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HomeMy WebLinkAbout2021-10-07 2600 Broad St. Closure Rpt Rev. 1Closure Report Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA October 7, 2021 (Rev. 1) Prepared For: Mr. John Hochleutner Pacific Petroleum California, Inc. 1615 Betteravia Road Santa Maria, CA 93268 Prepared By: Buena Resources, Inc. P.O. Box 2040 Santa Maria, CA 93457-2040 Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA TABLE OF CONTENTS 1.0 Excavation: 2.0 Soil Sampling of the Excavation: 3.0 Discussion of Results: 4.0 Conclusions: Appendix A Site Maps & Figures Appendix B Lab Summary Spreadsheets Appendix C Site Photographs Appendix D Laboratory & Chain of Custody Reports Appendix E Statement of Qualifications 2-5 5-6 6-7 7-8 General Contractor License #841453 Buenaresources P.O. Box 2040 Santa Maria, CA 93457-2040 P: (805) 346-1766 F: (805) 346-1767 October 7, 2021 Ms. Matheson Bliss, Haz Materials Coordinator City of San Luis Obispo Fire Department 2160 Santa Barbara Avenue San Luis Obispo, CA 93401-5240 Subject: Fuel Tank Removal and Soil Removal from a Site located at 2600 Broad Street in San Luis Obispo, CA Dear Mattie: Buena Resources, Inc. has prepared this Closure Report to summarize the work performed and the laboratory results at the above site. Pacific Petroleum of California was initially engaged by Natural Healing Center to remove an existing diesel tank from this site, which had been closed at some point in the past by filling with cement. The diesel tank was estimated to be 4'-dia. by 8' long in size. The excavation related to that tank site was 8' x 8' by 8' deep. Once the tank was removed, the underlying soils were found to have been impacted. A second site was the trench that was opened to place utilities during the construction activities at this site. Contamination was found in the trench which extended to the west where a large amount of lead impacted bricks were found. This second excavation, which was located adjacent and north of the removed tank, 12' x 12' by 12' deep. These areas are shown on the attached figure with the associated stockpile located near the excavation. Buenaresources A State Certified Small & WBE Business BUENARESOURCES Impacted soil was found below the tank, in the excavation bottom and on the sides of the excavation. Soil believed to be impacted from the diesel tank was removed and placed into 10 cyd. bins. A total of 64.51 tons of Cal Haz lead impacted and hydrocarbon impacted soil was removed and shipped to Waste Management's Kettleman Hills Class I TSD facility. We are not aware of the reasons for the historical diesel tank. There was no Phase I ESA Report completed for this site, which could have explored the historical use of this property. As we understand, there was a brick factory located close to this site. The tank was likely used for either fueling or for waste. The bricks are possibly left over from a demolished structure that may have been on the site or immediate area. The concrete slab may have been a cap for the fuel contamination located below it. Although the chromatographs for the TPH data show a weathered diesel pattern, it is possible that gasoline range organics may have been present and have degraded over time. Due to the presumed age of the site, this may have been leaded gasoline explaining the presence of lead. Approximately 15' to the NE of the Diesel Tank Excavation, between the former Quik Mart and the building that will be the NHC SLO, the groundwater was discovered at a depth of 2'. In the tank excavation, groundwater was discovered at a depth of 5'. No groundwater intruded into the second excavation where the bricks and concrete slab were found. 1.0 EXCAVATION: Diesel Tank Excavation This excavation was performed to remove an 4'-dia. x 8' metal tank that was likely used to dispense or store diesel fuel. Once the tank was removed from the excavation, four samples were taken to explore for contamination on March 25, 2021, which are OEC Lab IDs No. 2101841-01 through 04. Tank Wall Samples were taken at a depth of 4' in the center of each wall. OEC Lab samples 2101841-05 & 06 Tank Bottom Samples were taken at a depth of 8' at the inlet and outlet ends of the tank. These samples were located at the bottom center of the Buenaresources A State Certified Small & WBE Business 2 BUENARESOURCES east and west ends of the excavation, approximately 1' from the east and west walls, respectively. The sample locations can be seen on page 9 of the Closure Report. Lab data from these samples indicated the presence of chromium at 51 mg/kg in the Tank N Wall sample, OEC Lab ID 2101841-01. Further STLC analysis was ran on this sample resulting in a non -hazardous level of 0.13 mg/I reported. All other tank wall & floor samples reported results below action levels allowing the material to be left in place. Based on these results, the excavation was backfilled with clean soil. The soil excavated from the diesel tank removal generated a stockpile approximately 5' high by 8' in length and 4' wide. Stockpile Samples On March 25, 2021 composite samples were taken from the north, south and west sides of the pile, OEC ID Nos. 2101841-10, 11 & 12. Sampling was done by taking three equal amounts of soil from halfway up each side of the stockpile at intervals of approximately 1'5" and a depth of 6". These aliquots were mixed into three composite samples representing the three sides of the stockpile. A sample was not taken from the east side of stockpile as it was too close to the mouth of the excavation and not safe to try to obtain a sample. Trench Sampling A trench was dug approximately 3' deep to accommodate a water line. A stockpile of soil and bricks were generated from this trenching which was approximately 3' high, 6' long and 4' wide. A composite sample was taken from the stockpile by taking six equal amounts of soil from half way up the pile (1.5') at 2' intervals and a depth of approximately 6". These aliquots were combined into a single sample. As the excavation continued, the trench was segregated into two sections for sampling because half the length of the excavated material was composed of sol and the other length contained brick as well as soil. The length containing only soil was called the "Fire Trench" and the other "Sump Trench". Originally, samples were taken from the Buenaresources A State Certified Small & WBE Business 3 BUENAF�L;:�i1F_LLs west wall of the sump trench and at the bottom of the south end of the trench (OEC Lab ID Nos. 2101841-07 & 08. The results of these samples indicated elevated levels of TPH, chromium, copper and lead. The samples were then analyzed for STLC and TCLP levels with the results for lead coming back at 56 mg/l for STLC testing (lab ID. 2101841-07). Data indicated further excavation was required with a sample taken from the Sump Trench West side after this removal was completed (OEC ID 2103032-07) in the middle of the trench length, as that was where the majority of the brick was found. A sample was also taken from the bottom center of the trench (OEC ID. 21020302-03). This process was repeated for the Fire Trench with the inclusion of a sample on the east side of the trench where the material seemed to be consistent along the length of both trenches. These results indicated elevated levels of the same constituents prompting further excavation. Concrete Excavation During further excavation of the trench, the outline of a brick structure was discovered containing loose bricks and soil. As this material was removed, a concrete slab was uncovered. Brick and soil from this excavation was placed into several twenty cubic yard bins. This material was sampled by taking three samples from each bin. Material was taken from the center of each bin moving left to right at a distance of 3' apart for each sample (A, B & C), see OEC Lab ID Nos. 210508-01 thru 15. The concrete slab was removed and it was discovered that there was hydrocarbon impacted soil underneath the slab, most likely from the removed fuel tank. Five samples were taken from the floor of the excavation (See OEC Lab ID Nos. 2102742-01 thru 05). The sample locations are as follows: NW Corner@8', NE Corner@8', SE Corner@8', and the center of the excavation at 8'. The data for these samples indicated the presence of weathered hydrocarbon and that more material needed to be removed. Two twenty cubic yard bins of material was excavated and Buenaresources A State Certified Small & WBE Business 4 BUENARESOURCES sampled in the same manner as the other bins, see OEC ID Nos. 2103212-03 thru 08. Once it was believed that all contaminated material was removed, two verification samples were taken from the excavaton floor approximately 4' east and west from the center where the highest amount of petroleum had been removed, after an acceptable level was reached, the excavation was backfilled with clean soil. The area to the west and below the tanks were found to have been impacted by the diesel fuel along with Chromium, Nickel and Lead. All elevated metals above the SLTC testing threshold were tested, with all the Chromium and Nickel samples found to be below the Title 22 STLC (soluble) hazardous thresholds. Lead, however, did exceed the Title 22 threshold and would be considered California hazardous material. Additional testing by TCLP RCRA method all reported levels below the RCRA threshold. The underlying soils under this site has a band of Serpentine, which is likely accountable for the reported Chromium and Nickel levels. This greenish material is very hard and, in this case, weathered with cracks. The diesel fuel appears to have migrated into these cracks requiring these underlying soils to be impacted requiring removal. The last samples taken on June 0 were all below the Region II ESLs for all hydrocarbon ranges and meet the closure criteria established for this site. The depth of this excavation was approximately 12' and 12' x 12' in size. The excavations are shown in Appendix A as Figure 1. 2.0 SOIL SAMPLING OF THE EXCAVATION 2.1 Soil Sampling Plan Samples were taken from the excavation sides and bottom. All soil samples were analyzed for full range hydrocarbons (gasoline, diesel and motor oil ranges) by EPA method 8015, Volatile Organic Compounds by EPA method 8260b and CAM metals. Each sample was sealed, labeled, Buenaresources A State Certified Small & WBE Business 5 BUENAPSOURCES placed in a cooler with ice and shipped to the laboratory. Analyses were completed according to the various methods specified according to SW-846 guidelines. Action levels used at this site were the Regional Water Quality Control -Region II ESLs (Environmental Screening Levels) for residential soils. The reason for the selection of contaminants of concern (i.e. why weren't SVOCs, PAHs, etc. included in testing) is because these compounds were not considered necessary due to the nature of the site. There was no indication that these constituents would be present for any reason considering the location and the types of businesses in the area. 2.2 Sampling Maintenance and Securit Upon collection, the sample containers were labeled in accordance with EPA protocols and chilled pending transportation to OEC, a State certified analytical laboratory located in Santa Maria, California following chain -of -custody procedures. All samples were recorded on Chain -of - Custody forms in ink and transferred to the laboratory according to EPA SW-846 protocol. Any changes or corrections were made by drawing a line through the error and initialing and dating the correction, then entering the correct information. 3.0 DISCUSSION OF RESULTS: Samples were taken at four wall locations and at two bottom of excavation locations below the tank. In addition, seven trench and four soil piles were initially sampled and were found to have lead at levels considered Cal Haz for STLC Lead. The soils in the five bins were also sampled to confirm the contaminates were hazardous. All five bins reported STLC lead at levels which exceeded the Title 22 guidelines for hazardous waste thresholds and were subsequently shipped as Cal Haz STLC Lead impacted soils to Waste Management's Kettleman Hill's TSD facility. The samples taken on May 5th reported elevated diesel levels in three of the six samples. Those areas were further excavated with the final sampling on June 3rd reporting all bottom samples below the Region II ESL action levels for residential soils. All of the samples taken at the Buenaresources A State Certified Small & WBE Business BUENARESOURCES excavation sites reported no volatile organic compounds to at least the method detection limit (MDL) with the exception of the Soil Pile North Sample. The Soil Pile North sample reported n- Butylbenzene at 0.2 mg/kg, sec-Butylbenzene at 0.11 mg/kg and n-Propylbenzene at 0.15 mg/kg. All later samples taken after additional material had been removed, were below the MDL for all Method 8260b compounds. The CAMS reported nine samples with elevated chromium and six with elevated nickel levels requiring additional STLC testing to determine if the material was hazardous. The STLC levels were all below the California Title 22 hazardous thresholds for both the chromium and nickel and is not considered hazardous. It is important to note that elevated levels of these two metals are common in the Serpentine material found in this area. The reported TTLC levels were at levels high enough to require further STLC testing. All of those STLC results were well below Title 22 regulated STLC metal levels and likely would be considered typical background values for this area. 4.0 CONCLUSIONS. - The one cement filled diesel tank was successfully removed by PPC and shipped to WM McKittrick Landfill facility for landfilling. Impacted soil from the fuel and lead leakage was discovered below the tank and adjacent to the tank location and was subsequently removed. A total of 64.52 tons of Cal Haz STLC lead impacted soil was removed and shipped to Waste Management's Kettleman Hills TSD facility. This material also reported elevated diesel range hydrocarbons in the side slopes and bottom which was removed and included with the material shipped to Kettleman Hills. Based on the above reported results, it is our opinion that there is no further work required at this site due to the fuel contamination from the removed tank. We recommend that this site be closed and backfilled. Buenaresources A State Certified Small & WBE Business 7 BUENARESOURCES Thank you for the opportunity to be of service. If you have any questions, please contact this office at (805) 346-1766. Sincerely, Buena Resources, Inc. Daniel P. Ringstmeyer, P.E. (0435 Owner/Engineer Buenaresources A State Certified Small & WBE Business M 6 ' �'' - 1,, 'vo 0043540 Exp. Gl to APPENDIX A Site `laps & Figures VICINITY MAP Bishop . a C_ E m L] `Highland Dr Slack St 101 E Foothill Blvd G�tReal ��Iti EI Meta Dr Santa 0 Rosa PaTR. 'r to`: f San Luis �s Obispo v 20r2W-PBU 203A rg ZPr T11 ,``°� 2600 Broad St, San L.. 2o2A;. • ts�t4 0 5� 0,- 2600 Broad St 202,p Q•5 E`�` San Luis Obispo, CA High St 93401 South St T� Laguna Lake Park 4Park St 4 t: t �• Southwood Dr NO a d� a O 61 � G 2008 Jet Prado Rd 227 Q' Islay 4 Hill Park Gj Damon -Garcia Fav' o Rd ' 200 Sports Fields Tank Farm Rd pSan Luis n Obispo ")OF 5p t +C�cChesmy Field —rwz� e 46 ° Evans Rd 'I CI I "7 9' 198 ,Q �sa a 0 mi 0.5 1 1.5 2 Copyright© and (P)1988-2012 Microsoft Corporation and/or its suppliers. All rights reserved. http:/Amww.microsoit.com/streets/ Certain mapping and direction data © 2012 NAN TEQ. All rights reserved. The Data for areas of Canada includes information taken with permission from Canadian authorities, including: ©Her Majesty the Queen in Right of Canada, © Queen's Printer for Ontario. NAVTEQ and NAVTEQ ON BOARD are trademarks of NAN TEQ. © 2012 Tele Atlas North America, Inc. All rights reserved. Tele Atlas and Tele Atlas North America are trademarks ofTeleAtlas, Inc. © 2012 by Applied Geographic Solutions. All rights reserved. Portions © Copyright 2012 by Woodall Publications Corp.All rights reserved. 8' CONCRETE RETAINING WALL BASIS OF BEARINGS COORDINATES FOR THIS PROJECT ARE CALIFORNIA COORDINATE SYSTEM NAD83, CALIFORNIA ZONE 5, US SURVEY FEET, AS DETERMINED BY GPS OBSERVATIONS ON POINTS 8070, AND 8201 "MONTEREY" AS SHOWN ON THE CITY OF SAN LUIS OBISPO "HORIZONTAL CONTROL NETWORK" (JANUARY 2007). BENCFUMM THE ELEVATIONS SHOWN HEREON ARE NAVD88 AS DETERMINED BY MEASUREMENTS ON POINT 81 AS SHOWN ON THE CITY OF SAN LUIS OBISPO "BENCHMARK SYSTEM" (JANUARY 2007) HAVING PUBLISHED ELEVATION OF 210.28', Note: Fire trench is 3' deep with excavation expanding to the west to include the 15' x 15' by 10' deep trash pit of bricks which were removed to concrete floor at —7'. An additional 3' of impacted soil was removed below the concrete and sampled on the sides and center. Buenaresources ENVIRONMENTAL, CIVIL, & GENERAL CONTRACTING SERVICES P.O. Box 2 . Santa Man', CA OU67-209 PW5.34 A7W FW5.W.17V 0 5 10 1 INCH = 10 FEET SURVEY DATE: 06/10/2021 � McKittrick Waste Treatment Site W Reprint 56533 Hwy 58 W. - Ticket# 156247 WASTE MANAGEMENT MCK1ttrlck, CA, 93251 Ph: (661) 762-7366 Customer Name PACIFICPETRO PACIFIC PETROLEU Carrier Pacific Petroleum Pacific Petroleum Ticket Date 05/13/2021 Vehicle# PPC 570 Volume Payment Type Credit Account Container Manual Ticket# Driver Ryan Hauling Ticket# Check# Route North Billing # 0001772 State Waste Code Gen EPA ID Manifest PPC 2021-000473 Destination Grid LF PO Profile 647907CA (FORMER FUEL TANK) Generator 144-NATURAL SANLUISOBISPO 2600 NATURAL HEALING CENTER (2600 BROAD ST) Time Scale Operator Inbound Gross 39760 lb In 05/13/2021 09:33:05 INBOUND Dcarmical Tare 29540 lb Out 05/13/2021 12:49:25 OUTBOUND Dcarmical Net 10220 lb Tons 5.11 Comments Truck was held up pending paperwork corrections Receiving: Mon -Thu Drums 7-3, Liquids & Roll -offs 7-4, End Dumps 7-5 Product LD% Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------------------- 1 SpwasteSolidOth-Cu 100 1.00 Yards SANLUISOBI -- 2 EVF-P-Standard Env 100 SANLUISOBI 3 FUEL -Fuel Surcharg 100 % SANLUISOBI 4 RCR-P-Regulatory C 100 SANLUISOBI 5 WWM-P-Waste Water 100 SANLUISOBI 6 HARD2HANDLE-Hard T 100 1 Load SANLUISOBI Total Tax Total Ticket Driver's Signature C rtitn�H•''Lls Landfill Reprint 3 -Sky.li .Road, P.O. Box 471 Ticket# 55260 Ket4,'h&m m► Ems, 93239 Ticket Date 05/24/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667316JJK Grid B18 Volume Yards Carrier CAD981164312 Driver Arturo Vehicle # G249 Vehicle License 9F36934 Container # 4NP7786 Container License 4NP7786 Time Scale Operator In 05/24/2021 11:46 MANUAL WT A. Ortega Gross 75320 lb* Out 05/24/2021 12:41 A. Ortega Tare 44320 lb* * Manual Weight Net 31000 lb Tons 15.50 Comments Inbound Product Qty UOM Rate Tax Amount Origin 1 ------------------------------------------------------------------------------- NONH DISP-TONS-Non 100 15.50 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI ' 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature ease pdnt or type. (Form designed for use on elite (12•pdch) typewriter.) 1. Generator ID Number 2. Page 1 of 3. Emergm Response f UNIFORM HAZARDOUS WASTE MANIFEST _- _: __ Generator's S:1e Address (I 5 Gernrator's Name and Alailing Address Form Approved. OMB No.2050-W39 RWTracki Number 156M16 JJK Genarator'sPnone �:: '��"15" ` -- O.S. EPA ID Nu E. Transporter 1 Company Name � •<,� roe :n w, U S. EPA ID Number 8. Designated Fard ty Name amp IleAdaress T� - . • 'r•r . * � 7ar.=4�' •' Fadl fibs Prone: "' n Sh Name• Haz!Lss- ID tamt e , 10. Con ainers it. Total 12 Unit 13 Waste Codes 9a 9h. U S. DOT Cescripbon (ndudng Prne f P n9No Type OuanWy . HM and Packing G'ow (if any)) ,wry 110 - 2 - L 4. 1 1 1 1 1- 14.5pedal Handling Instructions and Additional tnfc motion X3 ,76 - v 15 GENERATOR'SIDFFEROR'S CERTIFICATION: I hereby dedae eiat the contents of this consignment are fully and accurately desrnroper bed above by Ire pshipping name and are dassffied, packaged. marked and labeled'placarded. am are in all respew in proper condition fortransport according to appl;rable ntam itiom' and national gcoemmental regula long if export stionem and 1 am dra Primary Exporter, I certify that the contents of #4s misignmera conform to the terms of the attached EPA Admadeogmem of Consent I certiy dmt N waste mmnmaabon statement dm fsd in 41 CFR 262.27(a) (B I am a large quantity generator) a (b) fir I am a sma, quanury generator) is me Signature ra Dorf' Generates'OflerotsPdnledrTypedName r!.! nn ICI t6.1 _..ttrona5ni:� - mpottoUS 1ExoadhanUS. Pc o'enay'exit — Date leamg U S . — Transporrar sgnaz�m (for exports only): 17. TranspaterAckno,Nedgment of Receipt of Mater als +� ran 1 Pri�tedTypel Uame signature ...�.r.Lllx I 18.Oisaapancy �^i i8a. Dlecrepancy 1edlcaaon Space � (yuan�y ❑ Type U R.,dL,e � f-'� I Pamal Reiemon ❑ Full Rly v Manifest P,e'ereace Ncmoec lab Alternate Fac.ity for Generator) U.S EPA iD Number 7 v U41 FaQlaVs Phase: .w x n> you 19. Hazards 4Yaste Report Management Method Codes (i- ,cedes for hazardous waste treahnent, disposal. and recycling systems) G 1 2 3 d L 3�- 20. Designated Fadlm/ Owner a Opa2Wc Certi;a`alan of receipt of hazardous materials covered by dre mar;fast ex-- p' as nded rc� I - m t8a nN Day Year Printedffyced• ',na _ a 2 :PAFom876.22(Rev 3-051 Prerousedihonsare obsolete . (}85.3' Er, �CI�ITY'O DE YfNATi r STATE (IF REQUIfiED) Cwman Halls Landfill Reprint 3 Skyline Road, P.O. Box 471 Ticket# 55489 Kev4►1wir&fz►r&idE"Er0A, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667317JJK Grid B18 -- Volume Yards Carrier CAD981164312 Driver Vehicle # G1076 Vehicle License 9F18973 Container # 4NC6734 Container License 4NC6734 Time Scale Operator In 05/28/2021 10:45 MANUAL WT A. Ortega Gross 71860 lb* Inbound Out 05/28/2021 12:25 A. Ortega Tare 43720 lb* * Manual Weight Net 28140 lb Tons 14.07 - Comments _. Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 NONH DISP-TONS-Non 100 14.07 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature TRH 6&rv/9Vjgj?3, TAL 5a0-1f �JW03y Please print or". (Form designed for use on elite (12-00) tvoewdtecl Form Annmvarf OMA Nn VgLMag UNIFORM HAZARDOUS 1. Ger "r ID Number 2. Page t of 3 Emergency Response Phone 4. Manifest TrackingNumber WASTE MANIFEST -,.-r - -. --- 1 __-_ t 1 i a R R 7� 1q 7 .1� C man Hills Landfill Reprint 3 Skyline.Road, P.O. Box 471 Ticket# 55500 Ke w&iA Ems, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667318JJK Grid B18 --- Volume Yards Carrier CAD981164312 Driver JUAN Vehicle # 65424M1 Vehicle License 65424M1 Container # Container License Time Scale Operator In 05/28/2021 12:43 MANUAL WT A. Ortega Gross 46680 lb* Inbound '- Out 05/28/2021 14:02 A. Ortega Tare 32740 lb* * Manual Weight Net 13940 lb Tons 6.97 Comments REPLACEMENT TICKET FOR TICKET # 55490 Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 6.97 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature qfq- 6!gq4jv,j ct I Please Print Of type. (Form designed fa use On elite (12-pkh) typewriter.) t UWo" HAZARDOUS I - Generator ID Number WASTE MANIFEST 2 Page 1 of 3. EmergencyZ PhoneManifest T Form Approved. OMB No. 205W39 N 5.0 G-rators Name and M*V Address' Genaraties 0156 7318 JJK Site Address (if differml than —Mij Gerwaws plione. 6. Transporter I Company Na z-, U.S EPA ID Number 7, Transporter 2 Company Name U.S EPA ID Number 8 Fac*ty Nam and Re Address U.S.EPA E Number '4 Faaws phone: ga 91b, U.S. DOT Description [-kl*g PmW SN*ng New. Hazard Class ID Number. HM 8nd%V9GW(rfany)) 10. Containers 11JOW 12. Unit No. Type Quantty, M.Nd. 13 Waste Codes Ct 20 z 2 14— "d`-fl9 instructions and Additional Information0 7 L( 15 GIDMTOR,Sipq: OR(IF 1 11 110111 Thereby declare 11 11 8me contents of this cmsignmantare u"Y — i—urarri"Y OeXrloed above by ft proper s" rig 11: .al:% and labelledifo%xt3d. and are in all respects —are d—WWka*. "op"condi'm for transport according to appik-bie W.8tionaland nor ay governmental E-V— I) IhM ft milents ofthis consignment" I cmfDrmtDU*IemsOfNaWedEPAAcknoWedrwMO,C, sent. --zabm-errientkWfiWtn4OCFR262,27(a)(diamawgeqmb�gemrdtDr)or(b, regulations. ffexpoq shipment and I am the primary lama - -1qua generakw Prilif , Signature V 1 Day year enternational shprrierlis El import to U.S ❑ Export him U.S. port i`J7 of entrylexit: TMWW wisture (t% exports only): 17. ThensporarrAonmledgmen, of Remo of Me Date leaving U S: TranscirrLw I Panted an* , Signature J1 —D-YY. I Tianscarku 2 Pin - LZ (It --L5 Month Day Year 18. Discrepaq 18a. Discrepancy k6cartion Space ❑ Quantity OTM ❑Radue ❑ Partial Rejection ❑ Full Rejection I 81b. Afternate Fad]4 (or U.S. EPA JO Number 18c. SVnatune OfAltenuate Fadity (a Generator) Month Day year 19. Hazardous Waste Report MaWment Method Codes (i.e codes for hazardous waste treatment, disposal, and W 1recoing systerns) . —L—L— 0 2 3. 20. Designated Facility Owrw or Operator: Certification of receipt of hazardous mawriall, covered by the manifest except asg in Itern 183 Prin" ype4 B.-O 1) , Signature_ed I . Y - I �Odffb jr yew IS EPA rOrMbfUU-aNOV.3-D5) PreviOm edifions; are obsolete 24 OJESIGI` D FAC�LIT� E IN ATI J STATE (IF REQUIRED) C m ls Landfill Reprint 3 s kwl ifqua ,Road, P.O. Box 471 Ticket# 55678 Ke*Whi3M21 4►RQidEgtigeFhA, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667326JJK Grid B18 Volume Yards Carrier CAD981164312 Driver Vehicle # G1072 Vehicle License 537551TZ Container # Container License Time Scale Operator In 06/04/2021 12:03 MANUAL WT A. Ortega Gross 68100 lb* Inbound Out 06/04/2021 13:38 A. Ortega Tare 45140 lb* * Manual Weight Net 22960 lb Tons 11.48 Comments Product Qty UOM Rate Tax Amount Origin 1 ------------------------------------------------------------------------------- CALH DISP-TONS-Cal 100 11.48 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature r,C �pr ase o. UNIFORM HAZARDOUS WASTE MANIFEST on elite wHC SLO 9BB HUSTON ST GROVER BEACH, C t 9343? us , Company Name PaclnD Petroietim Cz , Inc. Form Approved, OMS No. 20%-0039 3. Emengeocy Response Phone 4. Maront Tracking Numtm .4-�., - 0150r�7326 JJK ;eneratoes Site Address (if drfferent Bran mailing address) 2W EIR ; D _7 Sx v LUIS u6iS 0, Cr ;3431 US CAD"�1 164312 8 Designated Facility Name and Site Address U.S. EPA ID Number L" HEMIt;.AL ti `.�1STE MA1waGEAIEiaT, rNl: C ATW,k,+ 17 35251 OLD SK, JNE ROAD KETUIVIAN CITY, CA 93259 US Fadkty's Phorce: 559%M6.9711 9a. 9b. U.S. DOT Description (including PW Shipping Nam. Hazard Class. ID t1 cnber, 16. Conte oars 11. To al 12. Unit 13 Waste Codes HM and Packing Group (lany)) No. Type Quantity WINoI. X 1' R4, UN3077, EN`JiRONMENT4Lt , riA24RDOJ& S R.^TAN(E SOL rJ /y CM�) ?1.O.S tI-EaD 14. Special HareM rg hatruc6at and Amuontl Inkmnabon ©�� y L! rJear ah,appropna!e PPEf J (I 24 Houf' rMergeroy Re6Wse vt lbw 925-1947 Proitle R CA51-OW, 15. GENERATOR'SM EROR'S CERflFICATION: I M ereb/ declare tltat the contents of this consignment are hilly and accurately described above by the proper shipping narm, and are classified, paw, marked and labeledlplacarded, and are in all respects in proper condition for transport according to applicable international and national govemmatal regulations. l export shipmenl and I am Cie Primary Exporter, I certify Ctat the content of this consignment conform to the term of the attached EPAAclu vwiedgment of Consent. I barfly itat the waste malrnvaticn statement identified in 40 CFR 262.27{a) (l l am a large quantity genemlor) or (b) it I am a —0 a ty generator) is true. '°.'"`°'"°'""" '" ._ Li import to U.S. Transporter signature (ter exports only'): 17.Transporter AdIMMOdPOMofReceipt dMaterials Transporter 1 Pmdedrryped Name UAki P N 18.Disaepancy 188. Discrepancy Indication Space 0On* Type 18b. Alerate Facility(or Generator) J U ua Fad6ty's Phone: ExportfmmU.S. Portofentrylexit. Date leaving U.S.: ❑ Residue LJ Partial Reiectiar U S. EPA ID Number (I I ?a ❑ Full Rejection N19. Hazardous Waste Report Management Method Codes p.e.• codes 1a hazardous waste treatment disposal and recyc1mg systems) LU 1 xx �J 4 3 4 2. "`"5 20. Designated Facility Owner or Operator: Cartirrabon of receipt or hazardous materials covered by Cie manifest except as noted in 11em 18a Month Year Pmfedrryped Name SignaWre � ( 4 EPAFam870022(Rev.3051Previousedlionsagao wte• DESIGNAT6FACILITY TOGENERATOR STATE (IF REQUIRED) C 1w. ls Landfill Reprint 3 ,Road, P.O. Box 471 Ticket# 55679 Ke*A%1wm&u►r"dwE4iA, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667327JJK Grid B18 Volume Yards Carrier CAD981164312 Driver JAVIER Vehicle # G383 Vehicle License 65425M1 Container # 4ND3836 Container License 4ND3836 Time Scale Operator In 06/04/2021 11:44 MANUAL WT A. Ortega Gross 77000 lb* Out 06/04/2021 13:31 A. Ortega Tare 44020 lb* * Manual Weight Net 32980 lb Tons 16.49 Comments Inbound Product Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------- 1 CALH DISP-TONS-Cal 100 16.49 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 SANLUISOBI 4 FUEL -Fuel Surcharg 100 SANLUISOBI 5 RCR-P-Regulatory C 100 SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature APPENDIX B Lab Summary Spreadsheets c d a °C po o U a'"I 0No 14 00 V1 Vf W C O toV NO k -D 00 ON J r-I N r-I rl m 00 N V1 W N j J J~ tl� le lz lz n Z 6 22 N 6 N O M N z Q f� N O N (O V O O O V) O 0 0 N 0 0 0 0 _ �. � O n N CO N M N N LO u N .-I N tOl Ol I- 00 N ei NNM O � v^ w In.-iLD00mv q°° ow o� `^�oo 3 oov o a Ee m N O fV i O i, O V1 4.1 Ln O Cl O M W ON I N M 00 r� N O0 4 0 01 � 01 01 In NO W y V V p v �!1 r-I O O i� r-I Ct 00 D O a-i V O O� W Y O CO Y N C hbn cM E m � 1 E C G1 0 E a 3 y p v 0 V +�+ E E N E O a3+ u v O O O 2 E •� •� E S N 3� � .O �� s` O (7 O u+ N �TIZ (�6 N O u > C u C U Q. V c a 1,21 a f6 m N m t6 U 0 U y J Z N V1 tN t H> N N U 2 la— H pNp c o a d oC O O -4 e-I coN 0000 y N W C O � vi W N LO fD n r• LO00N O O N 0 CD M N r LO f- N N MU _ j O O O p LO N O O O N O O O 0 �� 00 N p O OD fV M N LO Q U U p N lDD N ri N �n 0) � O In N O " Nm Ln V a�-I 00 O QOj - � 01 ct DO fT C) ^ Ln O O r^-I Ln V V V • ai 0 6 v v v CDO m m N O O M O N O fT O t O01 O O'A 'n O n 9 -4 N N M V N v 0 6 ry-i a --I �7 N 0 0 'yi V pv pv u1 1� O O c v 'm a fn O N oo fT O CD �r1 N O y 01 rl M N y lD p O� QM1 O N O u1 rl N ri V v N v �' N O O N 0 0 V OV OV t0 00 O O c v co U M M O O M r-1 O lO N O a --I 'D Q1 L^f1 O O� N O OrIO N N M V . -I V N V 6 N 0 p-1 N a --I i--I O v O r� N W O O a a v am E tN .O m M O N O O-* N n N M p N fT ^ M p y N O t\ v V V •--i N 0 6 � fn a-i 0 r4 o) V O O r 00 O O O C V V v v v v 00 Q emn N O N Ln rl O a, to N O a --I n e-i m p^ O 01 00 01 N N O p O rl N M y v v y N O O -4-I N d' `"� 0 0 ryi V 0 0 0^ D O C v v V V m W • N N O O N w O 00 [t N O fT cn M y c O 0 tD m ri N O L/l W N M y V V tD N O O a I `� M 00 O a I V 0 0 0 Lo D O + v V O m t V Ln a --I N^ O �' Nr1i ri M m N lD ? fD W Ln LnO Ln 0 o m = al tM \M bbn tw w m X E E E N N b0 a— cc U W E 3 3 b\A oc O £ y E 'E d Q o 0 u m E E j a� E o o Y 3 41 tp o a, o O > r °' O E E .� E ,. fa Q > Y � c — M s u t u u z C7 C CL c J C > L -a O L-0 a O m ai O u °' a, > m c C a u U C Z u Q Q tp CO a1 CO to U s U 0 U 0 U-j 22 Z fn N H> N -f u N N U 2 F F- H coN c ° d d°C po0� o 0No'A 00 J Vf Nf W C E O O O OG � M h H W N GJ�1 H ul _� O n oOD N O N COO N N D O O p 0 0 0 0 0 0 0 0 0 0 0 J Ln U)O n O N N O N O N 0 0 O N 0 S 000 co U L r0+ f\ 0 Ln 0 Ln N O? 0o OV --t N Ov N ^ N N W n Ln •--� p M O V 00 M •-i N LD O 00 V^ M v v V^ c�-I O O v C L� O O N �? O N lD ei M p LIl 00 �' Ol V V V V L" � 0 0� r-I CP ei O Q oo V O r-i M Ln W v V V V V V) ar E LA V ^ p N p V N v M v Ln p ON N Ov Ln � Qn m 00 p 41 � O O O I� 0) O ?� O v O V 0 C lD ON N NC, N N 00 O Ln ^O n a-i O1 Ln V aN-.I V V v0 ', O O N M U5 O O N V O .-� W Ln W z d O (n O O M 00 O O N rl Ln Ol M 00 U ei V V n V O O it l0 3 eNi v v o v v v z Y C on Y E (0 op 00 C ccE H m Y y O w O V a0+ c E E j > 01 E E a3+ u r�'o N O O CcO C O 7 ++ (0 N Q U >T N `� (0 O U' 0 O 0JOu>G Li a- 0- V i Q i Q m Ln GJ co m U L U O U O U W J Z w= Ln in t H> m N = H coN Q f0 CE _ C N N (n N O N O — m 4- o W cLa Q O l0 J C yy O d •N O O W ONO -1-1 000 J H H W C O U u •CD NO O 0 00 O N l0 00 J N w r-I M N Vf W 2 J O D O O O �O O n p 0 0 00 0 N 0 O N O M 6 N 0 � 0 !Q 0 h 0 N 0 O N O p N 0 O 0 O 0 O 0 N U J O In O In O O n O O N O O N O p N 0 O 0 N 0 0 O 0 f` 0 N 0 O 0 N 0 N C 0 N 0 N i Q SO M O u v ;° 0 O 1N 00 m O o) It Ln N w 00 0 OO OO 00 o °1 0) Ql M O O N i i Ln O N V M ri O M r-I LD cj O V O V -4 a--1 O O O O C V V m Go Ln 14 CDM O � LnLn c) Ol � O In N O w 00 LnO N w 0) r1 I-q ^O �� Ql O 01 Ol O u1 M 00 m i i N N V') M O V lO N V V � r-I V M O O C V m a co � `� Ln 00 Ln Ol 1n rn Ln N r-I ^ n MM N M d' 00 al CF M 00 O N V M 1'1 O In 00 N O O r-1 In p` I V O O C V m u 1n O u N O M 0) O O n O M N OO ` ^OM 0 0O0 0 0-- M O oq O N V r-I O V VV.Im E C 'm O m 6 O O N 0) pc; O Ln r-I r-I � Ln 00of 00 M M NO , Nm Nrn v00 V -1 gn OVVV O O O f0 H C m V ,°n a O O Vl rj O O ei Ln O O r4 M M Ol �' O M fV O u"f aN-1 w N Ol O 00 O M M O N V V `'"I O V^ N V V M O V V V O O C V GG U qt cn 00 O c)O^ Cl) 0 O In In N O cn O ri Ql O N O d' C) V r4 p y n N 0 0 c1 n 0 0 N V O ai V M M O N O V co m Ol O 00 O O 1n Ol O lD O N 00 N O O O a-i `� tD O N m M00 O I.p I O M Ol i-.j O C^ O M O r-1 Ol N I i r1 M v e-ir-I O V I� N OV OV r I M p. a I V O O m a ^1 00 Ict � O Ocn OLn � al NO O N N 4 ^ cn OpN OO N VVO ppM VV O V V V V a-i mC Y � O) OO to 0\0 00 E c m00 0 m w X E E cEw�� �0\0 E =E a,�'� 7 0\0 y - p N 0 U +�+ E E 0) -a E 7 O O- 'C O •- C f0 7 +. m O O 9 O 3 3 E +� co ` !Z cOi j a� 'c — s U 0 O U f0 C U 'O C7 C i y N O u> Qj t li C C 2 2 2 t0 G C f6 00 N 00 co U s U O U 0 U J Z to V1 H to E N F- !- F- U U 00 U N N In H F T f0 E C_ C N N In N O M N i N 0 O•ca m n a- LLQ O m J c '60°J o00 O l0 k 0 W Ix J a1 N ei 00-4-4 000 � V1 H W C O b O p 0 0 O 00 CD N 1.0 00 J r-I nj � a1 M N Uj W 41 9 J J~ 0 Q 0 O O 0_ O N 0 0 O 000 0 N 0 O N O M a N 0 a— 0 lA 0 0 N 0 O N 6 O 25 O N O 11i O z O In O lfi O N fO J O O O O O O N O U O N M O O a— O O IT N O N O N O a — O N N _ a O OO N M N O u U M LD o N 1O N 00 mT -T N 41 p � 00 00 00 � n Q1 00 O N N V o M O O N v) M O O S a1 `1 � 3 p oq O O ai O O M 00 O i i i O ei v v v v V V V V C CC m O f" OT lZ ^ 0 n O N 1A N M ^ O O p N Ln 00 W O O M O p M N i i i C 1 N V v O V W O� Ol NO O N V O n p O C v LO � a 00 E �p M N O Vl O 0 Ln Ula1 N 00 O O O O ci O N V N a1 I� l0 V^ M O O a 4 rq 0t O a1 � V O V M N O 4- ci v v v v v ai m C V N 0w0 00 p O V1 O OM G1 tD 1- O O O Ol `""� O O 01 .* M O W N p r, 00 0 , 00 O O N V� a1 O V ai p a1 �f1 a1 M 0 a-. V O V O V O O O O H E v V V 00 m co � LQ M 0 l0 00 a1 N N Ol 00 O N o O N a�I 00 O V aOI N p ,1 a1 LO d O ai a1 V M p O O CV v v a�I 00 a � coc l9 V p N t!) O N N O CD M � M l0 M O a, m a --I Ln m M^ 00 00 i i N O C N a'i O V M O a1 a-1 ry�j 0 0^ v V p OD 00 0) b00 bbnOn \ b\A c OJ fb Y E, E W bp cc w E 3 \ b0 E bA 4. C O CEO E i �, E d 'Q O h O U +�+ C E E j �, OJ E E O Q_ "O E O -8 7 @ O '� C7 N O O ar O u E 2 .� +� N -U 7 �• O c Nra 7 t U 0 U a) J m U t Uw y L m L -0 O CL= O N O U �> i f6rJJJJJa- N U U r H U Q a [� 00 U U U U J Z V) Ln F— H H N j— N H VI H Fa- ONO !n m C -coO :3 N N O Cl) O L m U 0. o f6 J c d 000 O o O tD M Lo 00 � � N tD rI r-I J J W f^ C E bo 000 O O kD v U rl N10 N 00 O J J H W V1 IA 0l H In lD lfi 00 N � N O -. C.,Lo Il- N O U') O M to N U D O O � O 0 0 0 0 0 0 0 0 0 J O O r T U) N N N M N lIi I- N 0 O LO N O O i Q � � 000 Cl) O U 3 O N cn O NO p a vMm tD Ol M pO tD NDo O. ^N 00 00 N O O OVV -4�O O pip V V V VE 7 N 'a W 3 r-I Ol p N O O1 N N lD CF 0 r-I r, � 0) Cl) 0) V O1 00 r' �I M p 'i 4 V O O -i 1� p V V V V 0 0 V m H M >c W W r-iO N M N Il M N N M e-i M N p cn O1 n M Ol M 0) 4.1 O M� `- v vl M O p `-I `-I o0 O N `-i V p p- .--I m V y y V V V d fl. x MID N M lD 00 N al Ol 0 lD r-1 Q1 lD DO M r-q rl V V N ui O O lD O r-I M A N V O O lD H~ 3 jp 3 lD Ol p N N O N lD M N p N Dl M O O p V V Ul y `"'� O D c-I N N V Oy M N V V 0 v^ v 0 W 3 Lti O O M q ct N t7 Lfl Vl 00 M 00 Ol M N y y `� 0 0 r-I M N Q M tD V O O lD al V V V� Vf 3 Ql O O N Ql O N I� oo e I O O O m m 00 01 O1 N V VlLn V 00 a--1 O p ei N Ol O N^ N V O O M M O y y V V V y Z Y \ CU 000 0\0 00 C Y E N m OG own C a: —_ \ \ o E E E .0 N O () +�+ E j �. 01 E E O "a "O 3 m N ++ CCG1 L oC E U i 7 •7 '� c0 N O. 7 U >• N C L 'a �p L U G% J J o 'C�.. c? 0 c N- o-0 a v o u v> Fa c c0 U U a C 0- N a a f6 [0 w CO m U .`c U O U O U O Z y in in L H i N U i H U 'i0 l0 E C C NO N 7 N O A M N o U m N M a `0 m J c bo v r 1D oo vocq� -I J J ul W Vf C O p O t0 W u N 1D N 00 M � r, J J CA W Nf 1/1 J > H to LO O �O n 22 N O N O M O N O Ci 0 0 f6 U 2 O O O ti LO N O 00 0 N 0 N 0 M 0 N V N O U, Q U H � y' CL ^ ^ 0 Ln O Lq N 00 lD rl i- 00 p 00 00 O1 p 00 ? lD 0) I- Ol N� O O V p 0 V n rI fn M C 0 V rq V O V O* V w E V o 1� p Ln O ? 01 O N N a --I lD 1, O 00 cn d' al M N 00 O V LI1 O O -CTr-I N i-i p m u p p M N O V O V V V V U z N 01 N O N N l0 M OLn N e q 01 M M Ln Ln � 00 a V Ln p . �--I . .N-I . cn 0 0 e4 Ln 4 N V O V 00 00 .O V V V O V V v Vf Ln QlC a O O Ln 111 ^ Ln N Dp LO 00 �p p tD Ln Ln 01 VV' V N O V� O O r" M Ol a-i O nj M V p V ro V V v CA O lD M� N �n 00 M O n e-i TT 0) Ln Vl a 01 ^ O N Ln N O O` N lD I� OV M 4 V 0 0` 4 •-i V V V V V V V p V (A 00 Y v to E On v bA f0 w Y v C C IA DA N N C r O v M 0 £ 1 N i C v C Q) H C O y � p N L O j j +�' c E E= > v E E:3 •a3+ u r00 v O O � �, '''' 3 m pT, O cO L O u E 7 O +' r0 N 0_ 7 u T ` 3 -p (0 O 'L8 U 2 0 p m u a ++ � L a C rya N O u v> c0 (0 u O C 2 2 t0 O( v O V i a a (0 m v m f6 U t U 0 U 0 U 0 J Z v VI in L H> IV U S H CL CL 0N0 APPENDIX C Site Photographs AV Jf •� - � µ'di � 1 •� � �� I i•' ' �- •. �. ^.. � f _oil ice( fir• L i ..• - �y�__ , yam' i - •. J y v .A a -' .ram'• `- - - - -_ - { .. ^sti r - - r•` ior- ,fi ,. �r • + . it f � 1 ;f AO :r� I F; Im North Wall. )401 Law 2 — !st 7r "Ok, 71 -1 Nd6v 1 -IrElm Ol A* our A# 4f m zip Ak At ti•., �� �'. .. "-.�_ , rF.'.7.s':� r 'ter.✓ Ale "r J`-fir �+1 �'+ ," '= � .. �C. � y T� � � /`�" I r,`• 4 t 1 i^� �; - " • - `* =err Excavation Floor. Fact Wall " � ~'� • �• - ''~f �' � i�'Y-tip - �� 1 j,n �� = w' —M". - - r .� '-•�'1�',' * -,,t. "fir. F _ - `y!• y�� _ -3f •vA' .�. Ali �'�3i' .� � - _ .. `, 4 may. •• - ,_-�. � 1 `�: �,•� .:r ~ •_ -'' �, �1 'ty,� All dip •< .� • •- _ �'r .: _ - .. : kiwi . �� '� r-�' � _. ." �•� ram• ,r v� - . �_ti• � �:i .... a � `��"' '.Y J• -.+I Y-` vow _ ./y J � ✓ � � �� w.I�. . �� fir:-w' �- �N- �y� • .i_ ray_ .. � . � '` • }�s/"'• �� '7/, �„�' �'.� - - •�, `• � h�_ , L. - _ '1��.•. , ti � _ � '�r �.-� r :•.: -.fir � J1 East and South Wall lid - ±�~- :�� �, ���•f�.. � � . MA S_ K ,�"{ ;� may. � . - S Y � �FM1 ti _ . • P ..�• _� . ti . r •1 - _ • .9 �� ♦ %CAAti: Sr� _ t tii}'. i -' ''*tom. ► y �` lk low 1r � h. � 7 ''� 'V �'-�� r�y �rilr` '1•.� � r!r � ti!•''. 10 PL 4 f AO All �,� •. �S� � .. "�t-�t%r�� - • - y; � .- - � 1. - ' r; '� � ' � } .. Qmr APPENDIX D Laboratory Reports & Chain of Custody Forms Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds Pacific Petroleum California P. O. Box 2646 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street OEC Work Order: Report Date: 2103479 June 09, 2021 16:44 Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com This laboratory is accredited in accordance with the recognised International Standard ISO/IEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-IAF Communique dated April 2017) 307 Roemer Way, Suite 300 ''klllllp'/�. client.oec.com\reports Santa Maria, CA 93454 `�� www.oecusa.com Main: (805) 9224772 PJLA TNI 2016 & ISO/IEC 17025:2017 Fax: (805) 925-3376 : ����.N� ,�sclna CA-ELAP 2438, TNI 02666 Accreditation #99137 Page I of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Summary Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom East @ 12' 2103479-01 Solid Solid 06/03/2021 11:50 06/04/2021 12:50 Bottom West @ 12' 2103479-02 Solid Solid 06/03/2021 11:55 06/04/2021 12:50 Sample Batch Preparation Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B I F0145 06/04/2021 16:24 STLC Metals by 1CP 601013 STLC B I F0261 06/09/2021 08:56 STLC Metals Extraction STLC` Metals Extraction B 1 F0229 06/07/2021 16:29 Total Metals by CVAA Mercury Total EPA 7471 A B I F0194 06/07/2021 07:40 Total Metals by ICP 6010B Total B I F0197 06/07/2021 08:26 Volatile Organic Compounds by GUMS 926013 Full List B 1 F0146 06/04/2021 12:21 Volatile Organic TPH by GC/F1D 8015 TPH-Gasoline B 1 F0154 06/04/2021 10:34 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples 11 Sample ID : Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mg/kg 1 B 1 F0194 06/07/21 16:25 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B 1 F0197 06/07/21 14:12 EPA 601 OB Arsenic 5.6 1.9 " " Barium 1211 0.93 " " " Beryllium ND 0.47 " ^ Cadmium ND 0.23 Chromium 73 0.47 N-02 Cobalt 18 0.47 Copper 47 0.93 Lead 8.2 0.47 Molybdenum ND 0.47 Nickel 130 0.47 " Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 49 1.9 Zinc 65 1.9 STLC Metals by ICP Chromium ND 0.020 mg/L 2 B I F0261 06/09/21 14:34 STLC/EPA 601 OB Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) ND 4.5 mg/kg 1 Bi F0154 06/04/21 17:01 EPA 8015M Surrogate: 4-Bromo/luoroben_ene 92 %, (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-C22) ND 10 mg/kg I BIF0145 06/05/21 12:12 EPA 8015M TPII Motor Oil (('23-C40) ND 50 Surrogate: o-Terphem•l 87 (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 32 ( A WAMM im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kb 1 BIF0146 06/04/21 16:16 EPA8200B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobcnzcne ND 0.050 Chloroethanc ND 0.050 Chloroform ND 0.050 Chloroniethane ND 0.050 2-Chlorotoluene ND 0.050 4-Chlorotoluene ND 0.050 " Dibromochloromethane ND 0.050 1.2-Dibromo-3-chloropropane ND 0.050 1,24)ibrotnoethane (EDB) ND 0.050 Dibromomethane ND 0.050 1,2-Dichlorobenzene ND 0.050 1,3-Dichlorobenzcnc ND 0.050 1,4-Dichlorobenzcnc ND 0.050 Dichlorodifluoromethane ND 0.050 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 I,l-Dichloroethene ND 0.050 cis-12-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 2,2-Dichloropropane ND 0.050 1. 1 -Dichloropropene ND 0.050 " cis-1,3-Dichloropropcne ND 0.050 trans-13-Dichloropropcne ND 0.050 " Ethylbcnzene ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCI11 CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 32 --I Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples I Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlombutadiene ND 0.050 mg/kg 1 BIF0146 06/04/21 16:16 EPA8260B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1,1,1,2-1'etrachloroethane ND 0.050 1.1,2.2-Tetrachloroethane ND 0.050 Torachlorocthcne (PCE) ND 0.050 Toluene ND 0.050 1,2,3-Trichlorobenzcnc ND 0.050 1,2,4-Trichlorobenzene ND 0.050 " 1,1,1-Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 " Trichloroethene (TCE) ND 0.050 Trichlorofluoromethane ND 0.050 1,2.3-Trichloropropane ND 0.050 1,2,4-Trintethylbenzene ND 0.050 1,3,5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Dibromolluoromethcmr 103 N (74 - 122 ) Surrogate: Toluenc-d8 99 Y (65 - 128 ) Surrogate: 4-Bromo/luorobeu=eue 10.5 % (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 6 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 I Analytical Report for Samples I Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg I B1F0194 06/07/21 16:27 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1F0197 06/07/21 14:15 EPA 6010B Arsenic 7.4 1.9 Barium 160 0.96 Beryllium ND 0.48 . _ Cadmium ND 0.24 Chromium 51 0.48 Cobalt 14 0.48 Copper 63 0.90 Lead 8.9 0.48 Molybdenum 0.57 0.49 Nickel 88 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 52 1.9 Zinc 71 1.9 STLC Metals by ICP Chromium ND 0.020 mg/L 2 B I F0261 06/09/21 14:37 STLC/EPA 6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) ND 4.4 mglkg I BIF0154 06/04/21 17:29 EPA 8015M Sin-rogute: 4-Bromo/laoroben:ene 95 ` (39 - 157) N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 9.9 mg/kg 1 BIF0145 06/05/21 12:34 EPA 8015M TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Teiphen.11 90 % (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 '- Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.048 mglkg I B 1 F0146 06/04/21 15:48 EPA 8260B Bromobenzene ND 0.048 Bromochloromethane ND 0.048 Bromodichloromethane ND 0.048 - Bromoform NI) 0.048 Bromomethane ND 0.048 n-Butylbenzene NI) 0.048 " sec-Butylbenzene ND 0.048 tert-Butylbenzene ND 0.048 " Carbon tetrachloride NI.) 0.048 Chlorobenzcnc ND 0.048 Chloroethane ND 0.048 " C'hlorotonn NI) 0.048 Chloromethane ND 0.048 2-Chlorotoluene ND 0.048 4-C'hlorotoluene ND 0.048 Dibromochloromethane ND 0.048 1,2-Dibronto-3-chloropropane ND 0.048 1,2-Dibromocthane (EDB) ND 0.048 Dibromomethane ND 0.048 1.2-Dichlorobenzene ND 0.048 ' 13-Dichlorobenzene ND 0.048 14-Dichlorobenzene ND 0.048 " Dichlorodifluoromethane ND 0.048 - 1, 1 -Dichloroethane ND 0.048 1,2-Dichloroethane ND 0.048 1,1-Dichloroethene ND 0.048 cis-1.2-Diehl oroethene ND 0.048 " trans-l.2-Dichloroethene ND 0.048 " 1,2-Dichloropropane ND 0,048 I.3-Dichloropropane ND 0.048 2,2-Dichloropropane ND 0.048 1, 1 -Dichloropropene ND 0.048 cis-1.3-Dichloropropanc ND 0.048 trans-1,3-Dichloropropcne NI) 0.048 Ethylbenzene ND 0.048 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 0.048 mg/kg 1 BIF0146 06/04/21 15:48 EPA8260B 4-Isopropyl Toluene ND 0.048 Isopmpylbenzene ND 0.048 Methylene chloride ND 0.048 Naphthalene ND 0.048 n-Propylbenzene ND 0.048 " Styrene ND 0.048 1,1,1,2-1'etrachloroethane ND 0.048 " 1,1,2,2-Tetrachloroethanc ND 0.048 Tetrachlorocthcne WCF.) ND 0.048 Toluene ND 0.048 1,23-Trichloroben7ene ND 0.048 1.2,4-Trichlorobenzene ND 0.048 1, 1, 1 -Trichloroethane ND 0.048 1,1,2-Trichloroethane ND 0.048 Trichloroethene (TCE) ND 0.048 Trichlorolluoromethane ND 0.048 12,3-Trichloropropane ND 0.048 1,24-Trimethylbenzene ND 0.048 1,3.5-Trimethylbenzene ND 0.048 " Vinyl chloride ND 0.048 Xylenes (total) ND 0.048 " Surrogate: Dihromotluoromedmne 104 % ( 74 - 122 ) Surrogate: Toluene-d8 102 / ( 65 - 1 28) Surrogate: 4-SromoJhunnben_ene 104 °b (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 H Page 10 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO194 -EPA 7471A Preparation: EPA 7471A Pre1 Blank (B1F0194-BLKI) Mercury ND LCS (B1F0194-BSI) Mercury 0.782 LCS Dup (B1F0194-BSDI) Mercury 0.859 Duplicate (B1F0194-DUPl) Source: 2103489-02 Mercury ND Matrix Spike (B1F0194-MS1) Source: 2103489-02 Mercury 0.827 Matrix Spike Dup (B1F0194-MSD1) Source: 2103489-02 Mercury 0.839 Post Spike (B1F0194-PSI) Source:2103489-02 Mercury 5.52 06/07/21 07:40 Analyzed: 06/07/21 12:49 0.10 mg/kg Analyzed: 06/07/21 12:53 0.10 mg/kg 0.833 94 85-115 Analyzed: 06/07/21 13:30 0.10 mg/kg 0.833 103 85-115 9 20 Analyzed: 06/07/21 13:34 0.097 mg/kg ND 20 Analyzed: 06/07/21 13:37 0.091 mg/kg 0.755 ND 110 75-125 Analyzed: 06/07/21 13:39 0.089 mg -kg 0.742 ND 113 75-125 1 20 Analyzed: 06/07/21 13:41 ug/L 25.0 0.00199 22 85-115 QL-02 The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 -EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLKI) Analyzed: 06/07/21 13:30 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 Molybdenum ND 0.50 Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 " Thalliimi ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 LCS (BIF0197-BS1) Analyzed: 06/07/21 13:35 Antimony 92.0 2.5 mg/kg 100 92 80-120 Arsenic 97.2 2.0 100 97 80-120 Barium 99.6 1.0 100 100 80-120 Beryllium 95.1 0.50 100 95 80-120 Cadmium 98.2 0.25 100 98 80-120 Chromium 98.8 0.50 100 99 80-120 Cobalt 99.2 0.50 100 99 80-120 Copper 98.2 1.0 100 98 80-120 Lead 100 0.50 100 100 80-120 Molybdenum 96.0 0.50 100 96 80-120 Nickel 99.6 0.50 100 100 80-120 Selenium 96.4 2.0 100 96 80-120 Silver 4.92 0.50 5.00 98 80-120 Thallium 100 1.0 100 100 80-120 Vanadium 90.6 2.0 100 97 80-120 Zinc 98.6 2.0 100 99 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 32 r A 16M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 -EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSD1) Analyzed: 06/07/21 13:37 Antimony 94.8 2.5 mg/kg 100 95 80-120 3 20 Arsenic 98.8 2.0 100 99 80-120 2 20 Barium 101 1.0 100 101 80-120 1 20 Beryllium 96.5 0.50 100 96 80-120 1 20 Cadmium 99.2 0.25 100 99 80-120 1 20 Chromium 100 0.50 100 100 80-120 1 20 Cobalt 100 0.50 100 100 80-120 1 20 - Copper 99.8 1.0 100 ]00 80-120 2 20 Lead 101 0.50 100 101 80-120 1 20 Molybdenum 98.2 0.50 100 98 80-120 2 20 Nickel 101 0.50 100 101 80-120 1 20 Selenium 97.9 2.0 100 98 80-120 1 20 Silver 4.93 0.50 5.00 99 80-120 0.1 20 Thallium 102 1.0 100 102 80-120 1 20 Vanadium 98.0 2.0 100 98 80-120 1 20 Zinc 99.8 2.0 100 100 80-120 1 20 Duplicate (B1F0197-DUPl) Source: 2103489-01 Analyzed: 06/07/21 13:52 Antimony ND 2.4 mg/kg ND 20 Arsenic 1.22 1.9 ND 20 Barium 21.0 0.97 22.9 8 20 Beryllium ND 0.49 ND 20 - Cadmium ND 0.24 ND 20 Chromium 1.94 0.49 2.02 4 20 Cobalt 1.40 0.49 1.78 24 20 QR-04 - Copper 1.33 0.97 1.40 5 20 Lead 1.23 0.49 1.40 13 20 Molybdenum ND 0.49 ND 20 Nickel 1.31 0.49 134 2 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium f 3.86 1.9 4.18 8 20 Zinc 4.32 1.9 4.51 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MSI) Source: 2103489-01 Analyzed: 06/07/21 13:40 Antimony 70.3 2.3 mg/kg 93.4 ND 75 10-116 Arsenic 93.3 1.9 93.4 ND 100 77-121 Barium 119 0.93 93.4 22.9 102 30-169 Beryllium 90.1 0.47 93.4 ND 96 86-111 Cadmium 91.8 0.23 93.4 ND 98 81-112 Chromium 96.8 0.47 93.4 2.02 102 75-129 Cobalt 94.2 0.47 93.4 1.78 99 71-121 Copper 96.2 0.93 93.4 140 102 68-135 Lead 94.4 0.47 93.4 1.40 100 72-121 Molybdenum 88.2 0.47 93.4 ND 94 70-112 Nickel 95.2 0.47 93.4 1.34 101 73-121 Selenium 90.1 1.9 93.4 ND 97 76-116 Silver 4.56 0.47 4.67 ND 98 54-132 Thallium 92.3 0.93 93.4 ND 99 64-120 Vanadium 96.5 1 9 93.4 4.18 99 78-124 Zinc 98.0 1.9 93.4 4.51 100 50-143 Matrix Spike Dup (B1F0197-MSD1) Source: 2103489-01 Analyzed: 06/07/21 13:42 Antimony 70.4 2.4 mg/kg 95.8 ND 73 10-116 0.1 20 Arsenic 94.3 1.9 95.8 ND 98 77-121 1 20 Barium 116 0.96 95.8 22.9 97 30-169 3 20 Beryllium 91.2 0.48 95.8 ND 95 86-111 1 20 Cadmium 92.3 0.24 95.8 ND 96 81-112 0.6 20 Chromium 97.6 0.48 95.8 2.02 100 75-129 0.8 20 Cobalt 94.7 0.48 95.8 1.78 97 71-121 0.6 20 Copper 96.9 0.96 95.8 1.40 100 68-135 0.7 20 Lead 94.9 0.48 95.8 1.40 98 72-121 0.6 20 Molybdenum 88.6 0.48 95.8 ND 93 70-112 0.5 20 Nickel 95.5 0.48 95.8 1.34 98 73-121 0.3 20 Selenium 91.2 1.9 95.9 ND 95 76-110 1 20 Silver 4.64 0.49 4.79 ND 97 54-132 2 20 Thallium 93.1 0.96 95.9 ND 97 64-120 0.9 20 Vanadium 97.2 1.9 95.8 4.18 97 78-124 0.7 20 Zinc 103 1.9 95.8 4.51 103 50-143 5 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PS1) Source: 2103489-01 Analyzed: 06/07/21 13:45 Antimony 2.03 mg/l. 2.00 0.00248 101 75-125 Arsenic 2.04 2.00 0.0178 101 75-125 Barium 2.50 2.00 0.460 102 75-125 Beryllium 1.96 2.00 0.00219 98 75-125 Cadmium 2.00 2.00 -0.00308 100 75-125 Chromium 2.07 2.00 0.0408 101 75-125 Cobalt 2.06 2.00 0.0359 101 75-125 Copper 2.06 2.00 0.0293 102 75-125 Lead 2.07 2.00 0.0283 102 75-125 Molybdenum 2.01 2.00 -0.00109 101 75-125 Nickel 2.06 2.00 0.0271 102 75-125 Selenium 1.99 2.00 -0.0103 99 75-125 Silver 0.0945 0.100 -0.00169 94 75-125 Thallium 2.03 2.00 -0.00407 WI 75-125 Vanadium 2.08 2.00 0.0842 100 75-125 Zinc 2.10 2.00 0.0909 101 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0261- STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (BlF0261-BLK1) Analyzed: 06/09/21 13:50 Chromium ND 0.010 mg/l. LCS (B1F0261-BS1) Analyzed: 06/09/21 14:17 Chromium 10.1 0.010 mg/L 10.0 LCS Dup (BlF0261-BSD1) Analyzed: 06/09/21 14:19 Chromium 10.2 0.010 mg/L 10.0 Duplicate (BlF0261-DUP1) Source: 2103218-01 Analyzed: 06/09/21 14:27 Chromium 1.22 0.020 mg/l, 1.22 Leach Fluid Blank (B1F0261-LBKI) Analyzed: 06/09/21 13:52 Chromium ND 0.020 mg/L Leach Fluid Blank (BlF0261-LBK2) Analyzed: 06/09/21 13:55 Chromium ND 0.020 mg/L Leach Fluid Blank (BlF0261-LBK3) Analyzed: 06/09/21 13:58 Chromium ND 0.020 mg/L 101 80-120 102 80-120 0.5 20 0.08 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic TPH by 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLKI) Analyzed: 06/04/21 12:45 TPH Gasoline (C5-02) ND 0.49 mg/kg Surrogate.4-BromofTuorobenzeue 0.107 " 0.123 87 39-157 LCS (B1F0154-BS1) Analyzed: 06/04/21 11:48 TPH Gasoline (C5-C]2) 1.38 0.50 mg/kg 0.998 138 69-139 Surrogate:4-Brontolluorohenzene 0.15E 0.125 126 39-157 LCS Dup (B1F0154-BSDI) Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12) 1.29 0.50 mg/kg 1.00 128 68-139 7 20 Surrogate:4-Bromofluorohenzene 0.146 0.125 116 39-157 Duplicate (B1F0154-DUPI) Source: 2103455-02RE1 Analyzed: 06/04/21 15:35 TPH Gasoline (('5-C12) ND 0.50 mg/kg 0.113 20 Surrogate:4-Bromoflnorobenzene 0.113 110.124 92 39-157 Matrix Spike (B1F0154-MS1) Source: 2103429-02 Analyzed: 06/04/21 19:23 TPH Gasoline (('5-C12) 0.905 0.49 mg/kg 0.973 ND 93 10-171 Surroguie:4-Bromo/luorohenzene 0.132 " 0.122 109 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Drcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Semi -Volatile Organic TPH by 1 - Quality Control 77! Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) Analyzed: 06/04/21 11:45 TPH Dicscl (C13-('22) ND 10 mg!kg TPH Motor Oil (C23-C40) NI) 50 " Surrogate: o-Terphe»rl 41.5 50.0 83 65-136 LCS (B1F0145-BSI) Analyzed: 06/04/21 11:45 TPH Diesel ((',73-C22) 434 10 mg/kg 499 87 72-115 TPH Motor Oil (('23-C40) 420 50 499 84 74-126 Surrogate: o-Tciphenrl 45.8 49.9 92 65-136 LCS Dup (B1F0145-BSDI) Analyzed: 06/04/21 12:07 TPH Diesel (C13-C22) 444 10 mg/kg 499 89 72-115 2 20 " TPH Motor Oil (C23-C40) 441 50 499 88 74-126 5 20 Surrogate: o-Tciphcnrl 46.7 49.9 94 65-736 Duplicate (BIF0145-DUPl) Source: 2103472-01 Analyzed: 06/04/21 16:23 TPH Diesel (C13-C22) NI) 10 mg/kg ND 20 TPH Motor Oil (C23-C40) N1) 50 ND 20 Surrogate: o-Teiphen.l 40.5 49.9 81 65-136 Matrix Spike (B1F0145-MS1) Source: 2103472-01 Analyzed: 06/04/21 15:37 TPH Diesel (C13-('22) 452 10 mg!kg 498 ND 91 46-147 TPH Motor Oil (C23-C40) 500 50 498 ND 100 35-171 Surrogate: o-Teiphernl 41.6 49.8 84 65-136 Matrix Spike Dup (B1F0145-MSD1) Source: 2103472-01 Analyzed: 06/04/21 16:00 TPH Diesel (C13-C22) 496 10 mg/kg 498 NJ) 100 46-147 9 20 TPH Motor Oil (('23-C40) 517 50 498 ND 104 35-171 3 20 Surrogate: o4i,iphenyl 44.0 49.8 88 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 mum fflff__M� Page 18 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1) Analyzed: 06/04/21 11:32 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 Bronromethane ND 0.0050 " n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 " Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 " Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 " 12-Dibromoethane (EDB) ND 0.0050 " Dibromomethane ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " 1,3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 " DichlorodiFluoromethanc ND 0.0050 CCHI 1, 1 -Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 " I,1-Dichloroethene ND 0.0050 " cis-L'_-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " 1,2-Dichloropropene ND 0.0050 " 1,3-Dichloropropene ND 0.0050 " 22-Dichloropropene ND 0.0050 1, 1 -Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethylbenzene ND 0.0050 Hexachlorobutadiene ND 0.0050 4-1sopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilet piControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLKI) Analyzed: 06/04/21 11:32 Styrene ND 0.0050 mg'kg 1,1,1,2-Tetrachloroethane ND 0.0050 " 1,12,2-Tetrachloroethane ND 0.0050 Tetrachloroethane (PCE) ND 0.0050 " Toluene ND 0.0050 " 1,2,3-Trichlorobenzene ND 0.0050 " 1,2,4=1Yichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 " L1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorotluoronrethane ND 0.0050 1,2,3-Trichloropropane ND 0.0050 " I.2,4-Trimethylbenzene ND 0.0050 1,3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylenes (total) ND 0.0050 Surrogate: Uihrumq/7uorunicthunc 0.0516 0.0498 104 74-122 Surrogate: Toluene-d8 0.0503 0.0498 101 65-128 Surrogate: 4-Bromq/luorobenzene 0.0529 0.0498 106 7 5- 121 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 Benzene 0.0406 0.0050 mg/kg 0.0398 102 70-131 Bromobenzene 0.0466 0.0050 0.0398 117 74-130 Bromochloromethane 0.0399 0.0050 0.0398 100 64-133 Bromodichloromethane 0.0445 0.0050 0.0398 112 69-137 Bromotonn 0.0447 0.0050 0.0398 112 55-132 Bromomethane 0.0407 0.0050 0.0398 102 10-142 u-Butylbenzene 0.0476 0.0050 0.0398 120 64-156 sec-Butylbenzene 0.0493 0.0050 0.0398 124 75-155 tert-Butylbenzene 0.0482 0.0050 0.0398 121 74-144 Carbon tetrachloride 0.0442 0.0050 0.0399 111 67-135 Chlorobenzene 0.0445 0.0050 0.0398 112 73-134 Chloroethane 0.0390 0.0050 0.0398 98 10-167 C'hlorofonn 0.0412 0.0050 0.0398 104 69-124 Chloromethane 0.0297 0.0050 0.0398 75 34-136 2-Chlorotoluene 0.0454 0.0050 0.0399 114 75-135 4-C:hlorotoluene 0.0460 0.0050 0.0398 116 70-138 Dibromochloromethane 0.0439 0.0050 0.0398 110 67-135 1,2-Dibromo-3-chloropropanc 0.0435 0.0050 0.0398 109 41-149 1,2-Dibronroethane (EDB) 0.0409 0.(1(150 0.0398 103 68-131 Dibromomcthanc 0.0433 0.0050 0.0398 109 61-140 1,2-Dichlorobenzene 0.0458 0.0050 0.0398 115 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 1,3-Dichlorobcnzenc 0.0462 0.0050 mg/kg 0.0398 116 76-138 1.4-Dichlorobenzene 0.0457 0.0050 0.0398 115 72-132 Dichlorodifluoromcthanc 0.0210 0.0050 0.0398 53 10-155 1, 1 -Dichloroethane 0.0389 0.0050 0.0398 98 63-139 1,2-Dichloroethanc 0.0416 0.0050 0.0398 104 64-126 I,1-Dichloroethene 0.0342 0.0050 0.0398 86 52-167 cis-1 2-Dichloroethene 0.0401 0.0050 0.0398 101 70-135 trans-1,2-Dichloroethene 0.0392 0.0050 0.0398 99 67-147 1,2-Dichloropropane 0.0406 0.0050 0.0398 102 68-131 1,3-Dichloropropane 0.0405 0.0050 0.0398 102 64-129 - • 2,2-Dichloropropane 0.0432 0.0050 0.0398 109 63-154 1,1-Dichloropropene 0.0393 0.0050 0.0398 99 68-138 cis-1,3-Dichloropropene 0.0416 0.0050 0.0398 105 72-134 trans- l,3-Dichloropropene 0.0437 0.0050 0.0398 110 69-132 Ethylbenzene 0.0449 0.0050 0.0398 113 68-136 11exachlorobutadiene 0.0546 0.0050 0.0398 137 72-198 4-Isopropyl Toluene 0.0504 0.0050 0.0398 127 74-150 Isopropylbenzene 0.0473 0.0050 0.0398 119 71-149 Nlethylene chloride 0.0346 0.0050 0.0398 87 51-127 Naphthalene 0.0492 0.0050 0.0399 121 57-158 n-Propylbenzene 0.0474 0.0050 0.0398 119 70-143 . Styrene 0.0456 0.0050 0.0398 115 68-138 1, 1, 1,2-Tetrachloroethane 0.0459 0.0050 0.0398 115 76-130 1,1,2,2-Tctrachloroethanc 0.0399 0.0050 0.0398 100 60-136 Tetrachloroethene (PCE) 0.0443 0.0050 0.0398 111 73-138 Toluene 0.0430 0.0050 0.0398 108 72-128 1,2,3-Trichlorobenzene 0.0507 0.0050 0.0398 127 61-166 1,2.4-Trichlorobenzene 0.0502 0.0050 0.0398 126 71-158 _ 1, 1, 1 -Trichloroethane 0.0424 0.0050 0.0398 107 71-135 1. 1 .2-Trichloroethane 0.0414 0.0050 0.0398 104 64-132 Trichloroethene (WE) 0.0442 0.0050 0.0398 111 74-139 Trichlorofluorontethane 0.0429 0.0050 0.0398 108 30-156 1,2,3-Trichloropropane 0.0452 0.0050 0.0398 114 67-123 1,2,4-Trimethylbenzene 0.0454 0.0050 0.0398 114 68-134 1,3,5-Trimethylbenzene 0.0461 0.0050 0.0398 116 71-140 Vinyl chloride 0.0326 0.0050 0.0398 82 43-144 Xylenes (total) 0.133 0.0050 0.119 112 69-138 Surrogate. Uibromq/luorum(,thcttTe 0.0525 0.0497 106 74-122 Surrogate: T)luene-dh' 0.0517 0.0497 104 65-128 Surrogate: 4-Bromothtorohenzene 0.0530 0.0497 107 75-121 CCFH The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control �Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit i Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (BIF0146-BSDI) Analyzed: 06/04/21 10:13 Benzene 0.0423 0.0050 mgikg 0.0400 106 70-131 4 20 Bromobenzene 0.0498 0.0050 0.0400 124 74-130 7 20 Bromochlorotncthane 0.0412 0.0050 0.0400 103 64-133 3 20 Bromodichloromethane 0.0455 0.0050 0.0400 114 69-137 2 20 Bromotirrm 0.0458 0.0050 0.0400 115 55-132 2 20 Bromomethane 0.0391 0.0050 0.0400 98 10-142 4 20 n-Butylbenzene 0.0476 0.0050 0.0400 119 64-156 0.1 20 sec-Butylbenzene 0.0508 0.0050 0.0400 127 75-155 3 20 tert-Butylbenzene 0.0496 0.0050 0.0400 124 74-144 3 20 Carbon tetrachloride 0.0456 0.0050 0.0400 114 67-135 3 20 .- Chlorobenzcne 0.0457 0.0050 0.0400 114 73-134 3 20 Chloroethane 0.0394 0.0050 0.0400 98 10-167 1 20 Chloroform 0.0421 0.0050 0.0400 105 69-124 2 20 Chloromethane 0.0308 0.0050 0.0400 77 34-136 4 20 2-Chlorotoluene 0.0452 0.0050 0.0400 113 75-135 0.4 20 4-Chlorotoluene 0.0468 0.0050 0.0400 117 70-138 2 20 Dibrmnochloromethane 0.0463 0.0050 0.0400 116 67-135 5 20 1,2-1)ibmmo-3-chloropropane 0.0461 0.0050 0.0400 115 41-149 6 20 1,2-Dibromoethane (EDB) 0.0422 0.0050 0.0400 105 68-131 3 20 Dibronumrcthane 0.0459 0.0050 0.0400 115 61-140 6 20 1,2-Dichlorobenzene 0.0472 0.0050 0.0400 118 76-136 3 20 1,3-Dichlorobenzene 0.0489 0.0050 0.0400 122 76-138 6 20 1,4-Dichorobenzene 0.0472 0.0050 0.0400 118 72-132 3 20 Dichloroditluoromethane 0.0229 0.0050 0.0400 57 10-155 8 20 LI-Dichloroethane 0.0405 0.0050 0.0400 WI 63-139 4 20 1,2-Dichloroethane 0.0425 0.0050 0.0400 106 64-126 2 20 1,1-Dichloroethene 0.0347 0.0050 0.0400 87 52-167 2 20 cis-1,2-Dichloroethene 0.0420 0.0050 0.0400 105 70-135 5 20 trans-1,2-Dichloroethene 0.0401 0.0050 0.0400 100 67-147 2 20 1,2-Dichloropropane 0.0430 0.0050 0.0400 107 68-131 6 20 1,3-Dichloropropane 0.0426 0.0050 0.0400 106 64-128 5 20 2,2-Dichloropropane 0.0446 0.0050 0.0400 111 63-154 3 20 1,1-Dichloropropene 0.0406 0.0050 0.0400 102 68-138 3 20 cis-1.3-Dichloropropene 0.0434 0.0050 0.0400 108 72-134 4 20 trans-1,3-Dichloropropene 0.0454 0.0050 0.0400 114 69-132 4 20 Ethylbenzene 0.0470 0.0050 0.0400 118 68-136 5 20 Ilexachlorobutadiene 0.0549 0.0050 0.0400 137 72-198 0.5 20 4-Isopropyl Toluene 0,0514 0.0050 0.0400 128 74-150 2 20 Isopropylbenzene 0.0499 0.0050 0.0400 125 71-149 5 20 _ [Methylene chloride 0.0360 0.0050 0M400 90 51-127 4 20 Naphthalene 0.0511 0.0050 0.0400 128 57-158 6 20 n-Propylbenzene 0.0466 0.0050 0.0400 116 70-143 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCFH CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: 805 925-3376 Page 22 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 ,_. LCS Dup (B1F0146-BSDl) Analyzed: 06/04/21 10:13 Styrene 0.0479 0.0050 mg/kg 0.0400 120 68-138 5 20 1,1.1,2-T-etrachloroethane 0.0490 0.0050 0.0400 123 76-130 7 20 1,1,2,2-Tctrachloroethanc 0.0417 0.0050 0.0400 104 60-136 5 20 Tetrachloroethene IPCE) 0.0454 0.0050 0.0400 114 73-138 3 20 Toluene 0.0439 0.0050 0.0400 110 72-128 2 20 1,2,3-Trichlorobenzene 0.0520 0.0050 0.0400 130 61-166 3 20 1,2,4-Trichlorobenzene 0.0512 0.0050 0.0400 128 71-158 2 20 1, 1, 1 -Trichloroethane 0.0432 0.0050 0.0400 108 71-135 2 20 1,1,2-Trichloroethane 0.0448 0.0050 0.0400 112 64-132 8 20 Trichloroethene (TCE) 0.0448 0.0050 0.0400 112 74-139 1 20 - Trichlorofluoroniethane 0.0430 0.0050 0.0400 107 30-156 0.1 20 12,3-Trichloropropane 0.0463 0.0050 0.0400 116 67-123 3 20 1.2,4-Trimethylbeuzene 0.0459 0.0050 0.0400 115 68-134 1 20 1,3,5-Trimethylbenzene 0.0465 0.0050 0.0400 116 71-140 0.9 20 Vinyl chloride 0.0338 0.0050 0.0400 84 43-144 3 20 Xylenes (total) 0.139 0.0050 0.120 116 69-138 4 20 Surrogate. Dibronzulluoromethanc 0.0519 0.0500 104 74-122 Surrogate: Ttduene-d8 0.0510 0.0500 102 05-128 Surrogate:4-Bromolluorobenrene 0.0530 0.0500 106 75-121 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromethanc ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromoform ND 0.0050 ND 20 Bronroniethane ND 0.0050 ND 20 u-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 teit-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 C hlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropanc ND 0.0050 ND 20 12-Dibrontoethane (EDB) ND 0.0050 ND 20 Dibromomcthane ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. ISIo" S CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: (805) 925-3376 Page 23 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 ISIONNS 1,3-Dichlorobenzenc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromcthanc ND 0.0050 ND 20 CCHI ],I-Dichloroethane ND 0.0050 ND 20 1,2-Dichloroethane ND 0.0050 ND 20 I,1-Dichloroethene ND 0.0050 ND 20 cis-1.2-Dichloroethene ND 0.0050 ND 20 trans- l,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1, 1 -Dichloropropene ND 0.0050 ND 20 cis-1,3-Dichloropropene ND 0.0050 ND 20 trans- l,3-Dichloropropene ND 0.0050 ND 20 F.thylbenzene ND 0.0050 ND 20 tlexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0,0050 ND 20 1,1,1,2-Tetracliloroethane ND 0.0050 ND 20 1,1,2,2=Fetraclhlorocthanc ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,23-Trichlorobenzene ND 0.0050 ND 20 1.2,4- Trichlorobenzene ND 0.0050 ND 20 l,l.l-Trichloroethane ND 0.0050 ND 20 1.1.2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorofluoromethanc ND 0.0050 ND 20 1,2,3-Trichloropropmie ND 0.0050 ND 20 L2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibrotnofhtoromcvhane 0.0538 0.049E 108 74-122 Surrogate: Toluene-d8 0.0509 0.0498 102 65-128 Sarrogam:4-Bromolluorohenzene 0.0506 0.0491 102 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 _ www.oecusa.com FAX: (805) 925-3376 • Page 24 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Method Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NF.LAI' 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8o15M Solid OEC. CA-ELAP,NF.LAP STLC Metals by ICP 601013 STLC Chromium STLC/EPA 601013 Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Water OEC, Internal Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, Internal Total Metals by ICP 6010E Total Antimony EPA 6010B Solid OEC, CA-ELARNELAP 601013 Total Arsenic EPA 601013 Solid OEC, CA-F.LAP,NELAP 601013 Total Barium EPA 6010E Solid OEC, CA-ELARNELAP 6010B Total Beryllium EPA 601013 Solid OEC, CA-ELARNELAP 6010B Total Cadmium EPA 601013 Solid OEC, CA-ELAPNELAP 601013 Total Chromium EPA 6010B Solid OEC. CA-FLARNELAP 6010E Total Cobalt EPA 601013 Solid OEC, CA-ELARNELAP 601013 Total Copper EPA 6010B Solid OEC, CA-ELARNELAP 601013 Total Lead EPA 6010B Solid OEC, CA-ELARNELAP 6010E Total Molybdenum EPA 6010E Solid OEC, CA-ELARNELAP 60111E Total Nickel EPA 001013 Solid OFC, CA-ELAP,NEL.AP 6010E Total Selenium EPA 6010E Solid OEC, CA-ELAPNELAP 6010E Total Silver EPA 6010E Solid OEC, CA-ELAPNELAP 6010E Total Thallium EPA 6010E Solid OEC. CA-ELAP,NEI,AP 6010E Total Vanadium EPA 6010B Solid OEC, CA-ELAPNELAP 6010E Total Zinc F,PA 6010B Solid OEC, CA-ELARNELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA-F.LARNFLAP 8260B Full List EPA 8260E Solid OEC, Internal Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 DefinitionsNotes and Qualifier Definition MIN Method I,)etection Limit RL Reporting Limit (Quantitation Limit) ND Analyle NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference CCFli The CCV for this analyte tailed high. Results for this analyte may be biased high. CCHI The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. ISIowS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above I Ox STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC: control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 26 of 32 W JAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 32 7 x U rl 0 Q x a N E-i LO O O w X 4-) Pq � LO rl U N ry C O •r-I / Ul N z � D a / N Ln Q N O Q G., / rl CJ N .4 [x] CD O x N 1 U rn Q Guar U 75-� h U / C7 0 Ln -I(S)o UUo N�--i rl N S4 N C O A u-0 rvzw E 0 � H Z S4 N wI + o + o 0 0 (4 S-I r-I a i-I J-) Qa4 U r-I G IAA) M N `- -ri P4 U G N •ri •ri N r + 0 r cn 0 u� to I � �o 0 �o 0 d 0 Lq Oi 0 I � I rn 0 Ln co 0 0 00 0 Ui r' O 0 0 Lq co O (D O LO rn O O O 0 v I O O o ri O I O co O N O O N O l00 o 0 0 0 0 0 0 0 0 0 M N N W � (00 lL E F _Q 0 LL_ V O LL 2 0O k Ca W • H �' PO � I � to O Q W � O TS C O / .0 1-1 4-) (N N O tT �o U C) r� N C h C N Q Q O N N r S4 / O Q F H Ln O � H / r-I O O W N I x O� w x h U (Y) / t7 0 rl u v .. .. .. .. .. .. .. N Sa +-) N C (6 04 s4-0 (1)z44 FZ O N E C C 10 0 0 0 0 0 0 0 0 0 0 0 0 0 o O o J-) F4 C N H Z. 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Q U 00 ; z ❑ r w- L9 a w �.a F r o o 3 N E t z V V m G m 0 m❑ O y e u m� x no c C cc V o N 4 v E `Dv h cpsd C ~ 17 N E m (6 +� 8 C L .� N 1n er >, fl. m (n o� OI { vo o m N79 t , Q c �oLin w a O 00 U 0 rn'n N p ❑❑ m m 0 m CD d o F F Q CL �' L L M G o s o ►- m '� c c c N .a. E m U U E ►� i= '1 N z O H N z Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2103212 Pacific Petroleum California P. O. Box 2646 Report Date: May 28, 2021 10:05 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 24, 2021 13:05 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page I of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom West Center 2103212-01 Solid Solid 05/24/2021 11:20 05/24/2021 13:05 Bottom East Center 2103212-02 Solid Solid 05/24/2021 11:25 05/24/2021 13:05 Bin 20339-A 2103212-03 Solid Solid 05/24/2021 11:30 05/24/2021 13:05 _ Bin 20339-B 2103212-04 Solid Solid 05/24/2021 11:35 05/24/2021 13:05 Bin 20339-C 2103212-05 Solid Solid 05/24/2021 11:40 05/24/2021 13:05 Bin 20144-A 2103212-06 Solid Solid 05/24/2021 11:45 05/24/2021 13:05 Bin 20144-B 2103212-07 Solid Solid 05/24/2021 11:50 05/24/2021 13:05 Bin 20144-C 2103212-08 Solid Solid 05/24/2021 11:55 05/24/2021 13:05 Sample Batch Preparation — . Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B 1 E0696 05/25/2021 08:55 - STLC Metals Extraction STLC Metals Extraction B I E0743 05/26/2021 08:58 TCLP Metals by 1CP 001013 TCLP B 1 E0794 05/27/2021 10:55 TCLP Metals Extraction TCLP Metals Extraction B I E0744 05/26/2021 09:03 Total Metals by CVAA Mercury 'total EPA 7471 A B I E0694 05/25/2021 07:50 Total Metals by ICP 601013Total 131 E0693 05/25/2021 07:26 Volatile Organic Compounds by GC/MS 8260B Full List B 1 E0697 05/25/2021 09:00 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B 1 E0737 05/26/2021 06:59 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 57 C A OM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercurc 0.22 0.093 mgikg 1 B I E0694 05/25/21 14:04 EPA 7471 A Total Metals by ICP Antimony ND 2A mg/kg 1 BIE0693 05/25/2114:18 EPA 601OB Arsenic 7.0 1.9 Barium 560 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 120 0.48 N-02, N-03 Cobalt 21 0.48 Copper 43 0.96 Lead 7.3 OAS Nlolvbdenum 0.62 0.48 Nickel 160 0.48 " Selenium ND 1.9 " Silver ND 0.48 Thallium ND 0.96 Vanadium 46 1.9 Zinc 56 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B 1 E0794 05/27/21 19:15 EPA 1311 /EPA 601 OB Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) ND 0.50 mg/kg 1 BI E0737 05/26/21 13:56 EPA 8015M Surrogate: 4-Bromo/luorobenaene 10/ 111, (39 - 157) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 57 AT, B M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical t Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 51 10 mglkg 1 B I E0696 05/25/21 14:26 EPA 8015M TPFI Motor Oil ((:23-C40) ND 50 11 11 11" 11 Surrogate: o-kiphentd 90'% 1 65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 57 r A r a MW Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples I Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mglkg 1000 B 1 E0697 05/25/21 15:16 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 -- Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND L2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 r 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 1.4-Dichlorobcnzenc ND 1.2 Dichloroditluoromcthanc ND 1.2 l,l-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1. 1 -Dichloroethene ND 1.2 - cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dieliloropropane ND 1.2 1.3-Dichloropropene ND 1.2 2,2-Dichloropropene ND 1.2 1.1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 F.thylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 5 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg(cg 1000 B I E0697 05/25/21 15:16 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbeozene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 1,1,12-Tetrachloroethane ND 1.2 " 1.1,2,2-1'etrachloroethane ND 1.2 Tetrachlorocthenc WCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcnzcne ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 " 1,2,4-Trimethylbenzene ND 1.2 " 13,5-Triinethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromoiluoromethane 1111 `% (74 - 122) Surrogate: Toluene-tM 102 % (65 - 12 4 ) Surrogate: 4-Bromo1luorobenfene 97 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mg/kg 1 B I E0694 05/25/21 14:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 E0693 05/25/21 14:21 EPA 601 OB Arsenic 6.6 1.9 Barium 220 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 120 0.48 N-02, N-03 Cobalt 19 0.48 " Copper 39 0.96 Lead 8.3 0.48 Molybdenum ND 0.49 Nickel 150 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 51 1.9 Zinc 62 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/L I B I E0794 05/27/21 19:17 EPA 1311 /EPA 601 OB Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) 2.2 0.50 mg/kg I BIE0737 05/26/21 15:34 EPA 8015M D-04 Surrogate: 4-Bromo/luo1-oben_ene 118"% (39 - 157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 330 10 m80cg 1 B I E0696 05/25/21 14:03 EPA 8015M TPH Motor Oil (C23-C40) ND 50 11 11 11 11" Surrogate: o-Teiphenrl 108,111, (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg kg 1000 B 1 E0697 05/25/21 15:43 EPA 8260B Broniobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " .-• Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chloroclhanc ND 1.2 Chlorofonn ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 13-Dichlorobenzene ND 1.2 14-Dichlorobenzene ND 1.2 Dichlorodinuoromethane ND 1.2 " 1,1-Dichloroethene ND 1.2 1,2-Dichloroethene ND 1.2 LI-Dichloroethene ND 1.2 - , cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Fuylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples I Sample ID : Bottom East Center Sampled : 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mbtkg 1000 B1 F0697 05/25/21 15:43 F.PA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tctrachlorocthenc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzcne ND 1.2 1.2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1.2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1,2.4-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 12 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromofluoronnetkanc 101 Y. (74 - 122) Surrogate: Toluene-d8 102 9b (65 - 128 ) Surrogate: 4-Bromq/luorobencene 96 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples I Sample ID : Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.099 mg/kg 1 B 1 E0694 05/25/21 14:08 EPA 7471 A Antimony ND 2.5 mg/kg 1 B 1 E0693 0.5/25/21 14:24 EPA 601(1B _ Arsenic 5.1 2.0 Barium 230 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 N-02, N-03 Cobalt 21 0.49 Copper 47 0.99 Lead 11 0.49 I%lolvbdenum 0.74 0.49 f Nickel 190 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 62 2.0 "Zinc 72 2.0 TCLP Metals by ICP Chromium ND 0.050 nr,/L 1 BIE0794 05/27/21 19:20 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) -- 4.2 0.50 mg/kg 1 B I E.0737 05/26/21 16:26 EPA 8015M D-04 Surrogate: 4-Bronw luurohen:ene HS % (39 - 157) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples I Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GUND TPI1 Diesel (C13-C22) 350 10 TPH Motor Oil (C23-C40) 55 50 Surrogate: o-Teipher1•1 112 mg/kg 1 B1 F.0696 05/25/21 15:12 EPA 8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BIE0697 05125/2116:11 E.PA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 . Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibronio-3-chhxopropane ND 1.2 12-Dibronroethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodifluoromethane ND 1.2 ' l,l-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 " cis-1.2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND L2 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 " Ll-Dichloropropane ND 1.2 cis- 1.3 -Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 F.thylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples a Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mgtkg 1000 BIE0097 05/25/21 16:11 EPA8260B 4-Isopropyl Toluene ND 1.2 " " " " " Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND L2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 Tolucnc ND 1.2 I.2,3-Trichlorobenzcnc ND 1.2 1.2,4-Trichlorobenzene ND 1.2 1. 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (WE) ND 1.2 Trichlorotluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,2,4-Trintethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: 102 Y" (74 - 122 ) Surrogate. Toluenc-dig 103 °o ( 65 - 138 ) 11 11" Surrogate. 97 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 57 (M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Saniples Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 rng/kg 1 B I E0694 05/25/21 14:10 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B 1 E0693 05/25/21 14:26 EPA 601 OB Arsenic 10 1.9 Barium 290 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 710 0.48 N-02, N-03 Cobalt 47 0.48 " Copper 52 0.96 Lead 13 0.48 Molvbdenum 1.2 0.48 Nickel 1900 0.48 N-02 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 77 1.9 Zinc 83 1.9 TCLP Metals by ICP Chromium ND 0.050 nigrL 1 BIE0794 05/27/21 19:23 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) 0.76 0.50 mg/kg 1 BIE0737 05/26/21 17:I8 EPA 8015M D-04 Surrogate: 4-Bromg17eorohen_ene 101 (39 - 157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 57 WIL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-B Sampled : 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (C13-C22) 71 10 mg/kg I B1 F0696 05/25/21 13:41 F.PA 9015M TPII Motor Oil (C23-C40) ND 50 1. 11 11" 11 Surrogate: o-Tetphen. l 106 `% (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 57 r "M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mgIg 1000 BlF0697 05/25/21 16:38 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butvlbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromonrethane ND 1.2 12-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromcthane ND 1.2 l,l-Dichloroethane ND 1.2 12-Dichloroethane ND 1.2 l,l-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I-1-Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Fthylbenzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 17 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 B I E0697 05/25/21 16:38 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 " Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tctrachloroethene 1PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1.2.4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcnes (total) ND 1.2 Surrogate: Dibromolluoromethune 100 ` o (74 - 122) " Surrogate: Toluene-d8 101 ( 65 - 118 ) Surrogate: 4-Bromoiluorobc'n_ene 97 ( 75 - 121 ) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 18 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 1.4 0.092 mg/kg 1 B 1 E0694 05/25/21 14:12 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B1E0693 05/25/2114:13 EPA 6010B - Arsenic 6.1 2.0 Barium 220 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 140 0.50 Cobalt 21 0.50 l Copper 46 LO Lead 19 0.50 hlolvbdenum 0.57 0.50 " Nickel 180 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND H) " Vanadium 54 2.0 Zinc 87 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/1. 1 BIE0794 05/27/2 1 19:25 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: 4-Bromotluorobenrene N-02, N-03 2.3 0.50 mgikg 1 BI E0737 05/26/21 19:53 EPA 8015M D-04 107'-L (39- 157) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical i Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (03-C22) 390 10 mglkg I B 1 E0090 05/25/21 14:49 EPA 8015M TPH Motor Oil (C23-C40) ND 50 11 1. 11" 1. Surrogate: o-k1phemd 105 % (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.3 mg�kg 1000 BIE0697 05,125/21 17:05 EPA8260B Bromobenzene ND 1.3 Bromochloromethane ND 1.3 Bromodichloromethane ND 1.3 Broniol'ortn ND 1.3 Bromomethane ND 1.3 n-Butylbenzene ND 1.3 sec-Butylbenzene ND 1.3 " tert-Butylbenzene ND 1.3 Carbon tetrachloride ND 1.3 " Chlorobenzcnc NI) 1.3 Chlorocthane ND 1.3 Chlorotorm NI) 1.3 Chloromethane ND 1.3 2-Chlorotoluene ND 1.3 4-C'hlorotoluene ND 1.3 Dibromochloromethane ND 1.3 1,2-Dibromo-3-chloropropane ND 1.3 " 1,2-Dibromoethane (EDB) ND 1.3 Dibromomethane NI) 1.3 1,2-Dichlorobenzcne NJ) 1.3 1,3-Dichlorobcnzcne ND 1.3 1,4-Dichlorobcnzcne ND 1.3 Dichlorodifluoromcthane ND 1.3 l,l-Dichloroethane ND 1.3 1,2-Dichloroethane ND 1.3 ],I-Dichloroethene ND 1.3 cis-1.2-Dichloroethene ND 1.3 trans-1,2-Dichloroethene ND 1.3 1,2-Dichloropropane ND 1.3 1,3-Dichloropropane ND 1.3 2,2-Dichloropropane NI) 1.3 I,I-Dichloropropene ND 1.3 cis-1.3-Dichloropropene ND 1.3 " trans-1,3-Dichloropropene ND 1.3 Fthylbenzcne ND 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 57 r A "6M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 I lexachlorobutadiene ND 1.3 mg�kg 1000 B 1 E0697 05/25/21 17:05 EPA 8260B 4-Isopropyl Toluene ND 1.3 Isopropylbenzene ND 1.3 Methylene chloride ND 1.3 Naphthalene ND 1.3 n-Propylbenzene ND 1.3 Styrene ND 1.3 1,1,1,2-1'etrachloroethaue ND 1.3 1,1,22-Tetrachloroethane ND 1.3 Tctrachlorocthcnc (PCE,) ND 1.3 " Toluene ND 1.3 1,2,3-Trichlorobenzene ND 1.3 1,24-Trichlorobenzene ND 1.3 1, 1, 1 -Trichloroethane ND 1.3 1,1,2-Trichloroethane ND 1.3 Trichloroethene (TCE) ND 1.3 Trichlorofluoromethane ND 1.3 1,2,3-Trichloropropane ND 1.3 1,2,4-Trimethylbenzene ND 1.3 13.5-Trimethylbenzene ND 1.3 Vinyl chloride ND 1.3 Xylencs (total) ND 1.3 Surrogate: Dihnnnolluoromethane 1024; (74= 122) Surrogate: Toluene-dS 102 % ( 65-:128 ) Surrogate: 4-Bromo/luorohen_ene 9S 46 (75- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 22 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.23 0,093 mg/kg 1 B 1 E0694 05/25/21 14:14 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I B 1 E0693 05/25/21 14:37 EPA 601(1B Arsenic 4.9 2.0 Barium 230 0.99 Beryllium ND 0.50 . Cadmium ND 0.25 Chromium 150 0.50 N-02, N-03 Cobalt 25 0.50 " rl Copper 49 0.99 " Lead 41 0.50 Molybdenum 0.69 0.50 Nickel 190 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 " Vanadium 60 2.0 Zinc 82 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/l- 1 Bl E0794 05/27/21 19:28 EPA 1311 %EPA 601(1B Volatile Organic TPH by GC/FID TPII Ga-wlinc (CS-C12) 1.5 0.50 mg/kg 1 Bl E0737 05/26/21 20:45 EPA 8015M D-04 Surrogate: 4-Bromoguoroben_ene 115 % (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 23 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-A Sampled : 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 370 10 mg�kg 1 B 1 E0696 05/25/21 14:49 EPA 8015M —� "rPH Motor Oil (('23-C40) ND 50 Surrogate: o-kiphenrl 102 o (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 8D5 925-3376 Page 24 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BIE0697 05/25/21 17:33 EPA8260B Bromobenzene ND 1.2 Bronrochlorotnethane ND 1.2 Bromodichloromethane ND 1.2 " Bromofortn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzene ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichloroben7ene ND 1.2 " I A-Dichlorobenzene ND 1.2 " Dichlorodithtoromethane ND 1.2 " 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 12 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 " 1, 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlombutadiene ND 1.2 mgIg 1000 BIE0697 05/25/21 17:33 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene 2.8 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 " 1,2,3-Trichlorobenzene ND 1.2 " 1,2.4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethenc (TC E) ND 1.2 Trichlorotluoromethane ND 12 1,2,3-Trichloropropane ND 1.2 " 1,2,4-Trimcthylben7enc ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate Dibromojluoromethane 99 3;, (74 - 122) " Strrrogatr: lbluene-d8 102 (65 - 128) " Surrogate: 4-Bromolluorohenfene 96 ib ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl1ent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical t Sample ID : Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Dlercurc 0.19 0.093 mg/kg I Bl E.0694 05/25/21 14:16 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I E0693 05/25/21 14:40 EPA 6010B Arsenic 4.6 2.0 Barium 180 099 Beryllium ND 0.49 " Cadmium ND 0.25 Chromium 150 0.49 Cobalt 19 0.49 Copper 40 0.99 Lead 24 0.49 Molybdenum ND 0.49 Nickel 150 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 50 2.0 "Zinc 77 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BIE0794 05/27/2119:30 EPA 1311/EPA6010B N-02, N-03 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 2.2 0.50 mg!kg 1 B I E0737 05/26/21 21:36 EPA 8015M D-04 Surrogate: 4-BromoJluorohenzene 108 % (39 - 157) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 27 of 57 r A I sn Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7 Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C 13-C22) 320 9.9 mg/kg 1 B I E0696 05/25/21 15:12 EPA 8015M 7'Pll Motor Oil (C23-C40) ND 50 11 11 11 11" Surrogate: o-krpheml 95 % ( 65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mglkg 1000 B1 F0697 05/25/21 18:00 EPA 8200B Broniobenzene ND 1.2 Bronxichloromethane ND 1.2 Bromodichloromethane ND 1.2 --• Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 C'hlorobenzcnc ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 +� 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 1,4-Dichlorobcnzenc ND 1.2 Dichloroditluoromethane ND 1.2 -r 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1.1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 tans-1,2-Dichloroethene ND 1.2 12-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1-1-Dichloropropane ND 1.2 cis-1.3-Dichloropropenc ND 1.2 ' trans-1,3-Dichloropropcnc ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 29 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled : 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B I F.0697 05/25/21 18:00 F.PA 9260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene 2.3 1.2 n-Propylbenzenc ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachlomethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 ^ I.2,3-Trichlorobenzene ND 1.2 1,2.4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 1,2,3-Trichloropropanc ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 " Xylenes (total) ND 1.2 Surrogate: 1)ihromnlLrorourctltaue 100 % ( 74 - 12' ) Surrogate: Toluene-418 102 (65. 128) Surrogate: 4-Brom0/luorohen_cne 98 44, (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 30 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mg/kg 1 B 1 E0094 05/25/21 14:18 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I B I E0693 05/25/21 14:42 EPA 6010B Arsenic 5.0 2.0 Barium 1411 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 N-02, N-03 Cobalt 23 0.49 Copper 45 0.98 Lead 14 0.49 Nlolvbdemmni ND 0.49 Nickel 190 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 50 2.0 Zinc 71 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B I E0794 05/27/21 19:40 EPA 1311 T A 6010B Volatile Organic TPH by GOOD TPH Gasoline (C54712) 2.1 0.49 mg/kg 1 BIE0737 05/26/21 22:29 EPA 8015M D-04 Surrogate: 4-Bronw luoroben_cne 119 % (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples 1i Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 560 10 mg/kg TPI I Motor Oil (C23-C40) ND 50 1. Surrogate: o-leiphemd 120 /, (65 - 136 ) I B 1 E0696 05/25/21 14:26 EPA 8015M The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-337ti Page 32 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples 0 Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mglkg 1000 B 1 E0697 05/25/21 18:28 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromediane ND 1.2 " Bromofortn ND 1.2 " Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " .- sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 " Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 " 1.2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobenzene ND 1.2 " 1,4-Dichlorobenzene ND 1.2 Dichlorodifluoromethanc ND 1.2 " I,I-Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 " 1, 1 -Dichloroethene ND 1.2 " cis-L2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 " 1.1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-l.3-Dichloropropene ND 1.2 " F.thylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples 11 Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 llexachlorobutadiene ND 1.2 mgtkg 1000 B 1 E0697 05/25/21 18:28 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 •— Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 " I.1.1,2-Tetrachloroethane ND 1.2 I.1,2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne WE') ND 1.2 " Toluene ND 1.2 I.2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 l,l,l-Trichloroethane ND 12 — 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluorometbane ND 1.2 _ 1,2.3-Trichloropropane ND 1.2 1,2.4-1'rimethylbenzene ND 1.2 1,3,5-Triniethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dihronnolluoroinethanc 99 % (74 - 122 ) Surrogate• Toluene-a`8 1111 IN ( 65 - 128 ) Surrogate: 4-Bromo/luornhen_ene 96 In,, ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 34 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by CVAA - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - - Level Result Limits Limit Batch BlE0694 - EPA 7471A Preparation: EPA 7471A Prep 05/25/21 07:50 —• Blank (B1E0694-BLK1) Analyzed: 05/25/21 13:31 Mercury ND 0.10 mgkg LCS (B1E0694-BS1) Analyzed: 05/25/21 13:27 Mercury 0.840 0.10 mg'kg 0.833 101 85-115 LCS Dup (BlE0694-BSD1) Analyzed: 05/25/21 13:29 Mercury 0.949 0.10 mg/kg 0.833 102 85-115 1 20 Duplicate (B1E0694-DUP1) Source: 2103193-05 Analyzed: 05/25/21 13:47 Mercury 0.216 0.18 mg/kg 1.87 159 20 QR-04 Matrix Spike (BlE0694-MSI) Source: 2103193-05 Analyzed: 05/25/21 13:51 Mercury 1.04 0.093 mgAg 0.776 1.87 NR 75-125 QD1-07 Matrix Spike Dup (BlE0694-MSD1) Source: 2103193-05 Analyzed: 05/25/21 13:53 Mercury 1.69 0.090 mg/kg 0.751 1.87 NR 75-125 47 20 Q11-07, QR-04 Post Spike (BlE0694-PSI) Source: 2103193-02 Analyzed: 05/25/21 15:19 Mercury 5.28 ug/L 5.00 0.114 103 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 57 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Totalby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0693 -EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 -� Blank (BlE0693-BLK1) Analyzed: 05/25/21 14:02 Antimony ND 2.5 mg'kg Arsenic ND 2.0 " Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 Chromium ND 0.50 " �. Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " '- Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 " LCS (B1E0693-BS1) Analyzed: 05/25/21 14:45 Antimony 99.7 2.5 mg/kg 100 100 80-120 Arsenic 99.6 2.0 100 100 80-120 Barium 102 1.0 100 102 80-120 Beryllium 98.2 0.50 100 98 80-120 Cadmimn 100 0.25 100 100 80-120 Chromium 99.5 0.50 100 100 80-120 Cobalt 101 0.50 100 WI 80-120 Copper 101 1.0 100 101 80-120 Lead 102 0.50 100 102 80-120 Molybdenum 97.8 0.50 100 98 80-120 Nickcl 101 0.50 100 101 80-120 Selenium 99.0 2.0 100 99 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 LO 100 102 80-120 Vanadium 97.6 2.0 100 98 80-120 Zinc 100 2.0 100 100 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD �Wes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 - . LCS Dup (BlE0693-BSDI) Analyzed: 05/25/21 14:47 Antimony 100 2.5 mg/kg 100 100 80-120 0.5 20 Arsenic 99.7 2.0 100 100 80-120 0.1 20 Barium 101 1.0 100 101 80-120 0.05 20 Beryllium 98.5 0.50 100 98 80-120 0.3 20 Cadmium 100 0.25 100 100 80-120 0.2 20 Chromium 99.4 0.50 100 99 80-120 0.2 20 Cobalt 101 0.50 100 101 80-120 0.05 20 Copper 100 1.0 100 100 80-120 0.2 20 Lead 102 0.50 100 102 80-120 0.1 20 Molybdenum 98.4 0.50 100 98 80-120 0.6 20 Nickel 102 0.50 100 102 80-120 0.1 20 Selenium 100 2.0 100 100 80-120 1 20 Silver 4.96 0.50 5.00 99 80-120 0 20 Thallium 102 1.0 100 102 80-120 0.4 20 Vanadium 97.0 2.0 100 97 80-120 0.7 20 Zinc 100 2.0 100 100 80-120 0.2 20 Duplicate (BlE0693-DUPl) Source: 2103212-05 Analyzed: 05/25/21 14:15 Antimony ND 2.4 tng/kg ND 20 Arsenic 5.18 1.9 6.10 16 20 Barium 205 0.97 218 6 20 Beryllium 0.408 0.49 0.435 6 20 Cadmium ND 0.24 ND 20 Chromium 154 0.49 144 7 20 Cobalt 22.3 0.49 20.9 6 20 - Copper 48.8 0.97 46.3 5 20 Lead 17.9 0.49 19.3 8 20 Molybdenum 0.510 0.49 0.574 12 20 Nickel 196 0.49 179 9 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 _ Vanadium 52.3 1.9 54.0 3 20 Zinc 69.6 1.9 87.4 23 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Matrix Spike (B1E0693-MSI) Source: 2103212-05 Analyzed: 05/25/21 13:50 Antimony 13.1 2.4 mg/kg 97.9 ND 13 10-116 Arsenic 101 2.0 97.9 6.10 96 77-121 Barium 226 0.98 97.9 218 8 30-169 QNI-07 Beryllium 95.2 0.49 97.9 0.435 97 86-111 Cadmium 90.0 0.24 97.9 ND 92 81-112 Chromium 218 0.49 97.9 144 76 75-129 Cobalt 109 0.49 97.9 20.9 90 71-121 Copper 146 0.98 97.9 46.3 102 68-135 Lead 107 0.49 97.9 19.3 90 72-121 Molybdenum 35.0 0.49 97.9 0.574 35 70-112 QA9-07 Nickel 230 0.49 97.9 179 52 73-121 QDI-07 Selenium 85.9 2.0 97.9 ND 88 76-116 Silver 4.79 0.49 4.90 ND 98 54-132 Thallium 85.9 0.98 97.9 ND 88 64-120 Vanadium 138 2.0 97.9 54.0 86 78-124 Zinc 162 2.0 97.9 87.4 77 50-143 Matrix Spike Dup (BlE0693-MSD1) Source: 2103212-05 Analyzed: 05/25/21 13:52 Antimony 9.34 2.4 mglkg 95.8 ND 10 10-116 33 20 QR-02 Arsenic 96.6 1.9 95.8 6.10 95 77-121 4 20 Barium 295 0.96 95.8 218 80 30-169 26 20 QR-02 Beryllium 91.2 0.48 95.8 0.435 95 86-I11 4 20 Cadmium 85.1 0.24 95.8 ND 89 81-112 6 20 Chromium 271 0.48 95.8 144 133 75-129 22 20 QD1-07, QR-04 Cobalt 113 0.48 95.8 20.9 96 71-121 3 20 Copper 140 0.96 95.8 46.3 97 68-135 4 20 Lcad 104 0.48 95.8 19.3 88 72-121 3 20 Molybdenum 32.4 0.48 95.8 0.574 33 70-112 8 20 QNI-07 Nickel 319 0.48 95.8 179 146 73-121 32 20 Q11-07, QR-04 Selenium 79.5 1.9 95.8 ND 83 76-116 8 20 Silver 4.59 0.48 4.79 ND 96 54-132 4 20 Thallium 79.5 0.96 95.9 ND 83 64-120 8 20 Vanadium 147 1.9 95.8 54.0 97 78-124 6 20 Zinc 158 1.9 95.8 97.4 74 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 38 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Post Spike (BlE0693-PS1) Source: 2103212-05 Analyzed: 05/25/21 14:08 Antimony 1.99 me/l. 2.00 0.00347 99 75-125 Arsenic 2.07 2.00 0121 98 75-125 Barium 6.39 2.00 4.34 103 75-125 Beryllium 1.96 2.00 0.00863 98 75-125 Cadmium 1.83 2.00 -0.0417 91 75-125 Chromium 4.75 2.00 2.85 95 75-125 Cobalt 2.27 2.00 0.414 93 75-125 Copper 2.88 2.00 0.919 98 75-125 Lead 2.24 2.00 0.384 93 75-125 Molybdenum 1.97 2.00 0.0114 98 75-125 - Nickel 5.42 2.00 3.56 93 75-125 Selenium 1.80 2.00 -0.t20 90 75-125 Silver 0.0954 0.100 -0.00119 95 75-125 Thallium 1.78 2.00 -0.0164 89 75-125 Vanadium 3.01 2.00 1.07 97 75-125 Zinc 3.61 2.00 1.74 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 57 C A W&M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0794 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 05/27/21 10:55 Blank (BlE0794-BLK1) Analyzed: 05/27/21 18:35 Chromium ND 0.050 mg/L. LCS (BlE0794-BS1) Analyzed: 05/27/21 18:20 Chromium 10.0 0.050 mg/1. 10.0 LCS Dup (BlE0794-BSD1) Analyzed: 05/27/21 18:22 Chromium 9.84 0.050 mg/l, 10.0 Duplicate (BlE0794-DUPI) Source: 2102854-01 Analyzed: 05/27/21 18:52 Chromium ND 0.050 mg/l. ND Leach Fluid Blank (B1E0794-LBKI) Analyzed: 05/27/21 18:37 Chromium ND 0.050 mg/L Leach Fluid Blank (BlE0794-LBK2) Analyzed: 05/27/21 18:40 Chromium ND 0.050 mg/L Leach Fluid Blank (BlE0794-LBK3) Analyzed: 05/27/21 18:42 Chromium ND 0.050 mg/L Matrix Spike (BlE0794-MS1) Source: 2102854-01 Analyzed: 05/27/21 18:25 Chromium 10.2 0.050 mg/1. 10.0 ND Matrix Spike Dup (B1E0794-MSDI) Source: 2102854-01 Analyzed: 05/27/21 18:45 Chromium 10.2 0.050 mg/L. 10.0 ND 100 80-120 98 80-120 2 20 20 102 82-119 102 82-119 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8051925-3376 Page 40 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 N/olatile Organic TPH by 1 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0737 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/26/21 06:59 — - Blank (B1E0737-BLKl) Analyzed: 05/26/21 10:49 TPH Gasoline (C5-('l2) ND 0.50 mg/kg Surrogute: 4-Bromq luorohencene 0.12E " OJ25 102 39-157 -- LCS (BlE0737-BS1) Analyzed: 05/26/21 09:57 TPH Gasoline (C5-C12) 1.08 0.50 mg/kg 0.994 108 68-139 Surrogate. 4-Bromo/luoroheu_ene 0.146 " 0.124 117 39-157 LCS Dup (B1E0737-BSDl) Analyzed: 05/26/21 10:23 TPH Gasoline (C5-C12) 1.20 0.50 mg/kg 0.998 120 68-139 11 20 Surrogate• 4-Br•ornnfluorohenzene 0.154 110.125 123 39-157 Duplicate (BlE0737-DUPl) Source: 2103210-OIRE1 Analyzed: 05/26/21 13:04 TPH Gasoline (C5-('12) ND 0.49 mg/kg ND 20 Surrogate:4-Bromofluorobenzene 0.120 " 0.122 99 39-157 Matrix Spike (BlE0737-MS1) Source: 2103210-01RE1 Analyzed: 05/26/21 23:45 TPH Gasoline (('5-('12) 0.868 0.48 mg/kg 0.967 ND 90 10-171 Surrogate. 4-Bromnfluoroben_ene 0.142 " 0.121 117 39-157 Matrix Spike Dup (B1E0737-MSD1) Source: 2103210-01RE1 Analyzed: 05/27/21 00:11 TPH Gasoline (C'5-C12) 0.911 0.50 mg/kg 0.998 ND 91 10-171 5 20 Surrogate:4-Bromolluorohenrene 0.149 0.125 119 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 41 of 57 .(. �i W�� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Semi-Volatileby 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0696 - EPA 8015M Preparation: EPA 3550C 05/25/21 08:55 Blank (B1E0696-BLKI) Analyzed: 05/25/21 13:41 TPH Diesel (('13-C22) ND 10 mg/kg Till Motor Oil (C23-C40) ND 50 " Surrogate: o-Teuphenyl 43.3 50.0 87 65-136 LCS (B1E0696-BSl) Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22) 512 10 mg/kg 499 103 72-115 TPH Motor Oil (C23-('40) 473 50 499 95 74-126 Surrogate: o-Teuphe» yl 49.9 49.9 100 65-136 LCS Dup (BlE0696-BSD1) Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22) 487 Ill mg/kg 500 97 72-115 5 20 - TPH Motor Oil (C23-C40) 459 50 500 92 74-126 3 20 Surrogate: o-Tcuphenyl 48.7 " 50.0 97 65-136 Duplicate (BlE0696-DUPl) Source: 2103212-01 Analyzed: 05/25/21 14:03 TPII Diesel WI 3-('22) 35.5 9.9 mg/kg 50.9 36 20 QR-06 I PH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Tcipheurl 42.6 49.7 86 65-136 Matrix Spike (BIE0696-MSI) Source: 2103212-01 Analyzed: 05/25/21 12:55 TPH Diesel (C13-('22) 500 10 mg/kg 498 50.9 90 46-147 TPH Motor Oil (('23-C40) 432 50 498 ND 87 35-171 _ Surrogate: o-Teupheun•1 44.5 49.8 89 65-136 Matrix Spike Dup (B1E0696-MSDl) Source: 2103212-01 Analyzed: 05/25/21 13:18 TPH Diesel (C'13-('22) 497 9.9 mg/kg 497 50.9 90 46-147 0.6 20 _ TPH Motor Oil (C23-('40) 432 50 497 ND 87 35-171 0.2 20 Surrogate: o4ieiphruryl 44.3 49.7 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805' 925-3376 Page 42 of 57 161CUN Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (BlE0697-BLK1) Analyzed: 05/25/21 13:26 Benzene ND 0,25 mg/kg Bromobenzene NJ) 0.25 Bromochloromcthane ND 0.25 Bromodichloromethane ND 0.25 " Bromoform ND 0.25 " Bromomethane NI) 0.25 " n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 tert-Butyl benzene ND 0.25 Carbon tetrachloride ND 0.25 Chlorobenzene NI) 0.25 Chloroethane ND 0.25 Chloroform ND 0.25 Chloromethane NJ) 0.25 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene ND 0.25 Dibromoehloromethane ND 0.25 1,2-1.)ibromo-3-chloropropane ND 0.25 1,2-Dibromoethane (EDB) ND 0.25 Dibronxnnethanc ND 0.25 " 1,2-Dichlorobenzene ND 0.25 " 1,3-Dichloroben7ene ND 0.25 1,4-Dichlorobenzene ND 0.25 " Dichlorodilluoromethane ND 0.25 " 1, 1 -Dichloroethane NI) 0.25 1,2-Dichloroethane ND 0.25 LI-Dichloroethene ND 0.25 cis-1,2-Dichloroethene ND 025 trans-1,2-Dichloroethene NI) 0.25 1,2-Dichloropropane ND 025 1,3-Dichloropropane ND 0.25 2,2-Dichloropropane ND 0.25 I,l-Dichloropropene ND 0.25 cis-1.3-Dichloropropene ND 0.25 trans-1,3-Dichloropropene ND 0.25 " Ethvlbenzene ND 0.25 " Ilexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 " isopropylbenzene ND 0.25 " Methylene chloride ND 0.25 " Naphthalene ND 025 n-Propylbenzene NI) 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805; 925-3376 Page 43 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (BlE0697-BLK1) Analyzed: 05/25/21 13:26 Styrene ND 0.25 mg/kg 1,1,1,2-Tetrachlorocthane ND 0.25 " 1.1,2.2-Tetrachlorocthanc ND 0.25 Tetrachloroethene (PCE) ND 0.25 Toluene ND 0.25 " L23-Trichlorobenzene ND 0.25 " 1,2,4-Trichlorobenzene ND 0.25 1, 1, 1 -Trichloroethane ND 0.25 I,1.2-Trichloroethane ND 0.25 " Trichloroethene (TCE) ND 0.25 Trichlorofluoromethane ND 0.25 1,2,3-Trichloropropane ND 0.25 " 1,2.4-Trimethylbenzene ND 0.25 1,3,5-Trimethylbenzene ND 0.25 Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 Surrogate: Dibrumu/luoronrethunc 0.0496 0.0500 99 74-122 Surrogate Toluene-dS 0.0507 0.0500 101 65-128 Srn•ro,ate: 4-Bronmjluoraben:ene 0.0482 0.0500 96 75-121 LCS (BlE0697-BSI) Analyzed: 05/25/21 11:37 Benzene 1.80 0.25 mg/kg 1.98 91 70-131 Bromobenzene 2.09 0.25 1.98 105 74-130 Bromochloromethanc 1.77 0.25 1.98 89 64-133 Bromodichloromethane 2.12 0.25 1.99 107 69-137 Bromoforin 2.09 0.25 1.98 105 55-132 Bronwnrethane 1.51 0.25 1.98 76 10-142 n-Butylbenzene 2.47 0.25 " 1.98 125 64-156 sec-Butylbenzene 2.46 0.25 1.98 124 75-155 tert-Butylbenzene 2.34 0.25 1.98 118 74-144 Carbon tetrachloride 1.70 0.25 1.99 86 67-135 Chlorobenzene 2.08 0.25 1.98 105 73-134 Chloroethane 1.65 0.25 1.98 83 10-167 Chloroform 2.01 0.25 1.98 WI 69-124 Chloromethane 2.46 0.25 1.98 124 34-130 2-Chlorotoluene 2.16 0.25 1.98 109 75-135 4-Chlorotoluene 2.30 0.25 1.98 116 70-138 Dibrornochloromethane 2.01 0.25 1.98 102 (,7-135 1.2-I)ibromo-3-chloropropane 2.45 0.25 1.98 124 41-149 12-Dibromoethane (ED13) 1.98 0.25 1.98 100 08-131 Dibromomethane 1.92 0.25 1.98 97 61-140 1,2-Dichlorobenzene 2.20 0.25 1.98 111 76-t36 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS (BlE0697-BS1) Analyzed: 05/25/21 11:37 1,3-Dichlorobenzenc 2.30 0.25 mg/kg 1.98 116 76-138 IA-Dichlorobenzene 2.23 0.25 1.98 112 72-132 Dichlorodifluoromethane 1.51 0.25 1.98 76 10-155 1, 1 -Dichloroethane 1.90 0.25 1.99 96 63-139 1,2-Dichloroethane 2.04 0.25 1.98 103 64-126 1,1-Dichloroethene 1.79 0.25 1.98 90 52-167 cis-1,2-Dichloroethene 1.84 0.25 1.98 93 70-135 trans-1,2-Dichloroethene 1.69 0.25 1.98 85 67-147 1,2-Dichloropropane 3.19 0.25 1.98 161 68-131 1,3-Dichloropropane 1.91 0.25 1.98 96 64-128 2,2-Dichloropropane 2.11 0.25 1.98 107 63-154 1,1-Dichloropropene 1.82 0.25 1.98 92 68-138 cis-1,3-Dichloropropene 2.09 0.25 1.98 105 72-134 trans- l,3-Di chloropropene 2.16 0.25 1.98 109 69-132 Ethvlbenzene 1.92 0.25 1.98 97 68-136 1 lexa chlorobutadiene 2.24 0.25 1.98 113 72-198 4-Isopropyl Toluene 2.40 0.25 1.98 121 74-150 Isopropylbenzene 2.21 0.25 1.98 112 71-149 Methylene chloride 1,81 0.25 1.98 91 51-127 Naphthalene 2.29 0.25 1.98 116 57-158 n-Propylbenzene 2.29 0.25 1.98 116 70-143 Styrene 2.47 0.25 1.98 124 68-138 1, 1, 1,2-Tetrachloroethane 2.10 0.25 1.98 106 76-130 1,1,2,2-Tetrachlorocthanc 2.18 0.25 1.98 110 60-136 Tetrachloroethene WCE) 1.79 0.25 1.98 91 73-139 Toluene 1.99 0.25 1.98 101 72-128 1,2,3-Trichlorobenzene 2.47 0.25 1.98 125 61-166 1,2,4-Trichlorobenzene 2.43 0.25 1.98 123 71-158 1,1,1-Trichloroethane 1.92 0.25 1.98 97 71-135 1,12-Trichloroethane 2.23 0.25 1.98 113 64-132 Trichloroethane (TCE) 1.87 0.25 1.98 94 74-139 Trichlorotluoromethane 2.69 0.25 1.98 136 30-156 1,2,3-Triehloropropane 2.05 0.25 1.98 104 67-123 1,2,4-Trimethylbenzene 2.31 0.25 1.98 117 68-134 1,3,5-Trimethylbenzene 2.27 0.25 1.98 114 71-140 Vinyl chloride 2.14 0.25 1.98 108 43-144 Xylenes (totah 6.81 0.25 5.94 115 69-138 Surrogate: UihromolLror„methcrnc 0.0512 0.0495 103 74-122 Surrogate: "l7,laene-dg 0.0516 0.0495 104 65-128 Stnrogate:4-Bronco/luorohen_ene 0.0467 0.0495 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. QNI-08 California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 45 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet tt t by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (BlE0697-BSD1) Analyzed: 05/25/21 12:04 Benzene 1.74 0.25 mg/kg 1.99 87 70-131 3 20 Bromobenzene 2.08 0.25 1.99 104 74-130 0.4 20 Bromochloronicthane 1.69 0.25 1.99 85 64-133 5 20 Bromodichloromethane 2.14 0.25 1.99 107 69-137 0.8 20 Bromoform 2.06 0.25 1.99 103 55-132 1 20 Bromomethane 1.50 0.25 1.99 75 10-142 1 20 n-Butylbenzene 2.33 0.25 1.99 117 64-156 6 20 -� sec-Butylbenzene 2.25 0.25 1.99 113 75-155 9 20 tert-Butylbenzene 2.17 0.25 1.99 109 74-144 8 20 Carbon tetrachloride 1.60 0.25 1.99 80 67-135 6 20 .-, Chlorobenzene 2.07 0.25 1.99 104 73-134 0.3 20 Chloroethane 1.70 0.25 1.99 85 10-167 3 ' 20 Chloroform 1.93 0.25 1.99 97 69-124 4 20 Chlommethane 2.10 0.25 1.99 108 34-136 13 20 2-Chlorotoluene 2.05 0.25 1.99 103 75-135 5 20 4-Chlorotoluene 2.15 0.25 1.99 108 70-138 7 20 Dibromochloromethane 2.11 0.25 1.99 106 67-135 5 20 . 1,2-Dibromo-3-chloropropane 2.68 0.25 1.99 135 41-149 9 20 1,2-Dibronloethane(ED13) 2.01 0.25 1.99 101 68-131 t 20 Dibromomcthane 1.92 0.25 1.99 96 61-140 0.08 20 1,2-Dichlorobenzene 2.20 0.25 1.99 110 76-136 0.4 20 1,3-Dichlorobenzene 2.15 0.25 1.99 108 76-138 7 20 1,4-Dichlorobenzene 2.13 0.25 1.99 107 72-132 5 20 Dichlorodifluoromcthane 1.50 0.25 1.99 75 10-155 0.5 20 1,1-Dichloroethane 1.83 0.25 1.99 92 63-139 4 20 1,2-Dichlorocthane 2.01 0.25 1.99 101 64-126 2 20 LI-Dichloroethene 1.73 0.25 1.99 87 52-167 4 20 cis-L2-Dichloroethene 1.71 0.25 1.99 86 70-135 8 20 • _ trams-1,2-Dichloroethene 1.64 0.25 1.99 82 67-147 3 20 1,2-Dichloropropane 1.94 0.25 1.99 97 68-131 49 20 QR-04 13-Dichloropropane 2.05 0.25 1.99 103 64-128 7 20 2,2-Dichloropropane 2.00 0.25 1.99 100 63-154 5 20 1,1-Dichloropropene 1.75 0.25 1.99 88 68-138 4 20 cis-1.3-Dichloropropene 1.98 0.25 1.99 100 72-134 5 20 trans-1,3-Dichloropropene 2.25 0.25 1.99 113 69-132 4 20 Ethylbenzene 2.05 0.25 1.99 103 68-136 7 20 Hexachlorobutadiene 2.12 0.25 1.99 107 72-198 5 20 4-Isopropyl Toluene 2.23 0.25 1.99 112 74-150 7 20 Isopropylbenzene 2.24 0.25 1.99 112 71-149 1 20 Methylene chloride 1.79 0.25 1.99 90 51-127 1 20 Naphthalene 2.10 0.25 1.99 106 57-158 8 20 n-Propylbenzene 2.12 0.25 1.99 106 70-143 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 46 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSD1) Analyzed: 05/25/21 12:04 Styrcne 2.23 0.25 mg/kg 1.99 112 68-138 10 20 1, 1, 1,2-Tetrachloroethane 2.18 0.25 1.99 109 76-130 3 20 1,1,2,2-Tctrachlorocthanc 2.11 0.25 1.99 106 60-136 3 20 ^ Tetrachloroethene WCE) 1.81 0.25 1.99 91 73-139 0.8 20 Tolucnc 1.83 0.25 1.99 92 72-128 9 20 1,2,3-Trichlorobenzene 2.32 0.25 1.99 116 61-166 6 20 1,2,4-1'richlorobenzene 2.35 0.25 1.99 its 71-158 3 20 r 1, 1, 1 -Trichloroethane 1.86 0.25 1.99 93 71-135 3 20 1,1,2-Trichloroethane 2.18 0.25 1.99 109 64-132 2 20 Trichloroethene(TCE) 1.82 0.25 1.99 91 74-139 3 20 Trichlorofluoromethane 2.59 0.25 199 130 30-156 4 20 1,2,3-Trichloropropane 1.96 0.25 1.99 98 67-123 5 20 1.2.4-Trimethylbenzene 2.16 0.25 1.99 IN 68-134 7 20 1,3,5-Trimethylbenzene 2.13 0.25 1.99 107 71-140 6 20 '- Vinyl chloride 2.12 0.25 1.99 107 43-144 0.6 20 Xylenes (total) 6.17 0.25 5.98 103 69-139 10 20 Surrogate: Uihromglhmromethane� 0.0512 0.0498 103 74-122 T Surrogate: Toluene-d8 0.0510 0.0498 102 65-128 Surrogate: 4-Bromo luorohenrene 0.0499 0.0498 100 75-121 Duplicate (B1E0697-DUPl) Source: 210321041 Analyzed: 05/25/21 14:48 Benzcne ND 1.2 mg/kg ND 20 Bromobenzene ND 1.2 ND 20 Bromochloromethanc ND 1.2 " ND 20 Broniodichloromethane ND 1.2 ND 20 Bromoform ND 1.2 ND 20 Bromomethane ND 1.2 ND 20 n-Butylbenzene ND 1.2 ND 20 sec-Butylbenzene ND 1.2 ND 20 - tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzene ND 1.2 ND 20 Chloroethane ND 1.2 ND 20 Chloroform ND 1.2 ND 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 �• 4-Chlorotoluene ND 1.2 ND 20 Dibromochloromethane ND 1.2 ND 20 1,2-Dibromo-3-chloropropatic ND 1.2 ND 20 1,2-Dibromocthane (ED13) ND 1.2 ND 20 Dibromomethanc ND 1.2 ND 20 1.2-Dichlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by GUMS - Quality Control ,nalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Duplicate (BlE0697-DUPl) Source: 2103210-01 Analyzed: 05/25/21 14:48 1,3-Dichlorobenzenc ND 1.2 mgikg ND 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichloroditluoromethane ND 1.2 ND 20 El-Dichloroethene ND 1.2 ND 20 1,2-Dichloroethenc ND 1.2 ND 20 1,1-Dichloroethene ND 1.2 ND 20 cis-1,2-Dichloroethene ND 1.2 " ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropane ND 1.2 ND 20 1,3-Dichloropropaue ND 1.2 ND 20 2,2-Dichloropropane ND 1.2 ND 20 1, 1 -Dichloropropene ND 1.2 ND 20 cis-1,3-Dichloropropene ND 1.2 ND 20 trans-1,3-Dichloropropene ND 1.2 ND 20 Ethylbenzene ND 1.2 ND 20 Hexachlorobutadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 Isopropylbenzene ND 1.2 ND 20 methylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 ND 20 n-Propylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1,1,1.2-Tetrachloroethane ND 1.2 ND 20 1,1,2,2-Tetrachloroethanc ND 1.2 " ND 20 Tetrachloroethene ('PCE) ND 1.2 ND 20 Toluene ND 1.2 ND 20 1,2.3-Trichlorobenzene ND 1.2 ND 20 1,2,4-Trichlorobenzene ND 1.2 " ND 20 1, 1, 1 -Trichloroethane ND 1.2 ND 20 1,1,2-TrichloroethLine ND 1.2 ND 20 Trichloroethene (TCE) ND 1.2 ND 20 Trichlorofluoromethane ND 1.2 ND 20 1,2,3-Trichloropropane ND 1.2 ND 20 1,2,4-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 ND 20 Vinyl chloride NI.) 1.2 ND 20 Xylenes (total) ND 1.2 ND 20 Surrogate: Dibromolluoromethane 0.0503 0.0494 102 74-122 Surrogate: Toluene-dN 0.0514 0.0494 104 65-128 Surrogate:4-Bromo/luorohenzene 0.0478 0.0494 97 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 48 of 57 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Coinpounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes -- Level Result Limits Limit Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (BlE0697-MS1) Source: 2103212-01 Analyzed: 05/25/21 19:22 Benzene 9.97 1.2 mg!kg 9.94 ND 90 37-145 Bromobenzene 11.0 1.2 9.94 ND 111 29-147 Bromochloromcthanc 9.22 1.2 9.94 ND 93 40-145 Bromodichloromethane 10.9 1.2 9.94 ND 110 39-153 Bromotorm 10.7 1.2 9.94 ND 108 32-143 Bromomethane 10.3 1.2 9.94 ND 104 10-141 u-Butylbenzene 11.6 1.2 9.94 ND 117 10-162 sec-Butylbenzene 12.2 1.2 9.94 ND 123 14-168 tert-Butylbenzene 11.8 1.2 9.94 ND 119 21-159 Carbon tetrachloride 8.48 1.2 9.94 ND 85 28-148 Chlorobenzene 10.9 1.2 9.94 ND 110 32-148 Chloroethane 12.6 1.2 9.94 ND 127 11-166 Chloroform 9.94 1.2 9.94 ND 100 40-139 Chloromethane 10.4 1.2 9.94 ND 105 18-135 2-Chlorotoluene 10.8 1.2 9.94 ND 108 25-151 4-Chlorotoluene 11.3 1.2 9.94 ND 114 22-150 Dibromochloromethane 10.2 1.2 9.94 ND 103 40-147 1,2-Dibromo-3-chloropropane 12.4 1.2 9.94 ND 125 25-158 1,2-Dibromoethane (EDB) 10.1 1.2 9.94 ND 102 38-147 Dibromomcthanc 9.74 1.2 9.94 ND 98 39-150 1,2-Dichlorobenzene 11.4 1.2 9.94 ND 115 24-154 1,3-Dichlorobenzene 11.3 1.2 9.94 ND 114 21-153 1,4-Dichlorobenzene 10.9 1.2 9.94 ND 110 21-146 Dichloroditluoromcthanc 6.32 1.2 9.94 ND 64 10-149 1,1-Dichloroethene 9.32 1.2 9.94 ND 94 34-151 1,2-Dichlorocthanc 9.93 1.2 994 ND 100 40-137 LI-Dichloroethene 7.41 1.2 9.94 ND 74 21-172 cis-1,2-Dichloroethene 8.87 1.2 9.94 ND 89 38-147 trans-1,2-Dichloroethene 8.06 1.2 9.94 ND 81 30-160 12-Dichloropropane 10.0 1.2 9.94 ND 101 39-146 1,3-Dichloropropane 9.84 1.2 9.94 ND 99 39-141 2,2-Dichloropropanc 9.05 1.2 9.94 ND 91 26-149 -� ],I-Dichloropropene 9.03 1.2 9.94 ND 91 28-150 cis- 1.3 -Dichloropropene 9.92 1.2 9.94 ND 100 34-149 trans- l,3-Dichloropropene I H) 1.2 9.94 ND HI 36-143 F.thylbenzene 10.8 1.2 9.94 ND 109 23-150 Hexachlorobutadiene 11.4 1.2 9.94 ND 115 10-192 4-Isopropyl Toluene 11.9 1.2 9.94 ND 120 I1-165 Isopropylbenzene 11.7 1.2 9.94 ND 118 17-166 Methylene chloride 8.61 1.2 9.94 ND 87 28-135 Naphthalene 12.4 1.2 9.94 ND 124 10-174 n-Propylbenzene 11.3 1.2 9.94 ND 114 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilept Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MSI) Source: 2103212-01 Analyzed: 05/25/21 19:22 Styrene 11.5 1.2 mg/kg 9.94 ND 116 24-154 1,1,1,2-Tetrachloroethane 11.1 1.2 9.94 ND 111 38-149 1,1,2,2-Tetrachloroethane 10.7 1.2 9.94 ND 107 22-164 Tetrachloroethenel_PCE) 9.37 1.2 9.94 ND 94 25-153 Toluene 10.4 1.2 9.94 ND 105 26-149 1,23-Trichlorobenzene 12.7 1.2 9.94 ND 128 10-163 1,2.4-1'richloroben7ene 12.4 1.2 9.94 ND 124 10-162 1,1,1-Trichloroethane 9.87 1.2 9.94 ND 99 34-149 1,12-Trichloroethane 11.3 1.2 9.94 ND 113 25-175 Trichloroethene (WE) 9.24 1.2 9.94 ND 93 25-170 - Trichlorofluoromethane 12.0 1.2 9.94 ND 121 19-155 1,2,3-Trichloropropane 9,81 1.2 9.94 ND 99 32-165 1,2,4-Trimethylbenzene 11.7 1.2 9.94 ND 118 15-150 1.3,5-Trimethylbenzene 11.4 1.2 9.94 ND 114 10-158 Vinyl chloride 11.2 L2 9.94 ND 112 22-148 Xylenes (total) 32.3 1.2 29.8 ND IN 22-153 Surrogate: Dihrunu,/lunram<tl7une 0.0501t 0.0497 102 74-122 Surrogate: Tbluene-dR 0.0509 0.0497 102 65-128 Surrogate:4-BromnJluorobenzen" 0.0499 0.0497 100 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 50 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Method Summary lnalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 9015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 6010B TCLP Chromium EPA 1311 /EPA 601 OB Water OEC, CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-E.LAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471A Solid OEC, CA-ELAP Total Metals by ICP 6010E Total Antimony EPA 601013 Solid OF,C, CA-ELAP 6010E Total Arsenic EPA 6010E Solid OEC, CA-ELAP 6010B Total Barium EPA 601013 Solid OEC, CA-ELAP 601013 Total Beryllium EPA 601013 Solid OEC, CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010B Total Chromium EPA 601013 Solid OEC, CA-ELAP 601013 Total Cobalt EPA 6010E Solid OEC, CA-ELAP 601013Total Copper EPA 6010E Solid OEC, CA-ELAP 6010B Total Lead EPA 601013 Solid OEC. CA-ELAP 6010B Total Molvbdenum EPA 601OB Solid OEC. CA-ELAP 6010E Total Nickel EPA 6010B Solid OEC, CA-ELAP 6010E Total Selenium EPA 601013 Solid OEC, CA -FLAP 601013 Total Silver EPA 601013 Solid OEC, CA-ELAP 6010E Total Thallium EPA 6010E Solid OEC. CA-ELAP 601013 Total Vanadium EPA 601013 Solid OEC, CA-ELAP 6010B Total Zinc EPA 601013 Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 MethodSample Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA -FLAP -� Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPI1-6asoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC_ Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC. CA-ELAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC. Internal EPA 8015M Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 52 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 DefinitionsNotes and Qualifier Definition MDL Method Detection Limit RL Reporting Limit (QuantitationLimit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery andlor RPD values. QM -OR The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; how ever. both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. QR-06 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to non -homogenous sample matrix. QC batch accepted based on LCS and/or LCSD recovery and'or RPD values. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out -Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 53 of 57 U r-I O x w Ei 0 4 » C U N M IS Lf) F: N •ri W U) 0 Pra t~ / 04 N � � Ln N N •• ko In N O o W N 1-I cU N r Q O O N I / N �L H E1 i N r� SUM 12) C7 0 / Ln C--)o U N N f l M .. .. .. .. .. .. .. N S4 (a 0 SQ 0� z4-4 l) i4 (0•H �4H N S4 +-) S? U I � N b to co U •� -ri [i0aCHtn U Q LL_ N Cl) LO N W 0 O CO rG O In W o N+ 0 y d C0 a) n C. + N n 0 + N V h o + G1 Cl) n O + N N n 0 + N n 0 + N o O O O 0OOOO 0 0) 0 o O O OD 0 0 O O n 0 0 O O co 0 0 O O Lr) 0 0 O O O It 0 00 O O O M 0 0 0 O o O O O O N File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2612.D Operator RR Acquired 26 May 2021 1:56 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-01RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 12 Response_ 85000 80000 I 75000 70000 a 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOME2612.DT1D1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 0 x a H O N rn � N U �n U (V O / U) W �5 i N M Q0 Ln O m N •• � L N O O [x] / r-I rl (� N r 'v >i N N / N H r0 -I N aC U Cl) f� a C7o / Ln -1 U N (N r N .. .. .. .. .. .. .. a) Sa +-) a) a m O s4 a) z w °-) S 4 � H a) +z id -H t-4 r-i a) S-I 71 -P ¢i U O O O O O O O O O O 0) O O O O O O _ O O O O N _ Co U I m N o O LL O O N W i; in o 0 m L6 j 0 LO ri —_ M 1 N i O O fV d O O O O O O F h I-- r- n n n r O O O O O O O O 0 � in o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 c+ + + + + + + o 0 0 0 0 0 0 0 0 c N N N N d N N O CD O CD O 0 O O d co CO r In r V r Cl) r N r r r O WcoO O O O coN O O O MNN O O r V File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2614.D Operator RR Acquired 26 May 2021 3:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-02RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 14 Response_ 110000 I 105000 100000 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 GOME2614.D\FID1A 35000 30000 25000 20000 I 15000 l 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 x U O x a E� O L M Z3 Ln U N41 FG � >s o PQ / rn U � W 04 � N N kv to r Ol N � M O o W r-1 W N r (E) N M Q O O � N I / N E1 ro rl N < £UM Ll a C7 O / Ln —c--)M •• CJ N N rI M .. .. .. .. .. .. .. N Sa ra O Q u N z w 4 (1) H z ro -H i-I ri N }-I �l +-) Q U rl ,--1 N b" O E m N -H sz U C M -li -H GaOF. i-A(!)X 2 U m N LL to Cl) Lo N W 2 O m f6 rT N 0 Ln 0 0 0 0 0 0 0 „r O O of O 00 0 0 06 0 t r; 0 _o 0 _ rn QD - O _p f0 O ui O O LO 0 v _ � M r 7 o -- Cl) o N O O N O O O r` r- r- h r` O O O O O O O O O 0 C. 0 0 0 0 0 p o 0 0 0 0 0 + + + + + o C. o O o 0 o O O a) 0 a> a) D O O O O O O Cl O O ��-,' Ci N O O O O O O O O O W 00 h (O to M N >C U O x a r� O Ca � r � N b" LO U N O � PQ U R to N r lfl (N l0 u') r-i O O [r] N -A (J N a O O � N I / N C) a U O /XLn :vLn U N (N r N .. .. .. .. .. .. .. -I-I a) I~ (0 O Q u-0 a)zw F= JU-I iU-I � N H z M _H S4 rl a) S4 ;� 4-) ¢Q U r-I �-i (1) b" U U) (d •.-I Q U Cd -ri •rl Gu0FCHM� yr- o I- 0 r- 0 I-- 0 r 0 I. 0 r- 0 (I-o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 c+ + + + + + + + 0 0 0 0 0 0 0 0 0 0 0 0 0 0 C' Cu d m d d m d o 0 0 0 0 0 0 0 0 a n Co LO v r> Cy o O o 0 O o 0 0 0 .- c- m OOD r- COO � CD ItM N 0 0 0 0 0 0 0 0 m 0 0 of 0 00 0 0 00 0 0 0 r-- 0 co O O LO O V5 O .O to 0 _ In It File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2618.D Operator RR Acquired 26 May 2021 5:18 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-04RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 18 Response_ 85000 80000 750001 70000 65000 60000 550001 50000 45000; 400001 35000 30000 25000 20000 15000 i GOME2618.D\FID1A 10000 i 5000 s h� Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 0 U� 0 0 0 0 0 0 O 0 Un 00 0 0 00 0 0 0 0 to 2 U In 0 N O CO LL M M O UC L N LO W O m O O f0 LO rn U U 0 o x v a H O � L] 1-I - LO u) U Cl) O O (� •r-I M _ U � - W P U CV N Ol l0 u) cl' rs N l0 0 0 N O N o W / c-I N rl FJ O N U-) U? Q O O r N / N L1 -i O H (a r-I N q FC X U N Gl a C7 0 / Ln -IC--) UN N1-1Ch I.J. .. .. .. .. .. O o I~ r0 O Q r u4 (1)z4-4 E J O N }� i-I N I- O O � O - n O I,- � o O 0 0 0 0 0 o CD + + + + O O + + O O O O O O CD O O CD O O O O O O ,i }4 Qa U rl O N LO d V N Cl) Na) N N O r O CD O O O O O O Cl O O O O O O 0 O r-I N �' fn ul(a Q. N nO�aMQ -rl •r-I -H N 00 CO N E Gu 0 FC H cn X > w 1- File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2624.D Operator RR Acquired 26 May 2021 7:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-05RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 24 Response_ GOME2624.D\FID1A 85000I 80000 75000 70000 65000 60000+ I 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 0 0 0 0 0 0 of 0 0 of 0 OD 0 0 Co 0 U� r; 0 0 0 2 co U Q O o -o LL (fl Lo t� W Lr, 0 O •=3 - O 5-. c In rn U � H O O U� x •F v a . +-) � o U� Ca _ ri F�4 c M Ln N ��. (D / Qa U1 N N Ol l0 LO G 0) O N to O U-) N O N O W 0 }i N l0 Q' O O � N I / N Fl� ?fir E+ (6 rl N fa a U o Ln H UN Nr co O .. .. .. .. .. .. 0 m O �Z4-1 a O N E~ C7� 1 r- n- ti n n n n O o 0 0 0 0 0 0 0 iJ i4 �5 N H '�-, N O O O O O O O O O C. O C. O 0 O 0 O 0 O 0 O 0 0 0 b-H �� + + m + m + d + am + + o d am o 0 0 0 0 0 0 0 0 �� Q,0� n(D m o O o 0 0 0 0 0 Cl O E3 w ro e- 0) coO On (00 LO VO• M N �_ E -ri Q U C (� •ri -rl N F- Ga 0 FC H v� > � File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2626.D Operator RR Acquired 26 May 2021 8:45 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-06RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 26 Response 1 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 GOME2626.D\FID1A 25000 20000 15000 10000 5000 f 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 1 I� l V 141 � I 0.00 11.00 12.00 13.00 14.00 >C U rl O x a Ei O 4 -P a� ca U M O Ln C N r W � 0 W � / 04 N N Ln r 61 (N Lr) M O O W rl P� N rl NJ Q O O � N I / N F� >1 LO .-1 E-i ro rH N r� U M G1 a C7 0 Ln -1 oU • • U N N '--I M .. .. .. .. .. .. .. (1) i4 41 r a) r. ro O �t S4 (1) Z W -P °4 � a) H Z (0-H �-I.1 (1) is +-) 04 U ri .-I a) t5 m E m ro -HP4 G40r�HVi� 0 a) (D CD 4) d n cD to cn N N ��I I� � O O O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 + + o 0 0 0 0 0 0 0 0 °) o 0 0 0 0 0 0 0 0 c' W OD On too LO V M N File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2628.D Operator RR Acquired 26 May 2021 9:36 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-07RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 28 Response_ GOME2628.D\FID1A 85000i i 80000 75000 70000 65000 60000 55000 50000 45000 i 400001 350001 30000 25000 1 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 �4 U O x a H O 4 Ll -P M t7' Ln U N FC W o � W -rl U � QCO N Q0 ko Un N N •• � Ln N O O W � W N rl C�J >-I N 00 O O N I / N Ln I H ro r1 N aC � UM o / Ln a�rn U N N r N .. .. .. .. .. .. .. 1-1 N ro 0 ,Q (1) rz a�Hz N } 04 :n E U) ro cz U I~ (0 -H -H G4 o FC i-I U) 2: > 2 U co N LL_ M 04 N W CD O m m _O 0 0 0 Un 0 O 0 0 0 m 0 0 of 0 ao 0 0 00 O U� O 0 0 :n O O O O Uf u7 O O ui O z� O 0 G� Cl) O U) O N O r- r- r- P- P- r- 0 0 o O O o 0 0 0 �1 0 0 0 0 0 0 0 0 0 O o O o 0 0 0 0 N + + + + + + + + CD O O o 0 o CD U) N N N a) N a) a) W 0 0 O 0 0 O 0 CD c a co In M N r W On COD 0 0 M N 0 a F- File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2630.D Operator RR Acquired 26 May 2021 10:28 pm using AcgMethod GASBTEXE.M Instrument GC7 _ Sample Name: 2103212-08RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 30 Response_ 85000- 80000, 750001 70000 65000. 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOME2630.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 !1. 00 0 un N T O 00 '= U ciJo R LL N ma c Gn co m 41i A ro �° 'j r m C E E E A c 0 J N N cc0 c 1'- 1- 1.- m. Q':O m O m F N SPIIDS poA10810 IBM JilAIS"00 «� w O G 0 zoos ! Woos 80d ! issd rn f41114s11u81 t Q 30M S00AS l ¢ � m O y w LOB OW09 • dHl a CL E n L d S; m ePUVmS ! ePlueAO SApaeea •` F- °' zn a Z aO N y isll 110d SONS x �+ O a ca �„ A .i G �, Z ❑ '. :; sleiaw - ZZ elill 7. m `Y Si in m �`' •:M: p m V > > 0 � � • i i � i � � m N N a 3' ¢ 1 � N Q m 00011 IV .': _ a E EEl ''. qj U v. 00 3 • t— F- 0 ?iN z O 2 U p p p❑:�: m Eiv — C m o; c t� °ecltv n cg >a:.`• p p C y Q N U m N Y':: c am. #. E o W O a kn C c W r v o v o m m p N N a a O a. O 00 U 0 0 El m _ C /1 j v o ° C LS ,r�� cc co c� d c -- m� � c c c m� a w U I 'P cc z w w 3 1 U) Z 0 N Z Q U w I1 0) z U z O° o ■ f}§ f eggnog Cl) ~ ) } E 20 k \ CO`k� ° E ® ) k \ a) 0)7 0 ° - 2§ 0 z z - 2 E § _ §/t\2§ ® o ` $ ¥ 0 « ¥ 7 7 \ § § 2 k k 2£ E f a \ } k / Of/ \ �7 E - { R % $ $ 3 d)) b 3 ca ° ƒ } \ \ / k }} k / D cc - \ =2 em °)0 C E 3 3 k I°- / �m x§$E { F 2 k 7 \ / \ co k A § \ .2 E \ & 5 $ k w■ z a a O % ° 0\§� .0 CD s E 7 S c § - \ C § 7\ - _ E ¢ < [ k = e E a t 3 3@# a §)$ d 3 D g 7 7 ±§ a 2(® - §) / # \ \/) /\) m) E{ G A 2 § w w w w [CR j\E o§ ) § k�//k■.� G �� 2 0■ k 3 3 v ''■ " GLO o. V, N C N E Lddk E ULU N C O U� a� N N N v v v v v v v o o o v o v v o in c°n in c°n in in in in in c°n U) c°n ion 75 U) in in c c c c c c c c f0 Q O N Q O lC Q O fO Q O (9 3 Q O f0 Q O f6 Q O f0 Q O > > > > > N 00 O N O O N O O IL N O O N O O N w O N U.-l- N O N,�N N N NN NLL LL .V LL LL LL LL LL LL LL LL LL LLLL LL 0 .Q U 0 . Q Q Q> Q Q Q> Q> Q d N O N O N O N O N O N O N O N O c a> m > 2 > m > _m > m > m > m > 0 J C7 J 0 J C7 J C7 J (7 J U� J U J O N E N E N E N E N E N E N E N E O U 0 a0 0 N 0 a0 0 N 0 eD 0 N O -' O N 0 -' 0 N O oD O N O a0 O N 0 00 0 N c U • O V Q m Q m Q CD Q m Q m Q m Q CD Q m O N O N O M O M O O O O O O O O O O O fT] 3 " m o N1 co 0 to N T O co x cc E c� N .V L c Q� •— 0 y— 0 V •www'' - o W d D. CL f a W= U r LLO. m 2 anu �aa 1 c t0 e U U U U U U U U aa- A 0 0 2 v e a J U - J V J J J J N gL me U H U U U U �n m '0 a2S aLf o0 � m m m C a J M _ U U U Z - U (� L U U U D F E �= y ❑ 4 E mctiE U J U J U J U J J J U J 00 0 n COU) (n N V �uJi U) U) SPIIOS N PGAIOSIO 15301 1.n R3IAISO"00 O � O boos I V"Os cy 80d 13Sed A31114g31u81 N O OOLZs-SOOAS rn m V a O y L W9308OW0°J- dHl z E )PUInS �, as I GPIUSRO GAPaSaa d � � a Z ,e m N y 3519 llnd 909Zo v N ccL d t Z u SIS3SW - ZZ 81311 %{ X Ry. V1 U d tr m m } m to °s in > m 3 > . = 7CL m ♦ 3 1 1 v m N o iw �O E 'a 00 d ❑ ❑ 10 o u E EIS❑ ❑❑ in t' � • F ►= r o' U s 3 z00} �La a � �•• m ci m �$ m 0 m❑ c!1 (z a Z U ^ ) w C� 4x cc 1� $ "O o c y KAI O. p+ L00 C a O o a ac > a G. O 00 v U � �U3 Q rr ❑ ❑ m m m 0. E© �2! xw1��� V J r a3a3 d a o 6 z 0 U M m Q U W IL m Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2103479 Pacific Petroleum California P. O. Box 2646 Report Date: June 09, 2021 16:44 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvingoecusa.com This laboratory is accredited in accordance with the recognised International Standard ISO/IEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-IAF Communique dated Apri12017) 307 Roemer Way, Suite 300 \j /�y� client.oec.com\reports Santa Maria, CA 93454 �� !; www.oecusa.com Main: (805) 922-4772 ��-� rain TNI 2016 & ISO/IEC 17025:2017 Fax: (805) 925-3376 :j��\.�� Tt6Ltn9 CA-ELAP 2438, TNI 02666 %W Accreditation #99137 Page I of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum Califomia Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom East @ 12' 2103479-01 Solid Solid 06/03/2021 11:50 06/04/2021 12:50 Bottom West @ 12' 2103479-02 Solid Solid 06/03/2021 11:55 06/04/2021 12:50 SampleBatch Prepai-ation Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel do Motor Oil List B I F0145 06/04/2021 16:24 STLC Metals by ICP 601013 STLC BIF0261 06/09/2021 08:56 STLC Metals Extraction STLC Metals Extraction B 1 F0229 06/07/2021 16:29 Total Metals by CVAA Mercury Total EPA 7471A B IF0194 06/07/2021 07:40 Total Metals by ICP 601013 Total B I F0197 06/07/2021 08:26 Volatile Organic Compounds by GC/MS 8260B Full List BIF0146 06/04/2021 12:21 Volatile Organic TPH by GC/FID 8015 "1'PH-Gasoline B 1 F0154 06/04/2021 10:34 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: [805) 925-3376 Page 2 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mg/kg 1 B I F0194 06/07/21 16:25 EPA 747 ] A Total Metals by ICP Antimony ND 2.3 mg,/kg I B 1 F0197 06/07/21 14:12 EPA 6010B Arsenic r 5.6 1.9 Barium 120 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 73 0.47 Cobalt 18 0.47 Copper 47 0.93 Lead 8.2 0.47 Molybdenum ND 0.47 Nickel 130 0.47 f Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 49 1.9 Zinc 65 1.9 STLC Metals by ICP Chromium ND 0.020 mg/l. 2 BIF0261 06/09/21 14:34 STI.C/F.PA601(IB Volatile Organic TPH by GUND TPII Gasoline (('5-C12) ND 4.5 mg1kg 1 BIF0154 06/04/21 17:01 EPA 8015M Surrogate: 4-13romofhmroben_ene 929s, (39 - 157 ) N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 3 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 i Analytical Report for Samples E� Sample ID: Bottom East @ 12' Sampled : 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 mg/kg 1 BIF0145 TPH Motor Oil (('23-C40) ND 50 11 11" Surrogate: o-Teiphen1'1 R7 % (65 - 136 ) 11 06/05/21 12:12 EPA 8015M The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID : Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0,050 mg/kg 1 B1F0146 06/04/21 16:16 EPA8260B ^ Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 " Broniol'orm ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 r tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobenzenc ND 0.050 Chlorocthanc ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 4-Chlorotoluene ND 0.050 Dibromochloromethane ND 0.050 1,2-Dibromo-3-chloropropane ND 0.050 1,2-Dibronioethane (EDB) ND 0.050 Dibromomethane ND 0.050 1,2-Dichlorobenzene ND 0.050 " " 1.3-Dichlorobenzene ND 0.050 14-Dichlorobenzene ND 0.050 Dichlorodifluorcmiethanc ND 0.050 CCHI • 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 1, 1 -Dichloroethene ND 0.050 cis-1,2-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1.2-Dichloropropane ND 0.050 1,3-Dichloropropane ND 0.050 2,2-Dichloropropane ND 0.050 1.1-Dichloropropane ND 0.050 cis- 1.3-Dichloropropcne ND 0.050 trans- l,3-Dichloropropcne ND 0.050 Ethylbcnzcnc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical i Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.050 mg/kg 1 131F0140 06/04/21 16:16 EPA8200B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1. 1, 1,2-Tetrachloroethane ND 0.050 1.1,2,2-Tetrachloroethane ND 0.050 Tetrachlorocthcne (PCE) ND 0.050 Toluene ND 0.050 1,2,3-Trichlorobenzene ND 0.050 1.2,4-Trichlorobenzene ND 0.050 1,1,1-Trichloroethane ND 0.050 1,1,2-Trichlorocthane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorofluoromethane ND 0.050 1.2.3-Trichloropropane ND 0.050 1,2,4-Trimethylbenzene ND 0.050 13.5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Uihromofluoromethane 103 "/„ (74 - 12 2 ) Surrogate: Tolnene-(18 99 (65 - 128 ) Surrogate: 4-Brotnolluorohen_ene 105 % ( 75- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mglkg 1 B1 F0194 06/07/21 16:27 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B I F0197 06/07/21 14:15 EPA 601 OB Arsenic 7.4 1.9 Barium 160 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Cbromium 51 0.48 N-02 Cobalt 14 0.48 Copper 63 0.96 Lead 8.9 0.48 Molybdenum 0.57 0.49 Nickel 88 0.48 Selenium ND 1.9 Silver ND 0.49 " Thallium ND 0.96 Vanadium 52 1.9 Zinc 71 1.9 " STLC Metals by ICP Chromium ND 0.020 mg/L 2 B 1 F0261 06/09/21 14:37 STLC/EPA 6010B Volatile Organic TPH by GC/FID TPII Gasoline (('5-('12) ND 4.4 uig/kg 1 BIF0154 06/04/21 17:29 EPA 8015M Surrogate: 4-Bromq luorobcncene 95 % (.39 - 157) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples I Sample ID : Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GOOD TPH Diesel (03-C22) ND 9.9 mg,kg 1 BIF0145 06/0.5/21 12:34 EPA 8015M TPH Motor Oil (C23-C40) ND 50 Surrogate. o-Tetphenrl 90 3; (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.048 mglkg 1 BIF0146 06/04/21 15:48 EPA8260B Bromobenzene ND 0.048 Bronxichloromethane ND 0.048 Bromodichloromethane ND 0.048 Bromotorm ND 0.048 " Bromomethane ND 0.048 n-Butylbenzene ND 0.048 sec-Butylbenzene ND 0.048 tert-Butylbenzene ND 0.048 Carbon tetrachloride ND 0.048 Chlorobenzcnc ND 0.048 Chloroethane ND 0.048 " Chlorofonn ND 0.048 Chloromethane ND 0.048 2-Chlorotoluene ND 0.048 4-C'hlorotoluene ND 0.048 Dibromochloromethane ND 0.048 1,2-Dibronio-3-chloropropane ND 0.048 1,2-Dibromoethane (LDB) ND 0.048 Dibromomethane ND 0.048 1,2-Diehlorobenzene ND 0.048 1,3-Diehlorobenzene ND 0.048 1,4-Diehlorobenzene ND 0.048 " Dichloroditluoromethane ND 0.048 " I,1-Dichloroethane ND 0.048 1,2-Dichloroethane ND 0.048 1,1-Dichloroethene ND 0.048 cis-1.2-Dichloroethene ND 0.048 trans-1,2-Dichloroethene ND 0.048 1,2-Dichloropropane ND 0.048 " 1.3-Dichloropropane ND 0.048 2 2-Dichloropropane ND 0.048 " 1.1-Dichloropropene ND 0.048 cis- 1.3-Dichloropropcnc ND 0.048 " trans-1,3-Dichloropropcnc ND 0.048 Fthylbenzenc ND 0.048 CCIII The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.048 mgIg I B I F0146 06/04/21 15:48 EPA 8260B 4-Isopropyl Toluene ND 0.048 Isopropylbenzene ND 0.048 Methylene chloride ND 0.048 Naphthalene ND 0.048 n-Propylbenzene ND 0.048 Styrene ND 0.048 I_L1,2-Tetrachloroethane ND 0.048 1,L2,2-Tctrachloroethane ND 0.048 Tctrachlorocthcnc (PCE) ND 0.048 Toluene ND 0.048 1,2,3-Trichlorobenzene ND 0.048 1,2.4-Trichlorobenzene ND 0.048 1,1,1-Trichloroethane ND 0048 " 1.1,2-Trichloroethane ND 0.048 Trichloroethene (TCE) ND 0.048 Trichloro11uoromethane ND 0.048 1.2,3-Trichloropropane ND 0.048 1,2,4-1'rintethylbenzene ND 0.048 1.3.5-Trimethylbenzene ND 0.048 Vinyl chloride ND 0.048 " Xylcncs (total) ND 0.048 Surrogate: Dihronuilluuromethune 104 74 - 122) " Surrogate: Toluene-dS 102 (65 - 128) " Surrogate. 4-BronwJluorohen_ene 104 % ( 7.5 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 32 Oilfield Environmental &Compliance, Inc. I (-'�i W�� Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0194 -EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (B1F0194-BLK1) Analyzed: 06/07/21 12:49 Mercury ND 0.10 mglkg LCS (B1F0194-BSI) Analyzed: 06/07/21 12:53 ,_. Mercury 0.792 0.10 mg/kg 0.833 94 85-115 LCS Dup (B1F0194-BSD1) Analyzed: 06/07/21 13:30 Mercury 0.959 0.10 mg/kg 0.833 103 85-115 9 20 ' Duplicate (B1F0194-DUPl) Source: 2103489-02 Analyzed: 06/07/21 13:34 Mercury ND 0.097 mg,kg ND 20 Matrix Spike (B1F0194-MSI) Source: 2103489-02 Analyzed: 06/07/21 13:37 Mercury 0.827 0.091 mg/kg 0.755 ND 110 75-125 Matrix Spike Dup (B1F0194-MSD1) Source: 2103489-02 Analyzed: 06/07/21 13:39 Mercury 0.839 0.089 mg/kg 0.742 ND 113 75-125 1 20 Post Spike (B1F0194-PSI) Source: 2103489-02 Analyzed: 06/07/21 13:41 Mercury 5.52 ug/L 25.0 0.00199 22 85-115 QL-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page I of 32 r A Z rANR Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 -EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 ._. Blank (B1F0197-BLK1) Analyzed: 06/07/21 13:30 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 Chromium ND 0.50 Cobalt ND 0.50 Copper ND 1.0 Lead ND 0.50 " Molybdenum ND 0.50 Nickel N1) 0.50 Selenium N1) 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (B1F0197-BS1) Analyzed: 06/07/21 13:35 Antimony 92.0 2.5 mg/kg 100 92 80-120 Arsenic 97.2 2.0 100 97 80-120 Barium 99.6 1.0 100 100 80-120 Beryllium 95.1 0.50 100 95 80-120 Cadmium 98.2 0.25 100 98 80-120 Chromium 98.8 0.50 100 99 80-120 Cobalt 99,2 0.50 100 99 80-120 Copper 98.2 1.0 100 98 80-120 Lead 100 0.50 100 100 80-120 Molvbdenum 96.0 0.50 100 96 80-120 Nickel 99.6 0.50 100 100 80-120 Selenium 96.4 2.0 100 96 80-120 Silver 4.92 0.50 5.00 98 80-120 Thallimn 100 1.0 100 100 80-120 _ Vanadium 96.0 2.0 100 97 80-120 Zinc 98.6 2.0 100 99 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 12 of 32 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Totalby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 -EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSDI) Analyzed: 06/07/21 13:37 Antimony 94.8 2.5 mg/kg 100 95 80-120 3 20 Arsenic 98.8 2.0 100 99 80-120 2 20 Barium 101 1.0 100 101 80-120 1 20 Beryllium 96.5 0.50 100 96 80-120 1 20 Cadmium 99.2 0.25 100 99 80-120 1 20 Chromium 100 0.50 100 100 80-120 1 20 Cobalt 100 0.50 100 100 80-120 1 20 Copper 99.8 1.0 100 100 80-120 2 20 Lead 101 0.50 100 101 80-120 1 20 Molybdenum 98.2 0.50 100 98 80-120 2 20 - Nickel 101 0.50 100 101 80-120 1 20 Selenium 97.8 2.0 100 98 80-120 1 20 Silver 4.93 0.50 5.00 99 80-120 0.1 20 Thallium 102 1.0 100 102 80-120 1 20 Vanadium 98.0 2.0 100 98 80-120 1 20 Zinc 99.8 2.0 100 100 80-120 1 20 Duplicate (B1F0197-DUPI) Source: 2103489-01 Analyzed: 06/07/21 13:52 Antimony ND 2.4 mg'kg ND 20 Arsenic 1.22 1.9 ND 20 Barium 21.0 0.97 22.9 8 20 Beryllium ND 0.49 ND 20 Cadmium ND 0.24 ND 20 Chromium 1.94 0.49 2.02 4 20 Cobalt 1.40 0.49 1.78 24 20 QR-04 -� Copper 1.33 0.97 1.40 5 20 Lead 1.23 0.49 1.40 13 20 Molybdenum ND 0.49 ND 20 Nickel 1.31 0.49 1.34 2 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 3.86 1.9 4.18 8 20 Zinc 4.32 1.9 4.51 4 20 The results in this report apply to the samples analyzed in accordance with the chain ofcustody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MS1) Source: 2103489-01 Analyzed: 06/07/21 13:40 Antimony 70.3 2.3 mg/kg 93.4 ND 75 10-116 Arsenic 93.3 1.9 93.4 ND 100 77-121 Barium 119 0.93 93.4 22.9 102 30-169 Beryllium 90.1 0.47 93.4 ND 96 86-111 Cadmium 91.9 0.23 93.4 ND 98 81-112 Chromium 96.8 0.47 93.4 2.02 102 75-129 Cobalt 94.2 0.47 93.4 1.78 99 71-121 Copper 96.2 0.93 93.4 1.40 102 68-135 Lead 94.4 0.47 93.4 1.40 100 72-121 Molybdenum 88.2 0.47 93.4 ND 94 70-112 Nickel 95.2 0.47 93.4 1.34 101 73-121 Selenium 90.1 1.9 93.4 ND 97 76-116 Silver 4.56 0.47 4.67 ND 98 54-132 Thallium 92.3 0.93 93.4 ND 99 64-120 Vanadium 96.5 1.9 93.4 4.18 99 78-124 Zinc 98.0 1.9 93.4 4.51 100 50-143 Matrix Spike Dup (B1F0197-MSD1) Source: 2103489-01 Analyzed: 06/07/21 13:42 Antimony 70.4 2.4 mg/kg 95.8 ND 73 10-116 0.1 20 Arsenic 94.3 1.9 95.8 ND 98 77-121 1 20 Barium 116 0.96 95.8 22.9 97 30-169 3 20 Beryllium 91.2 0.48 95.8 ND 95 86-111 1 20 Cadmium 92.3 0.24 95.8 ND 96 81-112 0.6 20 Chromium 97.6 0.48 95.8 2.02 100 75-129 0.8 20 Cobalt 94.7 0.48 95.8 1.78 97 71-121 0.6 20 Copper 96.9 0.96 95.8 1.40 100 68-135 0.7 20 Lead 94.9 0.48 95.8 1.40 98 72-121 0.6 20 Molvbdenwn 89.6 0.48 95.9 ND 93 70-112 0.5 20 Nickel 95.5 0.48 95.8 1.34 98 73-121 0.3 20 Selenium 91.2 1.9 95.8 ND 95 76-116 1 20 Silver 4.64 0.48 4.79 ND 97 54-132 2 20 Thallium 93.1 0.96 95.8 ND 97 64-120 0.9 20 Vanadium 97.2 1.9 95.8 4.18 97 78-124 0.7 20 Zinc 103 1.9 95.8 4.51 103 50-143 5 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8051 925-3376 Page 14 of 32 r A i A 4 mma Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PS1) Source: 2103489-01 Analyzed: 06/07/21 13:45 Antimony 2.03 mg/L 2.00 0.00248 101 75-125 Arsenic 2.04 2.00 0.0178 101 75-125 Barium 2.50 2.00 0.460 102 75-125 Beryllium 1.96 2.00 0.00218 98 75-125 Cadmium 2.00 2.00 -0.00308 100 75-125 Chromium 2.07 2.00 0.0409 101 75-125 Cobalt 2.06 2.00 0.0359 101 75-125 Copper 2.06 2.00 0.0283 102 75-125 Lead 2.07 2.00 0.0283 102 75-125 Molybdenum 2.01 2.00 -0.00109 101 75-125 - • Nickel 2.06 2.00 0.0271 102 75-125 Selenium 1.99 2.00 -0.0103 99 75-125 Silver 0.0945 0.100 -0.00169 94 75-125 Thallium 2.03 2.00 -0.00407 101 75-125 Vanadium 2.08 2.00 0.0842 100 75-125 Zinc 2.10 2.00 0.0909 WI 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 STLC Metals by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0261 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (Bl F0261-BLKI) Analyzed: 06/09/21 13:50 Chromium ND 0.010 mg/L LCS (BlF0261-BS1) Analyzed: 06/09/21 14:17 Chromium 10.1 0.010 mg/L 10.0 LCS Dup (B1F0261-BSD1) Analyzed: 06/09/21 14:19 Chromium 10.2 0.010 mg/L 10.0 Duplicate (B1F0261-DUPI) Source: 2103218-01 Analyzed: 06/09/21 14:27 Chromium 1.22 0.020 mg/I, 1.22 Leach Fluid Blank (B1F0261-LBK1) Analyzed: 06/09/21 13:52 Chromium ND 0.020 mg/L Leach Fluid Blank (B1F0261-LBK2) Analyzed: 06/09/21 13:55 Chromium ND 0.020 mg/I. Leach Fluid Blank (BlF0261-LBK3) Analyzed: 06/09/21 13:58 Chromium ND 0.020 mg/L 101 80-120 102 80-120 0.5 20 0.08 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLKI) Analyzed: 06/04/21 12:45 TPH Gasoline (C5-C 12) ND 0.49 mg/kg Surrogate:4-Bromollruuobenzene 0.107 110.123 87 39-157 LCS (B1F0154-BS1) Analyzed: 06/04/21 11:48 TP11 Gasoline (C5-C12) 1.38 0.50 mg/kg 0.998 139 68-139 Surrogate:4-Bronrolluorobenzene 0.158 0.125 126 39-157 LCS Dup (B1F0154-BSDI) Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12) 1.29 0.50 mg/kg 1.00 128 68-139 7 20 Surrogate:4-BromoJluorobenzene 0.146 0.125 116 39-157 Duplicate (B1F0154-DUP1) Source: 2103455-02RE1 Analyzed: 06/04/21 15:35 TPH Gasoline (C5-('12) ND 0.50 mg/kg 0.113 20 Surrogate. 4-Bromognorohenzene 0.113 " 0.124 92 39-157 Matrix Spike (B1F0154-MSI) Source: 2103429-02 Analyzed: 06/04/21 19:23 TPH Gasoline (C5-('12) 0,905 0.49 mg/kg 0.973 ND 93 10-171 Surrogate: 4-Bromq luorohcnceue 0.132 " 0.122 109 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 wvvw.oecusa.com FAX: 805 925-3376 Page 17 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Semi-Volatile1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) Analyzed: 06/04/21 11:45 Tl'H Diesel WI3-('22) ND 10 ing/kg TPH Motor Oil (C23-C40) ND 50 11 Surrogate: n-Teipheiwl 41.5 " 50.0 83 65-136 LCS (B1F0145-BS1) Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22) 434 10 mg/kg 499 87 72-115 TPI I Motor Oil (C23-C40) 420 50 499 84 74-126 - Surrogate. o-Tciphenyl 45.8 49.9 92 65-136 LCS Dup (B1F0145-BSD1) Analyzed: 06/04/21 12:07 TPI I Diesel (C I 3-C22) 444 10 mg/kg 499 89 72-115 2 20 TPH Motor Oil (C23-C40) 441 50 499 88 74-126 5 20 Surrogate: o-Teiphernl 46.7 49.9 94 65-136 Duplicate (B1F0145-DUPI) Source: 2103472-01 Analyzed: 06/04/21 16:23 TPH Diesel (C13-('22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) ND 50 ND 20 Surrogate: o-Teiphenvl 40.5 49.9 81 65-136 Matrix Spike (B1F0145-MS1) Source: 2103472-01 Analyzed: 06/04/21 15:37 TPH Diesel (Cl3-C22) 452 10 mg/kg 498 ND 91 46-147 TPH Motor Oil (C23-C40) 500 50 498 ND 100 35-171 Surrogate: o-Teiphenvl 41.6 49.8 84 65-136 Matrix Spike Dup (B1F0145-MSD1) Source: 2103472-01 Analyzed: 06/04/21 16:00 TPH Diesel (C13-C22) 496 10 mg/kg 498 ND 100 46-147 9 20 TPH Motor Oil (('23-('40) 517 50 498 ND 104 35-171 3 20 Surrogate: o-Teiphenyl 44.0 49.8 88 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLKI) Analyzed: 06/04/21 11:32 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 Bromochloromcthanc ND 0.0050 Bromodiehloromethane ND 0.0050 " Bromoform ND 0.0050 " Bromomethane ND 0.0050 " n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride NI) 0.0050 " Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 " Chloromethane ND 0.0050 " 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromethane NI) 0.0050 1,2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (EDB) ND 0.0050 " Dibronximethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1,3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 " Dichloroditluoromethanc ND 0.0050 " I,1-Dichloroethene ND 0.0050 " I.2-Dichlorocthane ND 0.0050 " 1, 1 -Dichloroethene NI) 0.0050 cis-1,2-Dichloroethene ND 0.0050 " trans- I,2-Dichloroethene NI) 0.0050 1,2-Dichloropropane ND 0.0050 1,3-Dichloropropane NI) 0.0050 2.2-Dichloropropane ND 0.0050 1,1-Dichloropropene ND 0.0050 " cis-1.3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 " F,thylbenzene ND 0.0050 " Ilexachlorobutadiene ND 0.0050 " 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCHI CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 �. Blank (B1F0146-BLK1) Analyzed: 06/04/21 11:32 Styrene ND 0.0050 mg/kg 1.1.1,2-Tetrachloroethane ND 0.0050 1,1,2,2-1'etrachloroethane ND 0.0050 ` Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 1,2,3-Trichlorobenzene ND 0.0050 " - 1,2.4-Trichlorobenzene ND 0.0050 L1,1-Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 -- Trichlorotluoromethane ND 0.0050 " 1,23-Tricliloropropane ND 0.0050 1,2,4-Trimethylbenzene ND 0.0050 13,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylenes (total) ND 0.0050 Surrogate: Dibromu/luoromethane 0.0516 0.0498 104 74-122 Surrogate: Toluene-d8 0.0503 0.0498 10l 05-128 Surrogate:4-Bromolluorohenzene 0.0529 0.0498 106 75-121 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 Benzene 0,0406 0.0050 mglkg 0.0398 102 70-131 Bromobenzene 0.0466 0.0050 0.0398 117 74-130 Bromochloromcthane 0.0399 0.0050 0.0398 100 64-133 Bromodichloromethane 0,0445 0.0050 0.0398 112 69-137 ' Bromofonn 0.0447 0.0050 0.0398 112 55-132 Bromomethane 0.0407 0.0050 0.0398 102 10-142 n-Butylbenzene 0.0476 0.0050 0.0398 120 64-156 sec-Butylbenzene 0.0493 0.0050 0.0398 124 75-155 tert-Butylbenzene 0.0492 0.0050 0.0398 121 74-144 Carbon tetrachloride 0.0442 0.0050 0.0399 111 67-135 Chlorobenzene 0.0445 0.0050 0.0398 112 73-134 Chloroethane 0.0390 0.0050 0.0398 98 10-107 Chloroform 0.0412 0.0050 0.0398 104 69-124 Chloromethane 0.0297 0.0050 0.0398 75 34-136 2-Chlorotoluene 0.0454 0.0050 0.0398 114 75-135 ' 4-Chlorotoluene 0.0460 0.0050 0.0398 116 70-138 Dibromochloromethane 0.0439 0.0050 0.0398 110 67-135 1,2-Dibromo-3-chloropropanc 0.0435 0.0050 0.0398 109 41-149 1,2-Dibromocthane (EDB) 0.0409 0.0050 0,0398 103 68-131 - Dibromomethanc 0.0433 0.0050 0.0398 109 61-140 12-Dichlorobenzene 0.0458 0.0050 0.0398 115 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 1,3-Dichlorobenzcnc 0.0462 0.0050 mgtkg 0.0398 116 76-138 1,4-Dichlorobenzene 0.0457 0.0050 0.0398 115 72-132 Dichlorodifluoromcthanc 0.0210 0.0050 0.0398 53 10-155 CCFH 1,1-Dichloroethene 0.0389 0.0050 0.0398 98 63-139 12-Dichlorocthanc 0.0416 0.0050 0.0398 104 64-126 1,1-Dichloroethene 0.0342 0.0050 0.0398 86 52-167 cis-1.2-Dichloroethene 0.0401 0.0050 0.0398 101 70-135 trans-1,2-Dichloroethene 0.0392 0,0050 0.0398 99 67-147 1,2-Dichloropropane 0.0406 0.0050 0.0398 102 68-131 1,3-Dichloropropmie 0.0405 0.0050 0.0398 102 64-128 2,2-Dichloropropane 0.0432 0.0050 0.0398 109 63-154 1, 1 -Dichloropropene 0.0393 0.0050 0.0398 99 68-138 cis-1,3-Dichloropropene 0.0416 0.0050 0.0398 105 72-134 trans- l,3-Dichloropropene 0.0437 0.0050 0.0398 110 69-132 Ethylbenzene 0.0449 0.0050 0.0398 113 68-136 IiexacliIOrobutadiene 0.0540 0.0050 0.0398 137 72-198 4-Isopropyl Toluene 0.0504 0.0050 0.0398 127 74-150 Isopmpylbenzene 0.0473 0.0050 0.0398 119 71-149 Methylene chloride 0.0346 0.0050 0.0398 87 51-127 Naphthalene 0.0482 0.0050 0.0398 121 57-158 n-Propylbenzene 0.0474 0.0050 0.0398 119 70-143 Styrene 0.0456 0,0050 0.0398 115 68-139 1,1,1,2-Tetrachloroethane 0.0459 0.0050 0.0398 115 76-130 1,1,2,2-Tetrachloroethane 0.0399 0.0050 0.0398 100 60-136 Tetrachloroethane WCE) 0.0443 0.0050 0.0398 111 73-139 Toluene 0.0430 0.0050 0.0398 108 72-128 1,2,3-Trichlorobenzene 0.0507 0.0050 0.0398 127 61-166 1.2.4-Trichlorobenzene 0.0502 0.0050 0.0398 126 71-158 1,1,1-Trichloroethane 0.0424 0.0050 0.0398 107 71-135 1,12-Trichloroethane 0.0414 0.0050 0.0398 104 64-132 Trichloroethene (TCE) 0.0442 0.0050 0.0398 111 74-139 Trichlorotluoromethane 0.0429 0.0050 0.0398 108 30-156 1,2,3-Trieliloropropane 0.0452 0.0050 0.0398 114 67-123 12,4-Trimethylbenzene 0.0454 0,0050 0.0398 114 68-134 13,5-Trimethylbenzene 0.0461 0.0050 0.0398 116 71-140 Vinyl chloride 0.0326 0.0050 0.0398 82 43-144 Xylenes(total) 0.133 0.0050 0.119 112 69-138 Surrogate: Dihrantgihrorumethune 0.0525 0.0497 106 74-122 Surrogate: Toluene-dN 0.0517 0.0497 104 65-128 Surrogate:4-Bromolluorohenrerre 0.0530 0.0497 107 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control J Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSDI) Analyzed: 06/04/21 10:13 Benzene 0.0423 0.0050 mg/kg 0.0400 106 70-131 4 20 Bromobenzene 0.0498 0.0050 0.0400 124 74-130 7 20 Bromochloronrcthanc 0.0412 0.0050 0.0400 103 64-133 3 20 Bromodichloromethane 0.0455 0.0050 0.0400 114 69-137 2 20 Bromolorin 0.0458 0.0050 0.0400 115 55-132 2 20 Bromomethane 0.0391 0.0050 0.0400 98 10-142 4 20 n-Butylbenzene 0.0476 0.0050 0.0400 119 64-156 0.1 20 sec-Butylbenzene 0.0508 0.0050 0.0400 127 75-155 3 20 tert-Butylbenzene 0.0496 0.0050 0.0400 124 74-144 3 20 Carbon tetrachloride 0.0456 0.0050 0.0400 114 67-135 3 20 Chlorobenzene 0.0457 0.0050 0.0400 114 73-134 3 20 Chloroethane 0.0394 0.0050 0.0400 98 10-167 1 20 Chloroform 0.0421 0.0050 0.0400 105 69-124 2 20 (Woromethane 0.0308 0.0050 0.0400 77 34-136 4 20 2-Chlorotoluene 0.0452 0.0050 0.0400 113 75-135 0.4 20 44Chlorotoluene 0.0468 0.0050 0.0400 117 70-138 2 20 Dibromochloromethane 0.0463 0.0050 0.0400 116 67-135 5 20 1,2-Dibromo-3-chloropropane 0.0461 0.0050 0.0400 115 41-149 6 20 1.2-Dibromoethane (EDB) 0.0422 0.0050 0.0400 105 68-131 3 20 Dibromomethane 0.0459 0.0050 0.0400 115 61-140 6 20 1,2-Dichlorobenzene 0.0472 0.0050 0.0400 118 76-136 3 20 1,34)ichlorobenzenc 0.0489 0.0050 0.0400 122 76-138 6 20 1,4-Dichlorobenzene 0.0472 0.0050 0.0400 its 72-132 3 20 Dichlorodif loromethanc 0.0228 0.0050 0.0400 57 10-155 8 20 I,1-Dichloroethene 0.0405 0.0050 0.0400 101 63-139 4 20 1,2-Dichlorocthanc 0.0425 0.0050 0.0400 106 64-126 2 20 1,1-Dichloroethene 0.0347 0,0050 0.0400 87 52-167 2 20 cis-l2-Dichloroethene 0.0420 0.0050 0.0400 105 70-135 5 20 trans- l,2-Diehl oroethene 0.0411 0.0050 0.0400 100 67-147 2 20 1,2-Dichloropropane 0.0430 0.0050 0.0400 107 68-131 6 20 1.3-Dichloropropane 0.0426 0.0050 0.0400 106 64-129 5 20 2.2-Dichloropropane 0.0446 0.0050 0.0400 111 63-154 3 20 1,1-Dichloropropene 0.0406 0.0050 0.0400 102 68-138 3 20 cis-1.3-Dichloropropene 0.0434 0.0050 0.0400 108 72-134 4 20 trans-1,3-Dichloropropene 0.0454 0.0050 0.0400 114 69-132 4 20 Fthylbenzene 0.0470 0.0050 0.0400 118 68-136 5 20 Ilexachlorobutadiene 0.0549 0.0050 0.0400 137 72-198 0.5 20 4-Isopropyl Toluene 0.0514 0.0050 0.0400 128 74-150 2 20 Isopropylbenzene 0.0499 0.0050 0.0400 125 71-149 5 20 D(ethylene chloride 0.0360 0.0050 0.0400 90 51-127 4 20 Naphthalene 0.0511 0.0050 0.0400 128 57-158 6 20 n-Propylbenzene 0.0466 0.0050 0.0400 116 70-143 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCFH CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 32 i A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSDI) Analyzed: 06/04/21 10:13 Styrene 0.0479 0.0050 mgtkg 0.0400 120 68-138 5 20 1, 1, 1,2-Tetrachloroethane 0.0490 0.0050 0.0400 123 76-130 7 20 1.1,2,2-Tetrachlorocthanc 0.0417 0.0050 0.0400 104 60-136 5 20 Tetrachloroethene(PCE) 0.0454 0.0050 0.0400 114 73-138 3 20 Toluene 0.0439 0.0050 0.0400 110 72-128 2 20 1,2,3-Trichlorobenzene 0.0520 0.0050 0.0400 130 61-166 3 20 1,2.4-Trichlorobenzene 0.0512 0.0050 0.0400 128 71-158 2 20 1, 1, 1 -Trichloroethane 0.0432 0.0050 0.0400 108 71-135 2 20 1,1,2-Trichloroethane 0.0448 0.0050 0.0400 112 64-132 8 20 Trichloroethene (TCE) 0.0448 0.0050 0.0400 112 74-139 1 20 Trichlorotluoromethane 0.0430 0.0050 0.0400 107 30-156 0.1 20 1,2,3-Trichloropropane 0.0463 0.0050 0.0400 116 67-123 3 20 1,2,4-Trimethylbenzene 0.0459 0.0050 0.0400 115 68-134 1 20 1,3,5-Trimethylbenzene 0.0465 0.0050 0.0400 116 71-140 0.9 20 Vinyl chloride 0.0338 0.0050 0.0400 84 43-144 3 20 Xylenes (total) 0.139 0.0050 0.120 116 69-138 4 20 Surrogan•:1)ih+rnnoJTuurunrcghc++rc• 0.0519 0.0500 104 74-122 Surrogate: Toluene-dN 0.0510 0,0500 102 65-128 Surrogate:4-BromuJTuorohen_ene 0.0530 0.0500 106 7-5-I21 Duplicate (B1F0146-DUPI) Source: 2103474-01 Analyzed: 06/04/21 15:22 ISkrrns Benzene ND 0.0050 mgIg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromethane ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibrcnnochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropanc ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibromomcthane ND 0.0050 ND 20 12-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WwW.oecusa.com FAX: 805 925-3376 Page 23 of 32 .(., Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate(B1F0146-DUP1) Source:2103474-01 Analyzed: 06/04/21 15:22 ISIoHS 13-Dichlorobenzenc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene NI) 0.0050 ND 20 Dichlorodifluoromethanc ND 0.0050 ND 20 CCM 1,1-Dichloroethanc NI) 0.0050 ND 20 1.2-Dichloroethanc ND 0.0050 NI) 20 l,l-Dichloroethene ND 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 12-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2.2-Dichloropropane ND 0,0050 NI) 20 1,1-Dichloropropene ND 0.0050 ND 20 cis-1.3-Dichloropropene ND 0.0050 ND 20 mans-1,3-Dichloropropene ND 0.0050 ND 20 Ethylbenzene ND 0.0050 NJ) 20 ItexachlOTObutadiene ND 0.0050 ND 20 4-1sopropyl Toluene NI) 0.0050 ND 20 Isopropylbenzene ND 0.0050 " ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 " NI) 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1, 1, 1,2-Tetrachloroethane ND 0.0050 ND 20 1,1,2,2-Tetrachlorocthanc ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1.24-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane NI) 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorofluoromethane NI) 0.0050 ND 20 1,2,3-Trichloropropane NI) 0.0050 ND 20 I. A-Trinrethylbenzene ND 0.0050 NJ) 20 1,3,5-Trim ethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dihtvmuiluuromethanc 0.0538 0.0498 108 74-122 Surrogate:7oluene-d8 0.0509 0.0498 102 65-128 Surrogate:4-Bromofuoroben_ene 0.0506 0.0498 102 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Method Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal ' 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NELAP STLC Metals by ICP 6010E STLC Chromium STLC/EPA 601 UB Solid OEC, Internal r STLC Metals Extraction STLC Metals Extraction STLC Water OEC. Internal Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, Internal Total Metals by ICP - 6010B Total Antimony EPA 6010B Solid OEC, C A-ELAP,NELAP 6010B Total Arsenic EPA 6010B Solid OEC. CA-ELAP,NELAP 6010E Total Barium E13A 60108 Solid OEC, CA-ELARNELAP 6010B Total Beryllium EPA 6010E Solid OEC, CA-F.LAP,NELAP 6010E Total Cadmium EPA 6010B Solid OEC, CA-ELAP.NELAP 601013 Total Chromium EPA 6010E Solid OEC, CA-ELAP,NELAP 6010B Total Cobalt EPA 6010E Solid OEC, C'A-ELAP,NELAP 6010B Total Copper EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Lead EPA 6010B Solid OEC, CA-ELAP,NFLAP 601 OB Total Molybdenum EPA 6010B Solid OEC, CA-ELAP.NELAP 6010B Total Nickel EPA 001013 Solid OF('. CA-FLAP.NELAP 6010B Total Selenium EPA 6010B Solid OEC, CA-ELAP.NELAP 6010B Total Silver EPA 6010B Solid OEC, CA-ELAP.NELAP 6010B Total Thallium EPA 6010B Solid OEC, CA-FLAP,NELAP 6010E Total Vanadium EPA 6010B Solid OEC, CA-ELAP,NELAP 6010E Total Zinc EPA 6010E Solid OEC. CA-ELAP,NELAP Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC, CA-FLAP,NFLAP 8260B Full List EPA 8260B Solid OEC, Internal Volatile Organic TPH by GC/FID 8015 "1TH-Gasoline EPA 8015M Solid DEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 32 -7 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 DefinitionsNotes and Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference CCFH The CCV for this analyte tailed high. Results for this analyte may be biased high. CCl Il The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. IS1owS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above 1 Ox STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state!tederal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 26 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 32 0 0 0 0 0 0 0 0 O ai 0 0 0 co O O co O 0 0 r- 2 U Q O Un LL w N O 0 -O O U- I m � i ui C �4 U o O "' Q x � • a N F � H Lr) O O O O C X 4-) o N W O / tS M N Q, LO O ZT O l0 r. . 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T m m m r 0 a ¢ N U a: CL E . g m c 00 oil Q Y H N m E m E ❑ Q: " U 0 O0 zz w 0o m c .Q .°' o o a�. E c 0 O U ..m. m o ..0+ io C .m.. m G 8 Z V N Lp �❑ i X o c, A w o d of i. j5 ur N 'Q N A C w . p 0, C C G N 1 • CamC' C ��' a O o °' O o _, 3 i ca a a 0 90 U -� v, U N 8 o ❑❑ m m m 2 L m m m m A)CL E r N a N E o c°a Q s i F a FQ- .� c c r N v, o y C E A .�. E N C c C N� d d U I- 6i Z O F u F Z J Q U W a w Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102742 Pacific Petroleum California P. O. Box 2646 Report Date: May 06, 2021 17:25 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 05, 2021 08:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page I of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report t Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by: Lab ID : 2102742-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mg/kg 1 B1F0098 05/05/21 12:11 EPA 7471A Total Metals by ICP Antimony ND 2.5 mgtkg 1 B I F0102 05/06/21 13:33 EPA 6010B • Arsenic 7.8 2.0 Barium 120 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 44 0.50 Cobalt 18 0.50 Copper 36 0.99 Lead 16 0.50 Molybdenum ND 0.50 _ Nickel 71 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 43 2.0 Zinc 68 2.0 Volatile Organic TPH by GC/FID TPHGasoline (C5-C12) 19 4.4 mg/kg 1 BlE0095 05/05/2112:06 EPA9015M D-04 Surrogate: 4-Bromo/htoroben_ene 10911,11 (39 - 157) 11 Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 490 10 mg/kg 1 BI E 0062 05/05/21 19:52 EPA 8015M ' TPII Motor Oil (('23-C40) ND 50 " " " " " Surrogate: o-Tejphenrl 89'IN (65 - 136) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.coni FAX: 805 925-3376 Page 3 of 37 WK Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by : Lab ID: 2102742-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.3 mg/kg 1000 B1 E0101 05/05/21 16:56 EPA 8260B 4-Isopropyl Toluene ND 1.3 " " lsopropylbenzene ND 1.3 Methylene chloride ND 1.3 " Naphthalene ND 1.3 " n-Propylbenzene ND 1.3 Styrene ND 1.3 1,1.1,2-Tetrachloroethane ND 1.3 1.1,2,2-1'etrachloroethane ND 1.3 " Tctrachlorocthcnc (PCE) ND 1.3 Toluene ND 1.3 1,2,3-Triehlorobenzene ND 1.3 I.2,4-TTichlorobenzene ND 1.3 1, 1, 1 -Trichloroethane ND 1.3 ^ 1,1,2-Trichloroethane ND 1.3 Trichloroethene (TCE) ND 1.3 Trichlorotluoroniethane ND 1.3 1,23-Trichloropropane ND 1.3 1,2.4-Triniethylbenzene ND 1.3 1.3.5-Triniethylbenzene ND 1.3 Vinyl chloride ND 1.3 Xylencs (total) ND 1.3 Surrogate: Uihrmnuflamzmtethane 95 %, ( 74 - 122) " Surrogate: Toluene-d8 95 % ( 65 - 128 ) . Surrogate: 4-Bromn/lnnrollen_ene 90 ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : NE Corner Sampled: 05/04/21 14:35 Matrix: Solid Sampled by: Lab ID : 2102742-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mg/kg 1000 B 1 E0101 05/05/21 17:24 EPA 8260B Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 12 Chloroethane ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibronioethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 " Dichloroditluoromcthane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1.2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis- 1.3-Dichloropropcne ND 1.2 trans-1,3-Dichloropropcne ND 1.2 Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by: Lab ID: 2102742-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B I E0098 05/05/21 12:15 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 Bl E0102 05/06/21 13:46 EPA 601 OB Arsenic 4.5 1.9 Barium 200 0.93 Beryllium ND 0.47 r Cadmium ND 0.23 Chromium 310 0.47 N-02, N-03 Cobalt 55 0.47 " F' Copper 45 0.93 Lead 9.5 0.47 Molybdenum 0.68 0.47 Nickel 430 0.47 N-02 Selenium ND 1.9 Silver ND 0.47 -- Thallium ND 0.93 Vanadium 70 1.9 Zinc 69 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 7.8 5.0 mg/kg 1 BIE0095 05/05/2) 12:58 EPA8015M D-04 . Surrogate: 4-Brumo/luorobenzene 101 `/ (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 220 10 mg/kg I BIE0062 05/05/21 21:51 EPA 8015M TPH Motor Oil (C23-C40) ND 50 " " " " 1. Surrogate: o-TerphenYl 84 L (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 37 i Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by: Lab ID : 2102742-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlombutadiene ND 1.2 mg/kg 1000 B1E0101 05/05/21 17:51 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 12 Styrene ND 1.2 " 1, 1, 1,2-Tetrachloroethane ND 1.2 " 1,1,2,2-1'etrachloroethane ND 1.2 " Tetrachloroethane (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 " 12,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroelhane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1,2.4-Trimethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate. 93 % ( 74 - 122) " Surrogate: Toluene-dS 94 % (65 - 126 ) Surrogate: 4-Bromolluoroben_ene SH % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of 37 --I Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : SE Corner Sampled: 05/04/21 14:45 Matrix: Solid Sampled by : Lab ID : 2102742-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgikg 1000 B1E0101 0510512118:18 FPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 " Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chlorocthane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 " 1,2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobenzene ND 1.2 " 1,4-Dichlorobenzene ND 1.2 " Dichlorodifluoromethanc ND 1.2 1.1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 " 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 12-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropanc ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report Sample ID: Center Sampled: 05/04/21 14:50 Matrix: Solid Sampled by: Lab ID : 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.086 mg/kg 1 BIE0098 05/05/21 12:19 EPA 747]A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I E0102 05/06/21 13:52 EPA 601(1B Arsenic 7.0 1.9 Barium 140 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 72 0.48 N-02 Cobalt 22 0.48 Copper 78 0.96 Lead 15 0.48 blolvbdenum 0.99 0.49 Nickel 160 0.49 Selenium ND 1.9 Silver ND 0.49 Thallium 1.3 0.90 Vanadium 62 1.9 'Line 80 1.9 - Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 7.7 4.8 mg/kg I B 1 E0095 05/05/21 13:49 EPA 8015M D-04 Surrogale: 4-Bromofhtorohenzene 106 % (39 - 157) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 350 10 mg/kg I BIE0062 05/05/2122:38 EPA8015M TPH Motor Oil (C23-C40) ND 50 " " " " Surrogate: o-Terpheuvl 86 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: Center Sampled: 05/04/21 14:50 Matrix: Solid Sampled by: Lab ID : 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hex achlorobutadiene ND 1.2 mg/kg 1000 B1 E0101 05/05/21 18:46 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1.1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 F 1,2,3-Trichlorobcnzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " 1,1.2-Trichloroethane ND 1.2 Trichloroethene (TC'E) ND 1.2 Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1.14-Trimethylbenzene ND 1.2 1.3,5-Triwethylbenzene ND 12 Vinyl chloride - ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromolluoromethanc 94 % (74 - 122) Surrogate: Toluene-d8 95 ;'S, (65 - 128) Surrogate: 4-Brww!Iluorohen_ene 88 (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: f.805) 925-3376 Page 17 of 37 r-� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Total Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Blank (B1E0102-BLK1) Analyzed: 05/06/21 13:12 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium ND 0.50 „ Cobalt ND 0.50 " Copper ND 10 " Lead ND 0.50 Molybdenum ND 0.50 Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (B1E0102-BS1) Analyzed: 05/06/21 12:50 Antimony 99.2 2.5 mg/kg 100 99 80-120 Arsenic 99.8 2.0 " 100 100 80-120 Barium 102 1.0 100 102 80-120 Beryllium 96.5 0.50 100 96 80-120 Cadmium 101 0.25 100 101 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 102 0.50 100 102 80-120 Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium 97.7 2.0 100 98 80-120 Silver 4.81 0.50 " 5.00 96 80-120 Thallium 104 1.0 100 104 80-120 Vanadium 98.6 2.0 100 99 80-120 Zinc 101 2.0 100 101 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 37 1( M�� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Matrix Spike (B1E0102-MSI) Source: 2102717-02 Analyzed: 05/06/21 12:55 Antimony 26.4 2.5 mglkg 99.2 ND 27 10-116 Arsenic 105 2.0 99.2 8.39 98 77-121 Barium 193 0.99 99.2 97.2 97 30-169 Beryllium 93.6 0.50 99.2 0.691 94 86-111 Cadmium 93.6 0.25 99.2 ND 94 81-112 Chromium 118 0.50 99.2 16.2 103 75-129 Cobalt 102 0.50 99.2 8.09 94 71-121 Copper 119 0.99 99.2 19.7 too 68-135 Lead 105 0.50 99.2 11.8 94 72-121 Molybdenum 89.4 0.50 99.2 1.58 89 70-112 Nickel 114 0.50 99.2 19.7 95 73-121 Selenium 89.8 2.0 99.2 ND 91 76-116 Silver 4.31 0.50 4.96 ND 87 54-132 Thallium 89.0 0.99 99.2 ND 90 64-120 Vanadium 130 2.0 99.2 32.7 98 78-124 Zinc 158 2.0 99.2 64.4 94 50-143 Matrix Spike Dup (B1E0102-MSD1) Source: 2102717-02 Analyzed: 05/06/21 12:57 Antimony 29.7 2.4 mg1kg 94.4 ND 31 10-116 12 20 Arsenic 103 1.9 94.4 8.39 101 77-121 2 20 Barium 182 0.94 94.4 97.2 89 30-169 6 20 Beryllium 91.6 0.47 94.4 0.691 96 86-111 2 20 Cadmium 91.5 0.24 94.4 ND 97 81-112 2 20 Chromium 113 0.47 94.4 16.2 103 75-129 4 20 Cobalt 99.2 0.47 94.4 8.09 96 71-121 3 20 Copper 114 0.94 94.4 19.7 l00 68-135 4 20 Lead 102 0.47 94.4 11.8 96 72-121 3 20 Molybdenum 88.9 0.47 94.4 1.58 92 70-112 0.6 20 Nickel 111 0.47 94.4 19.7 96 73-121 3 20 Selenium 88.7 1.9 94.4 ND 94 76-116 1 20 Silver 4.23 0.47 4.72 ND 90 54-132 2 20 Thallium 87.0 0.94 94.4 ND 92 64-120 2 20 Vanadium 120 1.9 94.4 32.7 98 78-124 4 20 Zinc 153 1.9 94.4 64.4 94 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 4742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic TPH by 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1E0095 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/05/21 06:24 Blank (B1E0095-BLKI) Analyzed: 05/05/21 09:00 TPH Gasoline (C5-Cl2) ND 0.50 mg/kg Stu•rogate:4-Bromglluorvbenzene 0.134 110.124 108 39-157 -- LCS (B1E0095-BS1) Analyzed: 05/05/21 08:09 TPH Gasoline (C5-C12) 0.917 0.50 mg/kg 0.992 92 68-139 Surrogate:4-Bromofluorohenrene 0.158 " 0.124 127 39-157 - LCS Dup (B1E0095-BSD1) Analyzed: 05/05/21 08:34 TPH Gasoline (C5-C12) 1.03 0.50 mg/kg 0.994 103 68-139 11 20 Sur•rogate:4-Bromofluorohenzene 0.157 0.124 127 39-157 Duplicate (B1E0095-DUPI) Source: 2102652-01 Analyzed: 05/05/21 09:59 TPH Gasoline (('5-02) ND 5.2 mg/kg ND 20 Sur•rogate:4-Brontq/luorohenzene 1.30 111.30 100 39-157 Matrix Spike (B1E0095-MS1) Source: 2102652-01 Analyzed: 05/05/21 14:41 TPH Gasoline (C5-('12) 7.97 4.9 mg/kg 9.80 ND 81 10-171 Surrogate: 4-Bromofluorohen_c•ne 1.40 111.23 115 39-157 Matrix Spike Dup (B1E0095-MSD1) Source: 2102652-01 Analyzed: 05/05/21 15:07 TPH Gasoline (C5-02) 8.18 5.2 mg/kg 10.4 ND 78 10-171 3 20 Stnrogate:4-Brontofluorohen_ene 1.40 1.30 107 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatilepi Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLKI) Analyzed: 05/05/21 13:17 Benzene ND 0.25 tng/kg Bromobenzene ND 0.25 Bromochloromethanc ND 0.25 Bromodichloromethane ND 0.25 Bromoform ND 0.25 " Bromomethane NI) 0.25 n-Butylbenzene ND 0.25 sec-Butylbenzene NI) 0.25 tort-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 Chlorobenzene NI) 0.25 C'hloroethane NI) 0.25 " Chloroform ND 0.2.5 " Chloromethane ND 0.25 2-Chlorotoluene NI) 0.25 4-Chlorotoluene ND 0.25 " Dibromochloromethane ND 0.25 " 1,2-Dibromo-3-ch1oropropane ND 0.25 1,2-Dibromoethane (EDB) ND 0.25 " Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0.25 1.3-Dichlorobenzene ND 0.25 " 1,4-Dichlorobenzene NI) 0.25 Dichloroditluoromethane ND 0.25 1.1-Dichloroethene NI) 0.25 1,2-Dichlorocthanc ND 0.25 1,1-Dichloroethene ND 0.25 cis-1,2-Dichloroethene ND 0.25 " trans-1.2-Dichloroethene ND 0.25 1,2-Dichloropropane ND 0.25 " 1,3-Dichloropropane ND 0.25 2.2-Dichloropropane NI) 0.25 " 1, 1 -Dichloropropene ND 0.25 cis-1,3-Dichloropropene NI) 0.25 trans-1,3-Dichloropropene ND 0.25 Ethylbenzene NI) 0.25 Ilexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 Isopropylbenzene NI) 0.25 Methylene chloride ND 0.25 Naphthalene ND 0.25 n-Propylbenzene ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Coinpounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS (B1E0101-BSI) Analyzed: 05/05/21 12:22 1,3-Dichlorobenzenc 2.17 0.25 mg/kg 1.99 109 76-138 1,4-Dichlorobenzene 2.14 0.25 1.99 108 72-132 Dichloroditluoromethane 1.31 0.25 1.99 66 10-155 1, 1 -Dichloroethane 2.33 0.25 1.99 117 63-139 1,2-Dichloroethane 2.06 0.25 1.99 104 64-126 1,1-Dichloroethene 2.77 0.25 1.99 139 52-167 _ cis-1,2-Dichloroethene 2.07 0.25 1.99 104 70-135 trans- I .2-Dichloroethene 2.43 0.25 1.99 122 67-147 1.2-Dichloropropane 2.05 0.25 1.99 103 68-131 1,3-Dichloropropane 2.04 0.25 1.99 103 64-128 2,2-Dichloropropane 2.31 0.25 1.99 116 63-154 1,1-Dichloropropene 2.22 0.25 1.99 112 68-138 cis-1,3-Dichloropropene 2.09 0.25 1.99 105 72-134 trans-1,3-Dichloropropene 2.26 0.25 1.99 114 69-132 Ethylbenzene 2.46 0.25 1.99 124 68-136 1lexachlorobutadiene 2.20 0.25 1.99 111 72-198 4-Isopropyl Toluene 2.39 0.25 1.99 120 74-150 Isopropylbenzene 2.41 0.25 1.99 121 71-149 Methylene chloride 2.57 0.25 1.99 129 51-127 Q�1 08 Naphthalene 1.99 0.25 1.99 100 57-158 n-Propylbenzene 2.27 0.25 1.99 114 70-143 Styrene 2.25 0.25 1.99 113 68-138 1, 1, 1,2-Tetrachloroethane 1.92 0.25 1.99 97 76-130 1,1,2,2-Tetrachloroethanc 2.09 0.25 1.99 105 60-136 Tetrachloroethene(PCE) 2.09 0.25 1.99 105 73-138 Toluene 2.18 0.25 1.99 110 72-128 1,2.3-Trichlorobenzene 1.74 0.25 1.99 88 61-166 1.2,4-Trichlorobenzene 1.85 0.25 1.99 93 71-158 - - 1.1 .1-Trichloroethane 2.24 0.25 1.99 113 71-135 1.1.2-Trichloroethane 2.07 0.25 1.99 104 64-132 Trichloroethene (TCE) 1.92 0.25 1.99 97 74-139 Trichlorofluoromethanc 1.74 0.25 1.99 87 30-156 1,2,3-Trichlorolxopane 2.01 0.25 1.99 101 67-123 12.4-Trimethylbenzene 2.52 0.25 1.99 127 68-134 1.3,5-Trimethyl benzene 2.37 0.25 1.99 119 71-140 "nyl chloride 2.46 0.25 1.99 124 43-144 Xylenes (total) 7.54 0.25 5.96 126 69-138 Surrogate: Dibrurnojlnoronrethune 0.0485 0.0497 98 74-122 Surrogate: Toluene-d8 0.0471 0.0497 95 65-128 Stn•rogate:4-BrumgJluorohen_ene 0,0467 0.0497 94 75-121 - The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925.3376 Page 27 of 37 ^-1 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSDI) Analyzed: 05/05/21 12:49 Styrene 2.26 0.25 mglkg 1.99 114 68-138 0.4 20 1,1,1,2-Tetrachloroethane 1.96 0.25 1.99 99 76-130 2 20 1,1,2,2- Tetrachloroethane 2.08 0.25 1.99 105 60-136 0.2 20 Tetrachloroethene (PCE) 2.07 0.25 1.99 104 73-138 1 20 Toluene 2.21 0.25 1.99 Ill 72-128 1 20 1,2,3-Trichlorobenzene 1.87 0.25 1.99 94 61-166 7 20 1,2.4-Trichlorobenzene 1.89 0.25 1.99 95 71-158 2 20 1, 1, 1 -Trichloroethane 2.17 0.25 1.99 109 71-135 3 20 1,1,2-Trichloroethane 2.16 0.25 1.99 108 64-132 4 20 Trichloroethene(TCE) 1.89 0.25 1.99 95 74-139 1 20 Trichlorotluoromethane 1.58 0.25 1.99 79 30-156 10 20 1,2,3-Trichlompropane 1.90 0.25 1.99 95 67-123 6 20 1.2.4-Trimethylbenzene 2.60 0.25 1.99 131 68-134 3 20 1,3,5-Trimethylbenzene 2.38 0.25 1.99 120 71-140 0.6 20 Vinyl chloride 2.27 0.25 1.99 114 43-144 8 20 Xylenes (total) 7.47 0.25 5.96 125 69-138 0.9 20 Surrogate: Uibivmu/luuromrthanc 0.0486 0.0497 98 74-122 Surrogate: Toluene-d8 0.0467 0.0497 94 65-128 Surrogate:4-Bromolluorohenreue, 0.0459 0.0497 92 75-121 Duplicate (B1E0101-DUPI) Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 Benzene ND 1.3 mg/kg ND 20 Bromobenzene ND 1.3 ND 20 Bromochloromethanc ND 1.3 ND 20 Bromodichloromethane ND 1.3 ND 20 Bromolorm ND 1.3 ND 20 Bromomethane ND 1.3 ND 20 n-Butylbenzene ND 1.3 ND 20 sec-Butylbenzene ND 1.3 ND 20 tert-Butvlbenzene NI) 1.3 NI) 20 Carbon tetrachloride NJ) 1.3 ND 20 Chlorobenzene NI) 1.3 ND 20 Chloroethane NI) 1.3 ND 20 Chloroform ND 1.3 ND 20 Chloromethane ND 1.3 ND 20 2-Chlorotoluene ND 1.3 ND 20 4-Chlorotoluene ND 1.3 ND 20 Dibromochloromethane ND 1.3 ND 20 1,2-Dibromo-3-chloropropanc ND 1.3 ND 20 1,2-Dibromoethane (EDB) ND 1.3 ND 20 Dibromotncthane ND 1.3 ND 20 1,2-Dichlorobenzene NI) 1.3 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 37 OEC Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatilei po Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 •� Matrix Spike (B1E0101-MS1) Source: 2102742-02 Analyzed: 05/05/21 20:08 Benzene 11.1 1.3 mg/kg 10.0 ND Ill 37-145 Bromobenzene 9.57 1.3 10.0 ND 96 29-147 Bromochloromcthane 9.29 1.3 10.0 ND 93 40-145 Bromodichloromethane 10.2 1.3 10.0 ND 102 39-153 Bromoform 9.14 1.3 10.0 ND 91 32-143 Bromomethane 12.1 1.3 10.0 ND 121 10-141 n-Butylbenzene 12.3 1.3 10.0 ND 123 10-162 sec-Butylbenzene 12.5 1.3 10.0 ND 125 14-168 tert-Butylbenzene 11.8 1.3 10.0 ND 118 21-159 Carbon tetrachloride 10.4 1.3 10.0 ND 104 28-148 Chlorobenzene 10.6 1.3 10.0 ND 106 32-148 Chloroethane 11.0 1.3 10.0 ND 110 11-166 Chloroform 10.3 1.3 10.0 ND 103 40-139 Chloromethane 9.86 1.3 10.0 ND 98 18-135 �2-Chlorotoluene 10.7 1.3 10.0 ND 107 25-151 4-Chlorotoluene 10.7 1.3 10.0 ND 106 22-150 Dibromochloromethane 9.53 1.3 10.0 ND 95 40-147 1,2-Dibromo-3-chloropropane 9.97 1.3 10.0 ND 100 25-158 1,2-Dibromoethane (EDB) 9.29 1.3 10.0 ND 93 38-147 Dibromomcthane 7.54 1.3 10.0 ND 75 39-150 1,2-Diehlorobenzenc 10.6 1.3 10.0 ND 106 24-154 1,3-Dichlorobenzenc 1().9 1.3 10.0 ND 108 21-153 14-Dichlorobenzene 10.6 1.3 10.0 ND 106 21-146 Dichloroditluoromcthanc 5.88 1.3 10.0 ND 59 10-149 I,1-Dichloroethane 11.2 1.3 10.0 ND 112 34-151 1.2-Dichloroethane 10.1 1.3 10.0 ND 100 40-137 1,1-Diehloroethene 11.8 1.3 10.0 ND 118 21-172 cis- 1.2-Diehloroethene 9.65 1.3 10.0 ND 96 38-147 - trans-l.2-Diehloroethene 11.3 1.3 10.0 ND 112 30-160 1,2-Dichloropropane 10.4 1.3 10.0 ND 104 39-146 1,3-Dichloropropane 10.2 1.3 10.0 ND 102 39-141 2,2-Dichloropropane 9.32 1.3 10 0 ND 93 26-149 1, 1 -Dichloropropene 10.7 1.3 10.0 ND 106 28-150 cis-1.3-Dichloropropene 9.97 1.3 I().() ND 100 34-149 trans- l,3-Di chloropropene 10.7 1.3 10.0 ND 107 3o-143 _ Iithylbenzene 11.5 1.3 10.0 ND 115 23-150 IlexachlorObnladiene 11.1 1.3 10.0 ND Ill 10-192 4-Isopropyl Toluene 11.7 1.3 10.0 ND 117 I1-165 Isopropylbenzene 11.2 1.3 10.0 ND 112 17-166 Methylene chloride 12.0 1.3 10.0 ND 120 28-135 Naphthalene 12.0 1.3 10.0 ND 120 10-174 u-Propylbenzene 11.3 1.3 10.0 ND 113 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Sample td Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, CA -FLAP Total Metals by ICP 601013 Total Antimony EPA 601013 Solid OEC. CA -FLAP 601013 Total Arsenic EPA 601013 Solid OEC, CA -FLAP 6010B Total Barium EPA 6010B Solid OEC, CA -FLAP 601013 Total Beryllium EPA 6010B Solid OEC. CA -FLAP 6010B Total Cadmium EPA 601013 Solid OEC, CA -FLAP 601013 Total Chromium EPA 601013 Solid OEC, CA-ELAP 601013 Total Cobalt EPA 601OB Solid OEC. CA-ELAP 601013 Total Copper EPA 601013 Solid OEC, CA-ELAP 601013 Total Lead EPA 601013 Solid OEC. CA-ELAP 6010B Total Molybdenum EPA 6010B Solid OEC. CA-ELAP 6010B Total Nickel EPA 6010B Solid OEC. CA -FLAP 601013 Total Selenium EPA 601013 Solid OEC, CA-ELAP 601013 Total Silver EPA 601013 Solid OEC. CA-ELAP 601013 Total Thallium EPA 6010B Solid OEC, CA-ELAP 601013 Total Vanadium EPA 6010B Solid OF.C. CA -FLAP 601013 Total Zinc EPA 601013 Solid OEC, CA -FLAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260I3 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline Solid OEC. CA-ELAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 37 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0511.D Operator BNT Acquired 5 May 2021 12:06 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-01@ Misc Info : 1@B1E0095 GRO SO Vial Number: 11 Response_ 85000 80000 75000 70000 65000 60000 55000 50000 45000. 40000 35000 30000 20000- 15000 10000 5000 GOME0511.D\FID1A Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 - File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0513.D Operator BNT Acquired 5 May 2021 12:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-03@ Misc Info : 1@B1E0095 GRO SO Vial Number: 13 Response_ 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 25000 20000 15000 10000 5000 Time 0.00 1.00 l 2.00 3.00 4.00 5.00 6.00 GOME0513.D\FID1A 00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0515.D Operator BNT Acquired 5 May 2021 1:49 pm using AcgMethod GASBTEXE.M Instrument GC7 - Sample Name: 2102742-05@ Misc Info : 1@B1E0095 GRO SO Vial Number: 15 Response_ 85000, 80000 65000 60000 55000 50000 45000 40000 35000 30000 15000 10000 5000 T 0.00 1.00 GOME0515.D\FID1A 1 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 1 0.00 11.00 12.00 13.00 14.00 U r1 (D x a H 0 -P a) tr U C] b� d' •ri M U) LO �3 O W x X a O N co O tlO / M O O N I— W Ln N -i O W Ln 61 CJ O O N / O � � I N N N >� O Ln G < (N -A I` � IUN / co Ln C7 0 �R: I r i (ID x124Ln Nr-IM .............. (D �4 4J F a) �4-0 aaizw OJ S4 a) H z + a) S4 �5 4 i 0. U r-i .-1 (2) O" co E U) (o "i Q U G M -ri •ri 440<i-iW I,- I-- n P- P- n 0 O O 0 O 0 O 0 O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N + + + + + + 0 0 0 0 0 0 0 0 0 N N N y N N O O 0 0 0 O 0 O 0 0 2 0 M N O O O O O O O O O N 0 a0 r to Lf) It cM N U O x a H O a) iT U is Q � 00 U) M Ln O O Ln N / O r O O N W Ln O W LO r (2) O N 'T / O O r1 N I N N >H >1Lr)a /U) C7O .. '� Ln H C)00 p O Nr-IM c r0 O A u4 Z44 a M•r-i s4—i —i a) it U) U) rd -H Y+ U r. (0 _4 •H + + + + + + o 0 0 0 0 0 0 0 0 0 w 0) 0 N N O O O O O O O O O 0 0• O It M N O O O O O O O O O Vl m c0 I- CO O co N tY 0 ,o co 0 0 vi 0 f0 Lf) 0 0 N O O O �kcqli HO 0 t O M M O fD M M N M Hro r ri i O N [F N d NO 4F r O N N O ab N E H CO m No e C t (� A O 9 xC s 13 how E E E m� OGi a U E °t ° 1.0 0 N x ePI1OS PGNOSIO IGiOl m ci m /41AIV"00 o iv R G O � Z80B! V4808 ,q - 80d / isad /411 ei1uBl of � U x 30LZ8 - s30AS WS408OW09•dHl / L y � Z = n GPUInScc y as ! GplueAo GAaaeGa F- E W d C d wN y 191-1 11nd 808Z8 +1 Z u N G L ❑ slsieW - ZZ Gall � J h b 0 m m c m Of V > > 0 n yi�p1 H = a co Er a m C N ¢ m y C (n 00 00 CIO U � " E E gv7 — a � � ❑ F ~ d t c z:•n U 00 3 Z ❑ } p 3 m R O 0 G G Q❑ Z U m L' x b(❑ a . 3 W 0 d 0. c .r c= E -E R m O . a v o m O y Q ee t �}? Uo� tl > c ❑❑ m m m m m a V -0 C Q O E• Q m �"" (� t� �� L �C H 0 z 7 E. L C0 C C C N a L ix 6 z O H U z J Q v W IL !N m C. -) a s N c N E IL d U11L E O a� C O n� 2 N N N d X in v con (1) ton ton in c c c c c Y Y >Y >Y >Y a0 co Co Co Co CDN cm N O) l N O) N O N O d O ID O) ID m N O7 N OJ O _ LL LL LL LL LL LL LL LL LL .Q > >> i O( O � O I O � O a0+ (7 J 0 J U' J O O O O O O O O O O O U a N V N N V N N oU cQ 20 Q P mUn Nm o 0 0 0 0 0 0 0 0 a Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102508 Pacific Petroleum California P. O. Box 2646 Report Date: May 03, 2021 16:36 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 23, 2021 13:40 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@occusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 1 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bin 2094-A 2102508-01 Solid Solid 04/23/2021 11:00 04/23/2021 13:40 Bin 2094-B 2102508-02 Solid Solid 04/23/2021 11:05 04/23/2021 13:40 Bin 2094-C 2102508-03 Solid Solid 04/23/2021 11:10 04/23/2021 13:40 Bin 20340-A 2102508-04 Solid Solid 04/23/2021 11:15 04/23/2021 13:40 Bin 20340-B 2102508-05 Solid Solid 04/23/2021 11:20 04/23/2021 13:40 Bin 20340-C 2102508-06 Solid Solid 04/23/2021 11:25 04/23/2021 13:40 Bin 20158-A 2102508-07 Solid Solid 04/23/2021 11:30 04/23/2021 13:40 Bin 20158-B 2102508-08 Solid Solid 04/23/2021 11:35 04/23/2021 13:40 Bin 20158-C 2102508-09 Solid Solid 04/23/2021 11:40 04/23/2021 13:40 Bin 2088-A 2102508-10 Solid Solid 04/23/2021 11:45 04/23/2021 13:40 Bin 2088-B 2102508-11 Solid Solid 04/23/2021 11:50 04/23/2021 13:40 Bin 2088-C 2102508-12 Solid Solid 04/23/2021 11:55 04/23/2021 13:40 Bin 20376-A 2102508-13 Solid Solid 04/23/2021 12:00 04/23/2021 13:40 Bin 20376-B 2102508-14 Solid Solid 04/23/2021 12:05 04/23/2021 13:40 Bin 20376-C 2102508-15 Solid Solid 04/23/2021 12:10 04/23/2021 13:40 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample :. t Analysis Batch ID Preparation Date/Time *** DEFAULT GENERAL METHOD *** Asbestos Bulk PLM-(nun-soil& Asphalt)(sub) OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List BID0766 04/27/2021 07:10 STLC Metals by ICP 6010B STLC B I D0916 04/30/202 J 10:33 STLC Metals Extraction STLC Metals Extraction BID0838 04/28/2021 12:44 TCLP Metals by ICP 6010B TCLP B 1 D0919 04/302021 10:49 - - TCLP Metals Extraction TCLP Metals Extraction BID0839 04/29/2021 12:49 Total Metals by CVAA Mercury Total EPA 7471 A B ID0711 04/26:2021 09:00 Total Metals by ICP 6010B Total B 1 D0734 04/26/2021 07:37 Volatile Organic Compounds by GC/MS 8260B Full List B1D0650 04/23/2021 12:11 Volatile Organic TPH by GC/FlD 8015 TPI 1-Gasol ine B 1 D0692 04/23/2021 14:16 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by : Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.095 0.094 mg!kg 1 B 1 D0711 04/26/21 14:53 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B 1 D0734 04/26/21 13:51 EPA 6010B Arsenic 7.4 1.9 Barium 690 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 64 0.48 N-02 Cobalt 14 0.49 Copper 260 0.97 " " " " " N-02 Lead 2400 0.48 N-01, N-03 Molybdenum 2.0 0.48 Nickel 94 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 31 1.9 Zinc 1300 1.9 STLC Metals by ICP Chromium 0.28 0.10 mg/I. 2 B I D0916 05/03/21 12:58 STI.C/EPA 6010B Copper 1.6 0.10 TCLP Metals by ICP Lead 2.0 0.050 m,•/L I B 1 D0919 05/03/21 14:09 EPA 1311 TPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 WWW.vecusa.eom FAX: 805 925-3376 Page 4 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 I1:00 ' Matrix: Solid Sampled by : Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-02) ND 4.9 mg kg 1 BID0692 04/23/21 14:32 EPA 901.5M R-07 Surrogate: 4-BromnJluorohenzene 94 X, (39 - 157 ) Semi -Volatile Organic TPH by GC/FID - TPH Diesel (C13-C22) ND 10 mg/kg 1 BID0766 04/27/21 15:24 EPA 8015M TPH Motor Oil (C23-C40) 97 50 Surrogate: o-Terphenyl 84 % (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.051 mg/kg 1 BID0650 04/23/21 17:17 EPA8200B Bromobenzene ND 0.051 Bromochloromethane ND 0.051 Bromodichloromethane ND 0.051 .� Bromoform ND 0.051 Bromomethane ND 0.051 n-Butylbenzene ND 0.051 sec-Butylbenzene ND 0.051 tert-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobenzenc ND 0.051 Chloroethane ND 0.051 Chloroform ND 0.051 C'hloroinethane ND 0.051 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND 0.051 Dibromochloromethane ND 0.051 " 1,2-Dibroino-3-chloropropane ND 0.051 " 1,2-Dibroinoethane (EDB) ND 0.051 Dibromomethane ND 0.051 1,2-Dichlorobenzene ND 0.051 1.3-Dichlorobenzene ND 0.051 14-Dichlorobenzene ND 0.051 Dichloroditluoromcthane ND 0.051 1. 1 -Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 1,1-Dichloroethene ND 0.051 cis- 1,2-Dichloroethene ND 0.051 " trans-1,2-Dichloroethene ND 0.051 1,2-Dichloropropane ND 0.051 1,3-Dichloropropane ND 0.051 2,2-Dichloropropane ND 0.0.51 1,1-Dichloropropene ND 0.051 cis-l3-Dichloropropene ND 0.051 ' trans-1,3-Dichloropropene ND 0.051 Ethylbenzenc ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 0.0.51 mg/kg 1 B1D0650 04/23/2117:17 EPA8260B 4-Isopropyl Toluene ND 0.051 Isopropylbenzene ND 0.051 Methylene chloride ND 0.051 Naphthalene ND 0.051 " n-Propylbenzene ND 0.051 Styrene ND 0.051 L1,1,2-Tetrachloroethane ND 0.051 1.1.2,2-Tetrachloroethane ND 0.051 Tetrachloroctlienc WCE) ND 0.051 Toluene ND 0.051 1,2,3-Trichlorobcnzene ND 0.051 1,2,4-Trichlorobenzene ND 0.051 1, 1, 1 -Trichloroethane ND 0.051 1.1,2-Trichloroethane ND 0.051 Trichloroethene (TCE) ND 0.051 Trichlorofluoromethane ND 0.051 " 1-23-Trichloropropane ND 0,051 1,2,4-Trimethylbenzene ND 0.051 1,3,5-Trimethylbenzene ND 0.051 Vinyl chloride ND 0.051 Xylcnes (total) ND 0.051 " Surrogate: Dibromglluoromethanc 981,111, ( 74- 122) Surrogate: Toluene-dS 95 % (65- 12S ) Surrogate: 4-Bromolluoroben:cne S9 "/n ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B1D0711 04/26/21 15:02 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1D0734 04/26/21 13:54 EPA 6010B Arsenic 7.6 1.9 Barium 220 0.97 Beryllium ND 0.49 ^ Cadmium ND 0.24 Chromium 100 0.49 N-02, N-03 Cobalt 15 0.48 Copper 61 0.97 Lead 320 0.48 N-02, N-03 Molybdenum 1.6 0.48 Nickel 130 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 38 1.9 "Line 410 1.9 STLC Metals by ICP Chromium 0.29 0.10 mg/L 2 BID0916 05/03/21 13:00 STLC/EPA601013 Lead 20 0.10 " " " " " N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BID0919 05/03/21 14:26 EPA 1311/EPA6010B Lead 0.31 0.050 " " " " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 94 WAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 2094-B Sampled: 04/23/21 11.05 Matrix: Solid Sampled by: Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TP11 Gasoline (C5-('12) ND 4.8 mg/kg 1 BID0692 04/23/21 14:58 EPA 8015M R-07 Surrogate: 4-Bromo/luorobenzene 99 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 16 10 nig/kg 1 BID0766 04/27/21 15:24 EPA8015M D-06 TPH Motor Oil (C23-C40) 150 50 1. 11 11 11.. Surrogate: o-Teipheml 80 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.049 mg/kg 1 BID0650 04/23/21 17:45 EPA 9260B Bromobenzene ND 0.049 " Bromochloromethane ND 0.049 " Bromodichloromethane ND 0.049 " Bromofonn ND 0.049 Bromomethane ND 0.049 n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 Carbon tetrachloride ND 0.049 Chlorobcnzcnc ND 0.049 Chloroethane ND 0,049 Chloroform ND 0.049 Chloromethane ND 0.049 -- 2-Chlorotoluene ND 0.049 4-C'hlorotoluene ND 0.049 Dibromochloromethane ND 0.049 - 1,2-Dibromo-3-chloropropane ND 0.049 1,2-Dibromoethane (EDB) ND 0.049 " Dibromomethane ND 0.049 " 1,2-Dichlorobenzene ND 0.049 1.3-Dichlorobenzene ND 0.049 1,44Dichlorobenzenc ND 0.049 Dichlorodilluoromethane ND 0.049 " - 1,1-Dichloroethane ND 0.049 " 1,2-Dichloroethane ND 0.049 " I,1-Dichloroethene ND 0.049 cis-1,2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 1,2-Dichloropropane ND 0.049 1,3-1)ichhmopropane ND 0.049 2,24Dichloropropane ND 0.049 I,I-Dichloropropene ND 0.049 " cis-1,3-Dichloropropene ND 0.049 ' trans-1,3-Dichloropropene ND 0.049 Ethylbenzene ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 94 6-7�N Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical i Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.049 mglkg 1 131D0650 04/23/21 17:45 EPA 8260B 4-Isopropyl Toluene ND 0.049 lsopropylbenzene ND 0.049 Methylene chloride ND 0.049 " Naphthalene ND 0.049 n-Propylbenzene ND 0.049 Styrene ND 0.049 .r 1, 1, 1,2-Tetrachloroethane ND 0.049 I_I.2,2-Tetrachloroethane ND 0.049 Tctrachlorocthcnc (PCE) ND 0.049 Toluene ND 0.049 1,2,3-Trielhlorobenzene ND 0.049 1,2,4-Trichlorobenzene ND 0.049 1,1,1-Trichloroethane ND 0.049 — • 1,1,2-Trichloroethane ND 0.049 Trichloroethene (WE) ND 0.049 Trichlorofluoromethane ND 0.049 " 1,2.3-Trichi oropropane ND 0.049 " 1,2.4-Triniethylbenzenc ND 0.049 1,3.5-Triniethylbenzene ND 0.049 Vinyl chloride ND 0.049 ^ Xylencs (total) ND 0.049 Surrogate: Dihrarnglluoreuncthane 95 % ( 74 - 12 2 ) Surrogate: Toluene-d8 96'/ (65 - 128) .-, Surrogate: 4-Bronui luoroben_ene 90 % (75 - 121) ^1 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID: 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mcrcury 0.17 0.098 mg/kg I B 1 D0711 04/26/21 15:04 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:05 EPA 6010B . Arsenic 7.7 2.0 Barium 280 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 52 0.50 N-02 Cobalt 10 0.50 Copper 79 H) Lead 270 0.50 " " " " " N_02, N-03 Molybdenum 1.1 0.50 Nickel 69 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 34 2.0 Zinc 370 2.0 STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 B I D0916 05/03/21 13:03 STLC/EPA 6010B - Lead 22 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.11 0.050 mg/I. 1 B 1 D0919 05/03/21 14:29 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID: 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) Smrogate. 4-Bromgfluoroben_ene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate. o-Tetphenyl ND 4.8 mg/kg 1 B1 D0692 04/23/21 15:24 FTA 8015M R-07 93% (39-157) ND 10 mg/kg 1 BID0766 04/27/21 15:47 EPA 8015M 220 50 1. 11 11 11" 79% (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 94 -(-- �a P�� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16.36 Analytical Report foi- Sarnples Sample ID: Bin 2094-C Sampled: 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.049 mglkg I BID0650 04/23/21 18:12 EPA 8260B Bromobenzene ND 0.049 Bromochloromethane ND 0.049 Bromodichloromethane ND 0.049 Bromofonn ND 0.049 Bromomethane ND 0.049 n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 Carbon tetrachloride ND 0.049 Chlorobenzene ND 0.049 " -� Chloroethane ND 0.049 Chloroform ND 0.049 Chloromethane ND 0.049 - 2-Chlorotoluene ND 0.049 4-Chlorotoluene ND 0.049 Dibromochloromethane ND 0.049 1,2-Dibromo-3-chloropropane ND 0.049 1,2-Dibromocthane (ED13) ND 0.049 Dibromomethane ND 0.049 1,2-Dichloroben7ene ND 0.049 1.3-Dichlorobenzenc ND 0.049 1,4-Dichlorobenzene ND 0.049 Dichloroditluoromcthane ND 0.049 - 1, 1 -Dichloroethane ND 0.049 1,2-Dichloroethene ND 0.049 I,I-Dichloroethene ND 0.049 cis-1,2-Dichloroethene ND 0.049 " trans-1,2-Dichloroethene ND 0.049 1,2-Dichloropropane ND 0.049 1,3-Dichloropropane ND 0.049 22-Dichloropropane ND 0.049 1, 1 -Dichloropropene ND 0.049 cis- 1,3 -Dichloropropene ND 0.049 ' trans-1,3-Dichloropropenc ND 0.049 Ethylbenzenc ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www,oecusa.com FAX: 805 925-3376 Page 14 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 0.049 mg/kg 1 B1 D0650 04/23/21 18:12 EPA 8260B 4-Isopropyl Toluene ND 0_049 lsopropylbenzene ND 0.049 Methylene chloride ND 0.049 —. Naphthalene ND 0.049 n-Propylbenzene ND 0.049 Styrene ND 0.049 1.1,1,2-Tetrachloroethane r ND 0.049 1,L2,2-Tetrachloroethane ND 0.049 Tetrachlorocthene (PCE) ND 0.049 Toluene ND 0.049 1,2,3-Trichlorobenzene ND 0.049 1.2,4-Trichlorobenzene ND 0.049 1,1,1-Triehloroetliane ND 0.049 • 1,1,2-Trichloroethane ND 0,049 Trichloroethene (TCE) ND 0.049 Trichlorofluoromethane ND 0.049 1,2,3-Trichloropropane ND 0.049 1,2.4-Trimethylbenzene ND 0.049 1,3,5-Trimethylbenzene ND 0.049 Vinyl chloride ND 0.049 Xylencs (total) ND 0.049 Surrogate: Dibronuilluorome thane 97 % ( 74 - 122 ) Surrogate. Toluene-dS 96 % (65 - 128 ) - Surrogate: 4-BromoJluoroben_ene 92 %, ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercurc 0.13 0.087 mg,kg 1 BID0711 04/26/21 15:06 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I D0734 04/26/21 14:07 EPA 6010B —, Arsenic 7.3 2.0 Barium 230 0.98 Beryllium ND 0.49 _-. Cadmium ND 0.25 Chromium 58 0.49 N-02 Cobalt 12 0.49 Copper 63 0.98 Lead 390 0.49 N-02, N-03 Molebdenum 2.1 0.49 Nickel 69 0.49 " Selenium ND 2.0 Silver ND 0.49 `l Thallium ND 0.98 Vanadium 35 2.0 Zinc 530 2.0 STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 BI D0916 05/03/21 13:05 STLC/EPA 6010B — Lead 14 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/l. 1 Bl D0919 05/03/21 14:31 EPA 131 ] ,EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) Surrogate: 4-Brom nJluorohen_ene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Sm•rogate. o-Tetphenrl ND 5.2 ing/kg 1 BID0692 04/23/21 15:50 EPA 8015M R-07 99, (39-157) " 11 ND 10 nig/kg I B1D0766 04/27/2115:47 EPA8015M 170 50 11 11 11" 1. S6'14, (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 17 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report t Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by : Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.051 mg/kg 1 B 1 D0650 04/23/21 18:40 FPA 8260B Bromobenzene ND 0.051 Bromochloromethane ND 0.051 Bromodichloromethane ND 0.051 Bromoform ND 0.051 Bromomethane ND 0.051 " n-Butylbenzene ND 0.051 sec-Butylbenzene r ND 0.051 " tert-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobenzene ND 0.051 Chlorocthane ND 0.051 Chloroform ND 0.051 Chloromethane ND 0.051 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND 0.051 Dibromochloroniethane ND 0.051 . 1,2-Dibromo-3-chloropropane ND 0.051 1,2-Dibromoethane (EDB) ND 0.051 Dibromomethane ND 0.051 1,2-Dichlorobenzene ND 0.051 1,3-Dichlorobenzene ND 0.051 1,4-Dichlorobenzene ND 0.051 " Dichlorodifhtoromethane ND 0.051 1, 1 -Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 1, 1 -Dichloroethene ND 0.051 _ cis-1,2-Dichloroethene ND 0.051 trans-1,2-Dichloroethene ND 0.051 1.2-Dichloropropane ND 0.051 1,3-Dichloropropane ND 0.051 " 2,2-Dichloropropane ND 0.051 1.1-Dichloropropane ND 0.051 cis-1.3-Dichloropropenc ND 0.051 trans-1,3-Dichloropropcnc ND 0.051 Ethylbcnzcne ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Saniples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by : Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.051 mg/kg 1 BID0650 04/23/21 18:40 EPA8260B 4-Isopropyl Toluene ND 0.051 lsopropylbenzene ND 0.051 " Methylene chloride ND 0.051 " Naphthalene ND 0.051 " n-Propylbenzene ND 0.051 Styrene ND 0.051 " 1,1.1,2-Tetrachloroethane ND 0.051 1,1,22-Tetrachloroethane ND 0.051 Tetrachlorocthcne (PCE) ND 0.051 Toluene ND 0.051 I_2,3-Trichlorobenzene ND 0.051 1,2.4-Trichlorobenzene ND 0.051 1, 1, 1 -Trichloroethane ND 0.051 " 1,12-Trichloroethane ND 0.051 Trichloroethene (TCE) ND 0.051 Trichlorofluoromethane ND 0.051 • 1.2,3-Trichloropropane ND 0.051 1,2,4-Trimethylbenzene ND 0.051 I.3.5-Trimethylbenzene ND 0.051 Vinyl chloride ND 0.051 Xylenes (total) ND 0.051 Surrogate: Dibromolluoromethune 98 % ( 74 - 122 ) Surrogate: Tohtenc-dS 97 % ( 65 - 128) Surrogate: 4-Bronto/htoroben:ene 92 'N (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by : Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Di 0.095 0.091 mg/kg 1 B 1 D0711 04/26/21 15:08 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:10 EPA 6010B Arsenic 10 2.0 " Barium 240 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 50 0.49 " N-02 Cobalt 11 0.49 Copper 54 0.98 Lead 800 0.49 " " " " " N-02, N-03 6Tolvbdenum 0.77 0.49 " Nickel 79 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 37 2.0 "Zinc 350 2.0 STLC Metals by ICP Chromium 0.29 0.10 mg/1, 2 B1D0916 05/03/2113:08 STLC/EPA6010B . Lead 120 0.I0 " " " " " N-07 TCLP Metals by ICP Lead 0.23 0.050 mg{L 1 BID0919 0510312114:34 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID: 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C 5-C12) ND 5.0 mglkg 1 B1 D0692 04/23/21 16:16 EPA 8015M R-07 Surrogate. 4-Brotnq luoroben_ene 99 Y. (39 -157) " 11" Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 37 10 mg/kg 1 BID0766 04/27/21 16:09 EPA 8015M D-06 TPH Motor Oil (C23-C40) 280 50 Surrogate: o-Tcrphenrl 86 (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 94 �i M�� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg/kg 1 BI D0650 04/23/21 19:07 EPA 8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromofurm ND 0.047 " Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 " Chlorobenzene ND 0.047 Chlorocthane ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotohiene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 " 1,2-Dibromoethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 " 1,4-Dichloroben7ene ND 0.047 Dichlorodifluoromcthanc ND 0.047 1, 1 -Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 13-Dichloroethene ND 0.047 cis-1,2-Dichloroethene ND 0.047 " Hans-1,2-Dichloroethene N'D 0.047 " 1,2-Dichloropropane ND 0.047 13-Dichloropropane ND 0.047 " 2.2-Dichloropropene ND 0.047 I.1-Dichloropropene ND 0.047 cis-1.3-Dichloropropene ND 0.047 trans-1,3-Dichloropropene ND 0.047 Etliylbcnzcne ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 94 --r Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 0.047 mg/kg 4-Isopropyl Toluene ND 0.047 lsopropylbenzene ND 0.047 " Methylene chloride ND 0.047 " Naphthalene ND 0.047 " n-Propylbenzene ND 0.047 " Styrene ND 0.047 1,1,1,2-Tetrachloroethane ND 0.047 " 1,1,21-Tetrachloroethane ND 0.047 " Tetrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzenc ND 0.047 " 1,2,4-Trichloroben7.ene ND 0.047 " 1,1,1-Trichloroethane ND 0.047 " 1,1,2-Trichloroethane ND 0.047 " Trichloroethene (TCE) ND 0.047 " Trichlorolluoromethane ND 0.047 " 1,2,3-Tricliloropropane ND 0.047 1,24-Trimethylbenzene ND 0.047 " 13.5-Trimethylbenzene ND 0.047 " Vinyl chloride ND 0.047 " Xylenes (total) ND 0.047 " Surrogate: Difironwlluurwnetlrunc 98 % (74 - 122) Surrogate: Toluene-dfi 96 % (6 i - 128 ) Surrogate: 4-Branru/luorohen_ene 91 1% (75 - 121 ) 1 B 1 D0650 04/23/21 19:07 EPA 9260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 B 1 D0711 04/26/21 15:10 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 D0734 04/26/21 14:13 EPA 601 OB Arsenic 11 2.0 Barium 340 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 50 0.49 N-02 Cobalt 14 0.49 Copper 230 0.99 Lead 1200 0.49 " " " " " N-Ol N-03 Mol bdenum 1.7 0.49 Nickel 73 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 32 2.0 Zinc 1000 2.0 STLC Metals by ICP Chromium 0.32 0.10 nig/L 2 BID0910 05/03i2113:11 STLC/EPA6010B TCLP Metals by ICP Lead 0.84 0.050 mg/L 1 Bl D0919 05/03/1-1 14:36 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by : Lab ID: 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GOOD TPIIGasoline (C5-C12) ND 5.0 mglkg 1 BID0692 04/23/21 16:42 EPA8015M R-07 Surrogate: 4-Bromo/luorobencene 96 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 29 10 mg/kg 1 BID0766 04/27/21 16:09 EPA 8015M D-06 TPII Motor Oil (('23-C40) 150 50 11 11 11" 11 Surrogate: o-Teiphenrl 83 '%, (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mglkg l B1D0650 04/23/2119:35 EPA8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobenzenc ND OJ60 Chloroethane ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 4-Chlorotoluene ND 0.050 Dibromochlormnethane ND 0.050 1,2-Dibromo-3-chloropropane ND 0.050 1,2-Dibrontoethane (EDB) ND 0.050 DibrOmOmethane ND 0.050 1.2-Dichlorobenzene ND 0.050 1.3-Dichlorobenzenc ND 0.050 1,4-Dichlorobenzene ND 0.050 Dichlorodifluoromethane ND 0.050 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 1, 1 -Dichloroethene ND 0.050 " cis-1,2-Dichloroethene ND 0.050 " trans-1,2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 2.2-Dichloropropane ND 0.050 1,1-Dichloropropene ND 0.050 cis- I3-Dichloropropene ND 0.050 trans-1,3-Dichloropropenc ND 0.050 Ethylbcnzene ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 26 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by : Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 0.050 mg/kg 1 BID0650 04/23/2119:35 EPA8260B 4-Isopropyl Toluene ND 0.050 Isopropylbeuzene ND 0.050 Methylene chloride ND 0.050 —. Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1, 1, 1,2-Tetrachloroethane ND 0.050 1.1,2,2-Tetrachloroethane ND 0.050 Tetrachlorocthane (PCE) ND 0.050 Toluene ND 0.050 ' 1,2,3-Trichlorobenzcne ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 - 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorofluoromethane ND 0.050 _ 1,2.3-Trichloropropane ND 0.050 " 1,2,4-Trimethylbenzene ND 0.050 " 1,3,5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 f Xylencs (total) ND 0.050 Surrogate: Dihrom0fluorwnethmte 98IN ( 74- 122) Surrogate: Toluene-d8 95 % (65 - 128) ' Surrogate: 4-Bronu luoruhen_ene 90 f6 ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by : Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.11 0.092 mg/kg I B 1 D0711 04/26/21 15:12 EPA 7471 A Total Metals by ICP :Antimony 5.9 2.5 mg./kg 1 B1D0734 04/26/2114:16 EPA 6010B - Arsenic 8.5 2.0 Barium 260 0.98 Beryllium ND 0.49 . Cadmium ND 0.25 Chromium 65 0.49 N-02 Cobalt 11 0.49 Copper 77 0.98 Lead 530 0.49 ' " N-02 N-03 Molvbdenum 1.2 0.49 Nickel 91 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 34 2.0 Zinc 780 2.0 STLC Metals by ICP Chromium 0.59 0.10 mg/L 2 B 1 D0916 05/03/21 13:21 STLC/EPA 6010B - Lead 17 0.10 N-07 TCLP Metals by ICP Lead 0.12 0.050 mg/L 1 BID0919 05/03/21 14:39 EPA 1311/EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C 5-C12) ND 5.1 mg/kg 1 BID0692 04/23/21 17:08 EPA 9015M R-07 Surrogate: 4-Bromofluoroben_ene 98 `%h (39 - 1i7 ) Semi -Volatile Organic TPH by GC/FID _ TPH Diesel (C13-C22) 38 10 mg/kg 1 BID0766 04/27/21 16:32 EPA 8015M TPH Motor Oil (C23-C40) 150 50 Surrogate: o-kiphenYl 86 % (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 - Matrix: Solid Sampled by : Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GONIS R-07 Benzene ND 0.045 mg, kg 1 Bl D0650 04/23/21 20:02 EPA 8260B ' Bromobenzene ND 0.045 Bromochloromethane ND 0.045 " Bronrodichloromethane ND 0.045 " Bromofonn ND 0.045 " Bromomethane ND 0.045 " n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobcnzenc ND 0.045 ^ Chloroethane ND 0.045 Chlorofirrm ND 0.045 " C'hloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotohtene ND 0.045 Dibromochlorontethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 1,2-Dibromoethanc (EDB) ND 0.045 " Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobcnzcnc ND 0.045 1,4-Dichlorobcnzcnc ND 0.045 Dichloroditluoromcthanc ND 0.045 1. 1 -Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 1,1-Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 " trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1,3-Dichloropropane ND 0.045 2,2-Dichloropropane ND 0.045 1,1-Dichloropropene ND 0.045 cis-1,3-Dichloropropene ND 0.045 ' trans-1,3-Dichloropropene ND 0.045 Ethylbcnzenc ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Saniples Sample ID : Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 0.045 mgtkg 1 BID0650 04/23/21 20:02 F.PA 8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 „ . Naphthalene ND 0.045 n-Propylbenzene ND (1.045 Styrene ND 0.045 1. 1, 1.2-Tetrachloroethane ND 0.045 I.1.2,2-Tetrachloroethane ND 0.045 Tetrachlorocthcne IPCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1,1,1-Trichloroethane ND 0.045 - 1,1,2-Trichloroethane ND Q045 " Trichloroethene (TCE) ND 0.045 " Trichlorolluoromethane ND 0.045 1.2,3-Trichloropropane ND 0.045 12,4-Trimethvlbenzene ND 0.045 " 1,3,5-Trimethylbenzene ND 0.04.5 Vinyl chloride ND 0.045 Xylcncs (total) ND 0.045 Surrogate: Uibromo/luoromethone 96 IN (74 - 122 ) Surrogate: Toluene-d8 97 % (65 - 128 ) Surrogute: 4-Bromofl uuohcn:ene 93 % ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 31 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA MercurN 0.12 0.090 mg/kg 1 B 1 D0711 04/26/21 15:14 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:19 EPA 601OB Arsenic 6.5 2.0 Barium 270 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 86 0.49 N-02 Cobalt 25 0.49 Copper 60 0.99 Lead 190 0.49 " " " " " N-02 N-03 Molybdenum 1.0 0.49 Nickel 170 0.49 Selenium ND 2.0 Silvcr ND 0.49 Thallium ND 0.99 Vanadium 35 2.0 Zinc 380 2.0 STLC Metals by ICP Chromium 0.34 0.10 mg/L 2 Bl D0916 05/03/21 13:23 STLC/EPA 601 OB Lead 13 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.29 0.050 mg/l. 1 B 1 D0919 05/03/21 14:41 EPA 131 UEPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mg/kg 1 BID0692 04/23/21 17:34 EPA 8015M R-07 Surrogate: 4-Bronto/luorohencene 89 % (39 - 157) " Semi -Volatile Organic TPH by GOOD TPH Diesel (C13-C22) 93 40 mg/kg 4 BID0766 04/28/21 15:31 EPA 8015M D-06 TPH Motor Oil (C23-C40) 320 200 1. 11 11" 1. Surrogate: o-Tcuyhen.vl 84 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report i Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 77:Notes] Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.047 mgIg 1 B1D0650 04/23/2120:30 F.PA8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromotonn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Clilorobenzcnc ND 0.047 " Chloroethanc ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-C'hlorotoluene ND 0.047 Dibromochloromethane ND 0.047 " 1,2-Dibronio-3-chloropropane ND 0.047 1,2-Dibromoethane (F,DB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobcnzene ND 0.047 1,4-Dichlorobcnzene ND 0.047 Dichlorodifluoromcthane ND 0.047 1.1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 cis-1.2-Dichloroethene ND 0.047 trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0,047 2,2-Iichloropropane ND 0.047 1, 1 -Dichloropropene ND 0.047 cis- 1.3-Dichloropropene ND 0.047 trans-1,3-Dichloropropenc ND 0.047 F.thylbenzene ND 0.047 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 wvvw.oecusa.com FAX: (805) 925-3376 Page 34 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples R Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7 Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.047 mg/kg 1 Bl D0650 04/23/21 20:30 EPA 8260B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 " Methylene chloride ND 0.047 Naphthalene ND 0.047 " n-Propylbenzene ND 0.047 Styrene ND 0.047 1.1,12-Tetrachloroethane ND 0.047 1,1,2.2-Tetrachloroethane ND 0.047 Tetrachlorocthcne (PCE) ND 0.047 TOlrlenC ND 0,047 1,2,3-Trichlorobcnzene ND 0.047 1,2,4-Trichlorobenzene ND 0.047 " 1, 1, 1 -Trichloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorotluoromethane ND 0.047 1,2,3-Trichloropropane ND 0.047 1,2,4-Trimethylbenzene ND 0.047 1,3,5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 Xylenes (total) ND 0.047 Surrogate: Dibronwfluoromethaue 95 % ( 74 - 122) Surrogate: Toluene-elS 96 "/„ (65 - 128) Surrogate- 4-Bromolluoroben_ene 87 `io t 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mgtkg 1 B 1 D0711 04/26/21 15:16 EPA 7471 A Total Metals by ICP Antimonv 38 2.5 mg/kg I B 1 D0734 04/26/21 14:22 EPA 00I OB Arsenic 13 2.0 Barium 610 0.99 Beryllium ND 0.49 " Cadmium ND 0.25 Chromium 63 0.49 Cobalt 19 0.49 Copper 78 0.99 Lead 8000 49 100 04/26/2114:50 " Molybdenum 1.8 0.49 1 04/26/21 14:22 " Nickel 110 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 39 2.0 Zinc 2100 2.0 STLC Metals by ICP Chromium TCLP Metals by ICP 0.27 0.10 mg/L 2 B1D0916 05/03/21 13:26 STLC/EPA601OB Lead 0.054 0.050 mg/L I B I D0919 05/03/21 14:44 EPA 1311 /EPA 601 OB N-02 N-01, N-03 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 " Matrix: Solid Sampled by : Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 5.0 mg/kg 1 BID0692 04/23/21 18:00 EPA 9015M R-07 Surrogate: 4-Bromoflaorohen_ene 97 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 39 10 mg/kg 1 BID0766 04/27/21 16:32 EPA 8015M D-06 TPH Motor Oil (C23-C40) 110 50 Surrogate. o-kiphenYl 75 (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 37 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID: 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.052 mg/kg 1 B1D0650 04/23/21 23:41 EPA 8260B ^ Brotnobenzene ND 0.052 Bromochloromethane ND 0.052 Bromodichloromethane ND 0.052 Bromofonn ND 0.052 Bromomethane ND 0.052 n-Butylbenzene ND 0.052 sec-Butylbenzene ND 0.052 tert-Butylbenzene ND 0.052 Carbon tetrachloride ND 0.052 Chlorobenzene ND 0.052 Chloroethanc ND 0.052 Chloroform ND 0.052 Chloromethane ND 0.052 • 2-Chlorotoluene ND 0.052 4-C'hlorotoluene ND 0.052 Dibromochloromethanc ND 0.052 1,2-Dibromo-3-chloropropane ND 0.052 12-Dibrontoethane (EDB) ND 0.052 Dibromomethane ND 0.052 1,2-Dichlorobenzene ND 0.052 13-Dichlorobenzene ND 0.052 1,4-Dichloroben7ene ND 0.052 Dichloroditluoromcthanc ND 0.052 1, 1 -Dichloroethane ND 0.052 " 1,2-Dichloroethane ND 0.052 1,1-Dichloroethene ND 0.052 . cis-1,2-Dicliloroethene ND 0.052 trans-1,2-Dichloroethene ND 0.052 1,2-Dichloropropane ND 0.052 " 1,3-Dichloropropane ND 0.052 2,2-Dichloropropane ND 0.052 " 1,1-Dichloropropane ND 0.052 cis-L3-Dichloropropenc ND 0.052 trans-1,3-Dichloropropenc ND 0.052 " Lthylbenzcnc ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 38 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by : Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.052 mgIg 1 BID0650 04/23/2123:41 EPA8260B 4-Isopropyl Toluene ND 0.052 Isopropylbenzene ND 0.052 Methylene chloride ND 0.052 Naphthalene ND 0.052 n-Propylbenzene ND 0.052 Styrene ND 0.052 1, 1, 1,2-Tetrachloroethane ND 0.052 I.1,2,2-Tetrachloroethane ND 0.052 Tctrachlorocthcne (PCE) ND 0.052 Toluene ND 0.052 1,2,3-Trichlorobcnzcne ND 0.052 1,2,4-Trichlorobenzene ND 0.052 1, 1, 1 -Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 Trchloroethene (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 12,3-Trichloropropane ND 0.052 1.2,4-Trimethylbenzene ND 0,052 1,3,5-Trimethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylencs (total) ND 0.052 Surrogate: Dibrrnno/luuromethailu 97 (74 - 122) Surrogate: Tohiem,48 97 ( 65 - 138 ) Sun-ogate. 4-Bromq/luon ohen-e» e 91 ` (75. 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Dlercury 0.19 0.088 mg/kg 1 BID0711 04/26/21 15:18 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:25 EPA 6010B Arsenic 9.0 2.0 Barium 380 1.0 Beryllium ND 0.50 Cadmium 1.3 0.25 Chromium 44 0.50 Cobalt 13 0.50 Copper 36 1.0 Lead 360 0.50 " " " " " N-02, N-03 Molybdenum 0.73 0.50 Nickel 71 0.50 " Selenium ND 2.0 " Silver ND 0.50 " Thallium ND 1.0 Vanadium 35 2.0 Zinc 780 2.0 STLC Metals by ICP Lead 12 0.10 mg/L 2 131130916 05/03/21 13:28 STLC/EPA 6010E N-07 TCLP Metals by ICP Lead 0.092 0.050 mg/L I B 1 D0919 05/03/21 14:46 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 40 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 I Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FED TPH Gasoline (C5-C12) ND 4.6 mg/kg 1 B1D0692 04/23/21 18:26 EPA 8015M R-07 Surrogate: 4-Bromo/luorobenzene 98 (39 - 157) " Semi -Volatile Organic TPH by GC/FID r. TPH Diesel (C13-C22) 21 10 mg/kg 1 BID0766 04/27/21 16:54 EPA 8015M D-66 TPH Motor Oil (C23-C40) 140 50 11 11 11" 11 Surrogate: o-kiphem'l 80 `D� (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 41 of 94 r-, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.052 mg/kg 1 B l D0650 04/24/21 00:08 EPA 8260B Bromobenzene ND 0.052 Bromochloromethane ND 0.052 Brmnodichtoromethane ND 0.052 " Bromofonn ND 0.052 Bromomethane ND 0.052 " n-Butylbenzene ND 0.052 sec-Butylbenzene ND 0.052 tert-Butylbenzene ND 0.052 Carbon tetrachloride ND 0.052 Chlorobenzenc ND 0.052 Chlorocthane ND 0.052 Chloroform ND 0.052 " Chloromethane ND 0.052 2-Chlorotoluene ND 0.052 4-Chlorotoluene ND 0.052 Dibromochloromethane ND 0.052 " 1,2-Dibromo-3-chloropropane ND 0.052 1,2-Dibromoethane (EDB) ND 0.052 Dibromomethane ND 0.052 1,2-Dichlorobenzene ND 0.052 1,3-Dichlorobcnzenc ND 0.052 1,4-Dichlorobcn7enc ND 0.052 Dichlorodifluoromethanc ND 0.052 1,1-Dichloroethane ND 0.052 " 1,2-Dichloroethane ND 0.052 1,1-Dichloroethene ND 0.052 cis-1.2-Dichloroethene ND 0.052 " trans-1,2-Dichloroethene ND 0.052 " 1,2-Dichloropropane ND 0.052 13-Dichloropropane ND 0.052 22-Dichloropropane ND 0.052 1,1-Dichloropropane ND 0.052 cis-1.3-Dichloropropenc ND 0.052 trans-O-Dichloropropenc ND 0.052 Ethylbenzenc ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID: 2102508-10 Field Data: NA AnaIyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 flexachlorobutadiene ND 0.052 mglkg 4-Isopropyl Toluene ND 0.052 " Isopropylbenzene ND 0.052 " Methylene chloride ND 0.052 " Naphthalene ND 0.052 " n-Propylbenzene ND 0.052 " Styrene ND 0.052 1, 1. 1,2-Tetrachloroethane ND 0.052 1.1,22-Tetrachloroethane ND 0.052 " Tctrachlorocthcne (PCE) ND 0.052 " Toluene ND 0.052 1,2,3-Trichlorobcnzene ND 0.052 1,2,4-Trichlorobenzene ND 0.052 1, 1, 1 -Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 " Trichloroethene (TCE) ND 0.052 " Trichlorofluoromethane ND 0.052 " 1,2,3-Trichloropropane ND 0.052 " 1,2,4-Triniethylbenzene ND 0.052 13,54rimethylbenzene ND 0.052 " Vinyl chloride ND 0.052 Xylenes (total) ND 0.052 " Surrogate: Dibromoflaoromethune 97 % (74 - 1221) Surrogate: Toluene-d8 96 "/„ ( 65 - 128 ) Surrogate: 4-Bromnolluorobeirene 90 Y. (75 - 121) I BID0650 04/24/21 00:08 EPA 8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2088-B Sampled: 04/23/21 11:50 " Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA blercurc 0.11 0.099 mg!kg 1 BID0711 04/26/2115:20 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:28 EPA 6010B ,_. Arsenic 15 2.0 Barium 270 0.98 Beryllium ND 0.49 Cadmium 1.4 0.25 Chromium 130 0.49 N-02, N-03 Cobalt 16 0.49 Copper 68 0.98 Lead 440 0.49 " " " " " N-02, N-03 • Nlolvbdenum 1.2 0.49 Nickel 120 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 38 2.0 Zinc 1400 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/L 2 BID0916 05/03/2113:31 STLC/EPA6010B Lead 14 0.10 " " " " " N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BID0919 05/03/2114:49 EPA 1311/EPA6010B Lead 0.27 0.050 " " " " 1. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-B Sampled : 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.6 mg/kg 1 BID0692 04/23/21 20:35 EPA 8015M R-07 Sin•rogate: 4-Bromo/luorobenzene 97 �,i, (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C 13-C22) 17 10 mg/kg 1 B 1 D0766 04/27/21 16:54 EPA 8015M D-06 TPH Motor Oil (C23-C40) 87 50 Surrogate: o-TeiprhenYl r-, 74 '/ (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 45 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg/kg 1 BID0050 04/24/2100:35 EPA8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 ._ Naphthalene ND 0.045 n-Propylbenzene ND 0.045 " Styrene ND 0.045 1,1,1,2-Tetrachloroethane ND 0.045 ~ I.1,2,2-Tetrachloroethane ND 0.045 Tctrachlorocthcnc (PCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1, 1, 1 -Trichloroethane ND 0.045 1,1,2-Tricliloroethane ND 0.045 Trichloroethene (TC E) ND 0.045 Trichlorofluoromethane ND 0.045 1,2,3-Trichloropropane ND 0.045 12,4-I'riniethylbenzene ND 0.045 1,3,5-1'rimethylbenzene ND 0.045 Vinyl chloride ND 0.045 " Xylenes (total) ND 0.045 Surrogate: Dibromglluoromethanc 97 `S , (74 - 122) Surrogate: Toluene-d8 95 % ( 65 - 128 ) Surrogate: 4-Br,mu,/luuroben-ene 90 % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 94 C A W&-M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportI Analytical t Sample ID : Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mgkg 1 BID0711 04/26/2115:30 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1 D0734 04/26/21 14:31 EPA 601 OB —. Arsenic 13 2.0 " Barium 300 099 Beryllium ND 0.49 Cadmium 19 0.25 Chromium 56 0.49 " Cobalt 17 0.49 " r Copper 1100 0.99 Lead 390 0.49 N-02 N-02 N-02 N-02, N-03 Molybdenum 1.1 0.49 Nickel 100 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 34 2.0 "Zinc 660 2.0 STLC Metals by ICP Cadmium 0.088 0.050 mg/l. 2 BID0916 05/03/21 13:34 STLC/EPA601OB Chromium 0.24 0.10 Copper 0.69 0.1O Lead 10 O. I () " " „ " " N-07 --I The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 48 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by: Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes TCLP Metals by ICP Lead Volatile Organic TPH by GC/FID 0.085 0.050 mg/1- 1 B 1 D0919 05/03/21 14:59 EPA 1311 /EPA 601(1B TPH Gasoline W5-C12) ND 4.8 mg/kg 1 BID0692 04/23/21 21:01 EPA 8015M R-07 Surrogate: 4-Bromq luorobenzene 96 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 20 10 mg/kg 1 BID0766 04/27/21 17:17 EPA 8015M D-06 TPH Motor Oil (C23-C40) 130 50 Surrogate: u-Terphenyl 78 % (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 49 o f 94 O"IM fW ANN qu Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples -1� Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Sampled by: Matrix: Solid Field Data: NA Lab ID : 2102508-12 Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.045 mg'kg 1 BID0650 04/2412101:02 EPA8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 " Bromodichloromethane ND 0,045 Bromoform ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzcnc ND 0.045 Chlorocthanc ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 12-Dibrontoethane (EDB) ND 0.045 Dibromomethane ND 0.045 1.2-Dichlorobenzcne ND 0.045 13-Dichlorobenzcnc ND 0.045 1,4-Dichlorobenzcnc ND 0.045 Dichloroditluoromethane ND 0.045 1,1-Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 1, 1 -Dichloroethene ND 0.045 cis-1,2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 12-Dichloropropane ND 0.045 1,3-Dichloropropane ND 0.045 2,2-Didiloropropane ND 0.045 I,1-Dichloropropene ND 0.045 cis- 1,3-Dichloropropene ND 0.045 " trans-1,3-Dichloropropene ND 0.045 Ethylbenzenc ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 50 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report t Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexaclhlorobutadiene ND 0.045 mg/kg 1 BID0650 04/24/21 01:02 F.PA 8260B 4-Isopropyl Toluene ND 0.045 " Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 " Naphthalene ND 0.045 " n-Propylbenzene ND 0.045 Styrene ND 0.045 1, 1. 1,2-Tetrachloroethane ND 0.045 " 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachlorocthcne (PCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzcne ND 0.045 1,2,4-Trichlombenzene ND 0.045 1,1,1-Triehloroethane ND 0.045 1,1,2-Triehloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 Trichlorofluoromelhane ND 0.045 1,2.3-Trichloropropane ND 0.045 1,2.4-Trimethylbenzene ND 0.045 1,3,5-Trimethylbenzene ND 0.045 " Vinyl chloride ND 0.045 Xylencs (total) ND 0.045 Surrogate: Dibrornglhiorontethanc 95 1XI (74 - 122 ) Surrogate: Toluene-dS 9830 (65. 128 ) Surrogate: 4-8ro1noJluoroben_ene 88 Y. (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 ' Matrix: Solid Sampled by: Lab ID: 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg kg 1 BID0711 04/26/21 15:32 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I D0734 04/26/21 14:41 EPA 6010B Arsenic 7.0 2.0 Barium 360 1.0 Beryllium ND 0.50 Cadmium ND 0.25 ~ Chromium 48 0.50 Cobalt 10 0.50 Copper 620 LO " " " " " N-02 H Lead 940 0.50 " " N-02 N-03 Nlolvbdenum 1.4 0.50 —' Nickel 66 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 34 2.0 Zinc 610 2.0 a, STLC Metals by ICP Copper Lead TCLP Metals by ICP Lead 2.4 0.10 mg/L 2 BID0910 05/03/2113:36 STLC/EPA6010B 51 0.10 " " "11 1. N-07 4.7 0.050 ma/L 1 B1D0919 05/03/2115:01 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: ;805) 925-3376 Page 52 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-A Sampled : 04/23/21 12:00 Matrix: Solid Sampled by : Lab ID: 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.2 ing!kg 1 BID0692 04/23/21 21:27 EPA 8015M R-07 Surrogate: 4-Bromgfluorobenzene 92 "N, (39 - 157 ) Semi -Volatile Organic TPH by GC/FID — TPH Diesel (03-C22) 12 10 mg/kg 1 B1D0766 04/27/21 17:17 EPA 8015M D-06 TPH Motor Oil (C23-C40) 67 50 Surrogate: o-Teipher?rl 73 `% (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 53 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID: 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kg 1 B1D0650 04/24/2101:29 EPA8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 " Brontodichloromethane ND 0.050 . Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 " ^ sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 " Carbon tetrachloride ND 0.050 Chlorobenzenc ND 0.050 Chloroethane ND 0.050 Chloroform ND 0.050 Chlommethanc ND 0.050 " 2-Chlorotoluene ND 0.050 4-Clilorotoluene ND 0.050 Dibromochloromethanc ND 0.050 1,2-Dibronto-3-chloropropane ND 0.050 12-Dibromoethane (EDB) ND 0.050 Dibromomethane ND 0.050 1,2-Dichlorobenzene ND 0.050 1,3-Dichlorobenzene ND 0.050 1,4-Dichlorobenzene ND 0.050 Dichloroditluoromcthanc ND 0.050 " 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 " 13-Dichloroethene ND 0.050 cis-1,2-Dichloroethene ND 0.050 " trans-1,2-Dichloroethene ND 0.050 " 12-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 22-Dichloropropane ND 0.050 1. 1 -Dichloropropene ND 0.050 cis- 1.3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 Ethylbcnzenc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 54 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.050 mg/kg 1 BID0650 04/24/2101:29 EPA8260B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 " Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 I,1.I.2-Tetrachloroethane ND 0.050 1,1,2,2-1'etrachloroethane ND 0.050 " Tetrachlorocthcnc (PCE) ND 0.050 Toluene ND 0.050 1,2,3-Triehlorobenzenc ND 0.050 " 1,2,4-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 " 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorotluoromethane ND 0.050 1,2,3-Trichloropropane ND 0.050 1,2,4-Triniethylbenzene ND 0.050 1,3,5-Trunethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Dihromo/htorontethanc 96 % ( 74 - 122) Surrogate. Toluene-dS 96 i& (65 - 128 ) Surrogate: 4-Bronwfluoroben_ene S9 N, (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 55 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20376-B Sampled : 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.20 0.097 mg/kg 1 B1 D0711 04/26/21 15:34 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I BID0734 04/26/2114:44 EPA 6010B Arsenic 6.7 2.0 Barium 440 0.99 " Beryllium ND 0.50 Cadmium ND 0.25 Chromium 73 0.50 N-02 Cobalt 9.4 0.50 Copper 57 0.99 Lead 2000 0.50 N-01, N-03 Molybdenum 2.5 0.50 Nickel 68 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 30 2.0 Zinc 770 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/1- 2 B I D0916 05/03/21 13:39 STLC/EPA 6010B TCLP Metals by ICP Lead — 0.99 0.050 mg/L t BID0919 05/03/21 15:04 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: f.805' 925-3376 Page 56 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical _.. Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by : Lab ID: 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) ND 5.1 mg/kg 1 Bl D0692 04/23/21 21:53 EPA 8015M R-07 Surrogate: 4-Bromo/laorobenzene 96 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 uig/kg 1 BID0766 04/28/21 15:08 EPA 8015M TPH Motor Oil (C23-C40) 64 50 Surrogate: o-Tei phen l 79 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 57 of 94 WK Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20376-B Sampled: 04/23/21 12:05 ' Matrix: Solid Sampled by : Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GONIS R-07 Benzene ND 0.047 mg,kg 1 BID0650 04/24/2101:57 F.PA8260B Bromobenzene ND 0.047 Bromochlorometliane ND 0.047 Bromodiehloromethane ND 0.047 Bromofonn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 " ^ tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzene ND 0.047 " Chloroethane ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 - 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 " Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 1,2-Dibromoethane (EDB) ND 0.047 Dibromomethane ND 0.047 " 1,2-Dichlorobenzene ND 0.047 " 1,3-Dichlorobenzene ND 0.047 14-Dichlorobenzene ND 0.047 Dichlorodifluoromethane ND 0.047 1,1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 _ cis- 1.2-Dichloroethene ND 0.047 " trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1, 1 -Dichloropropene ND 0.047 cis-1.3-Dichloropropcnc ND 0.047 trans-1,3-Dichloropropcnc ND 0.047 Ethylbenzenc ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 _ Page 58 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 " Matrix: Solid Sampled by : Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 llexachlorobutadiene ND 0.047 mg/kg 1 BID0050 04/24/21 01:57 EPA 8260B . 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 " 1,1,12-Tetrachloroethane ND 0.047 1,1.22-Tetrachloroethane ND 0.047 Tetrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 ' 1,2.3-Trichlorobcnzcnc ND 0.047 1,2,4-Trichlorobenzene ND 0.047 " 1,1,1-Trichlorocthane ND 0.047 1.1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorolluoromethane ND 0.047 1,2.3-Trichloropropane ND 0.047 1,2.4-Triniethylbenzene ND 0.047 1,3,5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 Xylenes (total) ND 0.047 Surrogate: DihroinoJluoromethane 97 6 (74 - 122) Surrogate: Toluene-dg 96 % (65 - 128) Surrogate: 4-BromoJlucunhen_ene 91 `Si, ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 59 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mglkg 1 BID0711 04/26/21 15:36 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg I BID0734 04/20/21 14:47 EPA 601OB Arsenic 5.6 1.9 Barium 320 0.97 Beryllium ND 0.49 ^ Cadmium ND 0.24 Chromium 49 0.49 Cobalt 10 0.48 _ Copper 41 0.97 Lead 440 0.48 " " " " " N-02 N-03 Nlolvbdenum 0.80 0.48 - Nickel 68 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 38 1.9 Zinc 580 1.9 " STLC Metals by ICP Lead 40 0.10 nig/L 2 BID0916 05/03/21 13:41 STLC/EPA 60 1 OB N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/I. 1 B 1 D0919 05/03/21 15:06 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.6 mg/kg 1 B1 D0692 04/23/21 22:18 EPA 8015M R-07 Surrogate: 4-Bromn/luorohen_ene 94'A (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 140 20 mg/kg 2 B1D0766 04/28/21 16:38 EPA 8015M D-06 TPH Motor Oil (C23-C40) 360 100 11 11 1. 11" Surrogate: o-kiphenYl 120 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 61 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg/kg 1 B1D0650 04/24/21 02:24 EPA 8260B ' Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 " _., Bromol'onn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobcnzcnc ND 0.047 Chloroethane ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 1.2-Dibrontoethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,24)ichlorobenzene ND 0.047 - 1,3-Dichlorobenzene ND 0.047 1,4-Dichlorobenzene ND 0.047 Dichlorodifluoromethane ND 0.047 - 1, 1 -Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 " L I-Dichloroethene ND 0.047 cis-1.2-Dichloroethene ND 0.047 trans-1,2-Dichloroethene ND 0.047 " 1,2-Dichloropropane ND 0.047 I,3-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1,1-Dichloropropene ND 0.047 cis-1.3-Dichloropropcnc ND 0.047 ' trans-1,3-Dichloropropcnc ND 0.047 Ethylbcnzene ND 0.047 ' The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 62 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Volatile Organic Compounds by GUMS (Continued) R-07 Flexachlorobutadiene ND 0.047 mg/kg 1 B1D0650 04/24/2102:24 EPA8260B ^ 4-Isopropyl Toluene ND 0.047 lsopropylbenzene ND 0.047 Methylene chloride ND 0.047 __. Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1.1,1,2-Tetrachloroethane ND 0.047 - 1,1.2,2-Tetrachloroethane ND 0.047 Tetrachlorocthcnc (PCE) ND 0.047 " Toluene ND 0.047 ' 1,2,3-Trichlorobenzene ND 0.047 1,24-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 - • 1,1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 " 1,2.3-Trichloropropane ND 0.047 1,2,4-Trimethylbenzene ND 0.047 " 1.3.5-Trimethylbenzene ND 0.047 " Vinyl chloride ND 0.047 Xylcnes (total) ND 0.047 Surrogate: Dibromolhrorwncthmic 95 44, (74 - 122 ) 11 Surrogate. Toluene-dg 97 3f, (65 - 12b' ) -^ Surrogate: 4-Bromo9uorohen-ene 92 'N, ( 75 - 121) r1 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 63 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes �- Level Result Limits Limit Batch BlD0711 - EPA 7471A Preparation: EPA 7471A Prep 04/26/21 09:00 Blank (BlD0711-BLKI) Analyzed: 04/26/21 14:37 Mercury ND 0.10 mg/kg LCS (B1D0711-BS1) Analyzed: 04/26/21 14:31 Mercury 0.803 0.10 mg/kg 0.833 96 85-115 LCS Dup (B1D0711-BSD1) Analyzed: 04/26/21 14:33 Mercury 0.765 0.10 mg/kg 0.833 92 85-115 5 20 Duplicate (BlD0711-DUPl) Source: 2102489-02 Analyzed: 04/26/21 14:45 Mercury 0.0432 0.099 mg/kg 0.0418 3 20 Matrix Spike (BlD0711-MSI) Source: 2102489-02 Analyzed: 04/26/21 14:47 Mercury 0.943 0.090 mg/kg 0.746 0.0418 107 75-125 Matrix Spike Dup (B1D0711-MSDl) Source: 2102489-02 Analyzed: 04/26/21 14:49 Mercury 0.673 0.087 mg%kg 0.723 0.0418 87 75-125 22 20 QR-02 Post Spike (BlD0711-PS1) Source: 2102489-02 Analyzed: 04/26/21 14:51 Mercury 5.23 ug/L 5.00 0.273 99 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 64 of 94 - (.. �a P�� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Totalby Quality Coutrol Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0734 -EPA 6010B Preparation: EPA 3050B 04/26./21 07:37 Blank (BlD0734-BLKI) Analyzed: 04/26/21 13:29 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 " Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper NI) 1.0 Lead ND 0.50 Molybdenum ND 0.50 " -• Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 - Vanadium ND 2.0 " Zinc ND 2.0 LCS (B1D0734-BS1) Analyzed: 04/26/21 13:04 Antimony 97.0 2.5 mg/kg 100 97 80-120 Arsenic 100 2.0 100 100 80-120 Barium 93.5 1.0 100 94 80-120 - Beryllium 99.0 0.50 100 99 80-120 , Cadmium 99.2 0.25 100 99 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 100 0.50 100 100 80-120 Copper 104 1.0 100 104 80-120 Lcad 99.4 0.50 100 99 80-120 Molybdenum 98.4 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium lot 2.0 100 WI 80-120 Silver 5.04 0.50 5.00 101 80-120 Thallium 108 1.0 100 108 80-120 �. Vanadium 99.8 2.0 100 100 80-120 Zinc 97.0 2.0 100 97 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 65 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes -, Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 LCS Dup (BlD0734-BSDI) Analyzed: 04/26/21 13:06 Antimony 97.9 2.5 mg/kg 100 98 80-120 0.8 20 Arsenic 101 2.0 100 101 80-120 0.7 20 Barium 93.6 1.0 100 94 80-120 0.2 20 Beryllium 98.6 0.50 100 99 80-120 0.4 20 Cadmium 99.5 0.25 100 100 80-120 0.3 20 Chromium 103 0.50 100 103 80-120 0.8 20 - Cobalt 101 0.50 100 101 80-120 0.3 20 Copper 104 1.0 100 104 80-120 0.8 20 Lead 99.8 0.50 100 100 80-120 0.3 20 Molybdenum 99.4 0.50 100 99 80-120 0.9 20 Nickel 102 0.50 100 102 80-120 0.4 20 Selenium 101 2.0 100 101 80-120 0.1 20 Silver 5.04 0.50 5.00 101 80-120 0.1 20 Thallium 108 1.0 100 108 80-120 0.5 20 Vanadium 100 2.0 100 100 80-120 0.4 20 Zinc 97.4 2.0 100 97 80-120 0.4 20 Duplicate (BlD0734-DUPl) Source: 2102489-01 Analyzed: 04/26/21 13:35 Antimony ND 2.5 mg'kg ND 20 Arsenic 5.86 2.0 6.40 9 20 Barium 87.5 0.99 72.5 19 20 Beryllium 0.369 0.49 0.419 12 20 Cadmium ND 0.25 ND 20 Chromium 20.1 0.49 22.2 9 20 Cobalt 6.53 0.49 6.95 6 20 Copper 18.4 0.99 21.5 16 20 Lead 5.52 0.49 6.10 10 20 Molybdenum 1.50 0.49 2.18 37 20 QR-04 Nickel 25.9 0.49 30.4 16 20 Selenium ND 2.0 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.99 ND 20 _ Vanadium 18.9 2.0 20.6 9 20 Zinc 49.7 2.0 53.8 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 66 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total' - Quality Control I Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Matrix Spike (BlD0734-MSI) Source: 2102489-01 Analyzed: 04/26/21 13:08 Antimony 30.5 2.5 mg/kg 98.3 ND 31 10-116 Arsenic 102 2.0 98.3 6.40 97 77-121 Barium 159 0.98 98.3 72.5 88 30-169 Beryllium 93.2 0.49 98.3 0.419 94 86-111 Cadmium 90.1 0.25 98.3 ND 92 81-112 Chromium 124 0.49 98.3 22.2 103 75-129 Cobalt 98.3 0.49 98.3 6.95 93 71-121 Copper 123 0.98 99.3 21.5 103 68-135 Lead 95.5 0.49 98.3 6.10 91 72-121 Molybdenum 87.8 0.49 98.3 2.18 87 70-112 •-• Nickel 122 0.49 98.3 30.4 93 73-121 Selenium 91.6 2.0 98.3 ND 93 76-116 Silver 4.59 0.49 4.92 ND 93 54-132 Thallium 94.7 0.98 98.3 ND 96 64-120 - Vanadium 117 2.0 98.3 20.6 98 78-124 Zinc 142 2.0 99.3 53.8 89 50-143 Matrix Spike Dup (BlD0734-MSD1) Source: 2102489-01 Analyzed: 04/26/21 13:11 Antimony 28.7 2.4 mg,kg 97.7 ND 29 10-116 6 20 Arsenic 99.5 2.0 97.7 6.40 95 77-121 2 20 Barium 173 0.98 97.7 72.5 103 30-169 9 20 Beryllium 90.5 0.49 97.7 0.419 92 86-111 3 20 Cadmium 86.7 0.24 97.7 ND 89 81-112 4 20 Chromium 120 0.49 97.7 22.2 100 75-129 3 20 Cobalt 95.5 0.49 97.7 6.95 91 71-121 3 20 Copper 120 0.98 97.7 21.5 101 68-135 3 20 Lead 92.4 0.49 97.7 6.10 88 72-121 3 20 Molybdenum 85.4 0.49 97.7 2.18 85 70-112 3 20 Nickel 121 0.49 97.7 30.4 92 73-121 1 20 Selenium 87.5 2.0 97.7 ND 90 76-116 5 20 Silver 4.44 0.49 4.88 ND 91 54-132 3 20 Thallium 90.3 0.98 97.7 ND 92 64-120 5 20 Vanadium 115 2.0 97.7 20.6 96 78-124 2 20 Zinc 141 2.0 97.7 53.8 89 50-143 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 67 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 __. Post Spike (BlD0734-PS1) Source: 2102489-01 Analyzed: 04/26/21 13:14 Antimony 1.95 ma/1. 2.00 -0.00714 93 75-125 Arsenic 2.15 2.00 0.129 101 75-125 Barium 3.34 2.00 1.46 94 75-125 Beryllium 1.96 2.00 0.00843 97 75-125 Cadmium 1.88 2.00 -0.0200 94 75-125 Chromium 2.46 2.00 0.448 100 75-125 Cobalt 2.05 2.00 0.140 96 75-125 Copper 2.56 2.00 0.433 106 75-125 Lead 2.01 2.00 0.123 94 75-125 Molybdenum 1.97 2.00 0.0438 96 75-125 - - Nickel 2.55 2.00 0.613 97 75-125 Selenium 1.96 2.00 -0.0375 98 75-125 Silver 0.0965 0.100 -0.00476 96 75-125 Thallium 1.98 2.00 -0.0435 99 75-125 - Vanadium 2.41 2.00 0.416 100 75-125 Zinc 2.96 2.00 1.08 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 68 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 i Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0916 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:33 Blank (BlD0916-BLKI) Analyzed: 05/03/21 12:22 Cadmium ND 0.025 mg/L Chromium ND 0.050 Copper ND 0.050 Lead ND 0.050 " LCS (BlD0916-BS1) Analyzed: 05/03/21 12:35 Cadmium 9.62 0.025 mg/L 10.0 96 80-120 Chromium 9.56 0.050 10.0 96 80-120 Copper 9.66 0.050 10.0 97 80-120 Lead 9.70 0.050 10.0 97 80-120 LCS Dup (BlD0916-BSD1) Analyzed: 05/03/21 12:37 Cadmium 9.68 0.025 mg/L 10.0 97 80-120 0.6 20 Chromium 9.59 0.050 10.0 96 80-120 0.3 20 Copper 9.70 0.050 10.0 97 80-120 0.4 20 Lead 9.78 0.050 10.0 98 80-120 0.9 20 Duplicate (B1D0916-DUPl) Source: 2102467-01 Analyzed: 05/03/21 12:53 Cadmium ND 0.050 mg/L ND 20 Chromium 0.0860 0.10 0.111 25 20 QR-04 Copper 1.53 0.10 1.76 14 20 Lead 0.773 0.10 0.930 18 20 Leach Fluid Blank (B1D0916-LBK1) Analyzed: 05/03/21 12:25 Cadmium ND 0.050 mg/L Chromium ND 0.10 Copper ND 0.10 " Lead ND 0.10 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 69 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 TCLP Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0919 -EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:49 Blank (B1D0919-BLK1) Analyzed: 05/03/21 13:54 Chromium ND 0.050 mg/L Lead ND 0.050 " LCS (B1D0919-BS1) Analyzed: 05/03/21 14:02 Chromium 9.42 0.050 mg/L 10.0 Lcad 9.97 0.050 1.10.0 LCS Dup (BlD0919-BSD1) Analyzed: 05/03/21 14:04 Chromium 9.35 0.050 mg/L 10.0 Lead 9.82 0.050 1110.0 Duplicate (B1D0919-DUP1) Source: 2102508-01 Analyzed: 05/03/21 14:11 Chromium ND 0.050 mg/L ND Lead 1.60 0.050 112.02 Leach Fluid Blank (BlD0919-LBK1) Analyzed: 05/03/21 13:57 Chromium ND 0.050 mg/L Lead ND 0.050 " 94 80-120 100 80-120 94 80-120 0.7 20 98 80-120 2 20 20 24 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 70 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic TP" by 1 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0692 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 04/23/21 08:32 �- Blank (B1D0692-BLKI) Analyzed: 04/23/21 10:26 TPH Gasoline (C5-C12) ND 0.50 mg/kg Stu•rogate:4-Bromofluorohensene 0.128 110.125 103 39-157 — LCS (BlD0692-BSI) Analyzed: 04/23/21 09:34 TP14 Gasoline (('5-C12) 1.07 0.50 mg/kg 1.00 107 68-139 Surrogate.4-Bromolluorohenzene 0.146 110.126 116 39-157 LCS Dup (B1D0692-BSDl) Analyzed: 04/23/21 10:00 TPH Gasoline (C5-C12) 1.05 0.49 mg/kg 0.988 106 68-139 2 20 Surrogate: 4-Bromof torobenzene 0.150 0.124 121 39-157 Duplicate (BID0692-DUPI) Source: 2102433-01RE1 Analyzed: 04/23/21 22:44 TPH Gasoline (('5-C12) ND 4.8 nig/kg ND 20 Surrogate:4-Bromolluorobenzene 1.18 111.20 98 39-157 ^• Matrix Spike (B1D0692-MSl) Source: 2102433-01RE1 Analyzed: 04/23/21 23:10 TPH Gasoline (C'5-('12) 8.79 4.9 mg/kg 9.80 ND 90 10-171 Surrogate: 4-13romolluorohen_eae 1.34 1.23 109 39-157 Matrix Spike Dup (B1D0692-MSDl) Source: 2102433-01RE1 Analyzed: 04/23/21 23:36 TPH Gasoline (C5-C12) 8.26 4.4 mg/kg 8.77 ND 94 10-171 6 20 Surrogate: 4-Bromof uoroben_ene 1.29 111.10 118 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 71 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Semi -Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0766 - EPA 8015M Preparation: EPA 3550C 04/27/21 07:10 Blank (BlD0766-BLK1) Analyzed: 04/27/21 14:40 TPH Diesel (C13-('22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 11 Surrogate: o-Topheml 41.9 " 49.8 84 65-136 LCS (BlD0766-BS1) Analyzed: 04/27/21 13:53 TPH Diesel (Cl3-C22) 420 10 mg/kg 499 84 72-115 TPH Motor Oil (C23-C40) 404 50 499 81 74-126 Surrogate: o-Telphenyl 43.0 49.9 86 65-136 LCS Dup (B1D0766-BSD1) Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22) 420 10 mg/kg 500 84 72-115 0.2 20 TPH Motor Oil (C23-C40) 402 50 500 80 74-126 0.5 20 Surrogate: o-Tciphemd 42.3 50.0 85 65-136 Duplicate (BlD0766-DUPI) Source: 2102489-01 Analyzed: 04/27/21 15:02 TPH Diesel (C13-C22) ND 9.9 mg/kg ND 20 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Tclphenl] 38.9 49.6 78 65-136 Matrix Spike (B1D0766-MSl) Source: 2102489-01 Analyzed: 04/27/21 14:17 TPH Dicscl (C13-C22) 430 9.9 mg/kg 497 ND 86 46-147 TPII Motor Oil (('23-C40) 418 50 497 ND 84 35-171 Surrogate: o-Teiphel el 40.2 49.7 81 65-136 Matrix Spike Dup (B1D0766-MSD1) Source: 2102489-01 Analyzed: 04/27/21 14:40 TPH Diesel (C:I3-C22) 490 10 mg/kg 499 ND 96 46-147 11 20 TPH Motor Oil (C23-C40) 429 50 499 ND 86 35-171 3 20 Surrogate: o-Telphcm•l 44.5 49.9 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 72 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (B1D0650-BLK1) Analyzed: 04/23/21 16:50 Benzene ND 0.0050 mg/kg 13romobenzenc ND 0.0050 Bromochloromcthane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 " Bromomethane ND 0.0050 " u-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 C'hlorobenzene ND 0.0050 " Chloroethane ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (F.DB) ND 0.0050 " Dibromomethanc ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " 1,3-Dichlorobcnzenc ND 0.0050 1,4-Dichlorobenzene ND 0.0050 Dichlorodilluoromethanc ND 0.0050 I,1-Dichloroethene ND 0.0050 " 1,2-Dichlorocthanc ND 0.0050 1,1-Dichloroethene ND 0.0050 " cis-L2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 12-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 " 1,1-Dichloropropene ND 0.0050 cis-L3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethylbenzene ND 0.0050 Hexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " Nlethylene chloride ND 0.0050 Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3375 Page 73 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 VolatileiControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 �. Blank (BlD0650-BLK1) Analyzed: 04/23/21 16:50 Styrene ND 0.0050 mg/kg 1, 1, 1,2-Tetrachloroethane ND 0.0050 " 1,1,2.2-Tetrachlorocthane ND 0.0050 " Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 " 1,2,3-Trichlorobenzene ND 0.0050 " 1.2,4-1'richlorobenzene ND 0.0050 " 1,1,1-Trichlomethane ND 0.0050 1.12-Trichlomethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 " - Trichlorotluoromethane ND 0.0050 " 1,2,3-Trichloropropane ND 0.0050 1,24-Trimethylbenzene ND 0,0050 " 1.3,5-Trimethylbenzene ND 0.0050 " N'invl chloride ND 0.0050 " Xylenes (total) ND 0.0050 Surrogate: Uibronur/lunruntelhcrrrr 0.0484 0.0498 97 74-12' �. Surrogate. Toluene-d8 0.0479 0.0498 96 65-128 Surrogate:4-BramgJhrorohen_ene 0.0453 0.0498 91 75-121 LCS (B1D0650-BS1) Analyzed: 04/23/21 14:31 _ Benzene 0.0389 0.0050 mg/kg 0.0396 98 70-131 Bromobenzene 0.0369 0.0050 0.0396 93 74-130 Bromochloromethane 0.0351 0.0050 0.0396 89 64-133 Bromodichloromethane 0.0368 0.0050 0.0396 93 69-137 ' Bromoform 0.0337 0.0050 0.0396 85 55-132 Bromomethane 0.0397 0.0050 0.0396 100 10-142 u-Butylbenzene 0.0440 0.0050 0.0396 111 64-156 sec-Butylbenzene 0.0465 0.0050 0.0396 117 75-155 tert-Butylbenzene 0.0438 0.0050 0.0396 110 74-144 Carbon tetrachloride 0.0396 0.0050 0.0396 100 67-135 Chlorobenzene 0.0399 0.0050 0.0396 101 73-134 .-, Chloroethane 0.0366 0.0050 0.0396 92 10-167 Chloroform 0.0371 0.0050 0.0396 94 69-124 Chloromethane 0.0286 0.0050 0.0396 72 34-136 2-Chlorotoluene 0.0421 0.0050 0.0396 106 75-135 4-Chlorotoluene 0.0420 0.0050 0.0396 106 70-138 Dibromochloromethane 0.0370 0.0050 0.0396 93 67-135 1,2-Dibromo-3-chIoropropanc 0.0368 0.0050 0.0396 93 41-149 1,2-Dibronioethane(ED13) 0.0365 0.0050 0.0396 92 68-131 Dibromomethane 0.0322 0.0050 0.0396 81 61-140 1,2-Dichlorobenzene 0.0409 0.0050 0.0396 103 76-130 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805)925-3376 Page 74 of 94 EEO, E- C Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS (B1D0650-BS1) Analyzed: 04/23/21 14:31 1,3-Dichlorobenzene 0.0427 0.0050 mgticg 0.0396 108 76-138 IA-Dichlorobenzene 0.0410 0.0050 0.0396 104 72-132 Dichlorodifluoromcthanc 0.0196 0.0050 0.0396 50 10-155 I,I-Dichloroethene 0.0399 0.0050 0.0396 101 63-139 1,2-Dichloroethene 0.0359 0.0050 0.0396 91 64-126 1,1-Dichloroethene 0.0435 0.0050 0.0396 110 52-167 cis-12-Dichloroethene 0.0380 0.0050 0.0396 96 70-135 trans-1,2-Dichloroethene 0.0421 0.0050 0.0396 106 67-147 1,2-Dichloropropane 0.0368 0.0050 0.0396 93 68-131 1,3-Dichloropropane 0.0359 0.0050 0.0396 91 64-128 ^, 2,2-Dichloropropane 0.0404 0.0050 0.0396 102 63-154 l,l-Dichloropropene 0.0386 0.0050 0.0396 97 68-138 cis- I3-Dichloropropene 0.0376 0.0050 0.0396 95 72-134 trans-1,3-Dichloropropene 0.0385 0.0050 0.0396 97 69-132 Ethylbenzene 0.0404 0.0050 0.0396 102 68-136 Hexachlorobutadienc 0.0446 0.0050 0.0396 113 72-198 4-Isopropyl Toluene 0.0439 0.0050 0.0396 111 74-150 r , Isopropylbenzene 0.0429 0.0050 0.0396 108 71-149 Methylene chloride 0.0402 0.0050 0.0396 102 51-127 Naphthalene 0.0436 0.0050 0.0396 110 57-158 n-Propylbenzene 0.0435 0.0050 0.0396 110 70-143 Styrene 0.0412 0.0050 0.0396 104 68-138 1,1,1,2-Tetrachloroethane 0.0373 0.0050 0.0396 94 76-130 1,1,2,2-Tctrachlorocthanc 0.0407 0.0050 0.0396 103 60-136 Tetrachloroethene (PCE) 0.0381 0.0050 0.0396 96 73-139 Toluene 0.0371 0.0050 0.0396 94 72-128 1,2,3-Trichlorobenzene 0.0390 0.0050 0.0396 98 61-166 1,2,4-Trichlorobenzene 0.0406 0.0050 0.0396 103 71-158 1,1,1-Trichloroethane 0.0389 0.0050 0.0396 98 71-135 1,1,2-Trichloroethane 0.0341 0.0050 0.0396 86 64-132 Trichloroethene(TCE) 0.0374 0.0050 0.0396 94 74-139 Trichlorofluoromethane 0.0379 0,0050 0.0396 96 30-156 1,2,3-Trichloropropane 0.0383 0.0050 0.0390 97 67-123 1,2,4= Gimethylbenzene 0.0419 0.0050 0.0396 106 68-134 1,3,5-Trimethylbenzene 0.0440 0.0050 0.0396 111 71-140 X'invl chloride 0.0352 0.0050 0.0396 89 43-144 Xylenes (total) 0.122 0,0050 0.119 102 69-138 Surrogate: 0.0490 0.0495 99 74- 12 Surrogate: Toluene-dX O.10475 0.0495 96 65-128 Surrogate:4-Bromalluorohen_ene 0.0476 0.0495 96 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 75 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes -z Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (BlD0650-BSDI) Analyzed: 04/23/21 14:59 Benzene 0.0417 0.0050 mg/kg 0.0398 105 70-131 7 20 Bromobenzene 0.0394 0.0050 0.0398 99 74-130 6 20 Bromochloromethanc 0.0377 0.0050 0.0398 95 64-133 7 20 Bromodichloromethane 0.0392 0.0050 " 0.0398 98 69-137 6 20 Bromoform 0.0363 0.0050 0.0398 91 55-132 8 20 Bromomethane 0.0416 0.0050 0.0398 105 10-142 5 20 n-Butylbenzene 0.0475 0.0050 0.0398 120 64-156 8 20 sec-Butylbenzene 0.0493 0.0050 0.0398 124 75-155 6 20 tert-Butylbenzene 0.0464 0.0050 0.0398 117 74-144 6 20 Carbon tetrachloride 0.0418 0.0050 0.0398 105 67-135 5 20 Chlorobenzeue 0.0420 0.0050 0.0398 106 73-134 5 20 Chloroethane 0.0394 0.0050 0.0398 99 10-167 7 20 Chloroform 0.0392 0.0050 0.0398 99 69-124 5 20 Chloromethane 0.0302 0.0050 0.0398 76 34-136 5 20 ' 2-Chlorotoluene 0.0435 0.0050 0.0398 109 75-135 3 20 4-Chlorotoluene 0.0431 0.0050 0.0398 108 70-138 3 20 Dibromochloromethane 0.0397 0.0050 0.0398 100 67-135 7 20 1,2-Dibromo-3-chloropropane 0.0410 0.0050 0.0398 103 41-149 11 20 1,2-Dibrontoethane (EDB) 0.0388 0.0050 0.0398 98 68-131 6 20 Dibromomethane 0.0334 0.0050 0.0398 84 61-140 4 20 1,2-Dichlorobenzene 0.0429 0.0050 0.0398 108 76-136 5 20 1.3-Dichlorobenzene 0.0444 0.0050 0.0398 112 76-138 4 20 1,4-Dichlorobenzene 0.0436 0.0050 0.0398 110 72-132 6 20 Dichlorodifluoromcthane 0.0206 0.0050 0.0398 52 10-155 5 20 1, 1 -Dichloroethane 0.0424 0.0050 0.0398 107 63-139 6 20 1,2-Diclilorocthane 0.0395 0.0050 0.0398 99 64-126 t0 20 1, 1 -Dichloroethene 0.0446 0.0050 0.0399 112 52-167 2 20 cis-1,2-Dichloroethene 0.0413 0.0050 0.0398 104 70-135 8 20 trans-1.2-Dichloroethene 0.0447 0.0050 0.0398 112 67-147 6 20 1,2-Dichloropropane 0.0401 0.0050 0.0398 101 68-131 9 20 1,3-Dichloropropane 0.0383 0.0050 0.0398 96 64428 6 20 2,2-Dichloropropane 0.0436 0,0050 0.0398 110 63-154 8 20 1, 1 -Dichloropropene 0.0416 0.0050 0.0398 105 68-138 8 20 cis- 1,3 -Dichloropropene 0.0407 0.0050 0.0398 102 72-134 8 20 trans-1,3-Dichloropropene 0.0414 0.0050 0.0398 104 69-132 7 20 Ethylbenzene 0.0422 0.0050 0.0398 106 68-136 4 20 Ilexachlorobutadiene 0.0478 0.005II 0.0398 120 72-198 7 20 4-1sopropyl Toluene 0.0465 0.0050 0.0398 117 74-150 6 20 Isopropylbenzene 0.0461 0.0050 0.0398 116 71-149 7 20 Methylene chloride 0.0427 0.0050 0.0398 108 51-127 6 20 Naphthalene 0.0454 0.0050 0.0398 114 57-158 4 20 n-Propylbenzene 0.0460 0.0050 0.0398 116 70-143 6 20 - The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 76 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes r Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 r LCS Dup (BlD0650-BSDI) Analyzed: 04/23/21 14:59 Styrene 0.0437 0.0050 mgtkg 0.0398 110 68-138 6 20 1, 1, 1,2-Tetrachloroethane 0.0395 0.0050 0.0398 99 76-130 6 20 1,1,2,2-Tetrachlorocthanc 0.0415 0.0050 0,0398 104 60-136 2 20 Tetrachloroethene (PCE) 0.0400 0.0050 0.0398 100 73-138 5 20 Toluene 0.0399 0.0050 0.0398 100 72-128 7 20 1,2,3-Trichlorobenzene 0.0432 0.0050 0.0398 109 61-166 10 20 1,24-Trichlorobenzene 0.0439 0.0050 0.0398 110 71-158 8 20 1, 1, 1 -Trichloroethane 0.0415 0.0050 0.0398 104 71-135 6 20 1,1,2-Trichloroethane 0.0377 0.0050 0.0398 95 64-132 10 20 Trichloroethene (TCE) 0.0396 0.0050 0.0399 99 74-139 6 20 Trichlorofluoromethane 0.0412 0.0050 0,0398 104 30-156 9 20 1,2,3-Trichloropropane 0.0381 0.0050 0.0398 96 67-123 0.6 20 1,2.4-Trimethylbenzene 0.0448 0.0050 0.0398 113 68-134 7 20 1,3,5-Trimethylbenzene 0.0461 0.0050 0.0398 116 71-140 5 20 Vinyl chloride 0.0371 0.0050 0.0398 93 43-144 5 20 Xylenes(total) 0.128 0.0050 0.119 IN 69-138 5 20 Surrogate: Dibromo/lu nwmethane 0.0504 0.0497 MI 74-122 �. Surrogate: Toluene-dN 0.0476 0.0497 96 65-128 Surrogate:4-BronmJhrorohen_ene 0.0475 0.0497 96 75-121 Duplicate (BlD0650-DUPl) Source: 2102489-01 Analyzed: 04/24/21 03:18 �. Benzene ND 0.0050 mg!kg ND 20 Bromobenzenc ND 0.0050 ND 20 Brontochloromethanc ND 0.0050 ND 20 Bromodichloromethane ND 0,0050 ND 20 " Bromotbrm ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 �. Chloroethane ND 0.0050 ND 20 Chlorofonn ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0,0050 ND 20 ' 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1.2-Dibromo-3-chloropropanc ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibronx>mcthanc ND 0.0050 ND 20 1.2-Dichlorobenzenc ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 77 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic i by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Duplicate (B1D0650-DUPl) Source: 2102489-01 Analyzed: 04/24/21 03:18 1,3-Dichlorobcnzene ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 NI) 20 Dichlorodifluoromcthanc ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 1,2-Dichlorocthanc ND 0.0050 ND 20 l,l-Dichloroethene ND 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 12-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1, 1 -Dichloropropene NI) 0.0050 ND 20 cis-1.3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 NI) 20 Ethvlbenzene ND 0.0050 ND 20 1lexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 NI) 20 Nlethylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzenc ND 0.0050 ND 20 - ' Styrene ND 0.0050 ND 20 1,1,1,2-Tetraehloroethane ND 0.0050 ND 20 1,1,2,2-Tetraehloroethane ND 0.0050 ND 20 Tetraehloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Triehlorobenzene NI) 0.0050 ND 20 1.2.4-Triehlorobenzene ND 0.0050 NI) 20 - 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane ND 0.0050 NI) 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethanc ND 0.0050 ND 20 1,2,3-Trichloropropane NI) 0.0050 ND 20 1,24-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride NJ) 0.0050 ND 20 Xylenes (total) Ni) 0.0050 ND 20 Surrogate: Dihromgfhroromethane 0.0479 0.0490' 97 74-122 Surrogate Toluene-d8 0.04S5 0.0490 98 05-128 Surroguie:4-Bromollnorohrn_ene 0.0452 0.0496 91 75-121 - ' The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 78 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (BlD0650-MS1) Source: 2102489-02 Analyzed: 04/24/21 04:12 Benzene 0.0404 0.0050 mgIg 0.0402 ND 101 37-145 Bromobenzene 0.0359 0.0050 0.0402 ND 89 29-147 Bromochloromethanc 0.0367 0.0050 0.0402 ND 91 40-145 Bromodichloromethane 0.0384 0.0050 0.0402 ND 96 39-153 Bromoform 0.0332 0.0050 0.0402 ND 83 32-143 Bromomethane 0.0467 0.0050 0.0402 ND 116 10-141 n-Butylbenzene 0.0324 0.0050 0.0402 ND 81 10-162 sec-Butylbenzene 0.0408 0.0050 0.0402 ND 102 14-168 tert-Butylbenzene 0.0388 0.0050 0.0402 ND 97 21-159 Carbon tetrachloride 0,0380 0.0050 0.0402 ND 95 28-148 Chlorobenzene 0.0394 0.0050 0.0402 ND 96 32-148 Chloroethane 0.0502 0.0050 0.0402 ND 125 11-166 Chloroform 0.0400 0.0050 0.0402 ND 100 40-139 Chloromethane 0.0350 0.0050 0.0402 ND 87 18-135 2-Chlorotoluene 0.0362 0,0050 0.0402 ND 90 25-151 4-Chlorotoluene 0.0363 0.0050 0.0402 ND 90 22-150 Dibromochloromethane 0.0359 0,0050 0.0402 ND 89 40-147 1,2-1)ibromo-3-chloropropane 0.0390 0.0050 0.0402 ND 97 25-158 1.2-Dibromoelhane (EDB) 0.0369 0.0050 0.0402 ND 92 38-147 Dibromomethanc 0.0319 0.0050 0.0402 ND 79 39-150 1,2-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 24-154 1,3-Dichlorobenzene 0.0369 0.0050 0.0402 ND 92 21-153 1,4-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 21-146 Dichlorodifluoromethanc 0,0188 0.0050 0.0402 ND 47 10-149 13-Dichloroethane 0.0420 0.0050 0.0402 ND 105 34-151 1,2-Dichloroethane 0.0400 0.0050 0.0402 ND 100 40-137 1, 1 -Dichloroethene 0.0449 0.0050 0.0402 ND 112 21-172 cis-1,2-Dichloroethene 0.0385 0.0050 0.0402 ND 96 38-147 trans-1,2-Dichloroethene 0.0409 0.0050 0,0402 ND 102 30-160 1,2-Dichloropropane 0.0397 0.0050 0.0402 ND 99 39-146 1,3-Dichloropropane 0.0396 0.0050 0.0402 ND 99 39-141 2.2-Dichloropropane 0.0280 0.0050 0.0402 ND 70 26-149 1, 1 -Dichloropropene 0.0385 0.0050 0.0402 ND 96 28-150 cis-1.3-Dichloropropene 0.0371 0.0050 0.0402 ND 92 34-149 trans-1,3-Dichloropropene 0.0384 0.0050 0.0402 ND 96 36-143 Etylbenzene 0.0397 0.0050 0.0402 0.00290 92 23-150 Ilexachlorobutadiene 0.0313 0.0050 0.0402 ND 78 10-192 4-Isopropyl Toluene 0.0385 0.0050 0.0402 0.00290 89 11-165 Isopropylbenzene 0.0406 0.0050 0.0402 0.00202 96 17-166 Methylene chloride 0,0456 0.0050 0,0402 ND 114 28-135 Naphthalene 0.0441 0.0050 0,0402 0.00948 86 10-174 n-Propylbenzene 0.0393 0.0050 0.0402 0.00310 90 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 79 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 .. Matrix Spike (B1D0650-MSI) Source: 2102489-02 Analyzed: 04/24/21 04:12 Styrene 0.0397 0.0050 mg/kg 0.0402 ND 96 24-154 1,1,1,2-Tetrachloroethane 0.0367 0.0050 0.0402 ND 91 38-149 1,1,2,2-Tetrachloroethane 0.0397 0.0050 0.0402 ND 96 22-164 - Tetrachloroethane (PCE) 0.0349 0.0050 0.0402 ND 87 25-153 Toluene 0.0376 0.0050 0.0402 ND 94 26-149 1,2,3-Triclilorobenzene 0.0323 0.0050 0.0402 ND 80 10-163 1,24-Trichlorobenzene 0.0323 0.0050 0.0402 ND 81 10-162 1, 1, 1 -Trichloroethane 0.0387 0.0050 0.0402 ND 96 34-149 1,1.2-Trichloroethane 0.0397 0.0050 0.0402 ND 99 25-175 Trichloroethene (TCE) 0.0386 0.0050 0.0402 ND 96 25-170 -� Trichlorotluoromethane 0.0497 0.0050 0.0402 ND 121 19-155 1,2,3-Trichloropropane 0.0403 0.0050 0.0402 ND 100 32-165 1,2.4-Trimethylbenzene 0.0466 0.0050 0.0402 0.0183 70 15-150 1,3,5-Trimethyl benzene 0.0413 0.0050 0.0402 0.00496 90 10-158 Vinyl chloride 0.0446 0.0050 0.0402 ND 111 22-148 Xylenes (total) 0.130 0.0050 0.120 0.0173 93 22-153 Surrogate: Dibronuolhuoromethane 0.0487 0.0502 97 74-122 _ . Surrogate: Toluene -A 0.0484 0.0502 96 65-128 Surrogaie:4-BromoJluorohenzene 0.0474 0.0502 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 80 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List F13A 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OF,C, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals by ICP 6010B STLC Cadmium S'rLC/EPA 601013 Water OEC. CA-ELAP 601013 STLC Chromium STLC/EPA 601013 Water OEC, C A-ELAP 60108 STLC Copper STLC/EPA 001013 Water OEC, CA-ELAP 6010B STLC Lead STLC/EPA 601013 Water OEC, CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601013 TCLP Chromium EPA 13111EPA 601013 Water OEC, CA-ELAP 601013 TCLP Lead EPA 1311/F,PA 601013 Water OEC. CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 81 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method t nalysis Method Matrix Laboratory & Certification Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA -FLAP Total Metals by ICP 601013 Total Antimony EPA 6010B Solid OEC, CA -FLAP 601013 Total Arsenic EPA 6010B Solid OEC, CA-ELAP 6010B Total Barium EPA 6010E Solid OEC, CA-ELAP 6010B Total Beryllium EPA 6010B Solid OEC, CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010B Total Chromium EPA 6010E Solid OEC. CA-ELAP 601013 Total Cobalt EPA 6010E Solid OEC, CA-ELAP 601013 Total Copper EPA 601013 Solid OEC, CA -FLAP 6010B Total Lead EPA 601013 Solid OEC, CA-ELAP 6010E Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 6010B Total Nickcl EPA 6010E Solid OEC, CA-ELAP 6010B Total Selenium EPA 6010B Solid OEC, CA-ELAP 6010B Total Silver EPA 6010B Solid OEC. CA-ELAP 6010E Total Thallium EPA 6010E Solid OEC, CA-ELAP 6010B Total Vanadium EPA 6010E Solid OEC, CA-E:LAP 6010B Total Zinc EPA 6010E Solid OEC_ CA-ELAP Volatile Organic Compounds by GC/MS 8260B Pull List EPA 8260B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 82 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OL'C, CA-ELAP 8015 TPH-Gasolinc EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPI-1-Gasoline EPA 8015M Solid OEC, Internal 8015 TPI I -Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 'ITH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasolinc EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 83 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Notesi Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-01 Analyte concentration exceeds TTLC. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below stale/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 84 of 94 EMSL Analytical, Inc. 464 McCormick Street San Leandro, CA 94577 Tel/Fax: (510) 895-3675 / (510) 895-3680 - http://www.EMSL.com / sanleandrolab@emsl.com Attention: Shahanaz Parvin Oilfield Environmental and Compliance 307 Roemer Way Suite 300 Santa Maria, CA 93454-1105 Project: 2102508 EMSL Order: 092105912 Customer ID: OILF50 Customer PO: 2102508 Project ID: Phone: (805) 922-4772 Fax: (805) 925-3376 Received Date: 04/26/2021 8:45 AM Analysis Date: 04/26/2021 Collected Date: 04/23/2021 Test Report: Asbestos Analysis of Bulk Materials via EPA 600IR-931116 Method using Polarized Light Microscopy Non -Asbestos Asbestos Sample Description Appearance % Fibrous % Non -Fibrous y_ % Type 2102508-16 Tan 50% Quartz None Detected Non -Fibrous 50% Non -fibrous (Other) 092105912-0001 Homogeneous _ 2102508-17 Gray 50% Quartz None Detected Non -Fibrous 40% Ca Carbonate 092105912-0002 Homogeneous 10% Non -fibrous (Other) Analyst(s) Gavin Lee (2) Cecilia Yu, Laboratory Manager or Other Approved Signatory EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 "Interim Method") but augmented with procedures outlined in the 1993 ("final") version of the method. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non -friable organically bound materials present a problem matrix and therefore EMSL recommends gravimetric reduction prior to analysis. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Estimation of uncertainty is available on request. Samples analyzed by EMSL Analytical, Inc San Leandro, CA NVLAP Lab Code 101048-3, WA C884 J Initial report from: 04/26/2021 13:36:56 ASB PL.M 0008 0001 - 1.78 Printed: 4/26/2021 1:36 PM Page 1 of 1 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2314.D Operator EW Acquired 23 Apr 2021 2:32 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-01@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 14 Response_ GOMD2314.D\FID1A 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 I 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2315.D Operator EW Acquired 23 Apr 2021 2:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-02@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 15 Response_ 85006 r 80000 75000 70000 65000 55000- i 50000 45000- I 40000; 350001 30000- 25000 20000 15000 10000 5000 GOMD2315.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2316.D Operator EW Acquired 23 Apr 2021 3:24 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-03@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 16 Response_ GOMD2316.DT1D1A 95000 90000 I I 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2317.D Operator EW Acquired 23 Apr 2021 3:50 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-04@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 17 Response- GOMD2317.D\FID1A 90000 i 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 ibhhh1 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2318.D Operator EW Acquired 23 Apr 2021 4:16 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-05@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 18 Response_ 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000- 45000 40000 35000 30000 25000 20000 15000 GOMD2318.D\FID1A 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2319.D Operator EW Acquired 23 Apr 2021 4:42 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-06@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 19 Response- GOMD2319.D\FID1A 90000 85000 80000 I 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2320.D Operator EW Acquired 23 Apr 2021 5:08 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-07@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 20 Response 95006 �. 90000 r 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2320.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2321.D Operator EW Acquired 23 Apr 2021 5:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-08@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 21 Response_ 85000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2321.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2322.D Operator EW Acquired 23 Apr 2021 6:00 pm using AcgMethod GASBTEXE.M Instrument GC7 �. Sample Name: 2102508-09@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 22 Res7. 90000! i 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2322.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2323.D Operator EW Acquired 23 Apr 2021 6:26 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-10@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 23 Response_ GOMD2323.D\FID1A 90000 85000 80000. 75000, 70000� I 65000! 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 1 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2328.D Operator EW Acquired 23 Apr 2021 8:35 pm using AcgMethod GASBTEXE.M Instrument GC7 .- Sample Name: 2102508-11@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 28 Response_ GOMD2328.D\FID1A 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 T I., - 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2329.D Operator EW Acquired 23 Apr 2021 9:01 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-12@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 29 Response GOMD2329.D\FID1A 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2330.D Operator EW Acquired 23 Apr 2021 9:27 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-13@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 30 Response_ 950001 90000 50000 45000 40000 35000• 30000 25000 20000 15000 10000 5000 GOMD2330.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2331.D Operator EW Acquired 23 Apr 2021 9:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-14@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 31 Response_ GOMD2331.D\FID1A I i 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 I 35000 30000 25000 4 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2332.D Operator EW Acquired 23 Apr 2021 10:18 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-15@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 32 Response_ 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2332.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 R,, 4t c A n $ c s �mp C M J M O Mc E V K ~ $PlloS Pomos1O Idol �iIN*o+roO to ro a G C1 C zoos ltlWoo s y 8Od l l"a a U ltlli4ellu61 � ►��+ _ OOLZ8. sOOAS W9L0>:OWOD' dNl a � � z .W o � o a e a .. d S, a spWnS 1 *pluvA3 angasea FE R c p191111nj 809ZB x 0 GP .c z ❑ +d+ 'r VV cr a. a sIg1N1 ZZ •1411 X y a`�UOd > .7� a❑ 10 to m g 12 Q cc -� I� m n' < C G ❑ ❑ v 0 Q g N tY U # M 2 ❑.•Y w E W a a� Z (�j G M of ❑ Lri/� :r •'�� �. a U „ v°1! a `� t N V7 CL 12 c CO U) z O V H Z a W a O\ a C h 00 Qo 0. 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Pr N v 32 �Ep Ct y r fiT W a W� o rt $ ` t a 00 v arJ? \ ! a. u a �t as e c c a! . a w U F F s � !3 �dv F p rt mJi GROS PDAPSIQ 1"01 �^ AIV4-00 Q O Q zoos /woos �• r 80d I Ls•d a � U 00M-SOOAS w4L08 OwI,O • dPll jC Z y iA m o CL ads a „ �, at *pW"S i *PJUVA0 aapatOa o F- E co d Z �A 1s11 Ilnd 808t8 X Y 0 z N vvs�� C sta•w - sc rs`, v� U CY Q p4 r ca s CL S L aa a L ; rx CL N < c - N i¢ 110 c j o Z Y::);:. K ®❑ r W e h � c 0 0 gigON _ $� a e F F 4 w o p CL E w ° s E n QF, cn a c cr g U F K � � 3~ to O a' W U ►�- ►= IZ i N z F V D ac N z g U w a a a 0 0 a w ,QW/j �4 0 1= 00 00 O UCd- 0 r'- < (-j z 0 -0 00 < U U 0 2 cq C, E 00 cli 0 r RT co -a 0 m C4 E u r-I on co E C-1 Z 00 z w 11 T y :R S Cn N 'tea 06 Page 91 of 94 -i rn LL r- N �2 = O aav �f Q ,cli CO to 9 CS a Y a �44 a J a a a s t) U d tL d d F d d F F .. t~ 0 i� c� v U` c) L) U` c`� a F U O C J F U J F- U J F U J F U J F U _1 F U J F U J F U J F U _j F U J F � cn CO cn (n cn V U) fPllos PfMoflO If3ol a a a zoos i If Me i. ead r iffd v � Lil1lQf11u61 0 OOLZ8'fOOA8 S 0yn� VMOSOMOD-dHl rya Z fpying m E pggq > cA 4,1111nd BOAZQ X ° Z linenZZ foll xi` m �❑ C , � CL n CL w < ® a' Lrn r DO c EDD❑ e F e V CA L ❑ N z Q QY m w W r l- N Y N OI r, in a M. ry 00 a Q r� m a a 0 a a rn �i E.w N •OWL. o0 L04 v mom CL O) A du js js r$ a: r1 d F .6a. ILv d ~ m U U v a m00 C F co on 00 co coco 1- ccC spllo8 WMof1Q Idol '4lMsau03 G 79081 W208 L Sod I Pod DOM iOOAS � $ w9 t•08 QWOfl • dHl .. CL K a �, at +ins 1 eplurAD *Apo**W m 1 ' 2 d + + lsl 1 and 808Z8 0 Z (� 3 o m- ❑ sln+w zz *all .c ❑ CD a N Ya a 1 4 E �g c N< cu c. ❑❑ V CK • r. � t U `� ►+ 0 Z ❑ .y o. H y ❑ a 33 z0 a . c V} GT I N V coo d T K c UC y a .� G G A C h Y p 01 D d r °° A 0. o� V IR •X o __ t % H _g r-- ❑ ❑ m in m _ a s T a c a s E a u N t0 C C c m 8. m E c C o a CC N LO O r-I N O O CIO O� 0 l`� t^• {4� m U v L; O CO 0 6C i U a w r O ui U M � M a v> C'! ol F E °O U a Old O �t � � N L � M !n o Q U N N cd 4 Q: C CS t{EQ,ii c�v z tom: O G C •� G M a (on O a E ol z a E 'a '2 S Ln N N .0 N � L c. Q N � g� fi N 2 a A Page 94 of 94 Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director msprister@occusa.com California ELAP Certification # 2438 Client Connect: client.oee.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Revision History Previous Report Reason for Revision 2102032 04/07/2021 16:45 Complete report. ale Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received " Sump Trench W 2102032-01 Solid Solid 04/06/2021 10:25 04/06/2021 11:30 Sump Trench Pile 2102032-02 Solid Solid 04/06/2021 10:26 04/06/2021 11:30 Sump Trench Bottom 2102032-03 Solid Solid 04/06/2021 10:30 04/06/2021 11:30 Fire Trench Bottoms 2102032-04 Solid Solid 04/06/2021 10:36 04/06/2021 11:30 - . Fire Trench W 2102032-05 Solid Solid 04/06/2021 10:38 04/06/2021 11:30 Fire Trench E 2102032-06 Solid Solid 04/06/2021 10:40 04/06/2021 11:30 Sample Batch Preparation Summary Analysis Batch ID Preparation Date lime STLC Metals by ICP 601 OB STLC B 1 D0494 04/ 16/2021 15:40 STLC Metals Extraction STLC Metals Extraction BID0313 04/12/2021 14:18 TCLP Metals by ICP 601 OB TCLP B1 D0495 04/16/2021 15:41 TCLP Metals Extraction TCLP Metals Extraction B1 D0312 04/12/2021 14:17 Total Metals by CVAA Mercury Total EPA 7471 A B I DO 153 04/07/2021 07:54 Total Metals by 1CP 601 OB Total B 1 DO 123 04/06/2021 12:15 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Sample ID: Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by : Lab ID: 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercun 0.097 0.091 mg+'kg 1 B I D0153 04/07/21 14:55 EPA 7471 A Total Metals by ICP Antimony 7.5 2.3 mg/kg 1 B 1 D0123 04/07/21 13:25 EPA 6010B Arsenic 9.4 1.9 " Barium 200 0.93 " Beryllium ND 0.46 " Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 " Copper 67 0.93 " Lead 380 0.46 N-02, N-03 Molybdenum 2.0 0.46 " Nickel 98 0.46 " Selenium ND 1.9 " Silver ND 0.46 " Thallium ND 0.93 " Vanadium 31 1.9 " Zinc 410 1.9 " STLC Metals by ICP Chromium 0.70 0.10 mgi'L 2 B 1 D0494 04!19/21 12:57 STLC/EPA 6010B - Lead 3.6 0.10 TCLP Metals by ICP Lead 0.23 0.050 mg/L 1 B1D0495 04/19/2114:01 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples 1. Sample ID : Sump Trench Pile Sampled: 04/06/21 10:26 ' Matrix: Solid Sampled by: Lab ID : 2102032-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.12 0.094 mg/kg 1 B 1 D0153 04/07/21 14:57 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I BID0123 04/07/2113:28 EPA 6010B Arsenic 7.4 1.9 Barium 280 0.95 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 12 0.47 Copper 38 0.95 Lead 180 0.47 N-02 N-03 Molybdenum 1.2 0.47 Nickel 78 0.47 " Selenium ND 1.9 " Silver ND 0.47 Thallium ND 0.95 Vanadium 37 1.9 Zinc 250 1.9 STLC Metals by ICP Chromium 0.39 0.10 mg/L 2 B1D0494 04/19/21 13:00 STLC/EPA601OB Lead 15 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.086 0.050 mg/I. 1 B 1 D0495 04/19/21 14:04 EPA 1311 /ERA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Sump Trench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by: Lab ID : 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg I B 1 D0153 04/07/21 14:59 EPA 7471 A Total Metals by ICP Antimonv 2.5 2.4 mglkg 1 B 1 D0123 04/07/21 13:31 EPA 601 OB Arsenic 7.0 1.9 Barium 230 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.48 Copper 72 0.97 Lead 140 0.48 " " " " " N-02 N-03 Molvbdenum 1.1 0.48 " Nickel 190 0.49 Selenium ND 1.9 Silver ND 0.48 " Thallium ND 0.97 Vanadium 34 1.9 " Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 m./L 2 BID0494 04/19/21 13:02 STLC/EPA6010B Lead 7.6 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 mg/L 1 B1D0495 04/19/21 14:06 EPA 1311 'EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oeuksa.cotn FAX: 805 925-3376 Page 5 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report i Sample ID: Fire Trench Bottoms Sampled: 04/06/21 10:36 Matrix: Solid Sampled by: Lab ID : 2102032-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mgtkg 1 B1 D0153 04/07/21 15:01 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mgtkg 1 B I D0123 04/07/21 13:34 EPA 601 OB Arsenic 6.6 1.8 Barium 220 091 " Beryllium 0.63 0.46 Cadmium ND 0.23 Chromium 52 0.46 Cobalt 18 0.46 Copper 26 0.91 Lead 9.4 0.46 Molybdenum 0.46 0.46 Nickel 110 0.46 Selenium ND 1.8 Silver ND 0.46 Thallium ND 0.91 Vanadium 34 1.8 Zinc 28 1.8 STLC Metals by ICP Chromium ND 0.10 mgiL 2 Bl D0494 04/19/21 13:13 STLC/EPA 6010B N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Fire Trench W Sampled: 04/06/21 10:38 ' Matrix: Solid Sampled by: Lab ID : 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.13 0.090 mg/kg 1 B1D0153 04/07/21 15:04 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1D0123 04/07/2113:37 EPA 6010B . Arsenic 4.8 1.9 Barium 130 0.96 Beryllium ND 0.48 " Cadmium ND 0.24 Chromium 41 0.48 Cobalt 9.0 0.48 Copper 22 0.96 Lead 27 0.48 Molybdenum 1.1 0.48 Nickel 50 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 34 1.9 Zinc 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 20 r A i A mms Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalvtical Sample ID: Fire Trench E Sampled: 04/06/21 10:40 Matrix: Solid Sampled by : Lab ID: 2102032-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.12 0.094 mglkg 1 BID0153 04/07/2115:06 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg,/kg 1 BID0123 04/07/2113:17 EPA 6010B Arsenic 6.4 1.9 Barium 170 0.94 Beryllium ND 0.47 . _ Cadmium ND 0.24 Chromium 49 0.47 Cobalt 12 0.47 ry Copper 26 0.94 Lead 32 0.47 Molvbdenum 1.2 0.47 Nickel 73 0.47 Selenium ND 1,9 Silver ND 0.47 " Thallium ND 0.94 Vanadium 36 1.9 Zinc 64 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals r Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0153 - EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 Blank (B1D0153-BLKI) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg/kg LCS (B1D0153-BS1) Analyzed: 04/07/21 13:07 Mercury 0.909 0.10 mg/kg 0.833 97 85-115 LCS Dup (BID0153-BSD1) Analyzed: 04/07/21 13:09 Mercury 0.799 0.10 mg/kg 0.833 96 85-115 1 20 Duplicate (B1D0153-DUPl) Source: 2101942-01 Analyzed: 04/07/21 13:17 Mercury 0.0118 0.087 mg/kg 0.0145 21 20 QR-04 Matrix Spike (B1D0153-MSI) Source: 2101942-01 Analyzed: 04/07/21 13:19 - Mercury 0.804 0.097 mg/kg 0.809 0.0145 98 75-125 Matrix Spike Dup (B1D0153-MSDI) Source: 2101942-01 Analyzed: 04/07/21 13:21 Mercury 0.776 0.092 mg/kg 0.765 0.0145 100 75-125 4 20 Post Spike (B1D0153-PSI) Source: 2101942-01 Analyzed: 04/07/21 13:23 Mercury 5.16 ug/1. 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ControlTotal Metals by 1CP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Blank (B1D0123-BLK1) Analyzed: 04/07/21 12:48 Antimony ND 2.5 nig/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND LO " Lead ND 0.50 " Molybdenum ND 0.50 " -- Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 " Thallium ND H) y Vanadium ND 2.0 Zinc ND 2.0 LCS (B1D0123-BS1) Analyzed: 04/07/21 12:53 ' Antimony 97.5 2.5 mg/kg 100 98 80-120 Arsenic 100 2.0 100 .100 80-120 Barium 103 1.0 100 103 80-120 Beryllium 100 0.50 100 100 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 100 0.50 100 100 80-120 Cobalt 102 0.50 100 102 80-120 - • Copper 98.3 1.0 100 98 80-120 Lead 102 0.50 100 102 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 - Selenium 99.8 2.0 100 100 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 1.0 100 102 80-120 Vanadium 96.7 2.0 100 97 80-120 Zinc 102 2.0 100 102 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by ' Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSDl) Analyzed: 04/07/21 12:56 Antimony 100 2.5 mglkg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 1.0 100 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 80-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 101 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 1.0 100 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 100 104 80-120 2 20 Duplicate (B1D0123-DUPl) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mg/kg 1.40 20 Arsenic 5.99 1.9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 ND 20 Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 Copper 26.5 0.97 26.5 0.2 20 Lead 29.1 0.48 32.0 13 20 Molybdenum 56.4 0.48 1.20 192 20 QR-04 Nickcl 68.5 0.48 73.4 7 20 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 Vanadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Matrix Spike (B1D0123-MS1) Source: 2102032-06 Analyzed: 04/07/21 12:58 Antimony 37.4 2.4 mg/kg 97.7 1.40 37 10-116 Arsenic 101 2.0 97.7 6.36 97 77-121 Barium 250 0.98 97.7 169 83 30-169 Beryllium 94.0 0.49 97.7 0.395 96 86-111 Cadmium 90.0 0.24 97.7 ND 92 81-112 Chromium 144 0.49 97.7 48.9 98 75-129 Cobalt 102 0.49 97.7 11.8 92 71-121 Copper 122 0.98 97.7 26.5 98 68-135 Lead 120 0.49 97.7 32.0 90 72-121 Molybdenum 87.1 0.49 97.7 1.20 88 70-112 Nickel 156 0.49 97.7 73.4 85 73-121 Selenium 91.5 2.0 97.7 ND 94 70-116 Silver 4.87 0.49 4.88 ND 100 54-132 Thallium 85.3 0.98 97.7 ND 87 64-120 Vanadium 131 2.0 97.7 36.2 97 78-124 Zinc 163 2.0 97.7 64.5 100 50-143 Matrix Spike Dup (B1D0123-MSD1) Source: 2102032-06 Analyzed: 04/07/21 13:01 Antimony 38.1 2.5 mg/kg 98.3 1.40 37 10-116 2 20 Arsenic 108 2.0 98.3 6.36 103 77-121 6 20 Barium 263 0.99 98.3 169 96 30-169 5 20 Beryllium 97.9 0.49 98.3 0.395 99 86-111 4 20 Cadmium 94.3 0.25 98.3 ND 96 81-112 5 20 Chromium 156 0.49 98.3 48.9 109 75-129 8 20 Cobalt 106 0.49 98.3 11.8 96 71-121 4 20 • Copper 130 0.98 98.3 26.5 105 68-135 6 20 Lcad 126 0.49 98.3 32.0 95 72-121 4 20 Molybdenum 91.2 0.49 98.3 1.20 91 70-112 5 20 Nickel 167 0.49 98.3 73.4 95 73-121 7 20 Selenium 96.0 2.0 99.3 ND 98 76-116 5 20 Silver 4.99 0.49 4.92 ND 102 54-132 2 20 Thallium 89.8 0.98 98.3 ND 91 64-120 5 20 Vanadium 137 2.0 98.3 36.2 102 78-124 4 20 Zinc 167 2.0 98.3 64.5 104 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 20 161*ROilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PS1) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-12.5 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.88 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.559 WI 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 •- Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 \anadium 2.68 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 20 r A tnrd!!J�a� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 STLC Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0494 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 10:40 Blank (BlD0494-BLK1) Analyzed: 04/19/21 12:12 Chromium ND 0.050 mg/l. Lead ND 0.050 11 LCS (BlD0494-BSl) Analyzed: 04/19/21 12:23 Chromium 9.69 0.050 mg/L 10.0 Lcad 9.80 0.050 1110.0 LCS Dup (BlD0494-BSDI) Analyzed: 04/19/21 12:25 Chromium 9.72 0.050 mg/L 10.0 Lead 9.71 0.050 1110.0 Duplicate (BlD0494-DUPl) Source: 2101759-01 Analyzed: 04/19/21 12:46 Chromium 120 0.050 mg/L 112 Lead 54.3 0.050 1151.6 Leach Fluid Blank (B1D0494-LBK1) Analyzed: 04/19/21 12:15 Chromium ND 0.10 mg/L Lead ND 0.10 " Leach Fluid Blank (BlD0494-LBK2) Analyzed: 04/19/21 12:17 Chromium ND 0.10 mg/L Lead ND 0.10 Matrix Spike (BlD0494-MSl) Source: 2101759-01 Analyzed: 04/19/21 12:28 Chromium 116 0.10 mg/L 10.0 112 Lead 59.4 0.10 1110.0 51.6 Matrix Spike Dup (B1D0494-MSDl) Source: 2101759-01 Analyzed: 04/19/21 12:38 Chromium 134 0.10 mg/L 10.0 112 Lead 68.2 0.10 1110.0 51.6 97 80-120 98 80-120 97 80-120 0.3 20 97 80-120 1 20 6 20 5 20 42 89-115 78 86-114 Q11-4X QM-4X 214 89-115 14 20 QN14X 166 86-114 14 20 QN14X The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (B1D0495-BLKl) Analyzed: 04/19/21 13:46 Lead ND 0.050 mg/L LCS (BlD0495-BSl) Analyzed: 04/19/21 13:26 Lead 9.76 0.050 mg/I. 10.0 98 80-120 LCS Dup (BlD0495-BSDI) Analyzed: 04/19/21 13:28 Lcad 9.71 0.050 mg/L 10.0 97 80-120 0.5 20 Duplicate (B1D0495-DUPl) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lead ND 0.050 mg/L ND 20 Leach Fluid Blank (BlD0495-LBKI) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/L Leach Fluid Blank (B1D0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/I. Matrix Spike (B1D0495-MS1) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lcad 10.1 0.050 mg/L 10.0 ND 101 86-114 Matrix Spike Dup (BlD0495-MSD1) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lead 9.84 0.050 mg/L 10.0 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of20 '--t Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Sample Method Summary lnalysis Method Matrix Laboratory & Certification STLC Metals by ICP 6010B STLC Chromium STLC/EPA 6010B Water OEC. CA -FLAP 601 OB STLC Lead STLC/EPA 0010B Water OEC, CA -FLAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC. Internal TCLP Metals by ICP 601013 TCLP Lead EPA 1311/E.PA 6010B Water OEC, CA-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471A Solid OEC, CA-ELAP Total Metals by ICP 6010B Total Antimony EPA 6010B Solid OF.C, CA -FLAP 6010B Total Arsenic EPA 6010B Solid OEC_ CA-ELAP 0010B Total Barium EPA 6010B Solid OEC, CA-ELAP 6010B Total Beryllium EPA 601 OB Solid OEC. C A-ELAP 601 OB Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010B Total Chromium EPA 6010B Solid OEC, CA-ELAP 6010B Total Cobalt EPA 6010B Solid OEC, CA-ELAP 6010B Total Copper EPA 6010B Solid OEC, CA -FLAP 6010B Total Lead EPA 6010B Solid OEC, CA-ELAP 6010B Total Molybdenum EPA 6010B Solid OEC. CA-ELAP 6010B Total Nickel EPA 6010B Solid OEC, CA -FLAP 6010B Total Selenium EPA 6010B Solid OEC. CA-ELAP 601013"Total Silver EPA 6010B Solid OEC, CA -ELAN 601 OB Total Thallium EPA 6010B Solid OEC, CA-ELAP 6010B Total Vanadium EPA 601 OB Solid OEC, CA-ELAP 001013 Total Zinc EPA 601 OB Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Notes and Definitions Qualifier Definition MD1, Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 20 4 'Q C M S b m log F F cc E m�� sPIIoS paAloslO Isiol J �MsouoO a ro ro A p G G coos / VMS L « BOd ! lead d 411anluel U � � U = a OOLL9'600AS a L $' °1� WQ M 0W 0D - dHl zCL E m i T « apWnS 1 aplusLO anpasaa Z +� w a +� [. '� lsn Ilnd Booze Z ♦+ �y � � A L i O ❑ :+ r n slsiaW • ZZ s1311 y m r .c ❑ 7 >4 a Or m Or n E N Q C. g ❑❑ n d F F ❑0.i �:•❑ ci Un ^+ Z ❑ -> C m •S c ,mC m a o p L C E� f m Z0 a a o° v w 3 3N m P x no } i h � g et rl Lu N N J� OG �. 0. E Oa ry u qno N coi. 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E a) co 0 U) V LLI 0 I Z U xQ J r UU UU UIL U o ® U J~ JU JV J 1= 0 0 E mt� HUH �� E— p�, e J U) � -1 U) -j XU) U) -- XU) U) X =�j m XU) sPilos PSN0910 1e101 .J MAlsou00 m m a c o ZSOS / VMS f. 90d I lsed 0 U 5 ftA1gs31u01 � C Q N OO1Z8-s00AS � U o J � ' !6 w q O N WS308OW0J-dHl z to o o N 0 n m >z o 'm y `a *MSS 1 SPIus60 sAposea F- Evy a Z �, isle Ilnd 90SZ8 Z N � "� .0 is � ,� ❑ a 'vi U d d a %stew ZZ Simi m m JT41, 13 0. QN E N Q c 3 d ° U c. U a u ie W m N 0 Z V E P �° F x a y g Lr4}� r• � p � V y< V4Q� i y d � C, A. O °.° U uul ;;, ❑ ❑ to '�D a � C � � �� -,� E 3 w u I'- A N I t L1 w i Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director msprister(Ooecusa. com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Drcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by : Lab ID: 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.097 0.091 mglkg 1 B 1 DO153 04/07/21 14:55 EPA 7471 A Total Metals by ICP Antimony 7.5 2.3 mg/kg 1 B I D0123 04/07/21 13:25 EPA 601 OB ^ Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 " " " " " N-02, N-03 Molybdenum 2.0 0.46 Nickel 98 0.46 " Selenium ND 1.9 " Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium 0.70 0.10 mg/L 2 BID0494 04!19/21 12:57 STLC/EPA 601 OB Lead 3.6 0.10 TCLP Metals by ICP _ Lead 0.23 0.050 mg/L 1 BID0495 04/19/21 14:01 EPA 1311/EPA601OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of20 AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Sample ID : Sump Trench Bottom Sampled: 04/06/21 10:30 ' Matrix: Solid Sampled by: Lab ID : 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B1D0153 04,107/2114:59 EPA 7471A Total Metals by ICP Antimony 2.5 2.4 rng/kg 1 131DO123 04/07/21 13:31 EPA 6010B .— Arsenic 7.0 1.9 Barium 230 0.97 " Beryllium ND 0.48 Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.48 Copper 72 0.97 Lead 140 0.48 N-02, N-03 Molybdenum 1.1 0.48 Nickel 190 0.48 " Selenium ND 1.9 " Silver ND 0.48 " Thallium ND 0.97 Vanadium 34 1.9 Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 mg/l. 2 B1D0494 04/19/21 13:02 STLC/EPA601OB Lead 7.6 0.10 " " " " " N-07 TCLP Metals by 1CP Lead 0.10 0.050 mg/L 1 B 1 D0495 04/19/21 14:06 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Fire Trench W Sampled: 04/06/21 10:38 Matrix: Solid Sampled by: Lab ID: 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Line 0.13 0.096 mg/kg 1 B I D0153 04/07/21 15:04 EPA 7471 A ND 2.4 mg/kg 1 B 1 D0123 04/07/21 13:37 EPA 60I OB 4.8 1.9 130 0.96 ND 0.48 ND 0.24 41 0.48 9.0 0.49 22 096 27 0.48 1.1 0.48 50 0.48 ND 1.9 ND 0.48 ND 0.96 34 1.9 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.aecusa.corn FAX: (805) 925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0153 - EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 T- Blank (B1D0153-BLK1) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg/kg LCS (B1D0153-BS1) Analyzed: 04/07/21 13:07 Mercury 0.809 0.10 mg/kg 0.833 97 85-115 LCS Dup (BID0153-BSD1) Analyzed: 04/07/21 13:09 Mercury 0.799 0.10 mg/kg 0.833 96 85-115 1 20 Duplicate (B1D0153-DUPI) Source: 2101942-01 Analyzed: 04/07/21 13:17 Mercury 0.0118 0.087 mg/kg 0.0145 21 20 QR-04 Matrix Spike (B1D0153-MS1) Source: 2101942-01 Analyzed: 04/07/21 13:19 Mercury 0.904 0.097 mg/kg 0.809 0.0145 98 75-125 Matrix Spike Dup (BID0153-MSDI) Source: 2101942-01 Analyzed: 04/07/21 13:21 Mercury 0.776 0.092 mg/kg 0.765 0.0145 100 75-125 4 20 Post Spike (B1D0153-PSI) Source: 2101942-01 Analyzed: 04/07/21 13:23 Mercury 5.16 ug/L 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSD1) Analyzed: 04/07/21 12:56 Antimony 100 2.5 mgIg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 LO 100 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 80-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 101 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 1.0 100 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 100 104 80-120 2 20 Duplicate (B1D0123-DUPl) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mglkg 1.40 20 Arsenic 5.99 1.9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 ND 20 Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 Copper 26.5 0.97 26.5 0.2 20 Lead 28.1 0.48 32.0 13 20 Molybdenum 56.4 0.48 1.20 192 20 QR-04 Nickel 69.5 0.48 73.4 7 20 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 \anadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PSI) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.88 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.558 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 Vanadium 2.68 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center ' Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TCLP Metals by ' Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 _ Blank (BlD0495-BLKI) Analyzed: 04/19/21 13:46 Lead ND 0.050 mg/1_ LCS (BlD0495-BS1) Analyzed: 04/19/21 13:26 Lead 9.76 0.050 mg/l. 10.0 LCS Dup (BlD0495-BSDl) Analyzed: 04/19/21 13:28 Lcad 9.71 0.050 mg/L 10.0 Duplicate (B1D0495-DUPl) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lcad ND 0.050 mg/I. Leach Fluid Blank (B1D0495-LBK1) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/L Leach Fluid Blank (BlD0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/L. Matrix Spike (BlD0495-MSI) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lcad 10.1 0.050 mg/L 10.0 Matrix Spike Dup (B1D0495-MSDl) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lead 9.84 0.050 mg/I. 10.0 98 80-120 97 80-120 0.5 20 ND 20 ND 101 86-114 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Notes i Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above 1 Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and or LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 wvvw.oecusa.com FAX: 805 925-3376 Page 17 of 20 > E \ / @ E \ 6 z \ { \ \ \ - � � k E 2 / / CD 0 z z � \ / § z z co o & § 0 { a ) # < m � / A s = \ $ $ ) (L ) / E ) ) $ / I 0 A _ § £ -a7 f u o ? a o 0 « o E O G 3 3 < z z ) & k k IL 0 ■ ■ » ■ > » » > ■ > E )\ 3 / 0 £ = a / � CD 0 0 §�` — �2§ § a 0 2 0 §2)J«\ o �) J 0 > o I _ 2 g \ 0 2 m 2 0 3 -j o 2 2 /) ) { E K/ 3 0 E 3 ) ) k § 3 .0 cc\ 7 m erz )/ < I4 C 0 Co o »o .D J/kf) JE�E{])2\ } p 7 0 7[ 2& D — a E\« S k r K A 3 $ # a ® o ±2=oe \ \ k < ( k )_ ) )) « ) w rL E 0 k E 2 a a U U UJ U m �V J~J~J~ J I.- C3 d E m t o E �U CO HU vJ F-J cn H Un 0 = XU) xco XU) X sPilos peAlosla 11401 /(1iMsouo� ro w oaf � a c o zoos I V68oF L « sod / lsed 0 U x� - 411gsilu6l e g v CODOM ¢ - 93OAS a L � O N WQLoo onao • dmi � PC"� O •• E� is a eawns 1 oplue6o eApasea F E L m ai _0 Q ;sll Ilnd So9ZQ 2 N G 0 ° U UC� x a sinew - ZZ *mi a r/� O d OL Y c ❑ • • J nN a ��QTD T C" Co] Fng'- 7 m i7 ILJ y$ m � t N °° _ _:. o a 4 ca a a o°g ■ ° 41 r N xto. to g cr V o � a n rn c N Gi O �µEj1 Gp L Q � p r,a � ❑ ❑ m m m N Q Q c ' 44 WI u 6 Z O F- U y Z Q U al a Un Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: 1*6(A� CAI� Meredith Sprister, Business Director mspristcr@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report Sample ID : Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by : Lab ID : 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.097 0.091 mg/kg 1 B1D0153 04/07/2114:55 EPA 7471A Total Metals by ICP Antimonv 7.5 2.3 mg/kg 1 B I D0123 04/07/21 13:25 EPA 6010B -� Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 N-02 N-03 (Molybdenum 2.0 0.46 Nickel 98 0.46 Selenium ND 1.9 " Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium 0.70 0.10 mg/L 2 BID0494 04/19/2112:57 STLC/EPA6010B Lead 3.6 0.10 TCLP Metals by ICP Lead 0.23 0.050 mg/L 1 B 1 D0495 04/19/21 14:01 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report t Sample ID : Sump Trench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by: Lab ID : 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg'kg 1 Bl D0153 04/07/21 14:59 EPA 7471 A Total Metals by ICP Antimony 2.5 2.4 mg/kg 1 B1 D0123 04/07/21 13:31 EPA 6010B Arsenic 7.0 1.9 Barium 230 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.48 Copper 72 0.97 Lead 140 0.48 " " " " " N-02, N-03 Molvbdenum 1.1 0.48 Nickel 190 0.48 Selenium ND 1.9 Silver 1 ND 0.48 Thallium ND 0.97 " Vanadium 34 1.9 Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 BID0494 04/19/2113:02 STLC/FPA6010B Lead 7.6 0. I U " " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 mg/L 1 B1 D0495 04/19/21 14:06 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analvtical Report for Samples Sample ID: Fire Trench W Sampled: 04/06/21 10:38 Matrix: Solid Sampled by : Lab ID: 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.13 0.096 mglkg 1 BID0153 04/07/21 15:04 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 D0123 04/07/21 13:37 EPA 6010B ' Arsenic 4.8 1.9 " Barium 130 0.96 Beryllium ND 0.48 ., Cadmium ND 0.24 Chromium 41 0.48 Cobalt 9.0 0.48 -, Copper 22 0.96 Lead 27 0.48 Molybdenum 1.1 0.48 Nickel 50 0.48 Selenium ND 1.9 Silver ND 0.48 - . Thallium ND 0.96 Vanadium 34 1.9 Zinc 62 1.9 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: i8051925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 i Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0153 - EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 Blank (B1D0153-BLKI) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg1kg LCS (B1D0153-BSI) Analyzed: 04/07/21 13:07 Mercury 0.809 0.10 mg/kg 0.833 97 85-115 LCS Dup (B1D0153-BSDI) Analyzed: 04/07/21 13:09 Mercury 0.799 0.10 mg/kg 0.833 96 85-115 1 20 Duplicate (B1D0153-DUPl) Source: 2101942-01 Analyzed- 04/07/21 13:17 Mercury 0.0118 0.087 mg/kg 0.0145 21 20 QR-04 ., Matrix Spike (B1D0153-MS1) Source: 2101942-01 Analyzed: 04/07/21 13:19 Mercury 0.904 0.097 mg/kg 0.909 0.0145 98 75-125 Matrix Spike Dup (B1D0153-MSD1) Source: 2101942-01 Analyzed: 04/07/21 13:21 Mercury 0.776 0.092 mg/kg 0.765 0.0145 100 75-125 4 20 Post Spike (B1D0153-PS1) Source: 2101942-01 Analyzed: 04/07/21 13:23 Mercury 5.16 ug/1. 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total' Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0123 -EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSDl) Analyzed: 04/07/21 12:56 Antimony too 2.5 mg/kg 100 100 80-120 3 20 Arsenic 103 2.0 too 103 80-120 2 20 - Barium 105 1.0 too 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 .0.25 too 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 .� Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 too 80-120 2 20 Lead 104 0.50 too 104 80-120 2 20 Molybdenum 101 0.50 100 lot 80-120 3 20 . - Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 _ Thallium 105 1.0 too 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 too 104 80-120 2 20 . Duplicate (B1D0123-DUPl) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mg!kg 1.40 20 Arsenic 5.99 1.9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 NI) 20 Chromium 53.2 0.48 " 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 ^� Copper 26.5 0.97 26.5 0.2 20 Lcad 29.1 0.48 32.0 13 20 Molybdenum 56A 0.48 1.20 192 20 QR-04 Nickel 68.5 0.48 73.4 7 20 Selenium ND 1.9 ND 20 Silver ND 0.48 " NI) 20 Thallium ND 0.97 ND 20 Vanadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TotalControl Analyte Result RL Units Spike Source %REC %REC "D RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PS1) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.98 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 r+ Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.559 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 Vanadium 2.68 2.00 0,763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX (8051925-3376 Page 13 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TCLP Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (B1D0495-BLK1) Analyzed: 04/19/21 13:46 Lead ND 0.050 mg/L LCS (B1D0495-BSI) Analyzed: 04/19/21 13:26 Lead 9.76 0.050 mg/l. 10.0 98 80-120 LCS Dup (BlD0495-BSD1) Analyzed: 04/19/21 13:28 Lead 9.71 0.050 mg/L 10.0 97 80-120 0.5 20 Duplicate (BlD0495-DUPl) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lcad ND 0.050 mg/L ND 20 Leach Fluid Blank (BlD0495-LBK1) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/l. Leach Fluid Blank (BlD0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/L Matrix Spike (BlD0495-MSI) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lead 10.1 0.050 mg/l. 10.0 ND 101 86-114 Matrix Spike Dup (BlD0495-MSDI) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lead 9.84 0.050 mg/L 10.0 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA93454 www.oecusa.com FAX: (8051 925-3376 Page 15 of 20 r AL trzm Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Notesi Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and or LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC; control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 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Clarence Reynolds OEC Work Order: 2101841 Pacific Petroleum California P. O. Box 2646 Report Date: April 06, 2021 16:03 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Centers, 2600 Broad St. Enclosed is an analytical report for the above referenced project. The samples included in this report were received on March 25, 2021 15:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director mspristcr@oecusa.com California ELAP Certification # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 922-4772 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Revision Previous Report Reason for Revision 2101841 03/26/2021 17:07 Complete report. Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Tank NWall 2101841-01 Solid Solid 03/25/202111:15 03/25/2021 15:00 Tank S Wall 2101841-02 Solid Solid 03/25/2021 11:20 03/25/2021 15:00 Tank E Wall 2101841-03 Solid Solid 03/25/2021 11:25 03/25/2021 15:00 Tank W Wall 2101841-04 Solid Solid 03/25/2021 11:30 03/25/2021 15:00 ' Tank Bottom E. End 2101841-05 Solid Solid 03/25/2021 11:05 03/25/2021 15:00 Tank Bottom W. End 2101841-06 Solid Solid 03/25/2021 11:10 03/25/2021 15:00 Sump Trench W 2101841-07 Solid Solid 03/25/2021 11:35 03/25/2021 15:00 Sump Trench S 2101841-08 Solid Solid 03/25/2021 11:38 03/25/2021 15:00 Control 2101841-09 Solid Solid 03/25/202111:00 03/25/2021 15:00 Soil Pile N 2101841-10 Solid Solid 03/25/2021 11:40 03/25/2021 15:00 Soil Pile S 2101841-11 Solid Solid 03/25/2021 11:45 03/25/2021 15:00 Soil Pile W 2101841-12 Solid Solid 03/25/2021 11:50 03/25/2021 15:00 Soil Pile E 2101841-13 Solid Solid 03/25/2021 12:10 03/25/2021 15:00 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 2 of 79 161*44 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Batch Preparation Analysis Batch ID Preparation Date/Time Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B1('0798 03/25/2021 17:29 STLC Metals by ICP 6010B STLC BID0007 04/01/2021 09:01 STLC Metals Extraction STLC Metals Extraction B1('0891 03/30/,2021 10:02 TCLP Metals by ICP 6010B TCLP B 1 DO 112 04/06/2021 10:26 TCLP Metals Extraction TCLP Mcials Extraction B I C0898 03/30/2021 12:22 Total Metals by CVAA Mercury Total EPA 7471 A B I C0807 03/26/2021 07:43 Total Metals by ICP 6010B Total B 1 C0810 03/26/2021 08:36 Volatile Organic Compounds by GUMS 826011 Full List B I C0815 03/26,2021 09:17 8260B Full List BIC0817 03/26/2021 11:40 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B 1('0802 03/26/2021 05:22 8015 TPH-Gasoline 131C0804 03/26/2021 0526 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 tng1g I B1C0807 03/26/21 14:37 EPA 7471A Total Metals by ICP Antimony ND 2.4 mgtkg 1 B 1 C0810 03/26/21 13:30 EPA 6010B - Arsenic 8.9 2.0 Barium 150 0.98 Bervilium 0.61 0.49 Cadmium ND 0.24 Chromium 51 0.49 " " " N-02 Cobalt 17 0.49 " " •-, Copper 28 0.98 Lead 9.1 0.49 Nlolvbdenum 2.6 0.49 �. Nickel 76 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 39 2.0 " Zinc 32 2.0 " STLC Metals by ICP Chromium 0.13 0.10 mg/l. 2 B1D00(17 04/01/21 14:45 STLC/EPA6010B Volatile Organic TPH by GC/FID TPI1 Gasoline (C5-C12) ND 4.9 mg/kg 1 B1('0802 03/26/21 10:47 EPA SO ISM R-07 Surrogate: 4-Bromo/luoroben_ene 103 %'o ( 31 - 168) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 4 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg I BIC0798 03/26/21 07:48 EPA 8015M TPII Motor Oil (C23-(`40) ND 50 11 11 11" 11 Surrogate: o-TetphenYl 107 `N, (65 - 133) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 n 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank N Wall Sampled : 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mgtkg 1000 BIC0815 03/2621 11:52 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 12 „ n-Propylbenzene ND 12 " Styrene ND 1.2 1,I,1.2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 " Tetrachloroctliene (PCE) ND 1.2 Tolucnc ND 1.2 1,2,3-Trichlorobenzene ND 12 1,2,4-Trichlorobenzene ND 1.2 L1,1-Trichlomethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 " Frichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 12 1,2.3-Trichloropropane ND 1.2 " 1.2,4-Trimethylbenzene ND 1.2 " 1,3,5-Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 " " Xylcnes (total) ND 1.2 " Smrogate: Dibromo/luoromethane 97 % ( 75 - 122) " Surrogate: Toluene-db' Surrogate: 4-Bron t u/laoro ben= crt e 92% (66-128) 92 ":, (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by : Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.086 mg/kg I B1('0807 03/26/2114:39 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg kg 1 B I C0810 03/26/2) 13:33 EPA 601(1B Arsenic 4.1 2.0 Barium 11 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 9.0 0.49 Cobalt 1.4 0.49 " Copper 3.5 0.99 Lead 2.5 0.49 Molybdenum 3.3 0.49 Nickel 6.8 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 6.3 2.0 Zinc 9.7 2.0 " Volatile Organic TPH by GC/FID TPII Gasoline (C5-02') ND 4.5 mglkg 1 BIC0802 03/26'21 11:13 EPA 8015M R-07 Surrogate: 4-Bromo/Inorohen::ene 103 ` (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (Cl 3-C22) ND 10 mg/kg 1 B I ('0798 03/26/21 10:07 EPA 8015M TPH Motor Oil (('23-C40) ND 50 " " " 11 Surrogate: o-Terphenyl 106',';, (65 - 133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.oecusa.corn FAX: (805) 925-3376 Page 8 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgticg 1000 B 1 C0815 03/26/21 12:17 EPA 8260B T' Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-1utylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene NU 1.2 . - Chloroethanc ND 1.2 Chloroform ND 1.2 Chloronuthane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibronxiethane (FDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 " 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromcthanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 12-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1. 1 -Dichloropropene ND 1.2 cis- I .3-Dichloropropene ND 1.2 trans-1,3-Uichhiropropcne NU 1.2 Fthylbcnzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by : Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg'kg 1000 B I C0815 03/26/21 12:17 EPA 926013 ~ 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 " - Naphthalene ND 1.2 n-Propylbenzene ND L2 " Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2=letrachloroethanc ND 1.2 Tetrachlorocthcnc WCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 ' 1,1,2-Trichloroethane ND 1.2 Trichlorocthenc (TCE) ND 1.2 Trichlorofluoromethanc ND 1.2 1,2.3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride f ND 1.2 Xylencs (total) ND 1.2 Surrogate: I)ihromnihioromethanc 92 % (75.- 122) " Surrogate Toluene-dX 84 ';% (66 - 12S ) " Surrogate: 4-Rromolhroroben_ene 92 IN The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 79 OamAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA i Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg 1 B 1('0807 03/26/21 14:41 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mglkg 1 BIC0810 03/26/21 13:36 EPA 6010B • Arsenic 4.2 L9 Barium 140 0.95 Bervllium 0.51 0.47 -� Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 16 0.47 Copper 23 0.95 Lead 7.0 0.47 Molybdenum ND 0.47 - , Nickel 72 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 33 1.9 Zinc 20 1.9 STLC Metals by ICP Chromium ND 0.10 mg/L 2 BID0007 04/O1/2114:48 STLC/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (('5-C 12) ND 4.0 mg/kg 1 131 CONO2 03/26121 11:39 EPA 8015M R-07 Surrogate: 4-13roniglluorohen�ene 1114 (31 - 168) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 11 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID: 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 9.9 mg/kg l B I C'0798 03/26/21 08:02 IPA 8015M TPH Motor Oil (C23-('40) ND 50 1. 11 11" 11 Surrogate: o-Te)phenll 108 `% (05 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.oecusa.cam FAX: 805 925-3376 Page 12 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B1C0815 03/26/2112:43 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromcthane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 " Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 ^ 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 1.2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 14-Dichlorobenzenc ND 1.2 Dichlorodifluoromcthane ND 1.2 " 1,1-Dichloroethane ND 1.2 12-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 • cis-L2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1,1-Dichloropropane ND 1.2 cis-1,3-Dichloropropenc ND 1.2 trans-1,3-Dichloropropenc ND 1.2 L'thylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922- 4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples — Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID: 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 I lexachlorobutadiene ND 1.2 mgtkg 1000 B 1('0815 03/26/21 12:43 EPA 9260B 4-Isopropyl Toluene ND 1.2 Isopmpylbenzene ND 1.2 Methvlene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1.1,2-fetrachloroethane ND 1.2 1.1,22-1'etrachloroethanc ND 1.2 Tctrachlorocthcnc (ICE) ND 1.2 " Toluene NI) 1.2 1,2,3-Trichlorobcnzcne ND 1.2 1,24-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 12.4-I'rimethylbenzene ND 1.2 1,3,5-I'rimethylbeuzenc ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibrnmolhmromethanr 92 % ( 75 - 122 ) Surrogate: Toluene-d8 95 % ( 66 - 128 ) Surrogate: 4-8romnJ toroben_enc 90 4a (76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report i Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg 1 B1('0807 03/26/21 14:44 EPA 7471A Total Metals by ICP Antimony ND 2.3 mg%kg 1 Bl('0810 03/26/21 13:38 EPA 601OB Arsenic 2.6 1.8 Barium 5.8 092 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 6.9 0.46 Cobalt 0.92 OA6 — Copper 1.9 0.92 Lead 3.7 0.46 " Molybdenum 2.6 0.46 " Nickel 4.1 0.46 Selenium ND L8 Silver ND 0.40 Thallium ND 0.92 " Vanadium 4.6 1.8 Zinc 6.8 LS Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) 35 5.1 mg!kg I BIC0802 03/26/21 12:05 EPA 8015M Surrogate: 4-13ronwflumwbenzene 1.16 0;, (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 17 9.9 mg/kg I BIC0798 03126'21 11:03 EPA 8015M 0-04 " TPH Motor Oil (C23-C40) 72 50 D-04 Surrogate: o-Tcrphen l 107 3b (65 - 133 ) —1 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B1C0815 03/26/21 13:08 EPA8200B Bromobenzene ND 1.2 " Bromochlorometliane ND 1.2 Bromodichloromethane ND 1.2 -, Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromcthane ND 1.2 " ` 2-C'hlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronto-3-chloropropane ND 1.2 1.2-Dibromoethane (F.DB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 IA-Dichlorobenzene ND 1.2 Dichlorodifluoromethanc ND 1.2 ' 1. 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 - cis- 1,2-Dich loroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 1.3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 I,1-Dichloropropene NI) 1.2 cis-1,3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropc11c ND 1.2 Iithylbcnzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX::805; 925-3376 Page 16 of 79 i Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 B 1('0815 03/26/21 13:08 EPA 9260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 I,1,1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 1'etrachlorocthene (ICE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2A-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND L2 " Trichloroethane (TCE) ND 1.2 Trichlorotluoromethane ND 1.2 1.23-Trichloropropane ND 1.2 " 1,24-Trimethylbenzene ND 1.2 1,35-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dilnzmwfluoronu•thalle 95 '', ( 75 - 122 ) Sturrogatc: Toluenc-d8 95 " 6 ( 66 - 128) Surrogate: 4-Bromo%lu[n iben_ene 92 io ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 79 r A VA alft Oilfield Environmental &Compliance, Inc. INZW=�W Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical t Sample ID : Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mgtkg 1 B1('0807 03/26/21 14:46 EPA7471A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B 1 C0810 03/26/21 13:41 EPA 601 OB Arsenic 5.4 1.9 Barium 32 0.93 Beryllium ND 0.47 r Cadmium ND 0.23 Chromium 15 0.47 Cobalt 4.3 0.47 Copper 11 0.93 Lead 8.3 0.47 Molybdenum 2.9 0.47 Nickel 19 0.47 Selenium ND 1.9 Silver ND 0.47 " _ Thallium ND 0.93 Vanadium 13 1.9 " Zinc 19 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 35 4.9 mg/kg I BIC0802 03/26/21 12:31 EPA 8015M Surrogate: 4-Brontg1hmrohenzene 145 % (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-TerphenYl 11 10 mg/kg I 110 50 " " 106% (65-133) BIC0798 03/2621 11:31 EPA 8015M D-04 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 187 �^r Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by: Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mglkg 1000 B 1('0815 03/26/21 13:34 FPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromotiorm ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene NU 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-ehloropropane NI) 1.2 1.2-Dibromoethane (N)B) ND 1.2 Dibromomethanc ND 1.2 1,2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 14-Dichlorobcn7cnc ND 1.2 Dichloroditluoromcthane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Diehloroethene ND 1.2 cis-1,2-Diehloroethene ND 1.2 trans-l.2-Diehloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1. 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 F.thylbcnzene ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by: Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 llexachlorobutadiene ND 1.2 mg/kg 1000 B1('0815 03/26/21 13:34 EPAR260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 I.1,1,2-Tetrachloroethane ND 1.2 1.1,2,2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzcne ND 1.2 1.2,4-Trichlorobenzene ND 1.2 1.1.1-Trichloroethane ND 1.2 1,12-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1.2,3-Trichloropropane ND 1.2 1.24-Trinethylbenzene ND 1.2 13.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Uihromolhmromethane 95 1%6 (75 - 122) " Surrogate: Toluene-db' 86 % (66 - 128 ) Surrogate: 4-Bromn/luorohencene 94 `,':, ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.091 mgncg I B I C0807 03/26/21 14:48 EPA 7471 A Antimony ND 2.4 mg/kg 1 B I C0810 03/26/21 13:44 EPA 601(IB -, Arsenic ND 2.0 Barium 9.9 0.98 " Beryllium ND 0.49 " Cadmium ND 0.24 Chromium 8.0 0.49 Cobalt 1.2 0.49 Copper 1.6 0.98 Lead 3.4 0.49 " Molybdenum 1.1 0.49 Nickel 4.7 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 5.9 2.0 Zinc 7.9 2.0 --t Volatile Organic TPH by GC/FID 'fP11 Gasoline (C5-Cl2) 6.1 4.5 mglkg l B1C0804 03/26/21 10:55 EPA 8015M Sm-rogate: 4-Bromn/hrorohcn_cne 108 "o (31 - 168) Semi -Volatile Organic TPH by GOOD TPH Diesel (C13-C22) ND 9.9 mgrkg I B1C'0798 03/26/21 10:21 EPA 8015M TPH Motor Oil (('23-C40) ND 50 " " " " Surrogate: o-Tetphenrl 106 % (65 - 133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 79 161*44Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID: 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 BIC0815 03/26/2113:59 ITA8260B r Brontobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bratnofortn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcne ND 1.2 .. Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloronethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (P:D13) ND 1.2 Dibromomethane ND 1.2 _ 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dich1orobc117enc ND 1.2 Dichlorodifluoromethane ND 12 " 1, 1 -Dichloroethane ND 1.2 1.2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 - cis-1.2-Dichloroethene ND 1.2 " trans-1.2-Dichloroethene ND 1.2 12-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I,I-Dichloropropene ND 1.2 cis- 1.3 -Dichloropropene ND 1.2 t trans-1,3-Dichloropropene ND 1.2 Fthylbenzenc ND 1.2 - The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 79 WAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg!kg 1000 B 1 C0815 03/26/21 13:59 EPA 9260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 '.Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 " ., . 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2=retrachloroethane ND 1.2 Tetrachlorocthene (PCE) ND 1.2 Toluene ND 1.2 1.2,3-Trichlorobenzenc ND 1.2 1,2.4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Triehloroethene (TCE) ND 1.2 Trichlorotluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2A-T'rintethylbenzene ND 1.2 1,35-Trimethvlbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dihrcmu{1lua unu thmu 93 %, ( 75 - 122 ) Surrogate: Toluene-dS SS 'S', (66 - 128) " Surrogate: 4-Brorun/luorobea-ene 94 `/ ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg'kg 1 BIC0807 03/26/21 14:54 EPA 7471A Total Metals by ICP Antimony 8.2 2.4 mgtkg 1 B1COH10 03/26/21 13:47 EPA 601OB Arsenic 8.9 1.9 Barium 260 0.96 Beryllium ND 0.48 " Cadmium ND 0.24 Chromium 55 0.48 N-02 Cobalt 12 0.48 Copper 120 0.96 Lead 550 0.49 " " " " " N-02, N-03 Molybdenum 1.1 0.48 Nickel 150 0.48 Selenium ND 1.9 Silvcr ND 0.48 w Thallium ND 0.96 Vanadium 33 1.9 Zinc 720 1.9 STLC Metals by ICP Chromium 0.34 0.10 mg/L 2 B 1 D0007 04/01 /21 14:40 STLC/EPA 601 OB - Lead 56 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.25 0.050 mg/l. 1 B 1 D0112 04/06/21 12:18 EPA 1311 TPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 1.805 925-3376 Page 24 of 79 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples I Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-('12) ND 4.9 mg!kg 1 B1C0804 03/26'21 11:52 EPA 8015M R-07 . , Surrogate: 4-Bromo/luorobenzene 100 3fi (31 - 16N ) Semi -Volatile Organic TPH by GC/FID -- TPH Diesel (C13-C22) 71 40 mgtkg 4 BIC0798 03/26'21 11:59 EPA 8015M D-04 TPH Motor Oil (C23-C40) 520 200 1. 11 11^ D-04 Surrogate: o-Teipheitrl 108 IN (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B 1 C0815 03/26/21 14:25 EPA 8260B Bromobenzene ND 1.2 Bromochlorotnethane ND 1.2 Brontodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 C'hlorometliane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronto-3-chloropropanc ND 1.2 1.2-Dibronioethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromethanc ND 1.2 1,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 LI-Dichloroethene ND 1.2 cis-L2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 12-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I,I-Dichloropropane ND 1.2 cis- 1.3-Dichloropropcnc ND 1.2 trans- l,3-Dichloropropcnc ND 1.2 P.thylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 26 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mgtkg 1000 B 1 C0815 03/26/21 14:25 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzenc ND 1.2 Styrene ND 1.2 1,1-1.2-Tetrachloroethane ND 1.2 1.1.2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne WCE) ND 1.2 Toluene ND 1.2 1,2,1-Trichlorobenzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " 1,12-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 " 1,23-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 " Xylcncs (total) ND 1.2 Surrogatc : Uihrovtgthmrumethunr 97 ;'fi ( 75 - 12 2) Surrogate: Toluene-dS 90 N, 166 - 128) Surrogate: 4-Bromofhroroben_c ne SS °„ (76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7 Notes Total Metals by CVAA Mercury ND 0.098 mg/kg 1 B 1 C0807 03/26/21 14:56 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mglkg I BIC0810 03/26/21 13:50 EPA601OB Arsenic 4.1 1.9 Barium 180 0.96 Bervllium 0.53 0.48 —. Cadmium ND 0.24 Chromium 78 0.48 N-02 Cobalt 16 0.49 r Copper 31 0.96 Lead 37 0.48 Molybdenum ND 0.48 Nickel 100 0.48 Selenium ND 1.9 " Silver ND 0.48 Thallium ND 0.96 Vanadium 47 1.9 Zinc 69 1.9 STLC Metals by ICP Chromium 0.25 0.10 mg/L 2 BID0007 04/01/21 14:51 STLC/EPA 601 OB Volatile Organic TPH by GC/FID TPH (.iasoline (C5-('12) ND 4.7 mg/kg 1 B1('0804 03/26!21 12:20 EPA 8015M R-07 Surrogate: 4-&nniollaorohenrene 107 "- (31 - 168 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 28 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by : Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 27 9.9 mg/kg 1 B1('0798 03/26/21 13:02 EPA 8015M D-06 TPH Motor Oil (C23-C40) 610 50 " Surrogate: o-Teiphenrl 107 30 (65 - 133) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0050 mg/kg 1 B 1 C0817 03/26/21 13:46 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tort-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 " Chlorobenzcnc ND 0.0050 Chloroethanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 1.2-Dibronio-3-chloropropane ND 0.0050 1,2-Dibromoethane (EDB) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 14-Dichlorobenzene ND 0.0050 Dichlorodifluoromethane ND 0.0050 1, 1 -Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 " 1,1-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropene ND 0.0050 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropene ND 0.0050 1, 1 -Dichloropropene ND 0.0050 cis- 1.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Ethylbenzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by : Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) llexachlorobutadiene ND 0.0050 rng'kg 1 B1('0817 03/26/21 13:46 EPA8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.00.50 1,1.2.2-Tetrachloroethane ND 0.0050 Tctrachlorocthene (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobenzene ND 0.0050 1,2,4-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (T('E) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,23-Trichloropropane ND 0.0050 1.2.4-Trimethylbenzene ND 0.0050 13,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylenes (total) ND 0.0050 Surrogate: Uibromolluoromethane 94 , f 75 - 122 1 " Surrogate: Toluene-d,S 10 ",,, (66 - 12R) " Surrogate: 4-Bromnthtoroben:cne 89 `%4, 176 - 122 1 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID : 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.14 0.095 mg/kg 1 B1('0807 03/26/21 14:58 EPA7471A Total Metals by ICP Antimony ND 2.4 mg!kg I B1 C0810 03/26/21 13:52 EPA 6010B Arsenic 5.9 L9 Barium 170 0.97 Bervllium 0.50 0.49 ^ Cadmium ND 0.24 Chromium 41 0.49 Cobalt 16 0.49 •— Copper 27 0.97 Lead 10 0.49 Molybdenum ND 0.49 - Nickel 38 0.49 Selenium ND 1.9 ° Silver ND 0.49 _ Thallium ND 0.97 Vanadium 33 1.9 "Zinc 27 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C 5-C 12) ND 4.7 mg!kg I B I C0804 03/26/21 12:49 EPA 8015M R-07 Surrogate: 4-Bromo/luoroben7ene 96 S'i, (31 - 168) 11 " 11 Semi -Volatile Organic TPH by GC/FID TPI I Diesel (C I 3-C22) ND 10 mg/kg l BIC0798 03/26/2110:49 EPA8015M TPH Motor Oil (C23-C40) 85 50 " " " " Surrogate: o-Ter phenyl 105 % (65 - 133) 11 " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene NI) 0.0050 mgikg 1 B1C0817 03/26/21 14:44 EPA 8260B -Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromofonn ND 0.0050 Bromomethane NI) 0.0050 n-Butylbenzene ND 0.0050 _ sec-Butylbenzene ND 0.0050 tert-Butylbenzene NJ) 0.0050 Carbon tetrachloride NI) 0.0050 " Chlorobcnzene NJ) 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-C'hlorotoluene ND 0.0050 DibronwchIoromethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 1.2-Dibromoethane (EDB) ND 0.0050 Dibromomethanc ND 0.0050 I.2-Dichlorobenzenc NI) 0.0050 " - 1.3-Dichlorobcnzcnc NJ) 0.0050 14-Dichlorobcnzcnc ND 0.0050 Dichloroditluoromcthane ND 0.0050 " 1, 1 -Dichloroethane ND 0.0050 1.2-Dichloroethane ND 0.0050 " 1, 1 -Dichloroethene ND 0.0050 - cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 1.3-Dichloropropane ND 0.0050 2.2-Dichloropropane ND 0.0050 " I,1-Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 " Ethylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 79 Oilfield Environmental & Compliance, Inc. � J Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Control Sampled : 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) llexachlorobutadiene ND 0.0050 mg'hg 1 BIC0817 03/26/21 14:44 EPA 8260B 4-Isopropyl Toluene ND 0.0050 lsopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 - • Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.0050 1,1,2.2-Tetrachloroethane ND 0.0050 Tetrachloroethenc WCg) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobcn7cnc ND 0.0050 " 1,2,4-Trichlorobenrene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 •— 1,1,2-Trichloroethane ND 00050 Trichloroethane (TC'E) ND 0.0050 Trichlorolluoromethane ND 0.0050 " ._ 1.2.3-Trichloropropane ND 0.0050 " 1,2.4-Trimethylbenzene ND 0,0050 " 1.3.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 X_vlenes (total) ND 0.0050 Surrogatr Dihromulhrurumrthunr 93 '-, ( 75 - 122 ) Surrogate: Toluene-db' 95 "„ ( 66 - 128 ) " Surrogate" 4-Bronmlhrnrohen_enc 98 °„ / 76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com _ FAX: (805 925-3376 Page 34 of 79 � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by : Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7 Notes Total Metals by CVAA Mercury ND 0.099 mg/kg I B I ('0807 03/26/21 15:00 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I B I C0810 03/26/21 13:55 EPA 6010B Arsenic 3.6 2.0 Barium 13 1.0 Beryllium ND 0.50 ,�. Cadmium ND 0.25 Chromium 11 0.50 Cobalt 1.9 0.50 Copper 5.3 H) Lead 4.3 0.50 Molybdenum 2.5 0.50 Nickel 9.0 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND H) Vanadium 8.4 2.0 Zinc 8.8 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 42 4.9 mg/kg 1 BIC0804 03/26/21 13:17 EPA 8015M Surrogate: 4-Brontu/luorohen:ene 196 % (31 - 168) S-02 Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-C22) ND 9.9 mg/kg 1 BIC0798 03/26/21 10:35 EPA 8015M - TPH Motor Oil (C23-C40) 52 50 " " " " " Surrogate: o-Terphemd 106 %b (65 - 133 ) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 35 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101941 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Sampled by: Matrix: Solid Field Data: NA Lab ID : 2101841-10 Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.045 mg'kg 1 B 1('0817 03/20/21 12:49 EPA 8260B Bromobenzene ND 0.045 Bromochloromcthane ND 0.045 Bromodichloromethane ND 0.045 Bromoform ND 0.045 Bromomethane ND 0.045 a-BatVlbeuzene 0.22 0.045 " see-Batylbenzene 0.11 0.04.5 tert-13utylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 " C'hloroethane ND 0.045 Chloroform ND 0.045 Chloromethanc ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 " Dibromochloromethane ND 0.045 1,2-Dibronio-3-chloropropatic ND 0.045 1.2-Dibromoelhane (EDI3) ND 0.045 Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobenzene ND 0.045 1.4-Dichlorobenzene ND 0.045 Dichlorodilluoromethane ND 0.045 1,1-Dichlorocthane ND 0.045 " 1,2-Dichlorocthane ND 0.045 1,1-Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1.3-Dichloropropane ND 0,045 " 2.2-Dichloropropane ND 0.045 1,1-Dichloropropene ND 0.045 cis- I .3-Dichloropropene ND 0.045 trans- l,3-Dichloropropene ND 0.045 Ethylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 llexachlorobutadiene ND 0.045 mgIg 1 B 1('0817 03/26/21 12:49 EPA 9260B 4-Isopropyl Toluene ND 0.045 lsopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene 0.15 0.045 Styrene ND 0.045 1,1,12-Tetrachlomethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachloroethene (PCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 " 1,2,4-Trichlorobenzene ND 0.045 " I,1.I-Trichloroethanc ND 0.045 1,12-Trichloroethane ND 0.045 Trichloroethene O'CE) ND 0.045 Trichlorotluoromethane ND 0.045 1,23-Trichloropropanc ND 0.045 1.2.4-Trimethylbenzene ND 0.045 1.3.5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: Dihromolluoromethane 92 % ( 75 - 122 ) Surrogate: Toluene-d8 97 "c; (66 - 128 ) Surrogate: 4-BromoJluorobenzcne 99 % ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 79 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mg/kg 1 B1('0807 03/26/21 15:02 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg!kg I BI C0810 03/26/21 14:06 EPA 601(1B .� Arsenic 4.5 2.0 Barium 47 LO Beryllium ND 0.50 Cadmium ND 0.25 Chromium 18 0.50 Cobalt 3.6 0.50 Capper 9.8 1.0 Lead 16 0.50 Molybdenum 2.1 0.50 Nickel 36 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 - Vanadium 15 2.0 Zinc 29 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.4 mg'kg I BIC0804 03/26/21 13:46 EPA 8015M R-07 Surrogate: 4-Brotno1lta)-oben_ene 100111111 (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 mg/kg I B1C0798 03/26/21 12:27 EPA 8015M TPH Motor Oil (C23-C40) 260 50 "11" 11 Surrogate: o-Tetphetarl 108 4b (65 - 133) 11 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID : Soil Pile S Sampled : 03/25/21 11:45 Matrix: Solid Sampled by : Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0049 mgtkg 1 BIC0817 03/26/21 15:13 EPA826013 Bronrobenzene ND 0.0049 Bromochloromethane ND 0.0049 Bromodichloromethane ND 0.0049 • Bromoform ND 0.0049 Bronromethane ND 0.0049 n-Butylbenzene ND 0.0049 sec-Butylbenzene ND 0.0049 tort-Butylbenzene ND 0.0049 Carbon tetrachloride ND 0.0049 Chlorobenzenc ND 0,0049 Chlorocthanc ND 0.0049 Chloroform ND 0.0049 Chloronrethane ND 0.0049 --' 2-Chlorotoluene ND 0.0049 4-Chlorotoluene ND 0.0049 Dibromochloromethane ND 0.0049 1.2-Dibromo-3-chloropropane ND 0.0049 1,2-Dibromoethane (EDB) ND 0.0049 Dibromomethane ND 0.0049 12-Dichlorobenzene ND 0.0049 1.3-Dichlorobenzene ND 0.0049 " 1,4-Dich1orobenzene ND 0.0049 Dichlorodifluoromethane ND 0.0049 ' 1,1-Dichloroethane ND 0.0049 1,2-Dichloroethane ND 0.0049 I.I-Dichloroethene ND 0.0049 cis-12-Dichloroethene ND 0.0049 " trans-1,2-Dichloroethene ND 0.0049 L2-Dichloropropane ND 0.0049 1,3-Dichloropropane ND 0.0049 2.2-Dichloropropane ND 0.0049 1, 1 -Dichloropropene ND 0.0049 cis-1,3-Dichloropropene ND 0.0049 " ' trans-1,34)ichloropropenc ND 0.0049 Ethylbcnzene ND 0.0049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 79 i A WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID : Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Niue Volatile Organic Compounds by GUMS (Continued) Ilexachlorobutadiene ND 0.0049 mg -kg 1 BIC0817 03/26/21 15:13 FPA8200B - ' 4-Isopropyl Toluene ND 0.0049 Isopropylbenzene ND 0.0049 Methylene chloride ND 0.0049 -, Naphthalene ND 0.0049 n-Propylbenzene ND 0.0049 Styrene ND 0.0049 1,1,1,2-1'etrachloroethane ND 0.0049 " 1,1,2.2-Tetrachloroethane ND 0.0049 " Tctrachloroethene (PCE) ND 0.i1049 Tolucne ND 0.0049 1,2,3-Trichi orobenzene ND 0.0049 " 1,2,4-Trichlorobenzene ND 0.0049 " I,1,1-Trichloroethane ND 0.0049 • 1,1,2-Trichloroethane ND 0.0049 " Trichloroethane (TCE) ND 0.0049 Trichlorolluoromethane ND 0.0049 1,23-Trichloropropane ND 0.0049 1.24-Trimethylbenzene ND 0.0049 13,5-1'rimethylbenzene ND 0.0049 Vinyl chloride ND 0.0049 Xylenes (total) ND 0.0049 " Surrogate: 1)1%7'U717(/1111U/'(/!n['lhan[ 91 ( 75 - 122 ) Surrogate: Toluene-dg 95 "r, (66 - 128 ) Surrogate: 4-B/omolkuur/ben_ene 97 ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 I Analytical Report foi- Samples Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix : Solid Sampled by: Lab ID : 2101841-12 Field Data: NA Analyte Resuh RL Units Dilution Batch Analyzed Method Not" Total Metals by CVAA Mercury ND 0.097 mg'kg 1 BIC0807 03/26/21 15:04 EPA 7471A Total Metals by ICP Antimony ND 2.3 mgtkg I Bl ('0810 03/26/21 14:09 FPA 001013 - Arsenic 5.6 1.9 " Barium 23 0.93 Beryllium ND 0.47 " Cadmium ND 0.23 Chromium 14 0.47 Cobalt 2.5 0.47 Copper 6.8 0.93 Lead 73 0.47 " Alolvbdenum 3.7 0.47 Nickel 11 0.47 Selenium ND 1.9 Silver ND 0.47 " Thallium ND 0.93 Vanadium 15 1.9 Zinc 15 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.7 mg'kg 1 BIC0804 03/26!21 14:14 EPA 8015M R-07 S'tarngutc: 4-f3runm/luoruheir_cnc• 103 ". (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-('22) ND 9.9 mg'kg 1 B1('0798 03/20 21 11:17 EPA 9015M TPH Motor Oil (C23-C40) 75 50 "1. .1" D-04 Surrogate: o4iciphemd 107 1% (65 - 133) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925_3376 Page 41 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by : Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mgkg 1 BIC0817 03/26/21 15:43 EPA8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 -- Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzenc ND 0.0050 r Chlorocthanc ND 0.0050 Chlorotonn ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0,0050 Dibromochloromethane ND 0.0050 r 1,2-Dibromo-3-chloropropanc ND 0.0050 1,2-Dibromoethane (EDB) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 " 1.3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 Dichlorodithioromethanc ND 0.0050 " ' 1, 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 0.0050 --• cis- 1.2-Dichloroethene ND 0.0050 trans- I .2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 13-Dichloropropane ND 0.0050 2.2-Dichloropropane ND 0.0050 1,1-Di chloropropene ND 0.0050 cis -1,3-1)ichIoropropene ND 0.0050 trans- 1,3-Di chloropropene ND 0.0050 Ethylbenzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by : Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Hexachlorobutadiene ND 0.0050 mgukg 1 B1C0817 03/26/21 15:43 EPA8260B 4-Isopropyl Toluene ND 0.0050 lsopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1.1,2- Tetrachloroethane ND 0.0050 1,1,22-Tetrachloroethane ND 0.0050 7etrachlorocthenc (PCP.) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobenzene ND 0.0050 " 1,2.4-Trichlorobe117e11e ND 0.0050 I,I,1-Trichloroethane ND 0.0050 1.1.2-Trichloroethane ND 0.0050 Trichloroethane (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2.3-Trichloropropane ND 0.0050 12,4-Trimethy[benzene ND 0.0050 1,3.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: I)ihromolhtoromethane 91 " i, ( 75 - 122 ) Surrogate: Toluene-dS 94':,, ( 66 - 128 ) Surrogate: 4-Bromo/luoroben_ene 97 `''„ (76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mgikg 1 B 1 C0807 03/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B1C0810 03/2621 14:11 EPA 6010B . Arsenic 2.0 1.9 Barium 5.5 0.96 Beryllium ND 0.48 », Cadmium ND 0.24 Chromium 6.4 0.49 " Cobalt 0.76 0.48 " r Copper 1.8 0.96 Lead 3.7 0.48 Molybdenum 1.6 0.48 Nickel 3.9 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 5.2 1.9 Zinc 5.2 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.9 mg/kg 1 BIC0804 03/26/21 14:42 EPA 8015M R-07 Surrogate: 4-8romo/hcoroben_cne 102 30 (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 mg'kg I B1C0798 03126�21 11:45 EPA 8015M — TPH Motor Oil (C23-C40) 120 50 " " " " Surrogate: o-Teiphe77rl 107 `/,, (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 44 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 BIC0817 03/26/21 16:12 EPA8260B �Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 • Bromoform ND 0.0050 Bromomethane ND 0.0050 " n-Butvlbenzene ND 0.0050 sec-Butvlbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 Chlorobenzenc ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 " Chloromethane ND 0.0050 ' 2-Chlorotoluene ND 0.0050 4-C'hlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 1,2-Dibromo-3-chloropropane ND 0.0050 " 1.2-Dibromoethane (F:DB) ND 0.0050 Dibrotnomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene NI) 0.0050 I.4-Dichlorobenzene ND 0.0050 " Dichloroditluoromethane ND 0.0050 - 1, 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1.2-Dichloropropane ND 0.0050 1.3-Dichloropropane ND 0.0050 " 2.2-Dichloropropane NI) 0.0050 1. 1 -Dichloropropene NI) 0.0050 cis-1.3- Dichloropropanc ND 0.0050 trans-1,3-Dichloropropane ND 0.0050 Lthylbenzcnc ND 0.00.50 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 45 of 79 �I Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Ilexachlorobutadiene ND 0.0050 mg,kg I BIC0817 03/26/21 16:12 EPA8260B 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,l_1,2-TetrachloroethLine ND 0.0050 1. 1 .2,2-Tetrachloroethane ND 0.0050 Tetrachlorocthcne (PCE) ND 0.0050 " Toluene ND 0.0050 1.2,3-Trichlorobcnzenc ND 0.0050 1,2.4-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 00050 " 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 " Trichlorotluoromethane ND 0.0050 1.2,3-Trichloropropane ND 0.0050 12.4- Crimethylbenzene ND 0.0050 " 1,35-Trimethylbenzene ND 0,0050 Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: Dihromolluoromethane 91 % ( 75- 122) " Surrogate: Toluene-d8 95 3„ ( 66 - 138 ) Surrogate: 4-13run,q/hrornhe,ccne 97 `,, ( 76- 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 46 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Totali i Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0807 -EPA 7471A Preparation: EPA 7471A Prep 03/26/21 07:43 Blank (BlC0807-BLK1) Analyzed: 03/26/21 13:21 Mercury ND 0.10 mg kg LCS (BlC0807-BSI) Analyzed: 03/26/21 13:17 Mercury 0.792 0.10 mgikg 0.833 95 85-115 LCS Dup (B1C0807-BSD1) Analyzed: 03/26/21 13:19 Mercury 0.783 0.10 mg/kg 0.833 94 85-115 1 20 ~ Duplicate (BIC0807-DUPI) Source: 2101842-02 Analyzed: 03/26/21 13:25 Mcreury 0.0556 0.096 tnglkg 0.0554 0.3 20 Matrix Spike (BlC0807-MS1) Source: 2101842-02 Analyzed: 03/26/21 13:27 Mercury 0.855 0.096 mg/kg 0.796 0.0554 100 75-125 Matrix Spike Dup (BlC0807-MSDI) Source: 2101842-02 Analyzed: 03/26/21 13:29 Mercury 0.750 0.087 mgIg 0.727 0.0554 96 75-125 13 20 Post Spike (BlC0807-PS1) Source: 2101842-02 Analyzed: 03/26/21 13:31 Mercury 5.17 ug/L 5.00 0.347 97 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 79 AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Blank (B1C0810-BLK1) Analyzed: 03/26/21 12:16 Antimony ND 2.5 mglkg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " Nickel ND 0.50 Selenium ND 2.0 " Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 LCS (BlC0810-BS1) Analyzed: 03/26/21 12:40 Antimony 10(1 2.5 mgnkg 100 100 80-120 Arsenic 101 2.0 100 WI 80-120 Barium 102 1.0 100 102 80-120 - . Beryllium 103 0.50 100 103 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 103 0.50 100 103 80-120 Cobalt 103 0.50 100 103 80-120 Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 100 0.50 100 100 80-120 Nickel 103 0.50 100 103 80-120 Selenium 100 2.0 100 100 80-120 Silver 5.Oo 0.50 5.00 101 80-120 Thallium 104 LO 100 104 80-120 - . Vanadium 100 2.0 100 100 80-120 Zinc 103 2.0 100 103 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 48 of 79 WALMS Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes r Level Result Limits Limit Batch BIC0810 -EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 LCS Dup (B1C0810-BSDl) Analyzed: 03/26/21 12:43 Antimony 101 2.5 mg/kg 100 101 80-120 0.7 20 Arsenic 102 2.0 100 102 80-120 0.9 20 Barium 102 1.0 100 102 80-120 0.3 20 Beryllium 104 0.50 100 104 80-120 0.9 20 Cadmium 103 0.25 100 103 80-120 0.5 20 Chromium 104 0.50 100 104 80-120 1 20 .. Cobalt 104 0.50 100 104 80-120 0.5 20 Copper 104 1.0 100 104 80-120 0.9 20 Lead 104 0.50 100 104 80-120 0.8 20 Molybdenum 101 0.50 100 101 80-120 0.9 20 Nickel 104 0.50 100 104 80-120 0.5 20 Selenium 101 2.0 100 101 80-120 0.7 20 Silver 5.16 0.50 5.00 103 80-120 2 20 Thallium 104 LO 100 104 80-120 0.3 20 Vanadium 102 2.0 10U 102 80-120 1 20 Zinc 103 2.0 100 103 80-120 0.5 20 Duplicate (B1C0810-DUPl) Source: 2101840-03 Analyzed: 03/26/21 13:06 Antimony ND 2.4 mg/kg 0.966 20 Arsenic 2.64 1.9 3.12 17 20 Barium Hs s 0.95 116 2 20 Beryllium ND 0.47 ND 20 Cadmium ND 0.24 ND 20 Chromium 16.3 0.47 17.6 8 20 Cobalt 3.67 0.47 4.26 15 20 Copper 9.50 0.95 8.79 8 20 Lead 6.24 0.47 5.56 12 20 Molybdenum 1.46 0.47 1.27 14 20 Nickel 20.9 0.47 23.4 12 20 Selenium ND 1.9 ND 20 Silver ND 0.47 ND 20 Thallium ND 0.95 ND 20 • - Vanadium 15.0 1.9 15.4 3 20 Zinc 34.0 1.9 29.6 14 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes '-' Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Matrix Spike (B1C0810-MS1) Source: 2101840-03 Analyzed: 03/26/21 12:45 Antimony 49.9 2.4 mg/kg 97.6 ND 51 10-116 Arsenic 100 2.0 97.6 3.12 100 77-121 Barium 196 0.98 97.6 116 82 30-169 Beryllium 98.3 0.49 97.6 ND 101 86-111 Cadmium 93.4 0.24 97.6 ND 96 81-112 Chromium 113 0.49 97.6 17.6 97 75-129 Cobalt 96.4 0.49 97.6 4.26 94 71-121 Copper 106 0.98 97.6 8.79 100 68-135 Lead 99.5 0.49 97.6 5.56 95 72-121 Molybdenum 89.8 0.49 97.6 127 91 70-112 Nickel 111 0.49 97.6 23.4 90 73-121 Selenium 94.7 2.0 97.0 ND 97 76-116 Silver 4.74 0.49 4.88 ND 97 54-132 Thallium 91.2 0.99 97.6 ND 93 64-120 �Vanadium 112 2.0 97.6 15.4 99 78-124 Zinc 122 2.0 97.6 29.6 95 50-143 Matrix Spike Dup (B1C0810-MSD1) Source: 2101840-03 Analyzed: 03/26/21 12:55 Antimony 48.3 2.5 mg,'kg 98.0 ND 49 10-116 3 20 Arsenic 102 2.0 98.0 3.12 101 77-121 1 20 Barium 203 0.98 98.0 116 89 30-169 4 20 Bervllium 99.4 0.49 98.0 ND lot 86-111 1 20 Cadmium 95.0 0.25 98.0 ND 97 81-112 2 20 Chromium 117 0.49 98.0 17.6 101 75-129 4 20 Cobalt 98.2 0.49 98.0 4.26 96 71-121 2 20 Copper L10 0.98 98.0 8.79 103 08-135 3 20 Lead 100 0.49 98.0 5.56 97 72-121 2 20 Molybdenum 91.3 0.49 98.0 1.27 92 70-112 2 20 Nickel 113 0.49 98.0 23.4 92 73-121 2 20 - Selenium 96.4 2.0 98.0 ND 98 76-116 2 20 Silver 4.89 0.49 4.90 ND 100 54-132 3 20 Thallium 93.1 0.98 98.0 ND 95 64-120 2 20 Vanadium 115 2.0 98.0 15.4 102 78-124 3 20 Zinc 124 2.0 98.0 29.6 96 50-143 1 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report meant be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comkreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by ' Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Post Spike (BlC0810-PSI) Source: 2101840-03 Analyzed: 03/26/21 12:58 Antimony 1.97 mg/L 2.00 0.0203 98 75-125 Arsenic 2.08 2.00 0.0657 101 75-125 Barium 4.38 2.00 2.43 97 75-125 Beryllium 1.99 2.00 0.00456 99 75-125 Cadmium 1.89 2.00 -0.00476 94 75-12.5 Chromium 2.37 2.00 0.370 100 75-125 . Cobalt 1.97 2.00 0.0898 94 75-125 Copper 2.25 2.00 0.185 103 75-125 Lead 2.02 2.00 0.117 95 75-125 Molybdenum 1.98 2.00 0.0268 98 75-125 " Nickcl 2.37 2.00 0.492 94 75-125 SClenlnm 1.97 2.00 0.000298 98 75-125 Silver 0.0974 0.100 -0.00298 97 75-125 Thallium 1.88 2.00 -0.0363 94 75-125 - Vanadium 2.30 2.00 0.324 99 75-125 Zinc 2.50 2.00 0.623 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 STLC Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO007 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/01/21 09:01 Blank (B1D0007-BLK1) Analyzed: 04/01/21 14:11 Chromium ND 0.050 mg/L Lead ND 0.050 11 LCS (B1D0007-BSI) Analyzed: 04/01/21 14:24 Chromium 9.98 0.050 mg/L 10.0 Lcad 10.0 0.050 10.0 LCS Dup (B1D0007-BSDI) Analyzed: 04/01/21 14:27 Chromium 9.99 0.050 mg/[. 10.0 Lead 9.90 0.050 1110.0 Duplicate (B1D0007-DUPI) Source: 2101841-07 Analyzed: 04/01/21 14:42 Chromium 0.341 0.10 mg/L 0.342 Lead 58.7 0.10 1156.1 Leach Fluid Blank (BID0007-LBK1) Analyzed: 04/01/21 14:13 Chromium ND 0.10 mg/L Lead ND 0.10 " 100 80-120 100 80-120 99 80-120 0.9 20 99 80-120 2 20 0.3 20 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: (805) 925-3376 Page 52 of 79 (I. � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0112 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/06/21 10:26 —� Blank (BID0112-BLKI) Analyzed: 04/06/21 12:08 Lead ND 0.050 mg/L LCS (B1D0112-BSI) Analyzed: 04/06/21 12:13 •� Lcad 9.64 0.050 mg/L 10.0 96 80-120 LCS Dup (B1D0112-BSD1) Analyzed: 04/06/21 12:16 Lead 9.78 0.050 mg/l. 10.0 98 80-120 1 20 ~ Duplicate (B1D0112-DUPl) Source: 2101841-07 Analyzed: 04/06/21 12:21 Lead 0.242 0.050 mg/l. 0.246 2 20 Leach Fluid Blank (B1D0112-LBK1) Analyzed: 04/06/21 12:11 Lcad ND 0.050 mg/L The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 53 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatileby 1 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0802 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:22 - Blank (B1C0802-BLK1) Analyzed: 03/26/21 08:30 TPH Gasolinc (C5-('12) ND 0.50 mg/kg Surrogate. 4-Bromo/luorobenzene 0.127 110.125 101 31-168 t LCS (BlC0802-BS1) Analyzed: 03/26/21 06:59 TPH Gasoline (C5-C12) 1.01 0.50 mg/kg 1.00 101 62-151 Surrogatc:4-Bromolluoroben_ene 0.152 " 0.125 121 31-168 LCS Dup (B1C0802-BSD1) Analyzed: 03/26/21 07:25 TP11 Gasoline (C5-C12) 0.958 0.50 mg/kg 0996 96 62-151 5 20 Surrogate:4-Bromo/luorohenzene 0.142 " 0.125 114 31-168 Duplicate (B1C0802-DUPl) Source: 2101840-01 Analyzed: 03/26/21 09:29 TPH Gasoline (C5-('12) ND 0.50 mg/kg ND 20 Surrogate.4-Bromglluorobenzene 0.131 " 0.124 105 31-16S Matrix Spike (B1C0802-MSl) Source: 2101836-04 Analyzed: 03/26/21 16:07 TPH Gasoline (('54'12) 0.989 0.50 mg,'kg 1.00 ND 99 I0-166 Surrogate:4-Bromo/luorabcn::eiw 0.140 110.126 116 31-168 Matrix Spike Dup (B1C0802-MSDI) Source: 2101836-04 Analyzed: 03/26/21 16:33 TPH Gasoline (('5-('12) 0.971 0.50 mg/kg 0.992 ND 98 10-166 2 20 Su•rogate:4-Bronno/luorohenzene 0.149 0.124 120 31-168 Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Blank (Bl C0804-BLK1) Analyzed: 03/26/21 10:27 TPH Gasoline ((`5-('12) ND 0.50 mg/kg Surrogate.4-Bromnlluorobenzene 0.133 0.125 107 31-168 LCS (BlC0804-BSI) Analyzed: 03/26/21 09:30 TPH Gasoline (C5-('12) 1.24 0.50 mglkg 0.998 124 62-151 Surrogate:4-Bromolluorohenzene 0.147 " 0.125 1/8 31-168 LCS Dup (B1C0804-BSDI) Analyzed: 03/26/21 09:59 TPII Gasoline (C5-C12) 1.32 0.50 mgtkg 0.998 132 62-151 7 20 Surrogate:4-Bromohuoroben_ene 0.104 0.125 131 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 54 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic TPH by 1 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Duplicate (B1C0804-DUPl) Source: 2101841-06 Analyzed: 03/26/21 11:24 TPH Gasoline (('5-('12) 10.0 4.3 mg/kg 6.12 48 20 QR-03 Surrogate:4-Bromo/luorobenzcne 1.38 " 1.08 128 31-168 Matrix Spike (BlC0804-MS1) Source: 2101838-06 Analyzed: 03/26/21 20:00 TPH Gasoline (('5-C12) 1.13 0.49 mg%kg 0.978 ND 116 10-166 Surrogate:4-Brmnufluorohenzene 0.159 " 0.122 130 31-168 Matrix Spike Dup (BlC0804-MSD1) Source: 2101838-06 Analyzed: 03/26/21 20:29 TPH Gasoline (C5-C 12) 1.21 0.50 mg.tkg 1.00 ND 120 10-166 6 20 Surrogate:4-BromoJluorohenzene 0.155 0.125 123 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 55 of 79 C A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Semi-Volatileby 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0798 - EPA 8015M Preparation: EPA 3550C 03/25/21 17:29 Blank (BlC0798-BLKI) Analyzed: 03/26/21 07:35 TPH Diesel (C13-C'22) ND 10 mg/kg TPH Motor Oil (C23-C'40) ND 50 " Surrogate: o-Terphe» rl 53.7 1149.8 /ON 65-133 LCS (BlC0798-BSI) Analyzed: 03/26/21 07:07 TPH Diesel (C13-C22) 508 9.9 mgtkg 496 102 77-114 TPH Motor Oil(C23-C40) 549 50 496 ill 76-128 Srrrugutc: o-Terphcnyl W7 49.6 102 65-133 LCS Dup (B1C0798-BSD1) Analyzed: 03/26/21 07:21 TPH Diesel (C13-C22) 501 9.9 mg/kg 497 101 77-114 t 20 TPH Motor Oil (C23-C40) 557 50 497 112 76-128 2 20 Surrogate: o-Terphe»rl 53.5 49.7 108 65-133 Duplicate (B1C0798-DUPl) Source: 2101840-01 Analyzed: 03/26/21 08:44 TP11 Diesel (('13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (C23-C40) 43.1 50 44.8 4 20 Surrogate: o-Teiphe» i•1 53.4 49.8 107 65-133 Matrix Spike (BlC0798-MSI) Source: 2101840-01 Analyzed: 03/26/21 13:48 TPH Diesel (C13-C22) 507 9.9 mgrkg 497 ND 102 45-149 TPII Motor Oil (C23-C40) 556 50 497 44.8 103 34-175 Surrogate: o-Te,phen l 55.9 49.7 113 65-133 Matrix Spike Dup (B1C0798-MSD1) Source: 2101840-01 Analyzed: 03/26/21 14:02 TPH Diesel (('13-C22) 488 10 mg'kg 499 ND 98 45-149 4 20 TPH Motor Oil (('23-C40) 548 50 499 44.8 101 34-175 1 20 Surrogatc. o-Tcr1?hc•rn•1 55-2 49.9 111 65-133 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 56 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (B1C0815-BLK1) Analyzed: 03/26/21 11:26 Benzene ND 0.25 mg/kg Bromobenzene NI) 0.25 Brontochloromethane ND 0.25 Bromodichloromethane ND 0.25 Bromoform ND 0.25 " Bromomethane ND 0.25 " n-Butylbenzene ND 0.25 sec-Butylbenzene NI) 0.25 " tert-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 _ Chlorobenzene NI) 0.25 Chloroethane NI) 0.25 " Chloroform ND 0.25 Chloromethane ND 0.25 " - 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene ND 0.25 " Dibromochloromethane ND 0.25 " 1,2-1)ibromo-3-chloropropane ND 0.25 " 1,2-Dibromocthane (EDB) NI) 0.25 Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0.25 " 1,3-Dichlorobenzene ND 0.25 " 1,4-Dichlorobenzene ND 0.25 " Dichloroditluoromcthanc ND 0.25 _ I,1-Dichloroethane ND 0.25 " 1.2-Dichloroethane ND 0.25 1, 1 -Dichloroethene NJ) 0.25 cis-1.2-Dichloroethene ND 0.25 " • trans-1,2-Dichloroethene ND 0.25 1,2-Dichloropropane N1) 0.25 1,3-Dichloropropane ND 0.25 " 2.2-Dichloropropane ND 0.25 " I.I-Dichloropropene ND 0.25 " cis-1.3-Dichloropropene ND 0.25 trans-1,3-Dichloropropene ND 0.25 • Ethylbenzenc ND 0.25 " Iiexachlorobutadiene ND 0.25 " 4-Isopropyl Toluene ND 0.25 Isopropylbenzene ND 0.25 " btethylene chloride ND 0.25 " Naphthalene ND 0.25 n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.00cusa.com FAX: 805) 925-3376 Page 57 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (B1C0815-BLK1) Analyzed: 03/26/21 11:26 Styrene ND 0.25 mg1kg 1,1,1,2-Tetrachloroethane ND 0.25 1,1,2,2-Tetrachlorocthanc ND 0.25 Tetrachloroethene WCE) ND 0.25 Toluene ND 0.25 " 1,2,3-Trichlorobenzene NI) 0.25 " 1,2,4-1'richlorobenzene ND 0.25 " 1, 1, 1 -Trichloroethane ND 0.25 1,1.2-Trichloroethane ND 0.25 " Trichloroethene (TCE) ND 0.25 Prichlorofluorontethane ND 0.25 1,2,3-Trichloropropane ND 0.25 1,2,4-Trimethylbenzene ND 0.25 1,3,5-Trimethylbenzene ND 0.25 " Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 " Surrogate: 0.0445 0.0498 89 75-122 - . Surrogate: Toluene-c18 0.0455 0.049E 91 66-128 Sm•rogat<" 4-BrontgJluornhenrene 0.0479 0.0498 96 76-122 LCS (B1C0815-BS1) Analyzed: 03/26/21 09:44 Benzene 1.80 0.25 mg/kg 1.99 91 75-131 Bromobenzene 1.97 0.25 1.99 99 75-136 Bromochloromcthanc 1.67 0.25 1.99 84 70-135 Brotnodichloromethane 1.84 0.25 1.99 93 76-137 Bromol'orm 1.68 0.25 1.99 85 55-139 Bromomethane 1.49 0.25 1.99 75 10-157 n-Butylbenzene 2.38 0.25 1.99 120 62-166 sec-Butylbenzene 2.50 0.25 1.99 126 72-107 tort-ButVlbCo7elIe 2.33 0.25 1.99 117 69-158 Carbon tetrachloride 1.77 0.25 1.99 89 70-140 C'hlorobenzene 1.94 0.25 1.99 98 76-137 Chloroethane 2.09 0.25 1.99 105 10-104 Chloroform 1.80 0.25 1.99 91 75-123 Chloromethane 1.73 0.25 1.99 87 26-146 2-Chlorotoluene 2.11 0.25 1.99 106 73-145 4-Chlorotoluene 2.13 0.25 1.99 107 67-151 Dibromochloromethane 1.80 0.25 1.99 90 68-144 1,2-Dibronxi-3-chloropropane 1.63 0.25 1.99 82 45-148 1,2-Dibromoeihane (EDB) 1.80 0.25 1.99 91 73-134 Dibronx>methane 1.66 0.25 1.99 84 70-140 1,2-Dichlorobenzene 2.15 0.25 1.99 108 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX; 805 925-3376 Page 58 of 79 AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 - LCS (BlC0815-BSI) Analyzed: 03/26/21 09:44 1,3-Dichlorobcnzcnc 2.19 0.25 mg:'kg 1.99 110 76-146 1,4-Dichlorobenzene 2.10 0.25 1.99 106 72-140 Dichlomdilluoromethane 1.73 0.25 1.99 87 10-160 1,1-Dichloroethane 1.82 0.25 1.99 92 65-139 1,2-Dichloroethane 1.90 0.25 1.99 90 67-125 1,1-Dichloroethene 2.05 0.25 1.99 103 54-168 cis-L2-Dichloroethene 1.80 0.25 1.99 91 74-135 trans-1,2-Dichloroethene 1.98 0.25 1.99 100 68-149 1,2-Dichloropropane 1.77 0.25 1.99 89 74-130 1,3-Dichloropropane 1.83 0.25 1.99 92 68-130 2,2-Dichloropropane 1.95 0.25 1.99 98 33-187 l,l-Dichloropropene 1.95 0.25 1.99 98 71-140 cis- 1.3-Dichloropropene 1.79 0.25 1.99 90 78-135 trans- l,3-Di chloropropene 1.90 0.25 1.99 96 70-137 Ethvlbenzene 1.93 0.25 199 97 69-143 Ilexachlombutadiene 3.12 0.25 1.99 157 69-203 4-Isopropyl Toluene 2.38 0.25 1.99 120 74-154 Isopropylbenzene 2.11 0.25 1.99 106 72-157 Methylene chloride 1.75 0.25 1.99 88 49-129 Naphthalene 1.84 0.25 1.99 93 61-158 ❑-Propylbenzene 2.17 0.25 1.99 109 69-147 -� Styrene 1.92 0.25 1.99 97 71-144 1,1,1,2-Tetrachloroethane 1.92 0.25 1.99 97 78-132 1,1,2,2-Tetrachloroethane 1.90 0.25 1.99 96 64-138 Tetrachloroethane (PCE) 2.09 0.25 1.99 105 74-148 Toluene 1.82 0.25 1.99 92 76-131 1,2,3-Tiichlorobenzene 2.11 0.25 1.99 106 63-170 1,2.4-Trichlorobenzene 2.20 0.25 1.99 110 71-165 1, 1, 1 -Trichloroethane 1.97 0.25 1.99 99 74-137 1,1.2-Trichloroethane 1.82 0.25 1.99 91 68-134 Trichloroethene (TCE) 1,94 0.25 1.99 98 79-139 Trichlorofluorontethane 2.20 0.25 1.99 111 32-154 1.2,3-Trichloropropane 1.77 0.25 1.99 89 69-125 1.2,4-Trimethylbenzene 2.14 0.25 1.99 108 67-144 1,3.5-Trimethylben7ene 2.17 0.25 1.99 109 66-154 Vinyl chloride 2.27 0.25 1.99 114 39-150 Xylenes (total) 5.95 0.25 5,96 100 71-147 Surrogate: Uibromolhioront(,thun(, 0.0496 0.0497 100 75-11' Surrogate: T)htene-dR 0.0462 0.0497 93 06-128 Surrogate:4-Bromgllaorohen_eue 0.0451 0.0497 91 70-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805y 925-3376 Page 59 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilepi by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 �• LCS Dup (BlC0815-BSD1) Analyzed: 03/26/21 10:09 Benzene 1.87 0.25 mg/kg 2.00 94 75-131 4 20 Bromobenzene 2.02 0.25 2.00 101 75-136 2 20 Bromochloromethanc 1.69 0.25 2.00 85 70-135 2 20 Bromodichloromethane 1.93 0.25 2.00 97 76-137 5 20 Bromoform 1.80 0.25 2.00 90 55-139 7 20 Bromomethane 1.21 0.25 2.00 61 10-157 20 20 n-Butylbenzene 2.45 0.25 2.00 123 62-166 3 20 sec-Butylbenzene 2.48 0.25 2.00 124 72-167 0.9 20 tert-Butylbenzene 2.39 0.25 2.00 119 69-158 2 20 Carbon tetrachloride 1.87 0.25 2.00 94 70-140 6 20 - ' Chlorobenzene 2.07 0.25 2.00 104 76-137 7 20 Chlorocthane 2.21 0.25 2.00 111 10-164 6 20 Chloroform 1.81 0.25 2.00 90 75-123 0.4 20 Chloromethane 1.82 0.25 2.00 91 26-146 5 20 2-Chlorotoluene 2.20 0.25 2.00 113 73-145 7 20 4-Chlorotoluene 2,25 0.25 2,00 112 67-151 5 20 Dibromochloromethane 1.97 0.25 2,00 98 68-144 9 20 1,2-Dibromo-3-chloropropane 1.94 0.25 2.00 92 45-148 12 20 1,2-Dibromoethane (EDB) 1.98 0.25 2.00 99 73-134 9 20 Dibromomethanc 1.75 0.25 2.00 87 70-140 5 20 1,2-Dichlorobenzene 2.18 0.25 2.00 109 78-142 1 20 ' 1.3-Dichlorobenzene 2.30 0.25 2.00 115 76-146 5 20 IA-Dichlorobenzene 2.06 0.25 2.00 103 72-140 2 20 DichlorodiFluoromethanc 1.73 0.25 2.00 86 10-166 0.1 20 1. 1 -Dichloroethane 1.95 0.25 2.00 98 65-139 7 20 1 2-Dichloroethenc 1.93 0.25 2.00 96 67-125 7 20 LI-Dichloroethene 2.07 0.25 2.00 103 54-169 0.6 20 cis-L2-Dichloroethene 1.86 0.25 2.00 93 74-135 4 20 - trans-1,2-Dichloroethene 2.11 0.25 2.00 105 68-149 6 20 1.2-Dichloropropane 1.82 0.25 2.00 91 74-130 3 20 1,3-Dichloropropane 1.84 0.25 2.00 92 68-130 0.6 20 2,2-Dichloropropane 1.94 0.25 2.00 97 33-187 0.4 20 I.1-Dichloropropane 2.04 0.25 2.00 102 71-140 5 20 cis-1.3-Dichloroptopene 1.80 0.25 2,00 90 78-135 0.5 20 trans-1,3-Dichloropropene 1.94 0.25 2.00 97 70-137 2 20 _ Ethvlbenzene 2.06 0.25 2.00 103 69-143 6 20 1lexachlorobutadiene 3.30 0.25 2.00 165 69-203 6 20 4-Isopropyl Toluene 2.42 0.25 2.00 121 74-154 2 20 Isopropylbenzene 2.19 0.25 2.00 109 72-157 3 20 N'lethylene chloride 1.87 0.25 2.00 94 49-129 7 20 Naphthalene 2.04 0.25 2.00 102 61-158 IO 20 n-Propylbenzene 2.30 0.25 2.00 115 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 79 --I �1 LW Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 CompoundsVolatile Organic by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Duplicate (BlC0815-DUPI) Source: 2101841-07 Analyzed: 03/26/21 14:51 1,3-Dichlorobenzenc ND 1.2 mg/kg ND 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichlorodifluoromcthane ND 1.2 ND 20 1, 1 -Dichloroethane ND 1.2 ND 20 1,2-Dichloroethane ND 1.2 ND 20 1,1-Dichloroethene ND 1.2 ND 20 cis-1,2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropane ND 1.2 ND 20 1,3-Dichloropropane ND 1.2 ND 20 2,2-Dichloropropane ND 1.2 ND 20 1, 1 -Dichloropropene ND 1.2 ND 20 cis-L3-Dichloropropene ND 1.2 ND 20 trans-1,3-Dichloropropene ND 1.2 ND 20 F.thylbenzene ND 1.2 ND 20 Ilexachlorobatadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 Isopropylbenzene ND 1.2 ND 20 Methylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 ND 20 n-Propylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1,1,1,2-Tetrachloroethane ND 1.2 ND 20 1,1,2,2-Tetrachloroethane ND 1.2 ND 20 Tetrachloroethane (PCE) ND 1.2 ND 20 Toluene ND 1.2 " ND 20 1,23-Trichlorobenzene ND 1.2 ND 20 1,24-Trichlorobenzene ND 1.2 ND 20 1,1,1-Trichloroethane ND 1.2 ND 20 1,1,2-Trichloroethane ND 1.2 ND 20 Triehloroethene (TCE) ND 1.2 ND 20 Trichlorotluoroniethane ND 1.2 ND 20 1,2.3-Trichloropropane ND 1.2 ND 20 1,24-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 ND 20 Vinyl chloride ND 1.2 ND 20 Xylenes (total) ND 1.2 " ND 20 Surrogate: Dihrumolhwruntelhunr 11.1146E 0.0494 95 75-122 Surrogate: Toluene-ds 0.0455 0.0494 92 66-128 Surrogate:4-Broniolhiorobenzene 0.0466 0.0494 94 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 62 of 79 f AL i MA� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (B1C0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Benzene 9.51 1.2 mg/kg 9.92 ND 86 36-146 Bromobenzene 8.76 1.2 9.92 ND 88 28-152 Bromochloromethanc 8.53 1.2 9.92 ND 86 43-146 Bromodichloromethane 8.97 1.2 9.92 ND 90 43-153 Bromofonn 8.44 1.2 9.92 ND 85 26-151 Bromomethane 4.77 1.2 9.92 ND 48 10-158 ❑-Butylbenzene 9.02 1.2 9.92 0.499 76 10-171 sec-Butylbenzene 9.66 1.2 9.92 ND 97 10-176 tert-Butylbenzene 9.42 1.2 9.92 ND 95 19-168 Carbon tetrachloride 8.16 1.2 9.92 ND 82 29-151 Chlorobenzenc 8.93 1.2 9.92 ND 90 31-151 Chloroethane 10.4 1.2 9.92 ND 105 13-160 Chloroform 9.01 1.2 9,92 ND 91 44-137 Chloromethane 7.13 1.2 9.92 ND 72 10-144 2-Chlorotoluene 8.99 1.2 9.92 ND 91 24-158 4-Chlorotoluene 8.51 1.2 9.92 ND 86 19-160 Dibromoehloromethane 9.48 1.2 9.92 ND 96 40-153 1,2-Dibromo-3-chloropropane 9.07 1.2 9.92 ND 91 21-164 1,2-Dibromoethane (EDB) 9.81 1.2 9.92 ND 99 41-148 Dibromomethane 8.47 1.2 9.92 ND 85 45-158 1,2-Dichlorobenzene 9.26 1.2 9.92 ND 93 24-158 1,3-Dichlorobenzene 8.93 1.2 9.92 ND 90 19-160 1,4-Dichlorobenzene 8.53 1.2 9.92 ND 86 20-152 mchlorodilluoromethanc 6.47 1.2 9.92 ND 65 10-153 I,1-Dichloroethane 8.67 1.2 9.92 ND 87 35-148 1,2-Dichlorocthanc 9.37 1.2 9.92 ND 94 42-132 1,1-Dichloroethene 8.72 1.2 9.92 ND 88 18-174 cis-1,2-Dichloroethene 8.62 1.2 9.92 ND 87 41-146 vans-1,2-Dichloroethene 9.52 1.2 9.92 ND 96 27-161 12-Dichloropropane 8.67 1.2 9.92 ND 87 42-145 1,3-Dichloropropane 9.17 1.2 9.92 ND 92 42-141 2,2-Dichloropropane 8.42 1.2 9.92 ND 85 10-166 l,l-Dichloropropene 8.71 1.2 9.92 ND 88 28-151 cis-1,3-Dichloropropene 8.40 1.2 9.92 ND 85 38-148 trans-1,3-Dichloropropene 9.73 1.2 9.92 ND 98 36-144 I-'thylbenzene 8.85 1.2 9.92 ND 89 16-162 1lexachlorobutadiene 8.66 1.2 9.92 ND 87 10-193 4-Isopropyl Toluene 8.50 1.2 9.92 ND 86 11-167 Isopropylbenzene 9,00 1.2 9.92 ND 91 13-174 Nlethvlene chloride 8.75 1.2 9.92 ND 88 30-131 Naphthalene 9.21 1.2 9.92 ND 93 10-178 n-Propylbenzene 8.74 1.2 9.92 ND 88 12-160 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 63 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet t Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (B1C0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Styrene 8.81 1.2 mgfkg 9.92 ND 89 23-160 1,1,1,2-Tetrachloroethane 9.93 1.2 9.92 ND 100 36-152 1,1,2,24etrachloroethanc 9.13 1.2 9.92 ND 92 19-175 Telrachloroethene (PCE) 8.53 1.2 992 ND 86 23-162 Toluene 9.41 12 9.92 ND 85 26-152 1,2,3-Trichlorobenzene 8.62 1.2 9.92 ND 87 10-168 - 1,2,4-1'richlorobenzene 8.22 1.2 9.92 ND 83 10-170 1, 1, 1 -Trichloroethane 9.36 1.2 9,92 ND 94 36-150 1,1,2-Trichloroethane 9.70 1.2 9.92 ND 98 25-179 Trichloroethene (TCE) 8.55 1.2 9.92 ND 86 29-167 -- • Trichlorofluoromethane 8.61 1.2 9.92 ND 87 15-156 1,2,3-Trichloropropane 8.96 1.2 9.92 ND 90 26-177 1.2,4-Trimethylbenzene 8.51 1.2 9.92 ND 86 14-157 13,5-Trimethylbenzene 8.70 1.2 9.92 ND 88 10-167 - Vinyl chloride 9.41 1.2 9.92 ND 95 14-154 Xylenes (total) 26.2 1.2 29.8 ND 88 21-162 Surrogate: Dihronio luoromohane 0.0487 0.0496 98 75-122 _ Surrogate: Tohiene-d8 0.0457 0.0496 92 66-128 Surrogate:4-Bromo/luorohen_ene 0.0458 0.0496 92 76-122 Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (B1C0817-BLK1) Analyzed: 03/26/21 12:18 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " - Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromotirrm ND 0.0050 " Bromomethane ND 0.0050 " n-Butylbenzene ND 0.0050 " see-Butylbenzene ND 0.0050 " tert-Butylbcnzcnc ND 0.0050 " Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 " Chloroethane ND 0.0050 " Chloroform ND 0.0050 " Chloromethane ND 0.0050 2-Chlorotoluenc ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethanc ND 0.0050 1,2-Dibromo-3-chi oropropane ND 0.0050 " 1.2-Dibromoethane (EDB) ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 64 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank(B1C0817-BLKI) Analyzed: 03/26/21 12:18 Dibromomethanc ND 0.0050 mg/kg 1,2-Dichlorobenzene ND 0.0050 " 1.3-Dichlorobenzene ND 0.0050 IA-Dichlorobenzene ND 0.0050 " Dichluroditluoromcthanc ND 0.0050 1, 1 -Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 " 1,1-Dichloroethene ND 0.0050 cis-1,2-Dichlomethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 " --- 1,2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 " 2,2-Dichloropropane ND 0.0050 1.1-Diehloropropene ND 0.0050 " cis-1,3-Diehloropropene ND 0.0050 " trans-1,3-Diehloropropene ND 0.0050 Ethylbenzene ND 0.0050 Ilexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 " Isopropylbcnzcne ND 0.0050 " Nlethylene chloride ND 0.0050 �-+ Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 " Styrene ND 0.0050 " 1, 1, 1,2-Tetrachloroethane ND 0.0050 1,1,2,2-Tetrachloroethane ND 0.0050 " Tetrachloroethane (PCE) ND 0.0050 "Toluene ND 0.0050 " 1,2,3-Trichlorobenzene ND 0.0050 " 1,2,4-Trichlorobenzene ND 0-0050 1,1,1-Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 " Trichlorotluoromethane ND 0.0050 " 1,2,3-Trichloropropane ND 0.0050 1,2,4-1'rimethylbenzene ND 0.0050 " 1,3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 -� Surrogate: DibromoJluoromethane 0.0459 0.0495 93 75-122 Surrogate: Tiluene-d8 0.0472 0.0495 95 66-128 Surrogate: 4-Bronw luorohen_ene 0.0483 0.0495 98 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 65 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatileOrganic CoinpoundsQuality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (BlC0817-BSI) Analyzed: 03/26/21 10:22 Benzene 0.0342 0.0050 mg/kg 0.0398 86 75-131 Bromobenzene 0.0367 0.0050 0.0398 92 75-136 Bromochloromethane 0.0329 0.0050 0.0398 82 70-135 Bromodichloromethane 0.0334 0.0050 0.0398 84 76-137 Bromoform 0.0369 0.0050 0.0398 93 55-139 Bromomethane 0.0230 0.0050 0.0398 58 10-157 n-Butylbenzene 0.0396 0.0050 0.0398 99 62-166 sec-Butylbenzene 0.0452 0.0050 0.0398 114 72-167 tert-Butylbenzene 0.0427 0.0050 0.0398 108 69-158 Carbon tetrachloride 0.0348 0.0050 0.0398 87 70-140 Chlorobenzene 0.0374 0.0050 0.0398 94 76-137 Chloroethane 0.0413 0.0050 0.0399 104 10-164 Chloroform 0.0323 0.0050 0.0398 81 75-123 Chloromethane 0.0324 0.0050 0.0398 82 26-146 2-Chlorotoluene 0.0396 0.0050 0.0398 100 73-145 4-Chlorotoluene 0.0405 0.0050 0.0398 102 67-151 Dibromochloromethane 0.0371 0.0050 0.0398 93 68-144 1,2-Dibromo-3-chloropropane 0.0355 0.0050 0.0398 89 45-148 1,2-Dibromoethane (EDB) 0.0369 0.0050 0.0398 93 73-134 Dibromomethane 0.0328 0.0050 0.0398 82 70-140 1,2-Dichlorobenzene 0.0402 0.0050 0.0398 101 78-142 1.3-Dichlorobenzene 0.0406 0.0050 0.0398 102 76-146 1,4-Dichlorobenzene 0.0388 0.0050 0.0398 97 72-140 Dichloroditluoromcthane 0.0375 0.0050 0.0398 94 10-166 1, 1 -Dichloroethane 0.0342 0.0050 0.0398 86 65-139 1,2-Dichloroethane 0,0336 0.0050 0.0398 84 67-125 13-Dichloroethene 0.0360 0.0050 0.0399 90 54-168 cis-1,2-Dichloroethene 0.0346 0.0050 0.0398 87 74-135 trans-1,2-Dichloroethene 0.0375 0.0050 00398 94 68-149 1,2-Dichloropropane 0.0336 0.0050 0.0398 84 74-130 1,3-Dichloropropaue 0.0356 0.0050 0,0398 90 68-130 2,2-Dichloropropane 0.0394 0.0050 0.0398 99 33-187 1, 1 -Dichloropropene 0.0350 0.0050 0.0398 88 71-140 cis-1.3-Dichloropropene 0.0349 0.0050 0.0398 88 78-135 trans-1,3-Dichloropropene 0.0393 0.0050 0.0398 99 70-137 Etylbenzene 0.0379 0.0050 0.0398 95 69-143 Hexachlorobutadiene 0.0480 0.0050 0.0398 121 69-203 4-Isopropyl Toluene 0.0438 0.0050 0.0398 110 74-154 Isopropylbenzene 0.0408 0.0050 0.0398 102 72-157 methylene chloride 0.0320 0.0050 0.0398 80 49-129 Naphthalene 0.0429 0.0050 0.0398 108 61-158 n-Propylbenzene 0.0417 0.0050 0.0398 105 69-147 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 66 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilepoby Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (B1C0817-BS1) Analyzed: 03/26/21 10:22 Styrene 0.0384 0.0050 mg/kg 0.0398 97 71-144 1, 1, 1,2-Tetrachloroethane 0.0379 0.0050 0.0398 95 78-132 1,1,2,2-Tetrachloroethane 0.0390 0.0050 0.0398 98 64-138 Tetrachloroethene (PCE) 0.0386 0.0050 0.0398 97 74-148 Toluene 0.0330 0.0050 0.0398 83 76-131 1,2,3-Trichlorobenzene 0.0434 0.0050 0.0398 109 63-170 1,2,4-1'richloroben7ene 0.0433 0.0050 0.0398 109 71-165 _ 1,1,1-Trichloroethane 0.0349 0.0050 0.0399 88 74-137 1.1,2-Trichloroethane 0.0364 0.0050 0.0398 92 68-134 Trichloroethene (TCE) 0.0344 0.0050 0.0398 86 79-139 - , Trichlorofluoronmethane 0.0382 0.0050 0.0398 96 32-154 1,2,3-Trichloropropane 0.0367 0.0050 0.0398 92 69-125 1,2.4-Trimethylbenzene 0.0390 0.0050 0.0398 98 67-144 1,3,5-Trimethylbenzene 0.0409 0.0050 0.0398 103 66-154 Vinyl chloride 0.0373 0.0050 0.0398 94 39-150 Xylenes(total) 0.115 0.0050 0.119 97 71-147 Surrogate: Uibronuglhmromethane 0.0474 0.0497 95 75-122 Surrogate: Toluene-dR 0.0478 0.0497 96 66-128 Sin•rogate:4-BromgJluoroben_ene 0.0490 0.0497 99 76-122 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 Benzene 0.0353 0.0050 mg'kg 0.0398 89 75-131 3 20 Bromobenzene 0.0390 0.0050 0.0398 98 75-136 6 20 Bromochloromethanc 0.0339 0.0050 0.0398 85 70-135 3 20 Bromodichloromethane 0.0349 0.0050 0.0398 88 76-137 4 20 - Bromotorm 0.0390 0.0050 0,0398 98 55-139 6 20 Bromomethane 0.0259 0.0050 0.0398 65 10-157 12 20 n-Butylbenzene 0.0425 0.0050 0.0398 107 62-166 7 20 sec-Butylbenzene 0.0487 0.0050 0.0398 122 72-167 7 20 tert-Butylbenzene 0.0459 0.0050 0.0398 115 69-158 7 20 Carbon tetrachloride 0.0363 0.0050 0.0398 91 70-140 4 20 C hlorobenzene 0.0396 0.0050 0.0398 99 76-137 6 20 Chloroethane 0.0404 0.0050 0.0398 101 10-164 2 20 Chloroform 0.0339 0.0050 0.0398 85 75-123 5 20 Chloromethane 0.0344 0.0050 0.0398 86 26-146 6 20 2-Chlorotoluene 0.0425 0,0050 0.0398 107 73-145 7 20 - 4-Chlorotoluene 0.0431 0.0050 0.0398 108 67-151 6 20 Dibromochloromethane 0.0391 0.0050 0.0398 98 68-144 5 20 1.2-Dibromo-3-chloropropanc 0.0367 0.0050 0.0398 92 45-148 3 20 1,2-Dibromocthane (EDB) 0.0387 0.0050 0.0398 97 73-134 5 20 Dibronmonmcthanc 0.0337 0.0050 0.0398 85 70-140 3 20 1,2-Dichlorobenzene 0.0426 0.0050 0.0398 107 78-142 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 67 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Coinpounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 1,3-Dichlorobenzenc 0.0435 0.0050 mg/kg 0.0398 109 76-146 7 20 IA-Dichlorobenzene 0.0413 0.0050 0.0398 104 72-140 6 20 Dichlorodifluoromethane 0.0383 0.0050 0.0398 96 10-106 2 20 1,1-Dichloroethane 0.0354 0.0050 0.0398 89 65-139 4 20 1,2-Dichlorocthene 0.0346 0.0050 0.0398 87 67-125 3 20 1, 1 -Dichloroethene 0.0372 0.0050 0.0398 93 54-169 3 20 cis-] 2-Dichloroethene 0.0359 0.0050 0.0398 90 74-135 4 20 trans-1,2-Dichloroethene 0.0389 0.0050 0.0399 98 68-149 4 20 12-Dichloropropane 0.0350 0.0050 0.0398 88 74-130 4 20 1,3-Dichloropropane 0.0372 0.0050 0.0398 93 68-130 4 20 2,2-Dichloropropane 0.0403 0.0050 0.0398 101 33-187 2 20 l,l-Dichloropropene 0.0365 0.0050 0.0398 91 71-140 4 20 cis-13-Dichloropropene 0.0362 0.0050 0.0398 91 78-135 4 20 trans-1,3-Dichloropropene 0.0415 0.0050 0.0398 104 70-137 5 20 ' Ethylbenzene 0.0402 0.0050 0.0398 101 69-143 6 20 Ilexachlorobutadiene 0.0509 0.0050 0.0398 128 69-203 6 20 4-Isopropyl Toluene 0.0471 0.0050 0.0398 118 74-154 7 20 Isopropylbenzene 0.0437 0.0050 0.0398 110 72-157 7 20 Methylene chloride 0.0333 0.0050 0.0398 84 49-129 4 20 Naphthalene 0.0453 0.0050 0.0398 114 61-158 6 20 ❑-Propylbenzene 0.0443 0.0050 0.0398 111 69-147 6 20 Styrene 0.0410 0.0050 0.0398 103 71-144 6 20 1,1,1,2-Tetrachlorocthane 0.0402 0.0050 0.0398 101 78-132 6 20 1,1,2.2-Tetrachlorocthane 0.0407 0.0050 0.0398 102 64-138 4 20 Tetrachlorocthene WCE) 0A412 0.0050 0.0399 103 74-14S 6 20 Toluene 0.0349 0.0050 0.0398 88 76-131 6 20 1,2,3-Trichlorobenzene 0.0459 0.0050 0.0399 115 63-170 6 20 1,2,4-Trichlorobenzene 0.0448 0.0050 0.0399 112 71-165 4 20 . 1,1,1-Trichloroethane 0.0365 0.0050 0.0398 92 74-137 5 20 1,12-Trichloroethane 0.0386 0.0050 0.0398 97 68-134 6 20 Trichloroethene (TCE) 0.0365 0.0050 0.0398 92 79-139 6 20 Trichlorofluoromethane 0.0398 0.0050 0.0398 100 32-154 4 20 1,2,3-Trichloropropane 0.0384 0.0050 0.0398 96 69-125 5 20 1,24-Trimethylbenzene 0.0422 0.0050 0.0398 106 67-144 8 20 1,3.5-Trimethylbenzene 0.0437 0.0050 0.0398 110 66-154 7 20 Vinyl chloride 0.0382 0.0050 0.0398 96 39-150 2 20 Xylenes (total) 0.123 0.0050 0.120 103 71-147 7 20 Surrogate. Dibronwlhcoromethunc, 0.0467 0.049S 94 75-122 Surrogate: Toluene-dN 0.0473 0.0498 95 66-128 - , Surrogate: 4-BromoJluorobenzene 0.0495 0.0498 99 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 68 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 Benzene ND 0.0050 mg%kg ND 20 Bmmobenzene NI) 0.0050 ND 20 Bromochloromcthanc ND 0.0050 ND 20 Bromodichloromethane NI) 0.0050 ND 20 Bromofonn ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene NI) 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform NI) 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 NI) 20 4-C:hlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane ND 0.0050 ND 20 1,2-Dibronioethane (EDB) ND 0.0050 ND 20 Dibromomcthanc ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 NI) 20 1,3-Dich1orobenzene ND 0.0050 ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromethane ND 0.0050 ND 20 1,1-Dichloroethane ND 0.0050 ND 20 1,2-Dichloroethene ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 cis-L2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1.1-Dichloropropene ND 0.0050 ND 20 cis-1.3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 I:thylbenzene ND 0.0050 ND 20 Ilexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 lsopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 69 of 79 rZ Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (BlC0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 Styrene ND 0.0050 mg/kg ND 20 1, 1, 1,2-Tetrachloroethane ND 0.0050 " ND 20 1,1,2.2-Tetrachloroethane ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2.4-Trichloroben7ene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 I,12-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Triclilorofluoromethane ND 0.0050 ND 20 1,2,3-Trichloropropane ND 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate. Dibrornolluoromcthane 0.0460 0.0496 93 75-122 Surrogate: Toluene-d8 0.0472 0.0496 95 66-128 Surrogate: 4-Bromo/luorohenrene 0.0480 0.0496 97 76-122 Matrix Spike (BlC0817-MST) Source: 2101841-12 Analyzed: 03/26/21 20:05 Benzene 0.0322 0.0050 mgIg 0.0399 ND 81 36-146 Bromobenzene 0.0319 0.0050 0.0399 ND 80 28-152 Bromochloromcthane 0.0323 0.0050 0.0399 ND 81 43-146 Bromodichloromethane 0.0322 0.0050 0.0399 ND 81 43-153 Bromoform 0.0376 0.0050 0.0399 ND 94 26-151 Bromomethane 0.0290 0.0050 0.0399 ND 73 10-158 n-Butylbenzene 0.0242 0.0050 0.0399 ND 61 10-171 sec-Butylbenzene 0.0324 0.0050 0.0399 ND 81 10-176 tert-Butylbenzene 0.0335 0.0050 0.0399 ND 84 19-168 Carbon tetrachloride 0,0322 0.0050 0.0399 ND 81 29-151 Chlorobenzene 0.0337 0.0050 0.0399 ND 84 31-151 Chloroelhane 0.0346 0.0050 0.0399 ND 87 13-160 Chloroform 0.0316 0.0050 0.0399 ND 79 44-137 Chloromethane 0.0329 0.0050 0.0399 ND 82 10-144 2-Chlorotoluene 0.0335 0.0050 0.0399 ND 84 24-158 4-Chlorotoluene 0.0330 0.0050 0.0399 ND 83 19-160 Dibromochloromethatie 0.0370 0.0050 0.0399 ND 93 40-153 1,2-Dibromo-3-chloropropane 0.0333 0.0050 0.0399 ND 84 21-164 1,2-Dibromoethane (EDB) 0.0366 0.0050 0.0399 ND 92 41-148 Dibromomcthanc 0.0315 0.0050 0.0399 ND 79 45-158 1,2-Dichlorobenzene 0.0325 0.0050 0.0399 ND 82 24-158 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 70 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GUMS - Quality Control "alyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 r Matrix Spike (B1C0817-MSI) Source: 2101841-12 Analyzed: 03/26/21 20:05 13-Dichlorobenzenc 0.0321 0.0050 mgIg 0.0399 ND 80 19-160 IA-Dichlorobenzene 0.0305 0.0050 0.0399 ND 76 20-152 Dichlorodifluoromethane 0.0373 0.0050 0.0399 ND 93 10-153 1. 1 -Dichloroethane 0.0332 0.0050 0.0399 ND 83 35-148 1.2-Dichlorocthane 0.0321 0.0050 0.0399 ND 80 42-132 I,1-Dichloroethene 0.0345 0.0050 0.0399 ND 86 18-174 cis- 1,2-Dichloroethene 0.0335 0.0050 0.0399 ND 84 41-146 trans- I .2-Dichloroethene 0.0354 0.0050 0.0399 ND 89 27-161 1,2-Dichloropropane 0.0321 0.0050 0.0399 ND 80 42-145 1,3-Dichloropropane 0.0358 0.0050 0.0399 ND 90 42-141 .-- 2.2-Dichloropropane 0.0344 0.0050 0.0399 ND 86 10-166 l,1-Dichloropropene 0.0321 0.0050 0.0399 ND 80 28-151 cis-1,3-Dichloropropene 0.0320 0.0050 0.0399 ND 80 38-148 trans-1,3-Dichloropropene 0.0376 0.0050 0.0399 ND 94 36-144 Ethylbenzene 0.0324 0.0050 0.0399 ND 81 16-162 1lexachlorobutadiene 0.0223 0.0050 0.0399 ND 56 10-193 4-Isopropyl Toluene 0.0300 0.0050 0.0399 ND 75 11-167 Isopropylbenzene 0.0328 0.0050 0.0399 ND 82 13-174 Nlethylene chloride 0.0310 0.0050 0.0399 ND 78 30-131 Naphthalene 0.0314 0.0050 0.0399 ND 79 10-178 n-Propylbenzene 0.0325 0.0050 0.0399 ND 81 12-160 -- Styrene 0.0336 0.0050 0.0399 ND 84 23-160 1, 1, 1,2-Tetrachloroethane 0.0368 0.0050 0.0399 ND 92 36-152 1,1,2,2-Tetrachloroethanc 0.0305 0.0050 0.0399 ND 91 19-175 Tetrachloroethene WCE) 0.0339 0.0050 0.0399 ND 85 23-162 Toluene 0.0291 0.0050 0.0399 ND 73 26-152 1,2,3-Trichlorobenzene 0.0262 0.0050 0.0399 ND 66 10-168 1,24-Trichlorobenzene 0.0257 0.0050 0.0399 ND 64 10-170 - 1, 1, 1 -Trichloroethane 0.0334 0.0050 0.0399 ND 84 36-150 1,12-Trichloroethane 0.0364 0.0050 0.0399 ND 91 25-179 Trichloroethene (TCE) 0.0338 0.0050 0.0399 ND 85 29-167 Trichlorofluoroniethane 0.0379 0.0050 0.0399 ND 95 15-156 1,2.3-Tricliloropropane 0.0376 0.0050 0.0399 ND 94 26-177 1,2,4-Trimethylbenzene 0.0308 0.0050 0.0399 ND 77 14-157 1,35-Trimethylbenzene 0.0323 0.0050 0.0399 ND 81 10-167 Vinyl chloride 0.0368 0.0050 0.0399 ND 92 14-154 - 7 Xylenes (total) 0.0983 0.0050 0.120 ND 82 21-162 Surrogate: Dibromollttoromcthane 0.0459 0.0499 92 75-122 Surrogate: Toluene-d8 0.0473 0.0499 95 66-128 Su•rogate:4-Bromollaorohenzene 0.O486 0.0499 97 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 71 of 79 WIL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Total Metals by ICP 6010B Total Antimony EPA 6010B Solid OEC, CA-ELAP 6010B Total Arsenic EPA 6010B Solid OEC, CA-ELAP 6010B Total Barium EPA 6010B Solid OEC. CA-ELAP 6010B Total Beryllium EPA 6010B Solid OEC, CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010B Total Chromium EPA 6010B Solid OEC, CA-ELAP 6010B Total Cobalt EPA 6010B Solid OEC, CA-ELAP 6010B Total Copper EPA 6010B Solid OEC_ CA-ELAP 6010B Total Lead EPA 601 pB Solid OEC, CA-ELAP 6010B Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 6010B Total Nickel EPA 6010B Solid OEC, CA-ELAP 6010B Total Selenium EPA 6010B Solid OEC. CA-ELAP 0010B Total Silver EPA 6010B Solid OEC, CA-ELAP 6010B Total Thallium EPA 6010B Solid OEC, CA-ELAP 6010B Total Vanadium EPA 6010B Solid OEC, CA -FLAP 6010B Total Zinc EPA 6010B Solid OEC, CA -FLAP Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC. CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 73 of 79 w• �y W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 80151TH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OFC, CA-ELAP 8015 TPH-Gasoline EPA 9015M Solid OEC_ Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-F,LAP 8015 TPH-Gasoline EPA 9015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805.) 925-3376 Page 74 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference ' D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. D-00 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. --• N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-03 The RPD value for the sample duplicate or MSIMSD was outside of QC acceptance limits due to matrix interference. QC batch accepted based on LCS and or LCSD recovery and/or RPD values. ' QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. • S-02 The surrogate recovery for this sample cannot be accurately- quantified due to interference from coelutine organic compounds present in the sample extract. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 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Box 2646 Report Date: March 26, 2021 17:07 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Centers, 2600 Broad St. Enclosed is an analytical report for the above referenced project. The samples included in this report were received on March 25, 2021 15:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: 114:n.tdA6 �'A-) Meredith Sprister, Business Director msprister d)oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample Summary Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Tank N Wall 2101841-01 Solid Solid 03/25/2021 11:15 03/25/2021 15:00 Tank S Wall 2101841-02 Solid Solid 03/25/2021 11:20 03/25/2021 15:00 Tank E Wall 2101841-03 Solid Solid 03/25/2021 11:25 03/25/2021 15:00 Tank W Wall 2101841-04 Solid Solid 03/25/2021 11:30 03/25/2021 15:00 Tank Bottom E. End 2101841-05 Solid Solid 03/25/2021 11:05 03/25/2021 15:00 Tank Bottom W. End 2101841-06 Solid Solid 03/25/2021 11:10 03/25/2021 15:00 Sump Trench W 2101841-07 Solid Solid 03/25/2021 11:35 03/25/2021 15:00 Sump Trench S 2101841-08 Solid Solid 03/25/2021 11:38 03/25/2021 15:00 Control 2101841-09 Solid Solid 03/25/202111:00 03/25/2021 15:00 Soil Pile N 2101841-10 Solid Solid 03/25/2021 11:40 03/25/2021 15:00 Soil Pile S 2101841-11 Solid Solid 03/25/2021 11:45 03/25/2021 15:00 Soil Pile W 2101841-12 Solid Solid 03/25/2021 11:50 03/25/2021 15:00 Soil Pile E 2101841-13 Solid Solid 03/25/2021 12:10 03/25/2021 15:00 Sample Batch Preparation Analysis Batch ID Preparation Date/Time Semi -Volatile Organic TPH by GC/FID 9015 Diesel & Motor Oil List BIC0799 03/25/2021 17:29 Total Metals by CVAA Mercury Total EPA 7471 A B 1 C0807 03/26/2021 07:43 Total Metals by ICP 601013Total B 1 C0810 03/26/2021 08:36 Volatile Organic Compounds by GUMS 8260B Full List B I C0815 03/26/2021 09:17 8260B Full List B I C0817 03/26,2021 1 1:40 Volatile Organic TPH by GC/FID 8015 TPI I -Gasoline B 1 C'0802 03/26/2021 05:22 9015 TPH-Gasoline B 1 C0804 03/26/2021 05:26 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report foi- Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 B 1 C0807 03/26/21 14:37 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 Bl('0810 03/26/21 13:30 EPA6010B Arsenic 8.9 2.0 Barium 150 0.98 Bervllium 0.61 0.49 Cadmium ND 0.24 Chromium 51 0.49 N-02 Cobalt 17 0.49 .-, Copper 28 0.98 Lead 9.1 0.49 Molybdenum 2.6 0.49 Nickel 76 0.49 Selenium ND 2.0 " Silver ND 0.49 . Thallium ND 0.98 Vanadium 39 2.0 Zinc 32 2.0 " Volatile Organic TPH by GC/FID TPH Gasoline (C5-02) ND 4.9 mg/kg I BIC0802 03/26/21 10:47 EPA 8015M R-07 Surrogate: 4-BromnJluoroben_ene 103 94, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 BIC0798 03/26/21 07:48 EPA 8015M TPII Motor Oil (('23-C40) ND 50 " " " " 11 Surrogate: o-Teiphcnrl 107 , (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 65 ui Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BIC0815 03/26/21 11:52 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND L2 Chlorobcnzcne ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronui-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromcthanc ND 1.2 I,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-L2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND L2 Ethylbenzcnc ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 65 --I Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID : Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg%kg 1000 B I C0815 03/26'21 11:52 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 I.1,2,2-Tetrachloroethane ND 1.2 Tetrachlorocthene (ICE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1.1,2-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1.2,4-Trimethylbenzene ND 1.2 " 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcnes (total) ND 1.2 Surrogate: Dihromolluoromethanc 97 % (75 - 122 ) Surrogate: Toluene-d8 92 f ( 66 - 128) Surrogate: 4-Bromollum-oheu_ene 92 % (76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report mist be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical t Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by : Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mg/kg 1 B I C0907 03/26/21 14:39 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg!kg I B I C0810 03/26/21 13:33 EPA 601013 Arsenic 4.1 2.0 Barium 11 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 9.0 0.49 " Cobalt 1.4 0.49 Copper 3.5 0.98 Lead 2.5 0.49 Molybdenum 3.3 0.49 " Nickel 6.8 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 6.3 2.0 Zinc 9.7 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.5 mg/kg 1 BIC0802 03!26'21 11:13 EPA 8015M R-07 Surrogate: 4-Bromoguoroben_ene 103 3� (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-('22) ND 10 mg/kg 1 BIC0798 03/26/21 10:07 EPA 8015M TPH Motor Oil (C23-('40) ND 50 " " " " 11 Surrogate: o-TerphenYl 106 40 (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID : Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 BIC0815 03/26/21 12:17 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 r+ Bromofonn ND 1.2 Bromomelhane ND 1.2 " n-Butvlbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 r Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 12-Dibromo-3-chloropropane ND 1.2 12-Dibronioethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 " Dichlorodifluoromcthanc ND 1.2 I,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND 1.2 + cis- 1.2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 " 1.2-Dichloropropane ND 1.2 " 13-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 I.I-Dichloropropane ND 1.2 cis- I3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mgtkg 1000 B1 C0815 03/26/21 12:17 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 1,1,1,2-Tetrachlorocthane ND 1.2 1,1,2.2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (ICE.) ND 1.2 Toluene ND 1.2 1,2,3-Trichloroben7ene ND 1.2 1,24-Trichlorobenzene ND 1.2 1,1,1-Triehloroethane ND 1.2 1,1,2-Triehloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 12,4-Trimethylbenzene ND 1.2 13,5-Trimethylbeuzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogule. Dibromoflu romethane 92'N ( 75 - 122) Surrogate: Toluene-(M 84 ( 66 - 128 ) Surrogate: 4-Bromn/luoruben_ene 92 % (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank E Wall Sampled : 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg!kg 1 B 1('0807 03/26/21 14:41 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B I C0810 03/26/21 13:36 EPA 6010B Arsenic 4.2 1.9 Barium 140 0.95 Beryllium 0.51 0.47 - Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 16 0.47 r . Copper 23 0.95 Lead 7.0 0.47 Molybdenum ND 0.47 Nickel 72 0.47 " Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 33 1.9 Zinc 20 1.9 Volatile Organic TPH by GC/FID TPA Gasoline (C5-C12) ND 4.6 mg/kg I BI C0802 03/26121 11:39 EPA 8015M R-07 Surrogate: 4-Bromo%luoroben_ene 104 % (31 - 16N ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-('22) ND 9.9 mg'kg 1 B1('0798 03/26/21 08:02 EPA 8015M - TPH Motor Oil (C 23-('40) ND 50 " " " " " Surrogate: o-TetphenYl ION °1 (65 - 133) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 0%65 lit Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgtkg 1000 B1C0815 03/26/21 12:43 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bmniofonn ND 1.2 Bromomethane ND 1.2 n-Butvlbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chloroelhane ND 1.2 Chlorotbrnn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1.2-Dibromoethane (FDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodifluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 13-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 " 1, 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Fthylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analvtical Report Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID: 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 BIC0815 03/26/2112:43 EPA8260B r 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 " Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Sivrene ND 1.2 " 1,1,1,2-Tetrachloroethane ND 1.2 1,1.22-Tetrachloroethane ND L2 Torachloroethcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcnzcnc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroelhane ND 1.2 ^ 1,1,2-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 " Trichlorotluoromethane ND 1.2 _ 1,23-Trichloropropane ND 1.2 1,2,4-1'rimethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Uibromolluoromethane 92 , (75 - 122) " Surrogate: Tolnenc-db' 95 '%„ (66 - 12S) 11" Surrogate: 4-Bromq luoruben_ene 90 4& ( 76 - 122) 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 oj65 ( A im, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report i Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg 1 BIC0807 03/26/2114:44 EPA 7471A Total Metals by ICP Antimony ND 2.3 mgIg 1 BIC0810 03/26/2113:38 EPA 601OB Arsenic 2.6 1.8 Barium 5.8 0.92 Beryllium ND 0.46 Cadmium ND 0.23 " Chromium 6.9 0.46 Cobalt 0.92 0.46 Copper 1.9 00.92 Lead 3.7 0.46 Nlolvbdenum 2.6 0.46 Nickel 4.1 0.46 Selenium ND 1.8 Silver ND 0.46 Thallium ND 0.92 Vanadium 4.6 1.8 Zinc 6.8 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) 35 5.1 mg/kg 1 BIC0802 03/26/21 12:05 EPA 8015M Surrogate: 4-Bromo/luorohencene 14N IN, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (Cl3-C22) 17 9.9 mg/kg 1 BIC0798 03/26'21 11:03 EPA 8015M D-04 - TPH Motor oil (C23-C40) 72 50 " " " "11D-04 Surrogate: o-Teiphen l 107 (65 - 133) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B1C0815 03/26/21 13:08 EPA8260B . _ Brontobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butvlbenzene ND 1.2 T sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chlorocthane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethanc ND 1.2 ,.z 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromontethane ND 1.2 1,2-Dichloroben7enc ND 1.2 " - 1,3-Dichlorobenzenc ND 1.2 " 14-Dichlorobenzenc ND 1.2 Dichlorodilhuoromciliane ND 1.2 1, 1 -Dichloroethane ND 1.2 12-Dichloroethane ND 1.2 I,I-Dichloroethene ND 1.2 - cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 " �T 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 llexachlombutadiene ND 1.2 mglkg 1000 B1('0815 03/26/21 13:08 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 - Naphthalene ND 12 n-Propylbenzene ND 1.2 " Styrene ND 1.2 �- 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 " Tolucnc ND 1.2 1,2,3-Trichlorobenzcnc ND 1.2 1,2,4-Trichlombenzene ND 1.2 1,1,1-Trichlomeihane ND 1.2 '— 1,1,2-Trichloroethane ND 1.2 Tiichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 " 1,2.4-Triniethylbenzene ND 1.2 1,3.5-Trinmthylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate. Dihromolluoromethane 95 % ( 75 - 122 ) Surrogate: Toluene-d$ 95 % ( 66 - 12S) " Surrogate: 4-Bromolluuroheu_ene 92 % (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID : Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by: Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mg/kg I B 1 C 0807 03/26/21 14:46 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mglkg 1 B I C0910 03/26/21 13:41 EPA 601(1B Arsenic 5.4 1.9 " Barium 32 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 15 0.47 Cobalt 4.3 0.47 Copper it 0.93 " Lead 8.3 0.47 Molvbdenum 2.9 0.47 Nickel 19 0.47 Selenium ND 1.9 Silver ND 0.47 _ Thallium ND 0.93 Vanadium 13 1.9 Zinc 19 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 35 4.9 mg,!kg I BIC0802 03/26/21 12:31 EPA 8015M Surrogate: 4-Bromn/luurohenzcne 145 `%n (31 - 168) Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-C22) 11 10 mg/kg 1 BIC0798 03/2621 11:31 EPA 8015M D-04 TPH Motor Oil (C23-C40) 110 50 " " " "11D-04 Surrogate: o-Terphenrl 100 `%", (65 - 733) "11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 8D5 925-3376 Page 15 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mg/kg 1000 B1('0815 03/26/21 13:34 EPA8260B Bromobenzene ND 1.2 Bromochlorometlrane ND 1.2 Bromodichloromethane ND 1.2 - Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 .-- Chloroethanc ND 1.2 Chloroform ND 1.2 Chlorotnethane ND 1.2 ^ 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochlommethane ND 1.2 " 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibrontoethane (EDB) ND 1.2 Dibromomethanc ND 1.2 12-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 14-Dichlorobenzene ND 1.2 Dichlorodilluoromethanc ND 1.2 ^ 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 LI-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 " tans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 _ 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1. 1 -Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzcnc ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mglkg 1000 B1C0815 03/26/21 13:34 EPA8200B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1,12,2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 " 1.2.4-Trichlorobenaene ND 1.2 1,1,1-Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluorotnethane ND 1.2 1.2.3-Trichloropropane N'D 1.2 I.2,4-Trimethylbenzene ND 1.2 1.3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 " Surrogate: Dihnm:olluoro»ii'thaue 95,111, (75 - 122 ) Surrogate: Toluene-dS 86 W, (66 - 12S ) . , Surrogate: 4-Bron q luoroheteene 94 % ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 _ Matrix: Solid Sampled by: Lab ID: 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg!kg 1 Bl C0807 03/26/21 14:48 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgtkg 1 BIC0810 03/26/21 13:44 EPA 6010B Arsenic ND 2.0 Barium 9.9 0.98 Beryllium NI) 0.49 Cadmium ND 0.24 Chromium 8.0 0.49 Cobalt 1.2 0.49 Copper 1.6 0.98 Lead 3.4 0.49 " Molybdenum 1.1 0.49 Nickel 4.7 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 5.9 2.0 Zinc 7.9 2.0 ' Volatile Organic TPH by GC/FID 'IPH Gasoline (C5-('12) 6.1 4.5 mg'kg 1 Bl('0804 03/26/21 10:5.5 EPA 8015M Surrogate. 4-Bromn/luorohen:7ene 108 % (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-C22) ND 9.9 mgIg 1 Bl('0798 03/26/21 1021 EPA 8015M - . TPH Motor Oil (('23-C4111 ND 50 " " " " ° Surrogate o-Tetphenyl 106 b (65 - 133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID : Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by : Lab ID: 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mglkg 1000 B1 C0815 03/26/21 13:59 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " -• Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 T Chlorocthanc NU rr rr 1.2 rr rr rr Chloroform ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 _ 12-Dibromo-3-chloropropanc ND 1.2 " 1,2-Dibrontoethane (FDB) ND 1.2 Dibromomethane ND 12 " 1,2-Dichlorobenzene ND 1.2 " - 1,3-Dichlorobenzene ND 1.2 14-Dichlorobenzene ND 1.2 DichlorodiFluoromethanc ND 1.2 1,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropene ND 1.2 1,3-Dichloropropane ND 1.2 2.2-Dichloropropene ND 1.2 1, 1 -Dichloropropene ND L2 " cis-1.3-Dichloropropene ND L2 trans-1,3-Dichloropropene ND 1.2 Fthylbcnzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples 5 1 Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID: 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 I Iexachlorobutadiene ND 1.2 mg/kg 1000 B 1 C 0815 03/26/21 13:59 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 " Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 1,1,1,2-Tetrachloroethane .. ND 1.2 1,L2,2-Tetrachloroethane ND 1.2 TC1racliloroctllene (PCE) ND 1.2 Toluene ND 1.2 12,3-Trichloroben7enc ND 1.2 1,2,4-Trichloroben7ene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 - - 1,1,2-Trichloroethane ND 1.2 Trichloroethenc (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 L2,4-Trimethylbenzene ND 1.2 13.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dibromofluoromethane 93'% (75-122) Surrogate: Toluene-d8 88 '/ (66 - 128 ) Surrogate: 4-Brontolluoroben_ene 94 /, (76 - 122 ) --I The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by : Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mgtkg 1 B 1('0807 03/26/21 14:54 EPA 7471 A Total Metals by ICP Antimony 8.2 2.4 mg/kg 1 B 1('0810 03/26/21 13:47 EPA 601(IB - Arsenic 8.9 1.9 Barium 260 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 55 0.48 N-02 Cobalt 12 0.48 Copper 120 0.96 Lead 550 0.48 N-02, N-03 Molvbdenum 1.1 0.48 Nickel 150 0.48 Selenium ND 1.9 Silvcr ND 0.48 Thallium ND 0.96 " Vanadium 33 1.9 "Zinc 720 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) ND 4.9 mg/kg I B1C0804 03/26'21 11:52 EPA 8015M R-07 Surrogate: 4-Bromojluoruben:ene 100 %, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 71 40 mg/kg 4 BIC0798 03/26'21 11:59 EPA 8015M D-04 TPH Motor Oil (C23-C40) 520 200 " " " "11D-04 .Surrogate: o-Tel foetid 108 `/o (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg!kg 1000 B1 C0815 03/26/21 14:25 EPA 8260E Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butvlbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloridc ND 1.2 " Chlorobenzene ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzcnc ND 1.2 1,4-Dichlorobenzcnc ND 1.2 DichlorodiflttOrOnlethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 " cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1.1-Dichloropropene ND 1.2 cis- 1.3 -Dichloropropene ND 1.2 trans-1,3-Dichloropropcne ND 1.2 Ethylbcnzene ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sample ID : Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlombutadiene ND 1.2 mgtkg 1000 B1('0815 03/26/2114:25 F.PA9260B 4-Isopropyl Toluene ND 1.2 " Nopropylbenzene ND 1.2 Methylene chloride ND 1.2 " Naphthalene ND 1.2 " n-Propylbenzenc ND 1.2 " Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 Tetrachloroethane WE') ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichloroben7ene ND 1.2 " 1, 1. 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 " 12,4-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 " Xylenes (total) ND 1.2 Surrogate: Dihrom(;ihenrome thane 97'N ( 75 - 12 2 ) Surrogate: Toluene-dS 90 ";' (66 - 128 ) Surrogate: 4-Bro,no/lum-eihen_ene 88'S„ ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples — Sample ID: Sump Trench S Sampled: 03/25/21 11:38 ' Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mglkg I B 1 C0807 03/26/21 14:56 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgtkg I B 1 C0810 03/26/21 13:50 EPA 601(IB Arsenic 4.1 1.9 Barium 180 0.96 Bergilium 0.53 0.48 Cadmium ND 0.24 Chromium 78 0.48 N-02 Cobalt 16 0.49 Copper 31 0.96 Lead 37 0.49 Molybdenum ND 0.48 Nickel 100 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 47 1.9 " Zinc 69 1.9 Volatile Organic TPH by GC/FID Tell Gasoline (C5-C12) ND 4.7 mg/kg I BIC0804 03/26/21 12:20 EPA 8015M R-07 Surrogatc: 4-Bromollaoroben_ene 107 `!b (31 - 168) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 27 9.9 mg%kg 1 B 1('0798 03/26/21 13:02 EPA 8015M D-06 TPll Motor Oil (C23-C40) 610 50 " " " " 11 Snrrogule: o-Teiphenpl 107" (65 - 133) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 24 of 65 r A W6 TAR Ma Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report i Sample ID: Sump Trench S Sampled: 03/25/21 11:38 r' Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 Bl C 0817 03/26/21 13:46 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 " Chlorobcnzenc ND 0.0050 " Chlorocthanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 - 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromelhane ND 0.0050 1,2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (ED13) ND 0.0050 Dibromomethane ND 0.0050 1.2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 14-Dichlorobenzene ND 0.0050 Dichloroditluoromcthanc ND 0.0050 ` l,l-Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 " cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 12-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 2.2-Dichloropropane ND 0.0050 I,1-Dichloropropene ND 0.0050 cis-l3-Dichloropropene ND 0.0050 ' trans-1,3-Dichloropropene ND 0.0050 " L'thylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 65 i A W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by : Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Hexachlorobutadienc ND 0.0050 mg'kg 1 B I C0817 03/26/21 13:46 EPA 8200B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Piopylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.0050 1.1,22-Tetrachloroethane ND 0.0050 Tctrachlorocthcne Wli) ND 0.0050 Toluene ND 0.0050 ' 1,23-Trichlombenzenc ND 0.0050 1,2,4-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 •—• 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0,0050 1,2.3-Trichloropropane ND 0,0050 1,24-Trimethylben7ene ND 0.0050 1,3.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: Dibromolhuoromelhanc 94 % ( 75 - 122 ) Surrogate: Toluene-d8 89 44; ( 66 - 128 ) Surrogate: 4-Bronm/Iac roben_c'ne 89 %) ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples I Sample ID: Control Sampled: 03/25/21 11:00 -^ Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.14 0.095 mg/kg 1 B 1 C0807 03/26/21 14:58 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgtkg 1 B I C0810 03/26/21 13:52 EPA 6010B Arsenic 5.9 1.9 Barium 170 0.97 Beryllium 0.50 0.49 -� Cadmium ND 0.24 Chromium 41 0.49 Cobalt 16 0.49 .� Copper 27 0.97 Lead 10 0.49 Molybdenum ND 0.49 Nickel 38 0.49 " Selenium ND 1.9 Silver ND 0.49 Thallium ND 0.97 Vanadium 33 1.9 Zinc 27 1.9 Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 4.7 mg'kg 1 BIC0804 03/26/21 12:49 EPA 8015M R-07 Surrogate: 4-Bronm/luorohenzene 96 % (31 - 168) „ Semi -Volatile Organic TPH by GC/FID TPIIDiesel (C)3-C22) ND 10 mg/kg I BIC0798 03/26/2110:49 EPA8015M - . TPH Motor Oil (C23-C40) 85 50 " " " " " Surrogate: o-Telphem1 105 `%;, (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene NI) 0.0050 mg kg I BIC0817 03/20/21 14:44 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromofonn ND 0.0050 Bromomethane ND 0,0050 n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 C hlorobenzcnc ND 0.0050 " Chloroethanc ND 0.0050 Chlorofonn ND 0.0050 Chloromethane ND 0.0050 -- 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 12-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (EDB) NI) 0.0050 Dibromomethane ND 0.0050 1.2-Dichlorobenzene ND 0.0050 1.3-Dichlorobcnzcnc NJ) 0.0050 14-Dichlorobcnzcnc ND 0.0050 Dichlorodifluoromcthane ND 0.0050 ^ 1, 1 -Dichloroethane NI) 0.0050 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 " cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 " 1,2-Dichloropropane ND 0.0050 13-Dichloropropane NI) 0.0050 " 2,2-Dichloropropane ND 0.0050 I.I-Dichloropropene ND 0.0050 cis- I3-Dichloropropene ND 0.0050 ' trans- I3-Dichloropropene ND 0.0050 " Ethylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples — Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID : 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) ilexachlorobutadiene ND 0.0050 mglcg 1 BIC0817 03/26/21 14:44 EPA 826013 ' 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 " ., Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1.1,1.2-Tetrachloroethane ND 0.0050 I.1,2.2-Tetrachloroethane ND 0.0050 Torachlorocthcne (PCE) ND 0.0050 TolL1e11C ND 0.0050 1,2,3-Trichlorobcnzene ND 0.0050 1,2,4-Trichloroben7ene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 " �• 1,1.2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0,0050 Trichlorofluoromethane ND 0.0050 r 1,2,3-Trichloropropane ND 0.0050 1.2.4-Trimethylbenzene ND 0.0050 1.3.5-Trimethylbenzene ND 0.0050 " Vinyl chloride ND 0.0050 - Xylenes (total) ND 0.0050 Surrogate: Dihromofluoromethane 93 % (75 - 122) " Surrogate: Toluene-dS 95 "; (66 - 128 ) Surrogate: 4-Brtmto/luorohcn_cne 98 4;, (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mg -kg 1 BIC0807 03/26/21 15:00 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg!kg I B I C0810 03/26/21 13:55 EPA 6010B Arsenic 3.6 2.0 Barium 13 1.0 Beryllium ND 0.50 - Cadmium ND 0.25 Chromium 11 0.50 " Cobalt 1.9 0.50 " Copper 5.3 1.0 Lead 4.3 0.50 Molybdenum 2.5 0.50 " Nickel 9.0 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND LO Vanadium 8.4 2.0 Zinc 8.8 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: d-Bromn/luorohenzeue Semi -Volatile Organic TPH by GC/FID TPII Diesel (C 13-C22 ) �. TPH Motor Oil (C23-C40) Surrogate o-Terphen.11 42 4.9 mg/kg 1 BIC0804 03/26/2113:17 EPA8015M 196i111 (31-16S) 11 11S-01 ND 9.9 mg/kg I BIC0798 03/26/21 10:35 EPA 8015M 52 50 " " " " " 106 `50 (05 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 30 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.045 mg/kg 1 BI C0817 03/26/21 12:49 EPA 826013 Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodiehloromethane ND 0.045 Bromoform ND 0.045 Bromomethane ND 0.045 n-Butylbenzene 0.22 0.045 " - sec-Butylbenzene 0.11 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 C'hlorobenzene ND 0.045 Chloroethane ND 0.045 " Chloroform ND 0.045 " Chloromethanc ND 0.045 2-Chlorotoluenc ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 1,2-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 _ 1,2-DlchlOTobenzene ND 0.045 1,3-Dichlorobenzene ND 0.045 14-Dichlorobenzene ND 0.045 Dichlorodilluoromethane ND 0.045 1. 1 -Dichlorocthanc ND 0.045 I.2-Dichloroethene ND 0.045 I,1-Dichloroethene ND 0.045 • cis-1,2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1,3-Dichloropropane ND 0.045 2.2-Dichloropropane ND 0.045 I,1-Dichloropropene ND 0.045 cis-1.3-Dichloropropene ND 0.045 - trans-1,3-Dichloropropene ND 0.045 " Etylbenzene ND 0.045 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 31 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sample ID : Soil Pile N Sampled: 03/25/21 11:40 P Sam Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-t.D7 Ilexachlorobutadiene ND 0.045 mg/kg 1 B I C0817 03/26/21 12:49 EPA 8200B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 �. Naphthalene ND 0.045 n-Propylbenzene 0.15 0.045 Styrene ND 0.045 .� 1,1,1,2-Tetrachloroethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachloroethene (PCE) ND 0.045 Toluene ND 0,045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1, 1, 1 -Trichloroethane ND 0.045 — I.1,2-Trichloroethane ND 0.045 Trichloroethenc LIVE) ND 0.045 Trichlorolluoromethane ND 0.045 1,2,3-Trichloropropane ND 0.045 1,2A-Trimcthylbcnzcne ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 .-, Xylenes (total) ND 0.045 S+a•rogale: Dibrorno/Lurre methane 92 ;' ; (75 - 122 ) surrogutc: Toluene -de 97 % (66 - 128 ) Surrogate: 4-Bromu/luorobenzcrre 99 ("'0 (7(- 111 ) , r-. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 32 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report t Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by : Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mgtkg 1 B I C0807 03/26/21 15:02 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg'kg I B1('0810 03/26/2114:06 EPA 6010B Arsenic 4.5 2.0 " Barium 47 H) Beryllium ND 0.50 _ Cadmium l ND 0.25 Chromium 18 0.50 Cobalt 3.6 0.50 Copper 9.8 1.0 Lead 16 0.50 Nlolvbdenum 2.1 0.50 Nickel 36 0.50 Selenium ND 2.0 " Silver ND 0.50 Thallium ND 1.0 Vanadium 15 2.0 Zinc 29 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) ND 4.4 mg/kg 1 B I C0804 03/26/21 13:46 EPA 8015M R-07 Surrogate: 4-Bromo/7110r017e1_ene 100 (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 mg/kg 1 BIC0798 03/26/21 12:27 EPA 8015M 7 TPII Motor Oil (C23-C40) 260 50 " " " Surrogate: o-Telpher. l 108 `: o (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 65 ri A M=Ll Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid. Sampled by: Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0049 mg/kg I BIC0817 03/26/21 15:13 F.PA8260B Bromobenzene ND 0.0049 Brontochloromethane ND 0.0049 Bromodichlorotnethane ND 0.0049 Bromofonn ND 0.0049 Bromomethane ND 0.0049 n-Butylbenzene ND 0.0049 sec-Butylbenzene ND 0.0049 tert-Butylbenzene ND 0.0049 Carbon tctrachloridc ND 0.0049 Chlorobenzene ND 0.0049 Chloroethanc ND 0.0049 Chloroform ND 0.0049 Chloromethane ND 0.0049 2-Chlorotoluene ND 0.0049 4-Chlorotoluene ND 0.0049 Dibromochloromethane ND 0.0049 1,2-Dibronto-3-chloropropane ND 0.0049 1,2-Dibromoethane (EDB) ND 0.0049 Dibromomethane ND 0.0049 1,2-Dichlorobenzene ND 0.0049 " 1,3-Dichlorobcnzcnc ND 0.0049 1.4-Dichlorobcnzcnc ND 0.0049 Dichloroditluoromcthanc ND 0.0049 - 1,1-Dichloroethane ND 0.0049 1,2-Dicliloroethane ND 0.0049 l,l-Dichloroethene ND 0.0049 " cis-1.2-Dichloroethene ND 0.0049 " trans-1,2-Dichloroethene ND 0.0049 1,2-Dichloropropane ND 0.0049 1.3-Dichloropropane ND 0.0049 2,2-Diclloropropane ND 0.0049 1.I-Dichloropropane ND 0.0049 cis-1.3-Dichloropropanc ND 0.0049 ' trans-1,3-Dichloropropcne ND 0.0049 Ethylbcnzenc ND 0.0049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 34 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Sarnples Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by : Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Hexachlorobutadiene ND 0.0049 mg -kg 1 BIC0817 03/26/2115:13 EPA8260B 4-Isopropyl Toluene ND 0.0049 lsopropylbenzene ND 0.0049 " Methylene chloride ND 0.0049 " Naphthalene ND 0.0049 n-Propylbenzene ND 0.0049 Styrene ND 0.0049 1,1,1.2-1'etrachloroethane f ND 0.0049 1. 1 .2.2-Tetrachloroethane ND 0.0049 Tctrachloroethcnc (PCE) ND 0.0049 Toluene ND 0.0049 12,3-Trichlorobenzenc ND 0.0049 12.4-Trichlorobenzene ND 0.0049 1, 1, 1 -Trichloroethane ND 0.0049 - 1,1,2-Trichloroethane ND 0.0049 Trichloroethene (TC'E) ND 0.0049 Triehlorolluoromethane ND 0.0049 1.2.3-Trichloropropane ND 0.0049 1.2,4-Trintethylbenzene ND 0.0049 13,5-Trimethylbenzene ND 0.0049 Vinyl chloride ND 0.0049 Xylenes (total) ND 0.0049 Surrogate: Dihronujllaoromcthune 91 IN ( 75 - 12 2 ) Surrogate: Toluene-dfi 95 (66 - 12S) " Surrogate: 4-Brotnu1luorohen_cne 97 ON, ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample ID : Soil Pile W Analytical Report for Samples I Sampled : 03/25/21 11:50 ' Matrix: Solid Sampled by : Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mgtkg 1 B I C0807 03/26/21 15:04 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mgtkg 1 B 1 C0810 03/26/21 14:09 EPA 6010B Arsenic 5.6 1.9 Barium 23 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 14 0.47 Cobalt 2.5 0.47 Copper 6.8 0.93 Lead 7.3 0.47 Molybdenum 3.7 0.47 " Nickel 11 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 15 1.9 Zinc 15 1.9 - ' Volatile Organic TPH by GC/FID TPHGasoline (C5-C12) ND 4.7 mg/kg 1 BIC0804 03/26/2114:14 EPA8015M R-07 Surrogate: 4-B1-omo/btoroben_ene 10-3 "i, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-C22) ND 9.9 mg/kg 1 B1('0798 03t26 21 11:17 EPA 8015M TPH Motor Oil (C23-C40) 75 50 " " " " D-04 Surrogute: o-Teiphc'm 1 107'% (65 - 133 ) cm The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 36 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID : Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by : Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0050 mglkg 1 B I C0817 03/26/21 15:43 EPA 826013 Bromobenzene ND 0.0050 Brotnochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 -� Bromofonn ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene NJ) 0.0050 �sec-Butylbenzene NI) 0.0050 tert-Butylbenzene NI) 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzene NU 0.0050 Chloroethanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-C'hlorotoluene ND 0,0050 Dibromochloromethane ND 0.0050 1,2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibronioetliane (EDB) ND 0.0050 " Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 .. 1.3-Dichlorobcnzcnc ND 0.0050 14-Dichlorobcn7cnc ND 0.0050 Dichloroditluoromcthane ND 0.0050 " - ' 1 .1 -Dichloroethane NE) 0.0050 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 00050 - cis-1,2-Dichloroethene ND 0.0050 " trans-L2-Dichloroethene ND 0.0050 " 1,2-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 L I -Dichloropropene ND 0.0050 cis-1.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Ethylbenzenc NI) 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 65 rrr .-r r- r Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report t Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) Ilexachlorobutadiene ND 0.0050 mg/kg 1 B1('0817 03/26/21 15:43 EPA8260B 4-Isopropyl Toluene ND 0.0050 lsopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,12-Tetrachloroethane ND 0.0050 1,1,22=letrachloroethane ND 0.0050 Tetrachlorocthcne (PCE) ND 0.0050 Toluene ND 0.0050 1,2.3-Trichlorobenzcnc ND 0.0050 1,2,4-Trichlorobenzenc ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND Ol 0050 Trichlorolluoromethane ND 0.0050 1.2,3-Trichloropropane ND 0.0050 1.24-Trimethylbenzene ND 0.0050 0,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylcnes (total) ND 0.0050 Surrogate: Uibrmnolluoromethane 91 ` i, (75 - 12 2 ) Surrogate: Toluene-d8 94 ° ( 66 - 128 ) Surrogate: 4-Bromo/luoroben_ene 97 ; (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 38 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile E Sampled : 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mg/kg 1 B 1 C0807 03/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BIC0810 03/26'21 14:11 EPA 601OB Arsenic 2.0 1.9 " Barium 5.5 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 6.4 0.48 " Cobalt 0.76 0.48 Copper 1.8 0.96 Lead 3.7 0.48 Molybdenum 1.6 0.48 Nickel 3.9 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 5.2 1.9 " 5.2 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.9 mg!kg 1 BIC0804 03/26/21 14:42 EPA 8015M R-07 Surrogate: 4-Bromo/luoroben_cne 102 N (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 BIC0798 03/2621 11:45 EPA 8015M TPH Motor Oil (C23-C40) 120 50 " " " " 11 Surrogate: o-Teuphem•l 107 "6 (65 - 133) " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 39 of 65 W JAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sam Sample ID: Soil Pile E Sampled: 03/25/21 12:10 P Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mgfkg 1 B1C0817 03/20/21 16:12 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromoforn ND 0.0050 Bronximethane ND 0.0050 u-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobcnzcnc ND 0.0050 " W" Chloroethanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 .-, 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1.2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (EDB) ND 0,0050 Dibromotnethane ND 0.0050 " 1.2-Dichlorobenzenc ND 0.0050 1,3-Dichlorobenzenc ND 0.0050 1,4-Dichlorobenzenc ND 0.0050 Dichlorodilluoromethane ND 0.0050 -1 .1 -Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 cis- 1,2-Dichloroethene ND 0.0050 trans-l.2-Dichloroethene ND 0.0050 " 1.2-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 �2,2-Dichloropropane ND 0.0050 I.I-Dichloropropene ND 0.0050 cis- I3-Dichloropropenc ND 0.0050 trans-1,3-Dichloropropenc ND 0.0050 E.thylbcnzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 40 of 65 r-, --I i Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GONIS (Continued) Ilexachlombutadiene ND 0.0050 mg/kg 1 BIC0817 03/26/21 16:12 EPA8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenz_ene ND 0.0050 Styrene ND 0.0050 1, 1. 1 .2-Tetrachloroethane ND 0.0050 I.1,2,2-Tetrachloroethanc ND 0.0050 Tetrachlorocthcnc WCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobcnzene ND 0.0050 I.2,4-Trichlorobenzene ND 0.0050 1,1,1-Triehloroetharre ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (WE) ND 0.0050 Trichlorofluorotnethane ND 0.0050 1.2,3-Trichloropropane ND 0.0050 1,2.4=IYiniethylbenzene ND 0.0050 1.3.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylenes (total) ND 0.0050 Surrogate: Dihrornolhtoromethmre 91 ' ( 75 - 122 ) Surrogate: Toluenc,48 95 '%„ (66 - 128 ) Surrogate: 4-BrornuJluoroben_ene 97 %, ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report mast he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 41 of 65 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Totali Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0807 - EPA 7471A Preparation: EPA 7471A Prep 03/26/21 07:43 - Blank (B1C0807-BLK1) Analyzed: 03/26/21 13:21 Mercury ND 0.10 mg/kg LCS (B1C0807-BS1) Analyzed: 03/26/21 13:17 - Mercury 0.792 0.10 mgAg 0.833 95 85-115 LCS Dup (B1C0807-BSD1) Analyzed: 03/26/21 13:19 Mercury 0.783 0.10 mg/kg 0.833 94 85-115 1 20 Duplicate (B1C0807-DUPl) Source: 2101842-02 Analyzed: 03/26/21 13:25 Mercury 0.0556 0.096 mg/kg 0.0554 0.3 20 Matrix Spike (B1C0807-MSI) Source: 2101842-02 Analyzed: 03/26/21 13:27 Mercury 0.855 0.096 mg/kg 0.796 0.0554 100 75-125 Matrix Spike Dup (B1C0807-MSD1) Source: 2101842-02 Analyzed: 03/26/21 13:29 Mercury 0.750 0.087 mg/kg 0.727 0.0554 96 75-125 13 20 Post Spike (BIC0807-PSI) Source: 2101842-02 Analyzed: 03/26/21 13:31 Mercury 5.17 ug/L 5.00 0.347 97 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report merit be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 _ Blank (BlC0810-BLK1) Analyzed: 03/26/21 12:16 Antimony ND 2.5 mgIg Arsenic ND 2.0 Barium ND 1.0 '-' Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 - Copper ND 1.0 Lead ND 0.50 " Molybdenum ND 0.50 Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (BlC0810-BS1) Analyzed: 03/26/21 12:40 Antimony 100 2.5 mg/kg 100 100 80-120 Arsenic 101 2.0 100 WI 80-120 Barium 102 1.0 100 102 80-120 Beryllium 103 0.50 100 103 80-120 .-, Cadmium 102 0.25 100 102 80-120 Chromium 103 0.50 100 103 80-120 Cobalt 103 0.50 100 103 80-120 - Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molvbdemmn 100 0.50 100 100 80-120 Nickel 103 0.50 100 103 80-120 Selenium 100 2.0 100 100 80-120 Silver 5.06 0.50 5.00 101 80-120 Thallium 104 H) 100 104 80-120 Vanadium 100 2.0 100 100 80-120 Zinc 103 2.0 100 103 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0810 -EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 -� LCS Dup (B1C0810-BSDI) Analyzed: 03/26/21 12:43 Antimony 101 2.5 mg/kg 100 101 80-120 0.7 20 Arsenic 102 2.0 100 102 80-120 0.9 20 Barium 102 1.0 100 102 80-120 0.3 20 Beryllium 104 0.50 100 104 80-120 0.9 20 Cadmium 103 0.25 100 103 80-120 0.5 20 Chromium 104 0.50 100 104 80-120 1 20 - , Cobalt 104 0.50 100 104 80-120 0.5 20 Copper 104 1.0 100 104 80-120 0.9 20 Lead 104 0.50 100 104 80-120 0.8 20 Molybdenum 101 0.50 100 101 80-120 0.9 20 Nickel 104 0.50 100 104 80-120 0.5 20 Selenium 101 2.0 100 101 80-120 0.7 20 Silver 5.16 0.50 5.00 103 80-120 2 20 Thallium 104 LO 100 104 80-120 0.3 20 - Vanadium 102 2.0 100 102 80-120 1 20 Zinc 103 2.0 100 103 80-120 0.5 20 Duplicate (B1C0810-DUPI) Source: 2101840-03 Analyzed: 03/26/21 13:06 Antimony ND 2.4 mg/kg 0.966 20 Arsenic 2.64 1.9 3.12 17 20 Barium 118 0.95 116 2 20 Beryllium ND 0.47 ND 20 Cadmium ND 0.24 ND 20 Chromium 16.3 0.47 17.6 8 20 Cobalt 3.67 0.47 4.26 15 20 Copper 9.50 0.95 8.79 8 20 Lead 6.24 0.47 5.56 12 20 Molybdenum 1.46 0.47 1.27 14 20 Nickel 20.8 0.47 23.4 12 20 Selenium ND 1.9 ND 20 Silver ND 0.47 ND 20 Thallium ND 0.95 ND 20 Vanadium 15.0 1.9 15.4 3 20 Zinc 34.0 1.9 29.6 14 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 65 16-1*N Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Drcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Matrix Spike (BlC0810-MSI) Source: 2101840-03 Analyzed: 03/26/21 12:45 Antimony 49.8 2.4 mg/kg 97.6 ND 51 10-116 Arsenic 100 2.0 97.6 3.12 100 77-121 Barium 196 0.98 97.6 116 82 30-169 Beryllium 98.3 0.49 97.6 ND 101 96-111 Cadmium 93.4 0.24 97.6 ND 96 81-112 Chromium 113 0.49 97.6 17.6 97 75-129 Cobalt 96.4 0.49 97.6 4.26 94 71-121 Copper 106 0.98 97.6 8.79 100 68-135 Lead 98.5 0.49 97.6 5.56 95 72-121 Molybdenum 89.8 0.49 97.6 1.27 91 70-112 -� Nickel 111 0.49 97.6 23.4 90 73-121 Selenium 94.7 2.0 97.6 ND 97 76-116 Silver 4.74 0.49 4.88 ND 97 54-132 Thallium 91.2 0.98 97.6 ND 93 64-120 \anadium 112 2.0 97.6 15.4 99 78-124 Zinc 122 2.0 97.6 29.6 95 50-143 Matrix Spike Dup (B1C0810-MSD1) Source: 2101840-03 Analyzed: 03/26/21 12:55 Antimony 48.3 2.5 mg'kg 98.0 ND 49 10-116 3 20 Arsenic 102 2.0 98.0 3.12 101 77-121 1 20 Barium 203 0.98 98.0 116 89 30-169 4 20 Beryllium 99.4 0.49 98.0 ND WI 86-111 1 20 Cadmium 95.0 0.25 98.0 ND 97 81-112 2 20 Chromium 117 0.49 99.0 17.6 101 75-129 4 20 Cobalt 98.2 0.49 98.0 4.26 96 71-121 2 20 Copper 110 0.98 98.0 8.79 103 68-135 3 20 Lead 100 0.49 98.0 5.56 97 72-121 2 20 Molybdenum 91.3 0.49 98.0 1.27 92 70-112 2 20 Nickel 113 0.49 98.0 23.4 92 73-121 2 20 Selenium 96.4 2.0 98.0 ND 98 76-116 2 20 Silver 4.89 0.49 4.90 ND 100 54-132 3 20 Thallium 93.1 0.98 98.0 ND 95 64-120 2 20 Vanadium 115 2.0 98.0 15.4 102 78-124 3 20 Zinc 124 2.0 98.0 29.6 96 50-143 1 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 45 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Totalby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 _ . Post Spike (B1C0810-PS1) Source: 2101840-03 Analyzed: 03/26/21 12:58 Antimony 1.97 mg/l. 2.00 0.0203 98 75-125 Arsenic 2.08 2.00 0.0657 101 75-125 Barium 4.38 2.00 2.43 97 75-125 Beryllium 1.99 2.00 0.00456 99 75-125 Cadmium 1.89 2.00 -0.00476 94 75-125 Chromium 2.37 2.00 0.370 100 75-125 Cobalt 1.97 2.00 0.0898 94 75-125 Copper 2.25 2.00 0.185 103 75-125 Lead 2.02 2.00 0.117 95 75-125 Molybdenum 1.98 2.00 0.0268 98 75-125 -• Nickel 2.37 2.00 0.492 94 75-125 Selenium 1.97 2.00 0.000298 98 75-125 Silver 0.0974 0.100 -0.00289 97 75-125 Thallium 1.88 2.00 -0.0363 94 75-125 Vanadium 2.30 2.00 0.324 99 75-125 Zinc 2.50 2.00 0.623 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 46 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0802 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:22 Blank (B1C0802-BLK1) Analyzed: 03/26/21 08:30 TPH Gasoline (C5-Cl2) ND 0.50 mg/kg Surrogate:4-BromoJluorobcnzerrc 0.127 110.125 101 31-168 LCS (B1C0802-BS1) Analyzed: 03/26/21 06:59 TPH Gasoline (C5-C12) 1.01 0.50 mg,kg 1.00 101 62-151 Surrogate:4-Bromolluorobenrene 0.152 " 0.125 121 31-168 LCS Dup (B1C0802-BSD1) Analyzed: 03/26/21 07:25 TPFI Gasoline (C5-C12) 0.958 0.50 mg/kg 0.996 96 62-151 5 20 Surrogate:4-Bromolluaunbenzene 0.142 0.125 114 31-168 Duplicate (B1C0802-DUPl) Source: 2101840-01 Analyzed: 03/26/21 09:29 TPH Gasoline (C5-('12) ND 0.50 mg'kg ND 20 Surrogate: 4-Bromolluorobenzene 0.131 0.124 105 31-168 Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Blank (BlC0804-BLK1) Analyzed: 03/26/21 10:27 TPH Gasoline (('5-('12) ND 0.50 mg/kg Surrogate:4-Brome)lluorohcnzene 0.133 " 0.125 107 31-168 LCS (BlC0804-BS1) Analyzed: 03/26/21 09:30 TPH Gasoline (C5-02) 1.24 0.50 mg/kg 0.998 124 62-151 Surrogule:4-Bromolluarobenzene 0.147 0.125 118 31-168 LCS Dup (B1C0804-BSDl) Analyzed: 03/26/21 09:59 TPH Gasoline (('5-C'12) 1.32 0.50 mg/kg 0.998 132 62-151 7 20 Surrogale:4-Bromo/luorohenzene 0.164 " 0.125 131 31-168 Duplicate (BlC0804-DUPI) Source: 2101841-06 Analyzed: 03/26/21 11:24 TPH Gasoline (('5-C12) 10.0 4.3 mg/kg 6.12 48 20 QR-03 Surrogate:4-Bronuolluuorohertra•rue 1.38 " 1.08 128 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 65 �1 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Semi-Volatile1 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0798 - EPA 8015M Preparation: EPA 3550C 03/25/21 17:29 Blank (B1C0798-BLKI) Analyzed: 03/26/21 07:35 TPH Diesel (C13-('22) ND 10 mg!kg TPH Motor Oil (C23-C40) ND 50 " Surrogate: n-Terphenrl 53.7 " 49.8 108 65-133 LCS (BlC0798-BSI) Analyzed: 03/26/21 07:07 TPH Diesel (C13-C22) 508 9.9 mg/kg 496 102 77-114 TPII Motor Oil (C23-C40) 549 50 496 111 76-128 Surrogate: o4i, phenpl 50.7 49.6 102 65-133 LCS Dup (BlC0798-BSD1) Analyzed: 03/26/21 07:21 TPH Diesel (C13-C22) 501 9.9 mg/kg 497 101 77-114 1 20 TPH Motor Oil (C23-C40) 557 50 497 112 76-128 2 20 Surrogate: o4ophem'l 53.5 49.7 108 65-133 Duplicate (B1C0798-DUPI) Source: 2101840-01 Analyzed: 03/26/21 08:44 TPII Diesel (C13-('22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) 43.1 50 44.8 4 20 Surrogate: o-Teiphenrl 53.4 49.8 107 65-133 Matrix Spike (BlC0798-MSI) Source: 2101840-01 Analyzed: 03/26/21 13:48 TPII Dicscl (C13-('22) 507 9.9 mg,'kg 497 ND 102 45-149 TPH Motor Oil (C23-C40) 556 50 497 44.8 103 34-175 Surrogate: o-Teiphenirl 55.9 49.7 113 65-133 Matrix Spike Dup (B1C0798-MSD1) Source: 2101840-01 Analyzed: 03/26/21 14:02 TPH Diesel (C13-C22) 488 10 mg/kg 499 ND 98 45-149 4 20 TPH Motor Oil (C23-('40) 548 50 499 44.8 101 34-175 1 20 Surrogate: o-Teiphenpl 552 49.9 111 65-133 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 vAymoecusa.com FAX: 805 925-3376 Page 48 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (BIC0815-BLK1) Analyzed: 03/26/21 11:26 Benzene ND 0.25 mg/kg Bromobenzene ND 0.25 Bromochloromethane ND 0.25 Bromodichloromethane ND 0.25 " Bromoturm ND 0.25 Bromomethane ND 0.25 n-Butylbenzene ND 0.25 see-Butylbenzene ND 0.25 " tert-Butylbenzene ND 0.25 " Carbon tetrachloride ND 0.25 " Chlorobenzene ND 0.25 " Chloroethane ND 0.25 Chloroform ND 0.25 Chlorom ethane ND 0.25 ~ 2-Chlorotoluene ND 0.25 4-Chlorotoluene ND 0.25 Dibromochloromethane ND 0.25 1,2-Dibromo-3-chloropropane ND 0.25 " 1,2-Dibromoethane (EDB) ND 0.25 " Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0.25 �-T 1,3-Dichlorobenzene ND 0.25 IA-Dichlorobenzene ND 0.25 " Dichlorodifluoromethane ND 0.25 " 1,1-Dichloroethane ND 0.25 " 1.2-Dichloroethane ND 0.25 1,1-Dichloroethene ND 0.25 cis-1,2-Dichloroethene ND 0.25 " trans-1,2-Dichloroethene ND 0.25 12-Dichloropropane ND 0.25 13-Dichloropropane ND 0.25 21-Dichloropropane ND 0.25 " ' 1, 1 -Dichloropropene ND 0.25 " cis- 1.3 -Dichloropropene ND 0.25 " trans-1,3-Dichloropropene ND 0.25 lithvlbenzene ND 0.25 " Ilexachlorobutadiene ND 0.25 4-isopropyl Toluene ND 0.25 Isopropylbenzene ND 0.25 - = methylene chloride ND 0,25 Naphthalene ND 0.25 n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 49 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes ^ Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 .. Blank (B1C0815-BLK1) Analyzed: 03/26/21 11:26 Styrene ND 0.25 mgtkg 1, 1, 1,2-Tetrachloroethane ND 0.25 1, 1 .2,2-Tctrachlorocthanc ND 0.25 " Tetrachloroethene (PCE) ND 0.25 'toluene ND 0.25 1,2,3-Trichlorobenzene ND 0.25 " r 1,2,4-Trichloroben7ene ND 0.25 1, 1, 1 -Trichloroethane ND 025 1,1.2-Trichloroethane ND 025 " Trichloroethene (TCE) ND 0.25 " ^ Trichlorotluoromethane ND 0.25 1,2,3-Trichloropropane ND 0.25 1,14-Trimethylbenzene ND 0.25 " 1,3,5-Trimethylbenzene ND 0.25 - Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 Surrogate: Dibrataq/htornntethrtnc 0.0445 0.0498 89 75-122 r-� Surrogate: Tdtiene-d8 0.0455 " 0.0498 91 66-128 Surrogate:4-Bromolluorohenzene 0.0479 0.0498 96 76-122 LCS (B1C0815-BS1) Analyzed: 03/26/21 09:44 Benzene 1.80 0.25 mg'kg 1.99 91 75-131 Bromobenzene 1.97 0.25 1.99 99 75-136 Bromochloromethane 1.67 0.25 1.99 84 70-135 Bromodichloromethane 1.84 0.25 1.99 93 76-137 Bromoform 1.69 0.25 1.99 85 55-139 Bromomethane 1.49 0.25 1.99 75 10-157 n-Butylbenzene 2.38 0.25 1.99 120 62-166 sec-Butylbenzene 2.50 0.25 1.99 126 72-167 tert-Butylbenzene 2.33 0.25 1.99 117 69-158 Carbon tetrachloride 1.77 0.25 1.99 89 70-140 Chlorobenzene 1.94 0.25 1.99 98 76-137 - Chloroethane 2.09 0.25 1.99 105 10-164 Chloroform 1.80 0.25 1.99 91 75-123 Chloromethane 1.73 0.25 1.99 87 26-140 2-Chlorotoluene 2.11 0.25 1.99 106 73-145 4-Chlorotoluene 2.13 025 1.99 107 67-151 Dibromochloromethane 1.80 0.25 1.99 90 68-144 1,2-Dibromo-3-chloropropane 1.63 0.25 1.99 82 45-148 1,2-Dibro noethane (EDB) 1.80 0.25 1.99 91 73-134 Dibromomethanc 1.66 0.25 1.99 84 70-140 1,2-Dichlorobenzene 2.15 0.25 1.99 108 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report mast be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 50 of 65 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 -� LCS (BlC0815-BSI) Analyzed: 03/26/21 09:44 1,3-Dichlorobenzene 2.19 0.25 mg/kg 1.99 110 76-146 I A-Dichlorobenzene 2.10 0.25 1.99 106 72-140 Dichlorodifluoromethanc 1.73 0.25 1.99 87 10-166 I,1-Dichloroethane 1.82 0.25 1.99 92 65-139 1,2-Dichloroethanc 1.80 0.25 1.99 90 67-125 1,1-Dichloroethene 2.05 0.25 1.99 103 54-16S -. cis-1.2-Dichloroethene 1.80 0.25 1.99 91 74-135 trans-1,2-Dichloroethene 1.98 0.25 1,99 100 68-149 1,2-Dichloropropane 1.77 0.25 1.99 89 74-130 1,3-Dichloropropane 1.83 0.25 1.99 92 68-130 2,2-Dichloropropane 1.95 0.25 1.99 98 33-187 1, 1 -Dichloropropene 1.95 0.25 1.99 98 71-140 cis- l,3-Dichloropropene 1.79 0.25 1.99 90 78-135 trans-1,3-Dichloropropene 1.90 025 1.99 96 70-137 Ethvlbenzene 1.93 0.25 1.99 97 69-143 Hexachlorobutadiene 3.12 0.25 1.99 157 69-203 4-Isopropyl Toluene 2.38 0.25 1.99 120 74-154 Isopropylbenzene 2.11 0.25 1.99 106 72-157 Methylene chloride 1.75 0.25 1.99 88 49-129 Naphthalene 1.84 0.25 1.99 93 61-158 n-Propylbenzene 2.17 0.25 1.99 109 69-147 Styrene 1.92 0.25 1.99 97 71-144 1,1,1,2-Tetrachloroethane 1.92 0.25 1.99 97 78-132 1,1,2,2-Tetrachloroethane 1.90 0.25 1.99 96 64-138 Telrachloroelhene WCE) 2.09 0.25 1,99 105 74-148 Toluene 1.92 0.25 1.99 92 76-131 1,23-Trichlorobenzene 2.11 0.25 1.99 106 63-170 1,24-Trichlorobenzene 2.20 0.25 1.99 110 71-165 1, 1, 1 -Trichloroethane 1.97 0.25 1.99 99 74-137 I.1,2-Trichloroethane 1.82 0.25 199 91 68-134 Trichloroethane (TCE) 1.94 0.25 1.99 99 79-139 Trichlorotluoromethane 2.20 0.25 1.99 111 32-154 ' 1,23-Trichloropropane 1.77 0.25 1.99 89 69-125 12,4-Trimethylbenzene 2.14 0.25 1.99 108 67-144 1,3.5-Trimethylbenzene 2.17 0.25 1.99 109 66-154 Vinyl chloride 2.27 0.25 1.99 114 39-150 Xylenes (total) 5.95 0.25 5.96 100 71-147 Surrogate: DihromoPuburomc•thanc 0.0496 0.0497 100 75-122 Surrogate: Toluene-d8 0.0462 0.0497 93 66-128 -7 Surrogate:4-Bronutlluorohen:ene 0.0451 0.0497 91 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 51 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 CompoundsVolatile Organic Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (B1C0815-BSDI) Analyzed: 03/26/21 10:09 Benzene 1.87 0.25 mg/kg 2.00 94 75-131 4 20 Bromobenzene 2.02 0.25 2.00 101 75-136 2 20 Bromochloromcthane 1,69 0.25 2.00 85 70-135 2 20 Bromodichloromethane 1.93 0.25 2.00 97 76-137 5 20 Bromoform 1.80 0.25 2.00 90 55-139 7 20 Bromomethane 1.21 0.25 2.00 61 10-157 20 20 n-Butylbenzene 2.45 0.25 2.00 123 62-166 3 20 see-Butylbenzene 2.48 0.25 2.00 124 72-167 0.9 20 tert-Butylbenzene 2.38 0.25 2.00 119 69-158 2 20 Carbon tetrachloride 1.87 0.25 2.00 94 70-140 6 20 Chlorobenzene 2.07 0.25 2.00 104 76-137 7 20 Chloroethane 2.21 0.25 2.00 111 10-164 6 20 Chloroform 1.81 0.25 2.00 90 75-123 0.4 20 Chloromethane 1.82 0.25 2.00 91 26-146 5 20 2-Chlorotoluene 226 0.25 2.00 113 73-145 7 20 4-Chlorotoluene 2.25 0.25 2.00 112 67-151 5 20 Dibromochloromethane 1.97 0.25 2.00 98 68-144 9 20 1,2-Dibromo-3-chloropropane 1.84 0.25 2.00 92 45-149 12 20 1,2-Dibromoethane (ED13) 1.98 0.25 2.00 99 73-134 9 20 Dibromomethane 1.75 0.25 2.00 87 70-140 5 20 1,2-Dichlorobenzene 2.18 0.25 2.00 109 78-142 1 20 1,3-Dichlorobenzene 2.30 0.25 2.00 115 76-146 5 20 IA-Dichlorobenzene 2.06 0.25 2.00 103 72-140 2 20 Dichlorodilluoromcthane 1.73 0.25 2.00 86 10-166 0.1 20 1, 1 -Dichloroethane 1.95 0.25 2.00 98 65-139 7 20 1,2-Dichloroethane 1.93 0.25 2.00 96 67-125 7 20 1,1-Dichloroethene 2.07 0.25 2.00 103 54-168 0.6 20 cis-L2-Dichloroethene 1.86 0.25 2.00 93 74-135 4 20 trans-1,2-Dichloroethene 2.11 0.25 2.00 105 68-149 6 20 12-Dichloropropane 1.82 0.25 2.00 91 74-130 3 20 1,3-Dichloropropane 1.84 0.25 2.00 92 68-130 0.6 20 2.2-Dichloropropane 1.94 0.25 2.00 97 33-187 0.4 20 1, 1 -Dichloropropene 2.04 0.25 2.00 102 71-140 5 20 cis-1.3-Dichloropropene 1.80 0.25 2,00 90 78-135 0.5 20 trans- l,3-Dichloropropene 1.94 0.25 2.00 97 70-137 2 20 Ethylbenzene 2.06 0.25 2.00 103 69-143 6 20 Hexachlorobutadiene 3.30 025 2.00 165 69-203 6 20 4-1sopropyl Toluene 2.42 0.25 2.00 121 74-154 2 20 Isopropylbenzene 2.19 0.25 2.00 109 72-157 3 20 Methylene chloride 1.87 0.25 2.00 94 49-129 7 20 Naphthalene 2.04 0.25 2.00 102 61-158 1() 20 n-Propylbenzene 2.30 0.25 2.00 115 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www_oecusa.com FAX: 805 925-3376 Page 52 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 -- LCS Dup (B1C0815-BSDI) Analyzed: 03/26/21 10:09 Styrene 2.06 0.25 mg,kg 2.00 103 71-144 7 20 1, 1, 1,2-Tetrachloroethane 2.04 0.25 2.00 102 78-132 6 20 1,1,2.2-Tetrachlorocthane 2.02 0.25 2.00 101 64-138 6 20 Tetrachloroethene WCE) 2.18 0.25 2.00 109 74-148 4 20 Toluene 1.91 0.25 2.00 96 76-131 5 20 1,2,3-Trichlorobenzene 2.36 0.25 2.00 119 63-170 12 20 1,2,4-Trichlorobenzene 2.37 0.25 2.00 118 71-165 7 20 1, 1. 1 -Trichloroethane 1.98 0.25 2.00 99 74-137 0.8 20 IJ,2-Trichloroethane 1.92 0.25 2.00 96 68-134 6 20 Trichloroethene (TC'E) 1.92 0.25 2.00 96 79-139 0.9 20 - Trichlorolluoromethaue 2.15 0.25 2.00 107 32-154 3 20 1,2,3-Trichloropropane 1.78 0.25 2.00 89 69-125 0.3 20 1,2.4-Trimethylbenzene 2.19 0.25 2.00 110 67-144 2 20 1,3,5-Trim ethylbenzene 2.24 0.25 2.00 112 66-154 3 20 .� Vinyl chloride 2.22 0.25 2.00 111 39-150 2 20 Xylenes (total) 6.14 0.25 6.00 102 71-147 3 20 Surrogate: Uibr(intt)/htorontrthanc 0.0492 0.0500 98 75-122 Surrogate: Toluene-d8 0.0452 0.0500 90 66-128 Surrogate: 4-Bron:nJluornben--ene 0.0464 0.0500 93 76-122 Duplicate (B1C0815-DUPl) Source: 2101841-07 Analyzed: 03/26/21 14:51 Benzene ND 1.2 mg%kg ND 20 Bromobenzene ND 1.2 ND 20 Bromochloronrcthanc ND 1.2 ND 20 Bromodichloromethane ND 1.2 ND 20 Bromofonn ND 1.2 ND 20 Bromomethane ND 1.2 ND 20 n-Butylbenzene ND 1.2 ND 20 sec-Butylbenzene ND 1.2 ND 20 tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzene ND 1.2 ND 20 - Chloroethane ND 1.2 ND 20 Chloroform ND 1.2 ND 20 C'hloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 ' 4-Chlorotoluene ND 1.2 ND 20 Dibronwchloromethane ND 1.2 ND 20 1,24Dibromo-3-chloropropane ND 1.2 ND 20 1,2-Dibromoethane (EDB) ND 1.2 " ND 20 Dibronwmethanc ND 1.2 ND 20 1,2-Dichlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 53 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Duplicate (B1C0815-DUPl) Source: 2101841-07 Analyzed: 03/26/21 14:51 1,3-Dichlorobenzene ND 1.2 mgIg ND 20 1,4-Dichlorobenzene ND 1.2 NI) 20 Dichloroditluoromcthanc ND 1.2 ND 20 1,1-Dichloroethene ND 1.2 ND 20 1,2-Dichlorocthanc ND 1.2 ND 20 1,1-Dichloroethene ND 1.2 ND 20 cis-1,2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropaue ND 1.2 ND 20 1,3-Dichloropropaue ND 1.2 ND 20 2,2-Dichloropropaue ND 1.2 ND 20 1,1-Diehloropropene ND 1.2 ND 20 cis-1.3-Diehloropropene ND 1.2 ND 20 trans-1,3-Diehloropropene ND 1.2 ND 20 Ethvlbenzene ND 1.2 ND 20 Ilexachlorobutadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 Isopropylbenzene ND 1.2 ND 20 Methylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 ND 20 n-Propylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1,1,1,2-Tetrachloroethane ND 1.2 ND 20 1,1,2,2-Tetrachloroethane ND 1.2 ND 20 Tetrachloroethene (PCE) ND 1.2 ND 20 Toluene ND 1.2 ND 20 1,2,3-Trichlorobenzene ND 1.2 ND 20 1.24-Trichlorobenzene ND 1.2 ND 20 1, 1, 1 -Trichloroethane ND 1.2 ND 20 1.1.2-Trichloroethane ND 1.2 ND 20 Trichloroethene (TCE) ND 1.2 ND 20 "Trichlorotluoromethane ND 1.2 ND 20 1,2,3-Trichloropropane ND 12 ND 20 12,4-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 NI) 20 `v"invl chloride ND 1.2 ND 20 Xylenes (total) ND 1.2 ND 20 Surrogate: Uibromolluoromethane 0.0468 Ol0494 95 75-122 Surrogute: 7oluene-d8 0.0455 0.0494 92 66-128 Surrogate: 0.0466 0.0494 94 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 54 of 65 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 - • Blank (B1C0817-BLKI) Analyzed: 03/26/21 12:18 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 Bromochloromcthane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 " Bromonrethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 " - Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 " Chloroform ND 0.0050 " Chloromethane ND 0.0050 " 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-cliloropropane ND 0.0050 1,2-Dibromoethane (EDB) ND 0.0050 " Dibromomethane ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " - ' 13-Dichlorobenzene ND 0.0050 " 1,4-Dichlorobenzene ND 0.0050 " Dichlorodilluoromcthanc ND 0.0050 I,1-Dichloroethene ND 0.0050 " - 1,2-Dichlorocthanc ND 0.0050 1, 1 -Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 " - - trans-1,2-Dichloroethene ND 0.0050 12-Dichloropropene ND 0.0050 " 1,3-Dichloropropmie ND 0.0050 " 22-Dichloropropene ND 0.0050 " - 1, 1 -Dichloropropene ND 0.0050 " cis-1.3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethylbenzene ND 0.0050 " Ilexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.00.50 n-Propylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 55 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (B1C0817-BLK1) Analyzed: 03/26/21 12:18 Styrene ND 0.0050 mg/kg 1, 1, 1.2-Tetrachloroethane ND 0.0050 " 1,1,2,2-Tctrachloroethanc ND 0.0050 " �Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 1,2,3-Trichlorobenzene ND 0.0050 " 1,2,4-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 1,1.2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 " Trichlorotluoromethaoc ND 0.0050 " 1,23-Trichloropropane ND 0.0050 1,2,4-Trimethylben7ene ND 0.0050 1.3,5-Trimethylbenzene ND 0.0050 V'invl chloride ND 0.0050 " Xylenes (total) ND 0.0050 Surrogate: Dibrontu/luoromc°than(, 0.0459 0.0495 93 75-122 -• Surrogate: Toluene-dA' 0.0472 0.0495 95 66-128 Sinrogate:4-BromoJluorohenzene 0.0483 0.0495 9A 76-122 LCS (B1C0817-BSI) Analyzed: 03/26/21 10:22 - • Benzene 0.0342 0.0050 mg/kg 0.0398 86 75-131 Bromobenzene 0.0367 0.0050 0.0398 92 75-136 Bromochloromcthane 0.0329 0.0050 0.0398 82 70-135 Bromodichloromethane 0.0334 0.0050 0.0398 84 76-137 Bromoform 0.0369 0.0050 0.0398 93 55-139 Bromomethane 0.0230 0.0050 0.0399 58 10-157 n-Butylbenzene 0.0396 0.0050 0.0398 99 62-166 sec-Butylbenzene 0.0452 0.0050 0.0398 114 72-167 tert-Butylbenzene 0.0427 0.0050 0.0398 108 69-158 Carbon tetrachloride 0.0348 0.0050 0.0398 87 70-140 Chlorobenzene 0.0374 0.0050 0.0398 94 76-137 - Chloroethane 0.0413 0.0050 0.0398 104 10-104 Chlorofonn 0.0323 0.0050 0.0398 81 75-123 Chloromethane 0.0324 0.0050 0.0398 82 26-146 2-Chlorotoluene 0.0396 0.0050 0,0398 100 73-145 4-Chlorotoluene 0.0405 0.0050 0.0398 102 67-I51 Dibromochloromethane 0.0371 0.0050 0.0398 93 68-144 1.2-Dibromo-3-chloropropanc 0.0355 0.0050 0.0398 89 45-148 1,2-Dibromoethane (EDB) 0.0369 0.0050 0.0398 93 73-134 Dibromomcthanc 0.0328 0.0050 0.0398 82 70-140 1,2-Dichlorobenzene 0.0402 0.0050 0.0398 101 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8015) 925-3376 Page 56 of 65 -t �j Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatilet poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (B1C0817-BSI) Analyzed: 03/26/21 10:22 1,3-Diehlorobenzenc 0.0406 0.0050 mg/kg 0.0398 102 76-146 1,4-Dichlorobenzene 0.0388 0.0050 0.0398 97 72-140 Dichloroditluoromcthanc 0.0375 0.0050 0.0398 94 10-166 I,1-Dichloroethene 0.0342 0.0050 0.0398 86 65-139 1,2-Dichlorocthanc 0.0336 0.0050 0.0398 84 67-125 I,1-Dichloroethene 0.0360 0.0050 0.0398 90 54-168 cis-1,2-Dichloroethene 0.0346 0.0050 0.0398 87 74-135 trans-1,2-Dichloroetlene 0.0375 0.0050 0.0398 94 68-149 1,2-Dichoropropane 0.0336 0.0050 0.0398 84 74-130 1,3-Dichloropropane 0.0356 0.0050 0.0398 90 68-130 2,2-Dichloropropane 0.0394 0.0050 0.0398 99 33-187 1, 1 -Dichloropropene 0.0350 0.0050 0.0398 88 71-140 cis-1.3-Dichloropropene 0.0349 0.0050 0.0398 88 78-135 trans- l,3-Dichloropropene 0.0393 0.0050 0.0398 99 70-137 Ethylbenzene 0.0379 0.0050 0.0398 95 69-143 11exachlorobutadiene 0.0480 0.0050 0.0398 121 69-203 4-Isopropyl Toluene 0.0438 0.0050 0.0398 110 74-154 Isopropylbenzene 0.0408 0.0050 0.0398 102 72-157 Nlethylene chloride 0.0320 0.0050 0.0398 80 49-129 Naphthalene 0.0429 0.0050 0.0398 IN 61-158 n-Propylbenzene 0.0417 0.0050 0.0398 105 69-147 Styrene 0.0384 0.0050 0.0398 97 71-144 1,1,1,2-Tetrachloroethane 0.0379 0.0050 0.0398 95 78-132 1,1,2,2-Tetrachloroethane 0.0390 0.0050 0.0398 98 64-138 Tetrachloroethene (PCE) 0.0386 0.0050 0.0398 97 74-148 Toluene 0.0330 0.0050 0.0398 83 76-131 1,2,3-Trichlorobenzene 0.0434 0.0050 0.0398 109 63-170 1,24-Trichlorobenzene 0.0433 0.0050 0.0398 109 71-165 1, 1, 1 -Trichloroethane 0.0349 0.0050 0.0398 88 74-137 1,12-Trichloroethane 0.0364 0.0050 0.0398 92 68-134 Trichloroethene (TCE) 0.0344 0.0050 0.0398 86 79-139 Trichlorotluoromethanc 0.0382 0.0050 0.0398 96 32-154 1,2,3-Trichloropropane 0.0367 0.0050 0.0398 92 69-125 1.24-Trimethylbenzene 0.0390 0.0050 0.0398 98 67-144 1,3.5-Trim ethyl benzene 0.0409 0.0050 0.0399 103 66-154 Vinyl chloride 0.0373 0.0050 0.0398 94 39-150 Xylenes(total) 0.115 0.0050 0.119 97 71-147 Surrogate. Uibromolluoramc•thane 0.0474 0.0497 95 75-122 Surrogate: Toluene-dN 0.0478 0.0497 96 66-128 Surrogate:4-BromgJluomhen_rne 0.0490 0.0497 99 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: {8051 925-3376 Page 57 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 VolatileptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 • LCS Dup (B1C0817-BSDI) Analyzed: 03/26/21 10:51 Benzene 0.0353 0.0050 m 1g 0.0398 89 75-131 3 20 Bromobenzene 0.0390 0.0050 0.0398 98 75-136 6 20 Bromochloromcthanc 0.0339 0.0050 0.0398 85 70-135 3 20 Bromodiehloromethane 0.0349 0.0050 0.0399 88 76-137 4 20 Bromoform 0.0390 0.0050 0.0398 98 55-139 6 20 Bromomethane 0.0259 0.0050 0,0399 65 10-157 12 20 u-Butylbenzene 0.0425 0.0050 0.0398 107 62-166 7 20 sec-Butylbenzene 0.0487 0.0050 0.0399 122 72-167 7 20 tert-Butylbenzene 0.0459 0.0050 0.0398 115 69-158 7 20 Carbon tetrachloride 0.0363 0.0050 0.0398 91 70-140 4 20 Chlorobenzene 0.0396 0.0050 0.0398 99 76-137 6 20 Chloroethane 0.0404 0.0050 0.0398 101 10-164 2 20 Chloroform 0.0339 0.0050 0.0398 85 75-123 5 20 Chloromethane 0.0344 0.0050 0.0398 86 26-146 6 20 2-Chlorotoluene 0.0425 0.0050 0.0398 107 73-145 7 20 4-Chlorotoluene 0.0431 0.0050 0.0398 108 67-151 6 20 Dibromochloromethane 0.0391 0.0050 0.0398 98 68-144 5 20 I.2-Dibromo-3-chloropropane 0.0367 0.0050 0.0398 92 45-148 3 20 12-Dibromoethane (EDB) 0.0387 0.0050 0.0398 97 73-134 5 20 Dibromomethanc 0.0337 0.0050 0.0398 85 70-140 3 20 1,2-Dichlorobenzene 0.0426 0.0050 0.0398 107 78-142 6 20 1,3-Dichlorobenzene 0.0435 0.0050 0.0398 109 76-146 7 20 IA-Dichlorobenzene 0.0413 0.0050 0.0398 104 72-140 6 20 Dichlorodifluoromethanc 0.0383 0.0050 0.0398 96 10-166 2 20 1, 1 -Dichloroethane 0.0354 0.0050 0.0398 89 65-139 4 20 1,2-Dichloroethane 0.0346 0.0050 0.0398 87 67-125 3 20 1, 1 -Dichloroethene 0.0372 0.0050 0.0398 93 54-108 3 20 cis-1.2-Dichloroethene 0.0359 0.0050 0.0398 90 74-135 4 20 - trans-1,2-Dichloroethene 0.0389 0.0050 0.0398 98 68-149 4 20 1,2-Dichloropropane 0.0350 0.0050 0.0398 88 74-130 4 20 1,3-Dieliloropropane 0.0372 0.0050 0.0398 93 68-130 4 20 2,2-Dichloropropane 0.0403 0.0050 0.0398 101 33-187 2 20 1, 1 -Dichloropropene 0.0365 0.0050 0.0398 91 71-140 4 20 cis-1.3-Dichloropropene 0.0362 0.0050 0.0398 91 78-135 4 20 trans-1,3-Dichloropropene 0.0415 0.0050 0.0398 104 70-137 5 20 Ethylbenzene 0.0402 0.0050 0.0398 101 69-143 6 20 1lexachlorobutadiene 0.0509 0.0050 0.0398 128 69-203 6 20 4-Isopropyl Toluene 0.0471 0.0050 0.0398 118 74-154 7 20 Isopmpylbenzene 0.0437 0.0050 0.0398 110 72-157 7 20 -- Methylene chloride 0.0333 0.0050 0.0398 84 49-129 4 20 Naphthalene 0,0453 0.0050 0.0398 114 61-158 6 20 n-Propylbenzene 0.0443 0.0050 0.0398 111 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 58 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatilei poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 r- LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 Styrene 0.0410 0.0050 mg/kg 0.0398 103 71-144 6 20 1, 1, 1,2-Tetrachloroethane 0.0402 0.0050 0.0398 101 78-132 6 20 1.1,2,2-1'ctrachlorocthane 0.0407 0.0050 0.0398 102 64-138 4 20 Tetrachloroethene(PCE) 0.0412 0.0050 0.0398 103 74-149 6 20 Toluene 0.0349 0.0050 0.0398 88 76-131 6 20 1,2,3-Trichlorobenzene 0.0459 0.0050 0.0398 115 63-170 6 20 1,2.4-Trichlorobenzene 0.0448 0.0050 0.0398 112 71-165 4 20 1, 1, 1 -Trichloroethane 0.0365 0.0050 0.0399 92 74-137 5 20 1.1,2-Trichlomethane 0.0396 0.0050 0.0398 97 68-134 6 20 Trichloroethene (TCE) 0.0365 0.0050 0.0398 92 79-139 6 20 ^ ' Irichlorotluoromethane 0.0398 0.0050 0.0398 100 32-154 4 20 1,2,3-Trichloropropane 0.0384 0.0050 0.0398 96 69-125 5 20 1,2,4-Trimethylbenzene 0.0422 0.0050 0.0398 106 67-144 8 20 1.3,5-Trimethylbenzene 0.0437 0.0050 0.0398 110 66-154 7 20 .- Vinyl chloride 0.0382 0.0050 0.0398 96 39-150 2 20 Xylenes (total) 0.123 0.0050 0.120 103 71-147 7 20 Surrogate: Dibromolluoromethana° 0.0467 0.0498 94 75-122 -• Surrogate: Tohtene-dS 0.0473 0.0498 95 66-128 Surrogate:4-Bromollnorobenzene 0. 04 95 0.0498 99 76-122 Duplicate (BlC0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 �. Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0,0050 ND 20 Bromochloromcthanc ND 0.0050 ND 20 Bromodiehloromethane ND 0.0050 ND 20 - Bromotbrm ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 �- Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 C'hloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1.2-Dibromo-3-chloropropane ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibronwmethane ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 r, The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 59 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatilet pt by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPl) Source: 2101841-08 Analyzed: 03/26/21 14:15 1,3-Dichlorobcnzcnc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodilluoromcthane ND 0.0050 ND 20 ],I-Dichloroethane ND 0.0050 ND 20 1.2-Dichloroethane ND 0.0050 ND 20 1, 1 -Dichloroethene ND 0,0050 ND 20 cis- 1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 22-Dichloropropane ND 0.0050 ND 20 1,1-Dichlompropene ND 0.0050 ND 20 cis- 1,3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichlompropene ND 0.0050 ND 20 Ethylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Alethylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1,1.1,2-Tetrachloroethane ND 0.0050 ND 20 1.1,2,2-1'ctrachloroethane ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 "Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2,4-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethanc ND 0.0050 ND 20 1,2,3-Trichlompropane ND 0.0050 ND 20 1 .2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.00.50 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: 0L0460 00496 93 75-122 Surrogate:7;duene-d8 0.0472 " 0.0496 95 66-128 Surrogate:4-Bromo/hrorohenrene 0.0480 0.0490 97 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 60 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample Method Summary alysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 80ISM Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OFC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC_ Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OFC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA -FLAP Total Metals by ICP 601013 Total Antimony EPA 601013 Solid OEC. CA-ELAP 601013 Total Arsenic EPA 6010B Solid OEC, CA -FLAP 6010B Total Barium EPA 601013 Solid OEC, CA -FLAP 601013 Total Beryllium EPA 601013 Solid OEC, CA-ELAP 601013Total Cadmium EPA 601013 Solid OEC, CA -FLAP 601013 Total Chromium EPA 601013 Solid OFC, CA -FLAP 6010B Total Cobalt EPA 601013 Solid OEC, CA-ELAP 601013 Total Copper EPA 6010B Solid OEC. CA-ELAP 601013 Total Lead EPA 6010B Solid OEC, CA-ELAP 601013 Total Molybdenum EPA 601013 Solid OEC, CA-ELAP 601013 Total Nickel EPA 601013 Solid OEC, CA-ELAP 601013Total Selenium EPA 6010B Solid OEC, CA-ELAP 001013 Total Silver EPA 601013 Solid OEC, CA-ELAP 6010B Total Thallium EPA 601013 Solid OEC. CA-ELAP 601013'rotal Vanadium EPA601013 Solid OEC. CA-ELAP 6010B Total Zinc EPA 601013 Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 61 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC, CA -FLAP Volatile Organic TPH by GC/FID 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC. CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OF.C, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OFF, CA-ELAP 8015 TPH -Gasoline EPA 8015M Solid OEC, Internal - 8015 TPII-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 9015M Solid OEC, CA-ELAP Notes and Definitions Qualifier Definition - MDL :Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analvte NOT DETECTED at or above the method limit (MDL) Y RPD Relative Pcrccnt Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analytc concentration above 20x TCLP. OR-03 The RPD value for the sample duplicate or NISLMSD was outside of QC: acceptance limits due to matrix interference. QC batch accepted based on LCS and or LCSD recovery and/or RPD values. QR-04 The RPD exceeded the QC' control limits. R-07 Reporting limits arc at or below statcTcdcral hazardous waste criteria limits. S-02 The surrogate recovery for this sample cannot be accurately quantified due to interference from coeluting organic compounds present in the sample extract. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 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O W iL• c c �CO .� ! • ro.. a. w 0 00 U o ❑ m m m y a v a a Q o F c Q m L m m c c c £ Y d o E y 6 z _O r U N Q W a t2 O c�J a APPENDIX E Statement of Qualifications STATEMENT OF QUALIFICATIONS Buena Resources, Inc. is a locally owned and operated full -service environmental company providing environmental consulting, field services and analytical services. Our environmental professionals are experienced in Phase I assessment, Phase II subsurface investigations and Phase III remediation. Our staff consists of professional engineers and environmental technicians. Personnel are OSHA 40 hour trained to perform environmental work when hazardous chemicals are involved. Clients for whom we've performed our services include major oil company, large utilities, industrial facilities, lending institutions, real estate developers and property owners and sellers. The following professionals performed work related to this project: Mr. Daniel Ringstmeyer is a Registered Professional Engineer, Colorado and California, Registered Environmental Assessor, Certified OSHA 40-Hour Trained worker, 8-Hour Trained Haz-mat Supervisor and a licensed California General Engineering Contractor. Mr. Ringstmeyer holds a Bachelors of Science in civil engineering from the South Dakota State University. He is the Founder/Owner and Principal Engineer of Buena Resources, Inc. and CIRRUS Environmental, Inc. He is the Principle Engineer responsible for all work performed by the environmental consulting/contracting firm. Mr. Ringstmeyer has conducted Phase I ESA assessments, Phase II subsurface investigations and Phase III remediation projects for sites throughout California and Mexico. He has designed and managed many successful remediation projects utilizing soil vapor extraction/thermal oxidation, bioremediation, groundwater pump and treat, and carbon adsorption throughout California and Mexico including the closure of a large Class I TSD Landfill facility. He has also directly been responsible for the closure of several idled oil fields and illegal agriculture landfills.