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HomeMy WebLinkAbout2021-06-09 Analyticals[TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2103479 Report Date: June 09, 2021 16:44 NHC SLO, 2640 Broad StreetNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: This laboratory is accredited in accordance with the recognised International Standard ISO /IEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-IAF CommuniquØ dated April 2017) 307 Roemer Way, Suite 300 Santa Maria, CA 93454 client.oec.com\reports CA-ELAP 2438, TNI 02666 TNI 2016 & ISO/IEC 17025:2017 www.oecusa.com Fax: Main: (805) 925-3376 (805) 922-4772 Page 1 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix Bottom East @ 12’2103479-01 06/03/2021 11:50 06/04/2021 12:50Solid Solid Bottom West @ 12’2103479-02 06/03/2021 11:55 06/04/2021 12:50Solid Solid [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 06/04/2021 16:24B1F0145 STLC Metals by ICP 6010B STLC 06/09/2021 08:56B1F0261 STLC Metals Extraction STLC Metals Extraction 06/07/2021 16:29B1F0229 Total Metals by CVAA Mercury Total EPA 7471A 06/07/2021 07:40B1F0194 Total Metals by ICP 6010B Total 06/07/2021 08:26B1F0197 Volatile Organic Compounds by GC/MS 8260B Full List 06/04/2021 12:21B1F0146 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 06/04/2021 10:34B1F0154 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 2 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA [TOC_1]2103479-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A06/07/21 16:25mg/kg B1F01941Mercury0.087 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B06/07/21 14:12mg/kg B1F01971Antimony2.3 "5.6 """"Arsenic 1.9 "120 """"Barium 0.93 ND """ ""Beryllium 0.47 ND """ ""Cadmium 0.23 "73 """"Chromium 0.47 N-02 "18 """"Cobalt 0.47 "47 """"Copper 0.93 "8.2 """"Lead 0.47 ND """ ""Molybdenum 0.47 "130 """"Nickel 0.47 ND """ ""Selenium 1.9 ND """ ""Silver 0.47 ND """ ""Thallium 0.93 "49 """"Vanadium 1.9 "65 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B06/09/21 14:34mg/L B1F02612Chromium0.020 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M06/04/21 17:01mg/kg B1F01541TPH Gasoline (C5-C12)4.5 """( 39 - 157 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 3 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M06/05/21 12:12mg/kg B1F01451TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )87 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 4 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B06/04/21 16:16mg/kg B1F01461Benzene0.050 ND """ ""Bromobenzene 0.050 ND """ ""Bromochloromethane 0.050 ND """ ""Bromodichloromethane 0.050 ND """ ""Bromoform 0.050 ND """ ""Bromomethane 0.050 ND """ ""n-Butylbenzene 0.050 ND """ ""sec-Butylbenzene 0.050 ND """ ""tert-Butylbenzene 0.050 ND """ ""Carbon tetrachloride 0.050 ND """ ""Chlorobenzene 0.050 ND """ ""Chloroethane 0.050 ND """ ""Chloroform 0.050 ND """ ""Chloromethane 0.050 ND """ ""2-Chlorotoluene 0.050 ND """ ""4-Chlorotoluene 0.050 ND """ ""Dibromochloromethane 0.050 ND """ ""1,2-Dibromo-3-chloropropane 0.050 ND """ ""1,2-Dibromoethane (EDB)0.050 ND """ ""Dibromomethane 0.050 ND """ ""1,2-Dichlorobenzene 0.050 ND """ ""1,3-Dichlorobenzene 0.050 ND """ ""1,4-Dichlorobenzene 0.050 ND """ ""Dichlorodifluoromethane 0.050 CCHI ND """ ""1,1-Dichloroethane 0.050 ND """ ""1,2-Dichloroethane 0.050 ND """ ""1,1-Dichloroethene 0.050 ND """ ""cis-1,2-Dichloroethene 0.050 ND """ ""trans-1,2-Dichloroethene 0.050 ND """ ""1,2-Dichloropropane 0.050 ND """ ""1,3-Dichloropropane 0.050 ND """ ""2,2-Dichloropropane 0.050 ND """ ""1,1-Dichloropropene 0.050 ND """ ""cis-1,3-Dichloropropene 0.050 ND """ ""trans-1,3-Dichloropropene 0.050 ND """ ""Ethylbenzene 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 5 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B06/04/21 16:16mg/kg B1F01461Hexachlorobutadiene0.050 ND """ ""4-Isopropyl Toluene 0.050 ND """ ""Isopropylbenzene 0.050 ND """ ""Methylene chloride 0.050 ND """ ""Naphthalene 0.050 ND """ ""n-Propylbenzene 0.050 ND """ ""Styrene 0.050 ND """ ""1,1,1,2-Tetrachloroethane 0.050 ND """ ""1,1,2,2-Tetrachloroethane 0.050 ND """ ""Tetrachloroethene (PCE)0.050 ND """ ""Toluene 0.050 ND """ ""1,2,3-Trichlorobenzene 0.050 ND """ ""1,2,4-Trichlorobenzene 0.050 ND """ ""1,1,1-Trichloroethane 0.050 ND """ ""1,1,2-Trichloroethane 0.050 ND """ ""Trichloroethene (TCE)0.050 ND """ ""Trichlorofluoromethane 0.050 ND """ ""1,2,3-Trichloropropane 0.050 ND """ ""1,2,4-Trimethylbenzene 0.050 ND """ ""1,3,5-Trimethylbenzene 0.050 ND """ ""Vinyl chloride 0.050 ND """ ""Xylenes (total)0.050 """( 74 - 122 )103 %Surrogate: Dibromofluoromethane """( 65 - 128 )99 %Surrogate: Toluene-d8 """( 75 - 121 )105 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 6 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA [TOC_1]2103479-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A06/07/21 16:27mg/kg B1F01941Mercury0.092 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B06/07/21 14:15mg/kg B1F01971Antimony2.4 "7.4 """"Arsenic 1.9 "160 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "51 """"Chromium 0.48 N-02 "14 """"Cobalt 0.48 "63 """"Copper 0.96 "8.9 """"Lead 0.48 "0.57 """"Molybdenum 0.48 "88 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "52 """"Vanadium 1.9 "71 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B06/09/21 14:37mg/L B1F02612Chromium0.020 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M06/04/21 17:29mg/kg B1F01541TPH Gasoline (C5-C12)4.4 """( 39 - 157 )95 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 7 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M06/05/21 12:34mg/kg B1F01451TPH Diesel (C13-C22)9.9 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )90 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 8 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B06/04/21 15:48mg/kg B1F01461Benzene0.048 ND """ ""Bromobenzene 0.048 ND """ ""Bromochloromethane 0.048 ND """ ""Bromodichloromethane 0.048 ND """ ""Bromoform 0.048 ND """ ""Bromomethane 0.048 ND """ ""n-Butylbenzene 0.048 ND """ ""sec-Butylbenzene 0.048 ND """ ""tert-Butylbenzene 0.048 ND """ ""Carbon tetrachloride 0.048 ND """ ""Chlorobenzene 0.048 ND """ ""Chloroethane 0.048 ND """ ""Chloroform 0.048 ND """ ""Chloromethane 0.048 ND """ ""2-Chlorotoluene 0.048 ND """ ""4-Chlorotoluene 0.048 ND """ ""Dibromochloromethane 0.048 ND """ ""1,2-Dibromo-3-chloropropane 0.048 ND """ ""1,2-Dibromoethane (EDB)0.048 ND """ ""Dibromomethane 0.048 ND """ ""1,2-Dichlorobenzene 0.048 ND """ ""1,3-Dichlorobenzene 0.048 ND """ ""1,4-Dichlorobenzene 0.048 ND """ ""Dichlorodifluoromethane 0.048 CCHI ND """ ""1,1-Dichloroethane 0.048 ND """ ""1,2-Dichloroethane 0.048 ND """ ""1,1-Dichloroethene 0.048 ND """ ""cis-1,2-Dichloroethene 0.048 ND """ ""trans-1,2-Dichloroethene 0.048 ND """ ""1,2-Dichloropropane 0.048 ND """ ""1,3-Dichloropropane 0.048 ND """ ""2,2-Dichloropropane 0.048 ND """ ""1,1-Dichloropropene 0.048 ND """ ""cis-1,3-Dichloropropene 0.048 ND """ ""trans-1,3-Dichloropropene 0.048 ND """ ""Ethylbenzene 0.048 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 9 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B06/04/21 15:48mg/kg B1F01461Hexachlorobutadiene0.048 ND """ ""4-Isopropyl Toluene 0.048 ND """ ""Isopropylbenzene 0.048 ND """ ""Methylene chloride 0.048 ND """ ""Naphthalene 0.048 ND """ ""n-Propylbenzene 0.048 ND """ ""Styrene 0.048 ND """ ""1,1,1,2-Tetrachloroethane 0.048 ND """ ""1,1,2,2-Tetrachloroethane 0.048 ND """ ""Tetrachloroethene (PCE)0.048 ND """ ""Toluene 0.048 ND """ ""1,2,3-Trichlorobenzene 0.048 ND """ ""1,2,4-Trichlorobenzene 0.048 ND """ ""1,1,1-Trichloroethane 0.048 ND """ ""1,1,2-Trichloroethane 0.048 ND """ ""Trichloroethene (TCE)0.048 ND """ ""Trichlorofluoromethane 0.048 ND """ ""1,2,3-Trichloropropane 0.048 ND """ ""1,2,4-Trimethylbenzene 0.048 ND """ ""1,3,5-Trimethylbenzene 0.048 ND """ ""Vinyl chloride 0.048 ND """ ""Xylenes (total)0.048 """( 74 - 122 )104 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )104 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 10 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0194 - EPA 7471A Prep[TOC] Batch B1F0194 - EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (B1F0194-BLK1) [TOC_3]Blank (B1F0194-BLK1)[TOC] Analyzed: 06/07/21 12:49 Mercury mg/kgND0.10 LCS (B1F0194-BS1) [TOC_3]LCS (B1F0194-BS1)[TOC] Analyzed: 06/07/21 12:53 Mercury mg/kg0.782 0.10 0.833 85-11594 LCS Dup (B1F0194-BSD1) [TOC_3]LCS Dup (B1F0194-BSD1)[TOC] Analyzed: 06/07/21 13:30 Mercury mg/kg0.859 0.10 0.833 2085-115103 9 Duplicate (B1F0194-DUP1)Source: 2103489-02 [TOC_3]Duplicate (B1F0194-DUP1)[TOC] Analyzed: 06/07/21 13:34 Mercury mg/kgND0.097 ND 20 Matrix Spike (B1F0194-MS1)Source: 2103489-02 [TOC_3]Matrix Spike (B1F0194-MS1)[TOC] Analyzed: 06/07/21 13:37 Mercury mg/kg0.827 0.091 0.755 ND 75-125110 Matrix Spike Dup (B1F0194-MSD1)Source: 2103489-02 [TOC_3]Matrix Spike Dup (B1F0194-MSD1)[TOC] Analyzed: 06/07/21 13:39 Mercury mg/kg0.839 0.089 0.742 ND 2075-125113 1 Post Spike (B1F0194-PS1)Source: 2103489-02 [TOC_3]Post Spike (B1F0194-PS1)[TOC] Analyzed: 06/07/21 13:41 Mercury ug/L5.52 25.0 0.00199 QL-0285-11522 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 11 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0197 - EPA 3050B[TOC] Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLK1) [TOC_3]Blank (B1F0197-BLK1)[TOC] Analyzed: 06/07/21 13:30 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1F0197-BS1) [TOC_3]LCS (B1F0197-BS1)[TOC] Analyzed: 06/07/21 13:35 Antimony mg/kg92.0 2.5 100 80-12092 Arsenic "97.2 2.0 100 80-12097 Barium "99.6 1.0 100 80-120100 Beryllium "95.1 0.50 100 80-12095 Cadmium "98.2 0.25 100 80-12098 Chromium "98.8 0.50 100 80-12099 Cobalt "99.2 0.50 100 80-12099 Copper "98.2 1.0 100 80-12098 Lead "100 0.50 100 80-120100 Molybdenum "96.0 0.50 100 80-12096 Nickel "99.6 0.50 100 80-120100 Selenium "96.4 2.0 100 80-12096 Silver "4.92 0.50 5.00 80-12098 Thallium "100 1.0 100 80-120100 Vanadium "96.6 2.0 100 80-12097 Zinc "98.6 2.0 100 80-12099 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 12 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSD1) [TOC_3]LCS Dup (B1F0197-BSD1)[TOC] Analyzed: 06/07/21 13:37 Antimony mg/kg94.8 2.5 100 2080-12095 3 Arsenic "98.8 2.0 100 2080-12099 2 Barium "101 1.0 100 2080-120101 1 Beryllium "96.5 0.50 100 2080-12096 1 Cadmium "99.2 0.25 100 2080-12099 1 Chromium "100 0.50 100 2080-120100 1 Cobalt "100 0.50 100 2080-120100 1 Copper "99.8 1.0 100 2080-120100 2 Lead "101 0.50 100 2080-120101 1 Molybdenum "98.2 0.50 100 2080-12098 2 Nickel "101 0.50 100 2080-120101 1 Selenium "97.8 2.0 100 2080-12098 1 Silver "4.93 0.50 5.00 2080-12099 0.1 Thallium "102 1.0 100 2080-120102 1 Vanadium "98.0 2.0 100 2080-12098 1 Zinc "99.8 2.0 100 2080-120100 1 Duplicate (B1F0197-DUP1)Source: 2103489-01 [TOC_3]Duplicate (B1F0197-DUP1)[TOC] Analyzed: 06/07/21 13:52 Antimony mg/kgND2.4 ND 20 Arsenic "1.22 1.9 ND 20 Barium "21.0 0.97 22.9 208 Beryllium "ND 0.49 ND 20 Cadmium "ND 0.24 ND 20 Chromium "1.94 0.49 2.02 204 Cobalt "1.40 0.49 1.78 20 QR-0424 Copper "1.33 0.97 1.40 205 Lead "1.23 0.49 1.40 2013 Molybdenum "ND 0.49 ND 20 Nickel "1.31 0.49 1.34 202 Selenium "ND 1.9 ND 20 Silver "ND 0.49 ND 20 Thallium "ND 0.97 ND 20 Vanadium "3.86 1.9 4.18 208 Zinc "4.32 1.9 4.51 204 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 13 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MS1)Source: 2103489-01 [TOC_3]Matrix Spike (B1F0197-MS1)[TOC] Analyzed: 06/07/21 13:40 Antimony mg/kg70.3 2.3 93.4 ND 10-11675 Arsenic "93.3 1.9 93.4 ND 77-121100 Barium "119 0.93 93.4 22.9 30-169102 Beryllium "90.1 0.47 93.4 ND 86-11196 Cadmium "91.8 0.23 93.4 ND 81-11298 Chromium "96.8 0.47 93.4 2.02 75-129102 Cobalt "94.2 0.47 93.4 1.78 71-12199 Copper "96.2 0.93 93.4 1.40 68-135102 Lead "94.4 0.47 93.4 1.40 72-121100 Molybdenum "88.2 0.47 93.4 ND 70-11294 Nickel "95.2 0.47 93.4 1.34 73-121101 Selenium "90.1 1.9 93.4 ND 76-11697 Silver "4.56 0.47 4.67 ND 54-13298 Thallium "92.3 0.93 93.4 ND 64-12099 Vanadium "96.5 1.9 93.4 4.18 78-12499 Zinc "98.0 1.9 93.4 4.51 50-143100 Matrix Spike Dup (B1F0197-MSD1)Source: 2103489-01 [TOC_3]Matrix Spike Dup (B1F0197-MSD1)[TOC] Analyzed: 06/07/21 13:42 Antimony mg/kg70.4 2.4 95.8 ND 2010-11673 0.1 Arsenic "94.3 1.9 95.8 ND 2077-12198 1 Barium "116 0.96 95.8 22.9 2030-16997 3 Beryllium "91.2 0.48 95.8 ND 2086-11195 1 Cadmium "92.3 0.24 95.8 ND 2081-11296 0.6 Chromium "97.6 0.48 95.8 2.02 2075-129100 0.8 Cobalt "94.7 0.48 95.8 1.78 2071-12197 0.6 Copper "96.9 0.96 95.8 1.40 2068-135100 0.7 Lead "94.9 0.48 95.8 1.40 2072-12198 0.6 Molybdenum "88.6 0.48 95.8 ND 2070-11293 0.5 Nickel "95.5 0.48 95.8 1.34 2073-12198 0.3 Selenium "91.2 1.9 95.8 ND 2076-11695 1 Silver "4.64 0.48 4.79 ND 2054-13297 2 Thallium "93.1 0.96 95.8 ND 2064-12097 0.9 Vanadium "97.2 1.9 95.8 4.18 2078-12497 0.7 Zinc "103 1.9 95.8 4.51 2050-143103 5 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 14 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PS1)Source: 2103489-01 [TOC_3]Post Spike (B1F0197-PS1)[TOC] Analyzed: 06/07/21 13:45 Antimony mg/L2.03 2.00 0.00248 75-125101 Arsenic "2.04 2.00 0.0178 75-125101 Barium "2.50 2.00 0.460 75-125102 Beryllium "1.96 2.00 0.00218 75-12598 Cadmium "2.00 2.00 -0.00308 75-125100 Chromium "2.07 2.00 0.0408 75-125101 Cobalt "2.06 2.00 0.0359 75-125101 Copper "2.06 2.00 0.0283 75-125102 Lead "2.07 2.00 0.0283 75-125102 Molybdenum "2.01 2.00 -0.00109 75-125101 Nickel "2.06 2.00 0.0271 75-125102 Selenium "1.99 2.00 -0.0103 75-12599 Silver "0.0945 0.100 -0.00169 75-12594 Thallium "2.03 2.00 -0.00407 75-125101 Vanadium "2.08 2.00 0.0842 75-125100 Zinc "2.10 2.00 0.0909 75-125101 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 15 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: STLC Metals by ICP - Quality Control[TOC_1]STLC Metals by IC Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0261 - EPA 3010A Leachate[TOC] Batch B1F0261 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (B1F0261-BLK1) [TOC_3]Blank (B1F0261-BLK1)[TOC] Analyzed: 06/09/21 13:50 Chromium mg/LND0.010 LCS (B1F0261-BS1) [TOC_3]LCS (B1F0261-BS1)[TOC] Analyzed: 06/09/21 14:17 Chromium mg/L10.1 0.010 10.0 80-120101 LCS Dup (B1F0261-BSD1) [TOC_3]LCS Dup (B1F0261-BSD1)[TOC] Analyzed: 06/09/21 14:19 Chromium mg/L10.2 0.010 10.0 2080-120102 0.5 Duplicate (B1F0261-DUP1)Source: 2103218-01 [TOC_3]Duplicate (B1F0261-DUP1)[TOC] Analyzed: 06/09/21 14:27 Chromium mg/L1.22 0.020 1.22 200.08 Leach Fluid Blank (B1F0261-LBK1) [TOC_3]Leach Fluid Blank (B1F0261-LBK1)[TOC] Analyzed: 06/09/21 13:52 Chromium mg/LND0.020 Leach Fluid Blank (B1F0261-LBK2)Analyzed: 06/09/21 13:55 Chromium mg/LND0.020 Leach Fluid Blank (B1F0261-LBK3)Analyzed: 06/09/21 13:58 Chromium mg/LND0.020 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 16 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0154 - EPA 5035/5030B Solid GC[TOC] Batch B1F0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLK1) [TOC_3]Blank (B1F0154-BLK1)[TOC] Analyzed: 06/04/21 12:45 TPH Gasoline (C5-C12)mg/kgND0.49 "0.123 39-157Surrogate: 4-Bromofluorobenzene 870.107 LCS (B1F0154-BS1) [TOC_3]LCS (B1F0154-BS1)[TOC] Analyzed: 06/04/21 11:48 TPH Gasoline (C5-C12)mg/kg1.38 0.50 0.998 68-139138 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1260.158 LCS Dup (B1F0154-BSD1) [TOC_3]LCS Dup (B1F0154-BSD1)[TOC] Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12)mg/kg1.29 0.50 1.00 2068-139128 7 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1160.146 Duplicate (B1F0154-DUP1)Source: 2103455-02RE1 [TOC_3]Duplicate (B1F0154-DUP1)[TOC] Analyzed: 06/04/21 15:35 TPH Gasoline (C5-C12)mg/kgND0.50 0.113 20 "0.124 39-157Surrogate: 4-Bromofluorobenzene 920.113 Matrix Spike (B1F0154-MS1)Source: 2103429-02 [TOC_3]Matrix Spike (B1F0154-MS1)[TOC] Analyzed: 06/04/21 19:23 TPH Gasoline (C5-C12)mg/kg0.905 0.49 0.973 ND 10-17193 "0.122 39-157Surrogate: 4-Bromofluorobenzene 1090.132 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 17 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0145 - EPA 3550C[TOC] Batch B1F0145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) [TOC_3]Blank (B1F0145-BLK1)[TOC] Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "50.0 65-136Surrogate: o-Terphenyl 8341.5 LCS (B1F0145-BS1) [TOC_3]LCS (B1F0145-BS1)[TOC] Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22)mg/kg43410 499 72-11587 TPH Motor Oil (C23-C40)"420 50 499 74-12684 "49.9 65-136Surrogate: o-Terphenyl 9245.8 LCS Dup (B1F0145-BSD1) [TOC_3]LCS Dup (B1F0145-BSD1)[TOC] Analyzed: 06/04/21 12:07 TPH Diesel (C13-C22)mg/kg44410 499 2072-11589 2 TPH Motor Oil (C23-C40)"441 50 499 2074-12688 5 "49.9 65-136Surrogate: o-Terphenyl 9446.7 Duplicate (B1F0145-DUP1)Source: 2103472-01 [TOC_3]Duplicate (B1F0145-DUP1)[TOC] Analyzed: 06/04/21 16:23 TPH Diesel (C13-C22)mg/kgND10 ND 20 TPH Motor Oil (C23-C40)"ND 50 ND 20 "49.9 65-136Surrogate: o-Terphenyl 8140.5 Matrix Spike (B1F0145-MS1)Source: 2103472-01 [TOC_3]Matrix Spike (B1F0145-MS1)[TOC] Analyzed: 06/04/21 15:37 TPH Diesel (C13-C22)mg/kg45210 498 ND 46-14791 TPH Motor Oil (C23-C40)"500 50 498 ND 35-171100 "49.8 65-136Surrogate: o-Terphenyl 8441.6 Matrix Spike Dup (B1F0145-MSD1)Source: 2103472-01 [TOC_3]Matrix Spike Dup (B1F0145-MSD1)[TOC] Analyzed: 06/04/21 16:00 TPH Diesel (C13-C22)mg/kg49610 498 ND 2046-147100 9 TPH Motor Oil (C23-C40)"517 50 498 ND 2035-171104 3 "49.8 65-136Surrogate: o-Terphenyl 8844.0 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 18 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0146 - EPA 5035/5030B Solid[TOC] Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1) [TOC_3]Blank (B1F0146-BLK1)[TOC] Analyzed: 06/04/21 11:32 Benzene mg/kgND0.0050 Bromobenzene "ND 0.0050 Bromochloromethane "ND 0.0050 Bromodichloromethane "ND 0.0050 Bromoform "ND 0.0050 Bromomethane "ND 0.0050 n-Butylbenzene "ND 0.0050 sec-Butylbenzene "ND 0.0050 tert-Butylbenzene "ND 0.0050 Carbon tetrachloride "ND 0.0050 Chlorobenzene "ND 0.0050 Chloroethane "ND 0.0050 Chloroform "ND 0.0050 Chloromethane "ND 0.0050 2-Chlorotoluene "ND 0.0050 4-Chlorotoluene "ND 0.0050 Dibromochloromethane "ND 0.0050 1,2-Dibromo-3-chloropropane "ND 0.0050 1,2-Dibromoethane (EDB)"ND 0.0050 Dibromomethane "ND 0.0050 1,2-Dichlorobenzene "ND 0.0050 1,3-Dichlorobenzene "ND 0.0050 1,4-Dichlorobenzene "ND 0.0050 Dichlorodifluoromethane "ND 0.0050 CCHI 1,1-Dichloroethane "ND 0.0050 1,2-Dichloroethane "ND 0.0050 1,1-Dichloroethene "ND 0.0050 cis-1,2-Dichloroethene "ND 0.0050 trans-1,2-Dichloroethene "ND 0.0050 1,2-Dichloropropane "ND 0.0050 1,3-Dichloropropane "ND 0.0050 2,2-Dichloropropane "ND 0.0050 1,1-Dichloropropene "ND 0.0050 cis-1,3-Dichloropropene "ND 0.0050 trans-1,3-Dichloropropene "ND 0.0050 Ethylbenzene "ND 0.0050 Hexachlorobutadiene "ND 0.0050 4-Isopropyl Toluene "ND 0.0050 Isopropylbenzene "ND 0.0050 Methylene chloride "ND 0.0050 Naphthalene "ND 0.0050 n-Propylbenzene "ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 19 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1)Analyzed: 06/04/21 11:32 Styrene mg/kgND0.0050 1,1,1,2-Tetrachloroethane "ND 0.0050 1,1,2,2-Tetrachloroethane "ND 0.0050 Tetrachloroethene (PCE)"ND 0.0050 Toluene "ND 0.0050 1,2,3-Trichlorobenzene "ND 0.0050 1,2,4-Trichlorobenzene "ND 0.0050 1,1,1-Trichloroethane "ND 0.0050 1,1,2-Trichloroethane "ND 0.0050 Trichloroethene (TCE)"ND 0.0050 Trichlorofluoromethane "ND 0.0050 1,2,3-Trichloropropane "ND 0.0050 1,2,4-Trimethylbenzene "ND 0.0050 1,3,5-Trimethylbenzene "ND 0.0050 Vinyl chloride "ND 0.0050 Xylenes (total)"ND 0.0050 "0.0498 74-122Surrogate: Dibromofluoromethane 1040.0516 "0.0498 65-128Surrogate: Toluene-d8 1010.0503 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 1060.0529 LCS (B1F0146-BS1) [TOC_3]LCS (B1F0146-BS1)[TOC] Analyzed: 06/04/21 09:47 Benzene mg/kg0.0406 0.0050 0.0398 70-131102 Bromobenzene "0.0466 0.0050 0.0398 74-130117 Bromochloromethane "0.0399 0.0050 0.0398 64-133100 Bromodichloromethane "0.0445 0.0050 0.0398 69-137112 Bromoform "0.0447 0.0050 0.0398 55-132112 Bromomethane "0.0407 0.0050 0.0398 10-142102 n-Butylbenzene "0.0476 0.0050 0.0398 64-156120 sec-Butylbenzene "0.0493 0.0050 0.0398 75-155124 tert-Butylbenzene "0.0482 0.0050 0.0398 74-144121 Carbon tetrachloride "0.0442 0.0050 0.0398 67-135111 Chlorobenzene "0.0445 0.0050 0.0398 73-134112 Chloroethane "0.0390 0.0050 0.0398 10-16798 Chloroform "0.0412 0.0050 0.0398 69-124104 Chloromethane "0.0297 0.0050 0.0398 34-13675 2-Chlorotoluene "0.0454 0.0050 0.0398 75-135114 4-Chlorotoluene "0.0460 0.0050 0.0398 70-138116 Dibromochloromethane "0.0439 0.0050 0.0398 67-135110 1,2-Dibromo-3-chloropropane "0.0435 0.0050 0.0398 41-149109 1,2-Dibromoethane (EDB)"0.0409 0.0050 0.0398 68-131103 Dibromomethane "0.0433 0.0050 0.0398 61-140109 1,2-Dichlorobenzene "0.0458 0.0050 0.0398 76-136115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 20 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BS1)Analyzed: 06/04/21 09:47 1,3-Dichlorobenzene mg/kg0.0462 0.0050 0.0398 76-138116 1,4-Dichlorobenzene "0.0457 0.0050 0.0398 72-132115 Dichlorodifluoromethane "0.0210 0.0050 0.0398 CCFH10-15553 1,1-Dichloroethane "0.0389 0.0050 0.0398 63-13998 1,2-Dichloroethane "0.0416 0.0050 0.0398 64-126104 1,1-Dichloroethene "0.0342 0.0050 0.0398 52-16786 cis-1,2-Dichloroethene "0.0401 0.0050 0.0398 70-135101 trans-1,2-Dichloroethene "0.0392 0.0050 0.0398 67-14799 1,2-Dichloropropane "0.0406 0.0050 0.0398 68-131102 1,3-Dichloropropane "0.0405 0.0050 0.0398 64-128102 2,2-Dichloropropane "0.0432 0.0050 0.0398 63-154109 1,1-Dichloropropene "0.0393 0.0050 0.0398 68-13899 cis-1,3-Dichloropropene "0.0416 0.0050 0.0398 72-134105 trans-1,3-Dichloropropene "0.0437 0.0050 0.0398 69-132110 Ethylbenzene "0.0449 0.0050 0.0398 68-136113 Hexachlorobutadiene "0.0546 0.0050 0.0398 72-198137 4-Isopropyl Toluene "0.0504 0.0050 0.0398 74-150127 Isopropylbenzene "0.0473 0.0050 0.0398 71-149119 Methylene chloride "0.0346 0.0050 0.0398 51-12787 Naphthalene "0.0482 0.0050 0.0398 57-158121 n-Propylbenzene "0.0474 0.0050 0.0398 70-143119 Styrene "0.0456 0.0050 0.0398 68-138115 1,1,1,2-Tetrachloroethane "0.0459 0.0050 0.0398 76-130115 1,1,2,2-Tetrachloroethane "0.0399 0.0050 0.0398 60-136100 Tetrachloroethene (PCE)"0.0443 0.0050 0.0398 73-138111 Toluene "0.0430 0.0050 0.0398 72-128108 1,2,3-Trichlorobenzene "0.0507 0.0050 0.0398 61-166127 1,2,4-Trichlorobenzene "0.0502 0.0050 0.0398 71-158126 1,1,1-Trichloroethane "0.0424 0.0050 0.0398 71-135107 1,1,2-Trichloroethane "0.0414 0.0050 0.0398 64-132104 Trichloroethene (TCE)"0.0442 0.0050 0.0398 74-139111 Trichlorofluoromethane "0.0429 0.0050 0.0398 30-156108 1,2,3-Trichloropropane "0.0452 0.0050 0.0398 67-123114 1,2,4-Trimethylbenzene "0.0454 0.0050 0.0398 68-134114 1,3,5-Trimethylbenzene "0.0461 0.0050 0.0398 71-140116 Vinyl chloride "0.0326 0.0050 0.0398 43-14482 Xylenes (total)"0.133 0.0050 0.119 69-138112 "0.0497 74-122Surrogate: Dibromofluoromethane 1060.0525 "0.0497 65-128Surrogate: Toluene-d8 1040.0517 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 1070.0530 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 21 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) [TOC_3]LCS Dup (B1F0146-BSD1)[TOC] Analyzed: 06/04/21 10:13 Benzene mg/kg0.0423 0.0050 0.0400 2070-131106 4 Bromobenzene "0.0498 0.0050 0.0400 2074-130124 7 Bromochloromethane "0.0412 0.0050 0.0400 2064-133103 3 Bromodichloromethane "0.0455 0.0050 0.0400 2069-137114 2 Bromoform "0.0458 0.0050 0.0400 2055-132115 2 Bromomethane "0.0391 0.0050 0.0400 2010-14298 4 n-Butylbenzene "0.0476 0.0050 0.0400 2064-156119 0.1 sec-Butylbenzene "0.0508 0.0050 0.0400 2075-155127 3 tert-Butylbenzene "0.0496 0.0050 0.0400 2074-144124 3 Carbon tetrachloride "0.0456 0.0050 0.0400 2067-135114 3 Chlorobenzene "0.0457 0.0050 0.0400 2073-134114 3 Chloroethane "0.0394 0.0050 0.0400 2010-16798 1 Chloroform "0.0421 0.0050 0.0400 2069-124105 2 Chloromethane "0.0308 0.0050 0.0400 2034-13677 4 2-Chlorotoluene "0.0452 0.0050 0.0400 2075-135113 0.4 4-Chlorotoluene "0.0468 0.0050 0.0400 2070-138117 2 Dibromochloromethane "0.0463 0.0050 0.0400 2067-135116 5 1,2-Dibromo-3-chloropropane "0.0461 0.0050 0.0400 2041-149115 6 1,2-Dibromoethane (EDB)"0.0422 0.0050 0.0400 2068-131105 3 Dibromomethane "0.0459 0.0050 0.0400 2061-140115 6 1,2-Dichlorobenzene "0.0472 0.0050 0.0400 2076-136118 3 1,3-Dichlorobenzene "0.0489 0.0050 0.0400 2076-138122 6 1,4-Dichlorobenzene "0.0472 0.0050 0.0400 2072-132118 3 Dichlorodifluoromethane "0.0228 0.0050 0.0400 20 CCFH10-15557 8 1,1-Dichloroethane "0.0405 0.0050 0.0400 2063-139101 4 1,2-Dichloroethane "0.0425 0.0050 0.0400 2064-126106 2 1,1-Dichloroethene "0.0347 0.0050 0.0400 2052-16787 2 cis-1,2-Dichloroethene "0.0420 0.0050 0.0400 2070-135105 5 trans-1,2-Dichloroethene "0.0401 0.0050 0.0400 2067-147100 2 1,2-Dichloropropane "0.0430 0.0050 0.0400 2068-131107 6 1,3-Dichloropropane "0.0426 0.0050 0.0400 2064-128106 5 2,2-Dichloropropane "0.0446 0.0050 0.0400 2063-154111 3 1,1-Dichloropropene "0.0406 0.0050 0.0400 2068-138102 3 cis-1,3-Dichloropropene "0.0434 0.0050 0.0400 2072-134108 4 trans-1,3-Dichloropropene "0.0454 0.0050 0.0400 2069-132114 4 Ethylbenzene "0.0470 0.0050 0.0400 2068-136118 5 Hexachlorobutadiene "0.0549 0.0050 0.0400 2072-198137 0.5 4-Isopropyl Toluene "0.0514 0.0050 0.0400 2074-150128 2 Isopropylbenzene "0.0499 0.0050 0.0400 2071-149125 5 Methylene chloride "0.0360 0.0050 0.0400 2051-12790 4 Naphthalene "0.0511 0.0050 0.0400 2057-158128 6 n-Propylbenzene "0.0466 0.0050 0.0400 2070-143116 2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 22 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1)Analyzed: 06/04/21 10:13 Styrene mg/kg0.0479 0.0050 0.0400 2068-138120 5 1,1,1,2-Tetrachloroethane "0.0490 0.0050 0.0400 2076-130123 7 1,1,2,2-Tetrachloroethane "0.0417 0.0050 0.0400 2060-136104 5 Tetrachloroethene (PCE)"0.0454 0.0050 0.0400 2073-138114 3 Toluene "0.0439 0.0050 0.0400 2072-128110 2 1,2,3-Trichlorobenzene "0.0520 0.0050 0.0400 2061-166130 3 1,2,4-Trichlorobenzene "0.0512 0.0050 0.0400 2071-158128 2 1,1,1-Trichloroethane "0.0432 0.0050 0.0400 2071-135108 2 1,1,2-Trichloroethane "0.0448 0.0050 0.0400 2064-132112 8 Trichloroethene (TCE)"0.0448 0.0050 0.0400 2074-139112 1 Trichlorofluoromethane "0.0430 0.0050 0.0400 2030-156107 0.1 1,2,3-Trichloropropane "0.0463 0.0050 0.0400 2067-123116 3 1,2,4-Trimethylbenzene "0.0459 0.0050 0.0400 2068-134115 1 1,3,5-Trimethylbenzene "0.0465 0.0050 0.0400 2071-140116 0.9 Vinyl chloride "0.0338 0.0050 0.0400 2043-14484 3 Xylenes (total)"0.139 0.0050 0.120 2069-138116 4 "0.0500 74-122Surrogate: Dibromofluoromethane 1040.0519 "0.0500 65-128Surrogate: Toluene-d8 1020.0510 "0.0500 75-121Surrogate: 4-Bromofluorobenzene 1060.0530 Duplicate (B1F0146-DUP1)ISlowSSource: 2103474-01 [TOC_3]Duplicate (B1F0146-DUP1)[TOC] Analyzed: 06/04/21 15:22 Benzene mg/kgND0.0050 ND 20 Bromobenzene "ND 0.0050 ND 20 Bromochloromethane "ND 0.0050 ND 20 Bromodichloromethane "ND 0.0050 ND 20 Bromoform "ND 0.0050 ND 20 Bromomethane "ND 0.0050 ND 20 n-Butylbenzene "ND 0.0050 ND 20 sec-Butylbenzene "ND 0.0050 ND 20 tert-Butylbenzene "ND 0.0050 ND 20 Carbon tetrachloride "ND 0.0050 ND 20 Chlorobenzene "ND 0.0050 ND 20 Chloroethane "ND 0.0050 ND 20 Chloroform "ND 0.0050 ND 20 Chloromethane "ND 0.0050 ND 20 2-Chlorotoluene "ND 0.0050 ND 20 4-Chlorotoluene "ND 0.0050 ND 20 Dibromochloromethane "ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane "ND 0.0050 ND 20 1,2-Dibromoethane (EDB)"ND 0.0050 ND 20 Dibromomethane "ND 0.0050 ND 20 1,2-Dichlorobenzene "ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 23 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate (B1F0146-DUP1)ISlowSSource: 2103474-01 Analyzed: 06/04/21 15:22 1,3-Dichlorobenzene mg/kgND0.0050 ND 20 1,4-Dichlorobenzene "ND 0.0050 ND 20 Dichlorodifluoromethane "ND 0.0050 ND 20 CCHI 1,1-Dichloroethane "ND 0.0050 ND 20 1,2-Dichloroethane "ND 0.0050 ND 20 1,1-Dichloroethene "ND 0.0050 ND 20 cis-1,2-Dichloroethene "ND 0.0050 ND 20 trans-1,2-Dichloroethene "ND 0.0050 ND 20 1,2-Dichloropropane "ND 0.0050 ND 20 1,3-Dichloropropane "ND 0.0050 ND 20 2,2-Dichloropropane "ND 0.0050 ND 20 1,1-Dichloropropene "ND 0.0050 ND 20 cis-1,3-Dichloropropene "ND 0.0050 ND 20 trans-1,3-Dichloropropene "ND 0.0050 ND 20 Ethylbenzene "ND 0.0050 ND 20 Hexachlorobutadiene "ND 0.0050 ND 20 4-Isopropyl Toluene "ND 0.0050 ND 20 Isopropylbenzene "ND 0.0050 ND 20 Methylene chloride "ND 0.0050 ND 20 Naphthalene "ND 0.0050 ND 20 n-Propylbenzene "ND 0.0050 ND 20 Styrene "ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane "ND 0.0050 ND 20 1,1,2,2-Tetrachloroethane "ND 0.0050 ND 20 Tetrachloroethene (PCE)"ND 0.0050 ND 20 Toluene "ND 0.0050 ND 20 1,2,3-Trichlorobenzene "ND 0.0050 ND 20 1,2,4-Trichlorobenzene "ND 0.0050 ND 20 1,1,1-Trichloroethane "ND 0.0050 ND 20 1,1,2-Trichloroethane "ND 0.0050 ND 20 Trichloroethene (TCE)"ND 0.0050 ND 20 Trichlorofluoromethane "ND 0.0050 ND 20 1,2,3-Trichloropropane "ND 0.0050 ND 20 1,2,4-Trimethylbenzene "ND 0.0050 ND 20 1,3,5-Trimethylbenzene "ND 0.0050 ND 20 Vinyl chloride "ND 0.0050 ND 20 Xylenes (total)"ND 0.0050 ND 20 "0.0498 74-122Surrogate: Dibromofluoromethane 1080.0538 "0.0498 65-128Surrogate: Toluene-d8 1020.0509 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 1020.0506 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 24 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP,NELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP,NELAP8015 Diesel & Motor Oil List Solid STLC Metals by ICP STLC/EPA 6010B OEC, Internal6010B STLC Chromium Solid STLC Metals Extraction STLC OEC, InternalSTLC Metals Extraction Water Total Metals by CVAA EPA 7471A OEC, InternalMercury Total EPA 7471A Solid Total Metals by ICP EPA 6010B OEC, CA-ELAP,NELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP,NELAP8260B Full List Solid EPA 8260B OEC, Internal8260B Full List Solid Volatile Organic TPH by GC/FID EPA 8015M OEC, Internal8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 25 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL CCFH The CCV for this analyte failed high. Results for this analyte may be biased high. CCHI The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. ISlowS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above 10x STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 26 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: [TOC_1]Other Documents[ The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 27 of 32 File : C:\MSDCHEM\1\DATA\JUN21\060521\B0MF0512.DOperator : CMLAcquired : 05 Jun 2021 12:12 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103479-01@B1F0145(S) Misc Info : 1@ Vial Number: 100.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0MF0512.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\JUN21\060421\DOMF0414.DOperator : RRAcquired : 4 Jun 2021 5:01 pm using AcqMethod GAS-BTEX.MInstrument : GC4Sample Name: 2103479-01@1:10 prep Misc Info : 1@ Vial Number: 140.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50500010000150002000025000300003500040000450005000055000600006500070000750008000085000TimeResponse_DOMF0414.D\FID1A File : C:\MSDCHEM\1\DATA\JUN21\060521\B0MF0514.DOperator : CMLAcquired : 05 Jun 2021 12:34 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103479-02@B1F0145(S) Misc Info : 1@ Vial Number: 120.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0MF0514.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\JUN21\060421\DOMF0415.DOperator : RRAcquired : 4 Jun 2021 5:29 pm using AcqMethod GAS-BTEX.MInstrument : GC4Sample Name: 2103479-02@1:10 prep Misc Info : 1@B1F0154 GRO Solid Vial Number: 150.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.505000100001500020000250003000035000400004500050000550006000065000700007500080000TimeResponse_DOMF0415.D\FID1A Page 28 of 32 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLDemuekuieihemuekuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 29 of 32 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG5HFHLSW/RJLQ%\’$5HFHLSW5HYLHZHG%\$00Page 30 of 32 samples taken and received 6/4/2021 per client confirmation MLSPage 31 of 32 samples taken and received 6/4/2021 per client confirmation MLS01- added STLC Cr02- added STLC Cr; SP 6/7/21Page 32 of 32