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HomeMy WebLinkAbout2021-12-11 Closure Rpt 2600 Broad St Rev 3Closure Report Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA December 11, 2021 (Rev. 3) Prepared For: Mr. John Hochleutner Pacific Petroleum California, Inc. 1615 Betteravia Road Santa Maria, CA 93268 Prepared By: Buena Resources, Inc. P.O. Box 2040 Santa Maria, CA 93457-2040 Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA TABLE OF CONTENTS 1.0 Excavation: 2.0 Soil Sampling of the Excavation: 3.0 Discussion of Results: 4.0 Conclusions: Appendix A Site Maps & Figures Appendix B Lab Summary Spreadsheets Appendix C Site Photographs Appendix D Laboratory & Chain of Custody Reports Appendix E Statement of Qualifications 3-5 5-6 6-7 7-8 General Contractor License #841453 Buenaresources P.O. Box 2040 Santa Maria, CA 93457-2040 P: (805) 346-1766 F: (805) 346-1767 December 11, 2021 Ms. Matheson Bliss, Haz Materials Coordinator City of San Luis Obispo Fire Department 2160 Santa Barbara Avenue San Luis Obispo, CA 93401-5240 Subject: Fuel Tank Removal and Soil Removal from 2600 Broad Street in San Luis Obispo, CA Dear Mattie: Buena Resources, Inc. has prepared this Closure Report to summarize the work performed and the laboratory results at the above site. Pacific Petroleum of California was initially engaged by Natural Healing Center to remove an existing diesel tank from this site, which had been closed at some point in the past by filling with cement. The diesel tank was estimated to be 4'-dia. by 8' long in size. The excavation related to that tank site was 8' x 8' by 8' deep. Once the tank was removed, the underlying soils were found to have been impacted with hydrocarbons. A second site was the trench that was opened to place utilities during the construction activities at this site. Contamination was found in the trench which extended to the west where a large amount of lead impacted bricks and broken tile were found. This second excavation, which was located adjacent and north of the removed tank, 12' x 12' by 12' deep. These areas are shown on the attached figure with the associated stockpile located near the excavation. Buena..) _iLJr' A State Certified Small & WBE Business BUENARrSOURCES Impacted soil was found below the tank, in the excavation bottom and on the sides of the excavation. Soil believed to be impacted from the diesel tank was removed and placed into 10 cyd. bins. A total of 64.51 tons of Cal Haz lead impacted and hydrocarbon impacted soil was removed and shipped to Waste Management's Kettleman Hills Class I TSD facility from this location. We are not aware of the reasons for the historical diesel tank being located on this property. There was no Phase I ESA Report completed for this site, which could have explored the historical use of this property. As we understand, there was a brick factory located close to this site. The tank was likely used for either fueling or for waste. The bricks are possibly left over from a demolished structure that may have been on the site or immediate area. The concrete slab may have been a cap for the fuel contamination located below it. Although the chromatographs for the TPH data show a weathered diesel pattern, it is possible that gasoline range organics may have been present and have degraded over time. Due to the presumed age of the site, this may have been leaded gasoline explaining the presence of lead. A Control Sample was taken 3/25/21 in an area that was not impacted to utilize that data as a background reference level for the CAM metals results reported from the contaminated zones. Action levels for these sites are the ESLs for the Bay Area Region II Table S-1 for both residential and commercial shallow soil sites. The target for this site are the residential ESLs so the property would not have a Deed restricition. Approximately 15' to the NE of the Diesel Tank Excavation, between the former Quik Mart and the building that will be the NHC SLO, the groundwater was discovered at a depth of 2'. In the tank excavation, groundwater was discovered at a depth of 5'. No groundwater intruded into the second excavation where the bricks and concrete slab were found. Buenaresources A State Certified Small & WBE Business 2 BUENARESOURCES 1.0 EXCAVATION: Diesel Tank Excavation This excavation was performed to remove an 4'-dia. x 8' metal tank that was likely used to dispense and/or store diesel fuel. Once the tank was removed from the excavation, four samples were taken to explore for contamination on March 25, 2021, which are OEC Lab IDs No. 2101841-01 through 04. Tank Wall Samples were taken at a depth of 4' in the center of each wall. OEC Lab samples 2101841-05 & 06 Tank Bottom Samples were taken at a depth of 8' at the inlet and outlet ends of the tank. These samples were located at the bottom center of the east and west ends of the excavation, approximately 1' from the east and west walls, respectively. The sample locations can be seen on page 9 of the Closure Report. Lab data from these samples indicated the presence of chromium at 51 mg/kg in the Tank N Wall sample, OEC Lab ID 2101841-01. Further STLC analysis was ran on this sample resulting in a non -hazardous level of 0.13 mg/I reported. All other tank wall & floor samples reported results below action levels with no additional removal required. Based on these results, the excavation was backfilled with clean soil. The soil excavated from the diesel tank removal generated a stockpile approximately 5' high by Win length and 4' wide. Stockpile Samples On March 25, 2021 composite samples were taken from the north, south, east and west sides of the pile, OEC ID Nos. 2101841-10, 11, 12 & 13. Sampling was done by taking three equal amounts of soil from halfway up each side of the stockpile at intervals of approximately 1'5" and a depth of 6". These aliquots were mixed into three composite samples representing the three sides of the stockpile. A sample was taken from the east side of stockpile as well as the other three sides. Originally, it was thought to be not safe to access this area, but it was finally sampled and added to the COC by the lab. We have added that data to the laboratory data spreadsheets. Buenaresources A State Certified Small & WBE Business 3 BUENARESOURCES Trench SamL line A trench was dug approximately 3' deep to accommodate a water line. A stockpile of soil and bricks were generated from this trenching which was approximately 3' high, 6' long and 4' wide. A composite sample was taken from the stockpile by taking six equal amounts of soil from half way up the pile (15) at 2' intervals and a depth of approximately 6". These aliquots were combined into a single sample. As the excavation continued, the trench was segregated into two sections for sampling because half the length of the excavated material was composed of soil and the other length contained bricks as well as soil. The length containing only soil was called the "Fire Trench" and the other "Sump Trench". Originally, samples were taken from the west wall of the sump trench and at the bottom of the south end of the trench (OEC Lab ID Nos. 2101841-07 & 08. The results of these samples indicated elevated levels of TPH, chromium, copper and lead. The samples were then analyzed for STLC and TCLP levels with the results for lead coming back at 56 mg/I for STLC testing (lab ID. 2101841-07). Data indicated further excavation was required with a sample taken from the Sump Trench West side after this removal was completed (OEC ID 2103032-07) in the middle of the trench length, as that was where the majority of the bricks were found. A sample was also taken from the bottom center of the trench (OEC ID. 21020302- 03). This process was repeated for the Fire Trench with the inclusion of a sample on the east side of the trench where the material seemed to be consistent along the length of both trenches. These results indicated elevated levels of the same constituents prompting further excavation. ncrete Excavation During further excavation of the trench, the outline of a brick structure was discovered containing loose bricks and soil. As this material was removed, a concrete slab was uncovered. Brick and soil from this excavation was placed into several twenty cubic yard bins. Chips of the Buena_ ::>.! A State Certified Small & WBE Business 4 BUENARESOURCES concrete slab and pieces of tile were analyzed for asbestos on 4/23 with all results negative for asbestos in any of the materials. This material was sampled by taking three samples from each bin. Material was taken from the center of each bin moving left to right at a distance of 3' apart for each sample (A, B & C), see OEC Lab ID Nos. 210508-01 thru 15. The concrete slab was removed and it was discovered that there was hydrocarbon impacted soil underneath the slab, possibly from the removed fuel tank. It is not known if that was the source, although there was only one tank found and removed. All hydrocarbon contamination found in each excavation was removed until we had "clean" excavation limits. The area between the two excavation sites are not suspected of having any hydrocarbon impacts as the two walls on either side and the excavation bottom were below action levels. Five samples were taken from the floor of the excavation immediately below the removed concrete slab (See OEC Lab ID Nos. 2102742-01 thru 05). The sample locations are as follows: NW Corner@8', NE Corner@8', SE Corner@8', and the center of the excavation at 8', all taken below the slab. The data for these samples indicated the presence of weathered hydrocarbon and that more material needed to be removed. Two twenty cubic yard bins of material was excavated and sampled in the same manner as the other bins, see OEC ID Nos. 2103212-03 thru 08. Once it was believed that all contaminated material was removed, two verification samples were taken from the excavation floor approximately 4' east and west from the center where the highest amount of petroleum had been removed, after an acceptable level was reached, the excavation was backfilled with clean soil. These were samples Bot. east@12' and Bot. west@12'. The area to the west and below the tanks were found to have been impacted by the diesel fuel along with Chromium, Nickel and Lead. All elevated metals above the SLTC testing threshold were tested, with all the Chromium and Nickel samples found to be below the Title 22 STLC (soluble) hazardous thresholds. Lead, however, did exceed the Title 22 threshold and would be Buenaresources A State Certified Small & WBE Business 5 BUENARESOURCES considered California hazardous material. Additional testing by TCLP RCRA method all reported levels below the RCRA threshold. The underlying soils under this site has a band of Serpentine, which is likely accountable for the reported Chromium and Nickel levels. This greenish material is very hard and, in this case, weathered with cracks. The diesel fuel appears to have migrated into these cracks requiring these underlying soils to be impacted requiring removal. The last samples taken on June 41n were all below the Region II ESLs for all hydrocarbon ranges and meet the closure criteria established for this site. The depth of this excavation was approximately 12' and 12' x 12' in size. The excavations are shown in Appendix A as Figure 1. 2.0 SOIL SAMPLING OF THE EXCAVATION 2.1 Soil Sampling Plan Samples were taken from the excavation sides and bottom. All soil samples were analyzed for full range hydrocarbons (gasoline, diesel and motor oil ranges) by EPA method 8015, Volatile Organic Compounds by EPA method 8260b and CAM metals. Each sample was sealed, labeled, placed in a cooler with ice and shipped to the laboratory. Analyses were completed according to the various methods specified according to SW-846 guidelines. Action levels used at this site were the Regional Water Quality Control -Region II ESLs (Environmental Screening Levels) for residential soils. The reason for the selection of contaminants of concern (i.e. why weren't SVOCs, PAHs, etc. included in testing) is because these compounds were not considered necessary due to the nature of the site. There was no indication that these constituents would be present for any reason considering the location and the types of businesses in the area. Buena.!�r.:_ A State Certified Small & WBE Business [: BUENARESOURCES 2.2 Sampling Maintenance and Security Upon collection, the sample containers were labeled in accordance with EPA protocols and chilled pending transportation to OEC, a State certified analytical laboratory located in Santa Maria, California following chain -of -custody procedures. All samples were recorded on Chain -of - Custody forms in ink and transferred to the laboratory according to EPA SW-846 protocol. Any changes or corrections were made by drawing a line through the error and initialing and dating the correction, then entering the correct information. 3.0 DISCUSSION OF RESULTS: Samples were taken at four wall locations and at two bottom of excavation locations below the tank. In addition, seven trench and four soil piles were initially sampled and were found to have lead at levels considered Cal Haz for STLC Lead. The soils in the five bins were also sampled to confirm the contaminates were hazardous. All five bins reported STLC lead at levels which exceeded the Title 22 guidelines for hazardous waste thresholds and were subsequently shipped as Cal Haz STLC Lead impacted soils to Waste Management's Kettleman Hill's TSD facility. The samples taken on May 5tn reported elevated diesel levels in three of the six samples. Those areas were further excavated with the final sampling on June 3rd reporting all bottom samples below the Region II ESL action levels for residential soils. All of the samples taken at the excavation sites reported no volatile organic compounds to at least the method detection limit (MDL) with the exception of the Soil Pile North Sample. The Soil Pile North sample reported n- Butylbenzene at 0.2 mg/kg, sec -Butyl benzene at 0.11 mg/kg and n-Propylbenzene at 0.15 mg/kg. All later samples taken after additional material had been removed, were below the MDL for all Method 8260b compounds. The CAMS reported nine samples with elevated chromium and six with elevated nickel levels requiring additional STLC testing to determine if the material was hazardous. The STLC levels were all below the California Title 22 hazardous thresholds for both the chromium and nickel and is not considered hazardous. Buenaresources A State Certified Small & WBE Business VA BUENARESOURCES It is important to note that elevated levels of these two metals are common in the Serpentine material found in this area. The reported TTLC levels were at levels high enough to require further STLC testing. All of those STLC results were well below Title 22 regulated STLC metal levels and likely would be considered typical background values for this area. 4.0 CONCLUSIONS: The one cement filled diesel tank was successfully removed by PPC and shipped to WM McKittrick Landfill facility for landfilling. Impacted soil from the fuel and lead leakage was discovered below the tank and adjacent to the tank location and was subsequently removed. A total of 64.52 tons of Cal Haz STLC lead impacted soil was removed and shipped to Waste Management's Kettleman Hills TSD facility. This material also reported elevated diesel range hydrocarbons in the side slopes and bottom which was removed and included with the material shipped to Kettleman Hills. Based on the above reported results, it is our opinion that there is no further work required at this site. It is our recommendation that this site be closed and backfilled after you review the Closure Report. Thank you for the opportunity to be of service. If you have any questions, please contact this office at (805) 346-1766. Sincerely, Buena Resources, Inc. 9 C-,O/ 12,�� Daniel P. Ringstmeyer, P.E. (043540) Owner/Engineer Buenaresources A State Certified Small & WBE Business 0 APPENDIX A Site Maps & Figures VICINITY MAP � a Bishop,,, c E m U d'r Highland Dr Slack St 101 E Foothill Blvd ,(a Real ,)t'et2 Dr Santa E� O Rosa P k -� N San Luis Obispo _' v 2028..1:J3A G?� . T 202BO i-;' 0,,0 ' 1t5s °sir sr 2600 Broad St, San L.. 2o2A, 0 2600 Broad St F`'tP ��\'San Luis Obispo, CA High St 93401 1 ' South St S Laguna Lake Park 20 , 201 irra-1 er Pare t � Southwood Dr 0�� VJ 0 C�2006 �Prado Rd 227 ,per Z 1 C� Damon -Garcia Rd 3. Sports Fields Tank Farm Rd QL m 0 3 MA v 1 � a eA NLt 11/ I� N 19&_� Full[ San Luis Obispo Mcc- esney Field %1 in� oy it ^ Evans Rd 0 mi 0.5 1 1.5 Copyright© and (P)1988-2012 Microsoft Corporation and/or its suppliers. All rights reserved. http://www.microsoft.conVstreets/ Certain mapping and direction data ©2012 NAViEQ. All rights reserved. The Data for areas of Canada includes information taken with permission from Canadian authorities, including:© Her Majesty the Queen in Right of Canada,© Queen's Printer for Ontario. NAViEQ and NAVTEQ ON BOARD are trademarks cf NAVrEQ. ©2012 Tele Atlas North America, Inc. All rights reserved. Tele Atlas and Tele Atlas North America are trademarks ofTele Atlas, Inc.© 2012 by Applied Geographic Solutions. All rights reserved. Portions© Copyright 2012 by Woodall Publications Corp. All rights reserved. NW Corner (-8) Trash pile of bricks Top of concrete, Center (-7') asbestoes Sample* *ot.W 012' Fire Trench T. Sample NE Corner (-8) Fire T. 1 E. Side Sample Fire W. Side Sample Su p T. West Wall Sample (4/06/21) Sump Trench A Bot. Center Sump Trench Sample Bot. 11�12 Su Trench W. Side Sample Below concrete (-8) (3/ 21) Sump Trench S. End Bot. Sample BASIS OF BEARINGS COORDINATES FOR THIS PROJECT ARE CALIFORNIA COORDINATE SYSTEM NAD83, CALIFORNIA ZONE 5, US SURVEY FEET, AS DETERMINED BY GPS OBSERVATIONS ON POINTS 8070, AND 8201 "MONTEREY" AS SHOWN ON THE CITY OF SAN LUIS OBISPO "HORIZONTAL CONTROL NETWORK" (JANUARY 2007). B04CIRYMM THE ELEVATIONS SHOWN HEREON ARE NAVD88 AS DETERMINED BY MEASUREMENTS ON POINT 81 AS SHOWN ON THE CITY OF SAN LUIS OBISPO "BENCHMARK SYSTEM" (JANUARY 2007) HAVING PUBLISHED ELEVATION OF 210.28'. �O 0� Note: Fire trench is 3' deep with excavation expanding to the west to include the 15' x 15' by 10' deep trash pit of bricks which were removed to concrete floor at —7'. An additional 3' of impacted soil was removed below the concrete and sampled on the sides and center. \ k T\ot\E \n�@8 1 �� \ L\\I f N:5769833.36 E: 769833 aJ/ .46 EL: 233.67' !fVS�Wy11�4/ -234- - / / / sr N: 2293367.98 E:576982 EL:23 V���• v o 0 ,L60 CONCRETE RETAINING WALL Buenaresources ENVIRONMENTAL, CIVIL, & GENERAL CONTRACTING SERVICES P.O. Box 2040, Santa Man,, CA 9345J-2040 P 805346.1766 F 805.346A767 0 5 10 1 INCH = 10 FEET SURVEY DATE: 06/10/2021 SITE EXCAVATION SAMPLES 2600 BROAD STREET SAN LUIS OBISPO, CA DRANK BY DATE JOB 110, DR 6/15/2021 CHECKED BY SCALE I SHEET 1 of 1 W I* McKittrick Waste *k, 56533 Hwy 58 W. Treatment Site Reprint Ticket# 156247 WASTE MANAGEMENT McKittrick, CA, 93251 Ph: (661) 762-7366 Customer Name PACIFICPETRO PACIFIC PETROLEU Carrier Pacific Petroleum Pacific Petroleum Ticket Date 05/13/2021 Vehicle# PPC 570 Volume Payment Type Credit Account Container Manual Ticket# Driver Ryan Hauling Ticket# Check# Route North Billing # 0001772 State Waste Code Gen EPA ID Manifest PPC 2021-000473 Destination Grid LF PO Profile 647907CA (FORMER FUEL TANK) Generator 144-NATURAL SANLUISOBISPO 2600 NATURAL HEALING CENTER (2600 BROAD ST) Time Scale Operator Inbound Gross 39760 lb In 05/13/2021 09:33:05 INBOUND Dcarmical Tare 29540 1b Out 05/13/2021 12:49:25 OUTBOUND Dcarmical Net 10220 lb Tons 5.11 _. Comments Truck was held up pending paperwork corrections Receiving: Mon -Thu Drums 7-3, Liquids & Roll -offs 7-4, End Dumps 7-5 Product LD% Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------------------- 1 SpwasteSolidOth-Cu 100 1.00 Yards SANLUISOBI 2 EVF-P-Standard Env 100 SANLUISOBI 3 FUEL -Fuel Surcharg 100 SANLUISOBI 4 RCR-P-Regulatory C 100 % SANLUISOBI 5 WWM-P-Waste Water 100 SANLUISOBI 6 HARD2HANDLE-Hard T 100 1 Load SANLUISOBI Total Tax Total Ticket Drivers Signature NON -HAZARDOUS I. Generator ID Number 2. Page 1 of 3. Eme Berry Response Phone 4, Waste Tracking Number WASTE MANIFEST 5. Generators Name and Mailing Address Generator's Site Address id differem then mailing address) 'ia�OyPno ??(/ G /� _.:w,,: .^� ::— '�ryly✓6 &wsld' e-o Vsporter 1 Company Name=` U.S EPA ID Number �,Tlar sporter 2 Company Name - U.S. EPA ID Number 8. Des grated Fac l ty Name and —Se Address U.S. EPA ID Number �. sir 1`� �_i.. •_ is Phone. 8. Waste Shipping Name and Description 1. 2. 11 10. Containers 11 Total 12. Unit No. Type Quantity WtNd. 13. Special Handling Inswctwns and AddibonaInformation `�`I 14. GENERATOR'SIOFFEROR'S CERTIFICATION: I hereby declare that the contents of this corlsignmem are fully and accurately described above by the proper shipping name. and are classified.. packaged, marked and labeedlplacarded, and are in as respects in proper condition for panspod according to applicable irhemational and national governmental regula . ns. Ge�;rs0fleror' dmedrr pr;d Name 'net Momit Day Year I I_�, 1 7� 15. Imemational Shicments ❑ Import to U.S. ❑ Expotl U.. Pod of entryrexiP T er S ature I for a<nods ona t Date leav l U S 16. Transporter Ackriow*dgmenl of Receipt o! Materials Trarsp i Pdnted,Typed Name Signature Month Day Year [31^ Transporter 2 P' dlrytled Name --- 17, Discrepancy 17a. Discrepancy Indication Space ❑Quantity El Type t 17b. ABemate Facility (or Generator) J U tar Fadhtys Phone: W 17c. Signature of Al(emate Facility for Generator) Q a � to Wr p 1 18. De-s4qued Fai ...a- Operatar Ce.. coon 0-"ipt 01 dals covered by the manifest a pt as P ntedTyped Name 169-EtLC-0 6 104 91 � I ❑ Residue ❑ Partial Rejection ❑ Full Rejection andesl Reference Number. U.S. EPA ID Number Year moth Dar Year D FACILITY TO 6FNERATOR C man Hills Landfill Reprint 3' Skyline;Road, P.O. Box 471 Ticket# 55260 Keih�zimAerejA, 93239 Ticket Date 05/24/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667316JJK Grid B18 _ Volume Yards Carrier CAD981164312 Driver Arturo Vehicle # G249 Vehicle License 9F36934 Container # 4NP7786 Container License 4NP7786 Time Scale Operator In 05/24/2021 11:46 MANUAL WT A. Ortega Gross 75320 lb* Inbound Out 05/24/2021 12:41 A. Ortega Tare 44320 lb* * Manual Weight Net 31000 lb Tons 15.50 -• Comments _. Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 NONH DISP-TONS-Non 100 15.50 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature Please print or type. (Form desgned for, use on elite i 12I pitch) typewriter.) UNIFORM HAZARDOUS i. Generator ID Number 2. Page i of 3. Emergency Resaonse Phone WASTEMANIFEST vt_: '.=- - GeneratorsS:teAddresslddFzr 5 Generators Name and Mailing Address Genieraawrs Pnone r.,'Q1"" - _ _ - _ .. 8. Transporter 1 Company Name B.DasignatedFaa'NtyName and Site Adores$ ,,,E cr..F,T Le � Fac3irfsPnone: -`- :,•.�_'- 9b. U S. DCT Description. Gndudng Proper Shipping Nama, Hazard Class. !D Number, t0. Con a ne s HM and Paddng Group (d any))cc 27 c' Form Approved. OMB No. 2050-0039 rl�noZfj16 JJK than n ag address) Q,S. EPA 10 Number U.S. EPA ID Number U S. EPA ID Number I I. Total 12 UM 13 Waste Codes Quantity W1Nd. peaal Handling InsNuctions and Additional 1*-al- GENERATOR'S' ROR'S CERTIFICATION: I hereby declare that the contents of this consignment are Uy and a curate!y desoibed above by Ine proper S*, P g name and are dassi�e— Packaged. marked and laheled'p.'acarded, ana are in all respects in proper condition kr transport according to app%able :ntemaliona' and national govemmentar regUk tins. If expdrt aNpment and I am the Primary Exporter, I certify, Thai Ste contents of this consignment conform th rite terms of the attached EPAAdmMeagmem of Consent I cenify I'at the waste minim'izabdn stetamant ideafiPsd n 40 CFR 28227(a) (K I am a large quanbly generator) or (b) (d I am a smet quanary generator) is true. t17 Day ratr"rmemrsPrinle rypedNams Signature w r `� f7-7 I! 16.bx,bdralShi-r. ' �.,7ImpodtoU& ❑E.1tfttxnU.S.V Ponofenay?ex¢ — Transportersgnanre(fo exponsordy): DateleamyuB. 17. Transpwtertcknowledgment of Receipt of Materials _. 18. Discrepancy ffi 18a. Discrepant' lnd,cason Space Quantity Typo EI Res -due ❑ Paral Rejection Manrfes P,erzrer- "moec 18b Alternate Facility (or Generator U.S EPA ID Numb, C) tat Facility's Phone. W 18csilnelure of Alternate Faddy for Generator) Q z 0 d9. Hazardous Waste Report Management Method Codes (i a, codes for hazardous waste treatment disposal. and recycling systems) 0 1 2 3 t Morn!* Dav 'ea' f� Month Dav Year ❑ FU,I Reiefmcn 20. Designated Facitt'i Owner or Oparator. Certification of receipi of hazardous materials covered by rite manifest ex^ P! as nded in IP m i8a nth Day Year PrintedlTycsd a 2 Y'ODE PINATir STATE (IF�£QU!R£D) EPA Form870:•22(Rev 3-05)Prevouseditionsareobso!ete C man Hills Landfill Reprint 39= Skyline®Road, P.O. Box 471 Ticket# 55489 Ke*A%3%*m&TAmGidxjiqEr,fiA, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667317JJK Grid B18 _. Volume Yards Carrier CAD981164312 Driver Vehicle # G1076 Vehicle License 9F18973 Container # 4NC6734 Container License 4NC6734 Time Scale Operator In 05/28/2021 10:45 MANUAL WT A. Ortega Gross 71860 lb* Inbound Out 05/28/2021 12:25 A. Ortega Tare 43720 lb* * Manual Weight Net 28140 lb Tons 14.07 Comments T, Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 NONH DISP-TONS-Non 100 14.07 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 % SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Drivers Signature | - ----------- I 9b. U.S. DOT De finduding Propel" SIVPing Name. Hazard Class, ID Noter, 10. Containers; It. Total 12 Unit .7 HM ancl Packkq GrDW (if any)) No Type o-try m1vol. 13. Waste Codes 15. GENERATOR'SIOFFEROR'SCERTiFICATO: I hereby declare that the contents of this conArtmeni am fWly and accura" desunbed abwe by the proper shipping name, and are dassft, marked and labeledoacarded, and are in all respKts in VW c0ndlitiOn ibr transport axordrig to applicable mternabonal sad national governmental regL48tiDrs ff export shiptrend &V I am N Primary Exporrair. I MrfiN that thle ODnM Of this consAtirnerit conto to the terms of & aracbed EPAAMmlectment of Consent, I ceray ftl t1he waste minimizabon statement identified in 40 CFR 262 27(a) (it I am a Wge quarbity generator) or (b) (if I am a small is true. 16, International Shipments K] Import to U.S Export from U.S Pon of antry�exit: Tranvoilo signawre (for exports orgy): Date leaving U S: 17 Tiansporer Adjaidecigtonent of Receipt of Materials Transporter I Proled7yDed Nam 5 lonth Day Year 1 B. Discrepancy 18a. Discrepancy inkation Space El o,.tqy El Type iZ Faclity's Phone C' man Hills Landfill Reprint 3. Skyline,Road, P.O. Box 471 Ticket# 55500 Kerw►erft-n,, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667318JJK Grid B18 r Volume Yards Carrier CAD981164312 Driver JUAN Vehicle # 65424M1 Vehicle License 65424M1 Container # Container License Time Scale Operator In 05/28/2021 12:43 MANUAL WT A. Ortega Gross 46680 lb* Inbound '- Out 05/28/2021 14:02 A. Ortega Tare 32740 lb* * Manual Weight Net 13940 lb Tons 6.97 Comments REPLACEMENT TICKET FOR TICKET # 55490 Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 6.97 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature qjq_ 65441vj ' Please Print Or I)ijoe. (Form designed for use On elite (12-pich) lYpewriter.) UNIFORM )U 10 Number WAS=IFEST S I Generator - N on _-Re r2 �a"fc um be ,pitch, pewfte,) S Gn-:t,,,, ID G 5. Generators Name Mailing Address Gene GenwawPbories Phone. 6. Trans" 1 company Name 7, Tr.wsoort,, 9 Page 1 of TE -4 R.spmrsa �Ph. 9, 9K U.S. DOT D,,#, (-kd% Proper *Pmg Name- Retard Class ID Number, HM andP" Grout (if any)) 10. Contaimm No, 0 Form Approved. OMB No 205W39 Number 667318 JJK 11JOW 12. Unit Quan* Wl.Noj 13. Waste Codas 20 — - —-I — am AOMMU Informabon 2 074 15 GENERATWISICHME11101i I CERTIFICATION; 110111 1 hereby declare tlwt the contents of this CmWnment are fully and am I I C: MIgnarnw.i —alksc and 111�. and a' -Pecls'n Proper condition for 11311POrt according to applicable international national vemmerttal ;; are �d_wwk-*, IfexPOIsluorriantand lam U*P*ary EVOler i car* 04 ft CONeIVIS of this Consignment conform tollia terms OfftaWed EPAA6nowWqwj OfC. sent. stiltef"w"t identified in 40CFR 262,27(a) (it I am a large q-bly genera Of(b lama - llQua jgerieral5i sigra re Lj 11 iii! Day Year 1 6 �&matwal sw�w& El import to U.S. TrMPOOOr Mture (forez wts o*): ❑ Export from u S. Port ofenvylexit: 17. TmrsporarA*owWgrwt WReceipt ar Materials Date leaving U 5: J�� Signature Month Day Year 18. Dwepancy - 18a- Dweparicy Indication Sm. 11 Quantity ❑ T. ❑Rescue ❑ pmai R*O. ❑ Full Refecti. 18b. _Aft.,r_e _Fad_q(o, _Gae­re,—, ManVest Referem Number- Va. EPA �D Number FadWs Prom: rn 1 M HM*uS Waste Report Management meow codas (i.e codes for hazardous waste treatment disposal, and Ui 1. recycling systems) 0 20. DOSIgMtad Facility Dona Or OPK2W. Certification 01'receipt of hazardous materials Covered by the manifest except t T2!_ �"Ihm i1a I �Ot(6jro Signature year E Form 8700-22. Ov. 3Previous)Previouse6ors; are obsolete Its U ?J OESIGM 9:AC7LIT E INATIO J STATE (IF REQUIRED) Cman Hills Landfill 3` Skyline,Road, P.O. Box 471 KemaiA"ErfiA, 93239 Ph: (559) 386-9711 Reprint Ticket# 55678 Ticket Date 06/04/2021 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667326JJK Grid B18 -. Volume Yards Carrier CAD981164312 Driver Vehicle # G1072 Vehicle License 537551TZ Container # Container License Time Scale Operator In 06/04/2021 12:03 MANUAL WT A. Ortega Gross 68100 lb* Inbound Out 06/04/2021 13:38 A. Ortega Tare 45140 lb* * Manual Weight Net 22960 lb Tons 11.48 Comments Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 11.48 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Drivers Signature Olmec ,vint nr rvne IGmn Hacirv�ix�frr'iI , m afitp. N 7-nitrhi hrrPmitar l Form Approved. OMB No. 2050-0039 UNIFORM HAZARDOUS tT*rwrator ID Number F 2. Page 1 of 3. Emergency Response Plane 4. Manifest Tricking Number 015 6 6 3 2 6 A WASTE MANIFEST-1186U 1 BX-9_ 71_ :- 6 5. Generator's Name and Mailing Address Generatoes Site Address (d different than mailing address) r�HC SLO 908 HUSTON ST GROVER BEACH, Ck 934-3= US' 2640 6FST S�"q LUIS IS 0HiS�O. Gr �34u' US6. Gsremlor'sPtane: 7 d =�:: +=t Transporter 1 Carpany Name U.S. EPA ID Number Pacmc Petfo7 e0m C4,1nc. CAJ7941164312 7, Transporter 2 Company Name U.S. EPA ID Number 8. Designated Facility Name and Site Address U.S. EPA ID Number cHEM1c.AL+�','.ASTE MArwwGEnlEiuT.INC C4T7Cf�4.`+1' 35251 OLD SKY;_INE ROAD NETTLEMAM CITY, CA. 932,59 US F sPhone: 55t59'11 9z 9b. U.S. DOT Description (mdAng Proper Shipping Name, Hazard Class. ID Number, 10. Containers it. Total 12. Unit 13 Waste Codes No. Type HM and Packing Group (f any)) Quantity Wuvol. X 1' RG, UN3077, EhttRONMENTALs.: +-02ARDOL0,; Sv8"sTPACE Sr_11 0 zQ 161 or1.0. S L E,aD d z 2. i W 3. 4, 14. Special Handling Instructions and Addtional Information �l S �b� 2 c) �•/ v>ear ah.appropnale PGE 24 Hotir f nergencr ReWf1e >x,,50E) 925-1947 Prolie It CABIC-6 ; 15. GENERATOR'S/OFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are class K packaged, marled and Iabeladlplacarded, and are in d respects in proper condition for transpon according to applicable intemadonal and national governnenral regulations. If export shipment and I am the Primary Exporter, I cerl6y DW the contents of this consigmmend conform th to larms of the attached EPAAda %1*ment of Consent. I certdy that the waste minirnivdo i statement identified in 40 CFR 262.27(a) (if I am a large quantity generator) or (b) (d I am a small gypAttl generator) is true, �{ Month Day 7Year /� 1 16, Intamational Shipments El to U.S. I Ezpod(ranU.S Portofemryyezit. Z Transporter signature((orexportsonly): Date leavngU.S.: IX 17. T ampoterAdaaxledgn ant of Receipt of Materials Transporter 1 PrinteciTyped Name Signature March YW L) A� Cry aTransponer 2 PnMedry* Name March Day Year z 16. Discrepancy 18a. Discrepancy Indication Space quantity Type ❑ Residue El Partial Rejection ❑ FLA R*cbm Mandest Rafe ence Num�e I8b. Alternate Facility (or Generatorl US, EPA ID Number J U IL FadWs Phone: w 19c. Signature of Alternate Facility (or Generator) Month Day Year z N19. Hazardous Waste Report Management Method Codes [i.e.. miss for hazardous waste treatment, disposal, and recydkv systems) � 1 N\2. 32 3. 4 20. Designated facility Owner or Operator: Certification of receipt ofhazardous materials owed by the manifest except as noted in Item 188 PrintecliTyped lime Sgnadrre Month Day Year EPAForm8700-22(Rev.3-D5) Prevroutsedrborrsa2wosi-se. DESIGNATED FACILITY TO GENERATOR STATE (IF REQUIRED) CWM,i %,�-rZeman dills Landfill Reprint 3 .257 01.v Skyline, Road, P.O. Box 471 Ticket# 55679 KebAn§vsetau► ErikA, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667327JJK Grid B18 Volume Yards Carrier CAD981164312 Driver JAVIER Vehicle # G383 Vehicle License 65425M1 Container # 4ND3836 Container License 4ND3836 Time Scale Operator In 06/04/2021 11:44 MANUAL WT A. Ortega Gross 77000 lb* Inbound Out 06/04/2021 13:31 A. Ortega Tare 44020 lb* * Manual Weight Net 32980 lb Tons 16.49 - Comments Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 16.49 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Drivers Signature tAV - -19 38 0K1 i:3.53- HND3�` Pkmgp, ruint or tme. (Fam desitmed for use on elite 112-ttkh) tvoewriter.) Form Aooroved. OMB No. 2D50439 UNIFORM HAZARDOUS 1' morel" 2. Page 1 of 3. Emergency Response Phone 4. Men>cesl Trockkg Number WASTE MANIFEST 1 01 5 7 J J K _ i , _:r 5. C-w*mlWs Name and Maging Address Generator's Site Address (t c1ftent than maTmg address) NHC SLO 98B HUSTON S7 ^r,n _n `% BO GROVER ®EACH. C- V-4K 5 " Generamts Phone: r c_, + n,a SAN LUIS O&SPO. Cx �0401 US 6. Transporter 1 Canpany Name U.S. EPA ID Number Pactac Petroleum CA., foe C,AD981164312 7. Transporter 2 Company Name U.S. EPA ID Number 8.De*WedFackNarpeand Site Address CHEMC41 WASTE MANAGEMENT INC US. EPA ID Number 3SZ1 OLO SKYLINE ROAD CATi)QU6461,7 KEME61AN CITY, CA. 93239 US FaciWs Phone: 559.3*'9711 ga. 9b. U.S. DOT Descriplion (including Paper Shipping Name, Hazard Class. ID Number, 10. Cantor ne s it. Total 12, Unh HM and Parma Group It any)) Quent y ftw. 13. Wade Codes No. Type X 1. F0, UN3077, ENWOWBITi ,LLY HAZARDOUS SUES'nNCESOLIO N U. S. LEAD a�. Cs.I �� T' 181 — 2 LU 3. 4. 1 14, Special Hand) rig Instructions and Additional Information c2 wear aN appropriate PPE v� 1 OWE 24 Hour Emergency Response #I (t106) 4219d' A 03,39 Prvme #! CAS19920 15. GENERATORWDFFEROR'S CERTIFN;ATION: I heresy dedare, that the contents of this consignment are f k and aoanately described above by the proper shipping name, and are ciassrrred, packaged, marked and labeled/placarded, and are In all respects in proper mrkdfion for transport acm*9 to appkable international and national governmental regulations. If ee,ort shipment and I am the Primary Exporter, I kxrtty that the contacts of this corxignmerht mnkxm b the terns of the attatlad EPA Acknowledgment of Consent. artily that the waste mudmmlion staternent identified in 40 CFR 26227(a) (t I am a Iarge quantity generator) or (b) '' am a mail gntty generator) is true. G��gq�'.�o�slOB'er`oPs P`r"in�tedlryped Nance Signature Mordr Day Year F 1,. onai Shipments ❑ Import to U.S. — — — ❑ Expon from us Pat of antryfea Z Transporlarsignature(forexporlsonly): Dale leaving U.S. — — K 17. Transporter MaloutedgmentofRecoofMaterials 18. Discrepancy 18a. Discrepancy Imitation Space ❑ 0=6ty Signature ❑ Type ❑ Residue Manifest Reference Number. h 19. Hazardous Waste Report Management Method Codes (i.e., codes for hazardous waste treatment. disposal, and 1 2. 3. 20. Designated Facility Owner or Operator: Certification of receipt of hazardous materials covered by the manifest eu r"d yyed Name _ Signature �'(':h'P �at�hr0 PA Form 8700- 2 (Rev. 3-05) Previous edit ons a# obsolete nec Month Day oc Otta Montle Day I l I ❑ PaNal Rejedan ❑ Full Rejection U.S. EPA ID Number 1 Month Day 4, noted in hem 18a 1 11 Month Day Yaw UE6 FACILITY —c! GENERATOR STATE (IF REQUIRED) APPENDIX B Lab Summary Spreadsheets Q U U c Q C O u U X W Q (NC C N N N 02 U Y � C ca H . E N V) 0 O 4+ m O m J c .0 CA ta ors � 01O0 J � W N C E o o 0 O p �p V -1 N Lo e�-I N 00 O J J W N 1A J0) F 0 .-00 N 0NM� O N r ON O� N to N 0 0 p O D O O 0 0 0 0 0 o o 0 O O O M J O U) N r O N O O N V) O LO O N O NOO Q O 00 N Cl) N LO U 3 N 00 ONp O Cl 00 lfl Q M tD vl N Q. ^ N r-I 00 00 O O N r-1 O O O ri Ln `i V O p M n O N O E V V V V V V 7 N "O c W 3 ri Q1 p N O O1 a) N N lD ei NO ai f� Q1 G1 Ol Ol 0 0 ri q M � ri � rl O O �11 f� p v N V V V V V co Y H C YJ W N O N M N n M N �,/� M a --I M Ln Q M M 01 n M 01 M M 4. 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N E 7 OL a3+ v �' ra v O O d O u E — E i, ra a� Q 3 u > ai-Nd � •O E 'a ca s U ++ O 'O t7 c L i •l6 N O u > f6 �_ C 2 2 2 t0 C Q Q m v m m U t U O U O U Z N in I— > N N U 2 Y F H 00 V APPENDIX C Site Photographs }4 West Wall & Excavation Floor. Av •J OIL- _ . �, -y� , - 4 •M1 ^ _ice` � .w�+-� �•. -- .i c • yid yv -rY �� � "t •' ��, _t1.� '�'T � =.'rr' t fir. ~r- �: - ��� � - - � - - - -_ •„/ y'� �� - r •+der - '..;•. .r 1 /�. • :' .. - r r/r` � - is 75 J iy4t �J. r f� y f w • ' •f 1 fit ' f ` r '�1.� � .r - . .mac �,s, .• �•`�, � � 't ' ' , , ' �►.`, P lip jilm, F _0 ---~_-'� ` Excavation Floor. NO East Wall.' .,F� f,. - ►F.'. _-�'7•L� - '�yst:�4` r..`, •IM/z AL ,ice a.� '� ^�' .. '?fir• ,• r :r.• ---�y_ r ._!_�� s � ��� �" r . Iz13. ^. �a �,, • • � Y� � �r7J�r.jy� .ice _ �� `• - . •�, J��'., ��!_ y r .•5. L!�' - - r.Y,- ,�� tr� *^_�; s - •:• • '��•,. � f , �. Vo VIP- 14 �• ' � fir. , � .. rri! �• , F��[— .. � ~�' - R _+ ,• ' tilt'-r � � .� 40 mr, r T"yam �. �`.�, r'�i f ������ •- � •,fie. �� ,W,4 East and South Wall �ir�z,tir -+ ��'�'• �J! i ',_:... •_ I.J, -- 4ol' • •' Jiv �r•. yr� }ram,' y!. • . 'i1_ - - 'cam ►.. . _ , r / _ :r S•, - • . . .•• �.. -_•4' y -� � �� �Y�..V _ Y��"�r� v - � fir' - � - r de Aqw- LA yy'ttt yy- r _ k. w Y �~��`'L:. ,wry` '�,,, 4--: - i � y ++'��_ f _ � +�• : r ti '! � � � -.� ,�/�-..,.;�ra 1• .M ' k a�r' �(qLr } `. k ! ~F ''�• f` 7' 1i •• f ~ _ �'� . i +`y _ ..ram AW • .r �,f.� ;*c•� i,; •,'�'�=i�! �,; �R. fir, fi��� •w� �'. . Jk�.. •x AV . - Y ter/ 1�' .r� _.J^' •� .•� - ' r APPENDIX D Laboratory Reports & Chain of Custody Forms ( 6 iz Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2103212 Pacific Petroleum California P. O. Box 2646 Report Date: May 28, 2021 10:05 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 24, 2021 13:05 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 WWW.oecusa.com FAX: (805) 925-3376 Page 1 of57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom West Center 2103212-01 Solid Solid 05/24/2021 11:20 05/24/2021 13:05 Bottom East Center 2103212-02 Solid Solid 05/24/2021 11:25 05/24/2021 13:05 Bin 20339-A 2103212-03 Solid Solid 05/24/2021 11:30 05/24/2021 13:05 Bin 20339-B 2103212-04 Solid Solid 05/24/2021 11:35 05/24/2021 13:05 Bin 20339-C 2103212-05 Solid Solid 05/24/2021 11:40 05/24/2021 13:05 Bin 20144-A 2103212-06 Solid Solid 05/24/2021 11:45 05/24/2021 13:05 Bin 20144-B 2103212-07 Solid Solid 05/24/2021 11:50 05/24/2021 13:05 Bin 20144-C 2103212-08 Solid Solid 05/24/2021 11:55 05/24/2021 13:05 Sample Batch Preparation Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List BI E0696 05/25/2021 08:55 STLC Metals Extraction STLC Metals Extraction B I E0743 05/26/2021 08:58 TCLP Metals by ICP 601013 TCLP B I E0794 05/27/2021 10:55 TCLP Metals Extraction TCLP Metals Extraction B I E0744 05/26/2021 09:03 Total Metals by CVAA Mercury Total EPA 7471 A B I E0694 05/25/2021 07:50 Total Metals by ICP 601 OB Total B1 E0693 05/25/2021 07:26 Volatile Organic Compounds by GUMS 8260B Full List Volatile Organic TPH by GC/FID 8015 TPI1-Gasoline B1E0697 05/25/2021 09:00 B 1 E0737 05/26/2021 06:59 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 2 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by : Clarence Reynolds Lab ID: 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercurc 0.22 0.093 mg/kg 1 B I E0694 05/25/21 14:04 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B IE0693 05/25/21 14:18 EPA 6010B - Arsenic 7.0 1.9 Barium 560 0.96 Beryllium ND 0.48 -, Cadmium ND 0.24 Chromium 120 0.48 N-02, N-03 Cobalt 21 0.48 —� Copper 43 0.96 Lead 7.3 0.48 blolvbdenum 0.62 0.48 Nickel 160 0.48 " Selenium ND 1.9 Silvcr ND 0.48 Thallium ND 0.96 Vanadium 46 1.9 Zinc 56 1.9 TCLP Metals by ICP Chromium ND 0.050 mgiL 1 B1 E0794 05/27/21 19:15 EPA 1311 /EPA 601OB Volatile Organic TPH by GOOD TPH Gasoline (C5-('12) ND 0.50 mg/kg 1 BIE0737 05/26/21 13:56 EPA 8015M Surrogate: 4-Bromofluorobenzene 101 S' , (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: [8057 925-3376 Page 3 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) TPH Motor Oil (C23-C40) Surrogate: o-Teiphenvl 51 10 mgtkg 1 B I E0690 05/25/21 14:26 EPA 8015M ND 50 90% (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: _ 805 925-3376 Page 4 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg.!kg 1000 B 1 E0697 05/25/21 15:16 EPA 8260B Broinobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofortn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chlorocthanc ND 1.2 Chloro%rrm ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 12 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 1.4-Dichlorobcnzcnc ND 1.2 Dichlorodithioromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1.1-Dichloroethene ND 1-2 cis-1,2-Dichloroethene ND 1.2 trans-1.2-Dichloroethene ND 1.2 " 12-Dichloropropane ND 1.2 " 13-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1.1-Dichloropropene NI) 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbcnzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 805 925-3376 Page 5 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Wexachlorobutadiene ND 1.2 mg/kg 1000 BIE0697 05/25/21 15:16 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 " I.1.1,2-Tetrachloroethane ND 1-2 " 1.1.2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND L2 Toluene ND 12 1,2,3-Trichlorobenzene ND 1-2 1,2,4-Trichlorobenzene ND 1 2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1-2 Trichloroethene (TCE) ND 1 2 Trichlorofluoromethane ND 1-2 1,2,3-Trichloropropane ND 1 2 12,4-Triniethylbenzene ND 12 1,3,5-Trimethylbenzene ND 12 Vinyl chloride ND 1 2 Xylencs (total) ND 1. Surrogate: Dihromo/luoronreth(iiir lr+1 %,, r '.l L'2) Surrogate: Toluene-& M 2 ''r, { 65 - 1-Is 1 rr rr Surrogate: 4-Bromollimroben-ene 97 % { 7;m The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 57 ( A WAMS im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA AnAyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mglkg 1 B 1 E0694 05/25/21 14:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 E0693 05/25/21 14:21 EPA 6010B Arsenic 6.6 1.9 " Barium 220 0.96 " Beryllium ND 0.49 Cadmium ND 0.24 " Chromium 120 0.48 N-02, N-03 Cobalt 19 0.48 " Copper 39 0.96 " Lead 8.3 0.48 " Molybdenum ND 0.49 Nickel 150 0.48 " Selenium ND 1.9 " Silver ND 0.48 " ' Thallium ND 0.96 " Vanadium 51 1.9 " Zinc 62 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/t. 1 BI E0794 05/27/21 19:17 EPA 1311 /F.PA 6010B Volatile Organic TPH by GC/FID TPIIGasoline (C5-('12) 2.2 0.50 mg/kg 1 BIE0737 05/26/2115:34 EPA9015M D-04 Surrogate: 4-Bronu)/luorohc'n_ene II c� `J (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 330 10 mg/kg 1 B1E0696 05/25/21 14:03 �TPH Motor Oil (C23-C40) ND 50 11 11 11" Surrogate: o-Teiphenvl 108'i£, (65 - 136) EPA 8015M 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: (805)_925-3376 Page 8 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 15:43 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromofonn ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chlorocthanc ND 1.2 " Chlorotitrm ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibrontocthane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzenc ND 1.2 1,4-Dichlorobenzcne ND 1.2 DichlorodiFluoromethanc ND 1.2 " 1,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 LI-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene NI7 1.2 " 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1. 1 -Dichloropropene ND 1.2 cis-13-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbcnzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 Bl E0697 05/25/21 15:43 F.PA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 " 1, 1, 1 .2-Tetrachloroethane ND 1.2 1,L2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 " Toluene ND 1.2 " 1,2.3-Trichlorobcnzcnc ND 1.2 " 1.2,4-Trichlorobenzene ND 1.2 " 1, 1, 1 -Trichloroelhane ND 12 1,1,2-Trichloroelhane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluormnethane ND 1.2 " 1,2,3-Trichloropropane ND 1.2 1,2.4-Triniethylbenzene ND 1.2 " 1,3.5-Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2" Surrogate: Dihromollumantethane 101 % (74 - 122) Surrogate: Toluene-d8 102 (65 - 128) Surrogate: 4-Broma/luorohen_ene 96 °ii, (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 57 a A ircrQ Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mg!kg 1 BIE0694 05/25/21 14:08 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg I BI E0693 05/25/21 14:24 EPA 601 OB Arsenic 5.1 2.0 Barium 230 098 Beryllium ND 0.49 Cadmium ND 025 Chromium 160 0.49 N-02, N-03 Cobalt 21 0.49 Copper 47 0.99 Lead 11 0.49 N1olvbdenum 0.74 0.49 Nickel 190 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 62 2.0 Zinc 72 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L I BIE0794 05/27/21 19:20 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 4.2 0.50 mg/kg I BIE0737 05/26/21 16:26 EPA 8015M D-04 Surrogate: 4-8romu/luorohen_ene it R % (39 - 157) 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 57 CW K Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GUND TPH Diesel (C13-C22) 350 10 mgtkg 1 Bl E0696 05/25/21 15:12 EPA 9015M TPH Motor Oil (C23-C40) 55 50 Surrogate: o-Tetphen-vl 112 % (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analvtical Report Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mglkg 1000 BIE0697 05/25/21 16:11 EPA9260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 .� Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 " Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chlorocthane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromelhane ND 1.2 _.. 1.2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzenc ND 1.2 IA-Dichlorobenzenc ND 1.2 Dichloroditluoromethanc ND 1.2 1,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 ],I-Dichloroethene ND 1.2 " - cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 " 22-Dichloropropane ND 1.2 " 1.1-Dichloropropette ND 1.2 cis-1.3-Dichloropropenc ND 1.2 trans-1,3-Dichloropropenc ND 1_2 Ethylbenzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report foi- Samples Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 1.2 mg/kg 1000 BIF.0697 05/25/21 16:11 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 12 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,12-Tetracldoroethane ND 1.2 1,1.2.2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 Tolncnc ND 1.2 I.2,3-Trichlorobenzcnc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1.24-Trimeth0benzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromolluorwee'thane l02 % ( 74 - 122 ) Surrogate: Toluenc48 103 So (65 - 128) Surrogate: 4-8romo/luorohen_ene 97 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreponts TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:_(805) 925-3376 Page 14 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical i Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mg/kg I B I E0694 05/25/21 14:10 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 E0693 05/25/21 14:26 EPA 6010B Arsenic 10 1.9 Barium 290 0.96 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 710 0.49 N-02, N-03 Cobalt 47 0.48 Copper 52 0.96 Lead 13 0.48 Molybdenum 1.2 0.49 Nickel 1900 0.48 N-02 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 77 1.9 Zinc 83 1.9 TCLP Metals by ICP Chromium ND 0.050 mgil- 1 BlE0794 05/27/21 19:23 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 0.76 0.50 mg/kg l B1 E0737 05/26/21 17:18 EPA 8015M D-04 Surrogate: 4-Srontq/Iuorohen ene 101 I (39 - 157) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 57 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical t Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (C13-C22) 71 10 mg/kg 1 B I E0696 05/25/21 13:41 EPA 8015M TPt1 Motor Oil (C23-C40) ND 50 S17v0gat(•: 0-7ilphenrl 106 % (65- 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg�kg 1000 B1 E0697 05/25/21 16:38 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromometliane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tent-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 " Chloroethanc ND 1.2 Chlorofor n ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichlorobenzene ND 1.2 " 13-Dichlorobenzene ND 1.2 I A-Dichlorobenzene ND 1.2 Dichlorodifluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 LI -Dichloroethene ND 1.2 " cis-1,2-Dichloroethene ND L2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane NI) 1.2 1,3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1,1-Dichloropropane ND 1.2 cis-1,3-Dichloropropcne ND 1.2 trans-1,3-Dichloropropcne ND 1.2 Iithylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 16:38 EPA 8260B 4-Isopropyl Toluene ND 1.2 " Isopiopylbenzene ND 1.2 " Methylene chloride ND 1.2 " Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 " 1.1,2,2-Tetrachloroethane ND 1.2 " Tctrachloroethene p'CE) ND 1.2 " Toluene ND 1.2 " 1,2,3-Trichloroben7cne ND 1.2 " 1.2,4-Trichloroben7.ene ND 1.2 " 1,1,1-Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 " 1,2,4-Trimethylbenzene ND 1.2 " 13,5- Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 Xylcnes (total) ND 1.2 " Surrogate: Dihranolluoronietlunu' 100 Y ( 74 - 122) Surrogate: Toluene-d8 101 `,'l, ( 65. 128) Surrogate: 4-Bromglluoroh(,n_ene 97 ` , ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 1.4 0.092 mg/kg 1 B 1 E0694 05/25/21 14:12 EPA 747 ] A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I E0693 05/25/21 14:13 EPA 6010B Arsenic 6.1 2.0 Barium 220 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 140 0.50 N-02, N-03 Cobalt 21 0.50 Copper 46 1.0 Lead 19 0.50 Dlolvbdenum 0.57 0.50 Nickel 180 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND H) Vanadium 54 2.0 "Zinc 87 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BIE0794 05/27/2 1 19:25 EPA 1311/EPA601(1B Volatile Organic TPH by GOOD TPH Gasoline (C5-C12) 2.3 0.50 mg kg I B I F0737 05/26/21 19:53 EPA 8015M D-04 Surrogate: 4-Bronrojluoroben:cne 107 Y,„ (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical i Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPA Diesel (C13-C22) 390 10 mg/kg I B 1 E0696 05/25/21 14:49 EPA 8015M TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Teiphenyl 105 35 (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.3 mg/kg 1000 B1E0697 05/25/21 17:05 F.PA8260B Bromobenzene ND 1.3 Bmniochloromethane ND 1.3 Bromodichloromethane ND 1.3 Bromoform ND 1.3 Bromomethane ND 1.3 n-Butylbenzene ND 1.3 " sec-Butylbenzene ND 1.3 tert-Butylbenzene ND 1.3 Carbon tetrachloride ND 1.3 Chlorobcnzcne ND 1.3 Chlorocthane ND 1.3 Chloroform ND 1.3 Chloroniethane ND L3 2-Chlorotoluene ND 1.3 " 4-C'hlorotoluene ND 1.3 " Dibromochloroniethane ND 1.3 " 1.2-Dibronio-3-chloropropane ND 1.3 1,2-Dibromoelhane (EDB) ND 1.3 Dibromomethane ND 1.3 12-Dichlorobenzene ND 1.3 13-Dichlorobenzene ND 1.3 1,4-Dichlorobenzene ND 1.3 Dichloroditluonmtethanc ND 1.3 1. 1 -Dichloroethane ND 1.3 " 1,2-Dichloroethene ND 1.3 1, 1 -Dichloroethene ND 1.3 cis- 1.2-Dich loroethene ND 1.3 trans-1,2-Dichloroethene ND 13 12-Dichloropropane ND 1.3 1,3-Dichloropropane ND 1.3 2,2-Dichloropropane ND 1.3 I,I-Dichloropropene ND 1.3 cis- 1 .3 -Dichloropropene ND 1.3 trans-1,3-Dichloropropene ND 1.3 Ethylbenzenc ND 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples Sample ID : Bin 20339-C Sampled : 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.3 mg/kg 1000 BIE0697 05/25/21 17:05 EPA8200B 4-Isopropyl Toluene ND 1.3 Isopropylbenzene ND 1.3 " Methylene chloride ND 1.3 " Naphthalene ND 1.3 " n-Propylbenzene ND 1.3 " Styrene ND 1.3 " 1.1,12-Tetrachloroethane ND 1.3 1,1,2,2-Tetrachloroethane ND 1.3 " Tctrachloroethanc (PCE) ND 1.3 " Toluene ND 1.3 1,2,3-Trichlorobenzene ND 1.3 1,2,4-Trichlorobenzene ND 1.3 1, 1, 1 -Trichloroethane ND 1.3 1,1,2-Trichloroethane ND 1.3 " Trichloroethene (TCE) ND 1.3 Trichlorofluoromethane ND 1.3 " 1,23-Trichloropropane ND 1.3 " 1,2,4-Triinethylbenzene ND 1.3 " 13.5-Trimethylbenzene ND 1.3 " Vinyl chloride ND 1.3 " Xylencs (total) ND 1.3 " Surrogate: Dihromofluoromethane 102 %, (74 - 122 ) Surrogate: Toluene-c18 102 % ( 65 - 128) Surrogate: 4-Bromo1laorohen_ene 98 % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA 1llercury 0.23 0.093 mg!kg 1 B 1 F0694 05/25/21 14:14 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BIE0693 05/25/2114:37 EPA6010B Arsenic 4.9 2.0 " Barium 230 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 150 0.50 N-02, N-03 Cobalt 25 0.50 Copper 49 0.99 " Lead 41 0.50 Alolvbdenum 0.69 0.50 Nickel 190 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 60 2.0 Zinc 82 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B1 F0794 05/27/21 19:28 EPA 1311/EPA 6010B Volatile Organic TPH by GC/FID TPE1 Gasoline (C5-CE2) 1.5 0.50 mg/kg 1 B I E0737 05/26/21 20:45 EPA 8015M D-04 Surrogate: 4-Bromo/htoroben_ene 115 '%, (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 370 10 mglkg 1 B l E0696 05/25/21 14:49 EPA 8015M TPH Motor Oil (('23-C40) ND 50 " Surrogate: o-Teiphenrl 102 °o (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 24 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples I Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B1E0697 05/25/21 17:33 EPA8260B Bromobenzene ND 1.2 Broniochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND t.2 sec-Butylbenzene ND 12 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chlorometliane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibronio-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichloroditluormnelhane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis- 1.2-Diehl oroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropane ND 1.2 cis-1.3-Dichloropropenc ND 1.2 trans-1,3-Dichloropropenc ND 1.2 Ethylbcnzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mgtkg 1000 BIE0697 05/25/21 17:33 EPA8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 - Naphthalene 2.8 1.2 n-Propylbcnzene ND 1.2 Styrene ND 1.2 _ 1,1,1,2-Tetrachloroethane ND 1.2 1,1,2.2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 " Toluene ND 1.2 " 1,23-Trichlorobenzene ND L2 " 1,2.4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 "Trichlorolluoromcthane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimcthylbcn7cnc ND 1.2 1,3,5-Trimethylbenzene ND 1,2 Vinyl chloride ND 1.2 " Xylenes(total) ND 1.2 Surrogate: Uibromolluoromethaiie 99 1"" (74 - 122 ) 11 Surrogate: 7oluene-d8 102'/n (65 - 128) " Srn•rogatc: 4-Bromo/hrorohen_cne 96 % ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 57 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 lenort fc Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Nol.$ Total Metals by CVAA Mercury 0.19 0.093 mglkg 1 Bl E0694 05/25/21 14:16 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I E0693 05/25/21 14:40 EPA 6010B Arsenic 4.6 2.0 Barium 180 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 150 0.49 Cobalt 19 0.49 Copper 40 0.99 Lead 24 0.49 " Molybdenum ND 0.49 Nickel 150 0.49 " Selenium ND 2.0 " Silver ND 0.49 Thallium ND 0.99 Vanadium 50 2.0 " Line 77 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B1E0794 05/27/21 19:30 EPA 1311/EPA6010B N-02, N-03 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 2.2 0.50 mg/kg 1 BIE0737 05/26/21 21:36 EPA 8015M D-04 Surrogate. 4-Bromo/luoroben_ene 108 (39 - 157) 11" " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 320 9.9 mg/kg 1 Bl E0696 05/25/21 15:12 EPA 9015M TPH Motor Oil (C23-C40) ND 50 Surrogate: o-TeiphenYl 95 `/, (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 57 -, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg'kg 1000 B 1 E0697 05/25/21 18:00 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 " Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 " Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Clrlorotohiene ND 1.2 4-C'hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,24Dibronioethane (EDB) ND 1.2 Dibromomethane ND 1.2 " 1.2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobenzenc ND 1.2 1,4-Dichlorobenzenc ND 1.2 Dichlorodilluoromcthane ND 1.2 I,1-Dichloroethane ND 1.2 " 1.2-Dichloroethane ND 1.2 " 13-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-I.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 29 of 57 :0: E C Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Sample ID: Bin 20144-B Matrix: Solid Lab ID: 2103212-07 Analyte Oilfield Environmental & Compliance, Inc. Project: Pacific Petroleum Project Number: NHC SLO, 2640 Broad Street Project Manager: Clarence Reynolds Result RL Units Dilution Batch Volatile Organic Compounds by GC/MS (Continued) WO & Reported: 2103212 05/28/2021 10:05 Sampled: 05/24/21 11:50 Sampled by : Clarence Reynolds Field Data: NA Analyzed Method Notes I lexachlombutadiene ND 1.2 mg/kg 1000 B I F0697 05/25/21 18:00 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene 2.3 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 " „ 1,1,1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 . Tetrachloroethene (PCE) ND 1.2 " Toluene ND 1.2 " 1,2,3-Trichlorobenzene ND 1.2 " 1,2.4-Trichlorobenzene ND 1.2 " 1, 1. 1 -Trichloroethane ND L2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 - - 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimcthylbenzene ND 1.2 " 1,3,5-Trimethylbenzene ND 1.2 " „ Vinyl chloride ND 1.2 " Xylenes (total) ND 1.2 Surrogate: Dihroinglhroroniethane 100 44, ( 74, 122) " Surrogate: T,lurnc-d8 102 (' 65 - 128) " " Surrogate: 4-Bromq/lrmroben=ene 98 % (75 - 1 21) ' R-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical t Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mglkg 1 B 1 E0694 05/25/21 14:18 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mgfkg I B I E0693 05/25/21 14:42 EPA 601 OB Arsenic 5.0 2.0 Barium 140 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 " " N-02, N-03 Cobalt 23 0.49 Copper 45 0.98 Lead 14 0.49 Molybdenum ND 0.49 Nickel 190 0.49 Selenium ND 2.0 " Silver ND 0.49 Thallium ND 0.98 Vanadium 50 2.0 Zinc 71 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B 1 E0794 05/27/21 19:40 EPA 1311 /EPA OOI OB Volatile Organic TPH by GOOD Tpli Gasoline (C'5-('12) 2.1 0.49 mg/kg 1 BIE0737 05/26/21 22:28 EPA 8015M D-04 Surrogate. 4-Bronm/luoroben_cne 119`ib (39-157) 11 11 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 560 10 mg!kg I Bl F0696 05/25/21 14:26 EPA 8015M TPII Motor Oil (C23-C40) ND 50 Surrogate: o-kiphenrl l30 % (65 - 136) " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mgIg 1000 Bl E0697 05/25/21 18:28 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Broniofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chlorocthanc ND 1.2 Chlorofonn ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 " " 1.2-Dibromo-3-chloropropane ND L2 1,2-1)ibromoethane (FDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobcnzenc ND 1.2 " IA-Dichlorobcnzenc ND 1.2 Dichlorodilluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 13-Dichloroethene ND 12 cis-L2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 " " 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 " cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropane ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by : Clarence Reynolds Lab ID: 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlombutadiene ND 1.2 mg/kg 1000 BIE0697 05/25/21 18:28 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 -• Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1.1,2-Tetrachloroethane ND 1.2 1.1.2.2-Tetrachloroethane ND 1.2 Tetrachlorocthane (PCE) ND 1.2 T010.C11C ND 1.2 1,2,3-Trich1orobcnzcnc ND 1.2 " 1,24-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1.2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 • 1.2.3-Trichloropropane ND 1.2 " 1,2.4-Trimethylbenzene ND 1.2 " 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dihromolhrormnethanr 99 Y (74 - 122 ) Surrogate: Toluene-dX 101 %/ (65 - 12S) " Surrogate: 4-Bronm/luorohen_ene 96 % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 1805) 925-3376 Page 34 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Metals by CVAA - Quality ControlTotal Analyte Result RL Units Spike Source %REC %REC RPD RPD �te Level Result Limits Limit Batch BlE0694 - EPA 7471A Preparation: EPA 7471A Prep 05/25/21 07:50 --. Blank (B1E0694-BLKI) Analyzed: 05/25/21 13:31 Mercury ND 0.10 mg/kg LCS (BlE0694-BSI) Analyzed: 05/25/21 13:27 Mercury 0.940 0.10 mg/kg 0.833 101 85-115 LCS Dup (BlE0694-BSDI) Analyzed: 05/25/21 13:29 Mercury 0.849 0.10 mg/kg 0.833 102 85-115 1 20 Duplicate (BlE0694-DUP1) Source: 2103193-05 Analyzed: 05/25/21 13:47 Mercury 0.216 0.18 mg/kg 1.87 159 20 QR-04 Matrix Spike (B1E0694-MS1) Source: 2103193-05 Analyzed: 05/25/21 13:51 Mercury 1.04 0.093 mg/kg 0.776 1.87 NR 75-125 QD1-07 Matrix Spike Dup (BlE0694-MSDI) Source: 2103193-05 Analyzed: 05/25/21 13:53 Mercury 1.68 0.090 mg/kg 0.751 1.87 NR 75-125 47 20 QM-07, QR-04 Post Spike (B1E0694-PS1) Source: 2103193-02 Analyzed: 05/25/21 15:19 Mercury 5.28 ug/L 5.00 0.114 103 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Blank (BlE0693-BLK1) Analyzed: 05/25/21 14:02 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1.0 " Lead ND 0.50 Molybdenum ND 0.50 " ^' Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 Thallium ND 1.0 " Vanadium ND 2.0 " Zinc ND 2.0 " LCS (B1E0693-BS1) Analyzed: 05/25/21 14:45 Antimony 99.7 2.5 mg,kg 100 100 80-120 Arsenic 99.6 2.0 100 100 80-I20 Barium 102 LO 100 102 80-120 Beryllium 98.2 0.50 100 98 80-120 Cadmium 100 0.25 100 100 80-120 Chromium 99.5 0.50 100 100 80-120 Cobalt 101 0.50 100 101 80-120 Copper 101 1.0 100 101 80-120 Lcad 102 0.50 100 102 80-120 Molybdenum 97.8 0.50 100 98 80-120 Nickel 101 0.50 100 101 80-120 Selenium 99.0 2.0 100 99 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 1.0 100 102 80-120 Vanadium 97.6 2.0 100 98 80-120 Zinc 100 2.0 100 100 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 03212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 LCS Dup (BlE0693-BSDI) Analyzed: 05/25/21 14:47 Antimony 100 2.5 mg/kg 100 100 80-120 0.5 20 Arsenic 99.7 2.0 100 100 80-120 0.1 20 Barium 101 LO 100 101 80-120 0.05 20 Beryllium 98.5 0.50 100 98 80-120 0.3 20 Cadmium 100 0.25 100 100 80-120 0.2 20 Chromium 99.4 0.50 100 99 80-120 0.2 20 Cobalt 101 0.50 100 101 80-120 0.05 20 Cropper 100 1.0 100 100 80-120 0.2 20 Lead 102 0.50 100 102 80-120 0.1 20 Molybdenum 98.4 0.50 100 98 80-120 0.0 20 Nickel 102 0.50 100 102 80-120 0.1 20 Selenium 100 2.0 100 l00 80-120 1 20 Silver 4.96 0.50 5.00 99 80-120 0 20 Thallium 102 1.0 100 102 80-120 0.4 20 Vanadium 97.0 2.0 100 97 80-120 0.7 20 Zinc 100 2.0 100 100 80-120 0.2 20 Duplicate (BlE0693-DUPl) Source: 2103212-05 Analyzed: 05/25/21 14:15 Antimony ND 2.4 mg/kg ND 20 Arsenic 5.18 1.9 6.10 16 20 Barium 205 0.97 218 6 20 Beryllium 0.408 0.49 0.435 6 20 Cadmium ND 0.24 ND 20 Chromium 154 0.49 " 144 7 20 Cobalt 22.3 0.49 20.9 6 20 Copper 48.8 0.97 46.3 5 20 Lead 17.9 0.49 19.3 8 20 Molybdenum 0.510 0.49 0.574 12 20 Nickel 196 0.49 179 9 20 Selenium ND L9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 52.3 1.9 54.0 3 20 Zinc 69.6 1.9 87.4 23 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 _ www.oecusa.com FAX: 805 925-3376 Page 37 of 57 a A 6l, aL. a Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 'Votat Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 -. Matrix Spike (B1E0693-MS1) Source: 2103212-05 Analyzed: 05/25/21 13:50 Antimony 13.1 2.4 mg/kg 97.9 ND 13 10-116 Arsenic 101 2.0 97.9 6.10 96 77-121 Barium 226 0.98 97.9 218 8 30-169 Qt11-07 Beryllium 95.2 0.49 97.9 0.435 97 96-111 Cadmium 90.0 0.24 97.9 ND 92 81-112 Chromium 218 0.49 97.9 144 76 75-129 _ Cobalt 109 0.49 97.9 20.9 90 71-121 Copper 146 0.98 97.9 46.3 102 68-135 Lead 107 0.49 97.9 19.3 90 72-121 Molybdenum 35.0 0.49 97.9 0.574 35 70-112 Q.11-07 Nickel 230 0.49 97.9 179 52 73-121 Q11-07 Selenium 85.9 2.0 97.9 ND 88 76-116 Silver 4.79 0.49 4.90 ND 98 54-132 Thallium 85.9 0.98 97.9 ND 88 64-120 Vanadium 138 2.0 97.9 54.0 86 78-124 Zinc 162 2.0 97.9 87.4 77 50-143 Matrix Spike Dup (B1E0693-MSD1) Source: 2103212-05 Analyzed: 05/25/21 13:52 Antimony 9.34 2.4 mg,kg 95.8 ND 10 10-116 33 20 QR-02 Arsenic 96.6 1.9 95.8 6.10 95 77-121 4 20 Barium 295 0.96 95.8 218 80 30-169 26 20 QR-02 Beryllium 91.2 0.48 95.8 0.435 95 86-I11 4 20 Cadmium 95.1 0.24 95.8 ND 89 81-112 6 20 Chromium 271 0.48 95.8 144 133 75-129 22 20 QD1-07, QR-04 Cobalt 113 0.48 95.8 20.9 96 71-121 3 20 Copper 140 0.96 95.8 46.3 97 68-135 4 20 Lead 104 0.48 95.8 19.3 88 72-121 3 20 Molybdenum 32.4 0.48 95.8 0.574 33 70-112 8 20 QM-07 Nickel 319 0.48 95.8 179 146 73-121 32 20 Q11-07, QR-04 Selenium 79.5 1.9 95.8 ND 83 76-116 8 20 Silver 4.59 0.48 4.79 ND 96 54-132 4 20 Thallium 79.5 0.96 95.8 ND 83 64-120 8 20 Vanadium 147 1.9 95.8 54.0 97 78-124 6 20 Zinc 158 1.9 95.8 87.4 74 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 ..ww.oecusa.com FAX: 805 925-3376 Page 38 of 57 rob TAZ rQ Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Totalby Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Post Spike (BlE0693-PSI) Source: 2103212-05 Analyzed: 05/25/21 14:08 Antimony 1.98 mg/l. 2.00 0.00347 99 75-125 Arsenic 2.07 2.00 0.121 98 75-125 Barium 6.39 2.00 4.34 103 75-125 Beryllium 1.96 2.00 0.00863 98 75-125 Cadmium 1.83 2.00-0.0417 91 75-125 Chromium 4.75 2.00 2.85 95 75-125 Cobalt 2.27 2.00 0.414 93 75-125 Copper 2.88 2.00 0.919 98 75-125 Lead 2.24 2.00 0.384 93 75-125 Molybdenum 1.97 2.00 0.0114 98 75-125 Nickel 5.42 2.00 3.56 93 75-125 Selenium 1.80 2.00 -0.120 90 75-125 Silver 0.0954 0.100-0.00119 95 75-125 Thallium 1.78 2.00-0.0164 89 75-125 Vanadium 3.01 2.00 1.07 97 75-125 Zinc 3.61 2.00 1.74 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 39 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0794 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 05/27/21 10:55 Blank (B1E0794-BLK1) Analyzed: 05/27/21 18:35 Chromium ND 0.050 mg/L LCS (B1E0794-BSI) Analyzed: 05/27/21 18:20 Chromium 10.0 0.050 mg/L 10.0 LCS Dup (BlE0794-BSD1) Analyzed: 05/27/21 18:22 Chromium 9.84 0.050 mg/L 10.0 Duplicate (BlE0794-DUP1) Source: 2102854-01 Analyzed: 05/27/21 18:52 Chromitnn ND 0.050 mg/L Leach Fluid Blank (BlE0794-LBKI) Analyzed: 05/27/21 18:37 Chromium ND 0.050 mg/l. Leach Fluid Blank (BlE0794-LBK2) Analyzed: 05/27/21 18:40 Chromium ND 0.050 mg/L Leach Fluid Blank (B I E0794-LBK3) Analyzed: 05/27/21 18:42 Chromium ND 0.050 mg/L Matrix Spike (BlE0794-MSI) Source: 2102854-01 Analyzed: 05/27/21 18:25 Chromium 10.2 0.050 mg/L 10.0 Matrix Spike Dup (B1E0794-MSD1) Source: 2102854-01 Analyzed: 05/27/21 18:45 Chromium 10.2 0.050 mg/l. 10.0 100 80-120 98 80-120 2 20 ND 20 ND 102 82-119 ND 102 82-119 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic TPH by 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0737 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/26/21 06:59 �- Blank (B1EO737-BLKI) Analyzed: 05/26/21 10:49 TPH Gasoline (C5-02) ND 0.50 mg'Ig Surrogate:4-Bromn/luorobcnccne 0.128 110.125 102 39-157 LCS (BlE0737-BS1) Analyzed: 05/26/21 09:57 TPH Gasoline (C5-('12) 1.08 0.50 mgrkg 0.994 108 68-139 Surrogate. 4-BromoJluorohen_cne 0.146 110.124 117 39-157 • LCS Dup (BlE0737-BSDI) Analyzed: 05/26/21 10:23 TPH Gasoline (C5-C12) 1.20 0.50 mg/kg 0.998 120 68-139 11 20 .Surrogate:4-Bronmflaorobenzene 0.154 110.125 123 39-157 ---- Duplicate (B1E0737-DUPI) Source: 2103210-01RE1 Analyzed: 05/26/21 13:04 TPH Gasoline (C5-C 12) ND 0.49 mg/kg ND 20 Surrogate:4-Bromgfluorohenzene 0.120 110.122 99 39-157 Matrix Spike (BlE0737-MS1) Source: 2103210-01RE1 Analyzed: 05/26/21 23:45 TPH Gasoline (C5-C12) 0.868 0.48 mg/kg 0.967 ND 90 10-171 Surrogatc:4-Bromofluorabcn_ertc 0-142 110.121 117 39-157 Matrix Spike Dup (BlE0737-MSD1) Source: 2103210-01RE1 Analyzed: 05/27/21 00:11 TPH Gasoline (('5-02) 0.911 0.50 mg/kg 0.998 ND 91 10-171 5 20 Surrogate: 4-Br n iqf tombeu_ene 0.149 110.125 119 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 41 of 57 rA .61. W..49 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Semi -Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0696 - EPA 8015M Preparation: EPA 3550C 05/25/21 08:55 -- Blank (BlE0696-BLKI) Analyzed: 05/25/21 13:41 TPH Diesel (C13-('22) ND Ill mg/kg TPH Motor Oil (C23-C'40) ND 50 11 Surrogate: o-Terphe» t1 43.3 " 50.0 87 65-136 LCS (BlE0696-BS1) Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22) 512 10 mg/kg 499 103 72-115 TPH Motor Oil (('23-('40) 473 50 499 95 74-126 Stn•rugate: o-Terphen)°l 49.9 49.9 100 65-136 LCS Dup (BlE0696-BSD1) Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22) 487 10 mg/kg 500 97 72-115 5 20 TPII Motor Oil (C23-C40) 459 50 500 92 74-126 3 20 Surrogate: o4iclphcn.vl 48.7 50.0 97 65-136 Duplicate (BlE0696-DUPl) Source: 2103212-01 Analyzed: 05/25/21 14:03 TPH Diesel (Cl3-C22) 35.5 9.9 mg/kg 50.9 36 20 QR-06 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-T rphenyl 42.6 49.7 86 65-136 Matrix Spike (B1E0696-MS1) Source: 2103212-01 Analyzed: 05/25/21 12:55 TPH Diesel (( 13-('22) 500 10 mg/kg 498 50.9 90 46-147 TPH Motor Oil (('23-C40) 432 50 498 ND 87 35-171 Surrogate: o-Terpheml 44.5 49.8 89 65-136 Matrix Spike Dup (B1E0696-MSD1) Source: 2103212-01 Analyzed: 05/25/21 13:18 TPH Diesel (('13-C22) 497 9.9 mg/kg 497 50.9 90 46-147 0.6 20 TPH Motor Oil (('23-('40) 432 50 497 ND 87 35-171 0.2 20 Surrogate: o-TerpheaYl 44.3 49.7 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by GUMS - Quality Control =lyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1) Analyzed: 05/25/21 13:26 Benzene ND 0.25 mg/kg Bromobenzene ND 0.25 Bromochloromcthane ND 0.25 Bromodichloromethane ND 0.25 Bromoform ND 0.25 " Bromomelhane ND 0.25 n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 Chlorobenzene ND 0.25 " Chloroethane ND 0.25 " Chloroform ND 0.25 " Chloromethane ND 0.25 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene ND 0.25 Dibromochloromethane ND 0.25 1,2-Dibromo-3-chloropropane ND 0.25 " 1,2-Dibromoethane (EDB) ND 0.25 " Dibronxnncthane ND 0.25 1,2-Dichlorobenzene ND 0.25 1,3-Dichloroben7ene ND 0.25 IA-Dichlorobenzene ND 0.25 " Dichlorodifluoromethane ND 0.25 I,1-Dichloroethane ND 0.25 " 1,2-Dichloroethane ND 0.25 " 1,1-Dichloroethene ND 0.25 " cis- 1.2-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 " 1,2-Dichloropropane ND 0.25 1,3-Dichloropropane ND 0.25 2,2-Dichloropropane ND 0.25 " I,l-Dichloropropene ND 0.25 cis-1.3-Dichloropropene ND 0.25 trans-1,3-Dichloropropene ND 0.25 " Etylbenzene ND 0.25 " Ilexachlorobutadiene ND 0.25 " 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 Methylene chloride ND 0.25 Naphthalene ND 0.25 n-Propylbenzene ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet pt by Control Analyze Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1) Analyzed: 05/25/21 13:26 Styrene ND 0.25 mg/kg 1,1,1,2-Tetrachloroethane ND 0.25 " 1,1,2.2-Tetrachloroethane ND 0.25 Tetrachloroethane (PCE) ND 0.25 " Toluene ND 0.25 " 1.23-Trichlorobenzene ND 0.25 " 1,2,4-1'richlorobenzene ND 0.25 " 1, 1, 1 -Trich loroethane ND 0.25 " 1, 1 .2-Trichloroethane ND 0.25 " Trichloroethane (TCE) ND 0.25 " Trichlorolluorontethane ND 0.25 1,2,3-Trichloropropane ND 0,25 1,2.4-Trim ethyl benzene ND 0.25 " 1,3,5-Trimethylhen7ene ND 0.25 Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 " Surrogate: Dihrornnfluoromethane 0.0496 0.0500 99 74-122 Surrogate: Toluene-dR 0.0507 0.0500 101 65-128 Sarrogate:4-Bromo/luorohenzene 0.0482 0.0500 96 7.5-121 LCS (BlE0697-BSI) Analyzed: 05/25/21 11:37 Benzene 1.80 0.25 mg/kg 1.98 91 70-131 Bromobenzene 2.09 0.25 1.98 105 74-130 Bromochloromethane 1.77 0.25 1.98 89 64-133 Bromodichloronnethane 2.12 0.25 1.98 107 69-137 Bromofor"t 2.09 0.25 1.98 105 55-132 Bromomethane 1.51 0.25 1.98 Ili 10-142 n-Butylbenzene 2.47 0.25 1.98 125 64-156 sec-Butylbenzene 2.46 0.25 1.99 124 75-155 tert-Butylbenzene 2.34 0.25 1.98 Its 74-144 Carbon tetrachloride 1.70 0.25 1.99 86 67-135 Clilorobenzene 2.08 0.25 1.98 105 73-134 Chloroethane 1.65 0.25 1.98 83 10-167 Chloroform 2.01 0.25 1.98 MI 69-124 Chloromethane 2.46 0.25 1.98 124 34-136 2-Chlorotoluene 2.16 0.25 1.98 109 75-135 4-Chlorotoluene 2.30 0.25 1.98 116 70-138 Dibromochloromethane 2.01 0.25 1.98 102 67-135 1.2-Dibronto-3-chloropropanc 2.45 0.25 1.98 124 41-149 1,2-Dibromoethane (EDB) 1.98 0.25 1.98 100 68-131 Dibromomethane 1.92 0.25 1.98 97 61-140 1,2-Dichlorobenzene 2.20 0.25 1.98 111 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 44 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilept Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS (BlE0697-BSI) Analyzed: 05/25/21 11:37 1,3-Dichlorobenzenc 2.30 0.25 mglkg 1.98 116 76-138 1,4-Dichlorobenzene 2.23 0.25 1.98 112 72-132 Dichlorodifluorontethanc 1.51 0.25 1.98 76 10-155 1, 1 -Dichloroethanc 1.90 0.25 1.98 96 63-139 1,2-Dichloroethanc 2.04 0.25 1.98 103 64-126 1,1-Dichloroethene 1.79 0.25 1.98 90 52-167 cis-1,2-Dichloroethene 1.94 0.25 1.98 93 70-135 trans-1,2-Dichloroethene 1.69 0.25 1.98 85 67-147 1,2-Dichloropropaue 3.19 0.25 1.98 161 68-131 QNI-08 1,3-Dichloropropaue 1.91 0.25 1.99 96 64-129 2,2-Dichloropropaue 2.11 0.25 1.98 107 63-154 1.1-Dichloropropene 1.82 0.25 1.98 92 68-138 cis-13-Dichloropropene 2.08 0.25 1.98 105 72-134 trans-1,3-Dichloropropene 2.10 0.25 1.98 109 69-132 Ethvlbenzene 1.92 0.25 1.98 97 68-136 1lexaclhlorobutadiene 2.24 0.25 1.98 113 72-198 4-Isopropyl Toluene 2.40 0.25 1.98 121 74-150 Isopropylbenzene 2.21 0.25 1.98 112 71-149 Methylene chloride 1.81 0.25 1.98 91 51-127 Naphthalene 2.29 0.25 1.98 116 57-158 n-Propylbenzene 2.29 0.25 1.98 116 70-143 Styrene 2.47 0.25 1.98 124 68-138 1, 1, 1,2-Tetrachloroethane 2.10 0.25 1.98 106 76-130 1,1,2,2=1'ctrachloroethanc 2.18 0.25 1.98 110 60-136 Tetrachloroethene (PCE) 1.79 0.25 1.99 91 73-138 Toluene 1.99 0.25 198 101 72-128 1,2,3-Triclilorobenzene 2.47 0.25 1.99 125 61-166 1,24-Trichlorobenzene 2.43 0.25 1.98 123 71-158 1, 1, 1 -Trichloroethane 1.92 0.25 1.98 97 71-135 1,1,2-Trichloroethane 2.23 0.25 1.98 113 64-132 Trichloroethene(TCE) 1.87 0.25 1.98 94 74-139 Trichlorofluoromethane 2.69 0.25 1.98 136 30-156 1,2,3-Trichloropropane 2.05 0.25 1.98 104 67-123 1,2,4-Trimethylbenzene 2.31 0.25 1.98 117 68-134 1,3,5-Trimethylbenzene 2.27 0.25 1.98 114 71-140 Vinyl chloride 2.14 0.25 1.98 108 43-144 Xylenes (total) 6.81 0.25 5.94 115 69-138 Surrogate: Dihrunuilluoruntethrrnc 0.0512 0.0495 103 74-122 Surrogate: Toluene-da 0.11516 0.0495 104 05-128 Surrogatrc 4-Bramo/luorohen_enc 0.0467 0.0495 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: t,8051925-3376 Page 45 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by GC/MS - Quality Control knalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSDI) Analyzed: 05/25/21 12:04 Benzene 1.74 0.25 mg!kg 1.99 87 70-131 3 20 Bromobenzene 2.08 0.25 1.99 104 74-130 0.4 20 Bmmochloromcthanc 1.69 0.25 1,99 85 64-133 5 20 Bromodichloromethane 2.14 0.25 1.99 107 69-137 0.9 20 Bromofonn 2.06 0.25 1.99 103 55-132 1 20 Bromomethane 1.50 0.25 1.99 75 10-142 1 20 n-Butylbenzene 2.33 0.25 1.99 117 64-156 6 20 ^ sec-Butylbenzene 2.25 0.25 1.99 113 75-155 9 20 tert-Butylbenzene 2.17 0.25 1.99 109 74-144 8 20 Carbon tetrachloride 1.60 0.25 1.99 80 67-135 6 20 -� Chlorobenzene 2.07 0.25 1.99 104 73-134 0.3 20 Chloroethane 1.70 0.25 1,99 85 10-167 3 ' 20 Chloroform 1.93 0.25 L99 97 69-124 4 20 Chloromethane 2.16 0.25 1.99 108 34-136 13 20 2-Chlorotoluene 2.05 0.25 1.99 103 75-135 5 20 4-Chlorotoluene 2.15 0.25 1.99 108 70-138 7 20 Dibromochloromethanc 2.11 0.25 1.99 106 67-135 5 20 _ 1,2-Dibromo-3-chloropropane 2.68 0.25 1.99 135 41-149 9 20 1,2-Dibromoethane (EDB) 2.01 0.25 1.99 101 68-131 1 20 Dibromomcthanc 1.92 0.25 1.99 96 61-140 0.08 20 1,2-Dichlorobenzene 2.20 0.25 1.99 110 76-136 0.4 20 l,3-Dichlorobenzene 2.15 0.25 1.99 108 76-138 7 20 IA-Dichlorobenzene 2.13 0.25 1.99 107 72-132 5 20 Dichlorodifluoromcthane 1.50 0.25 1.99 75 10-155 0.5 20 1,1-Dichloroethene 1.83 0.25 1,99 92 63-139 4 20 1,2-Dichlorocthanc 2.01 0.25 1.99 101 64-126 2 20 1,1-Dichloroethene 1.73 0.25 1.99 87 52-167 4 20 cis-1.2-Dichloroethene 1.71 0.25 1.99 86 70-135 8 20 trans- l,2-Dichloroethene 1.64 0.25 1.99 82 67-147 3 20 1.2-Dichloropropane 1.94 0.25 1.99 97 68-131 49 20 QR-04 13-Dichloropropane 2.05 0.25 1.99 103 64-128 7 20 2.2-Dichloropropane 2.00 0.25 1.99 100 63-154 5 20 - ' 1, 1 -Dichloropropene 1.75 0.25 1.99 88 68-138 4 20 cis- I .3-Dichloropropene 1.98 0.25 1.99 100 72-134 5 20 trans-1,3-Dichloropropene 2.25 0.25 1.99 113 69-132 4 20 E.thylbenzene 2.05 0.25 1.99 103 68-136 7 20 11exachlorobutadiene 2.12 0.25 1.99 107 72-198 5 20 4-Isopropyl Toluene 2.23 0.25 1.99 112 74-150 7 20 Isopropylbenzene 2.24 0.25 1.99 112 71-149 1 20 Methylene chloride 1.79 0.25 1.99 90 51-127 I 20 Naphthalene 2.10 0.25 1.99 106 57-158 8 20 n-Propylbenzene 2.12 0.25 1.99 106 70-143 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 46 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (BlE0697-BSD1) Analyzed: 05/25/21 12:04 Styrene 2.23 0.25 mg/kg 1.99 112 68-138 10 20 1,1,1,2-Tetrachloroethane 2.18 0.25 1.99 109 76-130 3 20 1.1,12-Tetrachlorocthanc 2.11 0.25 1.99 106 60-136 3 20 - Tetrachloroethene (PCE) 1.81 0.25 1.99 91 73-138 0.8 20 Toluene 1.83 0.25 1.99 92 72-128 9 20 1,2,3-Trichlorobenzene 2.32 0.25 1.99 116 61-166 6 20 1,2.4-Trichlorobenzene 2.35 0.25 1.99 118 71-158 3 20 1, 1, 1 -Trichloroethane 1.86 0.25 1.99 93 71-135 3 20 1,1,2-Trichloroethane 2.19 0.25 1.99 109 64-132 2 20 Trichloroethene (TCE) 1.82 0.25 1.99 91 74-139 3 20 - Trichlorofluoromethane 2.59 0.25 1.99 130 30-156 4 20 1,2,3-Trichloropropane 1.96 0.25 1.99 98 67-123 5 20 L2.4-Trimethylbenzene 2.16 0.25 1.99 108 68-134 7 20 1,3,5-Trimethylbenzene 2.13 0.25 1.99 107 71-140 6 20 Vinyl chloride 2.12 0.25 1.99 107 43-144 0.6 20 Xylenes (total) 6.17 0.25 5.98 103 69-138 10 20 Surrogate. DibromgJluoromcthitil(, 0.0512 0.0498 /03 74-122 Surrogate. Toluene-d8 0.0510 0.0498 102 65-128 Surrogate:4-Bromgfannhenrene 0.0499 0.0498 100 75-121 Duplicate (BlE0697-DUPl) Source: 2103210-01 Analyzed: 05/25/21 14:48 Benzene ND 1.2 mg/kg ND 20 Bromobenzene NI) 1.2 ND 20 Bromochloromcthane ND 1.2 ND 20 Bromodichloromethane NJ) 1.2 ND 20 Bromoform ND 1.2 NI) 20 Bromomethane ND 1.2 ND 20 n-Butylbenzene ND 12 ND 20 sec-Butylbenzene ND 1.2 ND 20 tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzene ND 1.2 ND 20 C'hloroethane NI) 1.2 ND 20 Chloroform ND 1.2 NI) 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 4-Chlorotoluene ND 1.2 ND 20 Dibromochloromethanc ND 1.2 ND 20 1,2-Dibromo-3-clhloropropanc ND 1.2 ND 20 1,2-Dibronioethane (EDB) ND 1.2 ND 20 Dibromomethanc ND 1.2 ND 20 1.2-Dichlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 _ _ www.oecusa.com FAX: (805) 925-3376 Page 47 of 57 661�N Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic CoinpoundsControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes _ Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 �. Duplicate (B1E0697-DUPl) Source: 2103210-01 Analyzed: 05/25/21 14:48 1,3-Dichlorobcnzenc ND 1.2 mgIg ND 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichlorodifluoromethane ND 1.2 ND 20 1,1-Dichloroethane ND 1.2 ND 20 1,2-Dichloroethane ND 1.2 ND 20 1,1-Dichloroethene ND 1.2 ND 20 cis-1,2-Dichloroethene ND 1.2 ND 20 trans-l.2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropane ND 1.2 ND 20 1,3-Dichloropropaue ND 1.2 ND 20 2,2-Dichloropropane ND 1.2 ND 20 1, 1 -Dichloropropene ND 1.2 ND 20 cis- 1,3-Dichloropropene ND 1.2 ND 20 trans-1,3-Dichloropropene ND 1.2 ND 20 Ethylbenzene ND 1.2 ND 20 Hexachlorobutadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 Isopropylbenzene ND 1.2 ND 20 Methylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 ND 20 n-Propylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1, 1, 1.2-Tetrachloroethane ND 1.2 ND 20 1,1,2,2-Tetrachlorocthanc ND 1.2 ND 20 Tetrachloroethene (PCE) ND 1.2 ND 20 Toluene ND 1.2 ND 20 1,2,3-Trichlorobenzene ND 1.2 ND 20 1,24-Trichlorobenzene ND 1.2 ND 20 _ 1, 1, 1 -Trichloroethane ND 1.2 ND 20 1,12-Trichloroethane ND 12 ND 20 Trichloroethene (TCE) ND 1.2 ND 20 Trichlorofluoromethanc ND 12 ND 20 1,2,3-Trichloropropane ND 1.2 ND 20 1,2,4-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 ND 20 Vinyl chloride ND 1.2 ND 20 Xylenes (total) ND 1.2 ND 20 Surrogate. Dibromollttoromethane 0.0503 0.0494 102 74-122 Surrogate:7oluene-dR 0.0514 0.0494 104 65-128 Surrogate:4-Bromofluorohenzene 0.0478 0.0494 97 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 48 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet pt by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (BlE0697-MS1) Source: 2103212-01 Analyzed: 05/25/21 19:22 Benzene 9.97 1.2 nrg/kg 9.94 ND 90 37-145 Bromobenzene 11.0 1.2 9.94 ND 111 29-147 Bromochloromcthanc 9.22 1.2 9.94 ND 93 40-145 Bromodichloromethane 10.9 1.2 9,94 ND 1I0 39-153 Bromoform 10.7 1.2 9.94 ND 108 32-143 Brornomethane 10.3 1.2 9.94 ND 104 10-141 n-Butylbenzene 11.6 1.2 9.94 ND 117 10-162 sec-Butylbenzene 12.2 1.2 9.94 ND 123 14-168 tert-Butylbenzene 11.9 1.2 9.94 ND 119 21-159 Carbon tetrachloride 8.48 1.2 9.94 ND 85 28-148 Chlorobenzene 10.9 1.2 9.94 ND I10 32-148 Chloroethane 12.6 1.2 9.94 ND 127 11-166 Chloroform 9.94 1.2 9.94 ND 100 40-139 Chloromethane 10.4 1.2 9.94 ND 105 18-135 2-Chlorotoluene 10.8 1.2 9.94 ND 108 25-151 4-Chlorotoluene 11.3 1.2 9.94 ND 114 22-150 Dibromoclrloromethane 10.2 1.2 9.94 ND 103 40-147 1,2-Dibronro-3-clrloropropane 124 1.2 9.94 ND 125 25-158 1,2-Dibromoethane (EDB) 10.1 1.2 9.94 ND 102 38-147 Dibronronrethane 9.74 1.2 9.94 ND 98 39-150 1.2-Dichlorobenzene 11.4 1.2 9.94 ND 115 24-154 1,3-Dichlorobenzene 11.3 1.2 9.94 ND 114 21-153 IA-Dichlorobenzene 10.9 1.2 9.94 ND 110 21-146 Dichloroditluoromethane 6.32 1.2 9.94 ND 64 10-149 I,1-Dichloroethane 9.32 1.2 9.94 ND 94 34-151 1,2-Dichlorocthanc 9.93 1.2 9.94 ND 100 40-137 1,1-Dichloroethene 7.41 1.2 9.94 ND 74 21-172 cis-1,2-Dichloroethene 8.87 1.2 9.94 ND 89 38-147 trans-1,2-Dichloroethene 8.06 1.2 9.94 ND 81 30-160 12-Dichloropropane 10.0 1.2 9.94 ND 101 39-146 1,3-Dichloropropane 9.84 1.2 9.94 ND 99 39-141 22-Dichloropropane 9.05 1.2 9.94 ND 91 26-149 1,1-Dichloropropene 9.03 1.2 9.94 ND 91 28-150 cis-1,3-Dichloropropene 9.92 1.2 9.94 ND 100 34-149 trans-1,3-Dichloropropene 11.0 1.2 9.94 ND 111 36-143 Bthylbenzene 10.8 1.2 9.94 ND 109 23-150 Hexachlorobutadiene 11.4 1.2 9.94 ND 115 10-192 4-isopropyl Toluene 11.9 1.2 9.94 ND 120 11-165 Isopropylbenzene 11.7 1.2 9.94 ND 118 17-166 Methylene chloride 8.61 1.2 9.94 ND 87 28-135 Naphthalene 12.4 1.2 9.94 ND 124 10-174 n-Propylbenzene 11.3 1.2 9.94 ND 114 16-156 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 57 ( M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by GUMS - Quality Control lAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1) Source: 2103212-01 Analyzed: 05/25/21 19:22 Styrene 11.5 1.2 mg/kg 9.94 ND 116 24-154 1,1,1,2-Tetrachloroethane 11.1 1.2 9.94 ND 111 38-149 1,1,2,2-7'etrachlorocthane 10.7 1.2 9.94 ND 107 22-164 Tetrachloroethenc WCE) 9.37 1.2 9.94 ND 94 25-153 Toluene 10.4 1.2 9.94 ND 105 26-149 1,2,3-Trichlorobenzene 12.7 1.2 9.94 ND 128 10-163 1,2,4-Trichlorobenzene 12.4 12 9.94 ND 124 10-162 1. 1. 1 -Trichloroethane 9.87 1.2 9.94 ND 99 34-149 1,1,2-Trichloroethane 11.3 1.2 9.94 ND 113 25-175 Trichloroethene (TCE) 9.24 1.2 9.94 ND 93 25-170 Trichlorofluoromethane 12.0 1.2 9.94 ND 121 19-155 1,2,3-Trichloropropane 9.81 1.2 9.94 ND 99 32-165 1,2,4-Trimethylbenzene 11.7 1.2 9.94 ND 118 15-150 1,3,5-Trimethyl benzene 11.4 1.2 9.94 ND 114 10-158 Vinyl chloride 11.2 1.2 9.94 ND 112 22-148 Xylenes (total) 32.3 1.2 29.8 ND 108 22-153 Surrogate: Dibronuil7uorunndhcme 0.0508 0.0497 102 74-122 Surrogate: Toluene-dN 0.0509 0.0497 102 65-128 Surrogate: 4-Bromolhiorohen-rene 0.0499 0.0497 100 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 ,?f 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Method Summary alysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 6010B TCLP Chromium EPA 13111EPA 601013 Water OEC. CA-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471A Solid OEC. CA-ELAP Total Metals by ICP 6010E Total Antimony EPA 601013 Solid OEC, CA-ELAP 6010E Total Arsenic EPA 6010E Solid OEC CA-ELAP 6010B Total Barium EPA 6010E Solid OEC, CA-ELAP 601013Total Beryllium EPA 6010B Solid OEC, CA-ELAP 601013 Total Cadmium EPA 6010E Solid OEC, CA-ELAP 6010B Total Chromium EPA 6010B Solid OEC, CA-ELAP 6010E Total Cobalt EPA 601013 Solid OEC, CA-ELAP 601013 Total Copper EPA 601013 Solid OEC, CA-ELAP 6010B Total Lead EPA 6010B Solid OEC. CA-ELAP 60111B Total Molybdenum EPA 6010E Solid OEC, CA-ELAP 6010E Total Nickel EPA 601013 Solid OEC, CA -FLAP 601013 Total Selenium EPA 601013 Solid OEC, CA -FLAP 6010B Total Silver EPA 01013 Solid OEC, CA-ELAP 601013 Total Thallium EPA 6010E Solid OEC, CA-ELAP 6010B Total Vanadium EPA 6010B Solid OEC. CA-ELAP 6010B Total Zinc EPA 6010B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 51 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Sample Method Summary t alysis Method Matrix Laboratory & Certification Volatile Organic Compounds by GUMS 8260B Full List EPA 8260E Solid OEC, CA -FLAP Volatile Organic TPH by GC/FID 8015 TPH-Gasoline r . 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasolinc 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 ITH-Gasoline 8015 TPII-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline E,PA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC_ Internal EPA 8015M Solid OEC, CA-E,LAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OEC. Internal EPA 8015M Solid OEC, CA-E.LAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 52 of 57 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (QuantitationLimit ) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for yuantitation. N-02 Analyte concentration below TTLC but above 1 Ox STLC. N-03 Analyte concentration above 20x TCLP. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery and'or RPD values. QM -OR The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC' data. QR-04 The RPD exceeded the QC control limits. QR-06 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to non -homogenous sample matrix. QC batch accepted based on LCS and/or LCSD recovery and'or RPD values. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out -Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: BO5 925-3376 Page 53 of 57 File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2612.D Operator RR Acquired 26 May 2021 1:56 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-01RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 12 Response 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOME2612.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 9C U .-I 0 m a, E-H O 4 1a +-I rn N tS LO U N XC W x b) o I~ OQ r / m U � Q N M l0 Ln O Ol N to L N O O [x� -1 CQ N rl (--) N N Q O O � N I / N 7 Ln r H ro rl N �1 a c7 0 U (N (\A r N .. .. .. .. .. .. .. a) S4 J-) r a) rM0-Q O a) i~ z C 4-) �4 �5 a)H (0_H FAr- (L) S4 71 +) 04 rl a) b, U) iz- m (0 -rl a, U E~ r0 -" •'-' GaO<HWX 0 0 0 0 0 0 N ai 0 0 a) 0 N co 0 0 00 0 l 0 0 0 (D O O CO O f N i O O v 0 0 o N _ co � o - o ai ` N h n r- n I-- � h O O O O O 0 O 0 O NI 0 0 o O 0 0 0 0 0 0 0 0 0 0 0 0 �, U)+ + + + + + + 0 0 O o 0 0 0 0 0 m a) m m a) d a) 0 0 0 O 0 O o O O O 0 O 0 O O o CD N V M N O O a) .- 0)LO 0) coO p- It a) 1- File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2614.D Operator RR Acquired 26 May 2021 3:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-02RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 14 r' Response_ 110000 105000 100000 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 GOME2614.D\FID1A 35000 30000 25000 20000 I 15000 10000 ` V4 5000 i Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 x U 0 x a H O Ca � LO M b LO U N FC W x ry) o ci PQ -rl / m U � W CC G N N l0 Lf) ,—I al N l0 Lf) M O O W rl (� N r (7) Q O O N I / N H ro IN aC SUM Ll a C7 0 L.n ••UN NrIM .. .. .. .. .. .. .. N �+ -P 1-= N I~ M OA o�rzrl� J-J i4 NH2 N i4 �l +) ¢ U .-1 N t5 m ) ro a� ro•H•� f=+OFCHv)X> 2 U m N 0 LL_ LO Cl) Lo N W CD O m f0 m In - 4)i O+ N t t t O O O O n (O Lf) M N O O O m o co 0 0 0 Ln LQ 0 0 0 of 0 0 of 0 Ln co 0 -O 00 0 0 0 co O O (O O LA LO O A LO 0 � v 0 z�f �— W) (vj o0 ri 5 �• LC) N O O N ' O Lq O O O LA jj O I O O O O O O coLOLLO � O(M N CD E H File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2616.D Operator RR Acquired 26 May 2021 4:26 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-03RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 16 Response 85001 80000 75000 70000 65000 60000. 55000! 500J 45000. 40000 35000 30000 25000 20000 15000 10000 GOME2616.D\FID1A 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 U r-i O a H 0 f� +-) N b" (n U N aG W o W -rl / m W � M 04 (n N-41 lfl N •• lD Ln rl O o W rl W N �u ? N -;T FC O O (N I / N �Ln rl E- i tl r N / (n C--)(n U N (N r N .. .. .. .. .. .. .. +-) N a (0 0 s� �4 (1)zw 0 (1) a � 4-) is N H r0 -ri }-I rl N i-I �l +) 04 U rl ri N t5' u� E m rtl U (6 -ri •rl F=4 0 " W U in N LL 04 LO N W O m fa _m N � n ti o 0 0 0 0 0 0 0 0 O O O O O O O O O O O O O 0 O O + + + + + + + O O O O O O O O O a) a) a) m (1) N a) O O O O O O O O O (O LO V m N O O O O O O 0 O O O O O O O O O O O O O W O a0 O O 00 O (O r O O O N O 0 (O I' N O O lCi 0 N v 0 0 v O (O ri O 0 N 0 O N O O 0 O O O File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2618.D Operator RR Acquired 26 May 2021 5:18 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-04RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 18 Response 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 G0ME2618.DT1D1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 U 0 x a H O Q � N M M iT �n U N a O / V1 W � N 6l l0 N •• � � N O O [x] N r (Y) >+ N uO Q O O N I / N >, Lo ri E ro -I N FCC £ U M G1 i-1 C7 0 /din Puri U N N r-i (M .. .. .. .. .. .. .. a) � 41 a) i~(a0Q �-+ a) z w I~ � F 4 a) H z a) �4 71 +-i ¢ U r-i a) to U) (a C=+OFCHU)X> U m N W M M O N W 2 O m 16 ✓T 0) 0 0 0 0 -o 0 of 0 0 0 O co 0 0 00 0 O o C. O 0 O 1 IIrF O r LO .. O O O O 0 O v J 0 3 � i O O O _ - O M A' o O N til O O N O O - F 1- r- r- r� 0 0 0 0 0 o O 0 0 a)� w o 0 0 00 0 0 0 00 O 0 0 0 0 c + + + + + + 0 o O o O O o o O o a) d d CD a) am O O o 0 0 0 0 0 0 a L c1 N a- O N O O Or O 0 O CD O O O O a) m OOD CD L 7 M N � O O File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2624.D Operator RR Acquired 26 May 2021 7:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-05RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 24 Response_ 85000 80000 75000, 70000, i 65000I 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOME2624.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 U 0 x a p O N b" G1 U M � LO C (N r W U) x 0 PO � / Q co N 6l tf) C 61 N •• � U N O O W PO N rl CJ >- N to Q O O N I / N F2� Ln -I E-i M -1 N Q 7tU7o UN NrIM .. .. .. .. .. .. .. N l-I a--) N r: N O �4'0 NZw 4O- 7 S 4 N H z N }-I 71 J--) ¢ U r1 rl N 01 U) rz fn m -rl Q U C (0"' ." f=+ 0 FCC -I U) 2 > 2 U Q LL 6 LO 0 N W O m m m ail n m o U) + O d O U1 N n 0 + n 0 + m n 0 + d M r- n 0 + N n 0 + n 0 + o 0 0 0 O O 0 0 0 0 O 00 0 0 0 0 O n 0 0 0 0 O CO 0 0 0 0 CD O LO 0 0 0 0 0 O V 0 0 0 0 O M 0 0 0 0 0 0 0 0 O O N 0 0 0 0 0 0 0 0 U� 00 0 0 00 0 I- 0 0 r` 0 0 co 0 0 to 0 0 0 0 v 0 0 0 ri File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2626.D Operator RR Acquired 26 May 2021 8:45 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-06RE1@ Misc Info : 1OBlEO737 GRO Solid Vial Number: 26 Response_ 90000, 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 350001 30000 25000 20000 15000 10000 5000 GOME2626.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 � � I V1 0.00 11.00 12.00 13.00 14.00 U -4 O x a F '0 O 4 +-) N b" G1 U M � N -r{ O OQ F� / Qi N N k-0 In Ol N•• � (n M O O W .-I W N NJ >i N l� NO / N >1 N -i E-H ro 1-1 N Ll �l C7 0 / in --i ( ) U N (Ij c M .. .. .. .. .. .. .. +-) N G ro O Q N Z O C � 4-) � � 0 Z ro-H �-1 -� N S4 ;� l) 04 U r r-I N (n (n ro �04U1-:ro-1-'1 44 0 FC H-i X > 0 0 0 0 0 0 of 0 0 0 co 0 0 00 0 1- 0 0 r- 0 (n 2 U 0 Q 0 co � o m LO (n N W � O O m O LO f6 C _m (n U) 3 0 o (h O O M O N O O N 0 O O O Uf 0 O r� O P� O O 0 0 O O O o O 0 O 0 O 0 O 0 O 0 O O r� r- 0 O 0 O + + a) + + N N + CD + N + + O N N O O O O O O O O O O O O O O O O O r(D 0N M N O O O O O O OOCl 0) OD r- (O In 7 M N of File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2628.D Operator RR Acquired 26 May 2021 9:36 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-07RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 28 Response_ 850001 80000 75000 70000 65000 60000 55000 50000` 450001 40000 35000 30000 25000' 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 GOME2628.D\FID1A IhJ 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 �G U rl O x a H O 4j H � r) b Ln U (N a W o � PU -� / m U � • C1� v) N k-0 Q0 Ln N 0� N •• � � N O O W H CQ N .-I c ) ,7 N 00 O O N I / N H H ro rI N FC U (1) G1 a tU o /min Horn UN (NrIN .. .. .. .. .. .. .. N �4 -) 1~ N �-: ro O A �4 iS NZw ro•H �4r N S4 �5+-) rl rI N i5 ro •rl Pa U G ro •� -ri G4 0 ltC M U ro N LL M N N W 2 O m f6 _O O O O O O O O O 00 O O M O 00 O O 00 O n O O O O �o O O LO LO f z I O 0 ~• v 0 LO M � o _ ri _ U� N O O N Il' to O O - O _In -0 n d n r r (q n U n y r r M r n d N r r r d r o o O T 0 0 O 000 0 0 O � 0 0 O f00 0 0 O � 0 0 O M 0 0 O N 0 0 O E 0 0 O V H File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2630.D Operator RR Acquired 26 May 2021 10:28 pm using AcgMethod GASBTEXE.M Instrument GC7 _ Sample Name: 2103212-08RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 30 Response_ 85000 80000 I 75000 70000 65000 60000 550001 i 50000 I 450001 40000 35000 30000 25000 20000 15000 10000 GOME2630.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 p 00 O U') rn O ro c� N lim 0 a n m 0 d H roc , « a = a .� m .m. io• t o m�W o ti Q i S splloS peAlosla mol I4lAlso.uo3 « « « O ❑ ❑ Z9o91 Mos 80d I7sad y. O' fa1gp7N81 p o OOLES-SOOAS J a m - y wq we O Wd`J dHl a CL o cc epUlnS l eplus6o enpaeea y !— .•. Z m y lsl I IIe3 909Z9 i� /t a{ / 7� o slsieW - ZZ eUll v a ¢ a _ d r a,�y m M y c �yy o m fY Q X. t m � Q� m i6 00 °O 91 v 4 _ E❑❑: r U °.o z w LO } :Q: caOo m C ~ i::�' 3 Z ❑ ❑ ❑ u N N m v •E: n g' • ❑ L = � L1 t� 10 f a V E y U Z .2 u w C d a N z m 'I �+ N Ch c _E C, 3 vy 'O % •o « E Cc CD C Ci p+, CT C '� ip O L o m Q ins 11 El L t t L C1 S C ... E ` ( - .Y C) Q N N E a O N C C a a°Ji >a a�i m m m V rig c� E= rx w v ►'- "' Z zm 3 y w . . 6. \ C14 § 0 Ln r- 0 k E � !IN » ) e k k ,I, - 0 } } 0 LD § $ \ CL = E )f ca / \ ƒfI \ $ f ) I ƒ L0 ■ O o 0 \/ $ ) $ 0 a k ) _ § ƒ / - \ 0 3) o £ o ■ 0 0 $ § k k k k � Ecm: top 0 / _ ) / j j § 7 k - ® § 0 «) $ § a 7 § _ k—«�/ \ o (D ©= 0 & 0 ) £ D = \ ° ®^ -j a)2 3 0 3 I - m = e § # 3 0- rL / d 0 0 0 \ y ƒ 2 < < ��� -5t /(D x04)° < ® 7) \ § C/ �}A+ / § ) C 2 , _ J = ��-, (D -0 \ E k $ § \ j ® E < -, § # = e 0 0 0¥ a® 0$ k \ $ k E \ § ) ) 2 a< 2 2/ S w W w w ■ ) E q § E 2 6- CV N M O N C N E LLUdkLLL UU E O m C O am N N N a` am0 L a0 a0 AIR.mL�2- mmamIF 0 m72 0 ma0 m c c c c c c c c Y_ Y f6 3 Q O Y l9 3 Q O Y_ f6 3 Q O Y_ f0 M ¢ O Y_ f0 N Q O Y_ f6 R _ ¢ O Y_ fO _ Q O fC M _ Q o > > > > > > > > 00 CD � N co m d 00 N 00 00 I.: N W O W ON -p N a_ y a N '0 N '0N N � IU4N LL LL LL LL LL LL LL LL LL LL LL lL LL LL C .QO > ¢ Q > ¢ ¢ > ¢ > ¢ ¢ > ¢ d N N O N N O N N O N N O N N O N N O N N O N N O c > m> m> m> m> m> m> m> _m C. O U N O a0 O N N O aD E O N N O .O O N N O aD O N. N O E O N N 0 -O 0 N N O aD E O N N O a0 O N cU O co ¢ m¢0N m¢ m¢ m¢ m¢ m¢ m Q m O N 0 M 0 M 0 V 0 V 0 0 O 0 tD 0 f0 0 1� 0 h 0 O 0 C+D 0 >:,- m 7 m0 C QN JIN a� 0 O co 0 to N T O Go x cc LL E m � =. � N V Gi L .^O -- ay� o mom a c[� U LL0o V �U an m 0 c U U U U U U U U tan t,l ^ mo a a a J a U a s a U C) 1n r m c C N U ~ H � ~ U U ~ N od 06 06 N d o V 'o E m U U J U J J U J J J J 0 � `� to ai N ^ V ? _ to T SPnoS n1 POAfoS10 11401 LO If11NSauoO 8i to m N ci t�Q O p O ZOODI W808 80d 1 lsad ai M1f14s1WBf o �I O 001ZB-SOOAS a �+ y W9L08OWOJ dHl CL ePNInS I BPIUvAn a^poveN m I- u ca Q Z M N y jell i Ilnd 809Zf3 i� J %` `� ]G o u 6! N� � A •�, d R Z ❑ O u sfeisW ZZ GRU K v FL MA d d m -' `� n -a' m m a © > a o ~ m E s i t i cros m 0 G n i ILA•• L O Na ❑ ❑ a m to to m a •"c q a � �n U °.° 3. a z L R• r:; < od+ o o C A A m❑ 5:4 � o . v x ■❑ c E. � �` O m p E l] ° 0% a�i , E Af O d th a mE at fn u 0 L m c f4 G L O U a' � o N = a O ... El m m m �' H m v a cCL o IV aF a r ��! 1 d y yi Q s E~ t c a -~ to Q S. Q s d mo __ c c c m E r� K & Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2103479 Pacific Petroleum California P. O. Box 2646 Report Date: June 09, 2021 16:44 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@,oecusa.com This laboratory is accredited in accordance with the recognised International Standard ISO/IEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-IAF Communique dated Apri12017) 307 Roemer Way,Suite 300 .�\/�, ,� client.oec.com\reports Santa Maria, CA 93454 r www.oecusa.com Main: (805) 922-4772 TNI 2016 & ISO/IEC 17025:2017 Fax: (805) 925-3376 TestingJ'� CA-ELAP 2438, TNI 02666 Accreditation#99137 Page I of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum Califomia Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom East @ 12' 2103479-01 Solid Solid 06/03/2021 11:50 06/04/2021 12:50 Bottom West @ 12' 2103479-02 Solid Solid 06/03/2021 11:55 06/04/2021 12:50 SampleBatch Prepai-atioti Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/F1D 8015 Diesel & Motor Oil List B I F0145 06/04/2021 16:24 STLC Metals by ICP 601013 STLC B I F0261 06/09/2021 08:56 STLC: Metals Extraction STLC Metals Extraction B 1 F0229 06/07/2021 16:29 Total Metals by CVAA Mercury Total EPA 7471A BIF0194 06/07/2021 07:40 Total Metals by ICP 601013 Total 131 F0197 06/07/2021 08:2o Volatile Organic Compounds by GUMS 826013 Full List B I F0146 06/04/2021 12:21 Volatile Organic TPH by GC/FID 8015 TPH-Gasolinc B 1 F0154 06/04/2021 10:34 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Sample ID : Bottom East @ 12' MTTllllllllllllll Sampled : 06/03/21 11:50 Sampled by: C Reynolds Matrix: Solid Field Data: NA Lab ID : 2103479-01 Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mg/kg 1 BIF0194 06/07/21 16:25 EPA 7471A Total Metals by ICP Antimony ND 2.3 mg,/kg I B 1 F0197 06/07/21 14:12 EPA 601 OB Arsenic 5.6 1.9 Barium 120 0.93 Beryllium ND 0.47 Cadmium ND 0.23 ~ Chromium 73 0.47 " " N-02 Cobalt 18 0.47 Copper 47 0.93 Lead 8.2 0.47 Molybdenum ND 0.47 Nickel 130 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 49 1.9 Zinc 65 1.9 STLC Metals by ICP Chromium ND 0.020 mg/l. 2 B1 F0261 06/09/21 14:34 STI.C/EPA 6010B Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 4.5 mg/kg 1 BIF0154 06/04/21 17:01 EPA 8015M Surrogate: d-Bromo/luorohen_ene 92 % (39 - 157) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11.50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Teiphen1'1 87 mg/kg 1 BIF0145 06/05/21 12:12 EPA 8015M (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Sampled by: C Reynolds Matrix: Solid Field Data: NA Lab ID: 2103479-01 Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kg 1 B1 F0140 06/04/21 10:16 EPA 8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 " Bromoform ND 0.050 " Brontomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 " Chlorobcnzenc ND 0.050 Chloroethane ND 0.050 " " Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 4-0ilorotoluene ND 0.050 Dibromochloromethane ND 0.050 1,2-Dibronio-3-chloropropane ND 0.050 1,2-Dibromoethane (EDB) ND 0.050 Dibromomethane ND 0.050 " 1,2-Dichlorobenzene ND 0.050 13-Dichlorobcnzcnc ND 0.050 IA-Dichlorobcnzcnc ND 0.050 " Dichlorodilluoromcthane ND 0.050 " C�."�° 1, 1 -Dichloroethane ND 0.050 1.2-Dichloroethane ND 0.050 1,1-Dichloroethene ND 0.050 " cis- 1.2-Dichloroethene ND 0.050 trans-l.2-Dichloroethene ND 0.050 " 1,2-Dichloropropane ND 0.050 1,3-Dichloropropane ND 0.050 12-Dichloropropane ND 0.050 1, 1 -Dichloropropene ND 0.050 " cis-L3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 Ethylbenzenc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805,, 925-3376 Page 5 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.050 mgtkg 1 B 1 F0146 06/04/21 16:16 EPA 8260B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 I.1,1,2-Tetrachloroethane ND 0.050 1.1,2,2-Tetrachloroethane ND 0.050 Tctrachloroethcnc (PCE) ND 0.050 Toluene ND 0.050 1,23-Trichlorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1,1,1-Trichloroelhane ND 0.050 1,1,2-Trichloroelhane ND 0.050 Trichloroelhene (TCE) ND 0.050 Trichlorofluoromethane ND 0.050 1,2,3-Trichloropropane ND 0.050 1,2,4-Trimethylbenzene ND 0.050 1.3.5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Uibromgllnorontethanc, 103 ;'( (74 - 122) Surrogate: Toluene-dg 99 % (65 - 128) Surrogate: 4-BromoJ torohen_ene 105 S'� (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: ;805) 925-3376 Page 6 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 I Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg 1 BIF0194 06/07/21 16:27 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg I B I F0197 06/07/21 14:15 EPA 601013 Arsenic 7.4 1.9 Barium 160 0.96 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 51 0.49 " " " " N-02 Cobalt 14 0.48 Copper 63 0.96 Lead 8.9 0.48 Illolvbdenum 0.57 0.48 Nickel 88 0.48 Selenium ND 1.9 Silver ND 0.49 Thallium ND 0.96 Vanadium 52 1.9 Zinc 71 1.9 STLC Metals by ICP Chromium ND 0.020 mg/L 2 B I F0261 06/09/21 14:37 STLC/EPA 601013 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.4 mg/kg I B1F0154 U6104/21 17:29 EPA8015M Surrogate: 4-Bromo/hrorohomwe 95 i6, (39 - 157) 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 32 i A W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID : Bottom West @ 12' Sam Pled : 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.048 mg/kg I B 1 F0146 06/04/21 15:48 EPA 8260B Bromobenzene ND 0.048 Bromochloromethane ND 0.048 " Bromodichloromethane ND 0.048 " Bromotonn ND 0.048 Bromomethane ND 0.048 n-Butylbenzene ND 0.048 sec-Butylbenzene ND 0.048 tert-Butyl benzene ND 0.048 Carbon tetrachloride ND 0.048 Chlorobenzenc ND 0.048 Chloroethane ND 0.048 " Chlorofonn ND 0.048 Chloromethane ND 0.048 " 2-Chlorotoluene ND 0.048 " 4-Chlorotoluene ND 0.048 Dibromochloromelhane ND 0.048 " 1.2-Dibromo-3-chloropropane ND 0.048 1,2-Dibronioethane (EDB) ND 0.048 Dibronxnuethane ND 0.048 1.2-Dichlorobenzene ND 0.048 " 1.3-Dichlorobenzene ND 0.048 IA-Dichlorobenzene ND 0.048 Dichloroditluoromethane ND 0.048 CCI11 1, 1 -Dichloroethane ND 0.048 " 1,2-Dichloroethane ND 0.048 " 1, 1 -Dichloroethene ND 0.048 " cis-1.2-Dichloroethene ND 0.048 trans- 1.2-Dichloroethene ND 0.048 1,2-Dichloropropane ND 0.048 13-Dichloropropane ND 0.048 2,2-Dichloropropalie ND 0.048 1, 1 -Dichloropropene ND 0.048 cis- 1.3-Dichloropropene ND 0.048 " trans- I .3-Dichloropropene ND 0.048 Fthylbcnzene ND 0.048 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID : Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.048 mg/kg I BIF0146 06/04/2 1 15:48 EPA8260B 4-Isopropyl Toluene ND 0.048 Isopropylbenzene ND 0.048 Methylene chloride ND 0.048 Naphthalene ND 0.048 n-Propylbenzene ND 0.048 " Stvrene ND 0.048 1,1,1,2-Tenachloroethane ND 0.048 1,1,2,2-Tetrachloroethane ND 0.048 1'etrachlorocthene (PCE) ND 0.048 Toluene ND 0.048 1,23-Trichlorobenzene ND 0.048 1,2,4-Trichloroben7ene ND 0.048 " 1, 1, 1 -Trichloroethane ND 0.048 1,12-Trichloroethane ND 0.045 Trichloroethane (WE) ND 0.048 Trichlorofluorontethane ND 0.048 1,2,3-Trichloropropane ND 0.048 1,44-Trimethylbenzene ND 0.048 1.3,5=rrimethylbenzene ND 0.048 Vinyl chloride ND 0.048 Xylcncs (total) ND 0.048 Surrogate: Uihrounnlluuroync thayre 104 74 - 122) Surrogate. Toluene-d8 102 90 ( 65= 128) " Sulrrogate: 4-Bramo/luoroben_enc 104 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oee.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103474 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0194 - EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (B1F0194-BLKI) Analyzed: 06/07/21 12:49 Mercury ND 0.10 mg/kg LCS (B1F0194-BSI) Analyzed: 06/07/21 12:53 Mercury 0.782 0.10 mg%kg 0.833 94 85-115 LCS Dup (B1F0194-BSD1) Analyzed: 06/07/21 13:30 Mercury 0.859 0.10 mg/kg 0.833 103 85-115 9 20 Duplicate (B1F0194-DUPl) Source: 2103489-02 Analyzed: 06/07/21 13:34 Mercury ND 0.097 mg/kg ND 20 Matrix Spike (B1F0194-MS1) Source: 2103489-02 Analyzed: 06/07/21 13:37 Mercury 0.827 0.091 mg/kg 0.755 ND 110 75-125 Matrix Spike Dup (B1F0194-MSDI) Source: 2103489-02 Analyzed: 06/07/21 13:39 Mercury 0.839 0.089 mgkg 0.742 ND 113 75-125 1 20 Post Spike (B1F0194-PS1) Source: 2103489-02 Analyzed: 06/07/21 13:41 Mercury 5.52 ug/I. 25.0 0.00199 22 85-115 Ql, 02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 8051925-3376 Page 11 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 by Control I Total Metals Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLK1) Analyzed: 06/07/21 13:30 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 " Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (B1F0197-BS1) Analyzed: 06/07/21 13:35 Antimony 92.0 2.5 mgtkg 100 92 80-120 Arsenic 97.2 2.0 100 97 80-120 Barium 99.6 1.0 100 too 80-120 Beryllium 95.1 0.50 100 95 80-120 Cadmium 98.2 0.25 100 98 80-120 Chromium 98.8 0.50 100 99 80-120 Cobalt 99,2 0.50 100 99 80-120 Copper 98.2 1.0 100 98 80-120 Lcad 100 0.50 100 too 80-120 Molybdenum 96.0 0.50 100 96 80-120 Nickel 99.6 0.50 100 100 80-120 Selenium 96.4 2.0 100 96 80-120 Silver 4.92 0.50 5.00 98 80-120 Thallium 100 1.0 100 100 80-120 Vanadium 90.6 2.0 100 97 80-120 Zinc 98.6 2.0 100 99 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes -- Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 _.. LCS Dup (B1F0197-BSD1) Analyzed: 06/07/21 13:37 Antimony 94.8 2.5 mg/kg too 95 80-120 3 20 Arsenic 98.8 2.0 100 99 80-120 2 20 Barium 101 1.0 100 101 80-120 1 20 Beryllium 96.5 0.50 100 96 80-120 1 20 Cadmium 99.2 0.25 100 99 80-120 1 20 Chromium 100 0.50 100 100 80-120 1 20 Cobalt 100 0.50 100 100 80-120 1 20 Copper 99.8 1.0 100 100 80-120 2 20 Lead 101 0.50 100 101 80-120 1 20 Molybdenum 98.2 0.50 100 98 80-120 2 20 • Nickel 101 0.50 100 101 80-120 1 20 Selenium 97.8 2.0 100 98 80-120 1 20 Silver 4.93 0.50 5.00 99 80-120 0.1 20 Thallium 102 1.0 100 102 80-120 1 20 Vanadium 98.0 2.0 100 98 80-120 1 20 Zinc 99.8 2.0 100 100 80-120 1 20 Duplicate (B1F0197-DUPl) Source: 2103489-01 Analyzed: 06/07/21 13:52 Antimony ND 2.4 mg.,kg ND 20 Arsenic 1.22 1.9 NI) 20 Barium 21.0 0.97 22.9 8 20 _ Beryllium ND 0.49 ND 20 Cadmium ND 0.24 ND 20 Chromium 1.94 0.49 2.02 4 20 Cobalt 1.40 0.49 1.78 24 20 QR414 Copper 1.33 0.97 1.40 5 20 Lead 1.23 0.49 1.40 13 20 Molybdenum ND 0.49 ND 20 Nickel 1.31 0.49 1.34 2 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 3.86 1.9 4.18 8 20 Zinc 4.32 1.9 4.51 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Totalby Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MSI) Source: 2103489-01 Analyzed: 06/07/21 13:40 Antimony 70.3 2.3 mg/kg 93.4 ND 75 10-116 Arsenic 93.3 1.9 93.4 ND 100 77-121 Barium 119 0.93 93.4 22.9 102 30-169 Beryllium 90.1 0.47 93.4 ND 96 86-111 Cadmium 91.8 0.23 93.4 ND 98 81-112 Chromium 96.8 0.47 93.4 2.02 102 75-129 Cobalt 94.2 0.47 93.4 1.78 99 71-121 Copper 96.2 0.93 93.4 1.40 102 68-135 Lead 94.4 0.47 93.4 1.40 100 72-121 Molybdenum 88.2 0.47 93.4 ND 94 70-112 Nickel 95.2 0.47 93.4 1.34 101 73-121 Selenium 90.1 1.9 93.4 ND 97 76-116 Silver 4.56 0.47 4.67 ND 98 54-132 Thallium 92.3 0.93 93.4 ND 99 64-120 w Vanadium 96.5 1.9 93.4 4.18 99 78-124 Zinc 98.0 1.9 93.4 4.51 100 50-143 Matrix Spike Dup (B1F0197-MSD1) Source: 2103489-01 Analyzed: 06/07/21 13:42 Antimony 70.4 2.4 mg/kg 95.8 ND 73 10-110 0.1 20 Arsenic 94.3 1.9 95.8 ND 98 77-121 1 20 Barium 116 0.96 95.8 22.9 97 30-169 3 20 Beryllium 91.2 0.48 95.8 ND 95 86-111 I 20 Cadmium 92.3 0.24 95.8 ND 96 81-112 0.6 20 Chromium 97.6 0.48 95.8 2.02 100 75-129 0.8 20 Cobalt 94.7 0.48 95.8 1.78 97 71-121 0.6 20 -� Copper 96.9 0.96 95.8 1.40 100 68-135 0.7 20 Lead 94.9 0.48 95.8 1.40 98 72-121 0.6 20 Molybdenum 88.6 0.48 95.8 ND 93 70-112 0.5 20 Nickel 95.5 0.48 95.8 1.34 98 73-121 0.3 20 Selenium 91.2 1.9 95.8 ND 95 76-116 1 20 Silver 4.64 0.48 4.79 ND 97 54-132 2 20 Thallium 93.1 0.96 95.8 ND 97 64-120 0.9 20 _ Vanadium 97.2 1.9 95.8 4.18 97 78-124 0.7 20 Zinc 103 1.9 95.8 4.51 103 50-143 5 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 32 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by lCP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (BIF0197-PSI) Source: 2103489-01 Analyzed: 06/07/21 13:45 Antimony 2.03 mg/L 2.00 0.00248 101 75-125 Arsenic 2.04 2.00 0.0178 101 75-125 Barium 2.50 2.00 0.460 102 75-125 " Beryllium 1.96 2.00 0.00218 98 75-125 Cadmium 2.00 2.00 -0.00308 100 75-125 Chromium 2.07 2.00 0.0408 101 75-125 Cobalt 2.06 2.00 0.0359 101 75-125 Copper 2.06 2.00 0.0293 102 75-125 Lead 2.07 2.00 0.0283 102 75-125 Molybdenum 2.01 2.00 -0.00109 101 75-125 • Nickel 2.06 2.00 0.0271 102 75-125 Selenium 1.99 2.00 -0.0103 99 75-125 Silver 0.0945 0.100 -0.00169 94 75-125 Thallium 2.03 2.00 -0.00407 101 75-125 Vanadium 2.08 2.00 0.0842 100 75-125 Zinc 2.10 2.00 0.0909 101 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 STLC Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0261 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (BlF0261-BLK1) Analyzed: 06/09/21 13:50 Chromium ND 0.010 mg/I. LCS (B1F0261-BS1) Analyzed: 06/09/21 14:17 Chromium 10.1 0.010 mg/l. 10.0 101 80-120 LCS Dup (B1F0261-BSD1) Analyzed: 06/09/21 14:19 Chromium 10.2 0.010 mg/L 10.0 102 80-120 0.5 20 Duplicate (BlF0261-DUPl) Source: 2103218-01 Analyzed: 06/09/21 14:27 Chromium 1.22 0.020 mg/l. 1.22 0.08 20 Leach Fluid Blank (BlF0261-LBK1) Analyzed: 06/09/21 13:52 Chromium ND 0.020 mg/l. Leach Fluid Blank (BlF0261-LBK2) Analyzed: 06/09/21 13:55 Chromium ND 0.020 mgJL Leach Fluid Blank (B1F0261-LBK3) Analyzed: 06/09/21 13:58 Chromium ND 0.020 mg/L The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: {805) 925-3376 Page 16 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLK1) Analyzed: 06/04/21 12:45 TPI1 Gasoline (('5-C12) ND 0.49 mg/kg Surogate:4-Bromolluorobenrcne 0.107 " 0.123 87 39-157 LCS (B1F0154-BS1) Analyzed: 06/04/21 11:48 TPH Gasoline (C5-C12) 1.38 0.50 mgtkg 0.999 138 68-139 Surrogate:4-Brotng9uorohcn�ene 0.158 110.125 126 39-157 LCS Dup (B1F0154-BSD1) Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12) 1.29 0.50 mg/kg 1.00 128 68-139 7 20 Surrogate: 4-Bromo/luorohenzene 0.146 0.125 116 39-157 Duplicate (B1F0154-DUPl) Source: 2103455-02RE1 Analyzed: 06/04/21 15:35 TPH Gasoline (C5-C12) ND 0.50 mg/kg 0.113 20 Surrogate. 4-Bromolluorohenzene 0.113 " 0.124 92 39-157 Matrix Spike (B1F0154-MS1) Source: 2103429-02 Analyzed: 06/04/21 19:23 TPH Gasoline (C5-('12) 0.905 0.49 mg/kg 0.973 ND 93 10-171 Surrogate:4-Bromo/luoroben_enc 0.132 " 0.122 109 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.com\reports TEL: (805) 922-4772 n 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Semi -Volatile Organic TPH by GC/FID - Quality Control Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) Analyzed: 06/04/21 11:45 TPH Diesel (C13-('22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 11 Surrogate: r-TophenTl 41.5 50.0 83 05-136 LCS (B1F0145-BSI) Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22) 434 10 mg1kg 499 87 72-115 TPH Motor Oil (C23-C40) 420 50 499 84 74-126 Surrogate: o-Tcuphenyl 45.8 49.9 92 65-136 LCS Dup (B1F0145-BSDI) Analyzed: 06/04/21 12:07 TPII Diesel (C13-C22) 444 10 mg/kg 499 89 72-115 2 20 TPH Motor Oil (C23-C40) 441 50 499 88 74-126 5 20 Surrogate: o-TeuphenYl 46.7 49.9 94 65-136 Duplicate (B1F0145-DUPl) Source: 2103472-01 Analyzed: 06/04/21 16:23 TPfI Diesel (C13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) ND 50 ND 20 Surrogate: o-Teuphcm;l 40.5 49.9 81 65-136 Matrix Spike (B1F0145-MS1) Source: 210347241 Analyzed: 06/04/21 15:37 TPH Diesel (C13-C22) 452 10 mg/kg 498 ND 91 46-147 TPH Motor Oil (C23-C40) 500 50 498 ND 100 35-171 Surrogate: o-Teuphenrl 41.6 49.8 84 65-736 Matrix Spike Dup (B1F0145-MSD1) Source: 2103472-01 Analyzed: 06/04/21 16:00 TPH Diesel (C13-('22) 496 10 mg/kg 498 ND 100 46-147 9 20 TPH Motor Oil (('23-C40) 517 50 498 ND 104 35-171 3 20 Surrogate: a-Tcuphenyl 44.0 49.8 88 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 32 C A lwb-MOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLKI) Analyzed: 06/04/21 11:32 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " Bromochloromethane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 " Bromomethane ND 0.0050 " n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 " Chloromethane ND 0.0050 " 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (FDB) ND 0.0050 Dibromomcthane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 " 1,3-Dichlorobenzene ND 0.0050 " 1,4-Dichlorobenzene ND 0.0050 " Dichlorodifluoromcthanc ND 0.0050 --_-- 1, 1-Dichloroethane ND 0.0050 " I2-Dichlorocthane ND 0.0050 M-Dichloroethene ND 0.0050 " cis-1.2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " 1.2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 " 2.2-Dichloropropane ND 0.0050 1, 1 -Dichloropropene ND 0.0050 cis- L3 -Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Ethylbenzene ND 0.0050 Hexachlorobutadiene ND 0.0050 " 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (BIF0146-BLKI) Analyzed: 06/04/21 11:32 Styrene ND 0.0050 mglkg 1,1.1,2-Tetrachloroethane ND 0.0050 1,1,2,2-Tetrachloroethane ND 0.0050 " Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 " 1,2,3-Trichlorobenzene ND 0.0050 " 1,2,4-Trichloroben7ene ND 0.0050 1,1,1-Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 " Trichlorofluoromethane ND 0.0050 " 1,2.3-Trichloropropane ND 0.0050 1,2,4-Trimethylbenzene ND 0.0050 1.3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 Surrogate. Dibronzgfluortun(,thcrnc 0.0516 0.0498 104 74-122 Surrogate: Toluene-d8 0.0503 0.0498 101 65-128 Surrogate:4-Bromo/luorohenzene 0.0529 0.0498 106 75-121 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 Benzene 0.0406 0.0050 mglkg 0.0398 102 70-131 Bromobenzene 0.0466 0.0050 0.0398 117 74-130 Bromochloromcthanc 0.0399 0.0050 0.0398 100 64-133 Bromodichloromethane 0.0445 0.0050 0.0398 112 69-137 Bromoform 0.0447 0.0050 0.0398 112 55-132 Bromomethane 0.0407 0.0050 0.0398 102 10-142 n-Butylbenzene 0.0476 0.0050 0.0398 120 64-156 sec-Butylbenzene 0.0493 0.0050 0.0399 124 75-155 tert-Butylbenzene 0.0482 0.0050 0.0398 121 74-144 Carbon tetrachloride 0.0442 0.0050 0.0398 111 67-135 Chlorobenzene 0.0445 0.0050 0.0398 112 73-134 Chloroethane 0.0390 0,0050 0.0398 98 10-167 Chloroform 0.0412 0.0050 0.0398 104 69-124 C:hloromethane 0.0297 0.0050 0.0398 75 34-136 2-Chlorotoluene 0.0454 0.0050 0.0398 114 75-135 4-Chlorotoluene 0.0460 0.11050 0.0398 116 70-138 Dibromochloromethane 0.0439 0.0050 0.0398 110 67-135 1,2-I)ibromo-3-chloropropanc 0.0435 0.0050 0.0398 109 41-149 1,2-Dibronwcthane (EDB) 0.0409 0.0050 0.0398 103 68-131 Dibronwmcthane 0.0433 0.0050 0.0398 109 61-140 1,2-Dichlorobenzene 0.0458 0.0050 0.0398 115 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIlent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 32 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 CompoundsVolatile Organic by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 1,3-Dichlorobcnzene 0.0462 0.0050 mg/kg 0.0398 116 76-138 1,4-Dichlorobenzene 0.0457 0.0050 0.0398 115 72-132 Dichloroditluoronrcthane 0.0210 0.0050 0.0398 53 10-155 CCFH 1,1-Dichloroethane 0.0389 0,0050 0.0399 98 63-139 1,2-Dichlorocthanc 0.0416 0.0050 0.0398 104 64-126 1, 1 -Dichloroethene 0.0342 0.0050 0.0399 86 52-167 cis-1,2-Dichloroethene 0.0401 0.0050 0.0398 101 70-135 trans-l.2-Dichloroethene 0.0392 0.0050 0.0399 99 67-147 1,2-Dichloropropane 0.0406 0.0050 0.0398 102 68-131 1,3-Dichloropropane 0.0405 0.0050 0.0398 102 64-128 2,2-Dichloropropane 0.0432 0.0050 0.0398 109 63-154 1,1-Dichloropropene 0.0393 0.0050 0.0398 99 68-138 cis- 1.3-Dichloropropene 0.0416 0.0050 0.0398 105 72-134 trans-1,3-Dichloropropene 0.0437 0.0050 0.0398 110 69-132 Ethylbenzene 0.0449 0.0050 0.0398 113 68-136 1lexachlorobutadiene 0.0546 0.0050 0.0398 137 72-198 4-Isopropyl Toluene 0.0504 0.0050 0.0398 127 74-150 Isopropylbenzene 0.0473 0.0050 0.0398 119 71-149 Nlethylene chloride 0.0346 0.0050 0.0398 87 51-127 Naphthalene 0.0482 0.0050 0.0398 121 57-158 n-Propylbenzene 0.0474 0.0050 0.0398 119 70-143 Styrenc 0.0456 0.0050 0.0398 115 68-138 1,1.1,2-Tetrachloroethanc 0.0459 0.0050 0.0398 115 76-130 1.1,2.2-Tctrachloroethane 0.0399 0.0050 0.0398 too 60-136 Tetrachloroethene (PCE) 0.0443 0.0050 0.0398 111 73-138 Toluene 0.0430 0.0050 0.0398 108 72-128 1,2,3-Trichlorobenzene 0.0507 0.0050 0.0398 127 61-166 12.4-Trichlorobenzene 0.0502 0.0050 0.0398 126 71-158 1,1,1-Trichloroethanc 0.0424 0,0050 0.0398 107 71-135 L1,2-Trichloroethanc 0.0414 0.0050 0.0398 104 64-132 Trichloroethene (TCE) 0.0442 0.0050 0.0398 111 74-139 'Fri chlorolluoronrethane 0.0429 0.0050 0.0398 108 30-156 1,2.3-Trichloropropane 0.0452 0.0050 0.0398 114 67-123 1,2,4-Trimethylbenzene 0.0454 0.0050 0.0398 114 68-134 1.3,5-Trimethylbenzenc 0.0461 0.0050 0.0398 116 71-140 Vinyl chloride 0.0326 0.0050 0.0398 82 43-144 Xylenes (total) 0.133 0.0050 0.119 112 69-138 Smrogate. Dibronwllrarrontc.thernc 0.0525 0.0497 106 74-122 Surrogate: Toluene -A 0.0517 0.0497 104 65-128 Surrogate:4-Bromollumvhenrene 0.0530 0.0497 107 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum Califomia Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilet by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) Analyzed: 06/04/21 10:13 Benzene 0.0423 0.0050 mg/kg 0.0400 106 70-131 4 20 Bromobenzene 0.0498 0.0050 0.0400 124 74-130 7 20 Bromochlorotncthane 0.0412 0.0050 0.0400 103 64-133 3 20 F' Bromodichloromethane 0.0455 0.0050 0.0400 114 69-137 2 20 Bromofonn 0.0458 0.00.50 0.0400 115 55-132 2 20 Bromomethane 0.0391 0.0050 0.0400 98 10-142 4 20 n-Butylben7ene 0.0476 0.0050 0.0400 119 64-156 0.1 20 sec-Butylbenzene 0.0508 0.0050 0.0400 127 75-155 3 20 tert-Butylbenzene 0.0490 0.0050 0.0400 124 74-144 3 20 Carbon tetrachloride 0.0456 0.0050 0.0400 114 67-135 3 20 r Chlorobenzene 0.0457 0.0050 0.0400 114 73-134 3 20 Chloroethane 0.0394 0.0050 0.0400 98 10-167 1 20 Chloroform 0.0421 0,0050 0.0400 105 69-124 2 20 Chloromethane 0.0308 0.0050 0.0400 77 34-136 4 20 2-Chlorotoluene 0.0452 0.0050 0.0400 113 75-135 0.4 20 4-C:hlorotoluene 0.0468 0.0050 0.0400 117 70-138 2 20 Dibromochloromethane 0.0463 0.0050 0.0400 116 67-135 5 20 1,2-Dibmmo-3-chloropropane 0.0461 0.0050 0.0400 115 41-149 6 20 1.2-Dibromoethane (F.DB) 0.0422 0.0050 0.0400 105 68-131 3 20 Dibromomcthane 0.0459 0.0050 0.0400 115 61-140 6 20 1,2-Dichlorobenzene 0.0472 0.0050 0.0400 118 76-136 3 20 --• 1,3-Dichlorobenzene 0.0489 0.0050 0.0400 122 76-138 6 20 1,4-Dichlorobenzene 0.0472 0.0050 0.0400 118 72-132 3 20 Dichloroditluoromcthanc 0.0228 0.0050 0.0400 57 10-155 8 20 I,I-Dichloroethane 0.0405 0.0050 0.0400 101 63-139 4 20 ' 1,2-DichIorocthatic 0.0425 0.0050 0.0400 106 64-126 2 20 1,1-Dichoroethene 0.0347 0.0050 0.0400 87 52-167 2 20 cis-1.2-Dichloroethene 0.0420 0.0050 0.0400 105 70-135 5 20 trans-1,2-Dichloroethene 0.0401 0.0050 0.0400 100 67-147 2 20 1,2-Dichloropropane 0.0430 0.0050 0.0400 107 68-131 6 20 1,3-Dichloropropane 0.0426 0.0050 0.0400 106 64-128 5 20 2.2-Dichloropropane 0.0446 0,0050 0.0400 Ill 63-154 3 20 -• 1,1-Dichloropropene 0.0406 0.0050 0.0400 102 68-138 3 20 cis-I.3-Di chloropropene 0.0434 0.0050 0.0400 108 72-134 4 20 trans-1,3-Dichloropropene 0.0454 0.0050 0.0400 114 69-132 4 20 l?lhvlbenzene 0.0470 0,0050 0.0400 118 68-136 5 20 Ilexachlorobutadiene 0,0549 0.0050 0.0400 137 72-198 0.5 20 4-Isopropyl Toluene 0.0514 0.0050 0.0400 128 74-150 2 20 Isopropylbeniene 0.0499 0.0050 0.0400 125 71-149 5 20 _ Methylene chloride 0.0360 0.0050 0.0400 90 51-127 4 20 Naphthalene 0.0511 0.0050 0.0400 128 57-158 6 20 n-Propylbenzene 0.0466 0.0050 0.0400 116 70-143 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCFH CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 210347: Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilet poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) Analyzed: 06/04/21 10:13 Styrene 0.0479 0.0050 mg/kg 0.0400 120 68-138 5 20 1,1,1,2-Tetrachloroethane 0.0490 0.0050 0.0400 123 76-130 7 20 1,1,2,2-1'ctrachloroethane 0.0417 0.0050 0.0400 104 60-136 5 20 Tetrachloroethene WCE) 0.0454 0.0050 0.0400 114 73-138 3 20 Toluene 0.0439 0.0050 0.0400 110 72-128 2 20 1,2,3-Trichlorobenzene 0.0520 0.0050 0.0400 130 61-166 3 20 1,2,4-Trichlorobenzene 0.0512 0.0050 0.0400 128 71-158 2 20 1, 1, 1 -Trichloroethane 0.0432 0.0050 0.0400 108 71-135 2 20 1,1,2-Trichloroethane 0.0449 0.0050 0.0400 112 64-132 8 20 Trichloroethene (TCE) 0.0448 0.0050 0.0400 112 74-139 1 20 �• Trichlorofluormnethane 0.0430 0.0050 0.0400 107 30-156 0.1 20 1,2,3-Trichloropropane 0.0463 0.0050 0.0400 116 67-123 3 20 1,2.4-Trimethylbenzene 0.0459 0.0050 0.0400 115 68-134 1 20 1,3,5-Trimethylbenzene 0.0465 0.0050 0.0400 116 71-140 0.9 20 Vinyl chloride 0.0338 0.0050 0.0400 84 43-144 3 20 Xylenes(tota]) 0.139 0.0050 0.120 116 69-138 4 20 Surrogate: Dibroaui/luoromethanc 0.0519 0.0500 104 74-122 Surrogate: Toluene-d8 0.0510 0.0500 102 65-128 Surrogate:4-BromoJluorohen:ene 0.0530 0.0500 106 75-121 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 ISIo'A S Benzene ND 0.0050 mglkg ND 20 Bromobenzene ND 0,0050 " ND 20 Bromochloromethane ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 - Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 NI> 20 sec-Butylbenzene ND 0.0050 ND 20 - tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene NI) 0.0050 ND 20 - Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-C'hlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1.2-Dibromo-3-chloropropanc ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibromomcthane ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 23 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilei Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 ISIoHS 1.3-Dichlorobenzenc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene NI) 0.0050 ND 20 Dichlorodifluoromethane ND 0.0050 ND 20 CCHI 1,1-Dichloroethane ND 0.0050 ND 20 1,2-Dichlorocthane ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 NI) 20 1,3-Dichloropropane ND 0.0050 ND 20 22-Dichloropropane ND 0.0050 ND 20 1,1-Dichloropropene NI) 0.0050 ND 20 cis- 1.3 -Dichloropropene NI) 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 NI) 20 Ethylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Nlethylene chloride ND 0.0050 " ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane NI) 0.0050 NI) 20 1,1,22-Tctrachloroethanc ND 0.0050 ND 20 Tetrachloroethene WCE) ND 0.0050 " ND 20 Tolucnc ND 0.0050 NI) 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2,4-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1.2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorofluoromethane NI) 0.0050 NI) 20 1,2,3-Trichloropropane ND 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylben7ene NI) 0.0050 NI) 20 Vinyl chloride ND 0.0050 NI) 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dihronw/luorumethunc 0.0538 0.0498 108 74-122 Surrogate:7nluene-d8 0.0509 0.0498 102 6i-128 Surrogate: 4-Bromq/luorohenzene 00506 0.0498 102 7-5-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805; 925-3376 Page 24 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Method Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NF,LAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NELAP STLC Metals by ICP 6010B STLC Chromium STLC/EPA 6010B Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Water OEC, Internal Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OF;C, Internal Total Metals by ICP 0010B Total Antimony EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Arsenic EPA 6010B Solid OEC, CA-ELAP,NF.LAP 6010B Total Barium EPA 601OB Solid OEC, CA-ELAP,NELAP 601 OB Total Beryllium EPA 601 OB Solid OEC, CA-FLAP,NELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Chromium EPA 6010E Solid OF;C, CA-EL.AP,NELAP 6010B Total Cobalt EPA 601 OB Solid OEC, CA-ELAI',NEI.AP 6010B Total Copper EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Lead EPA 601 OB Solid OEC, CA-ELAP.NELAP 6010B "Total Molybdenum EPA 6010B Solid OEC, CA-ELARNELAP 0010B Total Nickel EPA 6010B Solid OEC, CA-IlLAP,NEI.AP 6010B Total Selenium EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Silver EPA 6010B Solid OEC, CA-ELARNELAP 6010B Total Thallium EPA 6010B Solid OHC, CA-FLARNELAP 6010B Total Vanadium EPA 6010B Solid OEC, CA-ELARNELAP 6010B Total Zinc EPA 6010B Solid OEC, CA-F.LARNELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA-ELAP,NELAP 8200B Full List EPA 8260B Solid OEC, Internal Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference C'CFti The CCV for this analyte failed high. Results for this analyte may be biased high. CC']ll The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. ISIowS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above I Ox STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below statelfederal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:.805 925-3376 Page 26 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 32 57 x U 0 Q x a N H N O O Ga O (3) � U N K4 O ZT O •r-I / U) H � N z � x a h / N Ln FC. N O Q G i pq [xj O O x N I U Q r- In l` U) 71 -� ;3, £ h U () / C7 0 u� r CJ 0 U UO Nrl rl ~roo.Q 0aa)ii �a 11 S4 �$ a) H z (0 .H Y4 r-i a) S4 �3 4-) ¢, U rl rl (1) U) U) (0 -.i 04 U I~ t0 •H ." [=+0FCHU)2> 0 0 4 0 0 0 0 0 0 0 0 N N C N N N + + O O O O O M N O O O m — — 1 1 W 00 CDn C- CO 0 0 O O 0 0 0 0 0 0 Lq 0 0 s 0 00 0 0 co 0 r; O 0 I, - CD Lq O O fD Cn O O 0 Lq O O Cl) O O Ch O N O 0 N O 47 I O 0 0 O O 0 O 0 O 0 O O O O O N O N lL CY) ►7i x C] W . w � I o FG Ga c x O �l O / I,- -1 4-) (\A a) ,3' x O t5 � U O Q r1 bi N S~ z CO h �3 N Q� iz O a) (N i-1 [� (f) O H Q .. / rl rl —1 CJ $� O O W N I x cl) a �v'T x rJ U M UPG .. .. .. .. .. .. .. a) � +J E aJ a(00 �4-0 a)z4-+ a 0a)E �a (Cl •H s4 r-I a) V (n F U) (d •r-I � U C. 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C� c ❑ ` c V r 4' m m a U > V m 4 r e m tm, S > C° w 5 n � m v m o m tl1 °1 ¢ U do IX 0: E m S m N N Q a+ ALA♦-♦ W q G � Im m N c N O E m E ai E ❑ ❑: a N F. z;Q U v, 00 # Z Q.:} 12 .. ❑" c w 3 p Z U U G C G N m ■❑ x _0} 0 R • �, 0 Y o Li ° w ` E m 0eq m W eq a H a N tm 3. . E ero G7 3 o, o G N t s p L 6 O W tiS 1 m aj .? Qu6 a. a O 00 U -, V cn 1-1 cl m m on c a`1 m L L c CL G fl c F o Q E r ar 7. c to C C C nE -� LIM it ���� w U t- i= Analytical Report Oilfielo Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102742 Pacific Petroleum California P. O. Box 2646 Report Date: May 06, 2021 17:25 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 05, 2021 08:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: =Aor Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page I of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Sample Suinniary Date Received Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled NW Comer 2102742-01 Solid Solid 05/04/2021 14:30 05/05/2021 08:00 NE Corner 2102742-02 Solid Solid 05/04/2021 14:35 05/05/2021 08:00 SW Corner 2102742-03 Solid Solid 05/04/2021 14:40 05/05/2021 08:00 SE Corner 2102742-04 Solid Solid 05/04/2021 14:45 05/05/2021 08:00 Center 2102742-05 Solid Solid 05/04/202114:50 05/05/202108:00 Sample Batch Preparation Sumniary Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FIU 9015 Diesel & Motor Oil List Bl E0062 05/0512021 10:31 Total Metals by CVAA Mercury Total EPA 7471 A B I E0098 05/05/2021 08:00 Total Metals by 1CP 601013lbtal B 1 E0102 05/05/2021 09:08 Volatile Organic Compounds by GC/MS 8260B Full List B11 0lD1 05/05/2021 09:05 Volatile Organic TPH by GC/FlD 8015 TPEI-Gasoline B 1 E0095 05/05/2021 06:24 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 -___ Page 2of37 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Sample ID: NW Corner Sampled: 05/04/21 14:30 Sampled by : Matrix: Solid Lab ID: 2102742-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mgfkg 1 B 1 F0098 05105,21 12:11 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg1kg 1 B I E0102 05/06/21 13:33 EPA 601 OB Arsenic 7.8 2.0 Barium 120 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 44 0.50 Cobalt 18 0.50 Copper 36 0.99 Lead 16 0.50 Molybdenum ND 0.50 Nickel 71 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND 0.99 Vanadium 43 2.0 Zinc 68 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) 19 4.4 mg/kg 1 B I E0095 05/05/21 12:06 EPA 9015M 0-04 Surrogate. 4-Bromofluoroben_cne 109111111 (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 490 10 mg'kg 1 B1 E0062 05/05/21 19:52 EPA 8015M TPH Motor Oil (('23-C40) ND 50 " " Sio•rogatc: o-Terphe t),l 89 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comWeports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 37 AL W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 1 7:25 Analytical Report for Sarnples Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by: Lab ID : 2102742-01 Field Data: NA Analyte Result RI- Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND I z rngikg ISI O B I E01111 fYS 05121 I 56 EPA 8260B Bromobenzene ND 1.3 " Bromochloromethane ND I.3 Bromodichloromethane ND 1.3 Bromofonn ND 1.3 Bromomethane ND 1.3 " n-Butylbenzene ND 1.3 " sec-Butylbenzene ND 1.3 " tert-Butylbenzene ND 1.3 Carbon tetrachloride ND 1.3 " Chlorobenzenc ND 1.3 Chloroethane ND 1.3 Chloroform ND 1.3 Chloromethane ND 1.3 2-Chlorotoluene ND 1.3 4-Chlorotoluene ND 1.3 Dibromochloromethane ND 1.3 1,2-Dibromo-3-chloropropane ND 1.3 " 1,2-Dibromoethane (EDB) ND 1.3 " Dibromomethane ND 1.3 1,2-Dichlorobenzene ND 1.3 1,3-Dichlorobcnzcnc ND 1.3 " 1,4-Dichlorobcnzcnc ND 1.3 Dichloroditluoromethane ND 1.3 " 1, 1 -Dichloroethane ND 1.3 1,2-Dichloroethane ND 1.3 1,1-Dichloroethene ND 1.3 cis-1,2-Dichloroethene ND 1.3 trans-1,2-Dichloroethene ND 1.3 1,2-Dichloropropane ND 1.3 1,3-Dichloropropane ND 1.3 2,2-Dichloropropane ND 1.3 1, 1 -Dichloropropene ND 1.3 cis- 1.3-Dichloropropene ND 1.3 trans-1,3-Dichloropropene ND 1.3 Ethylbcnzene ND 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 37 r A 6W TA5 M&� I Oilfield Environmental & Compliance, Inc. Pacific Petroleum C.aliforni:s Protect: Pacific Petroleum WO & Reported: P. O. Sox 264r, Project Dumber: Natural Healing Center k 10274s Drcun CA. 93457 Project Manager: Clarence Reynolds 05/06/202J 17:25 Ieunrt fc Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by : Lab ID : 2102742-01 Field Data: NA Analvte Result RL Units Dilution Batch Analyzed Method NoEes Lam---- — Volatile Organic Compounds by GC/MS (Continued) HexachlOrobutadiene ND 4-Isopropyl Toluene ND lsopropylbenzene ND Methylene chloride ND Naphthalene ND n-Propylbenzene ND Styrene ND 1.1.1,2-Tetrachloroethane ND 1.1,2,2-Tetrachloroethane ND Torachlon,cthene (10:) ND Toluene ND 1,2,3-Trichlorobcnzcnc ND 1,2,4-Tri ch lorobenzene ND 1,1,1-Trichloroethane ND I,1,2-Trichloroethane ND Trichloroethene (TCE) ND TrichloroflnorOtlrethane ND 1,2.3-Trichloropropane ND 1,2.4-Trimethylbenzene ND 1.3.5-Trimethylbenzene ND Vinyl chloride ND Xylencs (total) ND Surrogate: Uihrorria0h,oron,eth,uae Surrogate. Toluene -de Surrogate: 4-BromoJluuruhen-enr 1.3 mg/kg 1000 B1F0101 05/05/21 16:56 EPA8200B 1.3 1.3 1.3 1.3 1.3 1.3 „ 1.3 „ L3 „ 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 „ 1.3 1.3 95 (74 - 122) " 95 ° ; (65 - 128) 90 (75-121) R-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 37 (imOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Saniples Sample ID : NE Corner Sampled: 05/04/21 14:35 Matrix: Solid Sampled by: Lab ID : 2102742-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mgIg 1 B 1 E0098 05/05/21 12:13 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg(kg 1 B1 F.0102 05/06/21 13:36 EPA 601 OB Arsenic 5.0 1.9 Barium 140 0.94 Beryllium ND 0.47 _ Cadmium ND 0.24 Chromium 160 0.47 " Cobalt 22 0.47 Copper 37 0.94 Lead 6.8 0.47 " Molybdenum 0.51 0.47 Nickel 270 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium 1.7 0.94 " Vanadium 61 1.9 Zinc 59 1.9 Volatile Organic TPH by GC/FID N-02, N-03 N-02 TPH Gasoline (C5-C12) 5.6 4.3 mg/kg 1 B 1 E0095 05/05/21 12:32 EPA 8015M D-04 Surrogate: d-Bromo/Tuoroben_ene 108 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) TP11 Motor Oil (C23-('40) Surrogate: o-Teiyhem'l 310 10 mg1kg I BIE0062 05/05/2121:27 EPA8015M ND 50 " " " 85% (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : NE Corner Sampled : 05/04/21 14:35 Sampled by: Matrix: Solid Field Data: NA Lab ID: 2102742-02 Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 Bl Ii0101 05/05/21 17:24 EPA 8260B Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromotorm ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobcnzenc ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluenc ND 1.2 4-C'hlorotoluene ND 12 Dibromochloromethane ND 1.2 " 1,2-Dibronio-3-chloropropane ND 1.2 1,2-Dibromoethane(EDB) ND 1.2 " Dibromomethane ND 1.2 L2-Dichlorobenzene ND 1.2 " 13-Dichlorobcnzenc ND 1.2 1,4-Dichlorobcnzenc ND 1.2 Dichlorodifluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND L2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 F'.thylbcnzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 37 t� Oilfield Environmental & Compliance, Inc. Pacific Petroleum Califomi-- Project: Pacific Petroleum VrC & Reported: R Q. Box 264 Project Number: Natural Healing Center 2102742 Qrcutt CA. 93457 Project Manager: Clarence Pe"lolds 05/06/2021 11:25 art fc Sample ID: NE Corner Sampled: 05/04/21 14:35 Sampled by: Matrix: Solid Field Data: NA Lab ID : 2102742-02 Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) _ - R-07 11exachlorobutadiene ND 1.2 mg/kg 1000 BIE0101 05/05/21 17:24 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Torachlorocthene (PCi) ND 1.2 " Toluene ND 1.2 1,2,3-Trichlorobcnzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 Trichloro(luoromethane ND 1.2 " 1.2,3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Dihrcmao/luoromc,tllunc 95 % ( 74 - 122) " Surrogate. Toluene-d8 94 $b (65 - 128) " Surrogate: 9-Brun+o1hronncr1r_ene 86 ';4, 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 37 kE2 Pacific Petroleum California P. O. Box.2k4u Orca.tt CA.. 93457 Oilfield Environmental & Compliance, Inc. Project: Pacific Petroleum Project Number: Natural Healing Centel Project Manager: Clarence Reynolds `WO & Reported t102742 05/06/2021 l 7:25 Sampled: 05/04/21 14:40 Sample ID : SW Corner Sampled by Matrix: Solid Field Data: NA Lab ID : 2102742-03 Result RL Units Dilution Batch Analyzed Method Motes Analyte Total Metals by CVAA Total ND 0.093 mg/kg I B I E0099 05/05/21 12:15 EPA 7471 A Mercury Total Metals by ICP Ni) 2.3 mglkg 1 BI E,0102 05/06/21 13:46 EPA 6010B Antimony _ Arsenic 4.5 1.9 Barium 200 0.93 Beryllium ND 0.47 Cadmium NU 0.23 " N-02, Chromium 310 0.47 N-03 Cobalt 55 0.47 Copper 45 0.93 " Lead 9.5 0.47 Molybdenum 0.68 0.47 " " " " N-02 Nickel 430 0.47 " Selenium ND 1.9 Silver ND 0.47 " Thallium NU 0.93 anadiunr 70 1.9 Zinc 69 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (CS-C12) 7.8 5.0 mg'kg I B I E0095 05%05121 12:58 EPA 8015M DJ►4 Smrrugate 4-Brwno luoroben_ene 101 4a (39 - / i 7 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 220 10 mg/kg I BIE0062 05i05121 21:51 EPA 8015M THI Motor Oil (C'23-(-40) NU 50 Surrogate: o-Telphenrl 84 'N, (65- 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California FLAP Certificate # 2438 Client Connect: cllent. oee.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA93454 wvvw.oecusa.com FAX: 805 925-3376 Page 9 of 37 Pacific Petroleum Califonuo Project. Pacific Petroleum WO & Repotteal. P. O box 2646 Project number: Natural Healing Center 21412742 Orcun CA. 93457 project Manager: Clarence Reynolds 05/06/2021 1:25 Analytical Report for Samples Sample ID: SW Corner Sampled: OS/04/21 14:40 Matrix: Solid Sampled by : Lab ID: 2102742-03 Field Data: NA Analvte Resuh R°L Units Dilution Batch Analyzed lAethod Notes Volatile Organic Compounds by GGMS R-07 Benzene ND 1.2 mg/kg 1000 B 1 F0101 05/05/21 17:51 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 ~ tert-Butyl benzene ND 1.2 " Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 " ' Chloroethanc ND 1.2 " Chloroform ND 1.2 Chloromethane ND 1.2 " - 2-Chlorotoluene ND 1.2 " 4-C'hlorutoluene ND 1.2 Dibromochloromethane ND 1.2 " - 1,2-Dibromo-3-chloropropane ND 1.2 " 12-Dibromoethane (EDB) ND 1.2 " Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 12 1,4-Dichloroben7ene ND 1.2 Dichlorodilluoromcihane ND 1.2 " I.1-Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 " _ cis-1.2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane NT) 1.2 " 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 I,1-Dichloropropete ND 1.2 " " cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 F:thylbcnzcnc ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 1 California ELAP Certificate # 2438 Client Connect: client.oec,comlrep•orts TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecrusa.com FAX: 805 925-3376 Page 10 of 37 EEL Oilfield Environmental & Goo lianC8, inn. Pacific Petroleum California Project: ?acifc P'etroleutr, P. O ]sox 2646 Project Number: Natural Healing Centel Orenn CA. 43457 Project Manager. Clarence Reynolds WO & Reporied 110742 0,5/0612021 17:25 Sampled: 05/04/21 14:40 Sample ID : SW Corner Sampled by : Matrix: Solid Field Data: NA Lab ID : 2102742-03 _ f knalyre g Resuli RL units Dilution Batcb A-nalyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1 2 rng/kg Iwo Birmul 0511t5121 17:51 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 12 Methylene chloride ND II Naphthalene ND 1.2 „ n-Propylbenzene ND 1.2 " Styrene ND 1.2 „ 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-1'etrachloroethane ND 1.2 Tetrachlorocthcnc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcnzenc ND 1.2 „ 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (T('E) ND 1.2 Trichlorofluoromethane ND 1.2 „ 1,2,3-Trichloropropane ND 2 1. , 1,2.4-Triniethylbenzcne ND 1.2 " 1.3.5-Trinte1hylbeuzene ND 1.2 " Vinyl chloride ND 1.2 Xylcnes (total) ND 1.2 S„rrogate: 1),hi-oi lOJlnort)n,('lh(,,,i, 93 ' , ( 74 - 122) " Surrogate: Tohtene-dS 94 (65 - 128) " Sunwgalc: 4-Bronx,Jhn,ruhen_e,tc 88 `%b ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client,oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 - - Page 11 of 37 �1 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project dumber: Natural Healing Center 21112742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Report! Analytical Sam Sample ID : SE Corner Sampled: 05/04/21 14:45 P Matrix: Solid Sampled by: Lab ID: 2102742-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B 1 E0098 05/05/21 12:17 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 Bl E0102 05/06/21 13:49 EPA 6010B Arsenic 5.0 1.8 " Barium 180 0.92 " Beryllium ND 0.46 - Cadmium ND 0.23 Chromium 46 0.46 Cobalt 14 0.46 Copper 41 0.92 Lead 13 0.46 Molybdenum ND 0.46 Mickel ^' 85 0.46 " Selenium ND 1.8 Silver ND 0.46 Thallium 1.9 0.92 Vanadium 39 1.8 Zinc 57 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 5.6 4.4 mg/kg 1 B 1 E0095 05/05/21 13:24 EPA 8015M D414 Surrogate: 4-BronuoPuborohenzene 108 �11 (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 190 10 mg/kg I BIE0062 05/05/21 22:15 EPA 8015M LL TP11 Motor Oil (C23-('40) ND 50 1."11" Surrogate: o-Teiphenyl 85 '%L (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 12 of 37 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Sarnples Sample ID : SE Corner Sampled: 05/04/21 14:45 Sampled by : Matrix: Solid Field Data: NA Lab ID: 2102742-04 Analyze Result RL Units Dilution Batch Analyzed Method Alotes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mgtkg 1000 B1E0101 05/05/2118:18 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 ' Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND L2 " tert-Butylbenzene ND 1.2 " Carbon tetrachloride ND 1.2 " C'hlorobenzene ND 1.2 " Chloroethanc ND 1.2 " Chlorofonn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 Dibrumochloromethane ND 1.2 " •-- 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 " Dibromomethatie ND 1.2 _ 1,2-Dichlorobcnzenc ND 1.2 1,3-Dichlorobcnzenc ND 1.2 " 1,4-Dichlorobcnzenc ND 1.2 " Dichloroditluoromethane ND 1.2 " 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 ' cis-1.2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND L2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 " cis-1,3-Dichloropropane ND 1.2 " trans-1,3-Dichlorolwopcne ND 1.2 " Ethylbenzene ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa,com FAX: 805 925-3376 Page 13 of 37 SE2 C Pacific Petroleum California P. Q. Sox 264E Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. Proiect: Pacific Pctroleutn Project lumber: Natural Healing Center Project Manager. Clarence Reyttold5 WC} & Reported: 2W2742 05/06/2021 17:25 Analytical Report for Saniples Sample ID: SE Corner Sampled: 05/04/21 14:45 Sampled by: Matrix: Solid Lab ID : 2102742-04 Field Data: NA Anaiytc Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 B 1 E0101 05/05/21 18:18 EPA 8260B 4-Isopropyl Toluene ND 1.2 " Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 " 1,1,2,2-71'etrachloroethane ND 1.2 Tetrachloroethane (ICE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcnzcne ND 1.2 1,2,4-Trichlorobenzene ND 1.2 " 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Tricliloroethane ND 1.2 " Trichloroethene (TC'E) ND 1.2 Trichlorotluoromethane ND 1.2 1,2,3-Trich)oropropane ND 1.2 " 1,2.4-Trimethylbenzene ND 1.2 " 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 " Xylcncs (total) ND 1.2 Surrogate: Uihrwnujluuru»u t1m»c 98 V. (74 - 122) Surrogate: Toluene-d8 96 . (65 . 128) " Surrogate: 4-8ronm)luorohen_ene 90 Y. ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 or37 0iffield Environmenta.1& C mpliance, inc. Lacific petroleum California Project: Pacific Petroleum WO & Reported: '. O Box 2646 Project number. Natural Healing Center 21(12742 )rcutt CA, 9345-% Project Marvager: Clarence keytboids 05/06/2021 11:25 Sample ID: Center Matrix: Solid Lab ID • 2102742-05 Sampled: 05/04/21 14:50 Sampled by : Field Data: NA Analyte Result PIL 'Unirs Dilution Batch Axmalyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Celbalt Copper Lead 1lfolybdenum Nickel Selenium Silver Thallium Vanadium Zinc Volatile Organic TPH by GOOD TPH Gasoline W5-02) Storogalc: 4-Bromo/hroroben_ene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPII Motor Oil (('23-C40) Surrogate: o-Tc)phenYl — — ND 0.086 mg/kg I BIF0098 05/05/21 12:19 EPA 7471A ND 2.4 mg/kg 1 B I F0102 05/06/21 13:52 EPA 601013 7X 1.9 " 14C 0.96 ND 0.48 ND 0.24 72 0.48 " 22 0.48 " 73 0.96 i5 0.48 " 0.99 0.48 160 0.48 ND 1.9 ND 0.48 1.3 0.96 62 1.9 80 1.9 7.7 4.8 mg/kg I B 1 E0095 05/05/21 13:49 IPA 8015M 106%�, (39-157) 350 10 mg'kg I B 1 E0062 05/05/21 22:38 EPA 8015M ND 50 " 86 Ili, f 65 - 136) „ 11 11 h-02 M( The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comireparts TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecvsa.com FAX: 805 925-3376 Page 15 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: Center Sampled: 05/04/21 14:50 Matrix: Solid Sampled by: Lab ID : 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1-2 mg'kg 1000 BT Eft let 1 i15I05 21 18.40 F I -A 92HIR -, Bromobenzene ND 1.2 " Bromochloromethane ND 12 Bromodichloromethane ND 1.2. Bromoform ND 1.2 " Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzene ND 1.2 Chloroethane ND 1.2 C'hlorofonn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 " Dibromomethane ND 1.2 1,2-Dichtorobenzene ND 1.2 " - 1,3-Dichlorobcnzcnc ND 1.2 " 1,4-Dichlorobcnzcnc ND 1.2 Dichloroditluoromcthanc ND 1.2 " - I,l-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1•2 1,1-Dichloroethene ND 1.2 " - cis-1.2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 " cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 " Ethylbcnzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center :1.02742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: Center Sampled: 05/04/21 14:50 Matrix : Solid Sampled by : Lab ID : 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mgtkg 1000 B 1 E0101 05/05/21 18:46 EPA 9260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 " - Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 " Tctrachlorocthcne 1PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcnzcnc ND 1.2 " 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,12-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1,24-Trimethylbenzene ND 1.2 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 " Surrogate: Dihroniulluoromethanr 94 (74 - 122) Surrogate: Toluenc-dS 95 ;'b (65 • 128) " Surrogate: 4-Bronco/lnw-ohctr_e1'c xn ;<h (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecus.3.com FAX: 805 925-3376 Page 17 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. 0. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Metals ControlTotal by CN7AA - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO098 -EPA 7471A Preparation: EPA 7471A Prep 05/05/21 08:00 Blank (B1E0098-BLK1) Analyzed: 05/05/21 11:40 Mercury ND 0.10 mg/kg LCS (B1E0098-BS1) Analyzed: 05/05/21 11:35 _.. Mercury 0.802 0.10 mg/kg 0.833 96 85-115 LCS Dup (B1E0098-BSD1) Analyzed: 05/05/21 11:37 Mercury 0.931 0.10 mg/kg 0.833 100 85-115 4 20 Duplicate (B1E0098-DUPI) Source: 2102717-01 Analyzed: 05/05/21 11:44 Mercury 0.0262 0.10 mg/kg 0.0394 40 20 QR-04 Matrix Spike (B1E0098-MS1) Source: 2102717-01 Analyzed: 05/05/21 11:46 Mercury 0.836 0.097 mg/kg 0.812 0.0394 98 75-125 Matrix Spike Dup (B1E0098-MSDI) Source: 2102717-01 Analyzed: 05/05/21 11:48 Mercury 0.838 0.098 mg/kg 0.814 0.0394 98 75-125 0.3 20 Post Spike (B1E0098-PS1) Source: 2102717-01 Analyzed: 05/05/21 11:50 Mercury 5.22 ug/L 5.00 0.256 99 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8051925-3376 Page 18 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 8102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BI E0102 -EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 • Blank (BIE0102-BLK1) Analyzed: 05/06/21 13:12 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 r Beryllium ND 0.50 " Cadmium ND 0.25 Chromium ND 0.50 " -- • Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 Molybdenum ND 0.50 Y Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 LCS (B1E0102-BS1) Analyzed: 05/06/21 12:50 Antimony 99.2 2.5 tngAg 100 99 80-120 Arsenic 99.8 2.0 100 100 80-120 Barium 102 1.0 100 102 80-120 Beryllium 96.5 0.50 100 96 80-120 Cadmium 101 0.25 100 101 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 102 0.50 100 102 80-120 Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 98.1 0.50 100 98 90-120 Nickel 102 0.50 100 102 80-120 Selenium 97.7 2.0 100 98 80-120 Silver 4.81 0.50 5.00 96 80-120 Thallium 104 1.0 100 104 80-120 Vanadium 98.6 2.0 100 99 80-120 Zinc 101 2.0 100 101 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 tControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limil Batch BlEO102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 LCS Dup (B1E0102-BSD1) Analyzed: 05/06/21 12:52 Antimony 99.8 2.5 mg/kg 100 100 80-120 0.6 20 Arsenic 102 2.0 100 102 80-120 2 20 Barium 103 1.0 100 103 80-120 1 20 Beryllium 97.2 0.50 100 97 80-120 0.8 20 Cadmium 102 0.25 100 102 80-120 0.9 20 Chromium 103 0.50 100 103 80-120 0.6 20 Cobalt 103 0.50 100 103 80-120 0.6 20 Cropper 103 1.0 100 103 80-120 0.6 20 Lead 103 0.50 100 103 80-120 0.5 20 Molybdenum 99.6 0.50 100 100 80-120 2 20 Nickel 103 0.50 100 103 80-120 0.6 20 Selenium 100 2.0 100 100 80-120 3 20 Silver 4.89 0.50 5.00 98 80-120 2 20 Thallium 105 1.0 100 105 80-120 2 20 Vanadium 98.9 2.0 100 99 80-120 0.4 20 Zinc 102 2.0 100 102 80-120 0.6 20 Duplicate (B1E0102-DUPl) Source: 2102717-02 Analyzed: 05/06/21 13:17 Antimony ND 2.4 mg/kg ND 20 Arsenic 7.55 1.9 " 8.39 10 20 Barium 92.7 0.95 97.2 5 20 Beryllium 0.657 0.48 0.691 5 20 Cadmium ND 0.24 ND 20 Chromium 16.8 0.48 16.2 4 20 Cobalt 7.71 0.48 8.09 5 20 Copper 18.7 0.95 19.7 5 20 Lead 11.1 0.48 11.8 6 20 Molybdenum 1.43 0.48 1.59 10 20 Nickel 22.9 0.48 19.7 15 20 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.95 ND 20 Vanadium 32.2 1.9 32.7 2 20 Zinc 60.1 1.9 64.4 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 .T ,..�..` - - Page 20 of 37 r&wIJL3'wFOI Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 11112742 Orcuti CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Control Analyte Result RL Units Spike Source %REC %REC RFD RPI7 '`'ores Level Result Limits Limit Batch BlE0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Matrix Spike (B1E0102-MS1) Source: 2102717-02 Analyzed: 05/06/21 12:55 Antimony 26.4 2.5 mg/kg 99.2 ND 27 10-116 Arsenic 105 2.0 99.2 8.39 98 77-121 Barium 193 0.99 99.2 97.2 97 30-169 Beryllium 93.0 0.50 99.2 0.69.1 94 86-I11 Cadmium 93.6 0.25 99.2 ND 94 81-112 Chromium 118 0.50 99.2 16.2 103 75-129 Cobalt 102 0.50 99.2 8.09 94 71-121 Copper 119 0.99 99.2 19.7 100 68-135 Lead 105 0.50 99.2 11.8 94 72-121 Molybdenum 89.4 0.50 99.2 1.58 89 70-112 Nickel 114 0.50 99.2 19.7 95 73-121 Selenium 89.8 2.0 99.2 ND 91 76-110 Silver 4.31 0.50 4.96 ND 87 54-132 Thallium 89.0 0.99 99.2 ND 90 64-120 Vanadium 130 2.0 99.2 32.7 98 78-124 Zinc 158 2.0 99.2 64.4 94 50-143 Matrix Spike Dup (B1E0102-MSD1) Source: 210271742 Analyzed: 05/06/21 12:57 Antimony 29.7 2.4 tngIg 94.4 ND 31 10-116 12 20 Arsenic 103 1.9 94.4 8.39 101 77-121 2 20 Barium 182 0.94 94.4 97.2 89 30-169 6 20 Beryllium 91.6 0.47 94.4 0.691 96 86-111 2 20 Cadmium 91.5 0.24 94.4 NI) 97 81-112 2 20 Chromium 113 0.47 94.4 16.2 103 75-129 4 20 Cobalt 99.2 0.47 94.4 8.09 96 71-121 3 20 Copper 114 0.94 94.4 19.7 100 68-135 4 20 Lead 102 0.47 94.4 11.8 96 72-121 3 20 Molybdenum 88.9 0.47 94.4 1.58 92 70-112 0.6 20 Nickel 111 0.47 94.4 19.7 96 73-121 3 20 Selenium 88.7 1 9 94.4 ND 94 76-116 1 20 Silver 4.23 0.47 4.72 ND 90 54-132 2 20 Thallium 87.0 0-94 94.4 ND 92 64-120 2 20 Vanadium 126 1.9 94.4 32.7 98 78-124 4 20 Zinc 153 1.9 94.4 64.4 94 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 37 �1 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum W0 & Reported: P. 0. Box 2646 Prggect Number: Natural Healing Center 2102742 Orcun CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Total Nletals by lCP - Quality Control Analvte Result RL Units Spike Source %REC %REC RPD RPD adores Level Result Limits Limit Batch BlEO102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Post Spike (B1E0102-PS1) Source: 2102717-02 Analyzed: 05/06/21 13:00 Antimony 1.95 mg/L 2.00 -0.0338 98 75-125 Arsenic 2.25 2.00 0.171 104 75-125 Barium 3.97 2.00 1.98 99 75-125 Beryllium 1.97 2.00 0.0141 98 75-125 Cadmium 1.97 2.00 -0.0215 99 75-125 Chromium 2.42 2.00 0.330 104 75-125 Cobalt 2.15 2.00 0.165 99 75-125 Copper 2.51 2.00 0 401 105 75-125 Lead 2.20 2.00 0.240 98 75-125 Molybdenum 2.02 2.00 0.0322 99 75-125 Nickel 2.48 2.00 0.403 104 75-125 Selenium 1.96 2.00 -0.0744 98 75-125 Silver 0.0946 0.100 -0.00744 95 75-125 Thallium 1.88 2.00 -0.0732 94 75-125 Vanadium 2.71 2.00 0.668 102 75-125 Zinc 3.25 2.00 1.31 97 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 22 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported. P O. Box 2646 Project Number: Natural Healing Center 2102742 Orcun CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile1 -Quality Conti-ol Analvte Result RL Units Spike Source %REC %REC RFD RPD Notes Level Result Limits Limit Batch BlE0095 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/05/21 06:24 Blank (B1E0095-BLK1) Analyzed: 05/05/21 09:00 TPH Gasoline (C5-C1.2) ND 0.50 mg/kg Surrogate:4-Bronuq/laorobenzent, 0.134 110.124 108 39-157 LCS (B1E0095-BSI) Analyzed: 05/05/21 08:09 TPH Gasoline (C5-C2) 0.917 0.50 mg/kg 0.992 92 68-139 Sm'rogate•:4-Brcnnol1norobenzene 0.15E 110.124 127 39-157 LCS Dup (BIE0095-BSD1) Analyzed: 05/05/21 08:34 TPH Gasoline (C5-C12) 1.03 0.50 mg/kg 0.994 103 68-139 11 20 Surrogate:4-Bromo/luoruhen_ene 0.157 0.124 127 39-157 Duplicate (B 1 E0095-DUPI) Source: 2102652-01 Analyzed: 05/05/21 09:59 TPH Gasoline (C'5-('12) ND 5.2 mgtkg ND 20 Surrogate: 4-Bromolbtorohenzene 1.30 " 1.30 100 39-157 Matrix Spike (B1E0095-MS1) Source: 2102652-01 Analyzed: 05/05/21 14:41 TPH Gasoline (C'5-C'12) 7.97 4.9 mg/kg 9.80 ND 81 10-171 Surrogate: 4-Bromgflu1•oben_enc, 1.40 111.23 115 .39-157 Matrix Spike Dup (BIE0095-MSD1) Source: 2102652-01 Analyzed: 05/05/21 15:07 TPH Gasoline (C5-('12) 8.18 5.2 mg/kg 10.4 ND 78 10-171 3 20 Surrogate:4-Bromolhuo•obenzene 1.40 1.30 107 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 23 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Proiect: Pacific Petroleum ild() &: Reported: P. O. Sox 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Serni-Volatile Organic TPH by 1 Quality Conti-ol lsnalyte Result RL Units Spike Source %RE(' %REC RPD RPD Notes Level Result Limits Limit Batch BlEO062 -EPA 8015M Preparation: EPA 3550C 05/05/21 10:31 Blank (B1E0062-BLK1) TPH Diesel (C13-('22) TPH Motor Oil (C'23-C40) Surrogate: o-Teiphenrl LCS (B1E0062-BSl) TPH Diesel (C I 3-C22) TPH Motor Oil (('23-C40) Surrogate: o-Teiphenyl LCS Dup (B1E0062-BSDl) TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Teiphetirl Duplicate (B1E0062-DUPl) TPI1 Diesel (C'13-C22) TPH Motor Oil (C'23-C40) Surrogate: o-TeiphetYl Matrix Spike (B1E0062-MS1) TPH Diesel (CI 3-C22) TPH Motor Oil (C'23-C40) Surrogate: o-Teiphenrl Matrix Spike Dup (B1E0062-MSD1) TPH Diesel (('13-C22) TPH Motor Oil (('23-C40) Surrogate: o-Telphem4 ND ND 411 467 433 493 Source: 2102648-01 35.5 71.2 Source: 2102648-01 731 559 Source: 2102648-01 562 485 Analyzed: 05/05/21 17:58 10 mg/kg 50 " 37.8 49.9 Analyzed: 05/05/21 17:12 10 mg/kg 500 50 500 40.0 50.0 Analyzed: 05/05/21 17:35 10 mg/kg 499 50 499 41.1 49.9 Analyzed: 05/05/21 21:27 10 mg/kg 34.6 50 65.4 53.6 49.8 Analyzed: 05/05/21 21:51 10 mg/kg 499 34.6 50 499 65.4 44.1 49.9 Analyzed: 05/05/21 22:15 10 mgtkg 499 34.6 50 499 65.4 41.3 49.9 76 65-136 82 72-115 93 74-126 80 65-136 87 72-115 5 20 99 74-126 6 20 82 65-136 2 20 D-04 8 20 D-04 108 65-136 140 46-147 99 35-171 88 65-136 106 46-147 84 35-171 83 65-136 26 20 QR-02 14 20 The results in this report apply to the samples analyzed in accordance with the chain of custoay aocumenr. this anaryncat report mwi ae repraaucea in a., ea,ur y. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 37 f -m Oilfield Environmental & compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence ReNmolds 05/06/2021 IT25 Volatile Oi-ganic tControl Analyte Result RL Units Spike Source %REC °•oRL---RPD RPD Notes Level Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLKI) Analyzed: 05/05/21 13:17 Benzene ND 0.25 mg/kg Bromobenzene ND 0.25 " Bromochlorontcthane ND 0.25 Brontodichloromethane ND 0.25 Bromoform ND 0.25 Bromomethane NI) 0.25 " n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 " tert-Butylbenzene ND 0.25 " Carbon tetrachloride ND 0.25 Chlorobenzene ND 0.25 Chloroethane ND 0.25 Chloroform ND 0.25 Chloromethane ND 0.25 " 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene ND 0.25 Dibromochloromethane ND 0.25 1,2-Dibromo-3-chloropropane ND 0.25 1,2-Dibromoethane (EDB) ND 0.25 Dibromomcthanc ND 0.25 1,2-r)ichlorobenzene ND 0.25 " 13-Dichlorobenzenc ND 0.25 1,4-Dichlorobenzene ND 0.25 " Dichlorodilluorontcthane ND 0.25 ],1-Dichloroethene ND 0.25 1,2-Dichlorocthane ND 0.25 I,l-Dichloroethene ND 0.25 cis- 1.'_-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 1,2-Dichloropropane ND 025 1,3-Dichloropropane ND 0.25 2.2-Dichloropropane ND 0.25 " 1,1-Dichloropropene ND 0.25 cis-13-Dichloropropene ND 0.25 trans-1,3-Dichloropropene ND 0.25 Ethylbenzene ND 0,25 " Ilexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 Isopropylbenzene ND 0.25 " methylene chloride ND 0.25 " Naphthalene ND 0.25 n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 37 fWAIN--NM ESM P bm 'No Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: R O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatilet Analyte Result RL Units Spike Source %REC 9'oREC RPD RPD Notes Level Result Limits Limit Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLK1) Analyzed: 05/05/21 13:17 Styrene ND 0.25 rig/kg 1, 1, 1,2-Tetrachloroethane NI) 0.25 1,1,2,2-1'ctrachlorocthane ND 0.25 Tetrachloroethene (PCE) NI) 0.25 Toluene ND 0.25 1,2,3-Trichlorobenzene ND 0.25 1,2,4-77iclilorobenzene ND 0.25 " 1, 1, 1 -Trichloroethane NI) 0.25 1,1,2-Trichloroethane ND 0.25 Trichloroethene (TCE) ND 0.25 - Trichlorofluoroniethane NI) 0.25 1,2,3-Trichloropropane ND 0.25 " L2,4-Trinmethylbenzene ND 0.25 1,3,5-Trimethy[benzene ND 0.25 Vinyl chloride ND 0.25 Xylenes (total) ND 0.25 " Surrogate: Uibromo luoromethane 0.0468 0.0496 94 74-122 Surrogate: Toluene-d8 0.0462 " 0.0496 93 65-128 Surrogale:4-Bromo/luorohenzene 0.0431 0.0496 87 75-121 LCS (B1E0101-BS1) Analyzed: 05/05/21 12:22 Benzene 2.30 0.25 nmg/kg 1.99 116 70-131 Brotnobenzene 1.97 0.25 1.99 99 74-130 Bromochloromctlianc 1.95 0.25 1.99 93 64-133 Bromodichloromethane 1.99 0.25 1.99 100 69-137 " Bromoform 1.74 0.25 1.99 88 55-132 Bromomethane 1.64 0.25 1.99 83 10-142 n-Butylbenzene 2.58 0.25 1.99 130 64-156 sec-Butylbenzene 2.53 0.25 1.99 127 75-155 - tert-Butylbenzene 2.32 0.25 1.99 117 74-144 Carbon tetrachloride 2.18 0.25 1.99 110 67-135 Chlorobenzene 2.17 0.25 1.99 109 73-134 -.. Chloroethane 1.83 0.25 1.99 92 10-167 Chloroform 2.13 0.25 1.99 107 69-124 Chloromethane 2.32 0.25 1.99 117 34-136 2-C'hlorotoluene 2.14 0.25 1.99 107 75-135 4-C hlorotoluene 2.14 0.25 1.99 108 70-138 Dibronwchloronmethane 1.99 0.25 1.99 100 67-135 1,2-Dibromo-3-chloropropane 1.99 0.25 1.99 100 41-149 1,2-Dibromoethane (ED13) 1.92 0.25 1.99 97 68-131 Dibroniomcthane 1.48 0.25 1.99 74 61-140 1,2-Dichlorobenzene 2.07 0.25 1.99 104 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 37 Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Oilfield Environmental Project: Pacific Petroleum Project Number: Natural Healing Center Project Manager: Clarence Reynolds & Compliance, Inc. WO & Reported: 2102742 05/06/2021 17:25 fAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS (B1E0101-BS1) Analyzed: 05/05/21 12:22 1,3-Dichlorobenzenc 2.17 0.25 mg!kg 1.99 109 76-138 1,4-Dichlorobenzene 2.14 0.25 1.99 108 72-132 Dichlorodifluoromcthanc 1.31 0.25 1.99 66 10-155 1,1-Dichloroethane 2.33 0.25 1.99 117 63-139 1,2-Dichloroethenc 2.06 0.25 1.99 104 64-126 1, 1 -Dichloroethene 2.77 0.25 1.99 139 52-167 cis-1.2-Dichloroethene 2.07 0.25 1.99 104 70-135 trans- l,2-Diehl oroethene 2.43 0.25 1.99 122 67-147 1.2-Dichloropropane 2.05 0.25 1.99 103 68-131 13-Dichloropropane 2.04 0.25 1.99 103 64-128 2,2-Dichloropropane 2.31 0.25 1.99 116 63-154 1, 1 -Dichloropropene 2.22 0.25 1.99 112 68-138 cis-1,3-Dichloropropene 2.09 0.25 1.99 105 72-134 trans-1,3-Dichloropropene 2.26 0.25 1.99 114 69-132 Ethylbenzene 2.46 0.25 1.99 124 68-136 Hexachlorobutadiene 2.20 0.25 1.99 Ill 72-198 4-Isopropyl Toluene 2.39 0,25 1.99 120 74-150 ` Isopropylbenzene 2.41 0.25 1.99 121 71-149 Methylene chloride 2.57 0.25 1.99 129 51-127 E�'11-05 Naphthalene 1.99 0.25 1.99 100 57-158 n-Propylbenzene 2.27 0.25 1.99 114 70-143 Styrene 2.25 0.25 1.99 113 68-138 1, 1, 1,2-Tetrachloroethane 1.92 0.25 1.99 97 76-130 1,1,2,2-Tetrachlorocthanc 2.09 0.25 1.99 105 60-136 _ Tetrachloroethene (PCE) 2.09 0.25 1.99 105 73-138 Toluene 2.18 0.25 1.99 110 72-128 1,23-Trichlorobenzene 1.74 0.25 1.99 88 61-166 1.2,4-Trichlorobenzene 1.85 0.25 1.99 93 71-158 _ 1, 1, 1 -Trichloroethane 2.24 0.25 1.99 113 71-135 1,1.2-Trichloroethane 2.07 0.25 1.99 104 64-132 Trichloroethene(TCE) 1,92 0.25 1.99 97 74-139 Trichlorofluoromethane 1.74 0.25 1.99 87 30-156 1,2,3-Trichloropropane 2.01 0.25 1.99 101 67-123 1,2A-Trimethylbenzene 2.52 0,25 1,99 127 68-134 1,3,5-Trimethylbenzene 2.37 0.25 1.99 119 71-140 • Vinyl chloride 2.46 0.25 1.99 124 43-144 Xylenes(total) 7.54 0.25 5.96 126 69-138 Surrogate: Dihromollttoromethane 0.0485 0.0497 98 74-1 2 S:o-rogate: Toluene-d8 0.0471 0.0497 95 65-128 Surrogate: 4-Bromo/lunroben_ene 0.0467 0.0497 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatilet i t Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSDI) Analyzed: 05/05/21 12:49 Benzene 2.25 0.25 mg/kg 1.99 113 70-131 2 20 Bromobenzene 1.93 0.25 1.99 97 74-130 2 20 Bromochloronmcthane 1.85 0.25 1.99 93 64-133 0 20 Bromodichloromethane 2.00 0.25 1.99 101 69-137 0.5 20 Bromoform 1.81 0.25 1.99 91 55-132 3 20 Bromomethane 1.48 0.25 1.99 75 10-142 10 20 n-Butylbenzene 2.57 0.25 1.99 129 64-156 0.2 20 see-Butylbenzene 2.51 0.25 1.99 126 75-155 0.8 20 tert-Butylbenzene 2.34 0.25 1.99 118 74-144 1 20 Carbon tetrachloride 2.12 0.25 1.99 107 67-135 3 20 Chlorobenzene 2.20 0.25 1.99 110 73-134 1 20 Chloroethane 1.75 0.25 1.99 88 10-167 4 20 Chloroform 2.10 0.25 1.99 106 69-124 1 20 Chloromethane 2.15 0.25 1.99 108 34-136 8 20 2-Chlorotoluene 2.15 0.25 1,99 108 75-135 0.6 20 4-Chlorotoluene 2.15 0.25 1.99 108 70-138 0.5 20 Dibromochloromethane 1.94 0.25 1.99 98 67-135 2 20 1,2-Dibronmo-3-chloropropane 1.89 0.25 1.99 95 41-149 5 20 1,2-Dibronloethane(EDB) 1.96 0.25 1.99 99 68-131 2 20 Dibromomcthanc 1.52 0.25 1.99 76 61-140 3 20 1,2-Dichlorobenzene 2.12 0.25 1.99 107 76-136 2 20 1,3-Dichlorobenzene 2.17 0.25 1.99 109 76-138 (1 20 1,4-Dichlorobenzene 2.21 0.25 1.99 111 72-132 3 20 Dichloroditluoromcthanc 1.31 0.25 1.99 66 10-155 0.2 20 1,1-Dichloroethane 2.30 0.25 1.99 116 63-139 1 20 1,2-Dichloroethane 2.09 0.25 1.99 105 64-126 2 20 1, 1 -Dichloroethene 2.55 0.25 1.99 128 52-167 8 20 cis-1,2-Dichloroethene 2.01 0.25 1.99 101 70-135 3 20 trans-1,2-Dichloroethene 2.37 0.25 1.99 119 67-147 2 20 1,2-Dichloropropane 2.07 0.25 1.99 104 68-131 0.8 20 1,3-Dichloropropane 2.02 0.25 1.99 102 64-128 1 20 2,2-Dichloropropane 2.25 0.25 1.99 113 63-154 3 20 1,1-Dichloropropene 2.20 0.25 1.99 111 68-138 1 20 cis-1,3-Dichloropropene 2.06 0.25 1.99 103 72-134 2 20 trans-1,3-Dichloropropene 2.25 0.25 1.99 113 69-132 0.8 20 Ethylbenzene 2.47 0.25 1.99 124 68-136 0.2 20 1{exachlorobutadiene 2.25 0.25 1.99 113 72-198 2 20 4-Isopropyl Toluene 2.42 0.25 1.99 122 74-150 1 20 Isopropylbenzene 2.36 0.25 1.99 119 71-149 2 20 Methylene chloride 2.45 0.25 1.99 123 51-127 5 20 Naphthalene 2.00 0.25 1.99 101 57-158 0.9 20 n-Propylbenzene 2.29 0.25 1.99 115 70-143 0.9 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805+ 925-3376 Page 28 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & deported: P. O. Box 2646 Project Dumber: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Oroanic Coinpounds by GC/NIS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0101 -EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSDI) Analyzed: 05/05/21 12:49 Styrene 2.26 0.25 ntg/kg 1.99 114 68-138 0.4 20 1,1,1,2-Tetrachloroethane 1.96 0.25 1.99 99 76-130 2 20 1,1,2,2-1'ctrachloroethane 2.08 0.25 1.99 105 60-136 0.2 20 Tetrachloroethene (PCE) 2.07 0.25 1.99 104 73-138 1 20 Toluene 2.21 0.25 1.99 111 72-128 1 20 1,2,3-Trichlorobenzene 1.87 0.25 1,99 94 61-166 7 20 1,2.4-Trichlorobenzene 1.99 0.25 1.99 95 71-158 2 20 1,1,1-Trichloroethane 2.17 0.25 1.99 109 71-135 3 20 1,1,2-Trichloroethane 2.16 0.25 1.99 108 64-132 4 20 Trichloroethene (TCE) 1.89 0.25 1.99 95 74-139 1 20 - Trichlorotluoromethane 1.58 0.25 1.99 79 30-156 10 20 1,2,3-Trichloropropane 1.90 0.25 1.99 95 67-123 6 20 1,2.4-Trimethylbenzene 2.60 0.25 " 1.99 131 68-134 3 20 1,3,5-Trintethy]benzene 2.38 0.25 1.99 120 71-140 0.6 20 Vinyl chloride 2.27 0.25 1.99 114 43-144 8 20 Xylenes (total) 7.47 0.25 5.96 125 69-139 0.9 20 Surrogate: Dibronu)/luoronrc,that?e 0.0486 0.0497 98 74-122 Surrogate: Toluene-dS 0.0467 0.0497 94 65-128 Snrrogarc:4-Bromo/lnorohen_ene 0.0459 0.0497 92 75-121 Duplicate (BIE0101-DUPl) Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 ' Benzene ND 1.3 mg1kg ND 20 Bromobenzene ND 1.3 " ND 20 Bromochloromcthanc ND 1.3 ND 20 Bromodichloromethane ND 1.3 ND 20 Bnmtoform ND 1.3 " ND 20 Bromomethane ND 1.3 ND 20 n-Butylbenzene ND 1.3 ND 20 _ sec-Butylbenzene ND 1.3 ND 20 tert-Butylbenzene ND 1.3 ND 20 Carbon tetrachloride ND 1.3 ND 20 Chlorobenzene ND 1.3 ND 20 Chloroethane ND 1.3 ND 20 Chlorofomt ND 1 ND 20 C'hloromethane ND 1.3 ND 20 2-Chlorololuene ND 1.3 " ND 20 4-Chlorotoluene ND 1.3 ND 20 Dibromochloromethane ND 1.3 ND 20 1,2-Dibromo-3-chloropropanc ND 1.3 " ND 20 1,2-Dibromoethane (EDB) ND 1.3 ND 20 Dibromomcthanc ND 1.3 ND 20 1,2-Dichlorobenzene ND 1.3 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805,,925-3376 Page 29 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcuti CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatilei Analyze Result RL Units Spike Source %REC °' REC RFD RPD Notes •- • Level Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Duplicate (B1EO101-DUPl) Source: 2102742-OIRE1 Analyzed: 05/05/21 15:07 1,3-Dichlorobenzenc ND 1.3 mg./kg ND 20 1,4-Dichlorobenzene ND 1.3 ND 20 Dichloroditluoromethane ND 1.3 ND 20 " 1,1-Dichloroethane ND 1.3 ND 20 1,2-Dichloroethane ND 1.3 ND 20 LI-Dichloroethene ND 1.3 ND 20 cis -1,2-Dichloroethene ND 1.3 ND 20 trans-1,2-Dichloroethene ND 1.3 ND 20 1,2-Dichloropropane ND 1.3 ND 20 1,3-Dichloropropane ND 1.3 ND 20 • - 2,2-Dichloropropane ND 1.3 ND 20 1,1-Dichloropropene ND 1.3 ND 20 cis- 1 .3 -Dichloropropene ND 1.3 ND 20 trans-1,3-Dichloropropene ND 1.3 ND 20 Ethylbenzene ND 1.3 ND 20 Hexachlombutadiene ND 1.3 ND 20 4-Isopropyl Toluene ND 1.3 ND 20 . Isopropylbenzene ND 1.3 ND 20 Methylene chloride ND 1.3 ND 20 Naphthalene ND 1.3 ND 20 n-Propylbenzene ND 1.3 ND 20 Styrene ND 1.3 ND 20 1, 1, 1,2-Tetrachloroethane ND 1.3 ND 20 1,1,2,2-Tetrachlorocthanc ND 1.3 ND 20 Tetrachloroethene (PCE) ND 1.3 ND 20 Toluene 0.572 1.3 ND 20 A-01 1,2,3-Trichlorobenzene ND 1.3 ND 20 1,24-Trichlorobenzene ND 1.3 ND 20 _ 1, 1, 1 -Trichloroethane ND 1.3 ND 20 1.1.2-Trichloroethane ND 1.3 ND 20 Trichloroethane (TCE) ND 1.3 ND 20 Trichlorofluoromethane ND 1.3 ND 20 1,2,3-Trichloropropane ND 1.3 ND 20 1,2,4-Trimethylbenzene ND 1.3 ND 20 1,3,5-Trimethylbenzenc ND 1.3 ND 20 Vinyl chloride ND 1.3 ND 20 Xylenes (total) ND 1.3 ND 20 Surrogate: Uihromo/luoromethanc 0.0467 0.0502 93 74-122 Surrogate: Touene-d8 0.0475 0.0502 95 65-128 Surogate:4-Bromolluorohen_ene O10442 0.0.502 88 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 37 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatilept Analyte Result RL Units Spike Source DIRE( P.REC RPD RPD Notes Lcvcl Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1) Source: 2102742-02 Analyzed: 05/05/21 20:08 Benzene 11.1 1.3 mg/kg 10.0 ND Ill 37-145 Bromobenzene 9.57 1.3 10.0 NI) 96 29-147 Bromochloromethane 9.29 1.3 10.0 ND 93 40-145 Bromodichloromethane 10.2 1.3 10.0 ND 102 39-153 Bromofonn 9.14 1.3 10.0 ND 91 32-143 Bromomethane 12.1 1.3 10.0 ND 121 10-141 n-Butylbenzene 12.3 1.3 10.0 NI) 123 10-162 sec-Butylbenzene 12.5 1.3 10.0 ND 125 14-168 tert-Butylbenzene 11.8 1.3 10.0 ND 118 21-159 Carbon tetrachloride 10.4 1.3 10.0 ND 104 28-148 Chlorobenzene 10.6 1.3 10.0 NI) 106 32-148 Chloroethane 11.0 1.3 10.0 ND 110 11-106 Chloroform 10.3 1.3 10.0 ND 103 40-139 • - Chloromethane 9.86 1.3 10.0 ND 98 18-135 2-C'hlorotoluene 10.7 1.3 10.0 ND 107 25-151 4-C'hlorotoluene 10.7 1.3 10.0 ND 106 22-150 Dibromochloromethane 9.53 1.3 10.0 NI) 95 40-147 ' 1,2-Dibromo-3-chloropropane 9.97 1.3 10.0 ND 100 25-158 1,2-Dibromoethane (EDB) 9.29 1.3 10.0 ND 93 38-147 Dibronxnncthanc 7.54 1.3 10.0 NI) 75 39-150 1,2-Dichlorobenzene 10.6 1.3 10.0 NI) 106 24-154 1,3-Dichlorobenzene 10.9 1.3 10.0 ND 108 21-153 1,4-Dichlorobenzene 10.6 1.3 10.0 NI) 106 21-146 Dichloroditluoromethane 5,88 1.3 10.0 ND 59 10-149 - 1,1-Dichloroethane 11.2 1.3 10.0 ND 112 34-151 1,2-Dichlorocthanc 10.1 1-3 10.0 NI) 100 40-137 l,l-Dichloroethene 11.8 1.3 10.0 ND 119 21-172 cis-1.2-Dichloroethene 9.65 1.3 10.0 ND 96 38-147 trans- l,2-Dichloroethene 11.3 1.3 10.0 ND 112 30-160 1,2-Dichloropropane 10.4 1.3 10.0 NI) 104 39-146 1,3-Dichloropropane 10.2 1.3 10.0 ND 102 39-141 • 2.2-Dichloropropane 9.32 1.3 10.0 NI) 93 26-149 1, 1 -Dichloropropene 10.7 1.3 10.0 ND 106 28-150 cis-1,3-Dichloropropene 9.97 1.3 10.0 ND 100 34-149 trans-1,3-Dichloropropene 10.7 1.3 10.0 ND 107 3b-143 I'Ihvlbenzene 11.5 1.3 10.0 ND 115 23-150 Ilexachlorobutadiene 11.1 1.3 10.0 ND 111 10-192 4-Isopropyl Toluene 11.7 1.3 10-0 ND 117 11-165 lsopropylbenzene 11.2 1.3 10.0 NI) 112 17-166 Methylene chloride 12.0 1.3 10.0 ND 120 28-135 Naphthalene 12.0 1.3 10.0 ND 120 10-174 n-Propylbenzene 11.3 1.3 10.0 ND 113 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Dumber: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Compounds by GUMS - Quality Conti-ol Analyte Result R1. Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1) Source: 2102742-02 Analyzed: 05/05/21 20:08 Styrene 10.8 1.3 ntgrkg 10.0 ND 108 24-154 1, 1, 1,2-Tetrachloroethane 9.48 1.3 10.0 ND 95 38-149 1,1,2,2-1'ctrachloroethanc 11.0 1.3 10.0 ND 110 22-164 Tetrachloroelhene(PCE) 9.82 1.3 10.0 ND 98 25-153 Toluene 10.7 1.3 10.0 ND 107 26-149 1,2,3-Trichlorobenzene 10.2 1.3 10.0 ND 101 10-163 1,2,4-Trielilorobenzene 9.87 1.3 10.0 ND 99 10-162 1, 1, 1 -Trichloroethane 10.6 1.3 10.0 ND 106 34-149 1,1.2-Trichloroethane 9.74 1.3 10.0 ND 97 25-175 Trichloroethene (TCE) 9,32 1.3 10.0 ND 93 25-170 Trichlorofluorontethane 10.8 1.3 10.0 ND 107 19-155 1,2,3-Trichloropropane 10.3 1.3 10.0 ND 103 32-165 1,2,4-Trimethylbenzene 12.6 1.3 10.0 ND 126 15-150 1,3.5-Trimethylbenzene 11.7 1.3 10.0 ND 117 10-158 Vinyl chloride 10.9 1.3 10.0 ND 108 22-148 Xylenes (total) 35.6 1.3 30.1 ND 118 22-153 Surrogate. DibrornoJluoromrthane 0.0473 0.0501 94 74-122 ` Surrogate: Toluene-d8 0.0469 0.0501 94 65-128 Surrogalec 4-Br•omnJluorohen_ene 0.0453 0.0501 90 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 37 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil list EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP Total Metals by CVAA - Mercury Total EPA 7471A EPA 7471 A Solid OEC, CA -FLAP Total Metals by ICP 6010E Total Antimony EPA 6010B Solid OFC. CA -FLAP 6010E Total Arsenic EPA 601013 Solid OF.C, CA -FLAP 6010B Total Barium EPA 601013 Solid OEC, CA -FLAP 6010B Total Beryllium EPA 601013 Solid OEC. CA -FLAP 6010B Total Cadmium EPA 6010E Solid OFC, CA -FLAP 6010B Total Chromium EPA 001013 Solid OFC, CA -FLAP 6010B Total Cobalt EPA 6010B Solid OEC, CA-ELAP 6010B Total Copper EPA 601013 Solid OFC. CA-ELAP 6010B Total Lead EPA 6010E Solid OEC. CA -FLAP 6010B Total Molybdenum EPA 60108 Solid OEC, ('A-ELAP 6010B Total Nickel FPA 6010B Solid OFC, CA -FLAP 6010E Total Selenium EPA 6010E Solid OFC, CA -FLAP 601013 Total Silver EPA 6010B Solid OEC. CA -FLAP 6010B Total Thallium EPA 601013 Solid OEC. CA-ELAP 60108 Total Vanadium EPA 601pB Solid OEC. CA -FLAP 6010E Total 'Zinc EPA 6010E Solid OFC, CA -FLAP Volatile Organic Compounds by GUMS 8260B Full List EPA 820013 Solid OEC. CA-ELAP Volatile Organic TPH by GC/FID 8015 TPI1-Gasoline EPA 8015M Solid OFC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OFC. Internal 8015 TPH-Gasoline EPA 8015M Solid OE(', CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.com\repL TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Notes and Definitions Qualifier Definition MD1. Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference A-01 Potential carryover from previous high leveled sample. D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. QM -OR The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out -Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 34 of 37 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0511.D Operator BNT Acquired 5 May 2021 12:06 pm using AcgMethod GASBTEXE.M Instrument GC7 `- Sample Name: 2102742-01@ Misc Info : 1@B1E0095 GRO SO Vial Number: 11 Response_ 85000 80000 75000 60000 55000 50000� 45000 40000 35000 _ . 30000 25000 20000 15000 G0ME0511.D1FIDIA I4 `I li' 10000 l' l 5000 1`+. tiroY, ..T-j ..� Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0512.D Operator BNT Acquired 5 May 2021 12:32 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-02@ Misc Info : 1@B1E0095 GRO SO Vial Number: 12 GOME0512.D\FID1A 6.00 7. 0 8.00 9.00 10f00 11.00 12.00 13.00 14.00 File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0513.D Operator BNT Acquired 5 May 2021 12:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-03@ Misc Info : 1@B1E0095 GRO SO Vial Number: 13 G0ME0513.D\FID1A 95000 15000 10000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7 i T T 8.00 9.00 1 ul� ).00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0514.D Operator BNT Acquired 5 May 2021 1:24 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-04@ Misc Info : 1@B1E0095 GRO SO Vial Number: 14 GOME0514.D\FID1A 80000 35000 15000 10000 Rnnn Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0515.D Operator BNT Acquired 5 May 2021 1:49 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-05@ Misc Info : 1@B1E0095 GRO SO Vial Number: 15 Response_ GOME0515.D\FID1A 85000 65000 60000 55000 50000 30000 20000 15000 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7 00 8.00 9.00 V V� T _ - rr7-rn�Tr�r-".r- 1.00 11.00 12.00 13.00 14.00 H U 0 LL t0 N O O W O m (n U 0 x a H 0 4 4J N U Q � � -rl N 03 LO �3 CD W x X a O N W e-i io / G' O r O N N W LO LO .--I o •• PQ LO I— CTJ O O r-1 / O r-1 -i I N N N >H O Lo -V N ri [l / V ] L U O • • '.R: I r-I CJ l0 >C P'Lo Nr-1N +J f, 0 aro0'Q O N C�l n n n +Ju�lmHz (D o 0 0 0 ro -ri Sa r 1 c + +i + N S4 ":' 4J i�+ U r-I 0 0 a 0 a+i r-iNm U)m -ri ¢ U t~ ro •H w L*,OrC1�cn > 0 0 0 0 0 0 0 o ) 0 0 0 CD 0 0 0 m 000 r O ;o M 1 � fM O M 1r O � �M M _ 5 N o M o ri ` o _ m N C o cq � O n N 4 I O co N O N N O 'a N O M N O N N _O N O _o N 0 0 0 0 0 0 0 0 0 0 0 0 co w a M N — CN E U d 0 0 LO C) O W a O m �-+ C O ri (n U r-I O ac a p O N U p b� 1~ M Ul to O W � a O N [Q O 110 / (M O rI O N I- W In N .-I O •• m Lr) 0) CJ� O O N / O r-1 r-1 I N N N >-I O In a' Q N /u)Ln(4o X Pi L) Nr-1M .. .. .. .. .. 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N Q - a0o rl N C� to M � to O F O fD s1 N O Ln N pCl A 1.0 / •• O O ri O O N r-I W N CD P� N —4 GSJ O. O N N / O O N r-i N I N N Ilr >1 to a' 0 r.0 roar O U N N / if] U O 3Ln r-A C--)00OR I O r. ro O S� + O N E C�l F n n n n n n 0 0 0 0 0 0 0 O 0 O 0 O J-) S4 H U H •Z. N O O O O O O O + 0 O 0 O 0 O 0 O 0 O 0 0 0 0 (0-H �4 N 5 J R U H c + + a)m + + a> + d m o 0 0 0 0 o O o 0 I-i b" U)to ro C r r- r 0) (00 0 inCOD 00 Cl)O N 0 E -ri P4 U r- ro •rl •,-{ N 0 F. M. O . N W5 O O O LO O O O O O rn O (O V `c} O V a O M O N V O d O V U i rn Q Cl) CR LL_ M O O n M W 0 c Cl) a C) O x � Cl) O a F' Ci ri O 4-) o b Cl) o Cl) U O rn CDU1 N d' 'a O Lr) O O rz N Wx. Q O n O 00 N N (M �o / O O r I O O (O N I W (V In r I O pq o LO .--I E) N O N 07 / O O O rl N I N N nj >4 >1LO� ro r Ci /In (7O N to r-I (--)0 O ie O 0 N r-I C N N J-) N C (0 O N �4 d)zw f; 0 0) E r f n n n n n n O O O o O 0 Cl 0 O 0 O 0 0 0 O O O J-) F4 �l H Z N O O + O + O + O O O + + O O O O O O O O Cl ro .,� �.{ ,.1 C + d y m d d d o o O o o O o O o N sa �+.� �v-4 a `- 0 0 0 0 0 0 0 0 0 -q t rn ro M 00 n CO U) 'IT M N �_ •ri i� U C, ro •ri -.-I N F Cv09 tr I N G m X (O LL.. •� L6 N V4)L. o ymQ0 •V �� o O.Q.V a Q1 CAcc C F m )� () co N 0 m SZ O F m C _tea T � 4 mn.v = ov m t 0 SPIIOS Pa-MOSIC) 11401 AIMS0u0O Me VMS 8Od 1 Igad A!IlgRIu81 OORS-53OAS W908 OWOD • dHl aP01nS IaplunAo anp320a Isll lhd 808Z8 %roan • ZZ WILL O m � a CL = Fo co C oa 0 0O m C a � 33 zv t(❑ x A .'i O N a R po M GN C 2 co N ❑ ❑ Q a ^ 70 Q m a A IN t E 7 / § 9. a 2 0 ■ w ■ M-2� § & e zz \ k k ! \ HN { \ 5 � r- U) k E 2 � E / k k O o � \ / § k 16 k d k \ } E Q. \ ƒ # 0 \ - = t » f 3 § 2 £ CD$ 2 k ƒ } J goo 0 E / ƒ $ 7 D G�A_- § ƒ « # v 0 A k ) E o ■ v 0 3 § k k k 0 ■ ■ ■ ■ : ■ 71179-1]■E Aa » + 2 / A� / a , + . E # E CD c a : f\ x c )$E�19< q e- C2E" _ § _ { Q m = 2 J @ 200 k E$ k D ® E Q -a & 4 = e 6 0$ a- a o k% 7 ] E1EkI 0 < ofƒ d 2 w w ■ O 0 O O n■ O G � \ & \ « 7 q § 2 @ n U N N V N O N C N E E O m c —LLkLL 0 Uw nU N 1 N N N a` c v v 'o v v v v o v o U) o cn z U 0 0 (1) 0 U) 0 0 0 N 0 c c c c c Y Y Y Y Y co � W O O) "O Orn 'O m '0 m m m O) � V :O V � '� :O '0 = LL LL LL LL LL LL LL LL LL LL c 0 a .c Q Q Q Q Q C N N ow tll O N O N N O N 0 fN0 N 0 J U� J 0N [CE , I O O Eu N U N N N N �U c 0 0" Q m N N v 0 0 0 0 0 C¢7 0 MM 0 0 v 0 LO 0 0 m m d c O U > X n Fe f- r" 7 P" I 11 Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2102508 Pacific Petroleum California P. O. Box 2646 Report Date: May 03, 2021 16:36 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 23, 2021 13:40 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: &MMAZ Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page I of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bin 2094-A 2102508-01 Solid Solid 04/23/2021 11:00 04/23/2021 13:40 Bin 2094-B 2102508-02 Solid Solid 04/23/2021 11:05 04/23/2021 13:40 Bin 2094-C 2102508-03 Solid Solid 04/23/2021 11:10 04/23/2021 13:40 Bin 20340-A 2102508-04 Solid Solid 04/23/2021 11:15 04/23/2021 13:40 Bin 20340-B 2102508-05 Solid Solid 04/23/2021 11:20 04/23/2021 13:40 Bin 20340-C 2102508-06 Solid Solid 04/23/2021 11:25 04/23/2021 13:40 Bin 20158-A 2102508-07 Solid Solid 04/23/2021 11:30 04/23/2021 13:40 Bin 20158-B 2102508-08 Solid Solid 04/23/2021 11:35 04/23/2021 13:40 Bin 20158-C 2102508-09 Solid Solid 04/23/2021 11:40 04/23/2021 13:40 Bin 2088-A 2102508-10 Solid Solid 04/23/2021 11:45 04/23/2021 13:40 Bin 2088-B 2102508-11 Solid Solid 04/23/2021 11:50 04/23/2021 13:40 Bin 2088-C 2102508-12 Solid Solid 04/23/2021 11:55 04/23/2021 13:40 Bin 20376-A 2102508-13 Solid Solid 04/23/2021 12:00 04/23/2021 13:40 Bin 20376-B 2102508-14 Solid Solid 04/23/2021 12:05 04/23/2021 13:40 Bin 20376-C 2102508-15 Solid Solid 04/23/2021 12:10 04/23/2021 13:40 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 SampleBatch Preparation Analysis Batch ID Preparation Date/Time *** DEFAULT GENERAL METHOD *** Asbestos Bulk PLM-(non-soil& Asphalt)(sub) OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/F1D 8015 Diesel & Motor Oil List BID0766 04/27/2021 07:10 STLC Metals by ICP 6010B STLC B I D0916 04/30/2021 10:33 STLC Metals Extraction STLC Metals Extraction B1D0838 04/28/2021 12:44 TCLP Metals by ICP 6010B TCLP B I D0919 04/30/2021 10:49 TCLP Metals Extraction TCLP Metals Extraction B 1 D0839 04/28/2021 12:48 Total Metals by CVAA Mercury Total EPA 747] A B 1 D0711 04/26/2021 09:00 Total Metals by ICP 601 OB Total B 1 D07 34 04/26/2021 07:37 Volatile Organic Compounds by GUMS 8260B Full List BID0650 04/23/2021 12:11 Volatile Organic TPH by GC/F1D 8015 TPI ]-Gasoline B 1 D0692 04/23/2021 14:16 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.095 0.094 mg/kg 1 B 1 D0711 04/26/21 14:53 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 D0734 04/26/21 13:51 EPA 6010B Arsenic 7.4 L9 Barium 690 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 64 0.48 Cobalt 14 0.48 _-• Copper 260 0.97 Lead 2400 0.48 Molvbdenum 2.0 0.48 Nickel 94 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 31 1.9 Zinc 1300 1.9 STLC Metals by ICP Chromium 0.28 0.10 mg/L 2 B1 D0916 05/03/21 12:58 STI.C/EPA 6010B Copper 1.6 0.111 TCLP Metals by ICP Lead 2.0 0.050 mg/l. 1 BID0919 0510312114:09 EPA 1311/F.PA6010B N-02 N-02 N-01, N-03 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.9 mg!kg 1 B1D0692 04/23/21 14:32 EPA 8015M R-07 Surrogate: 4-Bromof7imroben:ene 94 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID - TPH Diesel (CI3-C22) ND 10 nig/kg 1 BID0766 04/27/21 15:24 EPA 8015M TPH Motor Oil (C23-C40) 97 50 Surrogate: o-Teiphenvl 84 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID : 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 0.051 mg/kg 1 BID0650 04/23/21 17:17 EPA8260B Bromobenzene ND 0.051 Broniochloromethane ND 0.051 Bromodichloromethane ND 0.051 Bromoform ND 0.051 Bromontethane ND 0.051 n-Butylbenzene ND 0.051 sec-Butylbenzene ND 0.051 tert-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobenzenc ND 0.051 r' Chloroethane ND 0.051 Chloroform ND 0.051 " Chloroniethane ND 0.051 -� 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND 0.051 Dibromochloromethane ND 0.051 12-Dibromo-3-chloropropane ND 0.051 1,2-Dibromoethane (EDB) ND 0.051 Dibromomethane ND 0.051 1,2-Dichlorobenzene ND 0.051 1,3-Dichlorobenzenc ND 0.051 1,4-Dicblorobenzenc ND 0.051 Dichlorodifluoromethane ND 0.051 - ' 1, 1 -Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 1,1-Dichloroethene ND 0.051 cis-1,2-Dichloroethene ND 0.051 trans-1,2-Dichloroethene ND 0.051 1,2-Dichloropropane ND 0.051 1,3-Dichloropropane ND 0.051 22-Dichloropropane ND 0.051 1,1-Dichloropropene ND 0.051 cis-1.3-Dichloropropene ND 0.051 trans-1,3-Dichloropropene ND 0.051 Ethylbenzene ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-A Sampled : 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID : 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 ]lexachlorobutadiene ND 0.051 mg/kg 1 B1D0650 04/23/21 17:17 EPA 8260B 4-Isopropyl Toluene ND 0.051 [sopropylbenzene ND 0.051 Methylene chloride ND 0.051 Naphthalene ND 0.051 " n-Propylbenzene ND 0.051 Stvrene ND 0.051 1,1,1,2-I'etrachloroethane ND 0.051 1.1.2,2-I'etrachloroethane ND 0.051 Tctrachlorocthcnc (PCE) ND 0.051 Tolucnc ND 0.051 1.2,3-Trichlorobenzene ND 0.051 1,2,4-Trichlorobenzene ND 0.051 I,1,1-Trichloroethane ND 0.051 1,1,2-Tricliloroetliane ND 0.051 Trichloroethene (TCE) ND 0.051 Trichlorolluoromelhane ND 0.051 12,3-Trichloropropane ND 0.051 " 1,2,4-Trimethylbenzene ND 0.051 1,3,5-1'rimethylbenzene ND 0.051 Vinyl chloride ND 0.051 Xylcncs (total) ND 0.051 Surrogate: Dibronagtlnoroniedranr 98 % (74 - 122) Surrogate: Toluene-dS 95 % ( 65 - 12S ) Surrogate: 4-Brcnnulluorobc•n_ene 89 IN, ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mglkg 1 B1D0711 04/26/21 15:02 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg Arsenic 7.6 1.9 Barium 220 0.97 " Beryllium ND 0.49 " _ Cadmium ND 0.24 " Chromium 100 0.49 " Cobalt 15 0.48 Copper 61 0.97 " Lead 320 0.48 " _ Molybdenum 1.6 0.48 " Nickel 130 0.48 " Selenium NI) 1.9 " Silver ND 0.48 " Thallium ND 0.97 " Vanadium 38 1.9 " Zinc 410 1.9 STLC Metals by ICP 1 B 1 D0734 04/26/21 13:54 EPA 6010B N-02, N-03 N-02. N-03 Chromium 0.29 0.10 mg/L 2 BID0916 0510312113:00 STLC/EPA601013 Lead 20 0.I0 " " " " " N-07 TCLP Metals by ICP t nrommni Lead ND 0.050 mg/L 1 BID0919 05/03/2114:26 EPA 1311/EPA6010B 0.31 0.050 " " " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.8 mg/kg 1 B1 D0692 04/23/21 14:58 EPA 8015M R-07 Surrogate. 4-Bromo/luorobenzene 99 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (CO-C22) 16 10 mg/kg 1 BID0766 04/27/21 15:24 EPA 8015M D-06 TPH Motor Oil (C23-C40) 150 50 Surrogate: o-Teiphenil 80 % (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.049 mg/kg 1 BID0650 04/23/21 17:45 EPA8260B "- Bromobenzene ND 0.049 Bromocliloromethane ND 0.049 Bromodichloroinethane ND 0.049 Bromoform ND 0.049 Bromomethane ND 0.049 n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 Carbon tetrachloride ND 0.049 Chlorobenzcne ND 0.049 Chloroethanc ND 0.049 Chloroform ND 0.049 Chloromethane ND 0.049 2-Chlorotoluene ND 0.049 4-Chlorotoluene ND 0.049 Dibromochloromethane ND 0.049 " 1.2-Dibromo-3-chloropropane ND 0.049 " 1,2-Dibromoethane (EDB) ND 0.049 Dibromomethane ND 0.049 " 1,2-Dichlorobenzene ND 0.049 13-Dichlorobcnzcne ND 0.049 I A-Dichlorobcnzcne ND 0.049 Dichlorodilluoromethane ND 0.049 " - 1,1-Dichloroethane ND 0.049 1,2-Dichloroethane ND 0.049 LI-Dichloroethene ND 0.049 cis-1,2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 1.2-Dichloropropane ND 0.049 1,3-Dichloropropane ND 0.049 2,2-Dichloropropane ND 0.049 1,1-Dichloropropene ND 0.049 cis- 1.3-Dichloropropene ND 0.049 trans-1,3-Dichloropropene ND 0.049 Etylbenzene ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.049 mglkg 1 BID0650 04/23/21 17:45 EPA 8260B 4-Isopropyl Toluene ND 0.049 Isopropylbenzene ND 0.049 " Methylene chloride ND 0.049 " Naphthalene ND 0.049 n-Propylbenzene ND 0.049 Styrene ND 0.049 1,1,1,2-Tetrachloroethane ND 0.049 1.1,2,2-Tetrachloroethane ND 0.049 Tctrachlorocthenc (PCE) ND 0.049 Toluene ND 0.049 1,2,3-Trichlorobenzene ND 0.049 1,2,4-Trichlorobenzene ND 0.049 1, 1, 1 -Trichloroethane ND 0.049 — 1,1,2-Trichloroethane ND 0.049 " Trichloroethene (TCE) ND 0.049 " Trichlorofluoromethane ND 0.049 " 1,2.3-Trichloropropane ND 0.049 1,2,4-Trimethylbenzene ND 0.049 1,3.5-Trimethylbenzene ND 0.049 Vinyl chloride ND 0.049 Xylencs (total) ND 0.049 " Surrogate: Dibromollnoromethane: 95 % ( 74 - 122) " Surrogate: Toluene-dg 96 % (65 -1_8 ) Surrogate. 4-Bromolluorohen_ene 90 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page I of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report t Sample ID: Bin 2094-C Sampled: 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID: 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercuri 0.17 0.098 mg/kg 1 B1D0711 04/26/2115:04 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 Bl D0734 04/26/21 14:05 EPA 601 OB Arsenic 7.7 2.0 Barium 280 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 52 0.50 N-02 Cobalt 10 0.50 Copper 79 1.0 Lead 270 0.50 " " " " N-02, N-03 Molvbdenum 1.1 0.50 Nickel 69 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 34 2.0 Zinc 370 2.0 STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 B 1 D0916 05/03/21 13:03 STLC/F.PA 601 OB Lead 22 I1.10 " " " " " N-07 TCLP Metals by ICP Lead 0.11 0.050 mg/I. 1 B 1 D0919 05/03/21 14:29 EPA 13111EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 12 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled: 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.8 mg/kg 1 BID0692 04/23/21 15:24 EPA 8015M R-07 Surrogate: 4-Bromq/luorohen<-ene 93 '% (39 - 157) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 BID0766 04/27/21 15:47 EPA 8015M TPH Motor Oil (C23-C40) 220 50 Surrogate: o-TeirhenYl 79 % (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID: 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R Benzene ND 0.049 mgtkg 1 BID0650 04/23/21 18:12 EPA8260B Bromobenzene ND 0.049 Bromochloromethane ND 0.049 Bromodichloromethane ND 0.049 " Bromofonn ND 0.049 Bromomethane ND 0.049 " n-Butylbenzene ND 0.049 " sec-Butylbenzene � ND 0.049 tert-Butylbenzene ND 0.049 Carbon tetrachloride ND 0.049 Chlorobcnzenc ND 0.049 Chlorocthanc ND 0.049 Chloroform ND 0.049 " Chloromethane ND 0.049 2-Chlorotoluene ND 0.049 4-C'hlorotoluene ND 0.049 Dibromochloromethanc ND 0.049 12-Dibronio-3-chloropropane ND 0.049 1,2-Dibromoetliane (LDB) ND 0.049 " Dibromomethauie ND 0.049 " 1.2-Dichlorobenzene ND 0.049 - 1,3-Dichlorobcnzcnc ND 0.049 IA-Dichlorobcnzcnc ND 0.049 D1ChIOTodifluoromethane ND 0.049 I,1-Dichloroethane ND 0.049 1,2-Dicliloroethane ND 0.049 1,1-Dichloroethene ND 0.049 cis- 1.2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 1,2-Dichloropropane ND 0.049 1,3-Dichloropropane ND 0.049 2,2-Dichloropropane ND 0.049 1, 1 -Dichloropropene ND 0.049 cis- 1.3 -Dichloropropene ND 0.049 trans- l,3-Dichloropropene ND 0.049 Ethylbenzene ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 - Page 14 of 94 W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 llexachlorobutadiene ND 0.049 mg/kg 1 BID0650 04/23/2118:12 EPA8260B 4-Isopropyl Toluene ND 0.049 Isopropylbenzene ND 0.049 Methylene chloride ND 0.049 Naphthalene ND 0.049 n-Propylbenzene ND 0.049 " Styrene ND 0.049 1, 1, 1,2-Tetrachloroethane ND 0.049 1,1,2,2-Tetrachloroethane ND 0.049 Tetraehlorocthcne (PCE) ND 0.049 Toluene ND 0.049 1,2,3-Trichlorobenzene ND 0.049 1,2,4-Trichlorobenzene ND 0.049 1,1,1-Triehloroethane ND 0.049 1,1,2-Triehloroethane ND 0.049 Triehloroethene (TCE) ND 0.049 Trichlorotluoromethane ND 0.049 " 1,2,3-Trieliloropropane ND 0.049 1,2.4-Trimethylbenzene ND 0.049 1,3,5-1'rimethylbenzene ND 0.049 Vinyl chloride ND 0.049 Xylenes (total) ND 0.049 Surrogate: Dihromolluoromethane 97 ON (74 - 12 2 ) Surrogate Toluene-dS 96 ( 65 - 128) Surrogate: 4-Bronwlhtorohen_ene 92 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.13 0.087 mg/kg 1 B 1 D0711 04/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:07 EPA 6010B Arsenic 7.3 2.0 Barium 230 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 58 0.49 N-02 Cobalt 12 0.49 _ Copper 63 0.98 Lead 390 0.49 " " " " " N-02, N-03 111olvbdenum 2.1 0.49 Nickel 69 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 35 2.0 " Zinc 530 2.0 STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 BID0916 05/03/21 13:05 STLC/EPA6010B Lead 14 O.11l " " " " " N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/L 1 B 1 D0919 05/03/21 14:31 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GOOD TPH Gasoline (('5-('12) ND 5.2 mg/kg I BID0692 04/23/21 15:50 EPA 8015M R-07 Surrogate: 4-Bromu/hn>roben_ene 99 %, (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (CI3-C22) ND 10 mg/kg 1 BID0766 04/27/21 15:47 EPA 8015M TPH Motor Oil (C23-C40) 170 50 Surrogate: o-Teiphenrl 86 `%f, (65 - 136) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805, 925-3376 Page 17 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.051 mg/kg 1 B1D0650 04/23/21 18:40 EPA9260B ' Bmmobenzene ND 0.051 Broniochloromethane ND 0.051 Bromodichloromethane ND 0.051 Bromoform ND 0,051 Bromomethane ND 0.051 n-Butvlbenzene ND 0.051 sec-Butylbenzene ND 0.051 tort-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobenzcne ND 0.051 Chloroethane ND 0.051 Chloroform ND 0.051 Chloromethane ND 0.051 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND 0.051 Dibromochloromethane ND 0.051 12-Dibromo-3-chloropropane ND 0.051 1,2-Dibromoethane (EDB) ND 0.051 " Dibromomethane ND 0,051 1,2-Dichlorobenzene ND 0.051 1,3-Dich1orobcnzcnc ND 0.051 1,4-Dichlorobenzenc ND 0.051 Dichloroditluoromethane ND 0.051 1, 1 -Dichloroetbane ND 0.051 1,2-Dichloroethene ND 0.051 1,1-Dichloroethene ND 0.051 cis-1,2-Dichloroethene ND 0.051 " trans- I .2-Dichloroethene ND 0.051 " 12-Dichloropropane ND 0.051 l3-Dichlorolnopane ND 0.051 22-Dichloropropane ND 0.051 1. 1 -Dichloropropene ND 0.051 cis- I3-Dichloropropcnc ND 0.051 trans-1,3-Dichloropropcnc ND 0.051 Ethylbenzcne ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 I Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.051 mg!kg 1 BID0650 04/23/21 18:40 EPA8260B 4-Isopropyl Toluene ND 0.051 Isopropylbenzene ND 0.051 Methylene chloride ND 0.051 Naphthalene ND 0.051 n-Propylbenzene ND 0.051 " Styrene ND 0.051 1,1.1,2-Tetrachloroethane ND 0.051 1.12,2- Tetrachloroethane ND 0.051 Tctrachlorocthcnc (PCE) ND 0.051 Toluene ND 0.051 1,2,3-Trichlorobenzene ND 0.051 1,2,4-Trichlorobenzene ND 0.051 1, 1, 1 -Trichloroethane ND 0.051 1,1,2-Trichloroethane ND 0.051 Trichloroethene (TCE) ND 0.051 Trichlorofluoromethane ND 0.051 " 1.2,3-Trichloropropane ND 0.051 " 1,2.4-Trimethylbenzene ND 0.051 1,35-Trimethylbenzene ND 0.051 Vinyl chloride ND 0.051 Xylencs (total) ND 0.051 Surrogate: Dihranglluoromedtmrc 98 °n ( 74- 122) Surrogate: Toluene-dS 97 % ( 65 - 128 ) " Surrogate: 4-Bromulhnn•uhen_cne 92 in (75. 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by : Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mcrcury 0.095 0.091 mg/kg 1 BID0711 04/26/21 15:08 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg I B 1D0734 04/26/21 14:10 EPA 6010B Arsenic 10 2.0 Barium 240 0.98 Bervllium ND 0.49 Cadmium ND 0.25 " Chromium 50 0.49 N-02 Cobalt 11 0.49 Copper 54 0.98 Lead 800 0.49 " " " " N-02, N-03 MoNlidenum 0.77 0.49 Nickel 79 0.49 Selenium ND 2.0 Silvcr ND 0.49 Thallium ND 0.98 " Vanadium 37 2.0 Zinc 350 2.0 STLC Metals by ICP Chromium 0.29 0.10 mg/L 2 B1 D0910 05/03/21 13:08 STLC/EPA 6010B _.. Lead 120 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.23 0.050 mg/I_ 1 B 1 D0919 05/03/21 14:34 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 _ www.oecusa.com FAX: 805 925-3376 Page 20 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by : Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mg/kg I BID0692 04/23/21 16:16 EPA 8015M R-07 Surrogate 4-Bromolluorobenzene 99 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 37 10 mg/kg I BID0766 04/27/21 16:09 EPA 8015M D-06 TPH Motor Oil (C23-C40) 280 50 Surrogate: o-TeiphenYl 86 % (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.047 mg/kg 1 BID0650 04/23/21 19:07 EPA8260B Broniobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromoform ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzcne ND 0.047 " Chloroethane ND 0.047 Chlorotorm ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 " 4-C'hlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibronno-3-chloropropane ND 0.047 " 1,2-Dibromoethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobenzcne ND 0.047 1,4-Dichlorobcnzene ND 0.047 Dichloroditluoromethanc ND 0.047 " 1,1-Dichloroethene ND 0.047 1,2-Dichloroetliane ND 0.047 1,1-Dichloroethene ND 0.047 " cis-1,2-Dichloroethene ND 0.047 " trans-1,2-Dichloroethene ND 0.047 " 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 2.2-Dichloropropane ND 0.047 1. 1 -Dichloropropene ND 0.047 cis- 1.3-Dichloropropene ND 0.047 - trans-l.3-Dichloropropene ND 0.047 " Ethylbcnzene ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID : Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID: 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7Notes Volatile Organic Compounds by GUMS (Continued) R-07 Flexachlorobutadiene ND 0.047 mg/kg 1 B1D0650 04/23/21 19:07 EPA 8260B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 - Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1, 1, 1,2-Tetrachloroethane ' ND 0.047 1.1,2,2-Tetrachloroethane ND 0.047 Tetrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzenc ND 0.047 1,2A-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 - 1,1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 1,2,3-Trichloropropane ND 0.047 12,4-Triniethylbenzene ND 0.047 1,3.5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 Xylencs (total) ND 0.047 Surrogate. 1.)ibronrol7troronretlrunc 93 `/ (74. 122 ) Surrogate: Toluene-dS 96 %, (65 • 128) " ~ Surrogate: 4-Bromofluorobeu_ene 91 N, ( 75 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 23 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 BID0711 04/26/2115:10 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1 D0734 04/26/21 14:13 EPA 6010B Arsenic 11 2.0 Barium 340 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 50 0.49 N-02 Cobalt 14 0.49 Copper 230 0.99 Lead 1200 0.49 " " " " N-01, N-03 Molybdenum 1.7 0.49 Nickel 73 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 32 2.0 Zinc 1000 2.0 STLC Metals by ICP Chromium 032 0.10 mg/L 2 BID0916 05/0312113:11 STLC/EPA6010B TCLP Metals by 1CP Lead 0.84 0.050 mgil. 1 B 1 D0919 05/03/21 14:36 EPA 1311 /F..PA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID: 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mg/kg 1 BID0692 04/23/21 16:42 EPA 8015M R-07 ^ Surrogate: 4-BromnJluoroben_ene 96 (39 - 157 ) Semi -Volatile Organic TPH by GC/FID _. TPH Diesel (C13-C22) 29 10 mg,kg 1 BID0766 04/27/21 16:09 EPA 8015M D-06 TP11 Motor oil (C23-C40) 150 50 Surrogate: o-kiphemd 83 % (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-C Sampled : 04/23/21 11:25 Matrix: Solid Sampled by : Lab ID: 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.050 mg/kg 1 B1D0650 04/23/21 19:35 EPA9200B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 " Bromodichloromethane ND 0.050 Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 " Carbon tetrachloride ND 0.050 Chlorobenzenc ND 0.050 Chlorocthane ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 " 4-Chlorotoluene ND 0.050 Dibromochloromethane ND 0.050 1.2-Dibromo-3-chloropropane ND 0.050 12-Dibronioethane (EDB) ND 0.050 Dibromomethane ND 0.050 " 1,2-Dichlorobenzene ND 0.050 " 1,3-Dichlorobenzene ND 0.050 1,4-Dichlorobenzene ND 0.050 Dichloroditluoromethanc ND 0.050 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 1,1-Dichloroethene ND 0.050 " cis-1.2-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 " 1.3-Dichloropropane ND 0.050 2.2-Dichloropropane ND 0.050 1.1-Dichloropropeue ND 0.050 cis- 1.3-Dichloropropane ND 0.050 trans-1,3-Dichloropropanc ND 0.050 Ethylbenzene ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com PAX: 605 925-3376 Page 26 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.050 mg/kg 1 BID0650 04/23/21 19:35 EPA8260B 4-Isopropyl Toluene ND 0.050 lsopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Piopylbenzene ND 0.050 Styrene ND 0.050 1,1,1,2=letrachloroethane ND 0.050 1.1,2,2-Tetrachloroethane ND 0.050 Torachloroethene (PCE) ND 0.050 " Toluene ND 0.050 1,2,3-Trichlorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1,1,1-Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorofluoromethane ND 0.050 1,2.3-Trichloropropane ND 0.050 1.24-Trimethylbenzene ND 0.050 1,3.5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Dibromofluoromethmrc, 98 Y. (74 - 122 ) Surrogate: Toluene-d8 95 % ( 65 - 128 ) Surrogate: 90 % (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 8( 05j 925-3376 Page 27 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: R O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.092 mg/kg l B 1 D0711 04/26/21 15:12 EPA 7471 A Total Metals by ICP Antimony 5.9 2.5 mg./kg 1 B 1 D0734 04/26/21 14:16 EPA 601 OB Arsenic 8.5 2.0 Barium 260 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 65 0.49 N-02 Cobalt 11 0.49 Copper 77 0.98 Lead 530 0.49 N-02. N-03 Molybdenum 1.2 0.49 Nickel 91 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 34 2.0 Zinc 780 2.0 STLC Metals by ICP Chromium 0.59 0.10 mg/L 2 B1D0916 05/03/2113:21 STLC/EPA 601 OB Lead 17 0.10 " " " " " N-m TCLP Metals by ICP Lead 0.12 0.050 mg/L I BID0919 05/03/21 14:39 EPA 1311 /EPA 60 1 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 28 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by : Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND Surrogate: 4-BromO/lnorohen ene Semi -Volatile Organic TPH by GC/FID 5.1 mg/kg 1 BID0692 04/23/21 17:08 EPA 8015M R-07 98 % (39 - 157) 11 " 11 TPH Diesel (C13-C22) 38 10 TPH Motor Oil (C23-C40) 150 50 Srn•rogate: o-kiphenyl 86 mg/kg I B 1 D0766 04/27/21 16:32 EPA 8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 29 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID: 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mglkg 1 B 1 D0650 04/23/21 20:02 EPA 8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 Bromoform ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzenc ND 0.045 Chlorocthanc ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 " Dibromochloromethane ND 0.045 " 1,2-Dibromo-3-chloropropane ND 0.045 1.2-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobenzcnc ND 0.045 1,4-I)iclilorobcnzcnc ND 0.045 Dichloroditluoronuthane ND 0.045 l,l-Dichlomethane ND 0.045 1,2-Dichloroethene ND 0.045 1, 1 -Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1.2-Dichloropropane NI) 0.045 1,3-Dichloropropane ND 0.045 22-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis-1.3-Dichloropropene ND 0.045 " trans-1,3-Dichloropropene ND 0.045 " Ethylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples Sample ID : Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg/kg 1 BID0650 04/23/2120:02 EPA8260B 4-Isopropyl Toluene ND 0.045 lsopropylbenzene ND 0.045 " Methylene chloride ND 0.045 Naphthalene ND 0.045 " n-Propylbenzene ND 0.045 Styrene ND 0.045 1.1,1,2-1'etrachloroethane ND 0.045 " 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachloroethene (PCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzcne ND 0.045 1,2,4-Trichlorobenzene ND 0.045 " LI.I-Trichloroethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethane (TCE) ND 0.045 " Triehlorolluoromethane ND 0.045 " 1,2.3-Trichloropropane ND 0.045 1,2,4-1'rimethylbenzene ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylencs (total) ND 0.045 Surrogate. Dibromolluoromethane 96 IN, (74 - 122 ) Surrogate. Toluene-dS 97 % (65- 128 ) Surrogate: 4-Bromo/luoroben_ene 93 ° , (75 - 127 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Nlcrcur� 0.12 0.090 mg/kg 1 BID0711 04/26/21 15:14 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1 D0734 04/26/21 14:19 EPA 6010B Arsenic 6.5 2.0 Barium 270 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 86 0.49 N-02 Cobalt 25 0.49 _ Copper 60 0.99 Lead 190 0.49 " " " " " N-02, N-03 N1olvbdenum 1.0 0.49 " Nickel 170 0.49 Selenium ND 2.0 Silvcr ND 0.49 Thallium ND 0.99 Vanadium 35 2.0 Zinc 380 2.0 STLC Metals by ICP Chromium 0.34 0.10 mg/L 2 B 1 D0916 05/03/21 13:23 STLC/EPA 6010B Lead 13 0.10 N-07 TCLP Metals by ICP Lead 0.29 0.050 nig/l. 1 B I D0919 05/03/21 14:41 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by : Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 5.0 mg/kg 1 B1D0692 04/23/21 17:34 EPA 8015M R-07 Surrogate: 4-Bromolluorohenrene 89 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 93 40 mg/kg 4 BID0766 04/28/21 15:31 EPA 8015M D-06 1'P11 Motor Oil (C23-C40) 320 200 '. Surrogate: o-TeiphenYl 84 % (65 - 136) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.047 mgIg 1 B1D0650 04/23/2120:30 EPA8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromoform ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 " tert-Butylbenzene ND 0.047 Carbon tetrachloride NI) 0.047 Chlorobenzene ND 0.047 " Chloroethane ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 ' _.. 2-Chlorotoluene ND 0.047 4-C'hlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane NI) 0.047 1,2-Dibrotnoethane (FDB) ND 0.047 Dibrontomethane ND 0.047 1,2-Dichlorobenzene NI) 0.047 1.3-Dichlorobenzene ND 0.047 1,4-Dichlorobenzene ND 0,047 Dichlorodifluoronicthane NI) 0.047 -- 1,1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 ],I-Dichloroethene ND 0.047 cis-1,2-Dichloroethene ND 0.047 " trans-1,2-Dichloroethene ND 0.047 12-Dichloropropane ND 0.047 13-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1,1-Dichloropropene ND 0.047 cis- 1,3-Dichloropropene ND 0.047 ' trans-1,3-Dichloropropene ND 0.047 " Ethylbenzene NI) 0.047 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805, 925-3376 Page 34 o f 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.047 mg/kg 1 BID0650 04/23/2120:30 EPA826013 ^ 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1, 1, 1,2-Tetrachloroethane ND 0.047 1,1,2,2'Tetrachloroethane ND 0.047 Tctrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 T 1,2,3-Trichlorobenzene ND 0.047 1,2,4-Trichloroben7ene ND 0.047 " 1,1,1-Trichloroethane ND 0.047 —. 1,1,2-Tricliloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 " Trichlorofluoromethane ND 0.047 1,2,3-Trichloropropane ND 0.047 1,2,4-Trimethylbenzene ND 0.047 " 1,3,5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 ' Xylencs (total) ND 0,047 Surrogate: Dihrc»noflunr<»netGane 95 ' o ( 74 - 122 ) Surrogate: Toluene-d8 96 / ( 65 - 128 ) Surrogate: 4-Bromo. luorobenccne 87 % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 e Page 35 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mgtkg 1 B I D0711 04/26/21 15:16 ITA 7471 A Total Metals by ICP Antimonc 38 2.5 mg/kg I Bl D0734 04/26/21 14:22 EPA 6010B Arsenic 13 2.0 Barium 610 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 63 0.49 N-02 Cobalt 19 0.49 Copper 78 0.99 Lead 8000 49 100 04/26/2114:50 N-01, N-03 111olvbdenum 1.8 0.49 1 04/26/21 14:22 Nickel 110 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 39 2.0 Zinc 2100 2.0 STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 B 1 D0916 05/03/21 13:26 STI.C/EPA 6010B TCLP Metals by ICP Lead 0.054 0.050 mg/L 1 B 1 D0919 05/03/21 14:44 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report foi- Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by : Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FED TPH Gasoline (C5-C12) ND 5.0 mg/kg I BID0692 04/23/21 18:00 EPA 8015M R-07 Surrogate: 4-Bromof&rorohenzene 97 /, (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 39 10 mg/kg 1 B1D0766 04/27/21 16:32 EPA 8015M D-06 TPH Motor Oil (C23-C40) 110 50 11 11 11" 11 Surrogate. o-Terphentd 75 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID: 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.052 mgtkg 1 BID0650 04/23/2123:41 EPA8260B Bromobenzene ND 0.052 Bronrochloromethane ND 0.052 Bromodichloromethane ND 0.052 Bromoforn ND 0.052 Bromomethane ND 0.052 n-Butylbenzene ND 0.052 sec-Butylbenzene ND 0.052 tert-Butylbenzene ND 0.052 Carbon tetrachloride ND 0.052 Chlorobenzcne ND 0.052 Chloroethanc ND 0.052 Chloroform ND 0.052 Chloronuthane ND 0.052 " 2-Chlorotoluene ND 0.052 4-Chlorotoluene ND 0.052 Dibromochloromethane ND 0.052 1,2-Dibromo-3-chloropropane ND 0.052 1,2-Dibrontoethane (EDB) ND 0.052 " Dibrotnomethane ND 0.052 " 1,2-Dichlorobenzene ND 0.052 1.3-Dichlorobenzene ND 0.052 1,4-Dichlorobenzene ND 0.052 Dichlorodifluoromethanc ND 0.052 1, 1 -Dichloroethane ND 0.052 1,2-Dichloroethane ND 0.052 " 1, 1 -Dichloroethene ND 0.052 cis-1,2-Dichloroethene ND 0.052 trans-1,2-Dichloroethene ND 0.052 1,2-Dichloropropane ND 0.052 1,3-Dichloropropane ND 0.052 2,2-Dichloropropane ND 0.052 1, 1 -Dichloropropene ND 0.052 cis- 1.3-Dichloropropane ND 0.052 trans-1,3-Dichloropropanc ND 0.052 Fthylbcnzene ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID: 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Hexachlorobutadiene ND 0.052 mg/kg 1 BID0650 04/23/2123:41 EPA8260B `^ 4-Isopropyl Toluene ND 0.052 Isopmpylbenzene ND 0.052 Methylene chloride ND 0.052 Naphthalene ND 0.052 n-Propylbenzene ND 0.052 Styrene ND 0.052 1. 1, 1,2-Tetrachloroethane ND 0.052 1,1,2.2-Tetrachloroethane ND 0.052 Tetrachloroethene (PCE) ND 0.052 Toluene ND 0.052 1,2,3-Trichlorobenzenc ND 0.052 1,24-Trichlorobenzene ND 0.052 1,1,1-Trichloroethane ND 0.052 • — 1,1,2-Trichloroethane ND 0.052 Trichloroethene (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 1.2,3-Trichloropropane ND 0.052 L2.4-Trintethylbenzene ND 0.052 1,3,5-Triniethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylencs (total) ND 0.052 Surrogate: Dlhrolnoiluoromethane 97 ",o ( 74. 122) Surrogate: Tohrene-d8 97 % 7 (65— 8) L Surrogate: 4-Broinolluoroben_ene 91 `% (75- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: ,f 805) 925-3376 Page 39 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 I Analytical Report for Samples Sample ID : Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID : 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Dlercurc 0.19 0.088 mg/kg 1 BID0711 04/26/21 15:18 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I D0734 04/26/21 14:25 EPA 601 OB Arsenic 9.0 2.0 " Barium 380 1.0 Beryllium ND 0.50 Cadmium 1.3 0.25 Chromium 44 0.50 Cobalt 13 0.50 " Copper 36 1.0 Lead 360 0.50 N-02, N-03 blohbdenum 0.73 0.50 Nickel 71 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND L() Vanadium 35 2.0 Zinc 780 2.0 STLC Metals by ICP Lead 12 0.10 mg/L 2 B 1 D0916 05/03/21 13:29 STLC/EPA 601 OB N-07 TCLP Metals by ICP Lead 0.092 0.050 mg/L I B1D0919 05/03/2114:46 EPA 1311 /EPA 60 1 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 4.6 mgtkg 1 BID0692 04/23/21 18:26 EPA 8015M R-07 - ' Surrogate: 4-BromoJluorobenzene 98 % (39 - 157) Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 21 10 mg/kg 1 BID0766 04/27/21 16:54 EPA 8015M D-06 TPH )Motor Oil (C23-C40) 140 50 Surrogate: o-Teiphenrl 80 Y. (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.oecusa.com FAX: 805 925-3376 Page 41 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID : 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 0.052 mg/kg 1 B l D0650 04/24/21 00:08 EPA 8260B Bromobenzene ND 0.052 Bromochloromethane ND 0.052 " Bromodichloromethane ND 0.052 " r Bromofonn ND 0.052 Bronuomethane ND 0.052 n-Butylbenzene ND 0.052 sec-Butylbenzene ND 0.052 .-- tert-Butylbenzene ND 0.052 " Carbon tetrachloride ND 0.052 " Chlorobenzenc ND 0.052 " Chlorocthane ND 0.052 Chloroform ND 0.052 Chloromethane ND 0.052 --• 2-Chlorotoluene ND 0.052 4-Chlorotoluene ND 0.052 " Dibromochloromethane ND 0.052 " 1,2-Dibromo-3-chloropropane ND 0.052 " 1,2-Dibromoethane (EDB) ND 0.052 Dibromomethane ND 0.052 " 1,2-Dichlorobenzene ND 0.052 " 13-Dichlorobenzcnc ND 0.052 " 1,4-Dich1orobenzcnc ND 0.052 " Dichlorodifluoromcthane ND 0.052 - 1,1-Dichloroethane ND 0.052 " 1,2-Dichloroethane ND 0.052 1, 1 -Dichloroethene ND 0.052 cis-1,2-Dichloroethene ND 0.052 " trans-1,2-Dichloroethene ND 0.052 12-Dichloropropane ND 0.052 " 13-Dichloropropane ND 0.052 " r 22-Dichloropropane ND 0.052 " 1,1-Dichloropropene ND 0.052 cis-1.3-Dichloropropene ND 0.052 trans-1,3-Dichloropropene ND 0.052 Ethylbcnzenc ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 1-lexachlorobutadiene ND 0.052 mgtkg 1 BID0650 04/24/2100:08 EPA8200B 4-Isopropyl Toluene ND 0.052 Isopropylbenzene ND 0.052 " Methylene chloride ND 0.052 " Naphthalene ND 0.052 n-Propylbenzene ND 0.052 Styrene ND 0.052 1, 1. 1,2-Tetrachloroethane ND 0.052 1,1,22-Tetrachloroethane ND 0.052 Tetrachloroethcne (PCE) ND 0.052 Toluene ND 0.052 1,2,3-Trichlorobenzene ND 0.052 1,2,4-Trichlorobenzene ND 0.052 1,1,1-Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 " Trichloroethane (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 1,2,3-Trichloropropane ND 0.052 1,2,4-Trinethylbenzene ND 0.052 " 1,3,5-Trimethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylenes (total) ND 0.052 Surrogate: Dibromglzuoromethane 97 %, (74 - 122) " Surrogate: Toluene-dS 96'X, ( 65 - 124 ) Surrogate: 4-BromoJluoroben_ene 90 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 43 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID : 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.11 0.099 mg./kg 1 BID0711 04/26/21 15:20 EPA 747]A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B1D0734 04/26/2114:28 EPA 6010B Arsenic 15 2.0 Barium 270 0.98 Beryllium ND 0.49 Cadmium 1.4 0.25 Chromium 130 0.49 N-02, N-03 Cobalt 16 0.49 Copper 68 0.98 Lead 440 0.49 " " " " N-02, N-03 Molybdenum 1.2 0.49 Nickel 120 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 38 2.0 " Zinc 1400 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/L 2 BID0916 05/03/21 13:31 STLC/EPA6010B Lead 14 0.10 " " " " " N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B1 D0919 05/03/21 14:49 EPA 1311/EPA 6010B Lead 0.27 0.050 " " " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 44 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPFl Gasoline (C5-C12) ND 4.6 mg/kg 1 BID0692 04/23/21 20:35 EPA 8015M R-07 Surrogate: 4-Bronwjluorobenzene 97 % (39 - 157) " Semi -Volatile Organic TPH by GOOD TPH Diesel (03-C22) 17 10 mg/kg 1 B1D0766 04/27/21 16:54 EPA 8015M D-06 TPH Motor Oil (C23-C40) 87 50 11 11 11" 11 Sm-rogate: o-Teiphe?td 74 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 45 of 94 J Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R4i7 Benzene ND 0.045 mg./kg 1 BID0650 04/24/2100:35 EPA8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 " . Broniolorm ND 0.045 " Bromomethane ND 0.045 " n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 " Chlorocthanc ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 .� 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 12-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 " 1.2-Dichlorobenzene ND 0.045 1,3-Dichloroben7ene ND 0.045 1,4-Dichlorobenzene ND 0.045 Dichlorodifluoromcthanc ND 0.045 1,1-Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 LI-Dichloroethene ND 0.045 cis-1,2-Dichloroethene IND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 " 1,3-Dichloropropane ND 0.045 22-Dichloropropane ND 0.045 1,1-Dichloropropane ND 0.045 cis-1,3-Dichloropropcnc ND 0.045 ' trans-1,3-Dichloropropcnc ND 0.045 Etylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 46 of 94 7 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 2088-B Sampled : 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GONIS (Continued) R-07 Ilexachlorobutadiene ND 0.045 mg/kg l BID0650 04/24/2100:35 EPA8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene ND 0.045 " Styrene ND 0.045 I.1,1.2-Tetrachloroethane ND 0.045 1.1,2,2=retrachloroethane ND 0.045 Tetrachlorocthene (PCE) ND 0.045 Toluene ND 0,045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1, 1, 1 -Trichloroethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 Trichlorofluoromethane ND 0.045 1,2,3-Trichloropropane ND 0.045 1,2,4-Trimethylbenzene ND 0.045 13.5-Trimethylbenzene ND 0.045 " Vinyl chloride ND 0.045 Xylencs (total) ND 0.045 Surrogate. Dihromgflnorwnethcrnc 97 % ( 74 - 122 ) Surrogate: Toluene-dS 95 % ( 65 - 128) Surrogate: 4-Bromo/luor(,ben_ene 90 IN, ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Saniples Sample ID : Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by: Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.096 mgtkg 1 BID0711 04/26/21 15:30 EPA 7471A Antimony ND 2.5 mg/kg 1 BID0734 04/26/21 14:31 EPA 6010B Arsenic 13 2.0 Barium 300 0.99 Beryllium ND 0.49 _ Cadmium 19 0.25 N-02 Chromium 56 0.49 " " " " " N-02 Cobalt 17 0.49 _. Copper 1100 0.99 " " " " " N-02 Lead 390 0.49 " " " " " N-02, N-03 lllolvbdenum 1.1 0.49 Nickel 100 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 34 2.0 Zinc 660 2.0 STLC Metals by ICP Cadmium 0.088 0.050 mg/L 2 B1D0916 05/03/21 13:34 STLC/EPA6010B - Chromium 0.24 0.10 "11" " " Copper 0.69 0.10 Lead 10 0.10 " " " " " N-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 48 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes TCLP Metals by ICP Lead 0.085 0.050 mg/I_ 1 B I D0919 05/03/21 14:59 EPA 1311 /EPA 601(1B Volatile Organic TPH by GC/FID TPI1 Gasoline W5-C12) ND 4.8 mg/kg I BID0692 04/23/21 21:01 EPA 8015M R-07 Surrogate: 4-Bromofluorobcn�ene 96 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 20 10 ing/kg 1 B1D0766 04/27/21 17:17 EPA 8015M D-06 TPH Motor Oil (C23-C40) 130 50 Surrogate: o-Tetphen.14 78 % (65 - 136) 11 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cI!ent.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 49 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Volatile Organic Compounds by GOMS Notes R-07 ND 0.045 mglkg 1 BID0650 04/2412101:02 EPA8260B Benzene Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 " Bromoform ND 0.045 Bromomethane ND 0.045 " n-Butylbenzene ND (1.045 , sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetracliloridc ND 0.045 " Chlorobenzene ND 0.045 " Chloroethane ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromelhane ND 0.045 " 1.2-Dibromo-3-chloropropane ND 0.045 " 1,2-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 12-Dichlorobcnzene ND 0.045 1,3-Dichlorobcnzenc ND 0.045 1,4-Dichlorobcnzenc ND 0.045 Dichlorodifluoromethanc ND 0.045 1,1-Dichloroethene ND 0.045 1,2-Dichloroetliane ND 0.045 1, 1 -Dichloroethene ND 0.045 cis- l2-Dichlorocthene ND 0.045 " trans- l,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 " 1,3-Dichloropropane ND 0.045 2,2-Dichloropropane ND 0.045 1,1-1)ichloropropene ND 0.045 " " cis- 1.3-Dichloropropenc ND 0.045 trans- l,3-Dichloropropenc ND 0,045 E,thylbenzenc ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 of 94 I (.- �a Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexaclilorobutadiene ND 0.045 mg!kg 1 B1D0650 04/24/21 01:02 EPA 8260B 4-Isopropyl Toluene ND 0.045 Isopropylbeuzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene ND 0.045 " Styrene ND 0.045 1. 1, 1,2-Tetrachloroethane ND 0.045 ~ 1.1,2,2-Tetrachloroethane ND 0.045 " Tetrachloroethcne iPCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1,1,1-Trichloroethane ND 0.045 -• 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 Trichlorotluoromethane ND 0.045 1,2,3-Trichloropropane ND 0.045 L2,4-Trimethylbenzene ND 0.045 1,3.5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylencs (total) ND 0.045 Surrogate: Uibromglhtoromethonc 95 %, (74 - 122) Surrogate: Toluene-dS 98 3=0 (65 - 128 ) Surrogate: 4-Brwnofhu robeu_ene SS % (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 51 of 94 Oilfield Environmental & Compliance, Inc. ?acific Petroleum California Project: Pacific Petroleum WO & Reported: O. Box 2646 Project Number: Natural Healing Center 2102508 )rcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample ID : Bin 20376-A Sampled: 04/23/21 12:00 Sampled by : Matrix: Solid Field Data: NA Lab ID : 2102508-13 Anall to Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA ND 0.091 mglkg 1 BID0711 04/26/21 15:32 EPA 7471A Mercury Total Metals by ICP ND 2.5 mg/kg 1 B 1 D0734 04/26/21 14:41 EPA 601(1B Antimony Arsenic 7.0 2.0 Barium 360 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 48 0.50 Cobalt 10 0.50 Copper 620 1.0 " " " " " N-02 Lead 940 0.50 " " N-02, N-03 Molybdenum 1.4 0.50 " Nickel 66 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 34 2.0 " Zinc 610 2.0 STLC Metals by ICP 2.4 0.10 mg/L 2 BID0916 05/0312113:36 STLC/EPA6010B Copper Lead 51 0.10 " " " " " N-07 TCLP Metals by ICP 4.7 0.050 mg/L 1 B1D0919 05/03/2115:01 EPA 1311/EPA6010B Lead The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805� 925-3376 Page 52 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.2 mg,'kg 1 B1D0692 04/23/21 21:27 EPA 8015M R-07 Sun-ogate.4-Broniglhiorohenzene 92'% (39-157) Semi -Volatile Organic TPH by GC/FID TPH Diesel(C13-C22) 12 10 nig/kg 1 BID0766 04/27/21 17:17 EPA8015M D-06 TPII Motor Oil (C23-C40) 67 50 Surrogate: o-kiphenyl 73 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 WWW.oecusa_coili FAX: 805 925-3376 Page 53 of94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kg 1 B1D0650 04/24/2101:29 EPA8260B Bromobenzene ND 0.050 " Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 " Bromoform ND 0.050 " Bromomethane ND 0.050 n-Butylbenzene ND 0.050 " sec-Butylbenzene ND 0.050 " tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 " Chlorobenzene ND 0.050 Chloroethane ND 0.050 " Chloroform ND 0.050 " Chloromethane ND 0.050 " 2-Chlorotoluene ND 0.050 4-Chlorotoluene ND 0.050 " Dibromochloromethane ND 0.050 1,2-Dibronio-3-chloropropane ND 0.050 " 1,2-Dibromoethane (EDB) ND 0.050 " Dibromomethane ND 0.050 L2-Dichlorobenzene ND 0.050 " 1,3-Dichlorobenzenc ND 0.050 " 1,4-Dichlorobenzenc ND 0.050 " Dichlorodifluoromethane ND 0.050 " 1,1-Dichloroethane ND 0.050 " 1,2-Dichloroethane ND 0.050 " 1,1-Dichloroethene ND 0.050 " _ cis- I .2-Dichloroethene ND 0.050 " trans- l,2-Dichi oroethene ND 0.050 " 1,2-Dichloropropane ND 0.050 " 13-Dichloropropane ND 0.050 22-Dichloroln-opane ND 0.050 " 1,1-Dichloropropene ND 0.050 " cis- 1.3-Dichloropropene ND 0,050 trans-1,3-Dichloropropene ND 0.050 " Ethylbcnzenc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 54 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report foi- Samples Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 0.050 mg/kg 1 BID0650 04/24/2101:29 EPA8200B ` 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 —. Naphthalene ND 0.050 " n-Propylbenzene ND 0.050 Styrene ND 0.050 1,1,1,2-T'etrachloroethane ND 0.050 1,1.2,2-1'etrachlorocthane ND 0.050 Tetrachlorocthene(PCE) ND 0.050 Toluene ND 0.050 " 1,2,3-Trichlorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 " Trichlorofluoromethane ND 0.050 1,2,3-Trichloropropane ND 0.050 1,2,4-Trimethylbenzene ND 0.050 1,3,5-Trimethylbenzene ND 0.050 " Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Dihroingtlnoromethonc 96 io (74 - 122 ) Surrogate: Toluene-dS 96 % ( 65 - 12,4) Surrogate: 4-Bro1nuJluorahen_ene 89 ro (75_ 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 55 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.20 0.097 mg/kg 1 B1D0711 04/26/21 15:34 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg I B 1 D0734 04/26/21 14:44 EPA 6010B Arsenic 6.7 2.0 Barium 440 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 73 0.50 N-02 Cobalt 9.4 0.50 " Copper 57 0.99 Lead 2000 0.50 N-01 N-03 Molybdenum 2.5 0.50 Nickel 68 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 30 2.0 " Zinc 770 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/L 2 B1 D0916 05/03/21 13:39 STLC/EPA 6010B TCLP Metals by ICP Lead 0.99 0.050 mg/L 1 B 1 D0919 05/03/21 15:04 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 56 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 20376-B Sampled: 04/23/21 12.05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.1 mg!kg 1 BID0692 04/23/21 21:53 EPA 8015M R-07 Surrogate: 4-BromofluorohensC17e 96 'X, (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 B1D0766 04/28/21 15:08 EPA 8015M TPH Motor Oil (C23-C40) 64 50 Surrogate: o-TeiphenTl 79 "',, (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 57 of 94 r A &W TAM�Lm" Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg/hg t BI D0650 04/24/21 01:57 EPA 8260B Bromobenzene ND 0.047 " Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromoforrn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0047 tert-Butylbenzene ND 0.047 Carbon tetrachloridc ND 0.047 C hlorobenzene ND 0.047 Chloroethanc ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1.2-Dibromo-3-chloropropane ND 0.047 1,2-Dibronioethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobcnzcnc ND 0.047 1,4-Dichlorobcnzcnc ND 0.047 " Dichlorodifluoromcthane ND 0.047 1, 1 -Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 cis-1.2-Dichloroethene ND 0,047 " trans-1,2-Dichloroethene ND 0.047 " 1,2-Dichloropropane ND 0.047 " 13-Dichloropropane ND 0.047 2.2-Dichloropropane ND 0,047 1,1-Dichloropropene ND 0.047 " cis-1.3-Dichloropropanc ND 0.047 trans-1,3-Dichloropropene ND 0.047 Ethylbcnzene ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 58 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Ilexachlorobutadiene ND 0.047 mgtkg 1 B1 D0650 04/24/21 01:57 EPA 8260B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 " Styrene ND 0.047 1, 1, 1,2-Tetrachloroethane ND 0.047 1,1,2,2-Tetrachloroethane ND 0.047 Tetrachloroethenc WCE.) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzcnc ND 0.047 1,2,4-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 " 1,12-Trichloroethane ND 0.047 Trichloroethane (TCE) ND 0.047 Trichlorolluoromethane ND 0.047 1,2.3-Trichloropropane ND 0.047 " 1,2.4-Triroethylbenzene ND 0.047 " 1,35-11iniethylbenzene ND 0,047 Vinyl chloride ND 0.047 Xylcncs (total) ND 0.047 " Surrogate: Dibromolhuoromethauc 97 % (74 - 122 ) Surrogate: Toluene-dS 96 % (65 - 128) " Surrogate: 4-Bronto/luorohctrene 91 % (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 59 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by : Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Total Metals by CVAA Mercury ND 0.094 mg -kg I B1D0711 04/26/21 15:36 EPA 7471A Total Metals by ICP Antimony ND 2A mg/kg I B1 D0734 04/26/21 14:47 EPA 601 OB Arsenic 5.6 1.9 " Barium 320 0.97 Beryllium ND 0.48 —� Cadmium ND 0.24 Chromium 49 0.48 Cobalt 10 0.48 ^ Copper 41 0.97 Lead 440 0.48 Molybdenum 0.80 0.48 " Nickel 68 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 38 1.9 Zinc 580 1.9 " STLC Metals by ICP N-02, N-03 Lead 40 0.10 me/L 2 BIDO916 05/03/2113:41 STLC/EPA6010B N-07 TCLP Metals by ICP Lead 0.20 0.050 mgil. 1 B1D0919 05/03/21 15:06 EPA 1311/EPA601OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 94 WAk Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) ND 4.6 mg/kg 1 BID0692 04/23/21 22:18 EPA 8015M R-07 Surrogate. 4-BromoJlnorohen_ene 94 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 140 20 mg/kg 2 B1 D0766 04/28/21 16:38 EPA 8015M D-06 TPH Motor Oil (C23-C40) 360 100 1. .1 11" 11 Surrogate: o-Teiphen.1,1 120 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria. CA 93454 www.oecusa.com FAX: 805 925-3376 Page 61 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.047 mglkg 1 B 1 D0650 04/24/21 02:24 EPA 8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 " Bromofonn ND 0.047 " Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobcnzcnc ND 0.047 Chloroethane ND 0.047 " Chlorotirrm ND 0.047 Chloromethane ND 0.047 - 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 " Dibromochloromethane ND 0.047 " 1,2-Dibromo-3-chloropropane ND 0.047 " 1,2-Dibromoethane (EDB) ND 0.047 " Dibromomethane ND 0.047 1.2-Dichlorobenzene ND 0.047 0-Dichlorobenzene ND 0.047 1,4-Dichlorobenzene ND 0.047 Dichloroditluoromcthane ND 0.047 " 1,1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 " 1,1-Dichloroethene ND 0.047 cis-1.2-Dichloroethene ND 0.047 trans- l,2-Dichloroethene ND 0.047 1.2-Dichloropropane ND 0.047 13-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1,1-Dichloropropane ND 0.047 " cis-1.3-Dichloropropcnc ND 0.047 trans-1,3-Dichloropropcnc ND 0.047 Fthylbenzenc ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 62 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 I Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by : Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 llexachlorobutadiene ND 0.047 mg/kg '^ 4-Isopropyl Toluene ND 0.047 " Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 " Naphthalene ND 0.047 " n-Propylbenzene ND 0.047 Styrene ND 0.047 I.1,1,2-Tetrachloroethane ND 0.047 " 1,1.2.2-Tetrachloroethane ND 0.047 " Tetrachlorocthcnc (PCE) ND 0.047 " Tolucne ND 0.047 " 1,2,3-Trichlorobenzenc ND 0.047 " 1,2,4-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 " • 1,1,2-Trichloroethane ND 0.047 " Trichloroethene (TCE) ND 0.047 " Trichlorotluoromethane ND 0.047 1,23-Trichloropropane ND 0.047 " 1,2,4-1Yimethylbenzene ND 0.047 " 1.3,5-Trimethylbenzene ND 0.047 " Vinyl chloride ND 0.047 " Xylenes (total) ND 0.047 " Surrogate: Dihromgllnorumethanc 95 S„ (74 - 12 2 ) Surrogate: Tohtene-dS 97 % ( 65 - 12S) Surrogate: 4-Bromo/hunohen_ene 92 °',, (75 - 121) 1 B 1 D0650 04/24/21 02:24 EPA 8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 63 of 94 161*4Y, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ControlTotal Metals by CN7AA - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0711 -EPA 7471A Preparation: EPA 7471A Prep 04/26/21 09:00 Blank (BlD0711-BLKI) Analyzed: 04/26/21 14:37 Mercury ND 0.10 mg/kg LCS (B1D0711-BS1) Analyzed: 04/26/21 14:31 Mercury 0.903 0.10 mg/kg 0.833 96 85-115 LCS Dup (BlD0711-BSD1) Analyzed: 04/26/21 14:33 Mercury 0.765 0.10 mg/kg 0.833 92 85-115 5 20 Duplicate (B1D0711-DUPl) Source: 2102489-02 Analyzed: 04/26/21 14:45 Mercury 0.0432 0.099 mg/kg 0.0418 3 20 Matrix Spike (BlD0711-MSI) Source: 2102489-02 Analyzed: 04/26/21 14:47 Mercury 0.843 0.090 mg/kg 0.746 0.0418 107 75-125 Matrix Spike Dup (B1D0711-MSDI) Source: 2102489-02 Analyzed: 04/26/21 14:49 Mercury 0.673 0.087 mg/kg 0.723 0.0418 87 75-125 22 20 QR-02 Post Spike (B1D0711-PSI) Source: 2102489-02 Analyzed: 04/26/21 14:51 Mercury 5.23 ug/l 5.00 0.273 99 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 64 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Blank (BlD0734-BLK1) Analyzed: 04/26/21 13:29 Antimony ND 2.5 mglkg Arsenic ND 2.0 " Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 Chromium ND 0.50 Cobalt ND 0.50 " Copper ND 1.0 Lead ND 0.50 " Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 " LCS (BlD0734-BS1) Analyzed: 04/26/21 13:04 Antimony 97.0 2.5 rngikg 100 97 80-120 Arsenic 100 2.0 100 100 80-120 Barium 93.5 LO 100 94 80-120 Beryllium 99.0 0.50 100 99 80-120 Cadmium 99.2 0.25 100 99 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 100 0.50 100 100 80-120 Copper 104 1.0 100 104 80-120 Lead 99.4 0.50 100 99 80-120 Molybdenum 98.4 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium 101 2.0 100 101 80-120 Silver 5.04 0.50 5.00 101 80-120 Thallium 108 1.0 100 108 80-120 Vanadium 99.9 2.0 100 100 80-120 Zinc 97.0 2.0 100 97 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 65 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Totalby ' - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 LCS Dup (B1D0734-BSDl) Analyzed: 04/26/21 13:06 Antimony 97.8 2.5 mg/kg 100 98 80-120 0.8 20 Arsenic 101 2.0 100 101 80-120 0.7 20 Barium 93.6 1.0 100 94 80-120 0.2 20 Beryllium 98.6 0.50 100 99 80-120 0.4 20 Cadmium 99.5 0.25 100 100 80-120 0.3 20 Chromium 103 0.50 100 103 80-120 0.8 20 Cobalt 101 0.50 100 101 80-120 0.3 20 Copper 104 1.0 100 104 80-120 0.8 20 Lead 99.8 0.50 100 100 80-120 0.3 20 Molybdenum 99.4 0.50 100 99 80-120 0.9 20 Nickel 102 0.50 100 102 80-120 0.4 20 Selenium 101 2.0 100 101 80-120 0.1 20 Silver 5.04 0.50 5.00 101 80-120 0.1 20 Thallium 108 1.0 100 108 80-120 0.5 20 Vanadium 100 2.0 100 100 80-120 0.4 20 Zinc 97.4 2.0 100 97 80-120 0.4 20 Duplicate (BlD0734-DUPl) Source: 2102489-01 Analyzed: 04/26/21 13:35 Antimony ND 2.5 mg'kg ND 20 Arsenic 5.86 2.0 6.40 9 20 Barium 87.5 0.99 72.5 19 20 Beryllium 0369 0.49 0.419 12 20 Cadmium ND 0.25 ND 20 Chromium 20.3 0.49 22.2 9 20 Cobalt 6.53 0.49 6.95 6 20 Copper 18.4 099 21.5 16 20 Lead 5.52 0.49 6.10 10 20 Molvbdenum 1.50 0.49 " 2.18 37 20 QR-04 Nickel 25.9 0.49 30.4 16 20 Selenium ND 2.0 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.99 ND 20 Vanadium 18.9 2.0 20.6 9 20 Zinc 49.7 2.0 53.8 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 66 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Totalby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes �. Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 __. Matrix Spike (B1D0734-MSI) Source: 2102489-01 Analyzed: 04/26/21 13:08 Antimony 30.5 2.5 mg/kg 98.3 ND 31 10-116 Arsenic 102 2.0 98.3 6.40 97 77-121 Barium 159 0.98 98.3 72.5 88 30-169 '- Beryllium 93.2 0.49 99.3 0.419 94 86-111 Cadmium 90.1 0.25 98.3 ND 92 81-112 Chromium 124 0.49 98.3 22.2 103 75-129 Cobalt 98.3 0.49 98.3 6.95 93 71-121 Copper 123 0.98 99.3 21.5 103 68-135 Lead 95.5 0.49 98.3 6.10 91 72-121 Molybdenum 87.8 0.49 98.3 2.18 87 70-112 Nickel 122 0.49 98.3 30.4 93 73-121 Selenium 91.6 2.0 98.3 ND 93 76-116 Silver 4.59 0.49 4.92 ND 93 54-132 Thallium 94.7 0.98 98.3 ND 96 64-120 - Vanadium 117 2.0 98.3 20.6 98 78-124 Zinc 142 2.0 98.3 53.8 89 50-143 Matrix Spike Dup (BlD0734-MSD1) Source: 2102489-01 Analyzed: 04/26/21 13:11 Antimony 28.7 2.4 mg -kg 97.7 ND 29 10-116 6 20 Arsenic 99.5 2.0 97.7 6.40 95 77-121 2 20 Barium 173 0.98 97.7 72.5 103 30-169 9 20 Beryllium 90.5 0.49 97.7 0.419 92 86-111 3 20 Cadmium 96.7 0.24 97.7 ND 89 81-112 4 20 Chromium 120 0.49 97.7 22.2 100 75-129 3 20 Cobalt 95.5 0.49 97.7 6.95 91 71-121 3 20 Copper 120 0.98 9T7 21.5 101 68-135 3 20 Lead 92.4 0.49 97.7 6.10 88 72-121 3 20 Molybdenum 85.4 0.49 97.7 2.18 85 70-112 3 20 Nickel 121 0.49 97.7 30.4 92 73-121 1 20 Selenium 87.5 2.0 97.7 ND 90 76-116 5 20 Silver 4.44 0.49 4.88 ND 91 54-132 3 20 Thallium 90.3 0.98 97.7 ND 92 64-120 5 20 Vanadium 115 2.0 97.7 20.6 96 78-124 2 20 Zinc 141 2.0 97.7 53.9 89 50-143 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: �805j 925-3376 Page 67 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 _. Post Spike (BlD0734-PS1) Source: 2102489-01 Analyzed: 04/26/21 13:14 Antimony 1.85 ma/L 2.00 -0.00714 93 75-125 Arsenic 2.15 2.00 0.129 101 75-125 Barium 3.34 2.00 1.46 94 75-125 Beryllium 1.96 2.00 0.00943 97 75-125 Cadmium 1.99 2.00 -0.0200 94 75-125 Chromium 2.46 2.00 0.448 100 75-125 Cobalt 2.05 2.00 0.140 96 75-125 Copper 2.56 2.00 0.433 106 75-125 Lead 2.01 2.00 0.123 94 75-125 Molybdenum 1.97 2.00 0.0438 96 75-125 Nickel 2.55 2.00 0.613 97 75-125 Selenium 1.96 2.00 -0.0375 98 75-125 Silver 0.0965 0.100 -0.00476 96 75-125 Thallium 1.98 2.00 -0.0435 99 75-125 Vanadium 2.41 2.00 0.416 100 75-125 Zinc 2.96 2.00 1.08 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 68 of 94 r;MA6V26V Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 STLC Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0916 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:33 Blank (BlD0916-BLKI) Analyzed: 05/03/21 12:22 Cadmium ND 0.025 mg/L Chromium ND 0.050 " Copper ND 0.050 " Lead ND 0.050 LCS (BlD0916-BSI) Analyzed: 05/03/21 12:35 Cadmium 9.62 0.025 mg/L 10.0 96 80-120 Chromium 9.56 0.050 10.0 96 80-120 Copper 9.66 0.050 10.0 97 80-120 Lead 9.70 0.050 10.0 97 80-120 LCS Dup (B1D0916-BSD1) Analyzed: 05/03/21 12:37 Cadmium 9.69 0.025 mg/L 10.0 97 80-120 0.6 20 Chromium 9.59 0.050 10.0 96 80-120 0.3 20 Copper 9.70 0.050 10.0 97 80-120 0.4 20 Lead 9.78 0.050 10.0 98 80-120 0.9 20 Duplicate (BlD0916-DUPl) Source: 2102467-01 Analyzed: 05/03/21 12:53 Cadmium ND 0.050 mg/L ND 20 Chromium 0.0860 0.10 0111 25 20 QR-04 Copper 1.53 0.10 1.76 14 20 Lead 0.773 0.10 0.930 18 20 Leach Fluid Blank (B1D0916-LBK1) Analyzed: 05/03/21 12:25 Cadmium ND 0.050 mg/L Chromium ND 0.10 Copper ND 0.10 " Lead ND 0.10 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: [805) 925-3376 Page 69 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 i t Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0919 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:49 Blank (B1D0919-BLK1) Analyzed: 05/03/21 13:54 Chromium ND 0.050 mg/L Lead ND 0.050 " LCS (BlD0919-BS1) Analyzed: 05/03/21 14:02 Chromium 9.42 0.050 mg/L 10.0 94 80-120 Lead 9.97 0.050 1110.0 100 80-120 LCS Dup (BlD0919-BSDI) Analyzed: 05/03/21 14:04 Chromium 9.35 0.050 mg/l. 10.0 94 80-120 0.7 20 Lead 9.82 0.050 1110.0 98 80-120 2 20 Duplicate (B1D0919-DUP1) Source: 2102508-01 Analyzed: 05/03/21 14:11 Chromium ND 0.050 mg/L ND 20 Lead 1.60 0.050 112.02 24 20 QR-04 Leach Fluid Blank (BlD0919-LBK1) Analyzed: 05/03/21 13:57 Chromium ND 0.050 mg/L Lead ND 0.050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 70 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic TPH by 1 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0692 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 04/23/21 08:32 Blank (B1D0692-BLK1) Analyzed: 04/23/21 10:26 TPH Gasoline (C5-C12) ND 0.50 mg�kg Surrogate: 4-Bromgllnorohen.ene 0.128 110.125 103 39-157 LCS (B1D0692-BS1) Analyzed: 04/23/21 09:34 TPH Gasoline (('5-C12) 1.07 0.50 mg/kg 1.00 107 68-139 Surrogate: 4-Bronuilharrobcnzcne 0.146 110.126 116 39-157 LCS Dup (B1D0692-BSD1) Analyzed: 04/23/21 10:00 TPH Gasoline (C5-C12) 1.05 0.49 mg/kg 0.988 106 68-139 2 20 Surrogate: 4-Bromq luorohenzene 0.150 110.124 121 39-157 Duplicate (BlD0692-DUPI) Source: 2102433-01RE1 Analyzed: 04/23/21 22:44 TPH Gasoline (C5-C12) ND 4.8 mg/kg ND 20 Surrogate:4-Broniglluorobenzene 1.IS 111.20 98 39-157 Matrix Spike (BlD0692-MS1) Source: 2102433-01RE1 Analyzed: 04/23/21 23:10 TPH Gasoline (('5-C2) 8.79 4.9 mg/kg 9.80 ND 90 10-171 Surrogatc:4-Bromolluorobensene 1.34 111.23 109 39-157 Matrix Spike Dup (BlD0692-MSDI) Source: 2102433-01RE1 Analyzed: 04/23/21 23:36 TPH Gasoline (C5-('12) 8.26 4.4 mg/kg 8.77 ND 94 10-171 6 20 Surrogate: 4-Bromojluorohenzene 1.29 111.10 118 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 71 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Semi-Volatileby 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0766 - EPA 8015M Preparation: EPA 3550C 04/27/21 07:10 Blank (BlD0766-BLKI) Analyzed: 04/27/21 14:40 TPH Diesel (('13-C22) ND 10 t»g/kg TPH Motor Oil (C23-C40) ND 50 11 Surrogate' o-Ter phem l 41.9 " 49.8 84 65-136 LCS (B1D0766-BSl) Analyzed: 04/27/21 13:53 TPH Diesel (('13-C22) 420 10 mglkg 499 84 72-115 TPI I Motor Oil (C23-C40) 404 50 499 81 74-126 Surrogate: o-TerphenYl 43.0 49.9 86 65-136 LCS Dup (B1D0766-BSDI) Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22) 420 10 mg/kg 500 84 72-115 0.2 20 TPH Motor Oil (C23-C40) 402 50 500 80 74-126 0.5 20 Surrogate: o-Teiphem4 42.3 50.0 85 65-136 Duplicate (B1D0766-DUPI) Source: 2102489-01 Analyzed: 04/27/21 15:02 TPH Diesel (03-C22) ND 9.9 mg/kg ND 20 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Teiphenl 38.9 49.0 78 65-136 Matrix Spike (B1D0766-MSI) Source: 2102489-01 Analyzed: 04/27/21 14:17 TPH Diesel (C13-('22) 430 9.9 mg/kg 497 ND 86 46-147 TPH Motor Oil (C23-C40) 418 50 497 ND 84 35-171 Surrogate: o-Te;phernd 40.2 49.7 81 65-136 Matrix Spike Dup (B1D0766-MSD1) Source: 2102489-01 Analyzed: 04/27/21 14:40 7'PH Diesel (C13-C22) 480 10 mglkg 499 ND 96 46-147 11 20 TPI1 Motor Oil (C23-C40) 429 50 499 ND 86 35-171 3 20 Surrogate: o-Teiphenrl 44.5 49.9 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 72 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (BlD0650-BLK1) Analyzed: 04/23/21 16:50 Benzene ND 0.0050 mglkg Bromobenzene ND 0.0050 Bromochloromcthanc ND 0.0050 - Bromodichloromethane ND 0.0050 Bromoform ND 0.0050 " Bromomethane NI) 0.0050 " n-Butylbenzene ND 0.0050 " sec-Butylbenzene NI) 0.0050 " tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 Chlorobenzene NI) 0.0050 " Chloroethane ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " _ 1,2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibrornoethane (FDB) ND 0.0050 " Dibromomcthanc ND 0.0050 1,2-Dichlorobenzene ND 0.0050 " " 1,3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene NI) 0.0050 " Dichlorodifluoromethane ND 0.0050 1,1-Dichloroethene NI) 0.0050 " 1,2-Dichloroethane ND 0.0050 LI-Dichloroethene NI) 0.0050 " cis-1,2-Dichloroethene ND 0.0050 " trans- l,2-Dichloroethene ND 0.0050 1,2-Dichloropropane NI) 0.0050 " 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 " 1, 1 -Dichloropropene ND 0.0050 cis- 1.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 " Iahylbenzene NI) 0.0050 " Iiexachlorobutadiene NI.) 0.0050 " 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " - [Methylene chloride ND 0.0050 Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 73 of 94 ( A WAMM im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic poby Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes •- Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 �. Blank (BlD0650-BLKI) Analyzed: 04/23/21 16:50 Styrene ND 0,0050 mg/kg 1,1,1,2-Tetrachloroethane ND 0.0050 " 1,1,12-Tetrachlorocthanc ND 0.0050 Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 1,23-Trichlorobenzene ND 0.0050 " 1,2,4-1'riclilorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2,3-Trichloropropane ND 0.0050 1,2,4-Trintethy[benzene ND 0.0050 " 1,3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylenes (total) NI) 0.0050 Surrogate: Dibromofluorumcthane 0.0484 0.0498 97 74-122 Surrogate.' Toluene-d8 0.0479 0.0498 96 b5-128 Surrogate:4-Bromolluoroben_cne 0.0453 0.0498 91 75-121 LCS (B1D0650-BS1) Analyzed: 04/23/21 14:31 Benzene 0.0389 0.0050 ma/kg 0.0396 98 70-131 Bromobenzene 0.0369 0.0050 0.0396 93 74-130 Bromochloromethanc 0.0351 0.0050 0.0396 89 64-133 Bromodichloromethane 0.0368 0.0050 0.0396 93 69-137 Bromoform 0.0337 0.0050 0.0396 85 55-132 Bromomethane 0.0397 0.0050 0.0396 100 10-142 n-Butylbenzene 0.0440 0.0050 0.0396 111 64-156 sec-Butylbenzene 0.0465 0.0050 0.0396 117 75-155 tent-Butylbenzene 0.0438 0.0050 0.0396 110 74-144 Carbon tetrachloride 0.0396 0.0050 0 0396 100 67-135 Chlorobenzene 0.0399 0.0050 0.0396 101 73-134 C'hloroethane 0.0366 0.0050 0.0396 92 10-167 Chloroform 0.0371 0.0050 0,0396 94 69-124 Chloromethane 0.0286 0.0050 0.0390 72 34-136 2-Chlorotoluene 0.0421 0.0050 0.0396 106 75-135 4-0hlorotoluene 0.0420 0.0050 0.0396 106 70-138 Dibromochlorotnethane 0.0370 0.0050 0.0396 93 67-135 1,2-Dibromo-3-chloropropane 0.0368 0.0050 0.0396 93 41-149 1,2-Dibroniocthane (EDB) 0.0365 0.0050 0,0396 92 68-131 Dibromomethane 0.0322 0.0050 0.0396 81 61-140 1,2-Dichlorobenzene 0.0409 0.0050 0.0396 103 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805' 925-3376 Page 74 of 94 i A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS (B1D0650-BS1) Analyzed: 04/23/21 14:31 1,3-Dichlorobenzcne 0.0427 0.0050 mg/kg 0.0396 108 76-138 1,4-Dichlorobenzene 0.0410 0.0050 0.0396 104 72-132 Dichlorodifluoromcthanc 0.0196 0.0050 0.0396 50 10-155 LI-Dichloroethene 0.0399 0.0050 0.0396 101 63-139 1,2-Dichlorocthanc 0.0359 0.0050 0.0396 91 64-126 1,1-Dichloroethene 0.0435 0.0050 0.0396 110 52-167 cis-1.2-Dichloroethene 0.0390 0.0050 0.0396 96 70-135 trans-1,2-Dichlorociliene 0.0421 0.0050 0.0396 106 67-147 1,2-Dichloropropane 0.0368 0.0050 0.0396 93 68-131 1,3-Dicliloropropane 0.0359 0.0050 0.0396 91 64-129 2,2-Dichloropropane 0.0404 0.0050 0.0396 102 63-154 LI-Dichloropropene 0.0386 0.0050 0.0396 97 68-138 cis-1.3-Dichloropropene 0.0376 0.0050 0.0396 95 72-134 trans-1,3-Dichloropropene 0.0385 0.0050 0.0390 97 69-132 Ethylbenzene 0.0404 0.0050 0.0396 102 68-136 Hexachlorobutadiene 0.0446 0.0050 0.0396 113 72-198 4-Isopropyl Toluene 0.0439 0.0050 0.0396 111 74-150 Isopropylbenzene 0.0429 0.0050 0.0396 108 71-149 Nlethylene chloride 0.0402 0.0050 0.0396 102 51-127 Naphthalene 0.0436 0.0050 0.0396 110 57-158 n-Propylbenzene 0.0435 0.0050 0.0396 110 70-143 Styrene 0.0412 0.0050 0.0396 104 68-138 1,1,1,2-Tetrachloroethane 0.0373 0.0050 0.0396 94 76-130 I,1.2,2-Tetrachlorocthane 0.0407 0.0050 0.0396 103 60-136 Tetrachloroethene WCE) 0.0381 0.0050 0.0396 96 73-138 Toluene 0.0371 0.0050 0.0396 94 72-128 1,23-Trichlorobenzene 0,0390 0.0050 0.0396 98 61-166 1,2,4-Trichlorobenzene 0.0406 0.0050 0.0396 103 71-158 1.I,1-Trichloroethane 0.0389 0.0050 0.0396 98 71-135 1.1,2-Trichloroethane 0.0341 0.0050 0.0396 86 64-132 Trichloroethane (TCE) 0.0374 0.0050 0.0396 94 74-139 Trichlorofluoromethane 0.0379 0.0050 0.0396 96 30-156 1,2,3-Trichloropropane 0.0383 0.0050 0.0396 97 67-123 L2,4-Trimethylbenzene 0.0419 0.0050 0.0396 106 68-134 1,3,5-Trimethylbenzene 0.0440 0.0050 0.0396 111 71-140 Vinyl chloride 0.0352 0.0050 0.0396 89 43-144 Xylenes (total) 0.122 0.0050 0.119 102 69-138 Surrogate: Dibromolluoromethane 0.0490 0.0495 99 74-122 Surrogate:7o/ttene-dR 0.0475 0.0495 96 65-128 Surrogate:4-BronmlAmrohenzene 0.0476 0.0495 96 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805' 925-3376 Page 75 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (BlD0650-BSD1) Analyzed: 04/23/21 14:59 Benzene 0.0417 0.0050 mg!kg 0.0398 105 70-131 7 20 Brontobenzene 0.0394 0.0050 0.0398 99 74-130 6 20 Bromochloromcthanc 0.0377 0.0050 0.0398 95 64-133 7 20 T Bromodichloromethane 0.0392 0.0050 0,0398 98 69-137 6 20 Bromoform 0.0363 0.0050 0.0398 91 55-132 8 20 Bromomethane 0.0416 0.0050 0.0398 105 10-142 5 20 _- u-Butylbenzene 0.0475 0.0050 0.0398 120 64-156 8 20 sec-Butylbenzene 0.0493 0.0050 0.0398 124 75-155 6 20 tert-Butylbenzene 0.0464 0.0050 0.0398 117 74-144 6 20 Carbon tetrachloride 0.0418 0.0050 0.0398 105 67-135 5 20 Chlorobenzene 0.0420 0.0050 0.0398 106 73-134 5 20 Chloroethane 0.0394 0.0050 0.0398 99 10-167 7 20 Chloroform 0.0392 0.0050 0.0398 99 69-124 5 20 Chloromethane 0.0302 0.0050 0.0399 76 34-136 5 20 2-Chlorotoluene 0.0435 0.0050 0.0398 109 75-135 3 20 4-Chlorotoluene 0.0431 0.0050 0.0398 log 70-139 3 20 Dibromochloromethane 0.0397 0.0050 0.0398 100 67-135 7 20 �. 1,2-Dibromo-3-chloropropane 0.0410 0.0050 0.0398 103 41-149 11 20 1,2-Dibromoethane (EDB) 0.0388 0.0050 0.0398 98 68-131 6 20 Dibromoinethanc 0.0334 0.0050 0.0398 84 61-140 4 20 1,2-Dichlorobenzene 0.0429 0.0050 0.0398 108 76-136 5 20 ' 1,3-Dichloroben7.ene 0.0444 0.0050 0.0398 112 76-138 4 20 IA-Dichlorobenzene 0.0436 0.0050 0.0398 110 72-132 6 20 Dichloroditluoromethanc 0.0206 0.0050 0.0398 52 10-155 5 20 I,I-Dichloroethene 0.0424 0.0050 0.0398 107 63-139 6 20 1,2-Dichlorocthanc 0.0395 0.0050 0.0398 99 64-126 l0 20 1, 1 -Dichloroethene 0.0446 0.0050 0.0398 112 52-167 2 20 cis-1,2-Dichloroethene 0.0413 0.0050 0.0398 104 70-135 8 20 trans-1,2-Dichloroethene 0.0447 0.0050 0.0398 112 67-147 6 20 1,2-Dichloropropane 0.0401 0.0050 0.0398 101 68-131 9 20 1,3-Dichloropropane 0.0383 0.0050 0.0398 96 64-128 6 20 2,2-Dichloropropane 0.0436 0.0050 0.0398 110 63-154 8 20 1, 1 -Dichloropropene 0.0416 0.0050 0.0398 105 68-138 8 20 cis- 1,3-Dichloropropene 0.0407 0.0050 0.0398 102 72-134 8 20 trans-1,3-Dichloropropene 0.0414 0.0050 0.0398 104 69-132 7 20 Ethylbenzenc 0.0422 0.0050 0,0398 106 68-136 4 20 1 lexach lorobutadiene 0.0478 0.0050 0,0398 120 72-198 7 20 4-Isopropyl Toluene 0.0465 0.0050 0,0398 117 74-150 6 20 Isopropylbenzene 0.0461 0.0050 0.0398 116 71-149 7 20 Methylene chloride 0.0427 0.0050 0.0398 108 51-127 6 20 Naphthalene 0.0454 0.0050 0.0398 114 57-158 4 20 n-Propylbenzene 0.0460 0.0050 0.0398 116 70-143 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 76 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (B1D0650-BSDI) Analyzed: 04/23/21 14:59 Styrene 0.0437 0.0050 mg/kg 0.0398 110 68-138 6 20 1,1,1,2-Tetrachloroethane 0.0395 0.0050 0.0398 99 76-130 6 20 1,1,2,2-Tetrachlorocthanc 0.0415 0.0050 0.0398 104 60-136 2 20 Tetrachloroethene (PCE) 0.0400 0.0050 0.0399 100 73-139 5 20 Toluene 0.0399 0.0050 0.0398 100 72-128 7 20 1,2,3-Trichlorobenzene 0.0432 0,0050 0.0398 109 61-166 10 20 -. 1,2,4-Trichlorobenzene 0.0439 0.0050 0.0398 110 71-158 8 20 1, 1, 1 -Trichloroethane 0.0415 0.0050 0.0398 104 71-135 6 20 1, 1,2-Trich loroethane 0.0377 0.0050 0.0398 95 64-132 10 20 Trichloroethene (TCE) 0.0396 0.0050 0.0398 99 74-139 6 20 7Yichlorofluoromethane 0.0412 0.0050 0.0398 104 30-156 9 20 1,2,3-Trichloropropane 0.0381 0.0050 0.0398 96 67-123 0.6 20 1,2.4-Trim ethyl benzene 0.0448 0.0050 0.0398 113 68-134 7 20 1,3,5-Trimethylbenzene 0.0461 0.0050 0.0398 116 71-140 5 20 Vinyl chloride 0.0371 0.0050 0.0398 93 43-144 5 20 Xylenes (total) 0.128 0.0050 0,119 108 69-138 5 20 Surrogate: Dihrontolhnavmethane, 0.0504 0.0497 101 74-122 Surrogate: Toluene-dH 0.0476 0.0497 96 65-12S Surrogate:4-BronmJluorohen_ene 0.0475 0.0497 96 75-121 Duplicate (B1D0650-DUPI) Source: 2102489-01 Analyzed: 04/24/21 03:18 �. Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromethane ND 0.0050 ND 20 Bromodichloromethane ND 0,0050 ND 20 Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 -i Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-I)ibromo-3-chloropropaoc ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibromomethanc ND 0.0050 ND 20 12-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 77 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatilet t by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 - Duplicate (BlD0650-DUPI) Source: 2102489-01 Analyzed: 04/24/21 03:18 1.3-Dichlorobenzenc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromethanc ND 0.0050 ND 20 LI-Dichloroethane ND 0.0050 ND 20 1,2-Dichlorocthanc ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 ,.._ cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1,1-Dichloropropene ND 0.0050 ND 20 cis-1,3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 Ethylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 _.. Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 ❑-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1, 1, 1,2-Tetrachloroethane ND 0.0050 ND 20 1,11,2-Tetrachlorocthanc ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,24-Trichlorobenzene ND 0.0050 ND 20 - 1,1,1-Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethanc ND 0.0050 ND 20 1,2,3-Trichloropropane ND 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylben7ene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dihromoiluoromethanc 0.0479 0.0496 97 74-122 Surrogate: Toluene-d8 0.0485 0.0496 98 65-128 Surrogate:4-Brotnalhau•ohen_ene 0.0452 0.0496 91 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 78 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (BlD0650-MSI) Source: 2102489-02 Analyzed: 04/24/21 04:12 Benzene 0.0404 0.0050 mgIg 0.0402 ND 101 37-145 Bromobenzene 0.0359 0.0050 0.0402 ND 89 29-147 Bromochloromethane 0.0367 0.0050 0.0402 ND 91 40-145 Bromodiehloromethane 0.0384 0.0050 0.0402 ND 96 39-153 Bromofonn 0.0332 0.0050 0.0402 ND 83 32-143 Bronioniethane 0.0467 0.0050 0.0402 ND 116 10-141 n-Butylbenzene 0.0324 0.0050 0.0402 ND 81 10-162 sec-Butylbenzene 0.0408 0.0050 0.0402 ND 102 14-168 tert-Butylbenzene 0.0388 0.0050 0.0402 ND 97 21-159 Carbon tetrachloride 0.0380 0.0050 0.0402 ND 95 28-148 Chktrobenzene 0.0384 0.0050 0.0402 ND 96 32-148 Chloroethane 0.0502 0.0050 0.0402 ND 125 11-166 Chloroform 0.0400 0.0050 0.0402 ND 100 40-139 Chloromethane 0.0350 0.0050 0.0402 ND 87 18-135 2-Chlorotoluene 0.0362 0.0050 0.0402 ND 90 25-151 4-Chlorotoluene 0.0363 0.0050 0.0402 ND 90 22-150 Dibromochloromethane 0.0359 0.0050 0.0402 ND 89 40-147 1,2-Dibromo-3-chIoropropane 0.0390 0.0050 0.0402 ND 97 25-158 1.2-Dibromoethane (EDB) 0.0369 0.0050 0.0402 ND 92 38-147 Dibromomcthane 0.0319 0.0050 0.0402 ND 79 39-150 1,2-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 24-154 0-Dichlorobenzene 0.0369 0.0050 0.0402 ND 92 21-153 1,4-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 21-146 Dichloroditluoromethane 0.0188 0.0050 0.0402 ND 47 10-149 LI-Dichloroethane 0.0420 0.0050 0.0402 ND 105 34-151 1,2-Dichloroethenc 0.0400 0.0050 0,0402 ND 100 40-137 1,1-Dichloroethene 0.0449 0.0050 0.0402 ND 112 21-172 cis-1.2-Dichloroethene 0.0385 0.0050 0.0402 ND 96 38-147 trans-1,2-Dichloroethene 0.0409 0.0050 0.0402 ND 102 30-160 1,2-Dichloropropane 0.0397 00050 0.0402 ND 99 39-146 1,3-Dichloropropane 0.0396 0.0050 0.0402 ND 99 39-141 2,2-Dichloropropane 0.0280 0.0050 0.0402 ND 70 26-149 1, 1 -Dichloropropene 0.0385 0.0050 0.0402 ND 96 28-150 cis- I3-Dichloropropene 0.0171 0.0050 0.0402 ND 92 34-149 trans-1,3-Dichloropropene 0.0384 0.0050 0.0402 ND 96 36-143 Fithvlbenzene 0.0397 0.0050 0.0402 0.00290 92 23-150 Ilexachlorobutadiene 0.0313 0.0050 0.0402 ND 78 10-192 4-1sopropyl Toluene 0.0385 0.0050 0.0402 0.00290 89 11-165 Isopropylbenzene 0.0406 0.0050 0.0402 0.00202 96 17-166 Methylene chloride 0.0456 0.0050 0.0402 ND 114 28-135 Naphthalene 0.0441 0.0050 0.0402 0.00948 86 10-174 ❑-Propylbenzene 0.0393 0.0050 0,0402 0.00310 90 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 79 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 �• Matrix Spike (B1D0650-MS1) Source: 2102489-02 Analyzed: 04/24/21 04:12 Styrene 0.0387 0.0050 mglkg 0.0402 ND 96 24-154 1, 1, 1,2-Tetrachloroethane 0.0367 0.0050 0.0402 ND 91 38-149 1,1,2,2-Tetrachlorocthane 0.0387 0.0050 0.0402 ND 96 22-164 '- Teu•achloroethene (PCE) 0.0349 0.0050 0.0402 ND 87 25-153 Toluene 0.0376 0.0050 0.0402 ND 94 26-149 1,2,3-Trichlorobenzene 0.0323 0.0050 0.0402 ND 80 10-163 1,2,4-Trichlorobenzene 0.0323 0.0050 0.0402 ND 81 10-162 1, 1, 1 -Trichloroethane 0.0387 0.0050 0.0402 ND 96 34-149 1,1,2-Trichloroethane 0.0397 0.0050 0.0402 ND 99 25-175 Trichloroethene (TCE) 0.0386 0.0050 0.0402 ND 96 25-170 Trichlorofluoromethane 0.0487 0.0050 0.0402 ND 121 19-155 1,2,3-Trichloropropane 0.0403 0.0050 0.0402 ND 100 32-165 1,2,4-Trimethylbenzene 0.0466 0.0050 0.0402 0.0183 70 15-150 1,3,5-Trimethylbenzene 0.0413 0.0050 0.0402 0.00496 90 10-158 Vinyl chloride 0.0446 0.0050 0.0402 ND 111 22-148 Xylenes (total) 0.130 0.0050 0.120 0.0173 93 22-153 Surrogate Dibrunu,Jluururnctlaane 0.0487 0.0502 97 74-122 Surrogate: Toluene-d8 0.0484 0.0502 96 65-128 Surrogate:4-Bromglluorohenzene 0.0474 0.0502 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:.805 925-3376 Page 80 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal �--i 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP T 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Intemal 8015 Diesel & Motor Oil List EPA 80ISM Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals by ICP 601013 STLC Cadmium STLC/EPA 601013 Water OEC, CA -FLAP 601OB STLC Chromium STLC/EPA 601013 Water OEC. CA-ELAP 0010B STLC Copper STLC/EPA 601013 Water OEC, CA-ELAP 601013 STLC Lead STLC/EPA 601013 Water OEC. CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601013 TCLP Chromium EPA 1311/EPA 601013 Water OEC, CA-ELAP ' 601 t1B TCLP Lead EPA 131 I/EPA 601013 Water OEC, CA-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC. CA -FLAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 81 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method i F nalysis Method Matrix Laboratory & Certification Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, CA -FLAP Total Metals by ICP 601013 Total Antimony EPA 601013 Solid OEC, CA -FLAP 601 OB Total Arsenic EPA 6010B Solid OEC, CA-ELAP 601013 Total Barium EPA 6010B Solid OEC, CA-ELAP 601013 Total Beryllium EPA 601013 Solid OEC, CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 601013 Total Chromium EPA 6010B Solid OEC. CA-ELAP 601013Total Cobalt EPA 6010B Solid OEC, CA-ELAP 6010B Total Cropper EPA 601013 Solid OEC, CA -FLAP 6010B Total Lead EPA 6010B Solid OEC, CA-ELAP 601013Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 601013 Total Nickel EPA 601013 Solid OEC, CA-ELAP 601013 Total Selenium EPA 601OB Solid OEC, CA-ELAP 6010B Total Silver EPA 6010B Solid OEC, CA-ELAP - 601013Total Thallimn EPA 601 OB Solid OEC. CA-ELAP 601013 Total Vanadium EPA 601013 Solid OEC, CA-ELAP 6010B Total Zinc EPA 6010B Solid OEC, CA-ELAP Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 82 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TP1I-Gasoline EPA 8015M Solid OEC Internal 8015 1TH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015'ITH-Gasoline EPA 8015M Solid OEC_ Internal 8015 TPI I -Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal • -, 8015TPR-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPI{-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH -Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 83 of 94 WAM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 NotesDeflnitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-01 Analyte concentration exceeds TTLC. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 84 of 94 EMSL Analytical, Inc. 464 McCormick Street San Leandro, CA 94577 Tel/Fax: (510) 895-3675 / (510) 895-3680 http://www.EMSL.com / sanleandrolab@emsl.com Attention: Shahanaz Parvin Oilfield Environmental and Compliance 307 Roemer Way Suite 300 Santa Maria, CA 93454-1105 Project: 2102508 EMSL Order: 092105912 Customer ID: OILF50 Customer PO: 2102508 Project ID: Phone: (805) 922-4772 Fax: (805) 925-3376 Received Date: 04/26/2021 8:45 AM Analysis Date: 04/26/2021 Collected Date: 04/23/2021 Test Report: Asbestos Analysis of Bulk Materials via EPA 600IR-931116 Method using Polarized Light Microscopy Non -Asbestos Asbestos Sample Description Appearance % Fibrous % Non -Fibrous _ % Type 2102508-16 Tan 50% Quartz None Detected Non -Fibrous 50% Non -fibrous (Other) 092105912-0001 Homogeneous 2102508-17 Gray 50% Quartz None Detected Non -Fibrous 40% Ca Carbonate 092105912-0002 Homogeneous 10% Non -fibrous tOtheri Analyst(s) Gavin Lee (2) Cecilia Yu, Laboratory Manager or Other Approved Signatory EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 "Interim Method") but augmented with procedures outlined in the 1993 ("final") version of the method. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non -friable organically bound materials present a problem matrix and therefore EMSL recommends gravimetric reduction prior to analysis. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Estimation of uncertainty is available on request. Samples analyzed by EMSL Analytical, Inc San Leandro, CA NVLAP Lab Code 101048-3, WA C884 Initial report from: 04/26/2021 13:36:56 ASt3 PLM 0008 0001 - 1.78 Printed: 4/26/2021 1:36 PM Page 1 of 1 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2314.D Operator EW Acquired 23 Apr 2021 2:32 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-01@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 14 GOMD2314.D\FID1A 90000 85000 70000 65000 600001 1 55000f 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2315.D Operator EW Acquired 23 Apr 2021 2:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-02@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 15 Response_ 85000 ~ 80000 " 75000 70000 65000 60000 30000 25000 20000 15000 10000 GOMD2315.D\FID1A 5000 L 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2316.D Operator EW Acquired 23 Apr 2021 3:24 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-03@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 16 Response_ GOMD2316.D\FID1A 95000l 1 90000' 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 1, 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2317.D Operator EW Acquired 23 Apr 2021 3:50 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-04@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 17 Response- GOMD2317.D\FID1A 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 + 1 30000 25000 20000 15000 10000� 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2318.D Operator EW Acquired 23 Apr 2021 4:16 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-05@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 18 Response_ GOMD2318.D\FID1A 95000 1 90000 85000 80000 75000 70000 65000 60000 550001 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 I 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2319.D Operator EW Acquired 23 Apr 2021 4:42 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-06@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 19 Response_ 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2319.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2320.D Operator EW Acquired 23 Apr 2021 5:08 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-07@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 20 Response_ 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 GOMD2320.D\FID1A 15000 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 1 0.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2321.D Operator EW Acquired 23 Apr 2021 5:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-08@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 21 Response- GOMD2321.D\FID1A 70000 65000 60000 50000 45000 40000 15000 10000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 �7.00 00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2322.D Operator EW Acquired 23 Apr 2021 6:00 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-09@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 22 Rest 90000 85000 80000 75000 70000 65000• 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 000 1.00 2.00 3.0 GOMD2322.D\FID1A File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2323.D Operator EW Acquired 23 Apr 2021 6:26 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-10@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 23 Response_ 1 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 30000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 GOMD2323.D\FID1A 1.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2328.D Operator EW Acquired 23 Apr 2021 8:35 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-11@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 28 90000 85000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 GOMD2328.D\FID1A r.00 8.00 9.00 1 0.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2329.D Operator EW Acquired 23 Apr 2021 9:01 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-12@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 29 Response_ GOMD2329.D\FID1A 850J 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2330.D Operator EW Acquired 23 Apr 2021 9:27 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-13@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 30 Response_ GOMD2330.D\FID1A 95000 90000 85000 80000' 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 Time 0.00 1.00 1 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2331.D Operator EW Acquired 23 Apr 2021 9:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-14@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 31 ,Response 60000 55000 50000 45000 40000, i 35000 i 30000 25000. i 20000 15000, 10000 5000 GOMD2331.D\FID1A ��... T -�- - 7 Time 0.00 1.00 T 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2332.D Operator EW Acquired 23 Apr 2021 10:18 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-15@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 32 GOMD2332.D\FID1A 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 M 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 9 a a$� »acl v cl 0 m U E mU 0 =i 69"1" ao-aoaa final zoos1111109 R i sod 1 iood �1lUgnlu0l � e � s DOLzs-s50AS g a An A O WM90WOD-d"I ra CIL m b y Y, oPWnS feWutAooAp000a F- ii pq > Oq C 1a111-d 809zs x Z N w = so a U V� d anew - zz awl X J� m rn CY d O4 ii ❑ m Co m S 0 O A¢ Q V d Ao 7r'X? .0 QL op y r/y ee ❑ ❑ n A w 3 _cj a a� J r 4 s 40 a �7 fl ° C $ a a t_ v N uCh j7,Pam to 1 a O U 7 in - o ❑❑ Z s �h Q1 E.IMME u3 N G�Wp 0. COL. C.? 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N o� Fir wort r7 I N rn 0 N rn 0 00 00 M «7 O` DD O Cd CL E. r � 0 CA = Ui M � Q r� 00 000 cn L U �O •yO? M � M CIA � O 4 .. a. U av Ekncv t � VS v, c Q 1 a V rr-a ai c eC ai c C7 W E 00 9 y d N N � Q c r'� N c 6 4 � 7 � N � Page 91 of 94 Y u xS L r-I F$ CJJ U U V U U U 4 !3 Maw i� a a a a a a E ci a F F can J J J J F- JE J t) a ri) ai U) U) 1 (1) sRltoS PONOBIG Idol Q Q Q zoo91vk9o9 L C god t issd v INIQ UBI onus-SOOAS S � 0 W9k09 OkrGD' dNl z A2 o ►1 o a E o epylnS 1splusAo eAgsssa t ea z � u ++ 3911 find so9Z9 o z H G r ii o ❑ .o ❑ CD cL,cx Q'. a ' In Stl {10fl V Q 0 Ca n r z ❑..r o yT1 b� c e W �vC .}[ 3 r3 Q Q Q ❑ A CAZ Gil N u» t x C ❑ } H g c E : v $ CL C R u q 0 u R¢ 2 l;� �' a ry ci CAL r a ri ❑❑ m m , , , E. EN Q Q g c c m h1 ii Z 0 H U Q W a H1 N irk d d n(71 J a M CL U U U U ci Y' x co (/l V) I (6 (/ tr1 *wins pa"lOsla lllol x` AIM —off e G O C Z808 / V 009 L r 80diWd $ U t ° 5a� � U DOZZO - SOOA8 Ic W9 We OW00 • dHl X a 04 a a0 C a opWng 1 owuvAD a"pasaa m F Y 4*1111nd 809Z9 N L O •Iq�W'ZZ+pil a❑ CD m W Nm Q V L F A�Y un n a k i tC E 7G +, Q of . ❑ Vtr Iz N i. ` E❑❑. � C S Z ❑ r 33 o Za. G❑ e Vi w W a V a L ©❑ s 4 x O - pY� F c L O Y 3 a E c+ c r Fr G :y ❑ ❑ m fz, y y i y m s 7. L 4 C O F O 7 E .}� .� .� E a d o a Y w� w � > C > C > I. n v vFawvI N 9 v O, I. m ON cri C C%i O Q W1 C" N 0 0 p4 Cz; Yti Q U 0 O G Rt C� w a� a Q G. 03 6 f s _ N 1 � L °E d i N V�'I Ct f � d O N C., fi Page 94 of 94 r-� Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: �*"Y '��Z-) Meredith Sprister, Business Director mspristcr@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Revision History Previous Report Reason for Revision 2102032 04/07/2021 16:45 Complete report. Sample Summary Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received ' Sump Trench W 2102032-01 Solid Solid 04/06/2021 10:25 04/06/2021 11:30 Sump Trench Pile 2102032-02 Solid Solid 04/06/2021 10:26 04/06/2021 11:30 Sump Trench Bottom 2102032-03 Solid Solid 04/06/2021 10:30 04/06/2021 11:30 Fire Trench Bottoms 2102032-04 Solid Solid 04/06/2021 10:36 04/06/2021 11:30 - Fire Trench W 2102032-05 Solid Solid 04/06/2021 10:38 04/06/2021 11:30 Fire Trench E 2102032-06 Solid Solid 04/06/2021 10:40 04/06/2021 11:30 Sample Batch Preparation Summary Analysis Batch ID Preparation Date/Iime STLC Metals by ICP 601OB STLC B1D0494 04/16/2021 15:40 STLC Metals Extraction STLC Metals Extraction BID0313 04/12/2021 14:18 TCLP Metals by ICP 6010B TCLP B I D0495 04/ 16/2021 15:41 TCLP Metals Extraction TCLP Metals Extraction B 1 D0312 04,/12/2021 14:17 Total Metals by CN'AA Mercury Total EPA 7471 A B1 D0153 04/07/2021 07:54 Total Metals by ICP 601 OB Total B I D0123 04i06/2021 12:15 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: [805'� 925-3376 Page 2 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by : Lab ID: 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.097 0.091 mg/kg 1 BID0153 04/07/21 14:55 EPA 7471A Total Metals by ICP Antimonv 7.5 2.3 mg/kg I BID0123 04/07/2113:25 EPA 6010B •- Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 Molvbdenum 2.0 0.46 Nickel 98 0.46 Selenium ND 19 Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium Lead TCLP Metals by ICP Lead 0.70 0.10 mgil- 2 BID0494 04i19,121 12:57 STLC/EPA6010B 3.6 0.10 " " " " 0.23 0.050 mg/L 1 B I D0495 04/ 19/21 14:01 EPA 1311 /EPA 601 OB N-02 N-02, N-03 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID : Sump Trench Pile Sampled: 04/06/21 10:26 Matrix: Solid Sampled by : Lab ID : 2102032-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA MercurN 0.12 0.094 mg/Ig 1 B1DO] 53 04/07/21 14:57 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg -/kg 1 BID0123 04/07/2113:28 EPA 6010B Arsenic 7.4 1.9 Barium 280 0.95 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 52 0.47 " " " " " N-02 Cobalt 12 0.47 Copper 38 0.95 Lead 180 0.47 N-02, N-03 Molvbdenum 1.2 0.47 Nickel 78 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 37 1.9 Zinc 250 1.9 STLC Metals by ICP Chromium 0.39 0.10 mg/l. 2 BID0494 04/19/21 13:00 STLC/EPA6010B Lead 15 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.086 0.050 mg/L 1 B I D0495 04/19/21 14:04 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 4 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalytical i Sample ID: Sump Trench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by : Lab ID : 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 BID0153 04/07/21 14:59 EPA 7471A Total Metals by ICP Antimony 2.5 2.4 mg/kg I BID0123 04/07/21 13:31 EPA6010B Arsenic 7.0 1.9 Barium 230 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.48 Copper 72 0.97 Lead 140 0.48 N-02, N-03 111olvbdenum 1.1 0.48 Nickel 190 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 34 1.9 Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 B1 D0494 04/19/21 13:02 STLCEPA 6010B _ Lead 7.6 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 mglL 1 B1 D0495 04/ 19/21 14:06 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Fire Trench Bottoms Sampled: 04/06/21 10:36 Matrix: Solid Sampled by: Lab ID: 2102032-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg/kg I BID0153 04/07/2115:01 EPA 7471A ~ Total Metals by ICP Antimony ND 2.3 mg/kg 1 B I D0123 04/07/21 13:34 EPA 6010E Arsenic r 6.6 1.8 Barium 220 0.91 Beryllium 0.63 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 18 0.46 Copper 26 0.91 Lead 9.4 0.46 Molybdenum 0.46 0.46 Nickel 110 0.46 Selenium ND 1.8 Silver ND 0.46 Thallium ND 0.91 Vanadium 34 1.8 Zinc 28 1.8 STLC Metals by ICP Chromium ND 0.10 mg/L 2 B1 D0494 04/19/21 13:13 STLC/EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID : Fire Trench W Sampled: 04/06/21 10:38 Matrix: Solid Sampled by : Lab ID : 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA MercurN Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Mohlbdenum Nickel Selenium Silver Thallium Vanadium Zinc 0.13 0.096 mg/kg 1 B 1 D0153 04/07/21 15:04 EPA 7471 A ND 2.4 mg/kg 1 B 1 D0123 04/07/21 13:37 EPA 601 OB 4.8 1.9 130 0.96 ND 0.48 ND 0.24 41 0.48 9.0 0.48 22 0.96 27 0.48 1.1 0.48 50 0.49 ND 1.9 ND 0.48 ND 0.96 34 1.9 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Saniples Sample ID : Fire Trench E Sampled: 04/06/21 10:40 Matrix: Solid Sampled by : Lab ID : 2102032-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.12 0.094 mg/kg 1 BIDO] 53 04/07/2115:06 EPA 7471A Total Metals by ICP Antimony ND 2.4 mglkg I BID0123 04/07/2113:17 EPA 6010B Arsenic 6.4 1.9 " Barium 170 0.94 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 49 0.47 Cobalt 12 0.47 Copper 26 0.94 Lead 32 0.47 Molybdenum 1.2 0.47 Nickel 73 0.47 Selenium NI) 1.9 Silver ND 0.47 Thallium ND 0.94 Vanadium 36 1.9 Zinc 64 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0153 - EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 Blank (B1D0153-BLKl) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg/kg LCS (B1D0153-BS1) Analyzed: 04/07/21 13:07 Mercury 0.809 0.10 mg/kg 0.833 97 85-115 LCS Dup (BID0153-BSD1) Analyzed: 04/07/21 13:09 Mercury 0.799 0.10 mg/kg 0.833 96 85-115 1 20 Duplicate (B1D0153-DUPl) Source: 2101942-01 Analyzed: 04/07/21 13:17 Mercury 0.0119 0.087 mg/kg 0.0145 21 20 QR-04 Matrix Spike (131D0153-MS1) Source: 2101942-01 Analyzed: 04/07/21 13:19 Mercury 0.904 0.097 mg/kg 0.809 0.0145 98 75-125 Matrix Spike Dup (B1D0153-MSDl) Source: 2101942-01 Analyzed: 04/07/21 13:21 Mercury 0.776 0.092 mgIg 0.765 0.0145 100 75-125 4 20 Post Spike (B1D0153-PS1) Source: 2101942-01 Analyzed: 04/07/21 13:23 Mercury 5.16 ug/L 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Blank (B1D0123-BLKI) Analyzed: 04/07/21 12:48 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 T Beryllium ND 0.50 " Cadmium ND 0.25 Chromium ND 0.50 " Cobalt ND 0.50 .- Copper ND 1.0 Lead ND 0.50 " Molybdenum ND 0.50 " - • Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (B1D0123-BS1) Analyzed: 04/07/21 12:53 - Antimony 97.5 2.5 mg!kg 100 98 80-120 Arsenic 100 2.0 100 100 80-120 Barium 103 1.0 100 103 80-120 Beryllium 100 0.50 100 100 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 100 0.50 100 100 80-120 Cobalt 102 0.50 100 102 80-120 - Copper 98.3 1.0 100 98 80-120 Lcad 102 0.50 100 102 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickcl 102 0.50 100 102 80-120 Selenium 99.8 2.0 100 100 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 1.0 100 102 80-120 _ kanadium 96.7 2.0 100 97 80-120 Zinc 102 2.0 100 102 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 20 OEC Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 -EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSDI) Analyzed: 04/07/21 12:56 Antimony 100 2.5 mg!kg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 1.0 100 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 80-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 101 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 1.0 100 105 80-120 2 20 ' Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 " 100 104 80-120 2 20 Duplicate (B1D0123-DUPI) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mg/kg 1.40 20 Arsenic 5.99 1.9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 ND 20 Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 - Copper 26.5 0.97 26.5 0.2 20 Lead 28.1 0.48 32.0 13 20 Molybdenum 56.4 0.49 1.20 192 20 QR-04 Nickel 69.5 0.48 73.4 7 20 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 Vanadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by lCP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Matrix Spike (B1D0123-MS1) Source: 2102032-06 Analyzed: 04/07/21 12:58 Antimony 37.4 2.4 mglkg 97.7 1.40 37 10-116 Arsenic 101 2.0 97.7 6.36 97 77-121 Barium 250 0.98 97.7 169 83 30-169 Beryllium 94.0 0.49 97.7 0.395 96 86-111 Cadmium 90.0 0.24 97.7 ND 92 81-112 Chromium 144 0.49 97.7 48.9 98 75-129 Cobalt 102 0.49 97.7 11.8 92 71-121 Copper 122 0.98 97.7 26.5 98 68-135 Lead 120 0.49 97.7 32.0 90 72-121 Molybdenum 87.1 0.49 97.7 1.20 88 70-112 -- Nickel 156 0.49 97.7 73.4 85 73-121 Selenium 91.5 2.0 97.7 ND 94 76-110 Silver 4.87 0.49 4.88 ND 100 54-132 Thallium 85.3 0.98 97.7 ND 87 64-120 Vanadium 131 2.0 97.7 36.2 97 78-124 Zinc 163 2.0 97.7 64.5 100 50-143 Matrix Spike Dup (B1D0123-MSD1) Source: 2102032-06 Analyzed: 04/07/21 13:01 '^ Antimony 38.1 2.5 mg/kg 98.3 1.40 37 10-116 2 20 Arsenic 108 2.0 98.3 6.36 103 77-121 6 20 Barium 263 0.98 98.3 169 96 30-169 5 20 Beryllium 97.9 0.49 98.3 0.395 99 86-I11 4 20 Cadmium 94.3 0.25 98.3 ND 96 81-112 5 20 Chromium 156 0.49 98.3 48.9 109 75-129 8 20 Cobalt 106 0.49 98.3 11.8 96 71-121 4 20 - Copper 130 0.98 98.3 26.5 105 68-135 6 20 Lcad 126 0.49 98.3 32.0 95 72-121 4 20 Molybdenum 91.2 0.49 98.3 1.20 91 70-112 5 20 Nickel 167 0.49 98.3 73.4 95 73-121 7 20 - Selenium 96.0 2.0 98.3 ND 98 76-116 5 20 Silver 4.99 0.49 492 ND 102 54-132 2 20 Thallium 89.8 0.98 98.3 ND 91 64-120 5 20 Vanadium 137 2.0 98.3 36.2 102 78-124 4 20 Zinc 167 2.0 98.3 64.5 104 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PS1) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.89 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.558 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00309 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 Vanadium 2.68 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: i8('5) 925-3376 Page 13 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 STLC Metals by ICP - Quality Control Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0494 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 10:40 Blank (BlD0494-BLK1) Chromium Lead LCS (BlD0494-BS1) Chromium Lcad LCS Dup (B1D0494-BSDl) Chromium Lead Duplicate (B1D0494-DUPl) Chromium Lead Leach Fluid Blank (B1D0494-LBK1) Chromium Lead Leach Fluid Blank (BlD0494-LBK2) Chromium Lead Matrix Spike (BlD0494-MSl) Chromium Lead Matrix Spike Dup (B1D0494-MSD1) Chromium Lead Analyzed: 04/19/21 12:12 ND 0.050 mg/l. ND 0.050 11 Analyzed: 04/19/21 12:23 9.69 0.050 mg/L 10.0 9.80 0.050 1110.0 Analyzed: 04/19/21 12:25 9.72 0.050 mg/L 10.0 9.71 0.050 1110.0 Source:2101759-01 Analyzed: 04/19/21 12:46 120 0.050 mg/L 112 54.3 0.050 1151.6 Analyzed: 04/19/21 12:15 ND 0.10 mg/L ND 0.10 Analyzed: 04/19/21 12:17 ND 0.10 mg/L ND 0.10 " Source:2101759-01 Analyzed: 04/19/21 12:28 116 0.10 mg/L 10.0 112 59.4 0.10 1110.0 51.6 Source:2101759-01 Analyzed: 04/19/21 12:38 134 0.10 mg/L 10.0 112 68.2 0.10 1110.0 51.6 97 80-120 98 80-120 97 80-120 0.3 20 97 80-120 1 20 6 20 5 20 42 89-115 79 86-114 214 89-115 166 86-114 Q�1-4X Q11-4X 14 20 QD14X 14 20 Q11 4X The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 i Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (BlD0495-BLK1) Analyzed: 04/19/21 13:46 Lead ND 0.050 mg/l. LCS (BlD0495-BSI) Analyzed: 04/19/21 13:26 Lead 9.76 0.050 mg/l. 10.0 98 80-120 LCS Dup (B1D0495-BSD1) Analyzed: 04/19/21 13:28 Lcad 9.71 0.050 mg/L 1O.O 97 80-120 0.5 20 Duplicate (B1D0495-DUPI) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lead ND 0.050 mg/L ND 20 Leach Fluid Blank (B1D0495-LBK1) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/l. Leach Fluid Blank (BlD0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/l. Matrix Spike (B1D0495-MS1) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lcad 10.1 0.050 mg/l. 10.0 ND WI 86-114 Matrix Spike Dup (B1D0495-MSDI) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lead 9.84 0.050 mg/L 10.0 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Samplei► Summarly lnalysis Method Matrix Laboratory & Certification STLC Metals by ICP 601013 STLC Chromium STLC/EPA 601013 Water OEC. CA -FLAP 601013 STLC Lcad STLC/EPA 601013 Water OEC, CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 6010B TCLP Lead EPA 1311/EPA 6010B Water OEC, CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA -FLAP Total Metals by CVAA Mercury "Dotal EPA 7471 A EPA 7471 A Solid OEC, CA -FLAP Total Metals by ICP 601013 Total Antimony EPA 601013 Solid OEC, CA -FLAP 001013 Total Arsenic EPA 601013 Solid OEC. CA -FLAP 6010B Total Barium EPA 601013 Solid OEC, CA -FLAP 601013 Total Beryllium EPA 6010B Solid OEC. CA -FLAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010B Total Chromium EPA 601013 Solid OEC, CA-ELAP 601013 Total Cobalt EPA 601013 Solid OF.C, CA -FLAP 601013 Total Copper EPA 601013 Solid OEC, CA -FLAP 601013 Total Lead EPA 601013 Solid OEC, CA-ELAP 601013 Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 6010B Total Nickel EPA 6010B Solid OEC, CA -FLAP 601013 Total Selenium EPA 6010B Solid OEC, CA-ELAP 601013Total Silver F.PA 601013 Solid OEC, CA -FLAP 601013Total Thallium EPA 6010B Solid OEC, CA-ELAP 6010E Total Vanadium EPA 6010E Solid OEC, CA-ELAP 6010E Total Zinc EPA 6010E Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 DefinitionsNotes and r Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above l Ox STLC'. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS andor LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17of20 A r ® 'l J Y 0 h� a E m,p Ci DNS sPIIOS P®AIOs10 Is101 AMAfs0Lo0 hi w � m W G G G zoos VL808 L d S0d / I"d if low �` liltlQsilusl e + ¢ten MEO 'sOOAS U a L M a W908 OWO'J' dHl Z "'� '0 epWnS 1 apfw.t0 sApasaa E > m ❑ `� v`t i a slslsW' ZZ •pfl y a � d ac } a❑ m M `` o o d x a E `� a n E #. 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U 3S a n ,] a z ❑:.? ® W G F t .}0c �0e 3 S O a ❑ 3 3 N a c° [`� c`� Y yr. %r Lf ulC'. �a o a°' ��— Z Ch16 0 rJ � � h ❑❑ m m m A`t 'O iii s a n CL ~ N = C CLD$ o T E (j � c � m 3� ���Haw�l-►- cv 6 Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2101841 Pacific Petroleum California P. O. Box 2646 Report Date: April 06, 2021 16:03 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Centers, 2600 Broad St. Enclosed is an analytical report for the above referenced project. The samples included in this report were received on March 25, 2021 15:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director msprister@occusa.com California ELAP Certification # 2438 Client Connect: client.oee.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Revision History Previous Report Reason for Revision 2101841 03/26/2021 17:07 Complete report. Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Tank N Wall 2101841-01 Solid Solid 03/25/2021 11:15 03/25/2021 15:00 Tank S Wall 2101841-02 Solid Solid 03/25/2021 11:20 03/25/2021 15:00 Tank E Wall 2101841-03 Solid Solid 03/25/2021 11:25 03/25/2021 15:00 Tank W Wall 2101841-04 Solid Solid 03/25/2021 11:30 03/25/2021 15:00 Tank Bottom E. End 2101841-05 Solid Solid 03/25/2021 11:05 03/25/2021 15:00 Tank Bottom W. End 2101841-06 Solid Solid 03/25/2021 11:10 03/25/2021 15:00 Sump Trench W 2101841-07 Solid Solid 03/25/2021 11:35 03/25/2021 15:00 Sump Trench S 2101841-08 Solid Solid 03/25/2021 11:38 03/25/2021 15:00 Control 2101841-09 Solid Solid 03/25/202111:00 03/25/2021 15:00 Soil Pile N 2101841-10 Solid Solid 03/25/2021 11:40 03/25/2021 15:00 Soil Pile S 2101841-11 Solid Solid 03/25/2021 11:45 03/25/2021 15:00 Soil Pile W 2101841-12 Solid Solid 03/25/2021 11:50 03/25/2021 15:00 Soil Pile E 2101841-13 Solid Solid 03/25/2021 12:10 03/25/2021 15:00 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 2 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sainple Batch ftepai-ation Summary • Analysis Batch ID Preparation Date/Time Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B 1('0798 03/25/2021 17:29 STLC Metals by ICP 6010B STLC B I D0007 04/01 /2021 09:01 STLC Metals Extraction STLC Metals Extraction B I C0891 03/30/2021 10:02 TCLP Metals by ICP of) 10B TCLP B I D0112 04(06/2021 10:20 TCLP Metals Extraction TCLP Metals Extraction B I C0898 03/30/2021 12:22 Total :Metals by CVAA Mercury Total EPA 7471 A B I C0807 03/26,2021 07:43 Total Metals by ICP 6010B Total B IC0810 03/26/2021 08:36 Volatile Organic Compounds by GUMS 8260B Full List BIC0815 0326,2021 09:17 8260B Full List B I C0817 03/26/2021 11:40 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B 1 C0802 03/26/2021 05:22 8015 TPH-Gasoline 131 C0804 03/26/2021 05:26 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 3 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg,kg 1 B1('0807 03/26/21 14:37 EPA 747]A Total Metals by ICP Antimony ND 2A mg/kg 1 B1C0810 03/26/21 13:30 EPA 6010B Arsenic 8.9 2.0 Barium 150 0.98 Bervllium 0.61 0.49 " Cadmium ND 0.24 Chromium 51 0.49 N-02 Cobalt 17 0.49 . Copper 28 0.98 Lead 9.1 0.49 Molvbdenum 2.6 0.49 Nickel 76 0.49 Selenium ND 2.0 Silver ND 0.49 "Thallium ND 0.98 " Vanadium 39 2.0 Line 32 2.0 STLC Metals by ICP Chromium 0.13 0.10 mg/l. 2 BID0007 04/01/21 14:45 STI.C/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline W5-02) ND 4.9 mg/kg 1 B1('0802 03/26/21 10:47 EPA 9015M R-07 Surrogate' 4-Brorno/luoroben_ene T5 103 ` (31 - 168) L 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-('22) ND 10 mgtkg TPH Motor Oil (C23-('40) ND 50 1. Surrogate: o-Tetphen}•I 107 `%b (65 -133 ) I BIC 0798 03/26/21 07:48 EPA 8015M The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgtkg 1000 B1('0815 03126'21 11:52 FPA 9260B Brotnobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butvlbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 12 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chlorocihanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibronio-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 " Dibromomethane ND 1.2 L2-Dichloroben7ene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 14-Dichlorobcn7enc ND 1.2 Diehl OrOdltlUorotnethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis- 1,2-Dich loroctliene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1,1-Dichloropropane ND 1.2 cis-1.3-Dichloropropenc ND 1.2 trans-1.3-Dichloropropenc ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 79 WAmML Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 11exachlorobutadiene ND 1.2 mgtkg 1000 BIC0815 03/26'21 11:52 EPA 826013 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1.2-Tetrachloroethane NI) 1.2 I.1.2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 " Tolucnc ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichi orobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Prichloroethene (TCE) ND 1.2 " Trichlorolluoromethane ND 1.2 1.2,3-Trichloropropane ND 1.2 12.4-Trimethylbenzene ND 1.2 1,3.5-Tiimethylbenzene ND 1.2 Vinyl chloride NJ) 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromolluoromethane 97 % ( 75 - 122 ) Surrogate: Toluene-dS 92 '% (66 - 728 ) Surrogate: 4-Bromolluoroberr_ene 92 °b ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled : 03/25/21 11:20 Matrix: Solid Sampled by : Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND O.086 mgrkg 1 B 1('0807 03/26/21 14:39 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg.kg I BIC0810 03/26/2) 13:33 EPA 6010B -- Arsenic 4.1 2.0 Barium 11 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 9.0 0.49 Cobalt 1.4 0.49 _ . Copper 3.5 0.98 Lead 2.5 0.49 Molybdenum 3.3 0.49 Nickel 6.8 0.49 Selenium ND 2.0 Silver ND 0.49 " _ Thallium ND 0.98 Vanadium 6.3 2.0 Zinc 9.7 2.0 Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 4.5 mg/kg 1 B I C0802 03/2621 11:13 EPA 8015M R-07 Surrogate: 4-Br•omo/htornhen_ene 103 , (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPI I Diesel (Cl 3-C22) ND 10 mglkg 1 BIC0798 03/26/2110:07 EPA8015M • TPII Motor Oil (C23-('40) ND 50 " " " " Surrogate: o-Ter pheml 106 i;, (65 - 133) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical i Sample ID : Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mglkg 1000 B 1 C0815 03/26/21 12:17 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 C hlorobenzenc ND 1.2 Chloroethanc ND 1.2 Chlorofonn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromelhane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 " Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1.3-Dichlorobcnzcnc ND 1.2 " I A-Dichlorobcnzcnc ND 1.2 " Dichlorodifluoromethanc ND 1.2 1,1-Dichloroethane ND 1.2 1,2-Dichloroetliane ND 1.2 " 1, 1 -Dichloroethene ND 1.2 cis- L2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1.1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropanc ND 1.2 " trans-1,3-Dichloropropcne ND 1.2 Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www_oecusa.com FAX: 805 925-3376 Page 9 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B1('0815 03/26/21 12:17 EPA926013 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 " 1,1,1.2-1'etrachloroethane ND 1.2 I_L2,2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 " 1, 1. 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethanc ND 1.2 " 1,2,3-Trichloropropane ND 1.2 " 1,14-Trimethylbenzene ND 1.2 " 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dihrnmulluorun7etTtmur 92's„ (75 - 122) " Surrogate: Toluene-dN X4 '; ; ( 66 - 138) Surrogate: 4-Bromolluorohenzene 92 ` (76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www,oecusa.com FAX: 805y 925-3376 Page 10 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. 0. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ; Analytical Report t Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID: 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg 1 BIC:0807 03/26/21 14:41 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1 C0810 03/26/21 13:36 EPA 6010B • Arsenic 4.2 1.9 Barium 140 0.95 Bervllium 0.51 0.47 Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 16 0.47 - Copper 23 0.95 Lead 7.0 0.47 Molybdenum ND 0.47 - . Nickel 72 0.47 " Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 33 1.9 Zinc 20 1.9 STLC Metals by ICP Chromium ND 0.10 mg/L 2 BID0007 04/01/21 14:48 STLC/EPA6010B • Volatile Organic TPH by GC/FID TPII Gasoline I('5-C12) ND 4.6 mg/kg 1 BIC0802 03126!21 11:39 EPA8015M R-07 Surrogate: 4-BromoJlaorobcn:cne 104 % (31 - 168 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 -j� Analytical Report for Samples Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID: 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (Cl 3-C 22) ND 9.9 mg/kg I BIC0798 03/26/21 08:02 EPA 8015M TPII Motor Oil (C23-('40) ND 50 Surrogate: o-Tenhen.vl 108 % (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3375 Page 12 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 77:Noiees] Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B1('0815 03/26/21 12:43 FPA9260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bronrodichloromethane ND 1.2 ^ Bromoform ND 1.2 Brontomethane ND 1.2 n-Butylbenzene ND 1.2 _., sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 12 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND L2 Dibromochloromethane ND 1.2 .� 1.2-Dibronio-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodilluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 • cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans- 1,3-1)ichIoropropcnc ND 1.2 " Ithylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg�kg 1000 B1('0815 03/26/21 12:43 EPA8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 " Methylene chloride ND 1.2 " • Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1.12-Tetrachloroethane ND 1.2 1,1,22-Tetrachloroethane ND 1.2 Tctrachlomcthcne (PCE) ND 1.2 TOIUCnC ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichloroben7cne ND 1.2 " 1,1,1-Trichloroelhane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichlorocthene (TCE) ND 1.2 Trichlorotluoroinethane ND 1.2 _ . 1.23-Trichloropropane ND 1.2 1,2,4=I'riin ethyl benzene ND 1.2 1,3,5- Triinethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromgfluoromethanc 92 % { 75 - 122) " Surrogate: Tolucnc48 95 % ( 66», 128 ) " Surrogate: 4-Bronudluorobeu_ene 90 4i, / 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.00cusa.com FAX: 805 925-3376 Page 14 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg 1 BIC0807 03/26/21 14:44 E•PA7471A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B1C0810 03/26/21 13:38 EPA 601OB • Arsenic 2.6 1.8 " Barium 5.8 0.92 Beryllium ND 0.40 Cadmium ND 0.23 Chromium 6.9 0.46 " Cobalt 0.92 0.46 Copper 1.9 0.92 Lead 3.7 0.46 Molvbdenum 2.6 0.46 - Nickel 4.1 0.46 Selenium ND 1.8 " Silver ND 0.46 Thallium ND 0.92 " Vanadium 4.6 1.8 Zinc 6.8 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 35 5.1 mgtkg 1 BIC0802 03/26/21 12:05 EPA 8015M Surrogate: 4-BromoIltrorohen7ene 14IV °S, (31 - 168) Semi -Volatile Organic TPH by GC/FID TPH Diesel (Cl3-C22) 17 9.9 m !kg I BIC0798 03/2621 11:03 EPA 8015M D-04 TPH Motor Oil (C23-C40) 72 50 " " " "11D-04 Surrogate: o-Terphem1 107 `Sb (65 - 133) " " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 79 -4m a =Iar Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 BIC0815 03/26/21 13:09 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 " C'hloroethanc ND 1.2 " Chloroform ND 1.2 Chloromethane ND 1.2 2-C'hlorotoluene ND 1.2 4-C'hlorotohtene ND 1.2 " Dibronwchloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 13-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodifluoromcthane ND 1.2 " 1,1-Dichloroethane ND 1.2 " 1,2-Dichloroethane ND t.2 " " 1.1-Dichloroethene ND 1.2 cis- 1,2-Dich loroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 12-Dichloropropane ND 1.2 " 13-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis- 1.3-Dichloropropenc ND 1.2 trans-1,3-Dichloropropenc ND 1.2 Fthylbcnzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oectisa.com FAX: 805 925-3376 Page 16 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachi orobutadiene ND 1.2 mg/kg 1000 B1('0815 03/26/21 13:08 EPA8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzeue ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 _ 1.1,1,2-Tetrachloroethane ND 1.2 1,1.22-Tetrachloroethane ND 1.2 Tetrachlorocthane WCE) ND 1.2 Toluene ND 1.2 1,2,3-Triclorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " 1,1,2-Trieliloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 " _ .. L2,3-Trichloropropane ND 1.2 1,2.4-Trimethylbenzene ND 1.2 1.3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: 95 % 175 - 122) Surrogate: Toluene-dS 95 "o ( 66. 128 ) Surrogale: 4-Bromo/luorohenzene 9' "S, l 76- 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical t Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg kg 1000 B1('0815 03/26/21 13:34 EPA 8260B Brornobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Brotnoform ND 1.2 Bromonrethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 " Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 - 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethanc ND 1.2 12-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 IA-Dichlorobenzene ND 1.2 Dichloroditluoromcthane ND 1.2 I,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 • cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1.1-Dichlompropene ND 1.2 cis-1.3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) is-07 IIexachIorobutadiene ND 1.2 mglkg 1000 BIC0815 03/26/21 13:34 EPA 826013 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,12-fetrachloroethane ND 1.2 1,1.2,2-'fetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 12,4-Trichlorobenzene ND 1.2 1,1,I-Trichloroethane ND 1.2 1,12-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1,24-Trimethylbenzene ND 1.2 " " 1,3,5-Trimethylbcnzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Dihronwf uoromethanc 95 3- ( 75 - 122 ) Surrogate: Toluene-dS S6 % (66 - 12S) $ro•rogate: 4-Bromofluorobenzenc 94 % 176 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Tank Bottom W. End Sampled: 03/25/21 11:10 Matrix: Solid Sampled by : Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 B 1('0807 03/26/21 14:48 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 C0810 03/26/21 13:44 EPA 601(1B ... Arsenic ND 2.0 Barium 9.9 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 8.0 0.49 Cobalt 1.2 0.49 . Copper 1.6 0.98 Lead 3.4 0.49 Molvbdenum 1.1 0.49 _ Nickel 4.7 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 5.9 2.0 Zinc 7.9 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 6.1 4.5 mg!kg 1 B 1('0804 03/26/21 10:55 HPA 8015M Surrogate 4-Bromo/laorohen::ene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 9.9 mgtkg 1 Bl('0798 03/26/21 10:21 EPA 8015M - TPH Motor Oil (('23-('40) ND 50 " " " 1. Siorogate o-Tetpheni'l 106 %, (65 - 13.3) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by : Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgIg 1000 B 1 C'0815 03/26/21 13:59 FPA 8260B Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 " Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 " Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethanc ND 12 Chloroform ND 1.2 Chloromethanc ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromocthane (ED13) ND 1.2 " Dibromomethane ND 1.2 " 1,2-Dichlorobcnzene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 " 1,4-Dichlorobcnzenc ND 1.2 Dichloroditluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 1, 1 -Dicliloroethene ND 12 cis- l,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethen e ND 1.2 1.2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans- I.3-Dichloropropene ND 1.2 Fthylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 22 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID: 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B1('0815 03/26/21 13:59 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 — Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1.2,2= retrachloroethane ND 1.2 Tetrachlorocthenc (PCE) ND 1.2 Toluene ND 1.2 I.2,3-Trichlorobenzcnc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 " Triehlorolluoromethane ND 1.2 " 1.2,3-Trichloropropane ND 1.2 1,2A-Trimethylbenzene ND 1.2 I.3,5-Trimethylbenzene ND 1.2 Vinyl chloride - ND 1.2 Xylencs (total) ND 1.2 Surrogate: DibrumulLunornetlranr 93 N (75- 122) Surrogate: Toluene-dS 88 °'o ( 66. 128 ) Surrogate: 4-Brunrn/luurubcn_enc 94'X, ( 76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg'kg 1 B I C0807 03/26/21 14:54 EPA 7471 A Total Metals by ICP Antimonv 8.2 2A rrng/kg 1 Bl C'0810 03/26/21 13:47 EPA 601 OB Arsenic 8.9 1.9 Barium 260 0.96 Beryllium ND 0.48 -^ Cadmium ND 0.24 Chromium 55 0.49 " " " " " N-02 Cobalt 12 0.48 - Copper 120 0.96 Lead 550 0.48 " " " " " N-02, N-03 Molybdenum 1.1 0.48 ^ Nickel 150 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 33 1.9 Zinc 720 1.9 STLC Metals by ICP Chromium 0.34 0.10 mg/[. 2 B1D0007 04/01/21 14:40 STI.C/FPA 601 OB - Lead 56 O.1 " " " " " N-07 TCLP Metals by ICP Lead 0.25 0.050 mg/t. 1 B 1 D0112 04/06/21 12:18 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (('5-('12) ND 4.9 mgIg 1 BIC0804 03/26'21 11:52 EPA 8015M R-07 Surrogate: 4-Bromo luorohenzene 100 % (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 71 40 mglkg 4 B IC0798 03/26'21 11:59 EPA 8015M D-04 TPH Motor Oil (C23-C40) 520 200 11 11 11 11 11D-04 Surrogate: o-kiphenYl 108 % (65 - 133) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mg%kg 1000 B 1 C'0815 03/26/21 14:25 EPA 9260B ' Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoforin ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzcne ND 1.2 Chloroethane ND 1.2 Chlorolirn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " _ 1,2-Dibromo-3-chloropropane ND 1.2 " 1.2-Dibromociliane (I:DB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromethanc ND 1.2 I,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 l,l-Dichloroethene ND 1.2 - cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 . y 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 " I,I-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 12 Fthylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: i805 925-3376 Page 26 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analvtical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachIorobutadiene ND 1.2 mg/kg 1000 B I C0815 03/26/21 14:25 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1.1.1.2-Tetrachloroethane ND 1.2 1,1,2.2-Tetrachloroethane ND 1.2 Tctrachlorocthcnc WCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcnzcnc ND 1.2 1.2,4-Trichlorobenzene ND 1.2 1,1,1-Trichlomethane ND 1.2 1.1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1.2.3-Trichloropropane ND 1.2 124-Trimethylbenzene ND 1.2 " 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 12 Surrogate: Dibranglhr nvmetlurrrr 97 ;' ( 7.5 - 122) " Surrogate: Toluene-dS 90 °-„ ( 66- 12S ) " Su wgatc: 4-Bro»tuJlu,» nht•» r'ne RS (76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID : Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mg -kg 1 BIC0807 03/26/21 14:56 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 C0910 03/26/21 13:50 EPA 601 t1B _ Arsenic 4.1 1.9 Barium 180 0.96 Bervllium 0.53 0.48 " . Cadmium ND 0.24 Chromium 78 0.48 " " " " N-02 Cobalt 16 0.48 Copper 31 0.96 Lead 37 0.48 Molybdenum ND 0.48 Nickel 100 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 47 1.9 Zinc 69 1.9 ' STLC Metals by ICP Chromium 0.25 0.10 mg/L 2 BID0007 04/01/21 14:51 STLC/EPA6010B Volatile Organic TPH by GC/FID TPII Gasoline (('5-('12) ND 4.7 mg/kg 1 B 1('0804 03/26/21 12:20 EPA 8015M R-07 Surrogate: 4-Brotno/htorobenzene 107 `%S, (31 - 16S) " Gal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.oecusa.com FAX: 805 925-3376 Page 28 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C134722) 27 9.9 TPH Motor Oil (C23-C40) 610 50 Surrogate: o-Tei phe Yl 107 3, mg!kg 1 BI('0798 03/26/21 13:02 EPA8015M D-06 (65-133) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Volatile Organic Compounds by GC/MS Benzene ND 0.0050 tng/kg 1 B 1('0817 03/26/21 13:46 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobcnzenc ND 0.0050 Chlorocthanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-C'hlorotuluene ND 0.0050 " Dibromochloromethane ND 0.0050 " I.2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (EDB) NU 0.0050 Dibromotnethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1,3-Dichlorobcnzene ND 0.0050 IA-Dichlorobcnzene ND 0.0050 Dichlorodifluoromethanc ND 0.0050 I,l-Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 l,l-Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 1,3-Dichloropropane N1) 0.0050 2,2-Dichloropropane ND 0.0050 1, 1 -Dichloropropene ND 0.0050 cis-1.3-Dichloropropene NU 0.0050 trans-1,3-Dichloropropene ND 0.0050 l`thylbcnzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 30 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by : Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Ilexachlorobutadiene ND 0.0050 mg%kg 1 B1('0817 03/26/21 13:46 F.PA 8260B 4-Isopropyl Toluene ND 0.0050 ' lsopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.00.50 1,1,2,2-Tetrachloroethane ND 0.0050 Tctrachlorocthcnc (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobenzene ND 0,0050 1,2,4-Trichloroben7ene ND 0.0050 I,I,1-Trichloroethane ND 0.0050 1,12-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,23-Trichloropropanc ND 0.0050 1,24-Trimethylbenzene ND 0.0050 13,5-Trinrethylbenz_ene ND 0.0050 Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 Surrogate: Dihrunui/luoruntrthanc 94 % ( 75- 122) Surrogate: Toluene-db' 891S„ ( 66- 12S) Surrogate' 4-Brona,/Ivorohen_ene 89 4'0 ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.14 0.095 mg/kg I B 1 ('0807 03/26/21 14:58 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B 1 C0810 03/26/21 13:52 TPA 6010B Arsenic 5.9 1.9 " Barium 170 0.97 Bervllium 0.50 0.49 " Cadmium ND 0.24 Chromium 41 0.49 " Cobalt 16 0.49 — Copper 27 0.97 Lead 10 0.49 Molybdenum ND 0.49 -• Nickel 38 0.49 Selenium ND 1.9 " Silver ND 0.49 " Thallium ND 0.97 Vanadium 33 1.9 Zinc 27 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.7 ing,kg I BIC0804 03/26/21 12:49 EPA 8015M R-07 Surrogate: 4-Brumn/luornhensene 96 % (31 - 16S ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 BIC0798 03/26/21 10:49 EPA 8015M TPH Motor Oil (C23-C40) 85 50 " " " " 11 Surrogate: o-Teiphern•I 105 % (65 - 133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 BIC0817 03/26/21 14:44 EPA8260B Bromobenzene ND 0.0050 Bromochloromcthane ND 0.0050 Bromodichloromethane ND 0.0050 - Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 " �Chlorocthanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 " " 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 1.2-Dibronio-3-chloropropane ND 0.0050 1.2-Dibromoethane (EDB) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 Dichlorodifluoromethane ND 0.0050 1, 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 �. cis-1,2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 1.2-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 " 1, 1 -Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Ethylbcnzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID : Control Sampled: 03/25/21 11:00 Sampled by: Matrix: Solid Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) Hexachlorobutadiene ND 0.0050 mg'kg I BIC0817 03/26/21 14:44 EPA8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 " Styrene ND 0.0050 1, 1, 1,2-Tetrachloroethane ND 0.0050 " 1,1,2.2-Tetrachloroethane ND 0.0050 " Tctrachlorocthenc (PC E) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobcnzcnc ND 0.0050 1,24-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.005(1 " 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 " Trichlorofluoromethane ND 0.0050 1.2.3-Trichloropropane ND 0.0050 " 1,2,4-Trimethylbenzene ND 0.0050 1.3.5-Trimethylbenzene ND 0.0050 " Vinyl chloride ND 0.0050 X_vIencs (total) ND 0.0050 Sarrogat(,: 93 ':,; ( 75 - 122 ) Surrogate: Toluene-d8 95 'sb ( 66 - 128) Surrogate. 4-Bro1u,/luorohc.71_c'1w 98 ,'„ ( 76 - 122 I The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 34 of 79 161*4yOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by : Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mg/kg 1 B 1 C0807 03/26/21 15:00 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B1 C0810 03/26/21 13:55 EPA 6010B Arsenic 3.6 2.0 Barium 13 LO Beryllium ND 0.50 �. Cadmium ND 0.25 Chromium 11 0.50 Cobalt 1.9 0.50 .� Copper 5.3 1.0 Lead 4.3 0.50 Molybdenum 2.5 0.50 Nickel 9.0 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 8.4 2.0 Zinc 8.8 2.0 ' Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 42 4.9 mg/kg 1 BIC0804 03/26/21 13:17 EPA 8015M Surrogate: 4-13romofluorohenzeue 196 % ( 31 - 168) S-02 Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 9.9 mg/kg 1 BIC0798 03/26/21 10:35 EPA 8015M - . TPH Motor Oil (C23-C40) 52 50 " " " " 11 Surrogate: o-Telphenpd 706 % (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 79 1-7 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 41 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Aeport 101, Sample ID: Soil Pile N Sampled : 03/25/21 11:40 Sampled by: Matrix: Solid Field Data: NA Lab ID : 2101841-10 Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R47 Benzene ND 0,045 mg'kg 1 B 1('0817 03/26/21 12:49 EPA 8260B Bromobenzene ND 0.045 Bromochloromcthane ND 0.045 Bromodichloromethane ND 0.045 Bromoiorm ND 0.045 " Bromomethane ND 0.045 n-But_vlbenzene 0.22 0.045 sec-$ntylbemene 0.11 0.045 tert-Butylbenzene ND 0.045 " Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 Chloroethane ND 0.045 " Chloroform ND 0.045 Chloromethanc ND 0.045 " 2-Chlorowluene ND 0.045 4-Chlorotoluene ND 0.045 " Dibromochloromethane ND 0.045 1,2-Dibromo-3-ehloropropanc ND 0.045 1.2-Dibromoethane (ED13) ND 0.045 Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobenzene ND 0.045 1.4-Dichlorobenzene ND 0.045 Dichloro(litluoromethane ND 0.045 1.1-Dichlorocthanc ND 0.045 1,2-Dichlorocthanc ND 0.045 1, 1 -Dichloroethene ND 0.045 cis- L2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1.3-Dichloropropane ND 0.045 " 2.2-Dichloropropane ND 0.045 1,1-Dichloropropene ND 0,045 cis-l3-Dichloropropene ND 0,045 trans-1,3-Dichloropropene ND 0.045 Ethyl benzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 I I exachlorobutadiene ND 0.045 mg1kg 1 B1('0917 03/26/21 12:49 F.PA8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene 0.15 0.045 Styrene ND 0.045 I,1J_2-Tetrachloroethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachloroethene (PCE) ND 0-045 Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 1,24-Trichlorobenzene ND 0.045 I,1.I-Trichloroethane ND 0.045 1.1.2-Trichloroethane ND 0.045 Trichloroethane (TCE) ND 0.045 Trichlorotluoromethane ND 0.045 1,23-Trichloropropanc ND 0.045 1,2.4-Trimethylbcnzenc ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: Dibromopluoromethane 92 "4, ( 75 - 122) Stn•rogatz: T)luenc-dN 971! (66- 128) Surrogate: d-Bromoguorohenzene 99'.'1-1'1 176 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 79 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples E Sample ID : Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by : Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method N0" Total Metals by CVAA Mercury ND 0.097 mglkg 1 B 1('0807 03/26/21 15:02 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mgukg 1 B1 C0810 03/26/21 14:06 EPA 601013 Arsenic 4.5 2.0 Barium 47 H) Beryllium ND 0.50 Cadmium ND 0.25 Chromium 18 0.50 Cobalt 3.6 0.50 Copper 9.8 1.0 Lead 16 0.50 Molvbdemum 2.1 0.50 Mickel 36 0.50 Selenium ND 2.0 " Silver ND 0.50 Thallium ND H) Vanadium 15 2.0 Zinc 29 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.4 mg/kg 1 BIC0804 03/26/21 13:46 EPA 8015M R-07 Surrogate: a -Brun q luore)hen_ene 100':", (31 - 16S) " Semi -Volatile Organic TPH by GOOD TPI1 Diesel (('13-C22) ND 10 mg'kg I B1('0798 03/26/21 12:27 IPA 8015M TPH Motor Oil (C23-C40) 260 50 " " " Sin•rogatc: o-7i-upheu(11 108'%o (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 79 WK Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0049 mg�kg 1 BIC0817 03/26/21 15:13 EPA 8260B F Bromobenzene ND 0.0049 Bromochloromethane ND 0.0049 Bromodichloromethane ND 0.0049 " . Bromofonn ND 0.0049 Broniomethane ND 0.0049 n-Butylbenzene ND 0.0049 sec-Butylbenzene ND 0.0049 tert-Butylbenzene ND 0.0049 " Carbon tetrachloride ND 0.0049 Chlorobenzenc ND 0.0049 C'hlorocthane ND 0.0049 Chlorofiinn ND 0.0049 C'hloromethane ND 0.0049 2-Chlorotoluenc ND 0.0049 " 4-Chlorotoluenc ND 0.0049 " Dibromochloromethane ND 0.0049 �. 1.2-Dibromo-3-chloropropane ND 0.0049 " 1,2-Dibromoethane(ED13) ND 0.0049 Dibronxnnethane ND 0.0049 1.2-Dichlorobenzene ND 0.0049 1,3-Dichlorobenzene ND 0,0049 14-Dichlorobenzene ND 0.0049 Dichloroditluoromethanc ND 0.0049 '-' 1, 1 -Dichloroethane ND 0.0049 1,2-Dichloroethane ND 0.0049 LI-Dichloroethene ND 0.0049 . - cis-1.2-Dichloroethene ND 0.0049 trans-1,2-Dichloroethene ND 0.0049 1.2-Dichloropropane ND 0.0049 1,3-Dichloropropane ND 0.0049 2.2-Dichloropropane ND 0.0049 1, 1 -Dichloropropene ND 0.0049 cis-1.3-Dichloropropene ND 0.0049 trans-1,3-Dichloropropene ND 0.0049 Ethylbenzenc ND 0.0049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Ana lytical Report for Samples - Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Nates Volatile Organic Compounds by GC/MS (Continued) Ilexachlorobutadiene ND 0.0049 mg'kg 1 BIC0817 03/26/21 15:13 ITA 8260B 4-Isopropyl Toluene ND 0.0049 Isopropylbenzene ND 0.0049 Methylene chloride ND 0.0049 Naphthalene ND 0.0049 n-Propylbenzene ND 0.0049 Styrene ND 0.0049 1, 1. 1,2-Tetrachloroethane ND 0.0049 1,1,2.2-Tetrachloroethanc ND 0.0049 Torachlorocthcnc IPCE) ND 0.0049 Toluene ND 0.0049 1,2,3-Trichlorobenzcne ND 0.0049 1,2,4-Trichloroben7ene ND 0.0049 " I,1,1-Trichloroethane ND 0.0049 1,1,2-Trichloroethane ND 0.0049 " Trichloroethane (TCE) ND 0.0049 Trichlorotluoromethane ND 0.0049 1,2,3-Trichloropropane ND 0.0049 1.24-Trimethylbenzene ND 0.0049 13,5-Triniethylbenzene ND 0,0049 Vinyl chloride ND 0.0049 Xylencs (total) ND 0.0049 Surrogate: Dihrumulluoromeihane 91 S , ( 75 • 121) " Surrogate: Toluene-d& 95 "i, (66 - 128) " Surrogate: 4-Bruniolluorohen_enr 97 °', ( 76 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 79 W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method times Total Metals by CVAA Mercury ND 0.097 mg'kg 1 B1 C0907 03/26/21 15:04 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mgtkg 1 B1C'0810 03/26/2114:09 EPA601013 Arsenic 5.6 1.9 Barium 23 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 14 0.47 Cobalt 2.5 0.47 Copper 6.8 0.93 Lead 7.3 0.47 Molybdenum 3.7 0.47 Nickel 11 0.47 Selenium ND 1.9 Silver ND 0.47 " Thallium ND 0.93 Vanadium 15 1.9 Zinc 15 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.7 mg/kg 1 BIC0804 03/26/21 14:14 EPA 8015M R-07 Surrogatc: 4-Bromo/hmrohen_c.ne 103 % (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPII Diesel (Cl3-('22) ND 9.9 mg'kg 1 B1C'0798 0312621 11:17 EPA 9015M - TPH Motor Oil (C23-C40) 75 50 " " D-04 Surrogate: o4i,tphcm.l 107 "i, (65 - 133) " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 41 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 BIC0817 03/26/2115:43 ITA8260B - Broniobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 - Bromofbrm ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tent-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 " Chlorobenzcne ND 0.0050 Chlorocthanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorololuene ND 0.0050 " Dibromochloromethanc ND 0.0050 .- 1.2-Dibronio-3-chloropropane ND 0.0050 " 1,2-Dibronioethane (EDB) ND 0.0050 Dibronioniethanc ND 0.0050 1.2-Dichlorobenzene ND 0.0050 -- 1.3-Dichlorobenzenc ND 0.0050 14-Dichlorobenzenc ND 0.0050 Dichloroditluoromcthanc ND 0.0050 " '- 1,1-Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 I,1-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 trans-1,2-Dicliloroetliene ND 0.0050 1,2-Dichloropropane ND 0.0050 1.3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 1,1-Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethylbenzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 42 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by : Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Ilexachlorobutadiene ND 0.0050 mg/kg 1 BIC0817 03/26/21 15:43 ITA8200B ' 4-Isopropyl Toluene ND 0.0050 Isopropylbcuzene ND 0,0050 Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzene ND 0.11050 Styrene ND 0.0050 " ._, 1, 1. 1,2-Tetrachloroethane ND 0.0050 1,1,2,2-Tetrachloroethane ND 0.0050 Tctrachloroethene (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobenzenc ND 0.0050 " 1,2,4-Trichlorobenzene ND 0.0050 1, 1, I-Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethane (TCE) ND 0.0050 Trichlorotluoromethane ND 0.0050 1,2.3-Trichloropropane ND 0.0050 1.24-Trimethylbenzene ND 0.0050 1,3.5-Trimethylbenzene ND 0.0050 " Vinyl chloride - ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: Uibrunurlluurumedrane 91 4& 175 - 122 ) Surrogate: Toluene-dR 94 IN ( 66 - 128) " Surrogate: 4-Bronur/hun'obcn_cne 97 i.`, ( 76 - 12 2) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA _ Mercury ND 0.090 mg/kg I B1('0807 03/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgikg 1 BIC0810 03/2621 14:11 EPA 6010B - Arsenic 2.0 1.9 " Barium 5.5 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 6.4 0.48 Cobalt 0.76 0.48 Copper 1.8 0.96 . Lead 3.7 0.48 Molybdenum 1.6 0.49 Nickel 3.9 0.48 Selenium ND 1.9 Silver ND 0.49 Thallium F ND 0.96 Vanadium 5.2 1.9 Zinc 5.2 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) ND 4.9 mg/kg 1 B I C0804 03/26/21 14:42 EPA 8015M R-07 Srnrngute: 4-Brnvw/hunubcrccnc• 102 %, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPII Diesel Wl3-('22) ND 10 mgIg 1 BIC0798 03/26 21 11:45 EPA 8015M TPH Motor Oil (C23-C40) 120 50 " " " " 1. Sm-rogatc: o-7ecphenl-1 107 3 ; (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: {805) 925-3376 Page 44 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0050 mg,kg 1 BIC0817 03/26/21 16:12 ITA8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 r sec-Butylbenzene ND 0.0050 tort-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzenc ND 0.0050 Chloroethane ND 0.0050 " Chloroform ND 0.0050 Chloromethane ND 0.0050 " ' 2-Chlorotohtene ND 0,0050 4-Chlorotoluene ND 0.0050 " Dibromochloromethane ND 0.0050 " 12-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (ED13) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1,3-Dichlorobcnzcnc ND 0.0050 I A-Dichlorobcnzcnc ND 0.0050 " Dichloroditluoromethane ND 0.0050 " 1, 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 I,1-Dichloroethene ND 0.0050 - - cis-1,2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " 1.2-Dichloropropane ND 0.0050 " 1.3-Dichloropropane ND 0.0050 " 2.2-Dichloropropane ND 0.0050 1,1-Dichloropropane ND 0.0050 cis-1.3-Dichloropropcnc ND 0_0050 trans-1,3-Dichloropropcnc ND 0.0050 Ethylbcnzcne ND 0.00.50 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 45 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) Elexachlorobutadiene ND 0.0050 mg,kg 1 BIC0817 03/26/21 16:12 EPA8260B 4-1sopmpyl Toluene ND 0.0050 lsopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1, 1. 1,2-Tetrachloroethane ND 0.0050 1.12.2-Tetrachloroethane ND 0.0050 Tctrachlorocthcne (1'CE) ND 0.0050 Toluene ND 0.0050 1.2,3-Trichlorobcnzene ND 0.0050 1,24-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 I.1,2-Trichloroethane ND 0.0050 Trichloroethane (TCE) ND 0.0050 Trichlorotluorotnethane ND 0.0050 1,23-Trichloropropane ND 0.0050 1,24-Trimethylbenzene ND 0.0050 1,3,5-Trimethylbenzene ND 0,0050 Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate. Uihromolluoromethunr 91 % (75 - 12 2) Surrogate: Toluene-d8 95 N, ( 66 - 128) " Surrogate: 4-Bronwf toruhen_enc 97 `:o ( 76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 46 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total �Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes • i Level Result Limits Limit Batch BIC0807 -EPA 7471A Preparation: EPA 7471A Prep 03/26/21 07:43 - - Blank (BlC0807-BLKI) Analyzed: 03/26/21 13:21 Mercury ND 0.10 mglkg LCS (BlC0807-BSI) Analyzed: 03/26/21 13:17 Mercury 0.792 0.10 mg'kg 0.833 95 85-115 LCS Dup (BlC0807-BSDI) Analyzed: 03/26/21 13:19 Mercury 0.793 0.10 mg/kg 0.833 94 85-115 1 20 Duplicate (B1C0807-DUPl) Source: 2101842-02 Analyzed: 03/26/21 13:25 Mercury 0.0556 0.096 mg%kg 0.0554 0.3 20 Matrix Spike (BlC0807-MS1) Source: 2101842-02 Analyzed: 03/26/21 13:27 Mercury 0.855 0.096 mg'kg 0.796 0.0554 100 75-125 Matrix Spike Dup (B1C0807-MSD1) Source: 2101842-02 Analyzed: 03/26/21 13:29 Mercury 0.750 0.087 mgIg 0.727 0.0554 96 75-125 13 20 Post Spike (B1C0807-PSI) Source: 2101842-02 Analyzed: 03/26/21 13:31 Mercury 5.17 ug/L 5.00 0.347 97 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0810 -EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 • Blank (B1C0810-BLKI) Analyzed: 03/26/21 12:16 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND LO Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " _.. Cobalt ND 0.50 " Copper ND LO " Lead ND 0.50 Molybdenum ND 0.50 " '- Nickel ND 0.50 Selenium ND 2.0 " Silver ND 0.50 Thallium ND 1.0 " Vanadium ND 2.0 " Zinc ND 2.0 " LCS (BlC0810-BS1) Analyzed: 03/26/21 12:40 Antimony 100 2.5 mgIg 100 100 80-120 Arsenic 101 2.0 100 MI 80-120 Barium 102 1.0 100 102 80-120 �.. Beryllium 103 0.50 100 103 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 103 0.50 100 103 80-120 Cobalt 103 0.50 100 103 80-120 Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 100 0.50 100 100 80-120 Nickel 103 0.50 100 103 80-120. Selenium 100 2.0 100 100 80-120 Silver 5.06 0.50 5.00 101 80-120 Thallium 104 1.0 100 104 80-120 - Vanadium 100 2.0 100 100 80-120 Zinc 103 2.0 100 103 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www_oecusa.com FAX: (805) 925-3376 Page 48 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 LCS Dup (B1C0810-BSDI) Analyzed: 03/26/21 12:43 Antimony 101 2.5 mg/kg 100 WI 80-120 0.7 20 Arsenic 102 2.0 100 102 80-120 0.9 20 Barium 102 1.0 100 102 80-120 0.3 20 Beryllium 104 0.50 100 104 80-120 0.9 20 Cadmium 103 0.25 100 103 80-120 0.5 20 Chromium 104 0.50 100 104 80-120 1 20 Cobalt 104 0.50 100 104 80-120 0.5 20 Copper 104 1.0 100 104 80-120 0.9 20 Lead 104 0.50 100 104 80-120 0.8 20 Molybdenum 101 0.50 100 101 80-120 0.9 20 Nickel 104 0.50 100 104 80-120 0.5 20 Selenium 101 2.0 100 101 80-120 0.7 20 Silver 5.16 0.50 5.00 103 80-120 2 20 Thallium 104 H) 100 104 80-120 0.3 20 Nanadium 102 2.0 100 102 80-120 1 20 Zinc 103 2.0 100 103 80-120 0.5 20 Duplicate (B1C0810-DUPI) Source: 2101840-03 Analyzed: 03/26/21 13:06 Antimom ND 2.4 mg/kg 0.966 20 Arsenic 2.64 1.9 3.12 17 20 Barium 118 0.95 116 2 20 Beryllium ND 0.47 ND 20 Cadmium ND 0.24 ND 20 Chromium 16.3 0.47 17.6 8 20 Cobalt 3.67 0.47 4.26 15 20 Copper 9.50 0.95 8.79 8 20 Lead 6.24 0.47 5.56 12 20 Molybdenum 1.46 0.47 1.27 14 20 Nickel 20.8 0.47 23.4 12 20 Selenium ND 1.9 ND 20 Silver ND 0.47 ND 20 Thallium ND 0.95 ND 20 Vanadium 15.0 1.9 15.4 3 20 Zinc 34.0 1.9 29.6 14 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 49 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by ICP - Quality Control I Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Matrix Spike (B1C0810-MS1) Source: 2101840-03 Analyzed: 03/26/21 12:45 Antimony 49.8 2.4 mg/kg 97.6 ND 51 10-116 Arsenic 100 2.0 97.6 3.12 100 77-121 Barium 196 0.98 97.6 116 82 30-169 Beryllium 98.3 0.49 97.0 ND 101 86-111 Cadmium 93.4 0.24 97.6 ND 96 81-112 Chromium 113 0.49 97.6 17.6 97 75-129 Cobalt 96.4 0.49 97.6 4.26 94 71-121 Copper 106 0.98 97.6 8.79 100 68-135 Lead 99.5 0.49 97.6 5.56 95 72-121 Molybdenum 89.8 0.49 97.6 1.27 91 70-112 Nickel 111 0.49 97.6 23.4 90 73-121 Selenium 94.7 2.0 97.0 ND 97 76-116 Silver 4.74 0.49 4.88 ND 97 54-132 Thallium 91.2 0.98 97.6 ND 93 64-120 Vanadium 112 2.0 97.6 15.4 99 78-124 7.inc 122 2.0 97.0 29.0 95 50-143 Matrix Spike Dup (B1C0810-MSDI) Source: 2101840-03 Analyzed: 03/26/21 12:55 Antimony 48.3 2.5 mg/kg 98.0 ND 49 10-116 3 20 ,arsenic 102 2.0 98.0 3.12 101 77-121 1 20 Barium 203 0.98 98.0 116 89 30-169 4 20 Beryllium 99.4 0.49 98.0 ND WI 86-111 1 20 Cadmium 95.0 0.25 98.0 ND 97 81-112 2 20 Chromium 117 0.49 98.0 17.6 101 75-129 4 20 Cobalt 98.2 0.49 98.0 4.26 96 71-121 2 20 Copper 110 0.98 98.0 8.79 103 68-135 3 20 Lead 100 0.49 98.0 5.56 97 72-121 2 20 Molybdenum 91.3 0.49 98.0 1.27 92 70-112 2 20 Nickel 113 0.49 98.0 23.4 92 73-121 2 20 Selenium 96.4 20 98.0 ND 98 76-116 2 20 Silver 4.89 0.49 4.90 ND 100 54-132 3 20 Thallitan 93.1 0 98 98.0 ND 95 64-120 2 20 Vanadium 115 2.0 98.0 15.4 102 78-124 3 20 Zinc 124 2.0 98.0 29.6 96 50-143 1 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 50 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by ICP - Quality Coutrol Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Post Spike (B1C0810-PSI) Source: 2101840-03 Analyzed: 03/26/21 12:58 Antimony 1.97 mg/l. 2.00 0.0203 98 75-125 Arsenic 2.08 2.00 0.0657 101 75-125 Barium 4.38 2.00 2.43 97 75-125 Beryllium 1.99 2.00 0.00456 99 75-125 Cadmium 1.89 2.00 -0.00476 94 75-125 Chromium 2.37 2.00 0.370 100 75-125 Cobalt 1.97 2.00 0.0898 94 75-125 Copper 2.25 2.00 0.185 103 75-125 Lead 2.02 2.00 0.117 95 75-125 Molybdenum 1.98 2.00 0.0268 98 75-125 Nickel 2.37 2.00 0.492 94 75-125 Selenium 1.97 2.00 0,000298 98 75-125 Silver 0.0974 0.100 -0.00288 97 75-125 Thallium 1.88 2.00 -0.0363 94 75-125 Vanadium 2.30 2.00 0.324 99 75-125 Zinc 2.50 2.00 0.623 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 51 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 STLC Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0007 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/01/21 09:01 -- Blank (B1D0007-BLKl) Analyzed: 04/01/21 14:11 Chromium ND 0.050 mg/1. Lead ND 0.050 ° LCS (B1D0007-BS1) Analyzed: 04/01/21 14:24 Chromium 9.98 0.050 mg/L 10.0 100 80-120 Lead 10.0 0.050 1110.0 100 80-120 LCS Dup (B1D0007-BSDl) Analyzed: 04/01/21 14:27 Chromium 9.99 0.050 mg/I. 10.0 99 80-120 0.9 20 Lead 9.90 0.050 1110.0 99 80-120 2 20 Duplicate (B1D0007-DUPl) Source: 2101841-07 Analyzed: 04/O1/21 14:42 Chromium 0.341 0.10 mg/L 0.342 0.3 20 Lead 58.7 0.10 1156.1 4 20 - Leach Fluid Blank (B1D0007-LBKl) Analyzed: 04/01/21 14:13 Chromium ND 0.10 mg/L Lead ND 0.10 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 52 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0112 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/06/21 10:26 Blank (B1D0112-BLK1) Analyzed: 04/06/21 12:08 Lead ND 0.050 mg/L LCS (B1D0112-BS1) Analyzed: 04/06/21 12:13 Lead 9.64 0.050 111g/1, 10.0 96 80-120 LCS Dup (B1D0112-BSD1) Analyzed: 04/06/21 12:16 Lcad 9.78 0.050 mg/I. 10.0 98 80-120 1 20 Duplicate (B1D0112-DUPl) Source: 2101841-07 Analyzed: 04/06/21 12:21 Lcad 0.242 0.050 mg/I, 0.246 2 20 Leach Fluid Blank (B1D0112-LBK1) Analyzed: 04/06/21 12:11 Lcad ND 0.050 mg/L The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 53 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0802 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:22 Blank (BlC0802-BLK1) Analyzed: 03/26/21 08:30 TPII Gasoline (C5-('l2) ND 0.50 mg,zkg Surrogate:4-Bromglluorobenzene 0.127 110.125 101 31-165 LCS (BlC0802-BS1) Analyzed: 03/26/21 06:59 TPH Gasoline (C5-('12) 1.01 0.50 mgtkg 1.00 101 62-151 Surrogate:4-Brzmzolluorohenzene, 0.152 110.125 121 31-168 LCS Dup (BlC0802-BSDI) Analyzed: 03/26/21 07:25 TP11 Gasoline (C5-C12) 0.958 0.50 mg/kg 0.996 96 62-151 5 20 Surrogate: 4-Brotngluorohenzene 0.142 110.125 114 31-168 Duplicate (B1C0802-DUP1) Source: 2101840-01 Analyzed: 03/26/21 09:29 TPH Gasoline (C5-('12) ND 0.50 mgtkg ND 20 Surrogate:4-Bromolluorohenzene 0.131 110.124 105 31-168 Matrix Spike (BlC0802-MSI) Source: 2101836-04 Analyzed: 03/26/21 16:07 TPH Gasoline (C5-(' l2) 0.989 0.50 mg -'kg 1.00 ND 99 10-166 Surrogate:4-Bromo/luorohenzcm, 0.146 110.126 116 31-168 Matrix Spike Dup (B1C0802-MSDI) Source: 2101836-04 Analyzed: 03/26/21 16:33 TPH Gasoline (('5-C12) 0.971 0.50 mg/kg 0.992 ND 98 10-166 2 20 Surrogate: 4-Bro nolluwnbenzene 0.149 110.124 120 31-168 Batch BIC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Blank (Bl C0804-BLK1) Analyzed: 03/26/21 10:27 TPH Gasoline (C5-('12) ND 0.50 mg/kg Surrogate:4-Brotnallnorohenzene 0.133 110.12.5 107 31-168 LCS (BlC0804-BSI) Analyzed: 03/26/21 09:30 TPH Gasoline (C5-('12) 1.24 0.50 mgfkg 0.998 124 62-151 Surrogate:4-Bromohuorohenrene 0.147 110.125 118 31-165 LCS Dup (B1C0804-BSDI) Analyzed: 03/26/21 09:59 TPH Gasoline (C5-('12) 1.32 0.50 mgtkg 0.998 132 62-151 7 20 Surrogate: 4-Brolno luornhen_ene 0.104 110.125 131 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 54 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic TPH by GC/FID - Quality Control I .nalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 - Duplicate (B1C0804-DUPl) Source: 2101841-06 Analyzed: 03/26/21 11:24 TPH Gasoline (('5-('12) 10.0 4.3 nig/kg 6.12 48 20 QR-03 Surrogate:4-Bromolluorobcnrcate 1.38 111.08 128 31-168 Matrix Spike (B1C0804-MS1) Source: 2101838-06 Analyzed: 03/26/21 20:00 TP1I Gasoline (C5-('12) 1.13 0.49 mg/kg 0.979 ND 116 10-166 Surrogate. 4-Bromolluorohenzene 0.159 110.122 130 31-168 Matrix Spike Dup (BlC0804-MSD1) Source: 2101838-06 Analyzed: 03/26/21 20:29 TPH Gasoline (C5-C12) 1.21 0.50 mg!kg 1.00 ND 120 10-166 6 20 Surrogate:4-Bromq/luorobenzene 0.155 0.125 123 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 805 925-3376 Page 55 of 79 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Semi -Volatile Organic TPH by GC/FID - Quality Control IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0798 - EPA 8015M Preparation: EPA 3550C 03/25/21 17:29 Blank (BlC0798-BLKI) Analyzed: 03/26/21 07:35 TPH Diesel (C13-('22) ND 10 mg/kg TPI I Motor Oil (C'23-C40) ND 50 Surrogate: o-TefphenYl 53.7 49.8 108 65-133 LCS (B1C0798-BSI) Analyzed: 03/26/21 07:07 TPH Diesel (C13-C22) 508 9.9 mg/kg 496 102 77-114 TPH Motor Oil (C23-C40) 549 50 496 111 76-128 Surrogate: o-Terphegcl 50.7 49.6 102 65-133 LCS Dup (BIC0798-BSD1) Analyzed: 03/26/21 07:21 TPH Diesel (CI3-C22) 501 9.9 mg/kg 497 101 77-114 1 20 TPH Motor Oil (C23-C40) 557 50 497 112 76-128 2 20 Surrogate: o-Teipher-rl 53.5 49.7 108 65-133 Duplicate (BlC0798-DUPI) Source: 2101840-01 Analyzed: 03/26/21 08:44 TPII Diesel (C13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) 43.1 50 44.8 4 20 Surrogate: o-Teiphen.Vl 53.4 49.h' 107 65-133 Matrix Spike (B1C0798-MS1) Source: 2101840-01 Analyzed: 03/26/21 13:48 TPFI Dicscl Wl3-C 22) 507 9.9 mg/kg 497 ND 102 45-149 TPH Motor Oil (C23-C40) 556 50 497 44.8 103 34-175 Surrogate: o-Teiphem•1 55.9 49.7 113 65-133 Matrix Spike Dup (BlC0798-MSD1) Source: 2101940-01 Analyzed: 03/26/21 14:02 TPH Diesel (('13-C22) 488 10 nig/kg 499 ND 98 45-149 4 20 TPII Motor Oil (('23-C40) 548 50 499 44.8 101 34-175 1 20 SmrogaR: o-Teipltcm./ 55.2 49.9 1/1 65-133 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 56 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank(B1C0815-BLK1) Analyzed: 03/26/21 11:26 Benzene ND 0.25 mg/kg Bromobenzene ND 0.25 " Bromochloromcthanc ND 0.25 " Bromodichloromethane ND 0.25 Bromofonn ND 0.25 " Bromomethane ND 0.25 n-Butylbenzene ND 0.25 " sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 '- Chlorobenzene ND 0.25 Chloroethane ND 0.25 " Chloroform ND 0.25 " Chloromethane ND 0.25 2-Chlorotoluene ND 0.25 4-Chlorotoluene ND 0.25 " Dibromochloromethanc ND 0.25 " - . 1,2-Dibromo-3-chloropropane ND 0.25 " 1,2-Dibromoethane (EDB) ND 0.25 " Dibromomethanc ND 0.25 " 1,2-Diclilorobenzene ND 0.25 " 1,3-Dichlorobenzenc ND 0.25 1,4-Dichlorobenzenc ND 0.25 Dichloroditluoromcthane ND 0.25 " 1, 1 -Dichloroethane ND 0.25 12-Dichloroethane ND 0.25 1,1-Dichloroethene ND 0.25 " cis-1,2-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 " 1.2-Dichloropropane ND 0.25 " 13-Dichoropropane ND 0.25 " 2,2-Dichloropropane ND 0.25 " 1,1-Dichloropropene ND 0.25 cis-1.3-Dichloropropene ND 0.25 " trans-1,3-Dichloropropene ND 0.25 " r, Ethylbenzene ND 0.25 " Hexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 r N9ethylene chloride NI7 0.25 " Naphthalene ND 0.25 n-Propylbenzene ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 57 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilepo Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 - Blank (BlC0815-BLK1) Analyzed: 03/26/21 11:26 Styrene ND 0.25 mgIg 1, 1, 1,2-Tetrachloroethane ND 0.25 1,1.2,2-Tetrachloroethane ND 0.25 " Tetrachloroethene (PCE) ND 0.25 Toluene ND 0.25 " 1,2.3-Trichlorobenzene ND 0.25 1,2,4-Trichlorobenzene ND 0.25 " 1,1,1-Trirhloroethane ND 0.25 1,1.2-Trichloroethane ND 0.25 " Trichloroethene (TCE) ND 0.25 " Trichlorotluoromethane ND 0.25 1,23-Trichloropropane ND 0.25 L2,4-Trimethylbenzene ND 0.25 1,3,5-Trimethylbenzene ND 0.25 Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 " Surrogate: Dibromolluoromcthane 0.0445 0.0498 89 75-122 • Surrogate: Toluene-d8 0.0455 0.0498 91 66-128 Sm•rogate:4-Br•omo/luoroben:ent, 0.0479 0.0498 96 76-122 LCS (BlC0815-BSI) Analyzed: 03/26/21 09:44 Benzene 1.80 0.25 mgIg 1.99 91 75-131 Bromobenzene 1.97 0.25 1.99 99 75-136 Bromochloromethanc 1.67 0.25 1.99 84 70-135 Bromodichloromethane 1.84 0.25 1.99 93 76-137 l3ronmform 1.68 0.25 1.99 85 55-139 Bromomethane 1.49 0.25 1.99 75 10-157 u-Butylbenzene 2.38 0.25 1.99 120 62-166 sec-Butylbenzene 2.50 0.25 1.99 126 72-167 tort-Butylbenzene 2.33 0.25 1.99 117 69-158 Carbon tetrachloride 1.77 0.25 1.99 89 70-140 C'hlorobenzene 1.94 0.2.5 1.99 98 76-137 - Chloroethane 2.09 0.25 1.99 105 I0-164 Chloroform 1.80 0.25 1.99 91 75-123 C'hloromethane 1.73 0.25 1.99 87 26-140 2-Chlorotoluene 2.11 0.25 1.99 106 73-145 4-Chlorotoluene 2.13 0.25 1.99 107 67-151 Dibromochloromethane 1.80 0.25 1.99 90 68-144 1,2-I)ibromo-3-chloropropanc 1.63 0.25 1.99 82 45-148 12-Dibromoethane (EDB) 1.80 0.25 1.99 91 73-134 Dibromomethanc 1.66 0.25 1.99 84 70-140 1,2-Dichlorobenzene 2.15 0.25 1,99 108 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 58 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 -• LCS (BlC0815-BS1) Analyzed: 03/26/21 09:44 1,3-Dichlorobenzcnc 2.19 0.25 mg/kg 1.99 110 76-146 1,4-Dichlorobenzene 2.10 0.25 1.99 106 72-140 Dichlorodifluoromcthanc 1.73 0.25 1.99 87 10-166 1, 1 -Dichloroethane 1.82 0.25 1.99 92 65-139 1,2-Dichlorocthene 1.80 0.25 1.99 90 67-125 1J-Dichloroethene 2.05 0.25 1.99 103 54-168 cis-1.2-Dichloroethene 1.80 0.25 1.99 91 74-135 trans-1,2-Dichloroethene 1.98 0.25 1.99 100 68-149 1,2-Dichloropropane 1.77 0.25 1.99 89 74-130 1.3-Dichloropropane 1.83 025 1.99 92 68-130 -' 2,2-Dichloropropane 1.95 0.25 1.99 98 33-187 1, 1 -Dichloropropene 1.95 0.25 1.99 98 71-140 cis-1.3-Dichloropropene 1.79 0.25 1.99 90 78-135 trans-1,3-Dichloropropene 1.90 0.25 1.99 96 70-137 Ethylbenzene 1.93 0.25 1.99 97 69-143 11exachlorobutadiene 3.12 0.25 1.99 157 69-203 4-Isopropyl Toluene 2.38 0.25 1.99 120 74-154 Isopmpylbenzene 2.11 0.25 1.99 106 72-157 Methylene chloride 1.75 0.25 1.99 88 49-129 Naphthalene 1.84 0.25 1.99 93 61-158 n-Propylbenzene 2.17 0.25 1.99 109 69-147 Styrcne 1.92 0.25 1.99 97 71-144 1,1,1,2-Tetrachloroethane 1.92 0.25 1.99 97 78-132 1,1,2,2-1'etrachlorocthane 1.90 0.25 1.99 96 64-138 Tetrachloroethene (PCE) 2.09 0.25 1.99 105 74-148 Toluene 1.82 0.25 199 92 76-131 1,23-Trichlorobenzene 2.11 0.25 1.99 106 63-170 1,24-Trichlorobenzene 2.20 0.25 1.99 110 71-165 1, 1, 1 -Trichloroethanc 1.97 0.25 1.99 99 74-137 1,12-Trichloroethane 1.82 0.25 1.99 91 68-134 Trichloroethene (TC E) 1.94 025 1.99 98 79-139 Trichlorofluoromethane 2.20 0.25 1.99 111 32-154 1,2,3-Trichloropropane 1.77 0.25 1.99 89 69-125 1,2,4-Trimethylbenzene 2.14 0.25 1.99 108 67-144 13.5-Trimethylben7ene 2.17 0.25 1.99 109 66-154 Vinyl chloride 2.27 0.25 1.99 114 39-150 Xylenes (total) 5.95 0.25 5.96 100 71-147 Surrogate: Uibromolluaromc'thunc 0.0496 0.0497 100 75-123 Surrogate: Toluene -de 0.0462 " 0.0497 93 66-128 - ' Sm-rogate: 4-Bromolluorohen_e11e 0.0451 0.0497 91 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 59 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (BlC0815-BSD1) Analyzed: 03/26/21 10:09 Benzene 1.87 0.25 mg%kg 2.00 94 75-131 4 20 Bromobenzene 2.02 0.25 2.00 101 75-136 2 20 Bromochloromethanc 1.69 0.25 2.00 85 70-135 2 20 Bromodichloromethane 1.93 0.25 2.00 97 76-137 5 20 Bromoform 1.80 0.25 2.00 90 55-139 7 20 Bromomethane 1.21 0.25 2.00 61 10-157 20 20 u-Butylbenzene 2.45 0.25 2.00 123 62-166 3 20 sec-Butylbenzene 2.48 0.25 2.00 124 72-167 0.9 20 tert-Butylbenzene 2.38 0.25 2.00 119 69-158 2 20 Carbon tetrachloride 1.87 0.25 2.00 94 70-140 6 20 Chlorobenzene 2.07 0.25 2.00 104 76-137 7 20 Chloroethane 2.21 0.25 2.00 111 10-164 6 20 Chloroform 1.81 0.25 2.00 90 75-123 0.4 20 Chloromethane 1.82 0.25 2.00 91 26-140 5 20 2-Chlorutoluene 2.26 0.25 2.00 113 73-145 7 20 4-C'hlorotolLien e 2.25 0.25 2.00 112 67-151 5 20 Dibromochloromethane 1.97 0.25 2.00 98 68-144 9 20 1,2-Dibronx•-3-chloropropane 1.84 0.25 2.00 92 45-148 12 20 1.2-Dibromoethane (ED13) 1.98 0.25 2.00 99 73-134 9 20 Dibromomethane 1.75 0.25 2.00 87 70-140 5 20 1,2-Dichlorobenzene 2.18 0.25 2.00 109 78-142 1 20 1,3-Dichlorobenzene 2.30 0.25 2.00 115 76-146 5 20 1,4-Dichlorobenzene 2.06 0.25 2.00 103 72-140 2 20 Dichlorodifluoromethanc 1.73 0.25 2.00 86 10-166 0.1 20 1.1-Dichloroethane 1.95 0.25 2.00 98 65-139 7 20 1.2-Dichloroethanc 1.93 0.25 2.00 96 67-125 7 20 1.1-Dichloroethene 2.07 0.25 2,00 103 54-168 0.6 20 cis-L2-Dichloroethene 1.86 0.25 2.00 93 74-135 4 20 - trans-1,2-Dichloroethene 2.11 0.25 2.00 105 68-149 6 20 1,2-Dichloropropene 1.82 0.25 2.00 91 74-130 3 20 1,3-Dichloropropene 1.84 0.25 2.00 92 68-130 0.6 20 2,2-Dichloropropane 1.94 0.25 2.00 97 33-187 0.4 20 1,1-Dichloropropene 2.04 0.25 2.00 102 71-140 5 20 cis-13-Dichloropropene 1.80 0.25 2.00 90 78-135 0.5 20 trans-1,3-Dichloropropene 1.94 0.25 2.00 97 70-137 2 20 - Ethvlbenzene 2.06 0.25 2.00 103 69-143 6 20 Hexachlorobutadiene 3.30 0.25 2.00 165 69-203 6 20 4-Isopropyl Toluene 2.42 0.25 2.00 121 74-154 2 20 Isopropylbenzene 2,19 0.25 2.00 109 72-157 3 20 Methylene chloride 1.87 0.25 2.00 94 49-129 7 20 Naphthalene 2.04 0.25 2.00 102 61-158 1O 20 n-Propylbenzene 2.30 0.25 2.00 115 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl!ient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 60 of 79 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilept Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 - LCS Dup (BlC0815-BSDI) Analyzed: 03/26/21 10:09 Styrene 2.06 0.25 mgtkg 2.00 103 71-144 7 20 1,1,1,2-Tetrachloroethane 2.04 0.25 2.00 102 78-132 6 20 1,1,2.2-Tetrachloroethane 2.02 0.25 2.00 101 64-138 6 20 Tetrachloroethane (PCE) 2.18 0.25 2.00 109 74-149 4 20 TOILICnC 1.91 0.25 2.00 96 76-131 5 20 1,2,3-Trichlorobenzene 2.36 0.25 2.00 118 63-170 12 20 _- 1,2,4-Trichlorobenzene 2.37 0.25 2.00 118 71-165 7 20 1, 1, 1 -Trichloroethane 1.98 025 2.00 99 74-137 0.8 20 1,12-Trichloroethane 1.92 0.25 2.00 96 68-134 6 20 Trichloroethene (TCE) 1.92 0.25 2.00 96 79-139 0.9 20 ^" Trichlorofluoromethane 2.15 0.25 2.00 107 32-154 3 20 1.2,3-Trichloropropane 1.78 0.25 2.00 89 69-125 0.3 20 1.2,4-Trimethylbenzene 2.19 0.25 2.00 I10 67-144 2 20 1,3,5-Trim ethylbenzene 2.24 0.25 2.00 112 66-154 3 20 Vinyl chloride 2.22 0.25 2.00 111 39-150 2 20 Xylenes (total) 6.14 0.25 0.00 102 71-147 3 20 Surrogate: Dibronui/hwrom<•thciitc. 0.0492 0.0500 98 75-122 - - Surrogate: Toluene-d8 0.0452 0.0500 90 66-128 Sm-rogate:4-Bromolhmrobenrene 0.0464 " 0.0500 93 76-122 Duplicate (B1C0815-DUPI) Source: 2101841-07 Analyzed: 03/26/21 14:51 Benzene ND 1.2 mg/kg ND 20 Bromobenzenc ND 1.2 ND 20 Bromochloromcthane ND 1.2 ND 20 Bromodichloromethane ND 1.2 ND 20 Bromoform ND 1.2 ND 20 Bromomethane ND 1.2 ND 20 n-Butylbenzene ND 1.2 ND 20 -, sec-Butylbenzene ND 1.2 " ND 20 tert-Butylbenzene ND 12 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzene ND 1.2 ND 20 - C'hloroethane ND 1.2 ND 20 Chlorofonn ND 1.2 ND 20 C'hloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 - 4-Chlorotoluene ND 1.2 ND 20 Dibromochloromethane ND 1.2 ND 20 1,2-Dibromo-3-chloropropane ND 1.2 ND 20 _ 1,2-Dibromoethane (EDI3) ND 1.2 ND 20 Dibromomethanc ND 1.2 ND 20 1,2-Dichlorobenzene ND 1.2 NI) 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 61 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Duplicate (B1C0815-DUPI) Source: 2101841-07 Analyzed: 03/26/21 14:51 1,3-Dichlorobenzenc ND 1.2 mg/kg NI) 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichlorodifluoromethanc ND 1.2 NI) 20 1, 1 -Dichloroethane NI) 1.2 ND 20 1,2-Dichlorocthanc ND 12 ND 20 1,1-Dichloroethene NI) 1.2 ND 20 cis-1.2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene NI) 1.2 ND 20 1,2-Dichloropropane ND 1.2 ND 20 13-Dichloropropane ND 1.2 ND 20 - 2,2-Dichloropropane ND 1.2 ND 20 1,1-Dichloropropene NI) 1.2 ND 20 cis-1.3-Dichloropropene ND 1.2 NI) 20 trans-1,3-Dichloropropene ND 1.2 NI) 20 Lthylbenzene NI) 1.2 ND 20 Ilexachlorobutadiene NI) 1.2 ND 20 4-Isopropyl Toluene ND 1.2 NI) 20 Isopropylbenzene ND 1.2 ND 20 Methylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 NI) 20 n-Propylbenzene NI) 1.2 NI) 20 " Styrene ND 1.2 NI) 20 1,1,1,2-Tetrachloroethane NI) 1.2 NI) 20 1,1,2,2-Tetrachloroethane ND 1.2 ND 20 Tetrachloroethene IPCE) ND 1.2 ND 20 Toluene ND 1.2 ND 20 1,23-Trichlorobenzene NI) 1.2 ND 20 12,4-Trichlorobenzene ND 1.2 NI) 20 1, 1, 1 -Trichloroethane N1) 1.2 ND 20 1.1,2-Trichloroethane NI) 1.2 NI) 20 Trichloroethene (TCE) ND 1.2 ND 20 Trichlorotluoroniethane ND 1.2 ND 20 1,2.3-Trichloropropane NI) 1.2 ND 20 1.24-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene NI) 1.2 NI) 20 Vinyl chloride NI) 1.2 NI) 20 Xylenes (total) NI) 1.2 NI) 20 Surrugutt: Uihrrnnglluorunu°thrtnr 0.0468 0.0494 95 75-122 Surrogate: Toluene-dh' 0.0455 0.0494 92 66-128 Surrogate:4-Bromglluorobcnzc•nc, 0.0466 0.0494 94 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX:_(805) 925-3376 Page 62 of 79 C A W&-MOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilepo Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (B1C0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Benzene 9,51 1.2 mg/kg 9.92 ND 86 36-146 Bromobenzene 8.76 1.2 9.92 ND 88 28-152 Bromochloromethane 9.53 1.2 9.92 ND 86 43-146 Bromodichloromethane 8.97 1.2 9.92 ND 90 43-153 Bromofonn 8.44 1.2 9.92 ND 85 26-151 Bromomethane 4.77 1.2 9.92 ND 48 10-158 n-Butylbenzene 8.02 1.2 9.92 0.499 76 10-171 sec-Butylbenzene 9.66 1.2 9.92 ND 97 10-176 tort-Butylbenzene 9.42 1.2 9.92 ND 95 19-168 Carbon tetrachloride 8.16 1.2 9.92 ND 82 29-151 .-- Chlorobenzene 8.93 1.2 9.92 ND 90 31-151 Chloroethane 10.4 1.2 9.92 ND 105 13-160 Chlorofonn 9.01 1.2 9.92 ND 91 44-137 Chloromethane 7.13 1.2 9.92 ND 72 10-144 2-Chlorotoluene 9.99 1.2 9.92 ND 91 24-158 4-Chlorotoluene 8.51 1.2 9.92 ND 86 19-160 Dibnunochloromethane 9.48 1.2 9.92 ND 96 40-153 1.2-Dibromo-3-chlompropane 9.07 1.2 9.92 ND 91 21-164 1,2-Dibromoethane (EDB) 9.81 1.2 9.92 ND 99 41-148 Dibromomcthane 8.47 1.2 9.92 ND 85 45-158 1,2-Dichlorobenzene 9.26 1.2 9.92 ND 93 24-158 1,3-Dichlorobenzene 8,93 1.2 9.92 ND 90 19-160 1,4-Dichlorobenzene 8.53 1.2 9.92 ND 86 20-152 Dichlorodifluoromethanc 6.47 1.2 9.92 ND 65 10-153 1,1-Dichloroethanc 8.67 1.2 9.92 ND 87 35-148 1,2-Dichlorocthanc 9.37 1.2 9.92 ND 94 42-132 1, 1 -Dichloroethene 8.72 1.2 9.92 ND 98 18-174 cis-1,2-Dichloroethene 8.62 1.2 9.92 ND 87 41-146 trans-1,2-Dichloroethene 9.52 1.2 9.92 ND 96 27-161 1,2-Dichloropropenc 8.67 1.2 9.92 ND 87 42-145 1,3-Dichloropropene 9,17 1.2 9.92 ND 92 42-141 2,2-Dichloropropene 8.42 1.2 9.92 ND 85 10-166 1, 1 -Dichloropropene 8.71 1.2 9.92 ND 88 28-151 cis-1,3-Dichloropropene 8.40 1.2 9.92 ND 85 38-148 trans-1,3-Dichloropropene 9.73 1.2 9.92 ND 98 36-144 Ethylbenzene 9.85 1.2 9.92 ND 89 16-162 liexachlorobutadiene 8.66 1.2 9.92 ND 87 10-193 4-Isopropyl Toluene 8.50 1.2 9.92 ND 86 11-167 Isopropylbenzene 9.00 1.2 9.92 ND 91 13-174 1vlethylene chloride 8.75 1.2 9.92 ND 88 30-131 Naphthalene 9.21 1.2 9.92 ND 93 10-178 n-Propylbenzene 8.74 1.2 9.92 ND 88 12-100 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 63 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet Control -] Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (BlC0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Styrene 8.81 1.2 mgtkg 9.92 NI) 89 23-160 1,1,1,2-Tetrachloroethane 9.93 1.2 9.92 NI) 100 36-152 1,1,2,2-Tctrachloroethanc 9.13 1.2 9.92 ND 92 19-175 Tetrachloroethene WCE) 8.53 1.2 9.92 ND 86 23-162 Toluene 8.41 1.2 9.92 ND 85 26-152 1,2,3-Trichlorobenzene 8.62 1.2 9.92 ND 87 10-168 1.2,4-1'richlorobenzene 8.22 1.2 9.92 ND 83 10-170 1, 1, 1 -Trichloroethane 9.36 1.2 9.92 ND 94 36-150 1,1,2-Trichloroethane 9.70 1.2 9.92 NI) 98 25-179 Trichloroethene(TCE) 8.55 1.2 9.92 ND 86 29-167 -- Trichlorofluoromethane 8.61 1.2 9.92 NI) 87 15-156 1,2,3-Trichloropropane 8.96 1.2 9.92 ND 90 26-177 1,2,4-Trimethylbenzene 8.51 1.2 9.92 NI) 86 14-157 1.3,5-Trimethylbenzene 8.70 1.2 9.92 ND 88 10-167 Vinyl chloride 9.41 1.2 9.92 NI) 95 14-154 Xylenes (total) 26.2 1.2 29.8 ND 88 21-162 Surrogate: Dibroinol7lairometh4inc 0.11487 0.0496 98 75-122 Surrogate: Toluene-d8 0.0457 0.0490 92 66-128 Surrogate:4-Bromolhtorobenz:ene 0.0458 0.0496 92 76-122 Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (B1C0817-BLK1) Analyzed: 03/26/21 12:18 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " ' Bromochloromethane ND 0.0050 " Bromodichloromethane ND 0.0050 Bromotbrm ND 0.0050 Broniomethane ND 0.0050 n-Butylbenzenc ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzenc ND 0.0050 Carbon tetrachloride NI) 0.0050 Chlorobenzene ND 0.0050 " Chloroethane ND 0.0050 " Chloroform ND 0.0050 " ' Chloromethane ND 0.0050 2-Chlorotoluene NI) 0.0050 4-Chlorotoluene ND 0.0050 Dibroniochloromethane ND 0.0050 1,2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibronioethane (F.DB) NI) 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 64 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatileptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 ._ Blank (B1C0817-BLK1) Analyzed: 03/26/21 12:18 Dibromomethanc ND 0.0050 mg/kg 1,2-Dichlorobenzene ND 0.0050 " I.3-Diclilorobcnzcne ND 0.0050 `-' 1,4-Dichlorobenzene ND 0.0050 " Dichlorodilluoromcthanc ND 0.0050 1,1-Dichloroethane ND 0.0050 " 1,2-Dichloroethane f ND 0.0050 " 1,1-Dichloroethene ND 0.0050 " cis-1.2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " - 1,2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 " I,I-Dichloropropene ND 0.0050 " cis-1,3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Fthylbenzene ND 0.0050 " I lexachlorobutadiene ND 0.0050 " 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.0050 1,1,2,2-71'etrachlorocthanc ND 0.0050 " Tetraehloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 " 1,23-Trichlorobenzene ND 0.0050 1,24-Trichlorobenzene ND 0.0050 " 1, 1, 1 -Trichloroethane ND 0.0050 1.1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorotluoromethane ND 0.0050 " 1,2.3-Trichloropropane ND 0.0050 " 1,2,4-Trimethylbenzene ND 0.0050 " 1,3,5-Trimethyl benzene ND 0.0050 " Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 Surrogate: Dibromolhioromethunc 0.0459 0.0495 Surrngute: Toluene-dR 0.0472 0.0495 Surrogate:4-Brnmo/hmrohen_ene 0.0483 0.049.5 93 75-122 9.5 66-128 98 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 65 of 79 �i Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (B1C0817-BSI) Analyzed: 03/26/21 10:22 Benzene 0.0342 0.0050 mg/kg 0.0398 86 75-131 Bromobenzene 0.0367 0.0050 0.0398 92 75-136 Bromochloromcthane 0.0328 0.0050 0.0398 82 70-135 Bromodichloromethane 0.0334 0.0050 0.0399 84 76-137 Bromofonn 0.0369 0.0050 0.0398 93 55-139 Bromomethane 0.0230 0.0050 0.0398 58 10-157 n-Butylbenzene 0.0396 0.0050 0.0398 99 62-166 sec-Butylbenzene 0.0452 0.0050 0.0398 114 72-167 tert-Butylbenzene 0.0427 0.0050 0.0398 108 69-158 Carbon tetrachloride 0.0348 0.0050 0.0398 87 70-140 Chlorobenzene 0.0374 0.0050 0.0398 94 76-137 Chloroethane 0.0413 0.0050 0.0399 104 10-164 Chloroform 0.0323 0.0050 0.0398 81 75-123 Chloromethane 0.0324 0.0050 0.0398 82 26-146 2-Chlorotoluene 0.0396 0.0050 0.0398 100 73-145 4-Chlorotoluene 0,0405 0.0050 0.0398 102 67-151 Dibromochloromethane 0.0371 0.0050 0.0398 93 68-144 1,2-Dibromo-3-chloropropane 0.0355 0.0050 0.0398 89 45-148 1,2-Dibromoetlrane (EDB) 0.0369 0.0050 0.0398 93 73-134 Dibmmomcthane 0.0329 0,0050 0.0399 82 70-140 1,2-Dichlorobenzene 0.0402 0.0050 0.0398 101 78-142 1,3-Dichlorobenzene 0.0406 0.0050 0.0398 102 76-146 1,4-Dichlorobenzene 0.0388 0.0050 0.0398 97 72-140 Dichloroditluoromcthane 0.0375 0.0050 0.0398 94 10-166 1,1-Dichloroethane 0.0342 0.0050 0.0398 86 65-139 1,2-Dichloroethane 0.0336 0.0050 0.0398 84 67-125 13-Dichloroethene 0.0360 0.0050 0,0399 90 54-168 cis-1,2-Dichloroethene 0.0346 0.0050 0.0398 87 74-135 trans-1,2-Dichloroethene 0.0375 0.0050 0.0398 94 68-149 1,2-Dichloropropane 0.0336 0.0050 0.0398 84 74-130 1,3-Dichloropropane 0.0356 0.0050 0.0398 90 68-130 2,2-Dichloropropane 0.0394 0.0050 0.0398 99 33-187 1. 1 -Dichloropropene 0.0350 0.0050 0.0398 88 71-140 cis-L3-Dichloropropene 0.0349 0.0050 0.0398 88 78-135 trans-1,3-Dichloropropene 0.0393 0.0050 0.0398 99 70-137 Ethylbenzene 0.0379 0.0050 0.0398 95 69-143 Hexaehlorobutadiene 0.0480 0.0050 0.0398 121 69-203 4-Isopropyl Toluene 0.0438 0.0050 0.0398 110 74-154 Isopropylbenzene 0.0408 0.0050 0.0398 102 72-157 Methylene chloride 0.0320 0.0050 0.0398 80 49-129 Naphthalene 0.0429 0.0050 0.0398 108 61-158 n-Propylbenzene 0.0417 0,0050 0.0398 105 69-147 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 66 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (BlC0817-BS1) Analyzed: 03/26/21 10:22 Styrene 0.0384 0.0050 mg/kg 0.0398 97 71-144 1, 1, 1,2-Tetrachloroethane 0.0379 0.0050 0.0398 95 78-132 1,1,2,2-Tctrachloroethane 0.0390 0.0050 0.0398 98 64-138 Tetrachloroethene (PCE) 0.0386 0.0050 0.0399 97 74-148 Toluene 0.0330 0.0050 0.0398 83 76-131 1,2,3-Trichlorobenzene 0.0434 0.0050 0.0398 109 63-170 1,2,4-Trichlorobenzene 0.0433 0.0050 0.0398 109 71-165 .� 1,1,1-Trichloroethane 0.0349 0.0050 0.0398 88 74-137 1,1,2-Trichloroethane 0.0364 0.0050 0.0398 92 68-134 Trichloroethene (TCE) 0,0344 0.0050 0.0399 86 79-139 Trichlorotluoromethane 0.0382 0.0050 0.0398 96 32-154 1,2,3-Trichloropropane 0.0367 0.0050 0.0398 92 69-125 1,2,4-Trimethylbenzene 0.0390 0.0050 0.0398 98 67-144 1,3,5-Trimethyl benzene 0,0409 0.0050 0.0398 103 66-154 Vinyl chloride 0.0373 0.0050 0.0398 94 39-150 Xylenes (total) 0.115 0.0050 0.119 97 71-147 Surrogate: Dibromq/luoromethane 0.0474 0.0497 95 75-122 ri Surrogate: Toluene-dN 0.0478 0.0497 96 66-128 Surrogate:4-Bromo/luorohenZrae 0.0490 0.0497 99 76-122 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 _ Benzcne 0.0353 0.0050 mg/kg 0.0398 89 75-131 3 20 Bromobenzene 0.0390 0.0050 0.0398 98 75-136 6 20 Bromochloromethane 0.0339 0.0050 0.0398 85 70-135 3 20 Bromodichloromethane 0.0349 0.0050 0.0398 88 76-137 4 20 Bromotorrm 0.0390 0.0050 0.0398 98 55-139 6 20 Bromomethane 0.0259 0.0050 0.0398 65 10-157 12 20 n-Butylbenzene 0.0425 0.0050 0.0398 107 62-166 7 20 sec-Butylbenzene 0.0487 0.0050 0.0398 122 72-167 7 20 tert-Butylbenzene 0.0459 0.0050 0.0398 115 69-158 7 20 Carbon tetrachloride 0.0363 0.0050 0.0399 91 70-140 4 20 Chlorobenzene 0.0396 0.0050 0.0398 99 76-137 6 20 .� Chloroethane 0.0404 0.0050 0.0398 101 10-164 2 20 Chloroform 0.0339 0.0050 0.0398 85 75-123 5 20 Chloromethane 0.0344 0.0050 0.0398 86 26-140 6 20 2-Chlorotoluene 0.0425 0.0050 0.0398 107 73-145 7 20 4-Chlorotoluene 0.0431 0.0050 0.0398 108 67-151 6 20 Dibromochloromcthane 0.0391 0,0050 0.0398 98 68-144 5 20 1,2-Dibromo-3-chloropropanc 0.0367 0.0050 0.0398 92 45-148 3 20 1,2-Dibromocthane (EDB) 0.0387 0.0050 0.0398 97 73-134 5 20 Dibromomcthanc 0,0137 0.0050 0.0398 85 70-140 3 20 1,2-Dichlorobenzene 0.0426 0.0050 0.0398 107 78-142 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 67 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 1,3-Dichlorobenzene 0.0435 0.0050 mg/kg 0.0398 109 76-146 7 20 1,4-Dichlorobenzene 0.0413 0.0050 0.0398 104 72-140 6 20 Dichlorodifluoromethane 0.0393 0.0050 0,0398 96 10-166 2 20 1, 1 -Dichloroethane 0.0354 0.0050 0.0398 89 65-139 4 20 1,2-Dichloroethane 0.0346 0.0050 0.0398 87 67-125 3 20 I,1-Dichloroethene 0.0372 0.0050 0.0398 93 54-169 3 20 cis-L2-Dichloroethene 0.0359 0.0050 0.0398 90 74-135 4 20 trans-1,2-Dichloroethene 0.0389 0.0050 0.0399 98 08-149 4 20 1,2-Dichloropropaue 0.0350 0.0050 0.0398 88 74-130 4 20 1,3-Dichloropropane 0.0372 0.0050 0.0398 93 68-130 4 20 2,2-Dichloropropane 0.0403 0.0050 0.0398 WI 33-187 2 20 1, 1 -Dichloropropene 0.0365 0.0050 0.0398 91 71-140 4 20 cis- 1,3-Dichloropropene 0.0362 0.0050 0.0398 91 78-135 4 20 trans-1,3-Dichloropropene 0.0415 0.0050 0.0398 104 70-137 5 20 F.thvlbenzene 0.0402 0.0050 0.0398 101 69-143 6 20 liexachlorobutadiene 0.0509 0.0050 0.0398 128 69-203 6 20 4-Isopropyl Toluene 0.0471 0.0050 0.0398 118 74-154 7 20 lsopropylbenzene 0.0437 0.0050 0.0398 110 72-157 7 20 Dlethylene chloride 0.0333 0.0050 0.0398 84 49-129 4 20 Naphthalene 0.0453 0.0050 0.0398 114 61-158 6 20 n-Propylbenzene 0.0443 0.0050 0.0398 111 69-147 6 20 • Styrene 0.0410 0.0050 0.0398 103 71-144 6 20 1,1,1,2-Tetraehloroethane 0.0402 0.0050 0.0398 101 78-132 6 20 1,1,2,2-Tetrachloroethanc 0.0407 0.0050 0.0398 102 64-138 4 20 Tetrachloroethene(PCE) 0.0412 0.0050 0.0398 103 74-148 6 20 Toluene 0.0349 0.0050 0.0398 88 76-131 6 20 1,2,3-Trichlorobenzene 0.0459 0.0050 0.0398 115 63-170 6 20 1,2,4-Trichlorobenzene 0.0448 0.0050 0.0398 112 71-165 4 20 . 1, 1, 1 -Trichloroethane 0.0365 0.0050 0.0398 92 74-137 5 20 1,1,2-Trichloroethane 0.0386 0.0050 0.0398 97 68-134 6 20 Trichloroethene (TC E) 0.0365 0.0050 0.0398 92 79-139 6 20 Trichlorotluoromethane 0.0398 0.0050 0.0398 100 32-154 4 20 ^ 1,2,3-Trichloropropane 0.0384 0.0050 0.0398 96 69-125 5 20 1,2,4-Trimethylbenzene 0.0422 0.0050 0.0398 106 67-144 8 20 1,3,5-Trimethy1benzene 0.0437 0.0050 0.0398 I10 66-154 7 20 Vinyl chloride 0.0382 0.0050 0.0398 96 39-150 2 20 Xylenes(total) 0,123 0.0050 0.120 103 71-147 7 20 Surrogate: Uibromolhioromcthane 0.0467 0.0498 94 75-122 Surrogate:7bluene-d8 0.0473 0.0498 95 66-128 Surrogate: 4-Bromofluorobenze11c 0.0495 0.0498 99 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 68 of 79 ti Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPl) Source: 2101841-08 Analyzed: 03/26/21 14:15 Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 " ND 20 Bromochloromcthanc ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-01101-otohiene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane ND 0.0050 ND 20 1.2-Dibronu)ethane (EDB) ND 0.0050 ND 20 Dibromomethane ND 0.0050 ND 20 1,2-Diehlorobenzene ND 0.0050 ND 20 1,3-Diehlorobenzene ND 0.0050 ND 20 1,4-Diehlorobenzene ND 0.0050 ND 20 Dichhxodifluoromethane ND 0.0050 ND 20 I,I-Dichloroethene ND 0.0050 ND 20 1,2-Dichloroethene ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 cis-1.2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropaue ND 0.0050 ND 20 22-Dichloropropane ND 0.0050 ND 20 1, 1 -Dichloropropene ND 0.0050 ND 20 cis-1.3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 1-thylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 69 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 Styrene ND 0.0050 mgIg ND 20 1, 1, 1,2-Tetrachloroethane ND 0.0050 ND 20 1,1,2,2-1'etrachlorocthanc ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2.4-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorofluoromethane ND 0.0050 ND 20 1,2,3-Trichloropropane ND 0.0050 ND 20 1,24-Trimethylbenzene ND 0.0050 ND 20 1,35-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibron:oJluorotnethune 0.0460 0.0496 93 75-122 _ Surrogate: Toluene-dS 0.0472 0.0496 9.5 66-128 Surrogate: 4-Bromofluorrber_ere 0.04511 0.0490 97 76-122 Matrix Spike (BlC0817-MS1) Source: 2101841-12 Analyzed: 03/26/21 20:05 Benzene 0.0322 0.0050 mg/kg 0.0399 ND 81 36-146 Bromobenzene 0.0319 0.0050 0.0399 ND 80 28-152 Bromochloromethanc 0.0323 0.0050 0.0399 ND 81 43-146 Bromodichloromethane 0.0322 0.0050 0.0399 ND 81 43-153 Bromoform 0.0376 0.0050 0.0399 ND 94 26-151 Bromomethane 0.0290 0.0050 0.0399 ND 73 10-158 n-Butylbenzene 0.0242 0.0050 0.0399 ND 61 10-171 sec-Butylbenzene 0.0324 0.0050 0.0399 ND 81 10-176 tert-Butylbenzene 0.0335 0.0050 0.0399 ND 84 19-168 Carbon tetrachloride 0.0322 0.0050 0.0399 ND 81 29-151 C'hlorobenzene 0.0337 0.0050 0.0399 ND 84 31-151 n C'hloroethane 0.0346 0.0050 0.0399 ND 87 13-160 Chloroform 0.0316 0.0050 0.0399 ND 79 44-137 Chloromethane 0.0329 0.0050 0.0399 ND 82 10-144 2-Chlorotoluene 0.0335 0.0050 0.0399 ND 84 24-158 ' 4-Chlorotoluene 0.0330 0.0050 0.0399 ND 83 19-160 Dibromochloromethane 0.0370 0.0050 0.0399 ND 93 40-153 12-Dibromo-3-chloropropanc 0.0333 0.0050 0.0399 ND 84 21-164 1,2-Dibromoelhane (EDB) 0.0366 0.0050 0.0399 ND 92 41-148 Dibromomethane 0.0315 0.0050 0.0399 ND 79 45-158 1,2-Dichlorobenzene 0.0325 0.0050 0.0399 ND 82 24-158 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 70 of 79 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlCO817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Matrix Spike (BlC0817-MS1) Source: 2101841-12 Analyzed: 03/26/21 20:05 1,3-Dichlorobenzene 0,0321 0.0050 mglkg 0.0399 ND 80 19-160 1,4-Dichlorobetizene 0.0305 0.0050 0.0399 ND 76 20-152 Dichlorodifluoromcthane 0.0373 0.0050 0.0399 ND 93 10-153 1, 1 -Dichloroethane 0.0332 0.0050 0.0399 ND 83 35-148 1.2-Dichlorocthanc 0.0321 0.0050 0.0399 ND 80 42-132 1, 1 -Dichloroethene 0.0345 0.0050 0.0399 ND 86 18-174 cis-1,2-Dichloroethene 0.0335 0.0050 0.0399 ND 84 41-146 trans-1,2-Dichloroethene 0.0354 0.0050 0.0399 ND 89 27-161 1.2-Dichloropropane 0.0321 0.0050 0.0399 ND 80 42-145 1,3-Dichloropropaue 0.0358 0.0050 0.0399 ND 90 42-141 2,2-Dichloropropaue 0.0344 0.0050 0.0399 ND 86 10-166 1,1-Dichloropropeue 0.0321 0.0050 0.0399 ND 80 28-151 cis-1,3-Dichloropropeue 0.0320 0.0050 0.0399 ND 80 38-148 trans-1,3-Dichloropropeue 0.0376 0.0050 0.0399 ND 94 36-144 Ethylbenzene 0.0324 0.0050 0.0399 ND 81 16-162 Hexachlorobutadiene 0.0223 0.0050 0.0399 ND 56 10-193 4-Isopropyl Toluene 0.0300 0.0050 0.0399 ND 75 11-167 Isopropylbenzene 0.0328 0.0050 0.0399 ND 82 13-174 Nlethylene chloride 0,0310 0.0050 0.0399 ND 78 30-131 Naphthalene 0.0314 0.0050 0.0399 ND 79 10-178 n-Propylbenzene 0.0325 0.0050 0.0399 ND 81 12-160 Styrene 0.0336 0.0050 0.0399 ND 84 23-160 1, 1, 1.2-Tetrachloroethane 0.0368 0.0050 0.0399 ND 92 36-152 1,1,2,2-Tetraclilorocthanc 0.0365 0.0050 0.0399 ND 91 19-175 Telrachloroethene WC E) 0.0339 0.0050 0.0399 ND 85 23-162 Toluene 0.0291 0.0050 0.0399 ND 73 26-152 1,23-Trichlorobenzene 0.0262 0.0050 0.0399 ND 66 10-168 1,14-Trichlorobenzene 0.0257 0.0050 0.0399 ND 64 10-170 1, 1, 1 -Trichloroethane 0.0334 0.0050 0.0399 ND 84 36-150 1,1.2-Trichloroethane 0.0364 0.0050 0.0399 ND 91 25-179 Trichloroethene (TCE) 0.0338 0.0050 0.0399 ND 85 29-167 Trichlorofluoromethane 0.0379 0.0050 0.0399 ND 95 15-156 1,2.3-Trichloropropane 0.0376 0.0050 0.0399 ND 94 26-177 1,2.4-Trimethylbenzene 0.0308 0,0050 0.0399 ND 77 14-157 1,3,5-Trimethy1benzene 0.0323 0.0050 0.0399 ND 81 10-167 Vinyl chloride 0,0368 0.0050 0.0399 ND 92 14-154 Xylenes (total) 0.0983 0.0050 0.120 ND 82 21-162 Surrogate: DibruntoJluuromethanc 0.0459 0.0499 92 75-122 Stnrogate: Toluene-d8 0.0473 0.0499 95 66-128 Surrogate:4-Bromolluorohenzene. 0.0486 0.0499 97 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 71 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sampletd Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPA by GC/FID Sol Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-F.LAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals by ICP 6010E STLC Chromium STLC/EPA 6010B Water OEC, CA-E.LAP 601013 STLC Lead STLC/EPA 601 oB Water OEC, CA -FLAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC. Internal TCLP Metals by ICP 6010E TCLP Lead EPA 13111EPA 601013 Water OEC, CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OF,C, CA -FLAP Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC,CA-FLAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 72 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary i analysis Method Matrix Laboratory & Certification Total Metals by ICP 60J OB Total Antimony EPA 6010B Solid OEC, CA -FLAP 601 OB Total Arsenic EPA 601OB Solid OF,C, CA -FLAP 601 OB Total Barium EPA 601OB Solid OEC, CA -FLAP 601 OB Total Beryllium EPA 601 OB Solid OEC, CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010B Total Chromium EPA 601 OB Solid OEC, CA-ELAP 6010B Total Cobalt EPA 601OB Solid OEC, CA-ELAP 6010B Total Copper EPA 601OB Solid OF,C, CA-ELAP 601 OB Total Lead EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 601 OB Total Nickel EPA 601 OB Solid OEC, CA-ELAP 601OB Total Selenium EPA 601 OB Solid OEC, CA-ELAP 6010B Total Silver EPA 601 OB Solid OEC, CA-ELAP 6010B Total Thallium EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Vanadium EPA 601 OB Solid OEC, CA-ELAP 601 OB Total 'Zinc EPA 601 OB Solid OEC, CA -FLAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 73 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) r nalysis Method Matrix Laboratory & Certitication Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal ..� 8015 TPH-Gasolinc EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal ~ 8015 TPH-Gasoline EPA 8015M Solid GEC, CA -FLAP 8015 TPH-Gasolinc EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPEI-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OFC, Internal 8015 TPH-Gasoline EPA 8015M Solid GEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 74 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) r ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. - N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLCanalyte concentration exceeds STLC limit. QR-03 The RPI) value for the sample duplicate or MSIMSD was outside of QC acceptance limits due to matrix interference. QC batch accepted based on LCS and or LCSD recovery and/or RPD values. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. • S-02 The surrogate recovery for this sample cannot be accurately quantified due to interference from coeluting organic compounds present in the sample extract. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 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Our environmental professionals are experienced in Phase I assessment, Phase II subsurface investigations and Phase III remediation. Our staff consists of professional engineers and environmental technicians. Personnel are OSHA 40 hour trained to perform environmental work when hazardous chemicals are involved. Clients for whom we've performed our services include major oil company, large utilities, industrial facilities, lending institutions, real estate developers and property owners and sellers. The following professionals performed work related to this project: Mr. Daniel Ringstmeyer is a Registered Professional Engineer, Colorado and California, Registered Environmental Assessor, Certified OSHA 40-Hour Trained worker, 8-Hour Trained Haz-mat Supervisor and a licensed California General Engineering Contractor. Mr. Ringstmeyer holds a Bachelors of Science in civil engineering from the South Dakota State University. He is the Founder/Owner and Principal Engineer of Buena Resources, Inc. and CIRRUS Environmental, Inc. He is the Principle Engineer responsible for all work performed by the environmental consulting/contracting firm. Mr. Ringstmeyer has conducted Phase I ESA assessments, Phase II subsurface investigations and Phase III remediation projects for sites throughout California and Mexico. He has designed and managed many successful remediation projects utilizing soil vapor extraction/thermal oxidation, bioremediation, groundwater pump and treat, and carbon adsorption throughout California and Mexico including the closure of a large Class I TSD Landfill facility. He has also directly been responsible for the closure of several idled oil fields and illegal agriculture landfills.