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HomeMy WebLinkAbout2021-06-01 Analyticals[TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2103212 Report Date: June 01, 2021 10:29 NHC SLO, 2640 Broad StreetNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 24, 2021 13:05 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com California ELAP Certification # 2438 client.oec.com\reportsClient Connect: Page 1 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix Bottom West Center 2103212-01 05/24/2021 11:20 05/24/2021 13:05Solid Solid Bottom East Center 2103212-02 05/24/2021 11:25 05/24/2021 13:05Solid Solid Bin 20339-A 2103212-03 05/24/2021 11:30 05/24/2021 13:05Solid Solid Bin 20339-B 2103212-04 05/24/2021 11:35 05/24/2021 13:05Solid Solid Bin 20339-C 2103212-05 05/24/2021 11:40 05/24/2021 13:05Solid Solid Bin 20144-A 2103212-06 05/24/2021 11:45 05/24/2021 13:05Solid Solid Bin 20144-B 2103212-07 05/24/2021 11:50 05/24/2021 13:05Solid Solid Bin 20144-C 2103212-08 05/24/2021 11:55 05/24/2021 13:05Solid Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 2 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 05/25/2021 08:55B1E0696 STLC Metals by ICP 6010B STLC 05/28/2021 09:36B1E0829 STLC Metals Extraction STLC Metals Extraction 05/26/2021 08:58B1E0743 TCLP Metals by ICP 6010B TCLP 05/27/2021 10:55B1E0794 TCLP Metals Extraction TCLP Metals Extraction 05/26/2021 09:03B1E0744 Total Metals by CVAA Mercury Total EPA 7471A 05/25/2021 07:50B1E0694 Total Metals by ICP 6010B Total 05/25/2021 07:26B1E0693 Volatile Organic Compounds by GC/MS 8260B Full List 05/25/2021 09:00B1E0697 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 05/26/2021 06:59B1E0737 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 3 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.22 B1E0694 05/25/21 14:04mg/kg 1Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:18mg/kg B1E06931Antimony2.4 "7.0 """"Arsenic 1.9 "560 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "120 """"Chromium 0.48 N-02, N-03 "21 """"Cobalt 0.48 "43 """"Copper 0.96 "7.3 """"Lead 0.48 "0.62 """"Molybdenum 0.48 "160 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "46 """"Vanadium 1.9 "56 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B05/28/21 13:17mg/L B1E08292Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:15mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 4 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M05/26/21 13:56mg/kg B1E07371TPH Gasoline (C5-C12)0.50 """( 39 - 157 )101 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M51B1E069605/25/21 14:26mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )90 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 5 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 15:16mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 6 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 15:16mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )101 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )97 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 7 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:06mg/kg B1E06941Mercury0.095 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:21mg/kg B1E06931Antimony2.4 "6.6 """"Arsenic 1.9 "220 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "120 """"Chromium 0.48 N-02, N-03 "19 """"Cobalt 0.48 "39 """"Copper 0.96 "8.3 """"Lead 0.48 ND """ ""Molybdenum 0.48 "150 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "51 """"Vanadium 1.9 "62 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B05/28/21 13:24mg/L B1E08292Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:17mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 8 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.2 B1E0737 05/26/21 15:34mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )118 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M330B1E069605/25/21 14:03mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )108 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 9 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 15:43mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 10 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 15:43mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )101 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )96 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 11 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-03 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:08mg/kg B1E06941Mercury0.099 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:24mg/kg B1E06931Antimony2.5 "5.1 """"Arsenic 2.0 "230 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "160 """"Chromium 0.49 N-02, N-03 "21 """"Cobalt 0.49 "47 """"Copper 0.98 "11 """"Lead 0.49 "0.74 """"Molybdenum 0.49 "190 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "62 """"Vanadium 2.0 "72 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B05/28/21 13:34mg/L B1E08292Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:20mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 12 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M4.2 B1E0737 05/26/21 16:26mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )118 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M350B1E069605/25/21 15:12mg/kg 1TPH Diesel (C13-C22)10 "55 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )112 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 13 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 16:11mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 14 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 16:11mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )102 %Surrogate: Dibromofluoromethane """( 65 - 128 )103 %Surrogate: Toluene-d8 """( 75 - 121 )97 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 15 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-04 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:10mg/kg B1E06941Mercury0.090 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:26mg/kg B1E06931Antimony2.4 "10 """"Arsenic 1.9 "290 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "710 """"Chromium 0.48 N-02, N-03 "47 """"Cobalt 0.48 "52 """"Copper 0.96 "13 """"Lead 0.48 "1.2 """"Molybdenum 0.48 "1900 """"Nickel 0.48 N-02 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "77 """"Vanadium 1.9 "83 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.11 B1E0829 05/28/21 13:37mg/L 2Chromium0.10 "0.37 """"Nickel 0.10 B-02 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:23mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 16 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M0.76 B1E0737 05/26/21 17:18mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )101 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M71B1E069605/25/21 13:41mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )106 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 17 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 16:38mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 18 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 16:38mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )100 %Surrogate: Dibromofluoromethane """( 65 - 128 )101 %Surrogate: Toluene-d8 """( 75 - 121 )97 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 19 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-05 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A1.4 B1E0694 05/25/21 14:12mg/kg 1Mercury0.092 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:13mg/kg B1E06931Antimony2.5 "6.1 """"Arsenic 2.0 "220 """"Barium 1.0 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "140 """"Chromium 0.50 N-02, N-03 "21 """"Cobalt 0.50 "46 """"Copper 1.0 "19 """"Lead 0.50 "0.57 """"Molybdenum 0.50 "180 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "54 """"Vanadium 2.0 "87 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.18 B1E0829 05/28/21 13:39mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:25mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 20 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.3 B1E0737 05/26/21 19:53mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )107 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M390B1E069605/25/21 14:49mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )105 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 21 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 17:05mg/kg B1E06971000Benzene1.3 ND """ ""Bromobenzene 1.3 ND """ ""Bromochloromethane 1.3 ND """ ""Bromodichloromethane 1.3 ND """ ""Bromoform 1.3 ND """ ""Bromomethane 1.3 ND """ ""n-Butylbenzene 1.3 ND """ ""sec-Butylbenzene 1.3 ND """ ""tert-Butylbenzene 1.3 ND """ ""Carbon tetrachloride 1.3 ND """ ""Chlorobenzene 1.3 ND """ ""Chloroethane 1.3 ND """ ""Chloroform 1.3 ND """ ""Chloromethane 1.3 ND """ ""2-Chlorotoluene 1.3 ND """ ""4-Chlorotoluene 1.3 ND """ ""Dibromochloromethane 1.3 ND """ ""1,2-Dibromo-3-chloropropane 1.3 ND """ ""1,2-Dibromoethane (EDB)1.3 ND """ ""Dibromomethane 1.3 ND """ ""1,2-Dichlorobenzene 1.3 ND """ ""1,3-Dichlorobenzene 1.3 ND """ ""1,4-Dichlorobenzene 1.3 ND """ ""Dichlorodifluoromethane 1.3 ND """ ""1,1-Dichloroethane 1.3 ND """ ""1,2-Dichloroethane 1.3 ND """ ""1,1-Dichloroethene 1.3 ND """ ""cis-1,2-Dichloroethene 1.3 ND """ ""trans-1,2-Dichloroethene 1.3 ND """ ""1,2-Dichloropropane 1.3 ND """ ""1,3-Dichloropropane 1.3 ND """ ""2,2-Dichloropropane 1.3 ND """ ""1,1-Dichloropropene 1.3 ND """ ""cis-1,3-Dichloropropene 1.3 ND """ ""trans-1,3-Dichloropropene 1.3 ND """ ""Ethylbenzene 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 22 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 17:05mg/kg B1E06971000Hexachlorobutadiene1.3 ND """ ""4-Isopropyl Toluene 1.3 ND """ ""Isopropylbenzene 1.3 ND """ ""Methylene chloride 1.3 ND """ ""Naphthalene 1.3 ND """ ""n-Propylbenzene 1.3 ND """ ""Styrene 1.3 ND """ ""1,1,1,2-Tetrachloroethane 1.3 ND """ ""1,1,2,2-Tetrachloroethane 1.3 ND """ ""Tetrachloroethene (PCE)1.3 ND """ ""Toluene 1.3 ND """ ""1,2,3-Trichlorobenzene 1.3 ND """ ""1,2,4-Trichlorobenzene 1.3 ND """ ""1,1,1-Trichloroethane 1.3 ND """ ""1,1,2-Trichloroethane 1.3 ND """ ""Trichloroethene (TCE)1.3 ND """ ""Trichlorofluoromethane 1.3 ND """ ""1,2,3-Trichloropropane 1.3 ND """ ""1,2,4-Trimethylbenzene 1.3 ND """ ""1,3,5-Trimethylbenzene 1.3 ND """ ""Vinyl chloride 1.3 ND """ ""Xylenes (total)1.3 """( 74 - 122 )102 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )98 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 23 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-06 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.23 B1E0694 05/25/21 14:14mg/kg 1Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:37mg/kg B1E06931Antimony2.5 "4.9 """"Arsenic 2.0 "230 """"Barium 0.99 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "150 """"Chromium 0.50 N-02, N-03 "25 """"Cobalt 0.50 "49 """"Copper 0.99 "41 """"Lead 0.50 "0.69 """"Molybdenum 0.50 "190 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 0.99 "60 """"Vanadium 2.0 "82 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.15 B1E0829 05/28/21 13:42mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:28mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 24 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M1.5 B1E0737 05/26/21 20:45mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )115 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M370B1E069605/25/21 14:49mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )102 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 25 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 17:33mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 26 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 17:33mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 "2.8 """"Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )99 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )96 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 27 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-07 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.19 B1E0694 05/25/21 14:16mg/kg 1Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:40mg/kg B1E06931Antimony2.5 "4.6 """"Arsenic 2.0 "180 """"Barium 0.99 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "150 """"Chromium 0.49 N-02, N-03 "19 """"Cobalt 0.49 "40 """"Copper 0.99 "24 """"Lead 0.49 ND """ ""Molybdenum 0.49 "150 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "50 """"Vanadium 2.0 "77 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.19 B1E0829 05/28/21 13:45mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:30mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 28 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 28 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.2 B1E0737 05/26/21 21:36mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )108 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M320B1E069605/25/21 15:12mg/kg 1TPH Diesel (C13-C22)9.9 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )95 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 29 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 29 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 18:00mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 30 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 18:00mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 "2.3 """"Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )100 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )98 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 31 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-08 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:18mg/kg B1E06941Mercury0.098 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:42mg/kg B1E06931Antimony2.5 "5.0 """"Arsenic 2.0 "140 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "160 """"Chromium 0.49 N-02, N-03 "23 """"Cobalt 0.49 "45 """"Copper 0.98 "14 """"Lead 0.49 ND """ ""Molybdenum 0.49 "190 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "50 """"Vanadium 2.0 "71 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.17 B1E0829 05/28/21 13:47mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:40mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 32 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.1 B1E0737 05/26/21 22:28mg/kg 1TPH Gasoline (C5-C12)0.49 D-04 """( 39 - 157 )119 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M560B1E069605/25/21 14:26mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )120 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 33 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 33 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 18:28mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 34 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 34 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 18:28mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )99 %Surrogate: Dibromofluoromethane """( 65 - 128 )101 %Surrogate: Toluene-d8 """( 75 - 121 )96 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 35 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 35 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0694 - EPA 7471A Prep[TOC] Batch B1E0694 - EPA 7471A Preparation: EPA 7471A Prep 05/25/21 07:50 Blank (B1E0694-BLK1) [TOC_3]Blank (B1E0694-BLK1)[TOC] Analyzed: 05/25/21 13:31 Mercury mg/kgND0.10 LCS (B1E0694-BS1) [TOC_3]LCS (B1E0694-BS1)[TOC] Analyzed: 05/25/21 13:27 Mercury mg/kg0.840 0.10 0.833 85-115101 LCS Dup (B1E0694-BSD1) [TOC_3]LCS Dup (B1E0694-BSD1)[TOC] Analyzed: 05/25/21 13:29 Mercury mg/kg0.849 0.10 0.833 2085-115102 1 Duplicate (B1E0694-DUP1)Source: 2103193-05 [TOC_3]Duplicate (B1E0694-DUP1)[TOC] Analyzed: 05/25/21 13:47 Mercury mg/kg0.216 0.18 1.87 20 QR-04159 Matrix Spike (B1E0694-MS1)Source: 2103193-05 [TOC_3]Matrix Spike (B1E0694-MS1)[TOC] Analyzed: 05/25/21 13:51 Mercury mg/kg1.04 0.093 0.776 1.87 QM-0775-125NR Matrix Spike Dup (B1E0694-MSD1)Source: 2103193-05 [TOC_3]Matrix Spike Dup (B1E0694-MSD1)[TOC] Analyzed: 05/25/21 13:53 Mercury mg/kg1.68 0.090 0.751 1.87 20 QM-07, QR-04 75-125NR 47 Post Spike (B1E0694-PS1)Source: 2103193-02 [TOC_3]Post Spike (B1E0694-PS1)[TOC] Analyzed: 05/25/21 15:19 Mercury ug/L5.28 5.00 0.114 85-115103 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 36 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 36 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0693 - EPA 3050B[TOC] Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Blank (B1E0693-BLK1) [TOC_3]Blank (B1E0693-BLK1)[TOC] Analyzed: 05/25/21 14:02 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1E0693-BS1) [TOC_3]LCS (B1E0693-BS1)[TOC] Analyzed: 05/25/21 14:45 Antimony mg/kg99.7 2.5 100 80-120100 Arsenic "99.6 2.0 100 80-120100 Barium "102 1.0 100 80-120102 Beryllium "98.2 0.50 100 80-12098 Cadmium "100 0.25 100 80-120100 Chromium "99.5 0.50 100 80-120100 Cobalt "101 0.50 100 80-120101 Copper "101 1.0 100 80-120101 Lead "102 0.50 100 80-120102 Molybdenum "97.8 0.50 100 80-12098 Nickel "101 0.50 100 80-120101 Selenium "99.0 2.0 100 80-12099 Silver "4.96 0.50 5.00 80-12099 Thallium "102 1.0 100 80-120102 Vanadium "97.6 2.0 100 80-12098 Zinc "100 2.0 100 80-120100 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 37 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 37 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 LCS Dup (B1E0693-BSD1) [TOC_3]LCS Dup (B1E0693-BSD1)[TOC] Analyzed: 05/25/21 14:47 Antimony mg/kg1002.5 100 2080-120100 0.5 Arsenic "99.7 2.0 100 2080-120100 0.1 Barium "101 1.0 100 2080-120101 0.05 Beryllium "98.5 0.50 100 2080-12098 0.3 Cadmium "100 0.25 100 2080-120100 0.2 Chromium "99.4 0.50 100 2080-12099 0.2 Cobalt "101 0.50 100 2080-120101 0.05 Copper "100 1.0 100 2080-120100 0.2 Lead "102 0.50 100 2080-120102 0.1 Molybdenum "98.4 0.50 100 2080-12098 0.6 Nickel "102 0.50 100 2080-120102 0.1 Selenium "100 2.0 100 2080-120100 1 Silver "4.96 0.50 5.00 2080-12099 0 Thallium "102 1.0 100 2080-120102 0.4 Vanadium "97.0 2.0 100 2080-12097 0.7 Zinc "100 2.0 100 2080-120100 0.2 Duplicate (B1E0693-DUP1)Source: 2103212-05 [TOC_3]Duplicate (B1E0693-DUP1)[TOC] Analyzed: 05/25/21 14:15 Antimony mg/kgND2.4 ND 20 Arsenic "5.18 1.9 6.10 2016 Barium "205 0.97 218 206 Beryllium "0.408 0.49 0.435 206 Cadmium "ND 0.24 ND 20 Chromium "154 0.49 144 207 Cobalt "22.3 0.49 20.9 206 Copper "48.8 0.97 46.3 205 Lead "17.9 0.49 19.3 208 Molybdenum "0.510 0.49 0.574 2012 Nickel "196 0.49 179 209 Selenium "ND 1.9 ND 20 Silver "ND 0.49 ND 20 Thallium "ND 0.97 ND 20 Vanadium "52.3 1.9 54.0 203 Zinc "69.6 1.9 87.4 20 QR-0423 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 38 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 38 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Matrix Spike (B1E0693-MS1)Source: 2103212-05 [TOC_3]Matrix Spike (B1E0693-MS1)[TOC] Analyzed: 05/25/21 13:50 Antimony mg/kg13.1 2.4 97.9 ND 10-11613 Arsenic "101 2.0 97.9 6.10 77-12196 Barium "226 0.98 97.9 218 QM-0730-1698 Beryllium "95.2 0.49 97.9 0.435 86-11197 Cadmium "90.0 0.24 97.9 ND 81-11292 Chromium "218 0.49 97.9 144 75-12976 Cobalt "109 0.49 97.9 20.9 71-12190 Copper "146 0.98 97.9 46.3 68-135102 Lead "107 0.49 97.9 19.3 72-12190 Molybdenum "35.0 0.49 97.9 0.574 QM-0770-11235 Nickel "230 0.49 97.9 179 QM-0773-12152 Selenium "85.9 2.0 97.9 ND 76-11688 Silver "4.79 0.49 4.90 ND 54-13298 Thallium "85.9 0.98 97.9 ND 64-12088 Vanadium "138 2.0 97.9 54.0 78-12486 Zinc "162 2.0 97.9 87.4 50-14377 Matrix Spike Dup (B1E0693-MSD1)Source: 2103212-05 [TOC_3]Matrix Spike Dup (B1E0693-MSD1)[TOC] Analyzed: 05/25/21 13:52 Antimony mg/kg9.34 2.4 95.8 ND 20 QR-0210-11610 33 Arsenic "96.6 1.9 95.8 6.10 2077-12195 4 Barium "295 0.96 95.8 218 20 QR-0230-16980 26 Beryllium "91.2 0.48 95.8 0.435 2086-11195 4 Cadmium "85.1 0.24 95.8 ND 2081-11289 6 Chromium "271 0.48 95.8 144 20 QM-07, QR-04 75-129133 22 Cobalt "113 0.48 95.8 20.9 2071-12196 3 Copper "140 0.96 95.8 46.3 2068-13597 4 Lead "104 0.48 95.8 19.3 2072-12188 3 Molybdenum "32.4 0.48 95.8 0.574 20 QM-0770-11233 8 Nickel "319 0.48 95.8 179 20 QM-07, QR-04 73-121146 32 Selenium "79.5 1.9 95.8 ND 2076-11683 8 Silver "4.59 0.48 4.79 ND 2054-13296 4 Thallium "79.5 0.96 95.8 ND 2064-12083 8 Vanadium "147 1.9 95.8 54.0 2078-12497 6 Zinc "158 1.9 95.8 87.4 2050-14374 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 39 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 39 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Post Spike (B1E0693-PS1)Source: 2103212-05 [TOC_3]Post Spike (B1E0693-PS1)[TOC] Analyzed: 05/25/21 14:08 Antimony mg/L1.98 2.00 0.00347 75-12599 Arsenic "2.07 2.00 0.121 75-12598 Barium "6.39 2.00 4.34 75-125103 Beryllium "1.96 2.00 0.00863 75-12598 Cadmium "1.83 2.00 -0.0417 75-12591 Chromium "4.75 2.00 2.85 75-12595 Cobalt "2.27 2.00 0.414 75-12593 Copper "2.88 2.00 0.919 75-12598 Lead "2.24 2.00 0.384 75-12593 Molybdenum "1.97 2.00 0.0114 75-12598 Nickel "5.42 2.00 3.56 75-12593 Selenium "1.80 2.00 -0.120 75-12590 Silver "0.0954 0.100 -0.00119 75-12595 Thallium "1.78 2.00 -0.0164 75-12589 Vanadium "3.01 2.00 1.07 75-12597 Zinc "3.61 2.00 1.74 75-12594 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 40 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 40 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: STLC Metals by ICP - Quality Control[TOC_1]STLC Metals by IC Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0829 - EPA 3010A Leachate[TOC] Batch B1E0829 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 05/28/21 09:36 Blank (B1E0829-BLK1) [TOC_3]Blank (B1E0829-BLK1)[TOC] Analyzed: 05/28/21 12:56 Chromium mg/LND0.050 Nickel "ND 0.050 LCS (B1E0829-BS1) [TOC_3]LCS (B1E0829-BS1)[TOC] Analyzed: 05/28/21 13:01 Chromium mg/L10.5 0.050 10.0 80-120105 Nickel "10.4 0.050 10.0 80-120104 LCS Dup (B1E0829-BSD1) [TOC_3]LCS Dup (B1E0829-BSD1)[TOC] Analyzed: 05/28/21 13:03 Chromium mg/L10.1 0.050 10.0 2080-120101 4 Nickel "10.1 0.050 10.0 2080-120101 3 Duplicate (B1E0829-DUP1)Source: 2103212-01 [TOC_3]Duplicate (B1E0829-DUP1)[TOC] Analyzed: 05/28/21 13:21 Chromium mg/L0.0790 0.10 0.0810 202 Nickel "0.329 0.10 0.345 205 Leach Fluid Blank (B1E0829-LBK1) [TOC_3]Leach Fluid Blank (B1E0829-LBK1)[TOC] Analyzed: 05/28/21 12:58 Chromium mg/LND0.050 Nickel "0.0385 0.050 B-02 Matrix Spike (B1E0829-MS1)Source: 2103212-01 [TOC_3]Matrix Spike (B1E0829-MS1)[TOC] Analyzed: 05/28/21 13:10 Chromium mg/L10.0 0.10 10.0 0.0810 82-11999 Nickel "10.0 0.10 10.0 0.345 80-11697 Matrix Spike Dup (B1E0829-MSD1)Source: 2103212-01 [TOC_3]Matrix Spike Dup (B1E0829-MSD1)[TOC] Analyzed: 05/28/21 13:12 Chromium mg/L10.3 0.10 10.0 0.0810 2082-119102 3 Nickel "10.3 0.10 10.0 0.345 2080-11699 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 41 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 41 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: TCLP Metals by ICP - Quality Control[TOC_1]TCL Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0794 - EPA 3010A Leachate[TOC] Batch B1E0794 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 05/27/21 10:55 Blank (B1E0794-BLK1) [TOC_3]Blank (B1E0794-BLK1)[TOC] Analyzed: 05/27/21 18:35 Chromium mg/LND0.050 LCS (B1E0794-BS1) [TOC_3]LCS (B1E0794-BS1)[TOC] Analyzed: 05/27/21 18:20 Chromium mg/L10.0 0.050 10.0 80-120100 LCS Dup (B1E0794-BSD1) [TOC_3]LCS Dup (B1E0794-BSD1)[TOC] Analyzed: 05/27/21 18:22 Chromium mg/L9.84 0.050 10.0 2080-12098 2 Duplicate (B1E0794-DUP1)Source: 2102854-01 [TOC_3]Duplicate (B1E0794-DUP1)[TOC] Analyzed: 05/27/21 18:52 Chromium mg/LND0.050 ND 20 Leach Fluid Blank (B1E0794-LBK1) [TOC_3]Leach Fluid Blank (B1E0794-LBK1)[TOC] Analyzed: 05/27/21 18:37 Chromium mg/LND0.050 Leach Fluid Blank (B1E0794-LBK2)Analyzed: 05/27/21 18:40 Chromium mg/LND0.050 Leach Fluid Blank (B1E0794-LBK3)Analyzed: 05/27/21 18:42 Chromium mg/LND0.050 Matrix Spike (B1E0794-MS1)Source: 2102854-01 [TOC_3]Matrix Spike (B1E0794-MS1)[TOC] Analyzed: 05/27/21 18:25 Chromium mg/L10.2 0.050 10.0 ND 82-119102 Matrix Spike Dup (B1E0794-MSD1)Source: 2102854-01 [TOC_3]Matrix Spike Dup (B1E0794-MSD1)[TOC] Analyzed: 05/27/21 18:45 Chromium mg/L10.2 0.050 10.0 ND 2082-119102 0.6 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 42 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 42 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0737 - EPA 5035/5030B Solid GC[TOC] Batch B1E0737 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/26/21 06:59 Blank (B1E0737-BLK1) [TOC_3]Blank (B1E0737-BLK1)[TOC] Analyzed: 05/26/21 10:49 TPH Gasoline (C5-C12)mg/kgND0.50 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1020.128 LCS (B1E0737-BS1) [TOC_3]LCS (B1E0737-BS1)[TOC] Analyzed: 05/26/21 09:57 TPH Gasoline (C5-C12)mg/kg1.08 0.50 0.994 68-139108 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1170.146 LCS Dup (B1E0737-BSD1) [TOC_3]LCS Dup (B1E0737-BSD1)[TOC] Analyzed: 05/26/21 10:23 TPH Gasoline (C5-C12)mg/kg1.20 0.50 0.998 2068-139120 11 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1230.154 Duplicate (B1E0737-DUP1)Source: 2103210-01RE1 [TOC_3]Duplicate (B1E0737-DUP1)[TOC] Analyzed: 05/26/21 13:04 TPH Gasoline (C5-C12)mg/kgND0.49 ND 20 "0.122 39-157Surrogate: 4-Bromofluorobenzene 990.120 Matrix Spike (B1E0737-MS1)Source: 2103210-01RE1 [TOC_3]Matrix Spike (B1E0737-MS1)[TOC] Analyzed: 05/26/21 23:45 TPH Gasoline (C5-C12)mg/kg0.868 0.48 0.967 ND 10-17190 "0.121 39-157Surrogate: 4-Bromofluorobenzene 1170.142 Matrix Spike Dup (B1E0737-MSD1)Source: 2103210-01RE1 [TOC_3]Matrix Spike Dup (B1E0737-MSD1)[TOC] Analyzed: 05/27/21 00:11 TPH Gasoline (C5-C12)mg/kg0.911 0.50 0.998 ND 2010-17191 5 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1190.149 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 43 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 43 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0696 - EPA 3550C[TOC] Batch B1E0696 - EPA 8015M Preparation: EPA 3550C 05/25/21 08:55 Blank (B1E0696-BLK1) [TOC_3]Blank (B1E0696-BLK1)[TOC] Analyzed: 05/25/21 13:41 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "50.0 65-136Surrogate: o-Terphenyl 8743.3 LCS (B1E0696-BS1) [TOC_3]LCS (B1E0696-BS1)[TOC] Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22)mg/kg51210 499 72-115103 TPH Motor Oil (C23-C40)"473 50 499 74-12695 "49.9 65-136Surrogate: o-Terphenyl 10049.9 LCS Dup (B1E0696-BSD1) [TOC_3]LCS Dup (B1E0696-BSD1)[TOC] Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22)mg/kg48710 500 2072-11597 5 TPH Motor Oil (C23-C40)"459 50 500 2074-12692 3 "50.0 65-136Surrogate: o-Terphenyl 9748.7 Duplicate (B1E0696-DUP1)Source: 2103212-01 [TOC_3]Duplicate (B1E0696-DUP1)[TOC] Analyzed: 05/25/21 14:03 TPH Diesel (C13-C22)mg/kg35.5 9.9 50.9 20 QR-0636 TPH Motor Oil (C23-C40)"ND 50 ND 20 "49.7 65-136Surrogate: o-Terphenyl 8642.6 Matrix Spike (B1E0696-MS1)Source: 2103212-01 [TOC_3]Matrix Spike (B1E0696-MS1)[TOC] Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22)mg/kg50010 498 50.9 46-14790 TPH Motor Oil (C23-C40)"432 50 498 ND 35-17187 "49.8 65-136Surrogate: o-Terphenyl 8944.5 Matrix Spike Dup (B1E0696-MSD1)Source: 2103212-01 [TOC_3]Matrix Spike Dup (B1E0696-MSD1)[TOC] Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22)mg/kg4979.9 497 50.9 2046-14790 0.6 TPH Motor Oil (C23-C40)"432 50 497 ND 2035-17187 0.2 "49.7 65-136Surrogate: o-Terphenyl 8944.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 44 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 44 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0697 - EPA 5035/5030B MEOH[TOC] Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1) [TOC_3]Blank (B1E0697-BLK1)[TOC] Analyzed: 05/25/21 13:26 Benzene mg/kgND0.25 Bromobenzene "ND 0.25 Bromochloromethane "ND 0.25 Bromodichloromethane "ND 0.25 Bromoform "ND 0.25 Bromomethane "ND 0.25 n-Butylbenzene "ND 0.25 sec-Butylbenzene "ND 0.25 tert-Butylbenzene "ND 0.25 Carbon tetrachloride "ND 0.25 Chlorobenzene "ND 0.25 Chloroethane "ND 0.25 Chloroform "ND 0.25 Chloromethane "ND 0.25 2-Chlorotoluene "ND 0.25 4-Chlorotoluene "ND 0.25 Dibromochloromethane "ND 0.25 1,2-Dibromo-3-chloropropane "ND 0.25 1,2-Dibromoethane (EDB)"ND 0.25 Dibromomethane "ND 0.25 1,2-Dichlorobenzene "ND 0.25 1,3-Dichlorobenzene "ND 0.25 1,4-Dichlorobenzene "ND 0.25 Dichlorodifluoromethane "ND 0.25 1,1-Dichloroethane "ND 0.25 1,2-Dichloroethane "ND 0.25 1,1-Dichloroethene "ND 0.25 cis-1,2-Dichloroethene "ND 0.25 trans-1,2-Dichloroethene "ND 0.25 1,2-Dichloropropane "ND 0.25 1,3-Dichloropropane "ND 0.25 2,2-Dichloropropane "ND 0.25 1,1-Dichloropropene "ND 0.25 cis-1,3-Dichloropropene "ND 0.25 trans-1,3-Dichloropropene "ND 0.25 Ethylbenzene "ND 0.25 Hexachlorobutadiene "ND 0.25 4-Isopropyl Toluene "ND 0.25 Isopropylbenzene "ND 0.25 Methylene chloride "ND 0.25 Naphthalene "ND 0.25 n-Propylbenzene "ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 45 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 45 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1)Analyzed: 05/25/21 13:26 Styrene mg/kgND0.25 1,1,1,2-Tetrachloroethane "ND 0.25 1,1,2,2-Tetrachloroethane "ND 0.25 Tetrachloroethene (PCE)"ND 0.25 Toluene "ND 0.25 1,2,3-Trichlorobenzene "ND 0.25 1,2,4-Trichlorobenzene "ND 0.25 1,1,1-Trichloroethane "ND 0.25 1,1,2-Trichloroethane "ND 0.25 Trichloroethene (TCE)"ND 0.25 Trichlorofluoromethane "ND 0.25 1,2,3-Trichloropropane "ND 0.25 1,2,4-Trimethylbenzene "ND 0.25 1,3,5-Trimethylbenzene "ND 0.25 Vinyl chloride "ND 0.25 Xylenes (total)"ND 0.25 "0.0500 74-122Surrogate: Dibromofluoromethane 990.0496 "0.0500 65-128Surrogate: Toluene-d8 1010.0507 "0.0500 75-121Surrogate: 4-Bromofluorobenzene 960.0482 LCS (B1E0697-BS1) [TOC_3]LCS (B1E0697-BS1)[TOC] Analyzed: 05/25/21 11:37 Benzene mg/kg1.80 0.25 1.98 70-13191 Bromobenzene "2.09 0.25 1.98 74-130105 Bromochloromethane "1.77 0.25 1.98 64-13389 Bromodichloromethane "2.12 0.25 1.98 69-137107 Bromoform "2.09 0.25 1.98 55-132105 Bromomethane "1.51 0.25 1.98 10-14276 n-Butylbenzene "2.47 0.25 1.98 64-156125 sec-Butylbenzene "2.46 0.25 1.98 75-155124 tert-Butylbenzene "2.34 0.25 1.98 74-144118 Carbon tetrachloride "1.70 0.25 1.98 67-13586 Chlorobenzene "2.08 0.25 1.98 73-134105 Chloroethane "1.65 0.25 1.98 10-16783 Chloroform "2.01 0.25 1.98 69-124101 Chloromethane "2.46 0.25 1.98 34-136124 2-Chlorotoluene "2.16 0.25 1.98 75-135109 4-Chlorotoluene "2.30 0.25 1.98 70-138116 Dibromochloromethane "2.01 0.25 1.98 67-135102 1,2-Dibromo-3-chloropropane "2.45 0.25 1.98 41-149124 1,2-Dibromoethane (EDB)"1.98 0.25 1.98 68-131100 Dibromomethane "1.92 0.25 1.98 61-14097 1,2-Dichlorobenzene "2.20 0.25 1.98 76-136111 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 46 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 46 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS (B1E0697-BS1)Analyzed: 05/25/21 11:37 1,3-Dichlorobenzene mg/kg2.30 0.25 1.98 76-138116 1,4-Dichlorobenzene "2.23 0.25 1.98 72-132112 Dichlorodifluoromethane "1.51 0.25 1.98 10-15576 1,1-Dichloroethane "1.90 0.25 1.98 63-13996 1,2-Dichloroethane "2.04 0.25 1.98 64-126103 1,1-Dichloroethene "1.79 0.25 1.98 52-16790 cis-1,2-Dichloroethene "1.84 0.25 1.98 70-13593 trans-1,2-Dichloroethene "1.69 0.25 1.98 67-14785 1,2-Dichloropropane "3.19 0.25 1.98 QM-0868-131161 1,3-Dichloropropane "1.91 0.25 1.98 64-12896 2,2-Dichloropropane "2.11 0.25 1.98 63-154107 1,1-Dichloropropene "1.82 0.25 1.98 68-13892 cis-1,3-Dichloropropene "2.08 0.25 1.98 72-134105 trans-1,3-Dichloropropene "2.16 0.25 1.98 69-132109 Ethylbenzene "1.92 0.25 1.98 68-13697 Hexachlorobutadiene "2.24 0.25 1.98 72-198113 4-Isopropyl Toluene "2.40 0.25 1.98 74-150121 Isopropylbenzene "2.21 0.25 1.98 71-149112 Methylene chloride "1.81 0.25 1.98 51-12791 Naphthalene "2.29 0.25 1.98 57-158116 n-Propylbenzene "2.29 0.25 1.98 70-143116 Styrene "2.47 0.25 1.98 68-138124 1,1,1,2-Tetrachloroethane "2.10 0.25 1.98 76-130106 1,1,2,2-Tetrachloroethane "2.18 0.25 1.98 60-136110 Tetrachloroethene (PCE)"1.79 0.25 1.98 73-13891 Toluene "1.99 0.25 1.98 72-128101 1,2,3-Trichlorobenzene "2.47 0.25 1.98 61-166125 1,2,4-Trichlorobenzene "2.43 0.25 1.98 71-158123 1,1,1-Trichloroethane "1.92 0.25 1.98 71-13597 1,1,2-Trichloroethane "2.23 0.25 1.98 64-132113 Trichloroethene (TCE)"1.87 0.25 1.98 74-13994 Trichlorofluoromethane "2.69 0.25 1.98 30-156136 1,2,3-Trichloropropane "2.05 0.25 1.98 67-123104 1,2,4-Trimethylbenzene "2.31 0.25 1.98 68-134117 1,3,5-Trimethylbenzene "2.27 0.25 1.98 71-140114 Vinyl chloride "2.14 0.25 1.98 43-144108 Xylenes (total)"6.81 0.25 5.94 69-138115 "0.0495 74-122Surrogate: Dibromofluoromethane 1030.0512 "0.0495 65-128Surrogate: Toluene-d8 1040.0516 "0.0495 75-121Surrogate: 4-Bromofluorobenzene 940.0467 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 47 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 47 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSD1) [TOC_3]LCS Dup (B1E0697-BSD1)[TOC] Analyzed: 05/25/21 12:04 Benzene mg/kg1.74 0.25 1.99 2070-13187 3 Bromobenzene "2.08 0.25 1.99 2074-130104 0.4 Bromochloromethane "1.69 0.25 1.99 2064-13385 5 Bromodichloromethane "2.14 0.25 1.99 2069-137107 0.8 Bromoform "2.06 0.25 1.99 2055-132103 1 Bromomethane "1.50 0.25 1.99 2010-14275 1 n-Butylbenzene "2.33 0.25 1.99 2064-156117 6 sec-Butylbenzene "2.25 0.25 1.99 2075-155113 9 tert-Butylbenzene "2.17 0.25 1.99 2074-144109 8 Carbon tetrachloride "1.60 0.25 1.99 2067-13580 6 Chlorobenzene "2.07 0.25 1.99 2073-134104 0.3 Chloroethane "1.70 0.25 1.99 2010-16785 3 Chloroform "1.93 0.25 1.99 2069-12497 4 Chloromethane "2.16 0.25 1.99 2034-136108 13 2-Chlorotoluene "2.05 0.25 1.99 2075-135103 5 4-Chlorotoluene "2.15 0.25 1.99 2070-138108 7 Dibromochloromethane "2.11 0.25 1.99 2067-135106 5 1,2-Dibromo-3-chloropropane "2.68 0.25 1.99 2041-149135 9 1,2-Dibromoethane (EDB)"2.01 0.25 1.99 2068-131101 1 Dibromomethane "1.92 0.25 1.99 2061-14096 0.08 1,2-Dichlorobenzene "2.20 0.25 1.99 2076-136110 0.4 1,3-Dichlorobenzene "2.15 0.25 1.99 2076-138108 7 1,4-Dichlorobenzene "2.13 0.25 1.99 2072-132107 5 Dichlorodifluoromethane "1.50 0.25 1.99 2010-15575 0.5 1,1-Dichloroethane "1.83 0.25 1.99 2063-13992 4 1,2-Dichloroethane "2.01 0.25 1.99 2064-126101 2 1,1-Dichloroethene "1.73 0.25 1.99 2052-16787 4 cis-1,2-Dichloroethene "1.71 0.25 1.99 2070-13586 8 trans-1,2-Dichloroethene "1.64 0.25 1.99 2067-14782 3 1,2-Dichloropropane "1.94 0.25 1.99 20 QR-0468-13197 49 1,3-Dichloropropane "2.05 0.25 1.99 2064-128103 7 2,2-Dichloropropane "2.00 0.25 1.99 2063-154100 5 1,1-Dichloropropene "1.75 0.25 1.99 2068-13888 4 cis-1,3-Dichloropropene "1.98 0.25 1.99 2072-134100 5 trans-1,3-Dichloropropene "2.25 0.25 1.99 2069-132113 4 Ethylbenzene "2.05 0.25 1.99 2068-136103 7 Hexachlorobutadiene "2.12 0.25 1.99 2072-198107 5 4-Isopropyl Toluene "2.23 0.25 1.99 2074-150112 7 Isopropylbenzene "2.24 0.25 1.99 2071-149112 1 Methylene chloride "1.79 0.25 1.99 2051-12790 1 Naphthalene "2.10 0.25 1.99 2057-158106 8 n-Propylbenzene "2.12 0.25 1.99 2070-143106 8 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 48 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 48 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSD1)Analyzed: 05/25/21 12:04 Styrene mg/kg2.23 0.25 1.99 2068-138112 10 1,1,1,2-Tetrachloroethane "2.18 0.25 1.99 2076-130109 3 1,1,2,2-Tetrachloroethane "2.11 0.25 1.99 2060-136106 3 Tetrachloroethene (PCE)"1.81 0.25 1.99 2073-13891 0.8 Toluene "1.83 0.25 1.99 2072-12892 9 1,2,3-Trichlorobenzene "2.32 0.25 1.99 2061-166116 6 1,2,4-Trichlorobenzene "2.35 0.25 1.99 2071-158118 3 1,1,1-Trichloroethane "1.86 0.25 1.99 2071-13593 3 1,1,2-Trichloroethane "2.18 0.25 1.99 2064-132109 2 Trichloroethene (TCE)"1.82 0.25 1.99 2074-13991 3 Trichlorofluoromethane "2.59 0.25 1.99 2030-156130 4 1,2,3-Trichloropropane "1.96 0.25 1.99 2067-12398 5 1,2,4-Trimethylbenzene "2.16 0.25 1.99 2068-134108 7 1,3,5-Trimethylbenzene "2.13 0.25 1.99 2071-140107 6 Vinyl chloride "2.12 0.25 1.99 2043-144107 0.6 Xylenes (total)"6.17 0.25 5.98 2069-138103 10 "0.0498 74-122Surrogate: Dibromofluoromethane 1030.0512 "0.0498 65-128Surrogate: Toluene-d8 1020.0510 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 1000.0499 Duplicate (B1E0697-DUP1)Source: 2103210-01 [TOC_3]Duplicate (B1E0697-DUP1)[TOC] Analyzed: 05/25/21 14:48 Benzene mg/kgND1.2 ND 20 Bromobenzene "ND 1.2 ND 20 Bromochloromethane "ND 1.2 ND 20 Bromodichloromethane "ND 1.2 ND 20 Bromoform "ND 1.2 ND 20 Bromomethane "ND 1.2 ND 20 n-Butylbenzene "ND 1.2 ND 20 sec-Butylbenzene "ND 1.2 ND 20 tert-Butylbenzene "ND 1.2 ND 20 Carbon tetrachloride "ND 1.2 ND 20 Chlorobenzene "ND 1.2 ND 20 Chloroethane "ND 1.2 ND 20 Chloroform "ND 1.2 ND 20 Chloromethane "ND 1.2 ND 20 2-Chlorotoluene "ND 1.2 ND 20 4-Chlorotoluene "ND 1.2 ND 20 Dibromochloromethane "ND 1.2 ND 20 1,2-Dibromo-3-chloropropane "ND 1.2 ND 20 1,2-Dibromoethane (EDB)"ND 1.2 ND 20 Dibromomethane "ND 1.2 ND 20 1,2-Dichlorobenzene "ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 49 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 49 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Duplicate (B1E0697-DUP1)Source: 2103210-01 Analyzed: 05/25/21 14:48 1,3-Dichlorobenzene mg/kgND1.2 ND 20 1,4-Dichlorobenzene "ND 1.2 ND 20 Dichlorodifluoromethane "ND 1.2 ND 20 1,1-Dichloroethane "ND 1.2 ND 20 1,2-Dichloroethane "ND 1.2 ND 20 1,1-Dichloroethene "ND 1.2 ND 20 cis-1,2-Dichloroethene "ND 1.2 ND 20 trans-1,2-Dichloroethene "ND 1.2 ND 20 1,2-Dichloropropane "ND 1.2 ND 20 1,3-Dichloropropane "ND 1.2 ND 20 2,2-Dichloropropane "ND 1.2 ND 20 1,1-Dichloropropene "ND 1.2 ND 20 cis-1,3-Dichloropropene "ND 1.2 ND 20 trans-1,3-Dichloropropene "ND 1.2 ND 20 Ethylbenzene "ND 1.2 ND 20 Hexachlorobutadiene "ND 1.2 ND 20 4-Isopropyl Toluene "ND 1.2 ND 20 Isopropylbenzene "ND 1.2 ND 20 Methylene chloride "ND 1.2 ND 20 Naphthalene "ND 1.2 ND 20 n-Propylbenzene "ND 1.2 ND 20 Styrene "ND 1.2 ND 20 1,1,1,2-Tetrachloroethane "ND 1.2 ND 20 1,1,2,2-Tetrachloroethane "ND 1.2 ND 20 Tetrachloroethene (PCE)"ND 1.2 ND 20 Toluene "ND 1.2 ND 20 1,2,3-Trichlorobenzene "ND 1.2 ND 20 1,2,4-Trichlorobenzene "ND 1.2 ND 20 1,1,1-Trichloroethane "ND 1.2 ND 20 1,1,2-Trichloroethane "ND 1.2 ND 20 Trichloroethene (TCE)"ND 1.2 ND 20 Trichlorofluoromethane "ND 1.2 ND 20 1,2,3-Trichloropropane "ND 1.2 ND 20 1,2,4-Trimethylbenzene "ND 1.2 ND 20 1,3,5-Trimethylbenzene "ND 1.2 ND 20 Vinyl chloride "ND 1.2 ND 20 Xylenes (total)"ND 1.2 ND 20 "0.0494 74-122Surrogate: Dibromofluoromethane 1020.0503 "0.0494 65-128Surrogate: Toluene-d8 1040.0514 "0.0494 75-121Surrogate: 4-Bromofluorobenzene 970.0478 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 50 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 50 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1)Source: 2103212-01 [TOC_3]Matrix Spike (B1E0697-MS1)[TOC] Analyzed: 05/25/21 19:22 Benzene mg/kg8.97 1.2 9.94 ND 37-14590 Bromobenzene "11.0 1.2 9.94 ND 29-147111 Bromochloromethane "9.22 1.2 9.94 ND 40-14593 Bromodichloromethane "10.9 1.2 9.94 ND 39-153110 Bromoform "10.7 1.2 9.94 ND 32-143108 Bromomethane "10.3 1.2 9.94 ND 10-141104 n-Butylbenzene "11.6 1.2 9.94 ND 10-162117 sec-Butylbenzene "12.2 1.2 9.94 ND 14-168123 tert-Butylbenzene "11.8 1.2 9.94 ND 21-159119 Carbon tetrachloride "8.48 1.2 9.94 ND 28-14885 Chlorobenzene "10.9 1.2 9.94 ND 32-148110 Chloroethane "12.6 1.2 9.94 ND 11-166127 Chloroform "9.94 1.2 9.94 ND 40-139100 Chloromethane "10.4 1.2 9.94 ND 18-135105 2-Chlorotoluene "10.8 1.2 9.94 ND 25-151108 4-Chlorotoluene "11.3 1.2 9.94 ND 22-150114 Dibromochloromethane "10.2 1.2 9.94 ND 40-147103 1,2-Dibromo-3-chloropropane "12.4 1.2 9.94 ND 25-158125 1,2-Dibromoethane (EDB)"10.1 1.2 9.94 ND 38-147102 Dibromomethane "9.74 1.2 9.94 ND 39-15098 1,2-Dichlorobenzene "11.4 1.2 9.94 ND 24-154115 1,3-Dichlorobenzene "11.3 1.2 9.94 ND 21-153114 1,4-Dichlorobenzene "10.9 1.2 9.94 ND 21-146110 Dichlorodifluoromethane "6.32 1.2 9.94 ND 10-14964 1,1-Dichloroethane "9.32 1.2 9.94 ND 34-15194 1,2-Dichloroethane "9.93 1.2 9.94 ND 40-137100 1,1-Dichloroethene "7.41 1.2 9.94 ND 21-17274 cis-1,2-Dichloroethene "8.87 1.2 9.94 ND 38-14789 trans-1,2-Dichloroethene "8.06 1.2 9.94 ND 30-16081 1,2-Dichloropropane "10.0 1.2 9.94 ND 39-146101 1,3-Dichloropropane "9.84 1.2 9.94 ND 39-14199 2,2-Dichloropropane "9.05 1.2 9.94 ND 26-14991 1,1-Dichloropropene "9.03 1.2 9.94 ND 28-15091 cis-1,3-Dichloropropene "9.92 1.2 9.94 ND 34-149100 trans-1,3-Dichloropropene "11.0 1.2 9.94 ND 36-143111 Ethylbenzene "10.8 1.2 9.94 ND 23-150109 Hexachlorobutadiene "11.4 1.2 9.94 ND 10-192115 4-Isopropyl Toluene "11.9 1.2 9.94 ND 11-165120 Isopropylbenzene "11.7 1.2 9.94 ND 17-166118 Methylene chloride "8.61 1.2 9.94 ND 28-13587 Naphthalene "12.4 1.2 9.94 ND 10-174124 n-Propylbenzene "11.3 1.2 9.94 ND 16-156114 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 51 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 51 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1)Source: 2103212-01 Analyzed: 05/25/21 19:22 Styrene mg/kg11.5 1.2 9.94 ND 24-154116 1,1,1,2-Tetrachloroethane "11.1 1.2 9.94 ND 38-149111 1,1,2,2-Tetrachloroethane "10.7 1.2 9.94 ND 22-164107 Tetrachloroethene (PCE)"9.37 1.2 9.94 ND 25-15394 Toluene "10.4 1.2 9.94 ND 26-149105 1,2,3-Trichlorobenzene "12.7 1.2 9.94 ND 10-163128 1,2,4-Trichlorobenzene "12.4 1.2 9.94 ND 10-162124 1,1,1-Trichloroethane "9.87 1.2 9.94 ND 34-14999 1,1,2-Trichloroethane "11.3 1.2 9.94 ND 25-175113 Trichloroethene (TCE)"9.24 1.2 9.94 ND 25-17093 Trichlorofluoromethane "12.0 1.2 9.94 ND 19-155121 1,2,3-Trichloropropane "9.81 1.2 9.94 ND 32-16599 1,2,4-Trimethylbenzene "11.7 1.2 9.94 ND 15-150118 1,3,5-Trimethylbenzene "11.4 1.2 9.94 ND 10-158114 Vinyl chloride "11.2 1.2 9.94 ND 22-148112 Xylenes (total)"32.3 1.2 29.8 ND 22-153108 "0.0497 74-122Surrogate: Dibromofluoromethane 1020.0508 "0.0497 65-128Surrogate: Toluene-d8 1020.0509 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 1000.0499 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 52 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 52 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid STLC Metals by ICP STLC/EPA 6010B OEC, CA-ELAP6010B STLC Chromium Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Nickel Water STLC Metals Extraction STLC OEC, InternalSTLC Metals Extraction Solid TCLP Metals by ICP EPA 1311/EPA 6010B OEC, CA-ELAP6010B TCLP Chromium Water TCLP Metals Extraction EPA 1311 OEC, CA-ELAPTCLP Metals Extraction Solid Total Metals by CVAA EPA 7471A OEC, CA-ELAPMercury Total EPA 7471A Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 53 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 53 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Sample Method Summary (Continued) Laboratory & CertificationMethodAnalysisMatrix Total Metals by ICP EPA 6010B OEC, CA-ELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP8260B Full List Solid Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 54 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 54 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL B-02 The method blank contains analyte at a J-flag concentration. D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery and/or RPD values. QM-08 The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. QR-06 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to non-homogenous sample matrix. QC batch accepted based on LCS and/or LCSD recovery and/or RPD values. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out-Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 55 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 55 of 59 File :V:\DATA\MAY21\052521\B0ME2532.DOperator : CMLAcquired : 25 May 2021 2:26 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-01@B1E0696(S) Misc Info : 1@ Vial Number: 300.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2532.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2612.D Operator : RR Acquired : 26 May 2021 1:56 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-01RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 12 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2612.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2529.DOperator : CMLAcquired : 25 May 2021 2:03 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-02@B1E0696(S) Misc Info : 1@ Vial Number: 270.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2529.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2614.D Operator : RR Acquired : 26 May 2021 3:34 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-02RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 14 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 100000 105000 110000 Time Response_GOME2614.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2535.DOperator : CMLAcquired : 25 May 2021 3:12 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-03@B1E0696(S) Misc Info : 1@ Vial Number: 330.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2535.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2616.D Operator : RR Acquired : 26 May 2021 4:26 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-03RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 16 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2616.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2527.DOperator : CMLAcquired : 25 May 2021 1:41 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-04@B1E0696(S) Misc Info : 1@ Vial Number: 250.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07TimeResponse_Signal: B0ME2527.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2618.D Operator : RR Acquired : 26 May 2021 5:18 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-04RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 18 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2618.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2533.DOperator : CMLAcquired : 25 May 2021 2:49 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-05@B1E0696(S) Misc Info : 1@ Vial Number: 310.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME2533.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2624.D Operator : RR Acquired : 26 May 2021 7:53 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-05RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 24 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2624.D\FID1A File :V:\DATA\MAY21\052521\B0ME2534.DOperator : CMLAcquired : 25 May 2021 2:49 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-06@B1E0696(S) Misc Info : 1@ Vial Number: 320.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2534.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2626.D Operator : RR Acquired : 26 May 2021 8:45 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-06RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 26 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOME2626.D\FID1A File :V:\DATA\MAY21\052521\B0ME2536.DOperator : CMLAcquired : 25 May 2021 3:12 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-07@B1E0696(S) Misc Info : 1@ Vial Number: 340.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07TimeResponse_Signal: B0ME2536.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2628.D Operator : RR Acquired : 26 May 2021 9:36 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-07RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 28 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2628.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2531.DOperator : CMLAcquired : 25 May 2021 2:26 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-08@B1E0696(S) Misc Info : 1@ Vial Number: 290.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07TimeResponse_Signal: B0ME2531.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2630.D Operator : RR Acquired : 26 May 2021 10:28 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-08RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 30 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2630.D\FID1A Page 56 of 59 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLDYRDeluikuieiheluikuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 57 of 59 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG5HFHLSW/RJLQ%\-9=5HFHLSW5HYLHZHG%\’$Page 58 of 59 STLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr, Ni & TCLP Crall added at 5/25/21; SPPage 59 of 59