""2,2-Dichloropropane 1.3 ND """ ""1,1-Dichloropropene 1.3 ND """ ""cis-1,3-Dichloropropene 1.3 ND """ ""trans-1,3-Dichloropropene 1.3 ND """ ""Ethylbenzene 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 4 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NW Corner Sampled : 05/04/21 14:30 Lab ID : 2102742-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 16:56mg/kg B1E01011000Hexachlorobutadiene1.3 ND """ ""4-Isopropyl Toluene 1.3 ND """ ""Isopropylbenzene 1.3 ND """ ""Methylene chloride 1.3 ND """ ""Naphthalene 1.3 ND """ ""n-Propylbenzene 1.3 ND """ ""Styrene 1.3 ND """ ""1,1,1,2-Tetrachloroethane 1.3 ND """ ""1,1,2,2-Tetrachloroethane 1.3 ND """ ""Tetrachloroethene (PCE)1.3 ND """ ""Toluene 1.3 ND """ ""1,2,3-Trichlorobenzene 1.3 ND """ ""1,2,4-Trichlorobenzene 1.3 ND """ ""1,1,1-Trichloroethane 1.3 ND """ ""1,1,2-Trichloroethane 1.3 ND """ ""Trichloroethene (TCE)1.3 ND """ ""Trichlorofluoromethane 1.3 ND """ ""1,2,3-Trichloropropane 1.3 ND """ ""1,2,4-Trimethylbenzene 1.3 ND """ ""1,3,5-Trimethylbenzene 1.3 ND """ ""Vinyl chloride 1.3 ND """ ""Xylenes (total)1.3 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 5 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NE Corner Sampled : 05/04/21 14:35 Lab ID : 2102742-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:13mg/kg B1E00981Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:36mg/kg B1E01021Antimony2.4 "5.0 """"Arsenic 1.9 "140 """"Barium 0.94 ND """ ""Beryllium 0.47 ND """ ""Cadmium 0.24 "160 """"Chromium 0.47 N-02, N-03 "22 """"Cobalt 0.47 "37 """"Copper 0.94 "6.8 """"Lead 0.47 "0.51 """"Molybdenum 0.47 "270 """"Nickel 0.47 N-02 ND """ ""Selenium 1.9 ND """ ""Silver 0.47 "1.7 """"Thallium 0.94 "61 """"Vanadium 1.9 "59 """"Zinc 1.9 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M5.6 B1E0095 05/05/21 12:32mg/kg 1TPH Gasoline (C5-C12)4.3 D-04 """( 39 - 157 )108 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M310B1E006205/05/21 21:27mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )85 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 6 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NE Corner Sampled : 05/04/21 14:35 Lab ID : 2102742-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 17:24mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 7 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NE Corner Sampled : 05/04/21 14:35 Lab ID : 2102742-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 17:24mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )94 %Surrogate: Toluene-d8 """( 75 - 121 )86 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 8 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SW Corner Sampled : 05/04/21 14:40 Lab ID : 2102742-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-03 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:15mg/kg B1E00981Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:46mg/kg B1E01021Antimony2.3 "4.5 """"Arsenic 1.9 "200 """"Barium 0.93 ND """ ""Beryllium 0.47 ND """ ""Cadmium 0.23 "310 """"Chromium 0.47 N-02, N-03 "55 """"Cobalt 0.47 "45 """"Copper 0.93 "9.5 """"Lead 0.47 "0.68 """"Molybdenum 0.47 "430 """"Nickel 0.47 N-02 ND """ ""Selenium 1.9 ND """ ""Silver 0.47 ND """ ""Thallium 0.93 "70 """"Vanadium 1.9 "69 """"Zinc 1.9 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M7.8 B1E0095 05/05/21 12:58mg/kg 1TPH Gasoline (C5-C12)5.0 D-04 """( 39 - 157 )101 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M220B1E006205/05/21 21:51mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )84 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 9 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SW Corner Sampled : 05/04/21 14:40 Lab ID : 2102742-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 17:51mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 10 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SW Corner Sampled : 05/04/21 14:40 Lab ID : 2102742-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 17:51mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )93 %Surrogate: Dibromofluoromethane """( 65 - 128 )94 %Surrogate: Toluene-d8 """( 75 - 121 )88 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 11 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SE Corner Sampled : 05/04/21 14:45 Lab ID : 2102742-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-04 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:17mg/kg B1E00981Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:49mg/kg B1E01021Antimony2.3 "5.0 """"Arsenic 1.8 "180 """"Barium 0.92 ND """ ""Beryllium 0.46 ND """ ""Cadmium 0.23 "46 """"Chromium 0.46 "14 """"Cobalt 0.46 "41 """"Copper 0.92 "13 """"Lead 0.46 ND """ ""Molybdenum 0.46 "85 """"Nickel 0.46 ND """ ""Selenium 1.8 ND """ ""Silver 0.46 "1.9 """"Thallium 0.92 "39 """"Vanadium 1.8 "57 """"Zinc 1.8 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M5.6 B1E0095 05/05/21 13:24mg/kg 1TPH Gasoline (C5-C12)4.4 D-04 """( 39 - 157 )108 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M190B1E006205/05/21 22:15mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )85 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 12 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SE Corner Sampled : 05/04/21 14:45 Lab ID : 2102742-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 18:18mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 13 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SE Corner Sampled : 05/04/21 14:45 Lab ID : 2102742-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 18:18mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 14 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples Center Sampled : 05/04/21 14:50 Lab ID : 2102742-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-05 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:19mg/kg B1E00981Mercury0.086 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:52mg/kg B1E01021Antimony2.4 "7.0 """"Arsenic 1.9 "140 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "72 """"Chromium 0.48 N-02 "22 """"Cobalt 0.48 "78 """"Copper 0.96 "15 """"Lead 0.48 "0.99 """"Molybdenum 0.48 "160 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 "1.3 """"Thallium 0.96 "62 """"Vanadium 1.9 "80 """"Zinc 1.9 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M7.7 B1E0095 05/05/21 13:49mg/kg 1TPH Gasoline (C5-C12)4.8 D-04 """( 39 - 157 )106 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M350B1E006205/05/21 22:38mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 15 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples Center Sampled : 05/04/21 14:50 Lab ID : 2102742-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 18:46mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 16 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples Center Sampled : 05/04/21 14:50 Lab ID : 2102742-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 18:46mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )94 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )88 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 17 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0098 - EPA 7471A Prep[TOC] Batch B1E0098 - EPA 7471A Preparation: EPA 7471A Prep 05/05/21 08:00 Blank (B1E0098-BLK1) [TOC_3]Blank (B1E0098-BLK1)[TOC] Analyzed: 05/05/21 11:40 Mercury mg/kgND0.10 LCS (B1E0098-BS1) [TOC_3]LCS (B1E0098-BS1)[TOC] Analyzed: 05/05/21 11:35 Mercury mg/kg0.802 0.10 0.833 85-11596 LCS Dup (B1E0098-BSD1) [TOC_3]LCS Dup (B1E0098-BSD1)[TOC] Analyzed: 05/05/21 11:37 Mercury mg/kg0.831 0.10 0.833 2085-115100 4 Duplicate (B1E0098-DUP1)Source: 2102717-01 [TOC_3]Duplicate (B1E0098-DUP1)[TOC] Analyzed: 05/05/21 11:44 Mercury mg/kg0.0262 0.10 0.0394 20 QR-0440 Matrix Spike (B1E0098-MS1)Source: 2102717-01 [TOC_3]Matrix Spike (B1E0098-MS1)[TOC] Analyzed: 05/05/21 11:46 Mercury mg/kg0.836 0.097 0.812 0.0394 75-12598 Matrix Spike Dup (B1E0098-MSD1)Source: 2102717-01 [TOC_3]Matrix Spike Dup (B1E0098-MSD1)[TOC] Analyzed: 05/05/21 11:48 Mercury mg/kg0.838 0.098 0.814 0.0394 2075-12598 0.3 Post Spike (B1E0098-PS1)Source: 2102717-01 [TOC_3]Post Spike (B1E0098-PS1)[TOC] Analyzed: 05/05/21 11:50 Mercury ug/L5.22 5.00 0.256 85-11599 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 18 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0102 - EPA 3050B[TOC] Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Blank (B1E0102-BLK1) [TOC_3]Blank (B1E0102-BLK1)[TOC] Analyzed: 05/06/21 13:12 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1E0102-BS1) [TOC_3]LCS (B1E0102-BS1)[TOC] Analyzed: 05/06/21 12:50 Antimony mg/kg99.2 2.5 100 80-12099 Arsenic "99.8 2.0 100 80-120100 Barium "102 1.0 100 80-120102 Beryllium "96.5 0.50 100 80-12096 Cadmium "101 0.25 100 80-120101 Chromium "102 0.50 100 80-120102 Cobalt "102 0.50 100 80-120102 Copper "103 1.0 100 80-120103 Lead "103 0.50 100 80-120103 Molybdenum "98.1 0.50 100 80-12098 Nickel "102 0.50 100 80-120102 Selenium "97.7 2.0 100 80-12098 Silver "4.81 0.50 5.00 80-12096 Thallium "104 1.0 100 80-120104 Vanadium "98.6 2.0 100 80-12099 Zinc "101 2.0 100 80-120101 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 19 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 LCS Dup (B1E0102-BSD1) [TOC_3]LCS Dup (B1E0102-BSD1)[TOC] Analyzed: 05/06/21 12:52 Antimony mg/kg99.8 2.5 100 2080-120100 0.6 Arsenic "102 2.0 100 2080-120102 2 Barium "103 1.0 100 2080-120103 1 Beryllium "97.2 0.50 100 2080-12097 0.8 Cadmium "102 0.25 100 2080-120102 0.9 Chromium "103 0.50 100 2080-120103 0.6 Cobalt "103 0.50 100 2080-120103 0.6 Copper "103 1.0 100 2080-120103 0.6 Lead "103 0.50 100 2080-120103 0.5 Molybdenum "99.6 0.50 100 2080-120100 2 Nickel "103 0.50 100 2080-120103 0.6 Selenium "100 2.0 100 2080-120100 3 Silver "4.89 0.50 5.00 2080-12098 2 Thallium "105 1.0 100 2080-120105 2 Vanadium "98.9 2.0 100 2080-12099 0.4 Zinc "102 2.0 100 2080-120102 0.6 Duplicate (B1E0102-DUP1)Source: 2102717-02 [TOC_3]Duplicate (B1E0102-DUP1)[TOC] Analyzed: 05/06/21 13:17 Antimony mg/kgND2.4 ND 20 Arsenic "7.55 1.9 8.39 2010 Barium "92.7 0.95 97.2 205 Beryllium "0.657 0.48 0.691 205 Cadmium "ND 0.24 ND 20 Chromium "16.8 0.48 16.2 204 Cobalt "7.71 0.48 8.09 205 Copper "18.7 0.95 19.7 205 Lead "11.1 0.48 11.8 206 Molybdenum "1.43 0.48 1.58 2010 Nickel "22.9 0.48 19.7 2015 Selenium "ND 1.9 ND 20 Silver "ND 0.48 ND 20 Thallium "ND 0.95 ND 20 Vanadium "32.2 1.9 32.7 202 Zinc "60.1 1.9 64.4 207 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 20 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Matrix Spike (B1E0102-MS1)Source: 2102717-02 [TOC_3]Matrix Spike (B1E0102-MS1)[TOC] Analyzed: 05/06/21 12:55 Antimony mg/kg26.4 2.5 99.2 ND 10-11627 Arsenic "105 2.0 99.2 8.39 77-12198 Barium "193 0.99 99.2 97.2 30-16997 Beryllium "93.6 0.50 99.2 0.691 86-11194 Cadmium "93.6 0.25 99.2 ND 81-11294 Chromium "118 0.50 99.2 16.2 75-129103 Cobalt "102 0.50 99.2 8.09 71-12194 Copper "119 0.99 99.2 19.7 68-135100 Lead "105 0.50 99.2 11.8 72-12194 Molybdenum "89.4 0.50 99.2 1.58 70-11289 Nickel "114 0.50 99.2 19.7 73-12195 Selenium "89.8 2.0 99.2 ND 76-11691 Silver "4.31 0.50 4.96 ND 54-13287 Thallium "89.0 0.99 99.2 ND 64-12090 Vanadium "130 2.0 99.2 32.7 78-12498 Zinc "158 2.0 99.2 64.4 50-14394 Matrix Spike Dup (B1E0102-MSD1)Source: 2102717-02 [TOC_3]Matrix Spike Dup (B1E0102-MSD1)[TOC] Analyzed: 05/06/21 12:57 Antimony mg/kg29.7 2.4 94.4 ND 2010-11631 12 Arsenic "103 1.9 94.4 8.39 2077-121101 2 Barium "182 0.94 94.4 97.2 2030-16989 6 Beryllium "91.6 0.47 94.4 0.691 2086-11196 2 Cadmium "91.5 0.24 94.4 ND 2081-11297 2 Chromium "113 0.47 94.4 16.2 2075-129103 4 Cobalt "99.2 0.47 94.4 8.09 2071-12196 3 Copper "114 0.94 94.4 19.7 2068-135100 4 Lead "102 0.47 94.4 11.8 2072-12196 3 Molybdenum "88.9 0.47 94.4 1.58 2070-11292 0.6 Nickel "111 0.47 94.4 19.7 2073-12196 3 Selenium "88.7 1.9 94.4 ND 2076-11694 1 Silver "4.23 0.47 4.72 ND 2054-13290 2 Thallium "87.0 0.94 94.4 ND 2064-12092 2 Vanadium "126 1.9 94.4 32.7 2078-12498 4 Zinc "153 1.9 94.4 64.4 2050-14394 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 21 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Post Spike (B1E0102-PS1)Source: 2102717-02 [TOC_3]Post Spike (B1E0102-PS1)[TOC] Analyzed: 05/06/21 13:00 Antimony mg/L1.95 2.00 -0.0338 75-12598 Arsenic "2.25 2.00 0.171 75-125104 Barium "3.97 2.00 1.98 75-12599 Beryllium "1.97 2.00 0.0141 75-12598 Cadmium "1.97 2.00 -0.0215 75-12599 Chromium "2.42 2.00 0.330 75-125104 Cobalt "2.15 2.00 0.165 75-12599 Copper "2.51 2.00 0.401 75-125105 Lead "2.20 2.00 0.240 75-12598 Molybdenum "2.02 2.00 0.0322 75-12599 Nickel "2.48 2.00 0.403 75-125104 Selenium "1.96 2.00 -0.0744 75-12598 Silver "0.0946 0.100 -0.00744 75-12595 Thallium "1.88 2.00 -0.0732 75-12594 Vanadium "2.71 2.00 0.668 75-125102 Zinc "3.25 2.00 1.31 75-12597 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 22 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0095 - EPA 5035/5030B Solid GC[TOC] Batch B1E0095 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/05/21 06:24 Blank (B1E0095-BLK1) [TOC_3]Blank (B1E0095-BLK1)[TOC] Analyzed: 05/05/21 09:00 TPH Gasoline (C5-C12)mg/kgND0.50 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1080.134 LCS (B1E0095-BS1) [TOC_3]LCS (B1E0095-BS1)[TOC] Analyzed: 05/05/21 08:09 TPH Gasoline (C5-C12)mg/kg0.917 0.50 0.992 68-13992 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1270.158 LCS Dup (B1E0095-BSD1) [TOC_3]LCS Dup (B1E0095-BSD1)[TOC] Analyzed: 05/05/21 08:34 TPH Gasoline (C5-C12)mg/kg1.03 0.50 0.994 2068-139103 11 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1270.157 Duplicate (B1E0095-DUP1)Source: 2102652-01 [TOC_3]Duplicate (B1E0095-DUP1)[TOC] Analyzed: 05/05/21 09:59 TPH Gasoline (C5-C12)mg/kgND5.2 ND 20 "1.30 39-157Surrogate: 4-Bromofluorobenzene 1001.30 Matrix Spike (B1E0095-MS1)Source: 2102652-01 [TOC_3]Matrix Spike (B1E0095-MS1)[TOC] Analyzed: 05/05/21 14:41 TPH Gasoline (C5-C12)mg/kg7.97 4.9 9.80 ND 10-17181 "1.23 39-157Surrogate: 4-Bromofluorobenzene 1151.40 Matrix Spike Dup (B1E0095-MSD1)Source: 2102652-01 [TOC_3]Matrix Spike Dup (B1E0095-MSD1)[TOC] Analyzed: 05/05/21 15:07 TPH Gasoline (C5-C12)mg/kg8.18 5.2 10.4 ND 2010-17178 3 "1.30 39-157Surrogate: 4-Bromofluorobenzene 1071.40 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 23 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0062 - EPA 3550C[TOC] Batch B1E0062 - EPA 8015M Preparation: EPA 3550C 05/05/21 10:31 Blank (B1E0062-BLK1) [TOC_3]Blank (B1E0062-BLK1)[TOC] Analyzed: 05/05/21 17:58 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "49.9 65-136Surrogate: o-Terphenyl 7637.8 LCS (B1E0062-BS1) [TOC_3]LCS (B1E0062-BS1)[TOC] Analyzed: 05/05/21 17:12 TPH Diesel (C13-C22)mg/kg41110 500 72-11582 TPH Motor Oil (C23-C40)"467 50 500 74-12693 "50.0 65-136Surrogate: o-Terphenyl 8040.0 LCS Dup (B1E0062-BSD1) [TOC_3]LCS Dup (B1E0062-BSD1)[TOC] Analyzed: 05/05/21 17:35 TPH Diesel (C13-C22)mg/kg43310 499 2072-11587 5 TPH Motor Oil (C23-C40)"493 50 499 2074-12699 6 "49.9 65-136Surrogate: o-Terphenyl 8241.1 Duplicate (B1E0062-DUP1)Source: 2102648-01 [TOC_3]Duplicate (B1E0062-DUP1)[TOC] Analyzed: 05/05/21 21:27 TPH Diesel (C13-C22)mg/kg35.5 10 34.6 20 D-042 TPH Motor Oil (C23-C40)"71.2 50 65.4 20 D-048 "49.8 65-136Surrogate: o-Terphenyl 10853.6 Matrix Spike (B1E0062-MS1)Source: 2102648-01 [TOC_3]Matrix Spike (B1E0062-MS1)[TOC] Analyzed: 05/05/21 21:51 TPH Diesel (C13-C22)mg/kg73110 499 34.6 46-147140 TPH Motor Oil (C23-C40)"559 50 499 65.4 35-17199 "49.9 65-136Surrogate: o-Terphenyl 8844.1 Matrix Spike Dup (B1E0062-MSD1)Source: 2102648-01 [TOC_3]Matrix Spike Dup (B1E0062-MSD1)[TOC] Analyzed: 05/05/21 22:15 TPH Diesel (C13-C22)mg/kg56210 499 34.6 20 QR-0246-147106 26 TPH Motor Oil (C23-C40)"485 50 499 65.4 2035-17184 14 "49.9 65-136Surrogate: o-Terphenyl 8341.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 24 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0101 - EPA 5035/5030B MEOH[TOC] Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLK1) [TOC_3]Blank (B1E0101-BLK1)[TOC] Analyzed: 05/05/21 13:17 Benzene mg/kgND0.25 Bromobenzene "ND 0.25 Bromochloromethane "ND 0.25 Bromodichloromethane "ND 0.25 Bromoform "ND 0.25 Bromomethane "ND 0.25 n-Butylbenzene "ND 0.25 sec-Butylbenzene "ND 0.25 tert-Butylbenzene "ND 0.25 Carbon tetrachloride "ND 0.25 Chlorobenzene "ND 0.25 Chloroethane "ND 0.25 Chloroform "ND 0.25 Chloromethane "ND 0.25 2-Chlorotoluene "ND 0.25 4-Chlorotoluene "ND 0.25 Dibromochloromethane "ND 0.25 1,2-Dibromo-3-chloropropane "ND 0.25 1,2-Dibromoethane (EDB)"ND 0.25 Dibromomethane "ND 0.25 1,2-Dichlorobenzene "ND 0.25 1,3-Dichlorobenzene "ND 0.25 1,4-Dichlorobenzene "ND 0.25 Dichlorodifluoromethane "ND 0.25 1,1-Dichloroethane "ND 0.25 1,2-Dichloroethane "ND 0.25 1,1-Dichloroethene "ND 0.25 cis-1,2-Dichloroethene "ND 0.25 trans-1,2-Dichloroethene "ND 0.25 1,2-Dichloropropane "ND 0.25 1,3-Dichloropropane "ND 0.25 2,2-Dichloropropane "ND 0.25 1,1-Dichloropropene "ND 0.25 cis-1,3-Dichloropropene "ND 0.25 trans-1,3-Dichloropropene "ND 0.25 Ethylbenzene "ND 0.25 Hexachlorobutadiene "ND 0.25 4-Isopropyl Toluene "ND 0.25 Isopropylbenzene "ND 0.25 Methylene chloride "ND 0.25 Naphthalene "ND 0.25 n-Propylbenzene "ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 25 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLK1)Analyzed: 05/05/21 13:17 Styrene mg/kgND0.25 1,1,1,2-Tetrachloroethane "ND 0.25 1,1,2,2-Tetrachloroethane "ND 0.25 Tetrachloroethene (PCE)"ND 0.25 Toluene "ND 0.25 1,2,3-Trichlorobenzene "ND 0.25 1,2,4-Trichlorobenzene "ND 0.25 1,1,1-Trichloroethane "ND 0.25 1,1,2-Trichloroethane "ND 0.25 Trichloroethene (TCE)"ND 0.25 Trichlorofluoromethane "ND 0.25 1,2,3-Trichloropropane "ND 0.25 1,2,4-Trimethylbenzene "ND 0.25 1,3,5-Trimethylbenzene "ND 0.25 Vinyl chloride "ND 0.25 Xylenes (total)"ND 0.25 "0.0496 74-122Surrogate: Dibromofluoromethane 940.0468 "0.0496 65-128Surrogate: Toluene-d8 930.0462 "0.0496 75-121Surrogate: 4-Bromofluorobenzene 870.0431 LCS (B1E0101-BS1) [TOC_3]LCS (B1E0101-BS1)[TOC] Analyzed: 05/05/21 12:22 Benzene mg/kg2.30 0.25 1.99 70-131116 Bromobenzene "1.97 0.25 1.99 74-13099 Bromochloromethane "1.85 0.25 1.99 64-13393 Bromodichloromethane "1.99 0.25 1.99 69-137100 Bromoform "1.74 0.25 1.99 55-13288 Bromomethane "1.64 0.25 1.99 10-14283 n-Butylbenzene "2.58 0.25 1.99 64-156130 sec-Butylbenzene "2.53 0.25 1.99 75-155127 tert-Butylbenzene "2.32 0.25 1.99 74-144117 Carbon tetrachloride "2.18 0.25 1.99 67-135110 Chlorobenzene "2.17 0.25 1.99 73-134109 Chloroethane "1.83 0.25 1.99 10-16792 Chloroform "2.13 0.25 1.99 69-124107 Chloromethane "2.32 0.25 1.99 34-136117 2-Chlorotoluene "2.14 0.25 1.99 75-135107 4-Chlorotoluene "2.14 0.25 1.99 70-138108 Dibromochloromethane "1.99 0.25 1.99 67-135100 1,2-Dibromo-3-chloropropane "1.99 0.25 1.99 41-149100 1,2-Dibromoethane (EDB)"1.92 0.25 1.99 68-13197 Dibromomethane "1.48 0.25 1.99 61-14074 1,2-Dichlorobenzene "2.07 0.25 1.99 76-136104 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 26 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS (B1E0101-BS1)Analyzed: 05/05/21 12:22 1,3-Dichlorobenzene mg/kg2.17 0.25 1.99 76-138109 1,4-Dichlorobenzene "2.14 0.25 1.99 72-132108 Dichlorodifluoromethane "1.31 0.25 1.99 10-15566 1,1-Dichloroethane "2.33 0.25 1.99 63-139117 1,2-Dichloroethane "2.06 0.25 1.99 64-126104 1,1-Dichloroethene "2.77 0.25 1.99 52-167139 cis-1,2-Dichloroethene "2.07 0.25 1.99 70-135104 trans-1,2-Dichloroethene "2.43 0.25 1.99 67-147122 1,2-Dichloropropane "2.05 0.25 1.99 68-131103 1,3-Dichloropropane "2.04 0.25 1.99 64-128103 2,2-Dichloropropane "2.31 0.25 1.99 63-154116 1,1-Dichloropropene "2.22 0.25 1.99 68-138112 cis-1,3-Dichloropropene "2.09 0.25 1.99 72-134105 trans-1,3-Dichloropropene "2.26 0.25 1.99 69-132114 Ethylbenzene "2.46 0.25 1.99 68-136124 Hexachlorobutadiene "2.20 0.25 1.99 72-198111 4-Isopropyl Toluene "2.39 0.25 1.99 74-150120 Isopropylbenzene "2.41 0.25 1.99 71-149121 Methylene chloride "2.57 0.25 1.99 QM-0851-127129 Naphthalene "1.99 0.25 1.99 57-158100 n-Propylbenzene "2.27 0.25 1.99 70-143114 Styrene "2.25 0.25 1.99 68-138113 1,1,1,2-Tetrachloroethane "1.92 0.25 1.99 76-13097 1,1,2,2-Tetrachloroethane "2.09 0.25 1.99 60-136105 Tetrachloroethene (PCE)"2.09 0.25 1.99 73-138105 Toluene "2.18 0.25 1.99 72-128110 1,2,3-Trichlorobenzene "1.74 0.25 1.99 61-16688 1,2,4-Trichlorobenzene "1.85 0.25 1.99 71-15893 1,1,1-Trichloroethane "2.24 0.25 1.99 71-135113 1,1,2-Trichloroethane "2.07 0.25 1.99 64-132104 Trichloroethene (TCE)"1.92 0.25 1.99 74-13997 Trichlorofluoromethane "1.74 0.25 1.99 30-15687 1,2,3-Trichloropropane "2.01 0.25 1.99 67-123101 1,2,4-Trimethylbenzene "2.52 0.25 1.99 68-134127 1,3,5-Trimethylbenzene "2.37 0.25 1.99 71-140119 Vinyl chloride "2.46 0.25 1.99 43-144124 Xylenes (total)"7.54 0.25 5.96 69-138126 "0.0497 74-122Surrogate: Dibromofluoromethane 980.0485 "0.0497 65-128Surrogate: Toluene-d8 950.0471 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 940.0467 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 27 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSD1) [TOC_3]LCS Dup (B1E0101-BSD1)[TOC] Analyzed: 05/05/21 12:49 Benzene mg/kg2.25 0.25 1.99 2070-131113 2 Bromobenzene "1.93 0.25 1.99 2074-13097 2 Bromochloromethane "1.85 0.25 1.99 2064-13393 0 Bromodichloromethane "2.00 0.25 1.99 2069-137101 0.5 Bromoform "1.81 0.25 1.99 2055-13291 3 Bromomethane "1.48 0.25 1.99 2010-14275 10 n-Butylbenzene "2.57 0.25 1.99 2064-156129 0.2 sec-Butylbenzene "2.51 0.25 1.99 2075-155126 0.8 tert-Butylbenzene "2.34 0.25 1.99 2074-144118 1 Carbon tetrachloride "2.12 0.25 1.99 2067-135107 3 Chlorobenzene "2.20 0.25 1.99 2073-134110 1 Chloroethane "1.75 0.25 1.99 2010-16788 4 Chloroform "2.10 0.25 1.99 2069-124106 1 Chloromethane "2.15 0.25 1.99 2034-136108 8 2-Chlorotoluene "2.15 0.25 1.99 2075-135108 0.6 4-Chlorotoluene "2.15 0.25 1.99 2070-138108 0.5 Dibromochloromethane "1.94 0.25 1.99 2067-13598 2 1,2-Dibromo-3-chloropropane "1.89 0.25 1.99 2041-14995 5 1,2-Dibromoethane (EDB)"1.96 0.25 1.99 2068-13199 2 Dibromomethane "1.52 0.25 1.99 2061-14076 3 1,2-Dichlorobenzene "2.12 0.25 1.99 2076-136107 2 1,3-Dichlorobenzene "2.17 0.25 1.99 2076-138109 0 1,4-Dichlorobenzene "2.21 0.25 1.99 2072-132111 3 Dichlorodifluoromethane "1.31 0.25 1.99 2010-15566 0.2 1,1-Dichloroethane "2.30 0.25 1.99 2063-139116 1 1,2-Dichloroethane "2.09 0.25 1.99 2064-126105 2 1,1-Dichloroethene "2.55 0.25 1.99 2052-167128 8 cis-1,2-Dichloroethene "2.01 0.25 1.99 2070-135101 3 trans-1,2-Dichloroethene "2.37 0.25 1.99 2067-147119 2 1,2-Dichloropropane "2.07 0.25 1.99 2068-131104 0.8 1,3-Dichloropropane "2.02 0.25 1.99 2064-128102 1 2,2-Dichloropropane "2.25 0.25 1.99 2063-154113 3 1,1-Dichloropropene "2.20 0.25 1.99 2068-138111 1 cis-1,3-Dichloropropene "2.06 0.25 1.99 2072-134103 2 trans-1,3-Dichloropropene "2.25 0.25 1.99 2069-132113 0.8 Ethylbenzene "2.47 0.25 1.99 2068-136124 0.2 Hexachlorobutadiene "2.25 0.25 1.99 2072-198113 2 4-Isopropyl Toluene "2.42 0.25 1.99 2074-150122 1 Isopropylbenzene "2.36 0.25 1.99 2071-149119 2 Methylene chloride "2.45 0.25 1.99 2051-127123 5 Naphthalene "2.00 0.25 1.99 2057-158101 0.9 n-Propylbenzene "2.29 0.25 1.99 2070-143115 0.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 28 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 28 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSD1)Analyzed: 05/05/21 12:49 Styrene mg/kg2.26 0.25 1.99 2068-138114 0.4 1,1,1,2-Tetrachloroethane "1.96 0.25 1.99 2076-13099 2 1,1,2,2-Tetrachloroethane "2.08 0.25 1.99 2060-136105 0.2 Tetrachloroethene (PCE)"2.07 0.25 1.99 2073-138104 1 Toluene "2.21 0.25 1.99 2072-128111 1 1,2,3-Trichlorobenzene "1.87 0.25 1.99 2061-16694 7 1,2,4-Trichlorobenzene "1.89 0.25 1.99 2071-15895 2 1,1,1-Trichloroethane "2.17 0.25 1.99 2071-135109 3 1,1,2-Trichloroethane "2.16 0.25 1.99 2064-132108 4 Trichloroethene (TCE)"1.89 0.25 1.99 2074-13995 1 Trichlorofluoromethane "1.58 0.25 1.99 2030-15679 10 1,2,3-Trichloropropane "1.90 0.25 1.99 2067-12395 6 1,2,4-Trimethylbenzene "2.60 0.25 1.99 2068-134131 3 1,3,5-Trimethylbenzene "2.38 0.25 1.99 2071-140120 0.6 Vinyl chloride "2.27 0.25 1.99 2043-144114 8 Xylenes (total)"7.47 0.25 5.96 2069-138125 0.9 "0.0497 74-122Surrogate: Dibromofluoromethane 980.0486 "0.0497 65-128Surrogate: Toluene-d8 940.0467 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 920.0459 Duplicate (B1E0101-DUP1)Source: 2102742-01RE1 [TOC_3]Duplicate (B1E0101-DUP1)[TOC] Analyzed: 05/05/21 15:07 Benzene mg/kgND1.3 ND 20 Bromobenzene "ND 1.3 ND 20 Bromochloromethane "ND 1.3 ND 20 Bromodichloromethane "ND 1.3 ND 20 Bromoform "ND 1.3 ND 20 Bromomethane "ND 1.3 ND 20 n-Butylbenzene "ND 1.3 ND 20 sec-Butylbenzene "ND 1.3 ND 20 tert-Butylbenzene "ND 1.3 ND 20 Carbon tetrachloride "ND 1.3 ND 20 Chlorobenzene "ND 1.3 ND 20 Chloroethane "ND 1.3 ND 20 Chloroform "ND 1.3 ND 20 Chloromethane "ND 1.3 ND 20 2-Chlorotoluene "ND 1.3 ND 20 4-Chlorotoluene "ND 1.3 ND 20 Dibromochloromethane "ND 1.3 ND 20 1,2-Dibromo-3-chloropropane "ND 1.3 ND 20 1,2-Dibromoethane (EDB)"ND 1.3 ND 20 Dibromomethane "ND 1.3 ND 20 1,2-Dichlorobenzene "ND 1.3 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 29 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 29 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Duplicate (B1E0101-DUP1)Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 1,3-Dichlorobenzene mg/kgND1.3 ND 20 1,4-Dichlorobenzene "ND 1.3 ND 20 Dichlorodifluoromethane "ND 1.3 ND 20 1,1-Dichloroethane "ND 1.3 ND 20 1,2-Dichloroethane "ND 1.3 ND 20 1,1-Dichloroethene "ND 1.3 ND 20 cis-1,2-Dichloroethene "ND 1.3 ND 20 trans-1,2-Dichloroethene "ND 1.3 ND 20 1,2-Dichloropropane "ND 1.3 ND 20 1,3-Dichloropropane "ND 1.3 ND 20 2,2-Dichloropropane "ND 1.3 ND 20 1,1-Dichloropropene "ND 1.3 ND 20 cis-1,3-Dichloropropene "ND 1.3 ND 20 trans-1,3-Dichloropropene "ND 1.3 ND 20 Ethylbenzene "ND 1.3 ND 20 Hexachlorobutadiene "ND 1.3 ND 20 4-Isopropyl Toluene "ND 1.3 ND 20 Isopropylbenzene "ND 1.3 ND 20 Methylene chloride "ND 1.3 ND 20 Naphthalene "ND 1.3 ND 20 n-Propylbenzene "ND 1.3 ND 20 Styrene "ND 1.3 ND 20 1,1,1,2-Tetrachloroethane "ND 1.3 ND 20 1,1,2,2-Tetrachloroethane "ND 1.3 ND 20 Tetrachloroethene (PCE)"ND 1.3 ND 20 Toluene "0.572 1.3 ND 20 A-01 1,2,3-Trichlorobenzene "ND 1.3 ND 20 1,2,4-Trichlorobenzene "ND 1.3 ND 20 1,1,1-Trichloroethane "ND 1.3 ND 20 1,1,2-Trichloroethane "ND 1.3 ND 20 Trichloroethene (TCE)"ND 1.3 ND 20 Trichlorofluoromethane "ND 1.3 ND 20 1,2,3-Trichloropropane "ND 1.3 ND 20 1,2,4-Trimethylbenzene "ND 1.3 ND 20 1,3,5-Trimethylbenzene "ND 1.3 ND 20 Vinyl chloride "ND 1.3 ND 20 Xylenes (total)"ND 1.3 ND 20 "0.0502 74-122Surrogate: Dibromofluoromethane 930.0467 "0.0502 65-128Surrogate: Toluene-d8 950.0475 "0.0502 75-121Surrogate: 4-Bromofluorobenzene 880.0442 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 30 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1)Source: 2102742-02 [TOC_3]Matrix Spike (B1E0101-MS1)[TOC] Analyzed: 05/05/21 20:08 Benzene mg/kg11.1 1.3 10.0 ND 37-145111 Bromobenzene "9.57 1.3 10.0 ND 29-14796 Bromochloromethane "9.29 1.3 10.0 ND 40-14593 Bromodichloromethane "10.2 1.3 10.0 ND 39-153102 Bromoform "9.14 1.3 10.0 ND 32-14391 Bromomethane "12.1 1.3 10.0 ND 10-141121 n-Butylbenzene "12.3 1.3 10.0 ND 10-162123 sec-Butylbenzene "12.5 1.3 10.0 ND 14-168125 tert-Butylbenzene "11.8 1.3 10.0 ND 21-159118 Carbon tetrachloride "10.4 1.3 10.0 ND 28-148104 Chlorobenzene "10.6 1.3 10.0 ND 32-148106 Chloroethane "11.0 1.3 10.0 ND 11-166110 Chloroform "10.3 1.3 10.0 ND 40-139103 Chloromethane "9.86 1.3 10.0 ND 18-13598 2-Chlorotoluene "10.7 1.3 10.0 ND 25-151107 4-Chlorotoluene "10.7 1.3 10.0 ND 22-150106 Dibromochloromethane "9.53 1.3 10.0 ND 40-14795 1,2-Dibromo-3-chloropropane "9.97 1.3 10.0 ND 25-158100 1,2-Dibromoethane (EDB)"9.29 1.3 10.0 ND 38-14793 Dibromomethane "7.54 1.3 10.0 ND 39-15075 1,2-Dichlorobenzene "10.6 1.3 10.0 ND 24-154106 1,3-Dichlorobenzene "10.9 1.3 10.0 ND 21-153108 1,4-Dichlorobenzene "10.6 1.3 10.0 ND 21-146106 Dichlorodifluoromethane "5.88 1.3 10.0 ND 10-14959 1,1-Dichloroethane "11.2 1.3 10.0 ND 34-151112 1,2-Dichloroethane "10.1 1.3 10.0 ND 40-137100 1,1-Dichloroethene "11.8 1.3 10.0 ND 21-172118 cis-1,2-Dichloroethene "9.65 1.3 10.0 ND 38-14796 trans-1,2-Dichloroethene "11.3 1.3 10.0 ND 30-160112 1,2-Dichloropropane "10.4 1.3 10.0 ND 39-146104 1,3-Dichloropropane "10.2 1.3 10.0 ND 39-141102 2,2-Dichloropropane "9.32 1.3 10.0 ND 26-14993 1,1-Dichloropropene "10.7 1.3 10.0 ND 28-150106 cis-1,3-Dichloropropene "9.97 1.3 10.0 ND 34-149100 trans-1,3-Dichloropropene "10.7 1.3 10.0 ND 36-143107 Ethylbenzene "11.5 1.3 10.0 ND 23-150115 Hexachlorobutadiene "11.1 1.3 10.0 ND 10-192111 4-Isopropyl Toluene "11.7 1.3 10.0 ND 11-165117 Isopropylbenzene "11.2 1.3 10.0 ND 17-166112 Methylene chloride "12.0 1.3 10.0 ND 28-135120 Naphthalene "12.0 1.3 10.0 ND 10-174120 n-Propylbenzene "11.3 1.3 10.0 ND 16-156113 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 31 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1)Source: 2102742-02 Analyzed: 05/05/21 20:08 Styrene mg/kg10.8 1.3 10.0 ND 24-154108 1,1,1,2-Tetrachloroethane "9.48 1.3 10.0 ND 38-14995 1,1,2,2-Tetrachloroethane "11.0 1.3 10.0 ND 22-164110 Tetrachloroethene (PCE)"9.82 1.3 10.0 ND 25-15398 Toluene "10.7 1.3 10.0 ND 26-149107 1,2,3-Trichlorobenzene "10.2 1.3 10.0 ND 10-163101 1,2,4-Trichlorobenzene "9.87 1.3 10.0 ND 10-16299 1,1,1-Trichloroethane "10.6 1.3 10.0 ND 34-149106 1,1,2-Trichloroethane "9.74 1.3 10.0 ND 25-17597 Trichloroethene (TCE)"9.32 1.3 10.0 ND 25-17093 Trichlorofluoromethane "10.8 1.3 10.0 ND 19-155107 1,2,3-Trichloropropane "10.3 1.3 10.0 ND 32-165103 1,2,4-Trimethylbenzene "12.6 1.3 10.0 ND 15-150126 1,3,5-Trimethylbenzene "11.7 1.3 10.0 ND 10-158117 Vinyl chloride "10.9 1.3 10.0 ND 22-148108 Xylenes (total)"35.6 1.3 30.1 ND 22-153118 "0.0501 74-122Surrogate: Dibromofluoromethane 940.0473 "0.0501 65-128Surrogate: Toluene-d8 940.0469 "0.0501 75-121Surrogate: 4-Bromofluorobenzene 900.0453 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 32 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid Total Metals by CVAA EPA 7471A OEC, CA-ELAPMercury Total EPA 7471A Solid Total Metals by ICP EPA 6010B OEC, CA-ELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP8260B Full List Solid Volatile Organic TPH by GC/FID EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 33 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 33 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL A-01 Potential carryover from previous high leveled sample. D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. QM-08 The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out-Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 34 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 34 of 37 File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0511.D Operator : BNT Acquired : 5 May 2021 12:06 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-01@ Misc Info : 1@B1E0095 GRO SO Vial Number: 11 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME0511.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0512.D Operator : BNT Acquired : 5 May 2021 12:32 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-02@ Misc Info : 1@B1E0095 GRO SO Vial Number: 12 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOME0512.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0513.D Operator : BNT Acquired : 5 May 2021 12:58 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-03@ Misc Info : 1@B1E0095 GRO SO Vial Number: 13 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOME0513.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0514.D Operator : BNT Acquired : 5 May 2021 1:24 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-04@ Misc Info : 1@B1E0095 GRO SO Vial Number: 14 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 Time Response_GOME0514.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0515.D Operator : BNT Acquired : 5 May 2021 1:49 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-05@ Misc Info : 1@B1E0095 GRO SO Vial Number: 15 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME0515.D\FID1A File : X:\MAY21\050521\B0ME0526.DOperator : RWSAcquired : 5-5-2021 07:52:41 PM using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-01@B1E0062 Misc Info : 1@ Vial Number: 262.00 2.10 2.20 2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20 4.30 4.40 4.50 4.60 4.70 4.80100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07 1.8e+07 1.9e+07 2e+07TimeResponse_Signal: B0ME0526.D\FID1A.CH File : X:\MAY21\050521\B0ME0534.DOperator : RWSAcquired : 5-5-2021 09:27:30 PM using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-02@B1E0062 Misc Info : 1@ Vial Number: 342.10 2.20 2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20 4.30 4.40 4.50 4.60 4.70 4.80 4.90 5.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME0534.D\FID1A.CH File : X:\MAY21\050521\B0ME0536.DOperator : RWSAcquired : 5-5-2021 09:51:16 PM using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-03@B1E0062 Misc Info : 1@ Vial Number: 361.80 2.00 2.20 2.40 2.60 2.80 3.00 3.20 3.40 3.60 3.80 4.00 4.20 4.40 4.60 4.80 5.00 5.20 5.40 5.60100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME0536.D\FID1A.CH File : X:\MAY21\050521\B0ME0538.DOperator : RWSAcquired : 05 May 2021 10:15 pm using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-04@B1E0062 Misc Info : 1@ Vial Number: 381.80 2.00 2.20 2.40 2.60 2.80 3.00 3.20 3.40 3.60 3.80 4.00 4.20 4.40 4.60 4.80 5.00 5.20 5.40 5.60 5.80 6.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME0538.D\FID1A.CH File : X:\MAY21\050521\B0ME0540.DOperator : RWSAcquired : 05 May 2021 10:38 pm using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-05@B1E0062 Misc Info : 1@ Vial Number: 402.10 2.20 2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20 4.30 4.40 4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME0540.D\FID1A.CH Page 35 of 37 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