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2600 Broad St Closure Rpt Rev 2
Closure Report Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA October 27, 2021 (Rev. 2) Prepared For: Mr. John Hochleutner Pacific Petroleum California, Inc. 1615 Betteravia Road Santa Maria, CA 93268 Prepared By: Buena Resources, Inc. P.O. Box 2040 Santa Maria, CA 93457-2040 Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA TABLE OF CONTENTS 1.0 Excavation: 2.0 Soil Sampling of the Excavation: 3.0 Discussion of Results: 4.0 Conclusions: Appendix A Site Maps & Figures Appendix B Lab Summary Spreadsheets Appendix C Site Photographs Appendix D Laboratory & Chain of Custody Reports Appendix E Statement of Qualifications 3-5 5-6 6-7 7-8 General Contractor License #841453 Buenaresources P.O. Box 2040 Santa Maria, CA 93457-2040 P: (805) 346-1766 F: (805) 346-1767 October 27, 2021 Ms. Matheson Bliss, Haz Materials Coordinator City of San Luis Obispo Fire Department 2160 Santa Barbara Avenue San Luis Obispo, CA 93401-5240 Subject: Fuel Tank Removal and Soil Removal from 2600 Broad Street in San Luis Obispo, CA Dear Mattie: Buena Resources, Inc. has prepared this Closure Report to summarize the work performed and the laboratory results at the above site. Pacific Petroleum of California was initially engaged by Natural Healing Center to remove an existing diesel tank from this site, which had been closed at some point in the past by filling with cement. The diesel tank was estimated to be 4'-dia. by 8' long in size. The excavation related to that tank site was 8' x 8' by 8' deep. Once the tank was removed, the underlying soils were found to have been impacted with hydrocarbons. A second site was the trench that was opened to place utilities during the construction activities at this site. Contamination was found in the trench which extended to the west where a large amount of lead impacted bricks and broken tile were found. This second excavation, which was located adjacent and north of the removed tank, 12' x 12' by 12' deep. These areas are shown on the attached figure with the associated stockpile located near the excavation. Buenaresources A State Certified Small & WBE Business BUENARESOURCES Impacted soil was found below the tank, in the excavation bottom and on the sides of the excavation. Soil believed to be impacted from the diesel tank was removed and placed into 10 cyd. bins. A total of 64.51 tons of Cal Haz lead impacted and hydrocarbon impacted soil was removed and shipped to Waste Management's Kettleman Hills Class I TSD facility from this location. We are not aware of the reasons for the historical diesel tank being located on this property. There was no Phase I ESA Report completed for this site, which could have explored the historical use of this property. As we understand, there was a brick factory located close to this site. The tank was likely used for either fueling or for waste. The bricks are possibly left over from a demolished structure that may have been on the site or immediate area. The concrete slab may have been a cap for the fuel contamination located below it. Although the chromatographs for the TPH data show a weathered diesel pattern, it is possible that gasoline range organics may have been present and have degraded over time. Due to the presumed age of the site, this may have been leaded gasoline explaining the presence of lead. A Control Sample was taken 3/25/21 in an area that was not impacted to utilize that data as a background reference level for the CAM metals results reported from the contaminated zones. Action levels for these sites are the ESLs for the Bay Area Region II Table S-1 for both residential and commercial shallow soil sites. The target for this site are the residential ESLs so the property would not have a Deed restricition. Approximately 15' to the NE of the Diesel Tank Excavation, between the former Quik Mart and the building that will be the NHC SLO, the groundwater was discovered at a depth of 2'. In the tank excavation, groundwater was discovered at a depth of 5'. No groundwater intruded into the second excavation where the bricks and concrete slab were found. Buenaresources A State Certified Small & WBE Business 2 BUENARESOURCES 1.0 EXCAVATION: Diesel Tank Excavation This excavation was performed to remove an 4'-dia. x 8' metal tank that was likely used to dispense and/or store diesel fuel. Once the tank was removed from the excavation, four samples were taken to explore for contamination on March 25, 2021, which are OEC Lab IDs No. 2101841-01 through 04. Tank Wall Samples were taken at a depth of 4' in the center of each wall. OEC Lab samples 2101841-05 & 06 Tank Bottom Samples were taken at a depth of 8' at the inlet and outlet ends of the tank. These samples were located at the bottom center of the east and west ends of the excavation, approximately I'from the east and west walls, respectively. The sample locations can be seen on page 9 of the Closure Report. Lab data from these samples indicated the presence of chromium at 51 mg/kg in the Tank N Wall sample, OEC Lab ID 2101841-01. Further STLC analysis was ran on this sample resulting in a non -hazardous level of 0.13 mg/I reported. All other tank wall & floor samples reported results below action levels with no additional removal required. Based on these results, the excavation was backfilled with clean soil. The soil excavated from the diesel tank removal generated a stockpile approximately 5' high by 8' in length and 4' wide. Stockpile Samples On March 25, 2021 composite samples were taken from the north, south, east and west sides of the pile, OEC ID Nos. 2101841-10, 11, 12 & 13. Sampling was done by taking three equal amounts of soil from halfway up each side of the stockpile at intervals of approximately 1'5" and a depth of 6". These aliquots were mixed into three composite samples representing the three sides of the stockpile. A sample was taken from the east side of stockpile as well as the other three sides. Originally, it was thought to be not safe to access this area, but it was finally sampled and added to the COC by the lab. We have added that data to the laboratory data spreadsheets. Buenaresources A State Certified Small & WBE Business 3 BUENARESOURCES Trench Samplin A trench was dug approximately 3' deep to accommodate a water line. A stockpile of soil and bricks were generated from this trenching which was approximately 3' high, 6' long and 4' wide. A composite sample was taken from the stockpile by taking six equal amounts of soil from half way up the pile (1.5') at 2' intervals and a depth of approximately 6". These aliquots were combined into a single sample. As the excavation continued, the trench was segregated into two sections for sampling because half the length of the excavated material was composed of soil and the other length contained bricks as well as soil. The length containing only soil was called the "Fire Trench" and the other "Sump Trench". Originally, samples were taken from the west wall of the sump trench and at the bottom of the south end of the trench (OEC Lab ID Nos. 2101841-07 & 08. The results of these samples indicated elevated levels of TPH, chromium, copper and lead. The samples were then analyzed for STLC and TCLP levels with the results for lead coming back at 56 mg/I for STLC testing (lab ID. 2101841-07). Data indicated further excavation was required with a sample taken from the Sump Trench West side after this removal was completed (OEC ID 2103032-07) in the middle of the trench length, as that was where the majority of the bricks were found. A sample was also taken from the bottom center of the trench (OEC ID. 21020302- 03). This process was repeated for the Fire Trench with the inclusion of a sample on the east side of the trench where the material seemed to be consistent along the length of both trenches. These results indicated elevated levels of the same constituents prompting further excavation. ncrete Excavation During further excavation of the trench, the outline of a brick structure was discovered containing loose bricks and soil. As this material was removed, a concrete slab was uncovered. Brick and soil from this excavation was placed into several twenty cubic yard bins. snips of the Buenaresources A State Certified Small & WBE Business 4 BUENARESOURCES concrete slab and pieces of tile were analyzed for asbestos on 4/23 with all results negative for asbestos in any of the materials. This material was sampled by taking three samples from each bin. Material was taken from the center of each bin moving left to right at a distance of 3' apart for each sample (A, B & C), see OEC Lab ID Nos. 210508-01 thru 15. The concrete slab was removed and it was discovered that there was hydrocarbon impacted soil underneath the slab, possibly from the removed fuel tank. It is not known if that was the source, although there was only one tank found and removed. All hydrocarbon contamination found in each excavation was removed until we had "clean" excavation limits. The area between the two excavation sites are not suspected of having any hydrocarbon impacts as the two walls on either side and the excavation bottom were below action levels. Five samples were taken from the floor of the excavation immediately below the removed concrete slab (See OEC Lab ID Nos. 2102742-01 thru 05). The sample locations are as follows: NW Corner@8', NE Corner@8', SE Corner@8', and the center of the excavation at 8', all taken below the slab. The data for these samples indicated the presence of weathered hydrocarbon and that more material needed to be removed. Two twenty cubic yard bins of material was excavated and sampled in the same manner as the other bins, see OEC ID Nos. 2103212-03 thru 08. Once it was believed that all contaminated material was removed, two verification samples were taken from the excavation floor approximately 4' east and west from the center where the highest amount of petroleum had been removed, after an acceptable level was reached, the excavation was backfilled with clean soil. These were samples Bot. east@12' and Bot. west@12'. The area to the west and below the tanks were found to have been impacted by the diesel fuel along with Chromium, Nickel and Lead. All elevated metals above the SLTC testing threshold were tested, with all the Chromium and Nickel samples found to be below the Title 22 STLC (soluble) hazardous thresholds. Lead, however, did exceed the Title 22 threshold and would be Buenaresources A State Certified Small & WBE Business 5 BUENARESOURCES considered California hazardous material. Additional testing by TCLP RCRA method all reported levels below the RCRA threshold. The underlying soils under this site has a band of Serpentine, which is likely accountable for the reported Chromium and Nickel levels. This greenish material is very hard and, in this case, weathered with cracks. The diesel fuel appears to have migrated into these cracks requiring these underlying soils to be impacted requiring removal. The last samples taken on June 4tn were all below the Region II ESLs for all hydrocarbon ranges and meet the closure criteria established for this site. The depth of this excavation was approximately 12' and 12' x 12' in size. The excavations are shown in Appendix A as Figure 1. 2.0 SOIL SAMPLING OF THE EXCAVATION 2.1 Soil Sampling Plan Samples were taken from the excavation sides and bottom. All soil samples were analyzed for full range hydrocarbons (gasoline, diesel and motor oil ranges) by EPA method 8015, Volatile Organic Compounds by EPA method 8260b and CAM metals. Each sample was sealed, labeled, placed in a cooler with ice and shipped to the laboratory. Analyses were completed according to the various methods specified according to SW-846 guidelines. Action levels used at this site were the Regional Water Quality Control -Region II ESLs (Environmental Screening Levels) for residential soils. The reason for the selection of contaminants of concern (i.e. why weren't SVOCs, PAHs, etc. included in testing) is because these compounds were not considered necessary due to the nature of the site. There was no indication that these constituents would be present for any reason considering the location and the types of businesses in the area. Buenaresources A State Certified Small & WBE Business C1 BUENARESOURCES 2.2 Sampling Maintenance and Securit Upon collection, the sample containers were labeled in accordance with EPA protocols and chilled pending transportation to OEC, a State certified analytical laboratory located in Santa Maria, California following chain -of -custody procedures. All samples were recorded on Chain -of - Custody forms in ink and transferred to the laboratory according to EPA SW-846 protocol. Any changes or corrections were made by drawing a line through the error and initialing and dating the correction, then entering the correct information. 3.0 DISCUSSION OF RESULTS: Samples were taken at four wall locations and at two bottom of excavation locations below the tank. In addition, seven trench and four soil piles were initially sampled and were found to have lead at levels considered Cal Haz for STLC Lead. The soils in the five bins were also sampled to confirm the contaminates were hazardous. All five bins reported STLC lead at levels which exceeded the Title 22 guidelines for hazardous waste thresholds and were subsequently shipped as Cal Haz STLC Lead impacted soils to Waste Management's Kettleman Hill's TSD facility. The samples taken on May 5t" reported elevated diesel levels in three of the six samples. Those areas were further excavated with the final sampling on June 3rd reporting all bottom samples below the Region II ESL action levels for residential soils. All of the samples taken at the excavation sites reported no volatile organic compounds to at least the method detection limit (MDL) with the exception of the Soil Pile North Sample. The Soil Pile North sample reported n- Butylbenzene at 0.2 mg/kg, sec-Butylbenzene at 0.11 mg/kg and n-Propylbenzene at 0.15 mg/kg. All later samples taken after additional material had been removed, were below the MDL for all Method 8260b compounds. The CAMs reported nine samples with elevated chromium and six with elevated nickel levels requiring additional STLC testing to determine if the material was hazardous. The STLC levels were all below the California Title 22 hazardous thresholds for both the chromium and nickel and is not considered hazardous. Buenaresources A State Certified Small & WBE Business 7 BUENARESOURCES It is important to note that elevated levels of these two metals are common in the Serpentine material found in this area. The reported TTLC levels were at levels high enough to require further STLC testing. All of those STLC results were well below Title 22 regulated STLC metal levels and likely would be considered typical background values for this area. 4.0 CONCLUSIONS: The one cement filled diesel tank was successfully removed by PPC and shipped to WM McKittrick Landfill facility for landfilling. Impacted soil from the fuel and lead leakage was discovered below the tank and adjacent to the tank location and was subsequently removed. A total of 64.52 tons of Cal Haz STLC lead impacted soil was removed and shipped to Waste Management's Kettleman Hills TSD facility. This material also reported elevated diesel range hydrocarbons in the side slopes and bottom which was removed and included with the material shipped to Kettleman Hills. Based on the above reported results, it is our opinion that there is no further work required at this site. It is our recommendation that this site be closed and backfilled after you review the Closure Report. Thank you for the opportunity to be of service. If you have any questions, please contact this office at (805) 346-1766. Sincerely, Buena Resources, Inc. Daniel P. Ringstmeyer, P.E. (043540) Owner/Engineer Buena_ A State Certified Small & WBE Business E-1 APPENDIX A Site Maps & Figures VICINITY MAP Bishop b C o' a E U S� Highland Dr 61ackSt: 101 E Foothill Blvd - t;.° Real ,�t�eta Dr Santa \.. o � Pasa Pzrk l San Leis # '= Obispo 2028TU3A m _r202BEI r O Tg� 2600 Broad St, San L.. 202A�� N �.�< 5o G' ` 26W Broad St �\\' San Luis Obispo, CA High St 93401 South St - 1�) - -- - Laguna Lake Park 201 Sinshepner Park Sj �p Southwood Dr ISO O rl' 131 16� {Ri m� < o mJ y� ., LU u3 0 mm,Prado Rd 227 G ,per Islay 4 Hill Park Damon -Garcia a�'k Farbt Rd + 200: Sports Fields Tank Farm Rd v San Luis n Obispo jA _Go -McChesney Field r : 6 Evans Rd m 19 ,� O' 98 r; 0 mi 0.5 1 1.5 Copyright© and (P)1988-2012 Microsoft Corporation and/or its suppliers. All rights reserved. http:/hwwvmicrosoft.conVstreets/ Certain mapping and direction data ©2012 NAVTEQ. All rights reserved. The Data for areas of Canada includes information taken with permission from Canadian authorities, induding: © Her Majesty the Queen in Right of Canada, © Queen's Printer for Ontado. NAVTEQ and NAVTEQ ON BOARD are trademarks of NAVrEQ. ©2012 Tele Atlas North America, Inc. All rights reserved. Tele Atlas and Tele Atlas North America are trademarks ofTele Atlas, Inc.© 2012 by Applied Geographic Solutions. All rights reserved. Portions © Copyright2012 by Woodall Publications Corp. All rights reserved. 2 NW Sample (-10) Trash pile of bricks Fire Trench T. Sample Fire T. E. Side Sample NE Sample (-10) Top of concrete, Center + Bot. (-7') asbestoes Sample Below concrete (-10) *ot.W @12' W. Side Sample p T. West Wall Sample (4/06/21) ,-,Sump Trench Bot. Center Sump Trench Sample Trench W. Side Sample I21) Sump Trench S. End Bot. Sample LIMITS OF EXCAVATION ockpile 293384. 76981 . 6 23 4' N�Corp6r � �E \ \ 00e// NVr C7er06 1 I \cotes\ \ \NX\ I Cen er08'+ T\B \ E o�E nj \� 11 II I I I B �t W Endt j I 1 1 I/// ti COORDINATES FOR THIS PROJECT ARE CALIFORNIA COORDINATE SYSTEM NAD83, CALIFORNIA ZONE 5, US SURVEY FEET, AS DETERMINED BY GPS OBSERVATIONS ON POINTS 8070, AND 8201 "MONTEREY" AS SHOWN ON THE CITY OF SAN LUIS OBISPO "HORIZONTAL CONTROL NETWORK" (JANUARY 2007). BEND THE ELEVATIONS SHOWN HEREON ARE NAVD88 AS DETERMINED BY MEASUREMENTS ON POINT 81 AS SHOWN ON THE CITY OF SAN LUIS OBISPO "BENCHMARK SYSTEM" (JANUARY 2007) HAVING PUBLISHED ELEVATION OF 210.28' Note: Fire trench is 3' deep with excavation expanding to the west to include the 15' x 15' by 10' deep trash pit of bricks which were removed to concrete floor at —7'. An additional 3' of impacted soil was removed below the concrete and sampled on the sides and center. N:2293374.36 E: 5769833.46 EL: 233.67' Tk Wa1164' Sr Comer�O6_ _/�ivy ,IIp4/ —234-- �N:2293367.911, � - ► •576982 N:2293366.74 E:5769812.13 EL- 230.32' CONCRETE RETAINING WALL EL•2j Y' �` gad 0 5 10 1 INCH =10 FEET SURVEY DATE: 06/10/2021 WWIMAMcKittrick Waste Treatment Site Reprint ,56533 Hwy 58 W. Ticket# 156247 WASTE MANAGEMENTMCKittrlck, CA, 93251 Ph: (661) 762-7366 Customer Name PACIFICPETRO PACIFIC PETROLEU Carrier Pacific Petroleum Pacific Petroleum Ticket Date 05/13/2021 Vehicle# PPC 570 Volume Payment Type Credit Account Container Manual Ticket# Driver Ryan -- Hauling Ticket# Check# Route North Billing # 0001772 State Waste Code Gen EPA ID Manifest PPC 2021-000473 Destination Grid LF PO Profile 647907CA (FORMER FUEL TANK) Generator 144-NATURAL SANLUISOBISPO 2600 NATURAL HEALING CENTER (2600 BROAD ST) Time Scale In 05/13/2021 09:33:05 INBOUND Operator Inbound Dcarmical Gross 39760 lb Out 05/13/2021 12:49:25 OUTBOUND Dcarmical Tare 29540 lb Net 10220 lb - Comments Truck was held up pending paperwork corrections Tons 5.11 Receiving: Mon -Thu Drums 7-3, Liquids & Roll -offs 7-4, End Dumps 7-5 Product ---------------------------------------------------------------------------- LD% Qty UOM Rate Tax Amount Origin 1 SpwasteSolidOth-Cu 100 1.00 Yards 2 EVF-P-Standard Env 100 % SANLUISOBI 3 FUEL -Fuel Surcharg 100 % SANLUISOBI 4 RCR-P-Regulatory C 100 SANLUISOBI 5 WWM-P-Waste Water 100 SANLUISOBI 6 HARD2HANDLE-Hard T 100 1 Load SANLUISOBI SANLUISOBI Total Tax Total Ticket Driver's Signature NON I. Generator i v `0' -HAZARDOUS ID Number WASTE MANIFEST 1 age t d 3 Eme ge cy Response Phone 4. Waste Tracking Number 5. Generators Name and Mailing Address Generators Site Address lit df(erem than mailing addressl .- -Y - -- � 6. Transporter t Comoanyltame U.S. EPA ID Number T Transporter 2 Company Name U.S EPA ID Number 8. Designated Facility Name and See Address U.S. EPA ID Number 9. Waste Shipping Name and Description 1 D Coro"nrs 11 Total 12. UnK No, Type Ouan6ly ",Vol. a 1 S3�pec�ial Handhng Instnldxlns and Addition• Information 14. GENERATOR'soFFEROR's CERTIFICATION: I hereby declare that the contents of This coms nnW are fully and accuralely dascribed above by the proper shipping name, and are classified, packaged, marked and laheledlplacarded, and are in all respects in proper condition for transport according to applicable imemational and national govemmental regulations. Generator' Offeroi dntelrr.pedName nalu, Mmth Day Year 1 15. International Shiements i ❑ Import b J.S. ❑Export h U. Pon of entryrexic Trarswer ' nmre for e— ds ea. Date Isav n U.S.: _ a 16. Transporter Acknowledgment of Receipt of Malerials ru' CE r I ranspa)Aq l PnnledrTyped Name Month Day Year j, 1pb 1 15�s Transporter 2 P' .tl Typed Name Signature Month Day Year r 17. Discrepancy 178. Discrepancy Indication Space ❑ Quantity ❑ Type ❑ Residue ❑ Pamaf Rejection ❑ FWI Rejection Manifest Reference Number: t J 17b. Aftemate Facility lot Generator) _ U.S. EPA ID Number U rat, FaciulysPhone: w 17c. Signature of Alternate Far,Kity lot Generator) Month Day Year a j ` W C n I 18. Desgnaud facility sner or Operator: 'catan of receipt of pals covered by me manifest a •pt as not in 17 PrintedTypedName runeonth Da Year 159-BLC•0 6 7049VRW-WOg) __77 7T_GNA1 ED FaCILITs 1`0 CENERATOR C man'Hiils Landfill Reprint 3 Skyline..Road, P.O. Box 471 Ticket# 55260 Keft4,1wmtuA Er,fiA, 93239 Ticket Date 05/24/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667316JJK Grid B18 Volume Yards Carrier CAD981164312 Driver Arturo Vehicle # G249 Vehicle License 9F36934 Container # 4NP7786 Container License 4NP7786 Time Scale Operator In 05/24/2021 11:46 MANUAL WT A. Ortega Gross 75320 lb* Out 05/24/2021 12:41 A. Ortega Tare 44320 lb* * Manual Weight Net 31000 lb Tons 15.50 Comments Inbound Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 NONH DISP-TONS-Non 100 15.50 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature Please Form Approved. OMB No.2050.0039 print or type. (Form diI I for use on elite (12-pdoh) typewriter.) 1. Geraator ID Number 2. Page i of 3. Emergency Response PMme 4. ManrfeSl�a6n�Num 3 16 J J K UNIFORM HAZARDOUS ((�t��JJ�I((li 7 WASTE MANIFEST -_ - ` Generatafs Site Address Id diEarent than mai4 g addressl 5 GensratVs Name and Mating Address Genem!ofs Phone U.S. EPA ID Number 8. transporter + Company Name - -� t- , US EPAIDNumber 7. Transporter 2 Compamy Name U S. EPA ID Number 8 Designated FaDTPy Name and Site Address _ . °E . _ %L Fadli^y'sPnone: V" �=---�. 9b. U.S. GOT DescriPton findurkng proper Shipping Name, Hazanl Cuss, !D Number. 10. Contains 11. Twi 12. UrA 13. Waste Codes WIM ga. Hand Padang Grow (d any)) No Type Ouandy o cl rY,� I. t4.5petial Harding IrsNuctons aid Additional Infcrmaton X3 76 - 15 GENERATOR'SIOFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are frdty as accura:e!y deswbed above by the proper shipping nameand are classified. Packaged. marked and Iabeleolp!acardedanti are in tip respects in proper cond'tion for transport acing to applicable intematiorry and naEonal gcvemmentat regulations. If export sNpment anti I am die Pdmary Exporter, I certify that d!e contents of III consignment conform b dte terms of th attached EPAAd=Mecgmen1 of Consenl I certify, that die waste minimization staiement'denfifed n 40 CFR 262.21(a) (ff I am a large quantity generator) Of (b) (dl am a sma" Quandry generator) is true Genemt�siOAerots Pdnledrfyped Name Sgrature Imo: Day Year ifi. Ir.' rr 4orall Sh_ . _ Import to U S ❑ E.d from U 5orvy'em _ — Transporter sgna,ure (tor exports ordy). Date leamg U S . 17. TrareperterAckrrowledgment of Receipt of Materals Trarg,*t,r 1 P' ted'fyped 'time signature 2 W T-s..ar� •r teul:� Sc^a'.. Month Day Year 18. Dwapancy rr nn 18a. Discrepancy indication Space ❑ Ouantty ❑Type u Residue LJ Pareal Reje ton ❑Full Relecah Manifest P,eference N'mxr 18b Atema!e Fatality (or Geremtori U.S EPA ID Number 7 V Fadlrys Phone: W 18c.SignavraofAhemateFadity?orGenemtor) Month Day Year a 1 y19. Hazardous Waste Repor! Management WOW Codes (i e., codes for hazardous waste treatment, disposal, and recycling systems1Jj) Q 1 terry/ 2 3 d L c) ^' 20. Designated Facll¢y Omer or Ope atcr. CeticabA of receipt of hazardous materials covered by the man'dest ex^ pt as nded in t-m 18a PrmtedlTyced - ',nor _ d+ Da', Year arEa - 2 EPAFom870! 22(Rev 3-0 Previousedibonsat-- obsolete. o •�; PL%V'_ITY-0 DE. GINATi: STATE (IF REQUIRED) C' eman Hills Landfill Reprint 3` ~Skyline®Road, P.O. Box 471 Ticket# 55489 Ke1k&h*wain► y"erf3A, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667317JJK Grid B18 -•. Volume Yards Carrier CAD981164312 Driver Vehicle # G1076 Vehicle License 9F18973 Container # 4NC6734 Container License 4NC6734 Time Scale Operator In 05/28/2021 10:45 MANUAL WT A. Ortega Gross 71860 lb* Inbound ' Out 05/28/2021 12:25 A. Ortega Tare 43720 lb* * Manual Weight Net 28140 lb Tons 14.07 - Comments �. Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 NONH DISP-TONS-Non 100 14.07 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 % SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature -fav TRLSRO-I %l-Arl7-7�d C. man Hills Landfill Reprint 3. Gkyline Road, P.O. Box 471 Ticket# 55500 Ki C4dXMEh6A, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667318JJK Grid B18 Volume Yards Carrier CAD981164312 Driver JUAN Vehicle # 65424M1 Vehicle License 65424M1 Container # Container License Time Scale Operator In 05/28/2021 12:43 MANUAL WT A. Ortega Gross 46680 lb* Inbound Out 05/28/2021 14:02 A. Ortega Tare 32740 lb* * Manual Weight Net 13940 lb Tons 6.97 Comments REPLACEMENT TICKET FOR TICKET # 55490 Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 6.97 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Drivers Signature qTq- 6542gp�i § Please print or We. (Form desigrted for use on elite (12-pRch) pewriter.) UNIFORMNAZARDOUS 1.GeneratorIDNumber WASTE MANIFEST 5. Generators Name and Mailing Address fienemto/s Plwne: -11-'r ; _ - _ - - - . _ 6. iranspo ter 1 Company Name Form Approved. OMB 7 If3. Emergency Responsephone /, Man'rfest T Number No.1050-0039 _- 015667318 JJK Gene a ors Site Addrass fif erent than mailing addmss) 8 Des riarled Facltiry F s Phone: '- - =-- - 9a 9b. U.S. DOT DeOOM 1-kding Pmpa Shipping Nine. Hazard Class. ID Nunber. t0. Comau ere Hm antl Paddng Group (it airy)) Number t1.Tot� 12.Unrt e Qaanhly Wt.yyd, 13. Waste Codes 20 14. Special H ant; Ntsbuchb is and Additional Information 15 GEIIERATOR'SWFEROR'S CEMICATION: I hereby declare that the contents of this consignment am fully and a=rateiy described above by the proper shi N name• aid am classified, packaged. a#<c and labeled eface clad, and are o respects in proper carditim for transport according to applicable intemeboralard national governmental regulations. 8 export shipment and I am the Primary Export r i cerd1y, cowl the coiderds of thus consirptment conform to the terms of the abached EPAAcknowiedg pant of C sent 1 certify m2l Pie x to muun izabon statement identified in 40 CFR 26227(a) (81 am a large quantity generato) o (h . I tam a •a11 qua- ge re alcr = GeneraMyslOfie ors /jy�pyg Signature Mom Day Yet kX 16. International ShiOtrsmS 11 Import to U.S ❑ Export from U.S. Pat of entryiew: Transpakrsgnahse Or exports only): Date eaving U.S.. 1T. TransporlwAdvowledgnent ofReceipt of Materials Transporter t Prmt47y* Name Sgnature Month Day Yea G-A TranscarLT 2 Pr ntedlTyped Marne Sr Month Day Yea to. Qisaepancy 18a. Discrepancy Indication Space ❑ Quar*, ❑ Type ❑ Residue ❑ Partial R*chon ❑ Fcli Rejection Madrfest Reference Number: 18b. Abemate Facility (or Generator) U.S. EPA 0 Number _J �.i LL F.Ws Phone: y 19. Hazardous Waste Report Management Method Codes (i.e.. codes for hazardous waste treatment, disposal, and recycling systems) UJI 20. Designated Facility Owner or OpeMa: Cedfiication of receipt of hazardous materials covered by the manifest except as ed in fiem 18a KW--ypedNA Signature Monti r arb�o '05 2� 12j :PA Fam870022 ev. 305) Previoustaddiansare obsolete TDE9113 -. D FACtt-11 E INATIO r STATE (IF REQUIRED) C man Hills Landfill Reprint 3' Skyline,Road, P.O. Box 471 Ticket# 55678 Ket&i3*wmA "Eef -n,, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NBCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667326JJK Grid B18 -. Volume Yards Carrier CAD981164312 Driver Vehicle # G1072 Vehicle License 537551TZ - Container # Container License Time Scale Operator In 06/04/2021 12:03 MANUAL WT A. Ortega Gross 68100 lb* Inbound -' Out 06/04/2021 13:38 A. Ortega Tare 45140 lb* * Manual Weight Net 22960 lb Tons 11.48 Comments Product ------------------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 11.48 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature please print or type. (Form desigr�i(kr use on elite (12-path) typewrltec) f5, NIFORM HAZARDOUS 1,'GenerataIDNumber WASTE MANIFEST 11e368d Generator's Name and Mailing Address uHC SLO 985 HUSTON ST GRUVER, BEACH, Cw 9-RK uS Generatals Ptwne:'' d= �- 1-t 6. Transporter 1 OomPanY Name Pam Pelfimm CG_, In(. 7, Transporter 2 Company Name 2. Page 1 of 3. Emergency Response Phone 4. rnarx+nr5wN.wfy�.,,..,., 2W PRE] 1) ST S,�`J LUIS 081"Co, cr >34C1 US OMB No. 2050-0039 CAC)P1164312 8. Des grated Fadlhy Name and Site Address U.S. EPA ID Number GHEMICALV,'ASTE MAtvrsGE}AEivT INC C4Tt7p[pd5,ii' 35251 OLD SKYuNE ROAD YET[LEMAN CITY, CA 93239 US Fa*s Phorre: 555-,%6.9711 90. 9b, U.S. DOT Dascziptlon [mmng Proper Shipping Name. Hazard Class. ID Number. 10, Containers 11. Total 12. UrA 13. Waste Codes HM and Packing Group (if any)) No. Type Quantity WtNol. Y. 1 FQ, UN3077, EN'I'PONMENTAL,_, sA?AA.DO t5 9uBaTANCE SOLD 161 l f1 pZ� �> 11,0.S LEAD 14, Special HardNng Insbudrons and Additiaul Information —"T� � I ` 5 � � �r I � � wear ah,approp alle PPE KL�,J L 24 Hour. fMergepey Re$prlsa # tom? 925-1947 Profile R CA61-O G' 15. GENEfUTOR'SIDFFERDR'S CERTIF1CAllON: I herabf dedareThat the rbntents of this consignmem are tuMy and accurately described above by the per shippng name, and are dassified, packaged, marked and labeladlplacarded. and are ls aq respe k in proper condition fa hmrspod aaad'mg fo appkcable intematlmal and national gmrervnemul regulations. fl expert sh'pmant and I am Ble Primary Name Exporter I tlut the contents of ax sigmrent cmform tu t e of the anadred EPAAdo wAedgmenl of Consent I ;�°r�M1, dual 0%waste minlm zatian s arement dentifi�d in d0 CFR 26227fa) { f I am a arge quam ty gene ato) o (b} [d I am a sma6 a sa Cr �nerdta} is t ue. Mon Day Year 0�� �ls cYCI � wyi 16. Intern io al Shipments hPon to U.S. ❑ Export Gan U.S. Port of entry — Transporfer signature (forezpats onty): Date leaving U.S.: IT TransporterAduawledgment of Receipt of Maiedals Signabue Month Day Year Trarsporter1PdntedTypedName ,,,J UA A� - Month ON, Yen I& Discrepancy tea. Discrepant)' Indication Space ❑ Quantity C Type ❑ Residue ❑ Partial Rejection ❑ FW Rejection Manifest Reference Number: U.S. EPA ID Number 18h. Alternate Fadlily (a Generator) J U LL FaaBtj s Ptane: Monty pay Year W 18c. SignaWre of Ntemate l' - [a GenaraW) tR N 19. Hazardous Waste Report Management Method Codes (1.e., codes for hazardous waste treatment. ftml, and retyding systems) 3. 4 O 1. W N 2. 2o. Designated Facility Owner or operator: Certification of receipt of hazardos materials mvered by fhe manifest except as noted in hem 18a Mom YW Ll =1: `r Signature f '14 EPA Form 8700-22 (Rev, 3-K Prev."edroonsarE rs==_te. DESIGNATED FACILITY TO GENERATOR STATE (IF REQUIRED) C man Hills Landfill Reprint 3 S41ine,,Road, P.O. Box 471 Ticket# 55679 Ket&Ji*wMA4)id"EF6A, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667327JJK Grid B18 _. Volume Yards Carrier CAD981164312 Driver JAVIER Vehicle # G383 Vehicle License 65425M1 Container # 4ND3836 Container License 4ND3836 Time Scale Operator In 06/04/2021 11:44 MANUAL WT A. Ortega Gross 77000 lb* Inbound Out 06/04/2021 13:31 A. Ortega Tare 44020 lb* * Manual Weight Net 32980 lb Tons 16.49 • Comments Product --- ----------------------------------------------------------------------- Qty UOM Rate Tax Amount Origin 1 CALH DISP-TONS-Cal 100 16.49 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature 4-8 - -19 38 OKI i�353. 4ND3j!t _,1 oloxo rviM nr nso (From rkcinnnA &x osa m alCa (12-0itodtl ivoewritecl Form Approved. OMB No. 2Ma39 ��� 5 1. Geremtar ®N 2. Page 1 of 3. Emergency Response Phone 4. MartftestTrockkg Number _ JJK WASTE MANIFEST 1 1�„1015667327 5. Generatots.Name and Meitog Address GeneratWs Sito Address (d ditem than maikrg address) NHC SLO 906 HUSTON aT G LUIS O, GROUP, VE4,CH. Ch 1�3433 "3 SAIN Gerneramr'sPlane:'-a-=d.l-nt4 �At1 LIJIBISPC. CN. 33431 Us 6. Transporter 1 Company Name U.S. EPA ID Number Pac*' Petroleum Cr,, Inc CADS81164312 7. Transporter 2 Compaq Name U.S. EPA ID Nurrbw 8. Designated Fw^ Name and Site Address U S. EPA ID Nunes CHEMGAl WASTE MAldAGEMENT, INCCAT000646i17 %251 OLD SKYLINE ROAD KETTLEMAN CRY, CA 93239 'JS F ' s phone 5%386-9711 ga. 9b. U.S. DOT Description (indudig Proper Sh#ing Name, Hazard Class. ID Number, 10. Cantamers 11. Tatal 12. Unit 13. Wase, Codes No. Type HM and Padkkg Group (dam')) Ouartity Mjw. a K 1, R0, UPM,7, ENVIROWEPRALti HAbkRDOU3 SUESTr,NCE.SOU0 aL C" 2.0 Y 181 N 0. S. LEAD - -- - LU 2 W 3. ' - - 4. 14 Spedal HWWV Instructions ad Additional lnkrrtna5on - QI Z0141} Wear all appropriate PPE 2d Hour Emergency Response 0 P06) 10339 Prome # CAS19M 15. CENERATOR'SiWEROR'S CERTIFICATION: I hereby declare that the contents of this domignmenf are fry and amuratdy described above by dte proper shipping name, and are dassifred, packaged, marked and Iateledfplacarded, aid are h aP respells in proper conditiert for Moor! aaurd'ag to applicable inlemabA and national govemmenW regulations. C export shipment and I am the Primary Exporter, I certify Chat the contents of 9% torment conform m the terms of It attadted EPA Acknowledgment of Consent. I certify that the waste mnen¢ation statement identified h 40 CFR 26227(a) (if I am a large quwffty gerrerator) or (b)'p am a aptly genemla) is true. WslOtterWsPri LxnyWName S Ir&re Mablh Day Year fiAAy A ✓ 0 0 � IL- ra5o Sh pnonts ❑ Import b U.S. ❑ Export from US • Pon of entrytexib Z Transporter Wkilure (tor exports only): Data leaving U.S.: K 17.TwspodaAcknat6#reNofRwWofkalerials Transporter 1 PdnteNfyped Name Signature Monts Day Year S 4►vi W• 06 I&A 11W-A C Twaporler 2 Printq&Typed I~ Sgnadre Momh flay Year 18. Disdepancy 18a. Disrveparq Indication Space ❑ ouan61y ❑ Type ❑ Residue ❑Partial Relanon ❑ Full Rejection kanifest Reference Number. 18b. Akemate FaCW (or Generator) U.S. EPA ID Number C.7 ra+. Fadty's Phone. 18c. Signatue ofAllemate Fadq (or Generator) Month Day Year Z h19 Hazardous Waste Report MamgemeM Melhod Codes (i.e., codes for Wardous waste treatment, disposal, ad recydirg systems) G 1 2. 3. 4. 20. Des grated Facility Ovmer or Operator: Ceff abon or receipt of Wardeus materials covered by the marAd except as noted in hem 18a - 'Typed Name - Signature Mordk ax year41 LA Do 1 EPA Form 870D2Z(Rev.3-05) PrevausedCas 3rt obsolete DESIGNATE6-FACILITY TO GENERATOR STATE (IF REQUIRED) APPENDIX B Lab Summary Spreadsheets Q U u CL C O u U X W Ca O C N O L6 N N c Y 03 O � L � C� a C � O .�. 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Co N U) N CC E O lD O N co O f6 J c a, oLO J ei N eI 00 1-4 00 H Vf W C O U O t W co O LD W M N 00 CA V1 W VI d H O Ln O LO r- 000 N LO O N O Lo N O h N O N O O O O� O O 0 p 0 0 0 0 0 u x O O O Lf)n `- 04 000 N N O N L17 f� N O Cl) Ili Q u u O O N v N LnO O 01 Ln O O N i 00 Q1 O Q1 � O CD 0) at Ov 00 0 Ov Ln l� O Ln O l" I In V v p p V O O m m ON M N LD C) 01 d' Ln N N Q1 O Ql 0 Q1 cyl0 n O Ln O rq N N NO M l� v N V d' r'i 0 0 .-I r�-I D O .-'I NO v 0 0 LOn O O c v 'm a Ln O N 00 V1 m O Ln N O Ln Q1 ri N O O N LniO-1 N .-t , n V v N v N O O N ct co V O O 0 00 O O c V V V v V GO y M M M ri O N O r-I D ^O °° to ^ Ln 0.-0 'i N M v v v N O o 0N OOO�moot ,� y c Q m 'A •D m C1 n OC) O 00 N N M O1 p N O O� oo l0 - O O r�-I M H p N O I\ v r-I N V `-'� Q1 N O O K d' N 0 ri � v 0 0 W O O O c v m m CN p Ln N Ln �,..� O 01 Ln N O r-I I� r-I O1 O n O d 01 a ao D1 N N O 00 O r-I M `^ r1lv "' N O O N r I 0 0 -11 v 0 0 0^ 0 0 N c V is W V N O O N lD O 00 N O O1 D1 M Ln D1 Op' p O1 O1 e-I N O O O w N M V v v lD Cj o o r-I M 00 pV Ln V pV pV Ln lD o 0 .: V V m N U Ln p N cf rl O N O r-I M M N lD p 00 � w Ol 0 l0 lD n O 0 3 o Ln v v v L1Dn O o ,N-i N d I: D o v o o v v v v v v v o m 0\A bD O OA E E \ E m to 0: dD EE E 23 n0 E c � O E H23 E CJ f6 N E E j > N E O O Y a+ f0 u c7 a, o � c O E u O 7— E E �, ca L Q. 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Qi 'C L_ to s u t u u Z y o D c a � '`m v-0 0 t o o v v O u > m a lu, a CL a N Z Q Q Q m m u U U u Z vi in H> IV u F- 1- I. x F- F 00 u vA N C O m m U X W L) m C to CL N E (N O C � O� -o a L E c to U w I cu f6 E O N O 2 L O f6 J co _d m C y'� O 0) .ib CF O tD O J rl N t0 ei 00 4 00 J H Nf W C O O O O O O O 1.0 rN-I (V Lo -q M NO 00 &A Vf W IN d N n GOO N LO N N LO r- N N N O O O p O D O O 0 t.�j 25 0 0 6 6 6 Q UJ iQ U LO O O r 04 O ONO o NNGO O O OO O N OO M U) U N �-1 v C 1 p v N v v^,1O�o�O�LnAtO000V O W N .--� M Q? p Ln 00 V Ol N O IA vi o0o oo�^ o n. o E m m H H N @J O ^^ O N Ln 0 0 O M 1.0 ^ M N M 00 ^ N p �t M Ol ^ � M 01 01 Ln NO m V V p V Ln .-� 0 0^ .-i d 00 � p V pO p� t0 O O m Y v EN N Y H = to C cc __ E i a)�' E N 7 0► O C 0 _ 0 L 0 1 tJ +� C E E E o ++ u m v o O as �C�� O v E '� '3 +� v 3 .O 7 t U ++ C O 'O 0 2 O� 2 2 O L i 2 � O � m a� L T 0 Y N— > NIA � C U _ t0 V C Q Q f6 m N m f6 U t U 0 U 0 U J Z N N H i IV N APPENDIX C Site Photographs R x West Wall & Excavation Floor. ' ' ; Jai �. ,_ � , . , ` :i0w ' • jv� �, - . Y'� �v afJ�Y *�� ,' ,^¢R• - wry ,. e•_'r.• .�7,+j� �� -•,t - _ 1 � ' Aw zw h' .T- r : r .ifi - • . JS-.?- Y,R:� _ fir. �` " '.:F` sy Oy ,'��' _'���, R .F !''=�".ate -• +G� i`. �"�'. ' - -< _a �_. . d Y • e - �:�+• Sa', '• 1 �~J_ '�"n� -4+' 114 1� ,, yyam�- ��r �_�' '• �g'r►� ^- r �- • - - x ��•� ��� ��� - ' �__ �" �. AS North Wall. �- j + y�•J ,- }, ''�-~ ice. J y - _rS + . �.. 'r•• . *: - r '�:' - :w }•_� to Alm - Vi— to �r>a .ram � -. - r• _ � � - - , F'�'.• � tit � �� !_�' _ ` ��Y C � � ' - _-J-• iJ, ,. .�. .I`",�� ��-•- _ L .� ��- yam_ i fir- �.� % � r •� F'�+,I � J % _ .4. 1 - , _ �" .� � � .' i ' - .t r. 4 �. • �� y "�•Lu t 4-t, ems''• � #. •; .�: " � '�- '� _ - • . , ,� � ' � i ,J / • �'.0 it 4 •� J f .y - L, J'� •'� a �Cy/I Ewra �4• AV, �� -' f, ' -" • - T = T Excavation Floor. _ � �, iSI, - w �'�.-• � r • `k�wr�:. � .�.. fir' Ili . 10 r to ; f - _. - �r � „ - ' �= .���^ - � . 1 a �w �' � •'�yi} NO C .J • � a4.�i r f • � ' � �, ',f�C � , ' i 01 x, East Wall. 86 i. r. r r �+-• �t 1. i. �r ter..• �� i � .� ram' .,..s' ��" � •�� � '{,- � •: ��,� - :''fir • y .ter' '' *' - � 7`` . PIS •� a F i� r East and South Wall Sol NAII Ap- PF 41,2 AW IL *• ���'._ µr;�',-. .,=�; ice.' � � L .' • � t4"�� y v . y _ ��: 1L, y -'ram Y :S•. -tip -�... i a rt� .Y L��i -. .�' _ � '. � �J ��— •• ��'/� - S '.4.� -,� _Li►rr. — - L y - • `;ff •�� � � ..� ram,."_ ��� ;"i":+T.• .�;-•.•i•� � �� �• Aw � •1 -� - �. ��,'i� tip. r � � • • `�� 1!�•'•.`�• ���x � ' � *, - l+ x � lb Y wog .� . � 1 t �� Y^�• . APPENDIX D Laboratory Reports & Chain of Custody Forms (izAnalytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2103212 Pacific Petroleum California P. O. Box 2646 Report Date: May 28, 2021 10:05 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 24, 2021 13:05 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 1 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample SununarN Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom West Center Bottom East Center Bin 20339-A Bin 20339-B 2103212-01 2103212-02 2103212-03 2103212-04 Solid Solid Solid Solid Solid Solid Solid Solid 05/24/2021 11:20 05/24/2021 11:25 05/24/2021 11:30 05/24/2021 11:35 05/24/2021 13:05 05/24/2021 13:05 05/24/2021 13:05 05/24/2021 13:05 Bin 20339-C 2103212-05 Solid Solid 05/24/2021 11:40 05/24/2021 13:05 Bin 20144-A 2103212-06 Solid Solid 05/24/2021 11:45 05/24/2021 13:05 Bin 20144-B 2103212-07 Solid Solid 05/24/2021 11:50 05/24/2021 13:05 Bin 20144-C 2103212-08 Solid Solid 05/24/2021 11:55 05/24/2021 13:05 Sample Batch Preparation Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B I E0696 05/25/2021 08:55 - STLC Metals Extraction STLC Metals Extraction B 1 E0743 05/26,12021 08:58 TCLP Metals by ICP 6010BTCLP BIE0794 05/27/2021 10:55 TCLP Metals Extraction TCLP Metals Extraction B I E0744 05/26/2021 09:03 Total Metals by CVAA Mercury Total EPA 7471 A B 1 E0694 05/25/2021 07:50 - Total Metals by ICP 6010B Total B1 E0693 05/25/2021 07:26 Volatile Organic Compounds by GUMS 8260B Full List Bl E0697 05/25/2021 09:00 Volatile Organic TPH by GC/FID 8015 TPII-Gasoline BIE0737 05/26/2021 06:59 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 57 WAM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Nlercurc 0.22 0.093 mg/kg 1 B I E0694 05/25/21 14:04 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BIE0693 05/25/2114:18 EPA6010B Arsenic 7.0 1.9 Barium 560 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 120 0.48 N-02, N-03 Cobalt 21 0.48 ~ Copper 43 0.96 Lead 7.3 0.48 " 11lolvbdenum 0.62 0.48 Nickel 160 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 46 1.9 "Zinc 56 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B 1 E0794 05/27/21 19:15 EPA 1311 /EPA 601(IB Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 0.50 mg!kg I BI E0737 05/26/21 13:56 EPA 8015M Surrogate: 4-Bromq/luorohen_ene 101 % (39 - 157) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 51 10 mglkg 1 B 1 E0690 05/25/21 14:26 FPA 8015M TPl1 Motor Oil (C23-C40) ND 50 Surrogate: o-Tetphemd 90 Y 165 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BI E0697 05/25/21 15:16 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 . sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronw-3-chloropropane ND 1.2 1.2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodithioromethanc ND 1.2 " 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 LI-Dichloroethene ND 1.2 - cis-1.2-Dichloroethene ND 1.2 " trans-l.2-Dichloroethene ND 1.2 " 1.2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 " I.I-Dichloropropene ND 1.2 cis-1.3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec,comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 llexachlorobutadiene ND 1.2 mg/kg 1000 B I E0697 05/25/21 15:16 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 — Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 " 1.L1,2-Tetrachloroethane ND 1.2 1.1,2,2-Tetrachloroethane ND 1.2 Tetrachloroethenc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 " 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene(TC:E) ND 1.2 " Trichlorofluoronrethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1.2,4-1'rimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Dibromolluoromethane 101 Y. (74 - 122) " Surrogate: Toluene-dS 102 "/., (65 - 128 ) Surrogate: 4-Bronmlluoroben-ene 97 (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Drcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mg/kg 1 BIE0694 05/25/21 14:06 EPA 747]A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 E0693 05/25/21 14:21 EPA 6010B Arsenic 6.6 1.9 Barium 220 0.96 Beryllium ND 0.48 -- Cadmium ND 0.24 Chromium 120 0.48 Cobalt 19 0.48 Copper 39 0.96 Lead 8.3 0.48 Molybdenum ND 0.48 Nickel 150 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 51 1.9 Zinc 62 1.9 " TCLP Metals by ICP Chromium ND 0.050 mg/l. I B 1 E0794 05/27/21 19:17 EPA 1311 /EPA 6010B Volatile Organic TPH by GC/FID N-02, N-03 TPH Gasoline (C5-('12) 2.2 0.50 mg/kg I BIE0737 05/26/21 15:34 EPA9015M V-04 Surrogate: 4-Bronue/Inorobca_ene 118,111) (39 - 157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report meat be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 57 � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical for Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11Diesel (C13-C22) 330 10 mgtkg 1 B1E0696 05/25/2114:03 TPH Motor Oil (C23-C40) ND 50 11 11 11" Surrogate: o-Teiphentd 108 % (65 - 136) EPA 8015M 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B I E0697 05/25/21 15:43 EPA 8200B Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tent-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzcnc ND 1.2 14-Dichlorobcnzcnc ND 1.2 Dichlorodithtorornethanc ND 1.2 1,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 " 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropatie ND 1.2 1.3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 I.I-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans- l,3-Dichloropropene ND 1.2 Fthylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 57 161*4yOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 B1 E0697 05/25/21 15:43 EPA 8260B ' 4-Isopropyl Toluene ND 1.2 Isopropylbeuzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1.1,1.2-Tetrachloroethane ND 1.2 1,L2.2-Tetrachloroethane ND 1.2 Tctrachlorocthcnc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1.2.4-Trichlorobenzene ND 12 1,1,1-Trichloroethane ND 1.2 - 1,1.2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1.2.3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3.5-Trimethylbeuzene ND 12 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Dihnnno/hroromethanc 101 % (74 - 122 ) Surrogate: Toluene-d8 1I12 's„ ( 65 - 128) Surrogate: 4-Bromn/lur» 'ohen_ene 96 �Ii) ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-A Sampled : 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mgtkg 1 B 1 F0094 05/25/21 14:08 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B1 E0693 05/25/21 14:24 EPA 6010B Arsenic 5.1 2.0 Barium 230 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 N-02, N-03 Cobalt 21 0.49 Copper 47 0.98 Lead 11 0.49 Molvbdenum 0.74 0.49 Nickel 190 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 62 2.0 Zinc 72 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B IE0794 05/27/21 19:20 EPA 1311 /EPA 6010B Volatile Organic TPH by GC/FID TPHGasoline (C5-C12) 4.2 0.50 mg/kg 1 BIE0737 05/26/21 16:26 EPA8015M D-04 Surrogate: 4-Branw/luoroben_ene 11 S Y" (39 - 157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page I of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPA Diesel (C13-C22) 350 10 TPH Motor Oil (C23-C40) 55 50 Surrogate: o-Teiphe2yl 112 Y, mgIg 1 B1E0696 05/25/21 15:12 EPA 8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BIE0697 05/25/21 16:1l EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chloroethanc ND 1.2 Chlorotbnn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 14-Dichloroben7ene ND 1.2 Dichlorodifluoromethanc ND 1.2 l,l-Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 " cis-1,2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Ilexachlombutadiene ND 1.2 mglkg 1000 BIE0697 05/25/21 16:11 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 — Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 12 1,1,1,2-Tetrachloroethaue ND 1.2 1,1.2.2-Tetrachloroethane ND 1.2 'I'ctrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " — 1,1,2-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,24-Trimethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND L2 Xylencs (total) ND 1.2 Surrogate: Dihromolluoromethtow 102 % (74 - 122) „ Surrogate: Toluene-d8 103 ?', (65 - 128) Surrogate: 4-8romnlluwvhcn_ene 97 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 14 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples I Sample ID : Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mg/kg 1 BIE0694 05/25/21 14:10 EPA 7471A Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc TCLP Metals by ICP ND 2.4 mg/kg 1 B 1 F0693 05/25/21 14:26 EPA 601 OB 10 1.9 290 096 ND 0.48 ND 0.24 " 710 0.48 47 0.48 52 0.96 13 0.48 " 1.2 0.48 1900 0.48 " ND 1.9 ND 0.48 ND 0.96 77 1.9 83 1.9 Chromium ND 0.050 mgiL 1 BIE0794 05/27/21 19:23 EPA 1311 /EPA 601 OB Volatile Organic TPH by GC/FID N-02, N-03 N-02 TPH Gasoline (C5-C12) 0.76 0.50 mrg/kg I B I E0737 05/26/21 17:18 EPA 8015M D-04 Surrogate: 4-Bromollaorobencene 101 % (39 - 157) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 57 6-M Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (C13-C22) 71 10 mglkg I BIE0696 05/25/21 13:41 EPA 8015M TPH Motor Oil (C23-C40) ND 50 11 11 11" 11 Surrogate: o-7c i phem l 106 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: t805) 925-3376 Page 16 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgtkg 1000 B I E0697 05/25/21 16:38 EPA 9260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 " Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethanc ND 1.2 1,2-Dibronto-3-chi oropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichlorobenzene ND 1.2 13-Dichlorobenzene ND 1.2 1.4-Dichlorobenzene ND 1.2 Dichloroditluoromethanc ND 1.2 " l,l-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 F.thylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 57 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-04 Field Data: NA F Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Ilexachlorobutadiene ND 4-Isopropyl Toluene ND Isopropylbenzene ND Methylene chloride ND Naphthalene ND n-Propylbenzene ND Styrene ND 1,1,1,2-Tetrachl oroethane ND 1.1,2,2- hetrachloroethane ND Tetrachlorocthcnc WCE) ND ToILIC11C ND 1,2,3-Trichlorobenzenc ND I.2,4-Trichlorobenzene ND 1, 1, 1 -Trichloroethane ND — 1,1,2-Trichloroethane ND Trichloroethene (TC'E) ND Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,24-Trimethylbenzene ND 13,5-Trimethylbenzene ND Vinyl chloride ND Xylenes (total) ND Surrogate Dibromolluorornethane Surrogate: Toluene-d8 l Surrogate:4-Bron:olluoroben_ene 1.2 mg/kg 1000 B 1 E0697 05/25/21 16:38 EPA 8260B 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 / 00 ,;/0 ( 74 - 122 ) 10111/„ (65- 128) 97%n ( 75 - 121) R-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Dlercun 1.4 0.092 -'kg I B 1 E0694 05/25/21 14:12 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BIE0693 05/25/2114:13 EPA 6010B - Arsenic 6.1 2.0 Barium 220 1.0 Beryllium ND 0.50 Cadmium ND 0.2.5 Chromium 140 0.50 N-02, N-03 Cobalt 21 0.50 " Copper 46 1.0 Lead 19 0.50 N1olvbdenum 0.57 0.50 Nickel 180 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND I.0 Vanadium 54 2.0 Line 87 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/l. I B I E0794 05/27/21 19:25 EPA 1311 /EPA 6010B Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) 2.3 0.50 mg/kg 1 BIE.0737 05/26/21 19:53 EPA 8015M D-04 Surrogate: 4-Bromo/7norobenzene 107'l,, (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report mast be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 o f 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 I Analytical Report for Samples Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (C 13-C22) 390 10 mg!kg 1 B 1 E0690 05/25/21 14:49 EPA 8015M TPH Motor Oil (C23-C40) ND 50 Surrogate: o-kiphenrl 105 % (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.3 mgtkg 1000 B I E0697 05/25/21 17:05 EPA 8260B Bromobenzene ND 1.3 Brotnochloromethane ND 1.3 Bromodichloromethane ND 1.3 " Bromoform ND 1.3 Bromomethane ND 1.3 " n-Butylbenzene ND 1.3 sec-Butylbenzene ND 1.3 tert-Butylbenzene ND 1.3 Carbon tetrachloride ND 1.3 Chlorobenzenc ND 1.3 " Chloroethane ND 1.3 Chloroform ND 1.3 Chloromethane ND 1.3 2-Chlorotoluene ND 1.3 4-Chlorotoluene ND 1.3 Dibromochloromethane ND 1.3 1.2-Dibromo-3-chloropropane ND 1.3 1.2-Dibronioethane (EDB) ND 1.3 Dibromomethane ND 1.3 1,2-Dichlorobenzene ND 1.3 1.3-Dichlorobenzene ND 1.3 1,4-Dichlorobenzene ND 1.3 Dichloroditluoromcthanc ND 1.3 1, 1 -Dichloroethane ND 1.3 " 1,2-Dichloroethane ND 1.3 1, 1 -Dichloroethene ND 1.3 cis-1,2-Dichloroethene ND 1.3 trans-1,2-Dichloroethene ND 1.3 1.2-Dichloropropane ND 1.3 1,3-Dichloropropane ND 1.3 2,2-Dichloropropane ND 1.3 I.1-Dichloropropene ND 1.3 cis- I3-Dichloropropene ND 1.3 trans- l,3-Dichloropropene ND 1.3 Ethylbcnzcnc ND 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.3 mglkg 1000 B I E0697 05/25/21 17:05 F.PA 9260B 4-Isopropyl Toluene ND 1.3 Isopropylbenzene ND 1.3 Methylene chloride ND 1.3 — Naphthalene ND 1.3 n-Propylbenzene ND 1.3 Styrene ND 1.3 1.1,1.2-Tetrachloroethane ND 1.3 1,1,2,2-Tetrachloroethane ND 1.3 Tchachlorocthcnc (PCE) ND 1.3 Toluene ND 1.3 1,2,3-Trichlorobenzcne ND 1.3 1,2,4-Trichlorobenzene ND 1.3 1, 1. 1 -Trichloroethane ND 1.3 1.1.2-Trichloroethane ND 1.3 Trichloroethene (TC`E) ND 1.3 Trichlorofluoromethane ND 1.3 1,2,3-Trichloropropane ND 1.3 1,2,4-Trimethylbenzene ND 1.3 1,3.5-Trimethylbenzene ND 1.3 Vinyl chloride ND 1.3 Xylcncs (total) ND 1.3 Surrogate: Dihroruul7uvrumcthane 102 `S ; (74 - 122 ) Surrogate: Toluene-d8 102 3f, (65 - 128 ) Surrogate: 4-Bromo/luorohen_ene 98 % (75. 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 11805 925-3376 Page 22 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Alercury 0.23 0.093 mg/kg I B 1 E0694 05/25/21 14:14 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg l BIE0693 05/25/2114:37 EPA 6010B Arsenic 4.9 2.0 Barium 230 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 150 0.50 N-02, N-03 Cobalt 25 0.50 Copper 49 0.99 " Lead 41 0.50 " Molvbdenum 0.69 0.50 Nickel 190 0.50 Selenium ND 2.0 Silver ND 0.50 " Thallium ND 0.99 Vanadium 60 2.0 "Zinc 82 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BIE0794 05/27/21 19:28 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 1.5 0.50 mg/kg 1 B I E0737 05/26/21 20:45 EPA 9015M D-04 Surrogate: 4-Bromo/luorobencene 115 '%5, (39 - 157) " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPA Diesel (C13-C22) 370 10 mgrkg I BI E0696 05/25/21 14:49 EPA 8015M "rPll Motor Oil (('23-C40) ND 50 Surrogate: o-Teiphenrl 102 % (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 17:33 EPA 8260B " Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 �• Bromofornn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbeuzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcne ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 ^- 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloroniethanc ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromocthane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodithtoromethane ND 1.2 " 1,1-Dichloroethene ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 " 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 57 � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID : Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlombutadiene ND 1.2 mgtkg 1000 B I E0697 05/25/21 17:33 EPA 8260E 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 Naphthalene 2.8 1.2 n-Propylbenzcnc ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,12-Tetrachlomethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorotluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimcthylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dihromglluoromethane 99 1/s, ( 74- 122) Surrogate: Toluenc-d8 102 ;'r (6 s . 128 ) Surrogate: 4-Brornolluorobenzene 96 % ! 75. 1211 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 26 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Sampled by: Clarence Reynolds Matrix: Solid Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA DlercurN 0.19 0.093 mg/kg 1 B 1 E0694 05/25/21 14:16 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I E0693 05/25/21 14:40 EPA 6010B Arsenic 4.6 2.0 Barium 180 0.99 " Beryllium ND 0.49 - Cadmium ND 0.25 Chromium 150 0.49 " " " N-02, N-03 Cobalt 19 0.49 Copper 40 0.99 Lead 24 0.49 Molybdenum ND 0.49 Nickel 150 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 " " Vanadium 50 2.0 'Line 77 2.0 " TCLP Metals by ICP Chromium ND 0.050 mglL I BIE0794 05/27/21 19:30 EPA 1311/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 2.2 0.50 nig/kg 1 Bl E0737 05/26/21 21:36 EPA 8015M D-04 Surrogate: 4-Bromo/luorobenrene ION N (39 - 157) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 320 9.9 mg,kg I BI E0696 05/25/21 15:12 EPA 8015M TPII Motor Oil (C23-C40) ND 50 Surrogate: o-kiphenrl 95 N, ( 65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg'kg 1000 B I E0697 05/25/21 18:00 EPA 820013 Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethane ND 1.2 Chlorotorn ND 1.2 " Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronto-3-chloropropane ND 1.2 1,2-Dibrontoethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 IA-Dichlorobenzene ND 1.2 Dichloroditluoromethane ND 1.2 " 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1.I-Dichloropropene ND 1.2 " cis-1,3-Dichloropropene ND 1.2 " trans-1,3-Dichloropropene ND 1.2 Fthylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report foi- Samples Sample ID : Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 I lexachlorobutadiene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 18:00 EPA 8260B 4-1sopropyl Toluene ND 1.2 Isopropylbenzene ND L2 " Methylene chloride ND 1.2 " - - Naphthalene 2.3 1.2 n-Propylbenzenc ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1,1,2.2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1.2.4-Trielilorobenzene ND 12 I,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " '1'richlorolluoromethane ND 1 1,2.3-Trichloropropane ND 1.2 " 1,2,4-Trimethylbenzene ND 1.2 " 1,35-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: DibromoJluoromethane 100 ;' , ( 74 - 122) Surrogate. 7oluene-d8 102 "Io ('65- 128) Surrogate: 4-Bromo/luoroben_ene 98 % ( 75 _ 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: N14C SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mg/kg 1 BIE0694 05/25/21 14:18 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I F.0693 05/25/21 14:42 EPA 6010B Arsenic 5.0 2.0 Barium 140 0.98 " Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 N-02, N-03 Cobalt 23 0.49 Copper 45 0.99 Lead 14 0.49 Molybdenum IUD 0.49 Nickel 190 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 50 2.0 Zinc 71 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B 1 E0794 05/27/21 19:40 EPA 1311 /EPA 6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 2.1 0.49 mg/kg I BIE0737 05/26/21 22:28 EPA 9015M D-04 Surrogatc: 4-Bromofluoroben_ene 119 `ib (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 31 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 18:28 EPA 9260B Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 " Branodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzene ND 1.2 " Chlorocthane ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronro-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 " Dibromoinethane ND 1.2 1,2-Dichlorobenzenc ND 1.2 1,3-Dichloroben7enc ND 1.2 1,4-Dichlorobenzenc ND 1.2 Dichloroditluoromcthane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethane ND 1.2 cis-1.2-Dichloroethane ND 1.2 " tans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 I.1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 " trans-l3-Dichloropropene ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 18:28 EPA 8260B 4-Isopropyl Toluene ND 1.2 " Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 " Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 1,1,1,2-1'etrachloroethane ND 1.2 " 1,1,2.2-1'etrachloroethane ND 1.2 letrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 " 1,2,3-Trichlorobenzcnc ND 1.2 1,2.4-Trichlorobenzene ND 1.2 " 1, 1, 1 -Trichloroethane ND 1.2 " 1,1.2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 " 1,2.3-Trichloropropane ND 1.2 " 1,2.4-Trimethylbenzene ND 1.2 " 1.3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 " —. Xylenes (total) ND 1.2 " Surrogate: Dihromoiluoromethanc 99 `: ' (74 - 122 ) Surrogate: Toluene-dS 101 / ( 65 - 12S ) Surnngale: 4-8ro,noJluoruhen_cne 96 % 175 - 121 J The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 34 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ControlTotal Metals by CVAA - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0694 -EPA 7471A Preparation: EPA 7471A Pre] Blank (B1E0694-BLK1) Mercury ND LCS (BlE0694-BS1) Mercury 0.840 LCS Dup (B1E0694-BSDI) Mercury 0.949 Duplicate (BlE0694-DUPl) Source: 2103193-05 Mercury 0.216 Matrix Spike (B1E0694-MS1) Source: 2103193-05 Mercury 1.04 Matrix Spike Dup (BlE0694-MSD1) Source: 2103193-05 Mercury 1.68 Post Spike (BlE0694-PSI) Source: 2103193-02 Mercury 5.28 05/25/21 07:50 Analyzed: 05/25/21 13:31 0.10 mg/kg Analyzed: 05/25/21 13:27 0.10 mg/kg 0.833 Analyzed: 05/25/21 13:29 0.10 mg/kg 0.833 Analyzed: 05/25/21 13:47 0.18 mg/kg 1.87 Analyzed: 05/25/21 13:51 0.093 mg/kg 0.776 1.87 Analyzed: 05/25/21 13:53 0.090 mg/kg 0.751 1.87 Analyzed: 05/25/21 15:19 ug/L 5.00 0.114 101 85-115 102 8.5-115 1 20 159 20 QR-04 NR 75-125 QNI-07 NR 75-125 47 20 Q1147, QR-04 103 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Bank (B1E0693-BLKI) Analyzed: 05/25/21 14:02 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 1 Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 " Vanadium ND 2.0 " Zinc ND 2.0 LCS (BlE0693-BS1) Analyzed: 05/25/21 14:45 Antimony 99.7 2.5 mgIg 100 100 80-120 Arsenic 99.6 2.0 100 100 80-120 Barium 102 1.0 100 102 80-120 Beryllium 98.2 0.50 100 98 80-120 Cadmium 100 0.25 100 100 80-120 Chromium 99.5 0.50 100 100 80-120 Cobalt 101 0.50 100 101 80-120 ' Copper 101 1.0 100 101 80-120 Lead 102 0.50 100 102 80-120 Molybdenum 97.8 0.50 100 98 80-120 Nickel 101 0.50 100 101 80-120 Selenium 99.0 2.0 100 99 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 1.0 100 102 80-120 Vanadium 97.0 2.0 100 98 80-120 Zinc 100 2.0 100 100 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 - - LCS Dup (BlE0693-BSD1) Analyzed: 05/25/21 14:47 Antimony 100 2.5 mg/kg 100 100 80-120 0.5 20 Arsenic 99.7 2.0 100 100 80-120 0.1 20 Barium 101 1.0 100 101 80-120 0.05 20 Beryllium 98.5 0.50 100 98 80-120 0.3 20 Cadmium 100 0.25 100 100 80-120 0.2 20 Chromium 99.4 0.50 100 99 80-120 0.2 20 _ Cobalt 101 0.50 100 101 80-120 0.05 20 Copper 100 1.0 100 100 80-120 0.2 20 Lead 102 0.50 100 102 80-120 0.1 20 Molybdenum 98.4 0.50 100 98 80-120 0.6 20 Nickel 102 0.50 100 102 80-120 0.1 20 Selenium 100 2.0 100 100 80-120 1 20 Silver 4.96 0.50 5.00 99 80-120 U 20 Thallium 102 1.0 100 102 80-120 0.4 20 Vanadium 97.0 2.0 100 97 80-120 0.7 20 Zinc 100 2.0 100 100 80-120 0.2 20 Duplicate (BlE0693-DUPI) Source: 2103212-05 Analyzed: 05/25/21 14:15 Antimony ND 2.4 mg/kg ND 20 Arsenic 5.18 1.9 6.10 16 20 Barium 205 0.97 218 6 20 _ Beryllium 0.408 0.49 0.435 6 20 Cadmium ND 0.24 ND 20 Chromium 154 0.49 144 7 20 Cobalt 22.3 0.49 20.9 6 20 Copper 48.8 0.97 46.3 5 20 I. -cad 1 Z9 0.49 19.3 8 20 Molybdenum 0.510 0.49 0.574 12 20 Nickel 196 0.49 179 9 20 Selenium ND 1-9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 52.3 1.9 54.0 3 20 Zinc 69.6 1.9 87.4 23 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Noes, Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 -_ Matrix Spike (B1E0693-MSl) Source: 2103212-05 Analyzed: 05/25/21 13:50 Antimony 13.1 2.4 mg'kg 97.9 ND 13 10-116 Arsenic 101 2.0 97.9 6.10 96 77-121 Barium 226 0.98 97.9 218 8 30-169 QNI-07 Beryllium 95.2 0.49 97.9 0.435 97 86-111 Cadmium 90.0 0.24 97.9 ND 92 81-112 Chromium 218 0.49 97.9 144 76 75-129 Cobalt 109 0.49 97.9 20.9 90 71-121 _ f Copper 146 0.99 97.9 46.3 102 68-135 Lead 107 0.49 97.9 19.3 90 72-121 Molybdenum 35.0 0.49 97.9 0.574 35 70-112 QA1-07 Nickel 230 0.49 97.9 179 52 73-121 QN"7 Selenium 85.9 2.0 97.9 ND 88 76-116 Silver 4.79 0.49 4.90 ND 98 54-132 Thallium 85.9 0.98 97.9 ND 88 64-120 Vanadium 138 2.0 97.9 54.0 86 78-124 Zinc 162 2.0 97.9 87.4 77 50-143 Matrix Spike Dup (B1E0693-MSD1) Source: 2103212-05 Analyzed: 05/25/21 13:52 Antimony 9.34 2.4 mg!kg 95.8 ND 10 IO-I16 33 20 QR-02 Arsenic 96.6 1.9 95.8 6.10 95 77-121 4 20 295 0.96 95.8 218 80 30-169 26 20 QR-02 Barium Beryllium 91.2 0.48 95.8 0.435 95 86-I11 4 20 . Cadmium 85.1 0.24 95.8 ND 89 81-112 6 20 Chromium 271 0.48 95.8 14 133 75-129 22 20 QD1-07, QR-04 Cobalt 113 0.48 95.8 20.9 96 71-121 3 20 Copper 140 0.96 " 95.8 46.3 97 68-135 4 20 Lead 104 0.48 95.8 19.3 88 72-121 3 20 Molybdenum 32.4 0.48 95.8 0.574 33 70-112 8 20 Q11-07 Nickel 319 0.48 95.8 179 146 73-121 32 20 Q11-07, QR-04 Selenium 79.5 L9 95.8 ND 83 76-116 8 20 Silver 4.59 0.48 4.79 ND 96 54-132 4 20 Thallium 79.5 0.96 95.8 ND 83 64-120 8 20 Vanadium 147 1.9 95.8 54.0 97 78-124 6 20 Zinc 158 1.9 95.8 87.4 74 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 - Post Spike (B1E0693-PS1) Source: 2103212-05 Analyzed: 05/25/21 14:08 Antimony 1.98 mg/l. 2.00 0.00347 99 75-125 Arsenic 2.07 2.00 0.121 98 75-125 Barium 6.39 2.00 4.34 103 75-125 Beryllium 1.96 2.00 0.00963 98 75-125 Cadmium 1.83 2.00 -0.0417 91 75-125 Chromium 4.75 2.00 2.85 95 75-125 Cobalt 2.27 2.00 0.414 93 75-125 Copper 2.88 2.00 0.919 98 75-125 Lead 2.24 2.00 0.384 93 75-125 Molybdenum 1.97 2.00 0.0114 98 75-125 Nickel 5.42 2.00 3.56 93 75-125 Selenium 1.80 2.00 -0.120 90 75-125 Silver 0.0954 0.100 -0.00119 95 75-125 Thallium 1.78 2.00 -0.0164 89 75-125 Vanadium 3.01 2.00 1.07 97 75-125 Zinc 3.61 2.00 1.74 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX (805) 925.3376 Page 39 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0794 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 05/27/21 10:55 Blank (BlE0794-BLK1) Chromium LCS (BlE0794-BSI) Chromium LCS Dup (B1E0794-BSDI) Chromium Duplicate (B1E0794-DUPI) Chromium Leach Fluid Blank (B1E0794-LBKI) Chromium Leach Fluid Blank (BlE0794-LBK2) Chromium Leach Fluid Blank (BlE0794-LBK3) Chromium Matrix Spike (B1E0794-MSI) Chromium Matrix Spike Dup (BlE0794-MSDl) Chromium Analyzed: 05/27/21 18:35 ND 0.050 mg/L Analyzed: 05/27/21 18:20 10.0 0.050 mg/L 10.0 100 80-120 Analyzed: 05/27/21 18:22 9.84 0.050 mg/1. 10.0 98 80-120 2 20 Source:2102854-01 Analyzed: 05/27/21 18:52 ND 0.050 mg/L ND 20 Analyzed: 05/27/21 18:37 ND 0.050 mg/L Analyzed: 05/27/21 18:40 ND 0.050 mg/L Analyzed: 05/27/21 18:42 ND 0.050 mg/1. Source:2102854-01 Analyzed: 05/27/21 18:25 10.2 0.050 mg/l. 10.0 ND 102 82-119 Source:2102854-01 Analyzed: 05/27/21 18:45 10.2 0.050 mg/L 10.0 ND 102 82-119 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0737 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/26/21 06:59 Blank (B1EO737-BLKl) Analyzed: 05/26/21 10:49 TPlI Gasoline (('5-C12) ND 0.50 mg/kg Surrogate:4-Bromolluorobenzene 0.128 0.125 102 39-157 -- - LCS (BlE0737-BS1) Analyzed: 05/26/21 09:57 TPH Gasoline (('5-('12) 1.08 0.50 mgtkg 0.994 108 68-139 Sunogate:4-Bromo/luorohen:ene 0.146 110.124 117 39-157 LCS Dup (B1E0737-BSD1) Analyzed: 05/26/21 10:23 TPH Gasoline (C5-C12) 1.20 0.50 mg/kg 0.998 120 68-139 11 20 .Surrogate:4-BromnJhiorohenzene 0.154 .' 0.125 123 39-157 -- - Duplicate (BlE0737-DUPI) Source: 2103210-01RE1 Analyzed: 05/26/21 13:04 TPH Gasoline (C 5-('12) ND 0.49 mg/kg ND 20 Surrogate:4-Bromofluorobenzene 0.120 0.122 99 39-157 Matrix Spike (B1E0737-MSl) Source: 2103210-01RE1 Analyzed: 05/26/21 23:45 TPH Gasoline (('5-C12) 0.868 0.48 mg.tkg 0.967 ND 90 10-171 Surrogate:4-Bromolluoroben:enc. 0.142 " 0.121 117 39-157 Matrix Spike Dup (B1E0737-MSD1) Source: 2103210-01RE1 Analyzed: 05/27/21 00:11 TP11 Gasoline (CS-C12) 0.911 0.50 mg/kg 0.998 ND 91 10-171 5 20 Surrogate:4-Bromolluorobenzene 0.149 110.125 119 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 41 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1E0696 - EPA 8015M Preparation: EPA 3550C 05/25/21 08:55 Blank (BlE0696-BLK1) Analyzed: 05/25/21 13:41 TPH Diesel (03-C22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 " Surrogate o-Terphernd 43.3 " 50.0 87 65-136 LCS (B1E0696-BSl) Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22) 512 10 mg/kg 499 103 72-115 TPH Motor Oil (C23-C40) 473 50 499 95 74-120 Surrogate: o-T'crphcnyl 49.9 49.9 100 65-136 LCS Dup (BlE0696-BSD1) Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22) 487 10 mg/kg 500 97 72-115 5 20 TPH Motor Oil (C23-C40) 459 50 500 92 74-126 3 20 Surrogate: o-7crphem1 48.7 50.0 97 65-136 Duplicate (B1E0696-DUP1) Source: 2103212-01 Analyzed: 05/25/21 14:03 TPII Diesel (('13-C22) 35.5 9.9 mg/kg 50.9 36 20 QR-06 TPH Motor Oil (('23-C40) ND 50 ND 20 Surrogate o-Terphenrl 42.6 49.7 86 65-136 Matrix Spike (BlE0696-MSI) Source: 2103212-01 Analyzed: 05/25/21 12:55 TPII Diesel (C13-('22) 500 10 mg/kg 498 50.9 90 46-147 TPI4 Motor Oil (('23-C40) 432 50 498 ND 87 35-171 Surrogate: o-Terphen.l 44.5 49.8 N9 65-136 Matrix Spike Dup (B1E0696-MSDl) Source: 2103212-01 Analyzed: 05/25/21 13:18 TPH Diesel (C13-('22) 497 9.9 mg/kg 497 50.9 90 46-147 0.6 20 TP11 Motor Oil (C23-('40) 432 50 497 ND 87 35-171 0.2 20 Surrogate: o-Terpherrul 44.3 49.7 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 42 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (BIE0697-BLK1) Analyzed: 05/25/21 13:26 Benzene ND 0.25 ingAg Bromobenzene ND 0.25 " Bromochloromethane ND 0.25 Bromodichloromethane ND 0.25 Brontoform ND 0.25 Bromomethane ND 0.25 " _ n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 Chlorobenzene ND 0.25 " Chloroethane ND 0.25 Chloroform ND 0.25 " Chloromethane ND 0.25 " �2-Chlorotuluene ND 0.25 " 4-Chlorotoluene ND 0.25 Dibromochloromethane ND 0.25 " _ 1,2-Dibromo-3-chloropropane ND 0.25 " 1,2-Dibromoethane (EDB) ND 0.25 Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0.25 1,3-Dichlorobcnzcnc ND 0.25 " 1,4-Dichlorobenzene ND 0.25 " DichlorodillUoromethane ND 0.25 " 1,1-Dichloroethane ND 0,25 1,2-Dichloroethane ND 0.25 I,I-Dichloroethene ND 0.25 " cis-1.2-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 " 1,2-Dichloropropane ND 0.25 13-Dichloropropane ND 0.25 " 22-Dichloropropane ND 0.25 " 1, 1 -Dichloropropene ND 0.25 cis-L3-Dichloropropene ND 0.25 trans-1,3-Dichloropropene ND 0.25 Ethylbenzene ND 0.25 " I lexach lorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 Isopropylbenzene ND 0.25 " Methylene chloride ND 0.25 " Naphthalene ND 0.25 n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 VolatileOrganic Compoundsby Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 - Blank (B1E0697-BLKI) Analyzed: 05/25/21 13:26 Styrene ND 0.25 mg/kg 1,1,1.2-Tetrachloroethane ND 0.25 " I,I 2,2-Tetrachloroethane ND 0.25 .-, Tetrachloroethane (PCE) ND 0.25 " Toluene ND 0.25 " 1,2.3-Trichlorobenzene ND 0.25 " T 1,2,4-Trichlorobenzene ND 0.25 " 1, 1, 1 -Trichloroethane ND 0.25 I,1.2-Trichloroethane ND 0.25 " Trichloroethene (TCE) ND 0.25 Trichlomfluoromethane ND 0.25 " 1,2,3-Trichloropropane ND 0.25 " 1,2.4-Trimethylbenzene NJ) 0.25 " 1,3.5-Trimethylbenzene ND 0.25 " i� Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 " Surrogate: l)ibromo/hrorumrthunc 0,0490' 0.0500 99 74-122 r- Surrogate. Toluene-d8 0.0507 0.0500 101 65-128 Surrogate:4-Brumo/luorohen_ene 0.0482 0.0500 96 75-121 LCS (B1E0697-BS1) Analyzed: 05/25/21 11:37 --• Benzene 1.80 0.25 mg/kg 1.98 91 70-131 Bromobenzene 2.09 0.25 1.99 105 74-130 Bromochloroniethane 1.77 0.25 1.98 89 64-133 Bromodichloromethane 2.12 0.25 1.98 107 69-137 Bromoform 2.09 0.25 1.98 105 55-132 Bromoniethane 1,51 0.25 1.98 76 10-142 n-Butylbenzene 2.47 0.25 1.98 125 64-156 _ sec-Butylbenzene 2.46 0.25 1.98 124 75-155 tert-Butylbenzene 2.34 0.25 1.98 118 74-144 Carbon tetrachloride 1.70 0.25 1.98 86 67-135 C:hlorobenzene 2.08 0.25 1.98 105 73-134 - Chloroethane 1.65 0.25 1.98 83 10-167 Chloroform 2.01 0.25 1.98 WI 69-124 Chloromethane 2.46 0.25 1.98 124 34-136 2-Chlorotoluene 2.16 0.25 1.98 109 75-135 4-Chlorotoluene 2.30 0.25 1.99 116 70-138 Dibromochloromethane 2.01 0.25 1.98 102 67-135 1.2-Dibromo-3-ell loropropane 2.45 0.25 1.98 124 41-149 _. 1,2-Dibromoethane (EDB) 1.98 0.25 1.98 100 68-131 Dibromomethanc 1.92 0.25 1.98 97 61-140 1,2-Dichlorobenzene 2.20 0.25 1.98 111 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS (BlE0697-BS1) Analyzed: 05/25/21 11:37 1,3-Dichlorobcnzcnc 2.30 0.25 mg/kg 1.98 116 76-138 1,4-Dichlorobenzene 2.23 0.25 1.98 112 72-132 Dichloroditluoromethanc 1.51 0.25 198 76 10-155 I,l-Dichloroethane 1.90 0.25 1.98 96 63-139 1,2-Dichlorocthanc 2.04 0.25 1.98 103 64-126 I,1-Dichloroethene 1.79 0.25 1.99 90 52-167 cis-l2-Dichloroethene 1.84 0.25 1.98 93 70-135 trans-1,2-Dichloroethene 1.69 0.25 1.99 85 67-147 1,2-Dichloropropane 1.19 0.25 1.98 161 68-131 Q11-08 1,3-Dichloropropane 1.91 0.25 1.99 96 64-128 2,2-Dichloropropane 2.11 0.25 1.98 107 63-154 1,1-Dichloropropene 1.82 0.25 1.98 92 68-138 cis-1,3-Dichloropropene 2.09 0.25 1.98 105 72-134 trans-1,3-Dichloropropene 2.16 0.25 1.98 109 69-132 Ethvlbenzene 1.92 0.25 1.98 97 68-136 ilexachlorobutadiene 2.24 0.25 1.98 113 72-198 4-Isopropyl Toluene 2.40 0.25 1.98 121 74-150 Isopropylbenzene 2.21 0.25 1.98 112 71-149 methylene chloride 1.81 0.25 1.98 91 51-127 Naphthalene 2.29 0.25 1.98 116 57-158 n-Propylbenzene 2.29 0.25 1.98 116 70-143 Styrene 2.47 0.25 1.98 124 68-138 1,1,1,2-Tetrachloroethane 2.10 0.25 1.98 106 76-130 1,1,12-Tetrachloroethane 2.18 0.25 1.98 110 60-136 Tetrachloroethene (PCE) 1.79 0.25 1.98 91 73-138 Toluene 1.99 0.25 1.98 101 72-128 1,2 3-Trichlorobenzene 2.47 0.25 1.98 125 61-166 1,24-Trichlorobenzene 2.43 0.25 1.98 123 71-158 1,1,1-Trichloroethane 1.92 0.25 1.98 97 71-135 1,1,2-Trichloroethane 2.23 0.25 1.98 113 64-132 Trichloroethene (TCE) 1.87 0.25 1.98 94 74-139 Trichlorotluoromethane 2.69 0.25 1.98 136 30-156 1,2.3-Trichloropropane 2.05 0.25 1.98 104 67-123 1,2,4-Trimethylbenzene 2.31 0.25 1.98 117 68-134 1,3,5-Trimethylbenzene 2.27 0.25 1.99 114 71-140 Vinyl chloride 2.14 0.25 1.98 108 43-144 Xylenes(Iota]) 6.81 0.25 5.94 115 69-138 Surrogate: 0.051-1 0.0495 10.3 74-122 Swwogale: Touene-dr' 0.0516 0.0495 104 6 5- 128 Surrogute: 4-Bromolluorohen_ene 0.0467 0.0495 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 45 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - . Level Result Limits Limit Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 _ LCS Dup (B1E0697-BSDI) Analyzed: 05/25/21 12:04 Benzene 1.74 0.25 mg/kg 1.99 87 70-131 3 20 Bromobenzene 2.08 0.25 1.99 104 74-130 0.4 20 Bromochloromcthanc 1.69 0.25 1.99 85 64-133 5 20 Bromodichloromethane 2.14 0.25 1.99 107 69-137 0.8 20 Bromofonn 2.06 0.25 1.99 103 55-132 1 20 Bromomethane 1.50 0.25 1.99 75 10-142 1 20 n-Butylbenzene 2.33 0.25 1.99 117 64-156 6 20 sec-Butylbenzene 2.25 0.25 1.99 113 75-155 9 20 tert-Butylbenzene 2.17 0.25 1.99 109 74-144 8 20 Carbon tetrachloride 1.60 0.25 1.99 80 67-135 6 20 --i Chlorobenzene 2.07 0.25 1.99 104 73-134 0.3 20 Chlomethane 1.70 0.25 1.99 85 10-167 3 ' 20 Chloroform 1.93 0.25 1.99 97 69-124 4 20 Chloromethane 2.16 0.25 1.99 108 34-136 13 20 2-Chlorotoluene 2.05 0.25 199 103 75-135 5 20 4-Chlorotoluene 2.15 0.25 1.99 108 70-138 7 20 Dibromochloromethane 2.11 0.25 1.99 106 67-135 5 20 1,2-Dibromo-3-chloropropane 2.68 0.25 1.99 135 41-149 9 20 1,2-Dibromoethane (FDB) 2.01 0.25 1.99 101 68-131 1 20 Dibromomcthane 1.92 0.25 1.99 96 61-140 0.08 20 1,2-Dichlorobenzene 2.20 0.25 1.99 110 76-136 0.4 20 1,3-Dichlorobcnzcnc 2.15 0.25 1.99 108 76-138 7 20 1,4-Diclilorobenzenc 2.13 0.25 1.99 107 72-132 5 20 Dichlorodil7uorontcthane 1.50 0.25 1.99 75 10-155 0.5 20 LI-Dichloroethane 1.83 0.25 1.99 92 63-139 4 20 1,2-Dichlorocthene 2.01 0.25 1.99 101 64-126 2 20 1,1-Dichloroethene 1.73 0.25 1.99 87 52-167 4 20 cis- L2-Dichloroethene 1.71 0.25 1.99 86 70-135 8 20 trans-1,2-Dichloroethene 1.64 0.25 1.99 82 67-147 3 20 1.2-Dichloropropane 1.94 025 1.99 97 68-131 49 20 QR-04 13-Dichloropropane 2.05 0.25 1.99 103 64-128 7 20 2,2-Dichloropropane 2.00 0.25 1.99 100 63-154 5 20 I,1-Dichloropropene 1.75 0.25 1.99 88 68-138 4 20 cis- 1.3-Dichloropropene 1.98 0.25 1.99 100 72-134 5 20 trans -1,3-Dichloropropene 2.25 0.25 1.99 113 69-132 4 20 Ethylbenzene 2.05 0.25 1.99 103 68-136 7 20 Hexachlorobutadienc 2.12 0.25 1.99 107 72-198 5 20 4-Isopropyl Toluene 2.23 0.25 1.99 112 74-150 7 20 Isopropylbenzene 2.24 0.25 1.99 112 71-149 1 20 Nlethylene chloride 1.79 0.25 1.99 90 51-127 1 20 Naphthalene 2.10 0.25 1.99 106 57-158 8 20 n-Propylbenzene 2.12 0.25 1.99 106 70-143 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 46 of 57 ( A WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 r LCS Dup (BlE0697-BSDI) Analyzed: 05/25/21 12:04 Styrene 2.23 0.25 mgtkg 1.99 112 68-138 10 20 1,1,1,2-Tetrachloroethane 2.18 0.25 1.99 109 76-130 3 20 1,1,2,2-Tetrachlorocthane 2.11 0.25 1.99 106 60-136 3 20 Teirachloroethene WCE) 1.81 0.25 1.99 91 73-138 0.8 20 Toluene 1.83 0.25 1.99 92 72-128 9 20 1,2.3-Trichlorobenzene 2.32 0.25 1.99 116 61-166 6 20 L2.4-Trichlorobenzene 2.35 0.25 1.99 118 71-158 3 20 1, 1, 1 -Trichloroethane 1.86 0.25 1.99 93 71-135 3 20 1,1,2-Trichloroethane 2.18 0.25 1.99 109 64-132 2 20 Trichloroethene (TCE) 1.82 0.25 1.99 91 74-139 3 20 Trichlorofluoromethane 2.59 0.25 1.99 130 30-156 4 20 1,23-Trichloropropane 1.96 0.25 1.99 98 67-123 5 20 1.2.4-Trimethylbenzene 2.16 0.25 1.99 108 68-134 7 20 1,3,5-Trimethylbenzene 2.13 0.25 1.99 107 71-140 6 20 ' Vinyl chloride 2.12 0.25 1.99 107 43-144 0.6 20 XvIenes (total) 6.17 0.25 5.98 103 69-138 10 20 Surrogate: Dibromolluoromethane 0.0512 0.0498 103 74-122 ._ Surrogate: Toluene-dS 0.0510 0.0498 102 65-128 Surrogate:4-BronmJluorohenzene 0.0499 0.0498 100 75-121 Duplicate (BlE0697-DUPI) Source: 2103210-01 Analyzed: 05/25/21 14:48 Benzene ND 1.2 mg!kg ND 20 Bromobenzene ND 1.2 ND 20 Bromochloromcthanc ND 1.2 ND 20 Bromodichloromethane ND 1.2 ND 20 Brontoform ND 1.2 ND 20 Bromomethane ND 1.2 ND 20 u-Butylbenzene ND 1.2 ND 20 sec-Butylbenzene ND 1.2 ND 20 tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzcne ND 12 ND 20 Chloroethane ND 1.2 ND 20 Chloroform ND L2 ND 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene NI) 1.2 ND 20 ' 4-Chlorotoluene ND 1.2 ND 20 Dibromochlorontethane ND 1.2 ND 20 1.2-Dibromo-3-chloropropanc ND 1.2 ND 20 1,2-Dibromoethane (EDB) ND 1.2 ND 20 - Dibromomethane ND 1.2 ND 20 1.2-Dielilorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 .nalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Duplicate (BlE0697-DUPl) Source: 2103210-01 Analyzed: 05/25/21 14:48 13-Dichlorobenzene ND 1.2 mg/kg ND 1,4-Dichlorobenzene ND 1.2 ND Dichlorodifluoromethane ND 1.2 ND 1, 1 -Dichloroethane ND 1.2 ND 1,2-Dichloroethane ND 1.2 ND I,1-Dichloroethene ND 1.2 ND cis-1.2-Dichloroethene ND 1.2 ND trans-1,2-Dichloroethene ND 1.2 ND 1,2-Dichloropropane ND 1.2 ND 1,3-Dichloropropane ND 1.2 ND 2,2-Dichloropropane ND 1.2 ND 1, 1 -Dichloropropene ND 1.2 ND cis-1,3-Dichloropropene ND 1.2 ND trans-1,3-Dichloropropene ND 1.2 ND Ethylbenzene ND 1.2 ND Flexachlorobatadiene ND 1.2 ND 4-Isopropyl Toluene ND 1.2 ND Isopropylbenzene ND 1.2 ND Methylene chloride ND 1.2 ND Naphthalene ND 1.2 ND n-Propylbenzene ND 1.2 ND Styrene ND 1.2 ND 1, 1, 1,2-Tetrachloroethane ND 1.2 ND 1,1,2,24'etrachlorocthanc ND 1.2 ND Tetrachloroethene (PC'E) ND 1.2 ND Toluene ND 1.2 ND 1,2,3-Trichlorobenzene ND 1.2 ND 1,2,4-Trichlorobenzene ND 1.2 ND 1, 1, 1 -Trichloroethane ND 1.2 ND 1,1,2-Trichloroethane ND 1.2 ND Trichloroethene (TC'E) ND 1.2 ND Trichlorofluoromethane ND 1.2 ND 1,2,3-Trichloropropane ND 1.2 ND 1,24-Trimethylbeuzene ND 1.2 ND 1,3,5-Trimethylbenzene ND 1.2 ND Piny] chloride ND 1.2 ND Xylenes (total) NI) 1.2 ND Surrogate: 0.0503 0.0494 Surrogate: Toluene-dN 0.0514 0.0494 Surrogate:4-Bromolhrorohen.;rne 0.0478 0.0494 103 74-122 104 65-128 97 75-121 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 48 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet pt Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1) Source: 2103212-01 Analyzed: 05/25/21 19:22 Benzene 8.97 1.2 mg/kg 9.94 ND 90 37-145 Bromobenzene 11.0 1.2 9.94 ND 111 29-147 Bromochloromethanc 9.22 1.2 9.94 ND 93 40-145 Bromodichloromethane 10.9 1.2 9.94 ND 110 39-153 Bromoform 10.7 1.2 9.94 ND 108 32-143 Bromomethane 10.3 1.2 9.94 ND 104 10-141 n-Butylbenzene 11.6 1.2 9.94 ND 117 10-162 sec-Butylbenzene 12.2 1.2 9.94 ND 123 14-168 tert-Butylbenzene 11.8 1.2 9.94 ND 119 21-159 Carbon tetrachloride 8.48 1.2 9.94 ND 85 28-148 .� Chlorobenzene 10.9 1.2 9.94 ND 110 32-148 Chloroethane 12.6 1.2 9.94 ND 127 11-166 Chloroform 9.94 1.2 9.94 ND 100 40-139 Chloromethane 10.4 1.2 9.94 ND 105 18-135 2-Chlorotoluene 10.8 1.2 9.94 ND 108 25-151 4-Chlorotoluene 11.3 1.2 9.94 ND 114 22-150 Dibromochloromethane 10.2 1.2 9.94 ND 103 40-147 1,2-Dibromo-3-chloropropane 12.4 1.2 9.94 ND 125 25-158 1,2-Dibromoethane (EDB) 10.1 1.2 9.94 ND 102 38-147 Dibromomethane 9.74 1.2 9.94 ND 98 39-150 1,2-Dichlorobenzene 11.4 1.2 9.94 ND 115 24-154 1,3-Dichlorobenzene 11.3 1.2 9.94 ND 114 21-153 1,4-Dichlorobenzene 10.9 1.2 9.94 ND 110 21-146 Dichlorodifluoromethanc 6.32 1.2 9.94 ND 64 10-149 1, 1 -Dichloroethane 9.32 1.2 9.94 ND 94 34-151 1,2-Dichloroethane 9.93 1.2 9.94 ND 100 40-137 1, 1 -Dichloroethene 7.41 1.2 9.94 ND 74 21-172 cis-l2-Dichloroethene 9.87 1.2 9.94 ND 89 38-147 . trans-1,2-Dichloroethene 8.06 1.2 9.94 ND 81 30-160 12-Dichloropropane 10.0 1.2 9.94 ND 101 39-146 1,3-Dichloropropane 9.84 1.2 9.94 ND 99 39-141 2,2-Dichloropropane 9.05 1.2 9.94 ND 91 26-149 1, 1 -Dichloropropene 9.03 1.2 9.94 ND 91 28-150 cis- 1,3-Dichloropropene 9.92 1.2 9.94 ND 100 34-149 trans-1,3-Dichloropropene 11.0 1.2 9.94 ND 111 36-143 Ethylbenzene 10.8 1.2 9.94 ND 109 23-150 1lexachlorobutadiene 11.4 1.2 9.94 ND 115 10-192 4-Isopropyl Toluene 11.9 1.2 9.94 ND 120 11-165 lsopropylbenzene 11.7 1.2 9.94 ND 118 17-166 Methylene chloride 8.61 1.2 9.94 ND 87 28-135 Naphthalene 12.4 1.2 9.94 ND 124 10-174 n-Propylbenz_ene 11.3 1.2 9.94 ND 114 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805[ ) 925-3376 Page 49 ,?f 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Coinpounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (BlE0697-MSI) Source: 2103212-01 Analyzed: 05/25/21 19:22 Styrene 11.5 1.2 mg/kg 9.94 ND 116 24-154 1,1,1,2-Tetrachloroethane 11.1 1.2 9.94 ND 111 38-149 1,1,2,2-Tetrachloroethanc 10.7 1.2 9.94 ND 107 22-164 " Tetrachloroethene WCE) 937 1.2 9.94 ND 94 25-153 Toluene 10.4 1.2 9.94 ND 105 26-149 1,2,3-Trichlorobenzene 12.7 1.2 9.94 ND 128 10-163 1,2.4-Trichlorobenzene 12.4 1.2 9.94 ND 124 10-162 1, 1, 1 -Trichloroethane 9.87 1.2 9.94 ND 99 34-149 1,1.2-Trichloroethane 11.3 1.2 9.94 ND 113 25-175 Trichloroethene (TCE) 9.24 1.2 9.94 ND 93 25-170 Trichlorofluoromethane 12.0 1.2 9,94 ND 121 19-155 1,2,3-Trichloropropane 9.81 1.2 9.94 ND 99 32-165 1,24-Trimethylbenzene 11.7 1.2 9.94 ND 118 15-150 1,3,5-Trimethylbenzene 11.4 1.2 9.94 ND 114 10-158 Vinyl chloride 11.2 1.2 9.94 ND 112 22-148 Xylenes (total) 32.3 1.2 29.8 ND 108 22-153 Surrogate: DihramuJluurumethunr 0.0508 0.0497 102 74-122 _ . Surrogate: Toluene-dN 0.0509 0.0497 102 05-128 Surrogate:4-BromoJhrorohenzene 0.0499 0.0497 100 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum Califomia Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sampletd Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal STLC Metals Extraction STI.0 Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601 OB TCLP Chromium EPA 1311 /EPA 601 OB Water OEC, CA-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA-ELAP Total Metals by ICP 601 OB Total Antimony EPA 601013 Solid OEC, CA-ELAP 601 OB Total Arsenic EPA 601 OB Solid OEC, CA -FLAP 001 OB Total Barium EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Beryllium EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Cadmium EPA 601 OB Solid OEC. CA -FLAP 601 OB Total Chromium EPA 601 OB Solid OEC, CA-ELAP 6010B Total Cobalt EPA 601 OB Solid OEC, CA-ELAP 6010B Total Copper EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Lead EPA 601OB Solid OEC. CA-ELAP 601 OB Total Molybdenum EPA 601 OB Solid OEC. CA-ELAP 601OB 'Total Nickel EPA 601013 Solid OEC, CA-ELAP 6010B Total Selenium EPA 601 OB Solid OEC, CA -FLAP 6010B Total Sih-er EPA 001OB Solid OEC, CA-ELAP 6010B Total Thallium EPA 001 OB Solid OF:C_ CA-ELAP 6010B Total Vanadium EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Zinc EPA 6010B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51757 CA Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Method t nalysis Method Matrix Laboratory & Certification Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA-ELAP Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPI I -Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 52 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Notes and Definitions Qualifler Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery andlor RPD values. QM-UR The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. QR-06 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to non -homogenous sample matrix. QC batch accepted based on LCS and/or LCSD recovery and/or RPD values. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out -Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 53 of 57 >C U 0 x a E� O 4 +-1 N b" L U N M G7 rn 0 PO � / 04 N l0 1n N C5) N klo Ln N O O W / rl r-I W N r NJ O O N I / N �Ln r1 E1 (0 1-1 N r.G zUM G1 a (D o / Ln -� c--) o U N N r M J-1 G (0 O 4 O N E3 si �5 4-) �4 �J a) H z ro -H is r1 -� f-1� U C r0 •� -rI F14 0 FCC H-i > 2 U Q LL 0 N Cl) O N W 2 O in (6 C O fn O O O O O O O O O O O O O O W O co O _O 00 O O r- O -O r 0 Lq co 0 O O O O O O O Lci 0 O 0 0 � o —x O Cl) O O Cl) 0 O N O -O N 0 O O O O O O 1 r 43) 0 N+ o d a(O N r ti 0 + N O r p- 0 + d 1� 0 + m M r r` 0 + am N r P- 0 + CD r n 0 + d r O 0 0 o O O) O O 0 0 CD O 00 O 0 0 0 a O f- O 0 0 0 0 O CO O 0 0 0 CD O O O 0 0 0 O V O 0 0 0 O M O O 0 0 0 0 0 0 O O N - File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2612.D Operator RR Acquired 26 May 2021 1:56 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-01RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 12 Response_ GOME2612.D\FID1A 85000 80000 75000 70000 65000 60000 55000 50000 i 45000 40000 35000. 30000. 25000 20000- 15000 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2614.D Operator RR Acquired 26 May 2021 3:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-02RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 14 Response_ 110000! 105000 100000 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOME2614.D\FID1A '� 5000 `�; ,I ,..7...�, Tom. y Time 0.60 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 >C U O x a H O Ll � Ire M i} (n U N FZ� W o U � H R4 (n N N 10 ui H Ol N 1.0 U) M O O Gx] / H N rl CJ N M FG Cl O � N I / N F�l o H E_, N r-I N FC XUM C] a 0 o / X L - vU M ••UN NHM .. .. .. .. .. .. .. N 1-I -P N aro0� �4Ts (1)zw 75 -IOJ N H 2 ror-A N 34 71 J-I ¢, U rl .-I N b" U) U] (a -.-1 iz U G N •�-�I -rl r.4 0 F:4H U}X 0 0 0 (n 0 0 0 0 0 of 0 0 of 0 co 0 0 00 0 0 0 r; 0 QD O O (D O Uf O O O O Un 1 - O 'C o _ o - = U) N O O N O I � 0 0 O O NI N h n I,- r- n n O CD 0 O O O O O N O O O O O O O O C. O O O O O O O c + + + + + + + 0 0 o O o 0 0 0 0 0 N CL (0 N In N N C l N N N N O O 0 O O O O O O O O 0 O O 0 O O O a- 0 O N 00 - (D Lr) V M N File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2616.D Operator RR Acquired 26 May 2021 4:26 pm using AcgMethod GASBTEXE.M Instrument GC7 _ Sample Name: 2103212-03RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 16 Response 85001 80000, 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOME2616.D\FID1A Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 x U .—I O x u, E� O 4 C] +J N N b" LO U N FZ� W / U) U � W U) Q4 CO N • • lt7 L O O [c] / rl r (q N rl vU >q N V Q O O � N I / N Ln ri E1 ro i N < £ U cM L1 f-1 U' O Ln .-1 Ua U-) U N (N —1 N .. .. .. .. .. .. .. N }4 a-) a) rl ro O-Q 0 a)4-4 ;I +-> pa) z 0 • SA .-i N tr m w ro •H la4v s ro•�-H 4� 0 rn 2 U m N !J LL N 04 N W O In f6 C _O W n 0 r O n 0 � O P- 0 � o � O � 0 O 0 0 0 0 0 0 0 0 0 y C:+ m + + + + + + + o 0 Cl 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0.M m m m N m a> 0 O 0 O 0 O 0 O 0 O C. O 0 0 0 0) W O� co n 1 O M O O N � 0 0 O rn 0 0 0 0 0 of 0 0 M O ao 0 0 00 0 r` 0 0 0 U� O -O f0 O O L6 O O In 0 v 0 0 v O N co O M 0 0 N O O N O O O O O O File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2618.D Operator RR Acquired 26 May 2021 5:18 pm using AcgMethod GASBTEXE.M Instrument GC7 �. Sample Name: 2103212-04RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 18 Response_ GOME2618.D\FID1A 85000 onnnn. 75000 60000 55000 50000 I 450001 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 f CD to I� 0 a .o 0 Ui O O 0) O co 0 0 00 O ti 0 0 r; fo co U o m o N O 0 LL Cl) M LO LO N W O O O m LO m x m O U _ Ln O x a —Jr- 0 Q U) r> ai LO U -- N FCC � W O b ai o C - O '.. o _ N 04 !!� (N •• l0 N N N O O W W Lq N rI CJ �+ N Lr) j Q O O 1 N I / N a >1Ln O E-H (6 r-i N Gl a C7 0 /din 0 ••UN Nr-iM to 'J .. O .. .. .. .. .. .. N �4 -P F- N G (b O S� N Nzw O(D> Q,75 I ti P o O O o O O O o O O O o O �J �4 �5 H 2Z O O O O O O O + O O O O O O O O CDO O O O ( -r-I F4 r-1 C + + N + d + + N N y O O 00 O O O O O O O O- LQ O O O O O M N ri C) I;'S' U) it U) N � W ao f� (O v .'A ¢i U G 0•ri -H N OF4"U)X> File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2624.D Operator RR Acquired 26 May 2021 7:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-05RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 24 Response_ i 850001 80000 750001 70000 65000 I 60000: 55000 50000 45000 40000 350001 30000 25000 20000 15000i 10000 G0ME2624.D\FID1A 5000 II, Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 x U x a H 0 rM LO rl N H w U) O Ill / p, U) r-I N Ln N l0 N N O O [] / rl N r-i CJ N l0 Q O O N I / N H rd H N U N N 1-1 (M .. .. .. .. .. .. .. N S-i -P (1) r. (0 O S� 0aa)) zr 4-) F4 a) H %, a)�4714 U� i a) b' m rz U) N •.-I 04 U r- rd -H -H Cu0FCC HU)X> r` r- r� � r- r- r- 0 0 0 0 0 0 o O Cl yI (D o 0 0 0 0 0 O o 0 0 0 0 00 0 0 (n + + + + + + + o 0 0 0 CD o 0 0 p a) a) a) Na) a) N O O 0 0 0 O 0 0 0 d t0 LO It M N O O O O O CDO O 0 ti N .- .- r- i 00 00 a (00 V) 7 M N 0 Lq -o 0 0 d 0 m 0 0 a) 0 U� ao 0 0 ao 0 0 O r; 0 Un 0 0 to 0 f Lo -4 I. It Y O O co O N O O N O O O O N E 1- File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2626.D Operator RR Acquired 26 May 2021 8:45 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-06RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 26 Response_ 90000 85000 80010 i 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 GOME2626.D\FID1A 25000! I i 20000 I 15000 100001 I 5000 d , Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 1 I ).00 11.00 12.00 13.00 14.00 X u H O x OW H O 4 +-) N G1 �U N -rl W co C 0 0 H N N l9 U') H 0) N •• kv Un M O O W / H H GQ N H u O O � N I / N H (a H N FC SUM f� a C7 0 / Ln w U Cl N H M .. .. .. .. .. .. .. N S4 .I-) E N rl r0 O Q (1)zw 4-) }-I N H (0 •H �4H N 54 ;� -P p U H H N O" m U] b f=+OX> O 0 0 0 0 -o 0 of 0 0 of 0 r" 0 0 rb 0 0 .o 0 U� co 2 U Q .o 0 co LL M U� Lo N W OO m Lo f0 C m CD } V 0 �v l o M �O -o Cl) I 0 N O O N O to O O UC O rn y 0 n O n O n n O O n O n n O O O O o O 0 O 0 O 0 O 0 O 0 0 O O 0 O C+ N + N + N t + d N + N + + O N N O O O O O O O O O O O O CD O CD O O d o (O CM N CDO O O O O O O 0 W r- N Im W On co L V co N O— File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2628.D Operator RR Acquired 26 May 2021 9:36 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-07RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 28 Response_ GOME2628.D\FID1A 850001 80000, 75000 70000 65000 60000 55000 50000• 45000' 400— 35000 30000 25000 20000 15000 10000 I� r Y 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 x U '-I O x a H O C] 4" N (M 3 LO U N a' O G / U) U 71 c 04 cn N Ul N G� N %lo L N O O W r1 P� N OD O O N I / N >1Ln -AH ra'IN FC U cn C] a c7 0 ••UN N.-iN .. .. .. .. .. .. .. N 5-I 4-) rg Q) rl (d O Si o�rza !-I �-I �J N H z r0•H i4-1 N S4 p +> R U rl v U) U) rN 0 0 0 0 0 0 0 0 0 0 of 0 co 0 0 00 0 r- 0 0 0 2 U .-to 00 CN O li 0 I fM LO N � O W L6 O m Ir LO m co O Lq v f' 0 o M � O d M -_ Lo ' N } i O O } N 0 O O O Iq O n n n rn n n n n 0 Cl 0 0 C. 0 O o 0 yo 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 + + + + + + + + 0 0 0 0 0 O o O o N n 0) co () to N v N m N N N 0) O O O O O 0 O 0 O 0 O 0 0 0 n 0 p) 0 00 0 n 0 0 LO V M N a- 0 V LL 1 0 1 Z TQ i CU ra 00 0 in N in 0 co CV m O a n mom° m c .. c a cmIL a E E E m w d a V 0 E W -- o C �, U ry sPHOS POAloslQ leiol 1i7 &IAIs01100m « « cc « p G p zoos fWoos A . 80d f 7sad ,� y �alllge71u81 y � a � ¢ vi O o OOUS-sOOAS O y W8108 OWd°J • dHl z 6 E ;: o ePUTAS f ePlueA3 anpoeea- rz cc Q Z isle IlOd 808Z8 iC +� /� Z slinow - ZZ sllll o /U� In s > k W m U a o N : 0. is 0% m co m a Go 00 4 :: E E E a n mol— Qrd inF- fill ':'u: 0 z }' :: o o E m � m❑ c 0 El VI I.�n ld (w C 0 '. . W :•- . � r aoi r o •O IlkCL � S in4, a C 0 E En p ; in 0 t v C O p N (fit �) V w a O 00 U U v, ❑❑ m -0C$� m'c 'Q Q aui i, u O .W U cz O F aA, i� E w U U g E 1- 1- a 6 z O U z J Q U W tl to t" h 0 h a § / § 0 \ - m � ) } k } Q ) 0 ® f CL \ LO V- CL k E 2 ƒ / \ } I § k } 0 LD d ku) k $ a a§ I E ) 2 < n § f co I % $ $ ) ) ƒ w 0 E ) / f 0 o ?, \ _ § ƒ / # \ 0 A t ] E 0 cc 0 4 3 / § \ k k k u /mcƒ\ / } ? £ = a 4 _0t 7 k . I § n % f �_ §�cc -\�� o CD co = k ± 0�£«C2 o f _ , 0 7 -J o 2 I t £ 5 C 0 \ 0 \ 0 \ 7 t g / °)0 CL - a) a . E § k f \ w & ) ƒ E I £ < 0 { E - ¥ I r E o 0 \ 7 \) / \ \ \ 2�L\<E7-$ 6 0§- a a 0] LL & D=o0 ] 7 - m 0 F ® ) ) k < ) ƒ)) k w w w w 9 0 2 n h O n U N �I N N M O 1-1 N C N E [[H H h E O U CD c `o a� N N N a` v v v v v v) o) v c°n ton in coio n n i Uo iva°iviUv in c°n c c c c c c c c Y Y Y_ Y_ Y_ Y Y_ Y_ _ l0 O Q O N Q O f6 3 Q O fO 3 Q O� fO Q O� f0 _ Q O R 3 _ Q O f6 R Q O >> > > , > > , > - > N N N HU- N ON O OO N OLaN) OEO'O NNNO ' LL LL ILL LL LL LL LL LL LL LL LL LL LL LL O .n Q Q Q Q Q Q Q Q a� N N O N En N co O N N O N M O w N O N N O N N O c m> m> m> m> m> m> m> m> J C7 J (� J (� J i.� J C7 J C� J U J C N N N E N N E N E N E N E O U 0 ap 0 N O a0 O N 0 ao 0 N O oD O N O a0 O N O a0 O N 0 .- 0 N 0 00 0 N cU O .2 U Q m Q m Q m Q m Q m Q m Q m Q m O N N M M �t l0 l0 CO CO f� I� M W >,F T m v CO. Cl) C_ � N OIL J N a: o U N w 9 0 ui N O co X cc U- E m M• N o Q .� 4�Q - c CL(� a c Li 1i c m l C14 cfl m o c U U U U U U U U tan �1 A c 0 = 9 m J J J U d d J N m e a U ~ H ot$ U U H U F- U f- in U a o. U 06 Z 06 otS 06 °� R E E Ein .N. G a J N a) Wot U U U U U U U U U U U •� .W .m Q o' E m U E J J J U U J J J U J -O -�.. i U) U) m C) T sPllos ry peA10810 IRO.L f4lAlsatl0C) O G O Z808 / Mos 80d 1 ased m All mintu61 - c �N DOM?-s00As O o c U ° ,T y W9L08OW09 dHl z � � n " z E t% ccm C.ePui�s �\ N T w 1 eplue60 enuaeaa !- dm� boa a z Zo + iy N y isl 1 Iled 809Z8 %� . tv p 6� N A C ^y ❑ i :+' U Z a�i slinow ZZ epll X %� x r ro m to ? m > m > C C o pf V m 5 - =a N Q cc7 g 00 q N ❑ ❑ a o E m m - o, E E ❑ . c F= r g;C d U y 3 O tl. Z0r o o E C A ❑ -�. �. +�+ y� Lz N Z V O t�6 G ty0 O N . L > x wN . n Y! C � 1 ` ■ ❑ } 4 at U I: n �a 0 o o .- = n C .t] y N �+ O CL fs x t� u m E o :: E .o w G" _ is a, a O eD u u v y 8 y ❑ ❑ to m m 'C ai C m n y � t t Cl. `c f Q E E � .� 0 H w Le E W Q o F o 0 > > o c i_ � C d a a+ c c c m w a i O F- U M N z 0 0 0. Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Summary Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom East @ 12' 2103479-01 Solid Solid 06/03/2021 11:50 06/04/2021 12:50 Bottom West @ 12' 2103479-02 Solid Solid 06/03/2021 11:55 06/04/2021 12:50 Sample Batch Preparation Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel Ix Motor Oil List B I F0145 061104/2021 16:24 STLC Metals by ICP 601013 STLC B I F0261 06/09/2021 08:56 STLC Metals Extraction STLC Metals Extraction BIF0229 06/07/2021 16:29 Total Metals by CVAA Mercury Total EPA 7471A BIF0194 06/07/2021 07:40 Total Metals by ICP 001013 Total B I F0197 06/07/2021 08:26 Volatile Organic Compounds by GC/MS 8260B Full List B 1 F0146 06/04/2021 12:21 Volatile Organic TPH by GC/FID 8015 1 PH-Gasolinc B 11`0154 06/04!2021 10:34 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 2 of 32 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample ID : Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mglkg I BIF0194 06/07/21 16:25 EPA 7471A Total Metals by ICP Antimony ND 2.3 mg/kg 1 BIF0197 06/07/21 14:12 EPA 6010B Arsenic 5.6 1.9 " Barium 120 0.93 " Beryllium ND 0.47 Cadmium ND 0.23 Chromium 73 0.47 " N-02 Cobalt 18 0.47 ^ Copper 47 0.93 Lead 8.2 0.47 Molybdenum ND 0.47 Nickel 130 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 49 1.9 Zinc 65 1.9 STLC Metals by ICP Chromium ND 0.020 mg/L 2 BIF0261 06/09/21 14:34 STI.C/EPA601(1B Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 4.5 mg!kg I BIF0154 06/04/21 17:01 EPA 8015M Surrogate: 4-Bronio/luorohen_ene 92 4s, (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Sample ID: Bottom East @ 12' Sampled: 06/03/2, 11.50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.050 mg/kg I BIF0146 06/04/21 16:16 EPA 8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 " Bromodichloromethane ND 0.050 " Bromofornn ND 0.050 Bromomethane ND 0.050 " n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 " tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 " Chlorobenzene ND 0.050 " Chlorocthanc ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 " 4-C'hlorotoluene ND 0,050 Dibromochloromethane ND 0.050 " " 1,2-Dibronio-3-chloropropanc ND 0.050 12-Dibronioethane (EDB) ND 0.050 Dibromomethane ND 0.050 12-Dichlorobenzene ND 0.050 1,3-Dichlorobcnzenc ND 0.050 14-Dichlorobcnzenc ND 0.050 " Dichloroditluoromethane ND 0.050 CCffi l,l-Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 LI-Dichloroethene ND W050 cis-1,2-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 2,2-Dichloropropane ND 0.050 1, 1 -Dichloropropene ND 0.050 cis-1.3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 Fthylbcnzcnc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.050 mg/kg I B1 F0146 06/04/21 16:16 EPA 8260B —4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 " 1. 1, 1,2-Tetrachloroethane ND 0.050 1.1.2,2-Tetrachloroethane ND 0.050 Tetrachloroethcnc (PCE) ND 0.050 Toluene ND 0.050 1,2,3-Trichlorobenzene ND 0.050 1.2,4-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 " 1,1,2-Trichloroethane ND 0.050 " Trichloroethene (TC'E) ND 0.050 Trichlorotluoromethane ND 0.050 1,2,3-Trichloropropane ND 0.050 1,2.4-Trimethylbenzene ND 0.050 " 1,3.5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylencs (total) ND 0.050 Surrogate: Uihronwfluoronuethane 103 74 - 122 ) Surrogate: Toluene-dg 99 % (65 - 128) " Surrogate: 4-BrnmuJTuuroheu_ene 105 3 ; (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg 1 B I F0194 06/07/21 16:27 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I BIF0197 06/07/21 14:15 EPA 601OB Arsenic 7.4 1.9 Barium 160 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 51 0.49 N-02 Cobalt 14 0.48 Copper 63 0.96 Lead 8.9 0.48 Molybdenum 0.57 0.48 Nickel 88 0.48 Selenium ND 1.9 Silver ND 0.49 Thallium ND 0.96 Vanadium 52 1.9 " Zinc 71 1.9 STLC Metals by ICP Chromium ND 0.020 mgiL 2 BIF0261 06/09/2114:37 STLC/E PA 601 OB Volatile Organic TPH by GC/FID TPHGasoline (C5-C12) ND 4A mg/kg I BIF0154 06/04/2117:29 EPA8015M Surrogate: 4-Bromo/hnnroben_ene 95 /, (39 - 157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 7 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C3-('22) ND 9.9 mglkg 1 BIF0145 TPH Motor Oil (C23-C40) ND 50 11 11" Surrogate o-Teiphenyl 90 % (65 - 136) 11 06/05/21 12:34 EPA 9015M The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street IA'" Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.048 mg/kg I BIF0146 06/04/21 15:48 EPA8260B Bromobenzene ND 0.048 " Brontochloromethane ND 0.048 Bromodichloromethane ND 0.048 Bromoform ND 0.048 Bromomethane ND 0.048 " n-Butylbenzene ND 0.048 sec-Butylbenzene ND 0.048 tert-Butylbenzene ND 0.048 Carbon tetrachloride ND 0.048 Chlorobenzene ND 0.048 Chloroethane ND 0.048 Chlorotbnn ND 0.048 Chloromethane ND 0.048 2-Chlorotoluene ND 0.048 4-Chlorotoluene ND 0.048 Dibromochloromelhane ND 0.048 1.2-Dibromo-3-chloropropane ND 0.048 " " 1,2-Dibromoethane (EDB) ND 0.048 Dibromomethane ND 0.048 1,2-Dichlorobenzene ND 0.048 1,3-Dichlorobcnzcne ND 0.048 1.4-Dichlorobcnzene ND 0.048 Dichlorodifluoronmthanc ND 0.048 1, 1 -Dichloroethane ND 0.048 1,2-Dichloroethane ND 0.048 " 1, 1 -Dichloroethene ND 0.048 cis-L2-Dichloroethene ND 0.048 " trans-1,2-Dichloroethene ND 0.048 " 12-Dichloropropane ND 0.048 13-Dichloropropane ND 0.048 22-Dichloropropane ND 0.048 I,I-Dichloropropane ND 0.048 cis- I3-Dichloropropcnc ND 0.048 trans-1,3-Dichloropropcnc ND 0.048 Ethylbcnzene ND 0.048 CC111 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 IlexachlOTobutadiene ND 0.048 mg/kg 1 BIF0146 ()6/04/2115:48 EPA8260B 4-Isopropyl Toluene ND 0.048 Isopropylbenzene ND 0.048 Methylene chloride ND 0.048 Naphthalene ND 0.048 n-Propylbenzene ND 0.048 Styrene ND 0.048 I,1.1.2-Teuachloroethane ND 0.048 1,1,2,2-Tetrachlorocthane ND 0.048 Tetrachlorocthcnc WCE) ND 0.048 Toluene ND 0.048 1,23-Trichlorobenzcne ND 0.048 1,2.4-Trichlorobenzene ND 0.048 1,1,1-Trichloroethane ND 0.049 1,1,2-Trichloroethane ND 0.048 Trichloroethene (TCE) ND 0.048 Trichlorofluoromethane ND 0.048 " 1.2.3-Trichloropropane ND 0.048 1.2.4-Trimcthylbenzene ND 0.048 1.3.5-Trimethylbenzene ND 0.048 Vinyl chloride ND 0,048 Xylenes (total) ND 0.048 Surrogate: Uibromolluoromethanc 104 % ( 74— 122) Surrogate: Toluene-ds 102 'N, (65. 128) Surrogate: 4-Bronw/luor4en_ene 104 % ( 75- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.corn FAX: 805 925-3376 Page 10 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0194 - EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (B1F0194-BLKI) Analyzed: 06/07/21 12:49 Mercury ND 0.10 mg!kg LCS (B1F0194-BSI) Analyzed: 06/07/21 12:53 Mercury 0.782 0.10 mg/kg 0.833 94 85-115 LCS Dup (B1F0194-BSDI) Analyzed: 06/07/21 13:30 Mercury 0.859 0.10 mg/kg 0.833 103 85-115 9 20 Duplicate (B1F0194-DUP1) Source: 2103489-02 Analyzed: 06/07/21 13:34 Mercury ND 0.097 mg/kg ND 20 Matrix Spike (B1F0194-MS1) Source: 2103489-02 Analyzed: 06/07/21 13:37 Mercury 0.927 0.091 mg/kg 0.755 ND 110 75-125 Matrix Spike Dup (131170194-MSDI) Source: 2103489-02 Analyzed: 06/07/21 13:39 Mercury 0.839 0.089 mg -kg 0.742 ND 113 75-125 1 20 Post Spike (B1F0194-PS1) Source: 2103489-02 Analyzed: 06/07/21 13:41 Mercury 5.52 ug/1. 25.0 0.00199 22 85-115 QL-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLK1) Analyzed: 06/07/21 13:30 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 " Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1.0 Lead ND 0.50 Molybdenum ND 0.50 Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (B1F0197-BS1) Analyzed: 06/07/21 13:35 Antimony 92.0 2.5 mg/kg 100 92 80-120 Arsenic 97.2 2.0 100 97 80-120 Barium 99.6 1.0 100 100 80-120 Beryllium 95.1 0.50 " 100 95 80-120 Cadmium 98.2 0.25 100 98 80-120 Chromium 98.8 0.50 100 99 80-120 Cobalt 99.2 0.50 100 99 80-120 Copper 98.2 1.0 100 98 80-120 Lead 100 0.50 100 100 80-120 Molybdenum 96.0 0.50 100 96 80-120 Nickel 99.6 0.50 100 100 80-120 Selenium 96.4 2.0 100 96 80-120 Silver 4.92 0.50 5.00 98 80-120 Thallium 100 LO 100 100 80-120 Vanadium 96.6 2.0 100 97 80-120 Zinc 98.6 2.0 100 99 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: N14C SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control malyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0197 -EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSDl) Analyzed: 06/07/21 13:37 Antimony 94.8 2.5 mg/kg 100 95 80-120 3 20 Arsenic 98.8 2.0 100 99 80-120 2 20 Barium 101 1.0 100 101 80-120 1 20 Beryllium 96.5 0.50 100 96 80-120 1 20 Cadmium 99.2 0.25 100 99 80-120 1 20 Chromium 100 0.50 100 100 80-120 1 20 Cobalt 100 0.50 100 100 80-120 1 20 Copper 99.8 1.0 100 100 80-120 2 20 Lead 101 0.50 100 101 80-120 1 20 Molybdenum 98.2 0.50 100 98 80-120 2 20 Nickel 101 0.50 100 101 80-120 1 20 Selenium 97.8 2.0 100 98 80-120 1 20 Silver 4.93 0.50 5.00 99 80-120 0.1 20 Thallium 102 1.0 100 102 80-120 1 20 Vanadium 98.0 2.0 100 98 80-120 1 20 Zinc 99.8 2.0 100 100 80-120 1 20 Duplicate (B1F0197-DUPI) Source: 2103489-01 Analyzed: 06/07/21 13:52 Antimony ND 2.4 mg -kg ND 20 Arsenic 1.22 1.9 ND 20 Barium 21.0 0.97 22.9 8 20 Beryllium ND 0.49 ND 20 Cadmium ND 0.24 ND 20 Chromium 1.94 0.49 2.02 4 20 Cobalt 1.40 0.49 1.78 24 20 QR-04 Copper 1.33 0.97 1.40 5 20 Lead 1.23 0.49 1.40 13 20 Molybdenum ND 0.49 ND 20 Nickel 1.31 0.49 1.34 2 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 3.80 1.9 4.18 8 20 Zinc 432 1.9 4.51 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MS1) Source: 2103489-01 Analyzed: 06/07/21 13:40 Antimony 70.3 2.3 mg!kg 93.4 ND 75 10-116 Arsenic 93.3 1.9 93.4 ND 100 77-121 Barium 119 0.93 93.4 22.9 102 30-169 Beryllium 90.1 0.47 93.4 ND 96 86-111 Cadmium 91.8 0.23 93.4 ND 98 81-112 Chromium 96.8 0.47 93.4 2.02 102 75-129 Cobalt 94.2 0.47 93.4 1.78 99 71-121 Copper 96.2 0.93 93.4 1.40 102 68-135 Lead 94.4 0.47 93.4 1.40 100 72-121 Molybdenum 88.2 0.47 93.4 ND 94 70-112 Nickel 95.2 0.47 93.4 1.34 101 73-121 Selenium 90.1 1.9 93.4 ND 97 76-116 Silver 4.56 0.47 4.67 ND 98 54-132 Thallium 92.3 0.93 93.4 ND 99 64-120 Vanadium 96.5 1.9 93.4 4.18 99 78-124 Zinc 98.0 1.9 93.4 4.51 100 50-143 Matrix Spike Dup (B1F0197-MSD1) Source: 2103489-01 Analyzed: 06/07/21 13:42 Antimony 70.4 2.4 mg'kg 95.8 ND 73 10-116 0.1 20 Arsenic 94.3 1.9 95.8 ND 98 77-121 l 20 Barium 116 0.96 95.8 22.9 97 30-169 3 20 Beryllium 91.2 0.48 95.8 ND 95 86-111 1 20 Cadmium 92.3 0.24 95.8 ND 96 81-112 0.6 20 Chromium 97.6 0.48 95.8 2.02 100 75-129 0.8 20 Cobalt 94.7 0.48 95.8 1.78 97 71-121 0.6 20 Copper 96.9 0.96 95.8 1.40 100 68-135 0.7 20 Lead 94.9 0.48 95.8 1.40 98 72-121 0.6 20 Molybdenum 88.6 0.48 95.8 ND 93 70-112 0.5 20 Nickel 95.5 0.48 95.8 1.34 98 73-121 0.3 20 Selenium 91.2 1.9 95.8 ND 95 76-116 1 20 Silver 4.64 0.48 4.79 ND 97 54-132 2 20 Thallium 93.1 0.96 95.9 ND 97 64-120 0.9 20 Vanadium 97.2 1.9 95.8 4.18 97 78-124 0.7 20 Zinc 103 1.9 95.8 4.51 103 50-143 5 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oee.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PS1) Source: 2103489-01 Analyzed: 06/07/21 13:45 Antimony 2.03 mg/L 2.00 0.00248 101 75-125 Arsenic 2.04 2.00 0.0178 101 75-125 Barium 2.50 2.00 0.460 102 75-125 Beryllium 1.96 2.00 0.0021E 98 75-125 Cadmium 2.00 2.00 -0.00308 100 75-125 Chromium 2.07 2.00 0.040E 101 75-125 Cobalt 2.06 2.00 0.0359 101 75-125 Copper 2.06 2.00 0.0283 102 75-125 Lead 2.07 2.00 0.0283 102 75-125 Molybdenum 2.01 2.00 -0.00109 101 75-125 - Nickel 2.06 2.00 0.0271 102 75-125 Selenium 1.99 2.00 -0.0103 99 75-125 Silver 0.0945 0.100 -0.00169 94 75-125 Thallium 2.03 2.00 -0.00407 101 75-125 Vanadium 2.08 2.00 0.0842 100 75-125 Zinc 2.10 2.00 0.0909 101 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLK1) Analyzed: 06/04/21 12:45 TPH Gasoline (C5-C12) ND 0.49 mg/kg Surrogate:4-Bromolluoroben:7ene 0.107 110.123 87 39-157 LCS (B1F0154-BS1) Analyzed: 06/04/21 11:48 TPH Gasoline (C5-C12) 1.38 0.50 mg/kg 0.999 138 68-139 Surrogate:4-Brwnulluoroben_ene 0.158 110.125 126 39-157 LCS Dup (B1F0154-BSDl) Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12) 1.29 0.50 mg/kg 1.00 128 68-139 7 20 Surrogate: 4-Bromglluorobenzene 0.146 110.125 116 39-157 . Duplicate (B1F0154-DUPl) Source: 2103455-02RE1 Analyzed: 06/04/21 15:35 TPH Gasoline (C'5-('12) ND 0.50 mg/kg 0.113 20 Surrogate:4-Bromgliuorobenzene 0.113 110.124 92 39-157 Matrix Spike (B1F0154-MS1) Source: 2103429-02 Analyzed: 06/04/21 19:23 TPH Gasoline (C5-('12) 0.905 0.49 mg/kg 0.973 ND 93 10-171 Surrogate:4-Bromolluorobeu:ene 0.132 110.122 109 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Semi-Volatile1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) Analyzed: 06/04/21 11:45 TPH Diesel (C13-('22) ND 10 mg/kg TP11 Motor Oil (C 23-C40) ND 50 " Surrogate: u-Terphenyl 41.5 " 50.0 83 65-136 LCS (B1F0145-BS1) Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22) 434 10 mg/kg 499 87 72-115 TPH Motor Oil (C23-C40) 420 50 499 84 74-126 Surrogate: o-Terphenyl 45.8 49.9 92 65-136 LCS Dup (B1F0145-BSD1) Analyzed: 06/04/21 12:07 TPH Diesel (C I 3-C22) 444 10 mg/kg 499 89 72-115 2 20 TPH Motor Oil (C23-C40) 441 50 499 88 74-126 5 20 Surrogate. o-Terphenyl 46.7 49.9 94 65-136 Duplicate (B1F0145-DUP1) Source: 2103472-01 Analyzed: 06/04/21 16:23 TP11 Diesel (('13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) ND 50 ND 20 Surrogate: o-Terphenyl 40.5 49.9 81 65-136 Matrix Spike (B1F0145-MS1) Source: 2103472-01 Analyzed: 06/04/21 15:37 TPH Dicscl (C13-C22) 452 10 mg./kg 498 ND 91 46-147 TPH Motor Oil (C23-C40) 500 50 498 ND 100 35-171 Surrogate: o-Terphenyl 41.6 49.8 84 65-136 Matrix Spike Dup (B1F0145-MSD1) Source: 2103472-01 Analyzed: 06/04/21 16:00 TPH Diesel (C13-C22) 490 10 mg/kg 498 ND 100 46-147 9 20 TPH Motor Oil (C23-C40) 517 50 498 ND 104 35-171 3 20 Surrogate: o-Terphenyl 44.0 49.8 88 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 18 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 .- Blank (B1F0146-BLKI) Analyzed: 06/04/21 11:32 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 Bromochloromcthanc ND 0.0050 " Bromodiehloromethane ND 0.0050 " Bromoform ND 0.0050 " Bromomethane ND 0.0050 " n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 " Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 " C'hloromethane ND 0.0050 " 2-Cllorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromuchloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibrontoethane (FDB) ND 0.0050 " Dibromomcthanc ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " 1,3-Dichlorobenzene ND 0.0050 1,4-Diclorobenzene ND 0.0050 Dichlorodifluorontcthanc ND 0.0050 CCHI 1, 1 -Dichloroethane ND 0.0050 " 1,2-Dichlorocthane ND 0.0050 I,1-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " 1.2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 " 2.2-Dichloropropane ND 0.0050 - 1,1-Dichloropropene ND 0.0050 cis-L3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 " Etylbenzene ND 0.0050 " Hexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " - Nlethylene chloride ND 0,0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1) Analyzed: 06/04/21 11:32 Styrene ND 0.0050 mgtkg 1,1.1,2-Tetrachloroethane ND 0.0050 " 1,1.2,2-Tetrachloroethanc ND 0.0050 Tetrachloroethene (PCE) NI) 0.0050 " Toluene ND 0.0050 1,23-Trichlorobenzene ND 0.0050 " 1,2,4-1'richloroben7ene ND 0.0050 1,1,1-Trichloroethane NI) 0.0050 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) NI) 0.0050 " �-+ Trichlorofluoromethanc ND 0.0050 " 1,2.3-Trichloropropane ND 0.0050 1,24-Trimethylbenzene ND 0.0050 1,3,5-Trimethylbenzene ND 0.0050 R' Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 " Surrogate: Dibroniulluorometheutc 0.0516 110.0498 104 74-122 Surrogate: Tohiene-d8 0.0503 110.0498 lull 65-128 Surrogate: 4-BromoPuborobenzene 0.0529 " 0.0498 106 75-121 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 Benzene 0.0406 0.0050 mg/kg 0.0398 102 70-131 Bromobenzene 0.0466 0.0050 0.0399 117 74-130 Bromochloromcthane 0.0399 0.0050 0.0398 100 64-133 Bromodichloromethane 0.0445 0.0050 0.0398 112 69-137 Bromoform 0.0447 0.0050 0.0398 112 55-132 Bromomethane 0.0407 0.0050 0.0398 102 10-142 n-Butylbenzene 0.0476 0.0050 " 0.0398 120 64-156 sec-Butylbenzene 0,049; 0.0050 0.0398 124 75-155 tort-Butylbenzene 0.0482 0.0050 0.0398 121 74-144 Carbon tetrachloride 0.0442 0.0050 0.0398 111 67-135 Chlorobenzene 0.0445 0.0050 0.0398 112 73-134 Chloroethane 0.0390 0.0050 0.0398 98 10-167 Chloroform 0.0412 0.0050 0.0398 104 69-124 Chloromethane 0.0297 0.0050 0.0398 75 34-136 2-Chlorololuene 0.0454 0.0050 0.0398 114 75-135 ' 4-Chlorotoluene 0.0460 0.0050 0.0398 116 70-138 Dibromochloromethane 0.0439 0.0050 0.0398 110 67-135 1,2-Dibromo-3-chloropropane 0.0435 0,0050 " 0.0399 109 41-149 1,2-Dibromoethane(ED13) 0.0409 0.0050 0.0398 103 68-131 Dibromomcthane 0.0433 0.0050 0.0398 109 61-140 1,2-Dichlorobenzene 0.0458 0.0050 0.0398 115 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.vecusa,c❑m FAX: (805) 925-3376 Page 20 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 VolatileOrganic CoinpoundsControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes •- Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 1.3-Dichlorobcnzene 0.0462 0.0050 mg/kg 0.0398 116 76-138 1,4-Dichlorobenzene 0.0457 0.0050 0.0398 115 72-132 Dichlorodilluoronuthanc 0.0210 0.0050 0.0398 53 10-155 CCFH 1,1-Dichloroethene 0.0389 0.0050 0.0398 98 63-139 1,2-Dichlorocthanc 0.0416 0.0050 0.0398 104 64-126 1. 1 -Dichloroethene 0.0342 0.0050 0.0399 86 52-167 _ cis-1.2-Dichloroethene 0.0401 0.0050 0.0398 WI 70-135 trans-1,2-Dichloroethene 0.0392 0.0050 0.0398 99 67-147 1,2-Dichloropropane 0.0400 0.0050 0.0398 102 68-131 13-Dichloropropane 0.0405 0.0050 0.0398 102 64-128 - 2,2-Dichloropropane 0.0432 0.0050 0.0398 109 63-154 1,1-Dichloropropene 0.0393 0.0050 0.0398 99 68-138 cis- 1.3 -Dichloropropene 0.0416 0.0050 0.0398 105 72-134 trans-1,3-Dichloropropene 0.0437 0.0050 0.0398 110 69-132 Ethylbenzene 0.0449 0.0050 0,0398 113 68-136 Hexachlorobutadiene 0.0546 0.0050 0.0398 137 72-198 4-Isopropyl Toluene 0.0504 0.0050 0.0398 127 74-150 Isopropylbenzene 0.0473 0.0050 0.0398 119 71-149 Niethylene chloride 0.0346 0.0050 0.0398 87 51-127 Naphthalene 0.0482 0.0050 0.0398 121 57-158 n-Propylbenzene 0.0474 0.0050 0.0398 119 70-143 Styrene 0.0456 0,0050 0.0398 115 68-138 1,1,1,2-Tetrachloroethane 0.0459 0.0050 0.0398 115 76-130 1JI22-Tetrachloroethanc 0.0399 0.0050 0.0398 100 60-136 Tetrachloroethene (PCE) 0.0443 0.0050 0.0398 111 73-138 Toluene 0.0430 0.0050 0.0398 108 72-128 1,2,3-Trichlorobenzene 0.0507 0.0050 0.0398 127 61-166 L2.4-Trichlorobenzene 0.0502 0.0050 0.0398 126 71-158 1,1,1-Trichloroethane 0.0424 0.0050 0.0398 107 71-135 1,1,2-Trichloroethane 0.0414 0.0050 0.0398 104 64-132 Trichloroethene (TCE) 0.0442 0.0050 0.0399 111 74-139 Trichlorotluoromethane 0.0429 0.0050 0.0398 108 30-156 1,2,3-Trichloropropane 0.0452 0.0050 0.0398 114 67-123 1.2,4-Trimethylbenzene 0.0454 0.0050 0.0398 114 68-134 1,3,5-Trimethylbenzene 0.0461 0.0050 0.0398 116 71-140 Vinyl chloride 0.0326 0.0050 0.0398 82 43-144 Xylenes (total) 0.133 0.0050 0.119 112 69-138 Surrogate: Dibronwlluorunrethcure 0.0525 0.0497 106 74-122 Surrogate: Toluene-d$ 0.0517 0.0497 104 65-128 Surrogate:4-Bromolluorohenzene 0.0530 0.0497 107 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) Analyzed: 06/04/21 10:13 Benzene 0.0423 0.0050 mg/kg 0.0400 106 70-131 4 20 Bromobenzene 0.0498 0.0050 0.0400 124 74-130 7 20 Bromochloromethanc 0.0412 0.0050 0.0400 103 64-133 3 20 Bromodichloromethane 0.0455 0.0050 0.0400 114 69-137 2 20 Bromotorni 0.0458 0.0050 0.0400 115 55-132 2 20 Bromomethane 0.0391 0.0050 0.0400 98 10-142 4 20 n-Butylbenzene 0.0476 0.0050 0.0400 119 64-156 0.1 20 sec-Butylbenzene 0.0508 0.0050 0.0400 127 75-155 3 20 tert-Butylbenzene 0.0496 0.0050 0.0400 124 74-144 3 20 Carbon tetrachloride 0.0456 0.0050 0.0400 114 67-135 3 20 Chlorobenzene 0.0457 0.0050 0.0400 114 73-134 3 20 Chloroethane 0.0394 0.0050 0.0400 98 10-167 1 20 Chloroform 0.0421 0.0050 0.0400 105 69-124 2 20 C:hloromethane 0.0308 0.0050 0.0400 77 34-136 4 20 2-Chlorotoluene 0.0452 0.0050 0.0400 113 75-135 0.4 20 4-Chlorotoluene 0.0468 0.0050 0.0400 117 70-138 2 20 Dibromochloromethane 0.0463 0.0050 0.0400 116 67-135 5 20 1,2-Dibromo-3-chloropropane 0.0461 0.0050 0.0400 115 41-149 6 20 1,2-Dibromoethane (F.DB) 0.0422 0.0050 0.0400 105 68-131 3 20 Dibromomcthane 0.0459 0.0050 0.0400 115 61-140 6 20 1,2-Diclilorobenzene 0.0472 0.0050 0.0400 118 76-136 3 20 1,3-Dichloroben7enc 0.0489 0.0050 0.0400 122 76-138 6 20 1,4-Dichlorobenzene 0.0472 0.0050 0.0400 118 72-132 3 20 Dichloroditluoromcthanc 0.0228 0.0050 0.0400 57 10-155 8 20 CCFH I,1-Dichloroethane 0.0405 0.0050 0.0400 WI 63-139 4 20 1,2-Dichloroethane 0.0425 0.0050 0.0400 106 64-126 2 20 1, 1 -Dichloroethene 0.0347 0,0050 0.0400 87 52-167 2 20 cis- I .2-Dichloroethene 0.0420 0.0050 0.0400 105 70-135 5 20 trans-1,2-Dichloroethene 0.0401 0.0050 0.0400 100 67-147 2 20 1,2-Dichloropropaue 0.0430 0.0050 0.0400 107 68-131 6 20 1.3-Dichloropropaue 0.0426 0.0050 0.0400 106 64-128 5 20 2,2-Dichloropropaue 0.0446 0.0050 0.0400 111 63-154 3 20 1, 1 -Dichloropropene 0.0406 0.0050 0.0400 102 68-138 3 20 cis-1,3-Dichloropropene 0.0434 0.0050 0.0400 108 72-134 4 20 trans-1,3-Dichloropropene 0.0454 0.0050 0.0400 114 69-132 4 20 Ethylbenzene 0.0470 0.0050 0.0400 118 68-136 5 20 Hexachlorobutadiene 0,0549 0.0050 0.0400 137 72-198 0.5 20 4-Isopropyl Toluene 0.0514 0.0050 0.0400 128 74-150 2 20 Isopropylbenzene 0.0499 0.0050 0.0400 125 71-149 5 20 Nlethylene chloride 0.0360 0.0050 0.0400 90 51-127 4 20 Naphthalene 0.0511 0.0050 0.0400 128 57-158 6 20 n-Propylbenzene 0.0466 0.0050 0.0400 116 70-143 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 VolatileOrganic Compoundsby Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) Analyzed: 06/04/21 10:13 Styrene 0.0479 0.0050 mg/kg 0.0400 120 68-138 5 20 1, 1, 1,2-Tetrachloroethane 0.0490 0.0050 0.0400 123 76-130 7 20 1,1,2,2-1'ctrachloroethanc 0.0417 0.0050 0.0400 104 60-136 5 20 Tetrachloroethene WCE) 0.0454 0.0050 0.0400 114 73-138 3 20 Toluene 0.0439 0.0050 0.0400 110 72-128 2 20 1,2,3-Trichlorobenzene 0.0520 0.0050 0.0400 130 61-166 3 20 1,2,4-"I'richlorobenzene 0.0512 0.0050 0.0400 128 71-158 2 20 1, 1, 1 -Trichloroethane 0.0432 0.0050 0.0400 108 71-135 2 20 1,1.2-Trichloroethane 0.0449 0.0050 0.0400 112 64-132 8 20 Trichloroethene (TCE) 0.0448 0.0050 0.0400 112 74-139 1 20 Trichlorolluoromethane 0.0430 0.0050 0.0400 107 30-156 0.1 20 1,23-Trichloropropane 0.0463 0.0050 0.0400 116 67-123 3 20 1,2.4-Trintethvlbenzene 0.0459 0.0050 0.0400 115 68-134 1 20 1,3,5-Trimethylbenzene 0.0465 00.0050 0.0400 116 71-140 0.9 20 Vinyl chloride 0.0338 0.0050 0.0400 84 43-144 3 20 Xylenes (total) 0.139 0.0050 0.120 116 69-138 4 20 Surrogate: Dibrotnolluoromethane 0.0519 0.0500 104 74-122 Surrogate: Toluene-d8 0.0510 0.0500 102 65-128 Surogate:4-Bromolluorohen_ene 0.0530 0.0500 106 75-121 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 Blows Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromcthane ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromofonn ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochhxomethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropanc ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibronx>mcthane ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 23 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilet tControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate(B1F0146-DUPI) Source:2103474-01 Analyzed: 06/04/21 15:22 ISIo'S 1,3-Dichlorobenzene ND 0.0050 mgIg ND 20 1,4-Dichlorobeuzene ND 0.0050 ND 20 Dichlorodifluoromcthanc ND 0.0050 NI) 20 CCHI I.l-Dichloroethene NI) 0.0050 ND 20 1.2-Dichlorocthanc ND 0.0050 NI) 20 I,1-Dichloroethene NI) 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 NI) 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 N1) 20 1,1-Dichloropropene ND 0.0050 ND 20 cis-I.3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 Ethylbenzene ND 0.0050 ND 20 1lexachlorobutadiene ND 0.0050 ND 20 4-1sopropyl Toluene NI) 0.0050 NI) 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride NI) 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene NI) 0.0050 ND 20 Styrene ND 0.0050 ND 20 1, 1, 1,2-Tetrachloroethane ND 0.0050 ND 20 1,1,2,2-Tctrachlorocthanc ND 0.0050 ND 20 Tetrachloroethene WCE) ND 0.0050 ND 20 Tolucnc ND 0.0050 NI) 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2,4-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,12-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethane Ni) 0.0050 NI) 20 1,2,3-Trichloropropane NI) 0.0050 ND 20 1,2,4-Trimethvlbenzene NI) 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 NI) 20 Vinyl chloride ND 0.0050 NI) 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibromolluoromethane 0.053E " 0.0498 108 74-122 Surrogate: Touene-dR 0.0509 0. 04 98 102 65-128 Surrogate:4-Bromo/luorohenreme 0.0506 0.0498 102 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Method Summary 1nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal ' 8015 Dicscl & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAPNELAP STLC Metals by ICP 6010B STI.0 Chromium STLC/EPA 6010B Solid OEC, Internal " STLC Metals Extraction STLC Metals Extraction STLC Water OEC, Internal _. Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, Internal Total Metals by ICP 6010B Total Antimony EPA 601013 Solid OEC, CA-ELAP,NELAP 601013 Total Arsenic EPA 601013 Solid OEC, CA-ELAP,NELAP 601013Total Barium EPA 601013 Solid OEC, CA-ELAP_NELAP 601013 Total Beryllium EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Cadmium EPA 6010B Solid OEC. CA-ELAP,NELAP 6010B Total Chromium EPA 601013 Solid OEC, CA-FLAP,NELAP 001013 Total Cobalt EPA 601013 Solid OEC, CA-ELAP,NFLAP 601013 Total Copper EPA 601 pB Solid OEC. CA-ELAP,NELAP 6010B Total Lead EPA 6010B Solid OEC, CA-FLAP.NELAP 601013Total Molybdenum EPA 601013 Solid OEC, CA-ELAP,NELAP 6010B Total Nickel EPA 601013 Solid OEC, CA-ELAPNF.LAP 601013 Total Selenium EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Silver EPA 6010B Solid OF"C, C A-ELAP,NELAP 601013 Total Thallium EPA 601013 Solid OFC_ CA-ELAP,NELAP 601013 Total Vanadium EPA 6010B Solid OEC, CA-ELAP,NELAP 6010B Total Zinc EPA 6010B Solid OEC, CA-ELAP,NELAP Volatile Organic Compounds by GUMS 8260B Fun List EPA 826013 Solid OEC, CA-FLAP,NELAP 826013 Full List EPA 8200B Solid OEC, Internal Volatile Organic TPH by GC/FID 8015 TPH-gasoline FPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805r 925-3376 Page 25 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NBC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 DefinitionsNotes and Qualifier Definition MDI, Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference CCFll The CCV for this analyte failed high. Results for this analyte may be biased high. CCTiI The CCV for this analyte tailed high. Analyte result is ND. Data is not impacted. ISIowS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above I Ox STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 32 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 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E cu C6 to 0 E .0 z ce w u E IR A I A A co O N U- Em h- r MMr N ...00 it a. o. 0 E� U A r0: cfl 04 0 n: C A a { _ IL m C C y W E E CC E y c U � 1= 1= i- C] ❑ 0 0 m FJ- sPlloS PeAloslO 1e101 A11AISQUOD m io ei o ci m O G � zoos I VON 83d / 328d .� v � A101GelluBt _C [G a 6 N Q o OOUS-SOOAS J c In y WS09OW0S-dHl U y 'a Q ter, y r O E ePUlnS u H i �0 1 ePIUBAD aAUaeea z A 1sl-1 Ilnd 809ZB o Y d N +�$ Q a L.H s Z ❑ L +° U a d sleleW ZZ ePll a 96 in U CV d a m aD to m h o Fes^ S o > a mm m > > o A CL m p o m Q C N d Qf C 00 00 ' DD ® m m a E❑[� tn r` tll z ❑ } w O el T T '•� 00 m C L jp m y r Y = D L 11� to Cs. 00 z U n G e? y` •L N . ❑ } pe x 2• � r - `' C, n a N Em a w an c cA °o eq dCL dE wt, oak a c o N m o cB a a0. OW -5 (D41) ❑❑ m m m N a a r E ea m A C C C a; w tJ U E i= J � & 6 z 0 v N z J Q U w a w Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102742 Pacific Petroleum California Report Date: May 06, 2021 17:25 P. O. Box 2646 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 05, 2021 08:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page I of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received NW Corner 2102742-01 Solid Solid 05/04/2021 14:30 05/05/2021 08:00 NE Corner 2102742-02 Solid Solid 05/04/2021 14:35 05/05/2021 08:00 SW Corner 2102742-03 Solid Solid 05/04/2021 14:40 05/05/2021 08:00 SE Corner 2102742-04 Solid Solid 05/04/2021 14:45 05/05/2021 08:00 Center 2102742-05 Solid Solid 05/04/202114:50 05/05/202108:00 Saiiiple' Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GUM 8015 Diesel & Motor Oil List Bl E0062 05/05/2021 10:31 Total Metals by CVAA Mercury Total EPA 7471 A B I E0098 05/05/2021 08:00 Total Metals by ICP 6010B Total 131 E0102 05/05/2021 09:08 Volatile Organic Compounds by GUMS 8260B Full List BIF,0101 05/05/2021 09:05 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B 1 E0095 05/05/2021 06:24 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 _ - -- ---c— �` Page 2 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. 0. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by : Lab ID: 2102742-01 Field Data: NA Analyze Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mglcg I B11:0098 05'05,21 12:11 EPA 7471A Total Metals by ICP Antimony ND 2.5 mgckg 1 B I E0102 05/06/21 13:33 EPA 6010B Arsenic 7.8 2.0 Barium 120 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 44 0.50 Cobalt 18 0.50 Copper 36 0.99 Lead 16 0.50 " Molybdenum ND 0,50 " Nickel 71 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 43 2.0 " Zinc 68 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 19 4.4 mgtkg 1 B I E0095 05/05/21 12:06 EPA 8015M D-04 Surrogate: 4-Bromn/luorohen_ene 109'111, (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 490 10 mg'kg 1 B 1 E0062 05/05/21 19:52 EPA 8015M TPH Motor Oil (C23-C40) Ni) 50 " "1111 Surrogate: o-Tctphernd 89'% (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 37 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 1 7:25 I Analytical Report for Saniples Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by: Lab ID : 2102742-01 Field Data: NA Analytc Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R`07 Benzene ND 1.3 m6rkg 1000 BI FO101 II5105+121 1636 EPA 8200B Bromobenzene ND 1.3 " Bromochloromethane ND 1.3 Bromodichloromethane ND 1.3 Bromofonn ND 1.3 Bromomethane ND 1.3 n-Butylbenzene ND 1.3 " sec-Butylbenzene ND 1.3 tert-Butylbenzene ND 1.3 Carbon tetrachloride ND 1.3 " Chlorobcnzcnc ND 1.3 " Chlorocthane ND 1.3 Chlorotunn ND 1.3 Chloromethane ND 11 2-Chlorotoluene ND 1.3 4-C'hlorotoluene ND 1.3 " Dibromochloromethane ND 1.3 1,2-Dibronto-3-chloropropane ND 1.3 1,2-Dibromoethane (EDB) ND 1.3 Dibromomethane ND 1.3 1,2-Dichlorobenzene ND 1.3 1,3-Dichlorobenzene ND 1.3 1,4-Dichlorobenzene ND 1.3 Dichloroditluoromcthane ND 1.3 I,l-Dichloroethane ND 1.3 1,2-Dichloroethane ND 1.3 1, 1 -Dichloroethene ND 1.3 cis-1,2-Dichloroethene ND 1.3 " trans-1,2-Dicliloroethene ND 1.3 " 1,2-Dichloropropane ND 1.3 1,3-Dichloropropane ND 1.3 " 2,2-Dichloropropane ND 1.3 1,1-Dichloropropene ND 1.3 cis- 1.3-Dichloropropene ND 1.3 trans-1,3-Dichloropropene ND 1.3 Ethylbcnzenc ND 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 4 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & deported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by : Lab ID : 2102742-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.3 mg/kg 1000 BIE0101 05/05/21 10:56 F.PA9260B 4-Isopropyl Toluene ND 1.3 Isopropylbenzene ND 1.3 Methylene chloride ND 1.3 Naphthalene ND 1.3 n-Propylbenzene ND 1.3 " Styrene ND 1.3 1, 1, 1,2-Tetrachloroethane ND 1.3 " 1.1,2,2-1'etrachloroethane ND 1.3 7'ctrachlorocthcnc WCE) ND 1.3 Toluene ND 1.3 1,2,3-Trichloroben7cne ND 1.3 1,2,4-Trichlorobenzene ND 1.3 1, 1, 1 -Trichloroethane ND 1.3 1,1,2-Trichloroethane ND 1.3 Trichloroethene (TCE) ND 1.3 Trichlorolluoromethane ND 1.3 " 1,2.3-Trichloropropane ND 13 1,2.4-Trimethylbenzene ND 1.3 13,5-Trimethylbenzene ND 1.3 Vinyl chloride ND 1.3 Xylencs (total) ND 1.3 Surrogate: Dihrnlnoffifor methane 95 0;, (74 - 122 ) " Surrogate: Toluene-d8 95 % ( 65 - 12,Y) Surrogate: 4-BI'U711n/hlorohelcc'rtt' 90 �/. ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Z102742 Orcutt CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Saniples Sample ID : NE Corner Sampled: 05/04/21 14:35 Matrix: Solid Sampled by : Lab ID : 2102742-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Nutes Total Metals by CVAA Mercury Total Metals by ICP ND 0.093 mg/kg 1 BIF0098 05/05/2112:13 EPA 7471A Antimony ND 2.4 mg/kg 1 B1 E0102 05/06/21 13:36 EPA 6010B Arsenic 5.0 1.9 Barium 140 0.94 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 160 0.47 " N-02, N-03 Cobalt 22 0.47 Copper 37 0.94 Lead 6.8 0.47 " Molybdenum 0.51 0.47 Nickel 270 0.47 N-02 Selenium ND 1.9 Silver ND 0.47 Thallium 1.7 0.94 Vanadium 61 1.9 Zinc 59 1.9 " Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 5.6 4.3 mg/kg 1 B 1 E0095 05/05/2) 12:32 EPA 8015M D-04 Surrogate: d-Bromo/luorobemene 108 o (39 - 157) 11 11" Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 310 10 mg!kg 1 B 1 E0062 05/05/21 21:27 EPA 8015M TPH Motor Oil (C'23-C'40) ND 50 " " " " 1. Surrogate: o-Telphen.il 85 X (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: NE Corner Sampled: 05/04/21 14:35 Matrix: Solid Sampled by : Lab ID : 2102742-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg,kg 1000 B1 EO101 05/05/21 17:24 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichlorotnethane ND 1.2 Bromoform ND 1.2 Bromontethane NI) 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 12 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzcne ND 1.2 " Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloroniethane NI) 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibrontoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodiiluoromcthanc ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND L2 2,2-Dichloropropane ND L2 1, 1 -Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropanc ND 1.2 " Ethylbenzenc ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 37 W Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: NE Corner Sampled: 05/04/21 14:35 Matrix: Solid Sampled by : Lab ID: 2102742-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 1lexachlorobuladiene ND 1.2 mg/kg 1000 B I E0101 05/05/21 17:24 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbeuzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2=I'etrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 " Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 " 1,2,4-Trichlorohenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1.2,3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 " Xylencs (total) ND 1.2 Sarivgate: Dibromo/luoromethane 95 % ( 74- 122) Surrogate' Toluene-dS 94 % (65. 128) Surrogate: 4-Bromolluo oben_ene X6 ''N ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O Box 2646 Project Number: Natural Healing Center 21412742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by : Lab ID : 2102742-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B I E0098 05/05/21 12:15 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B I E0102 05/06/21 13:46 EPA 601 OB Arsenic 4.5 1.9 Barium 200 0.93 Beryllium ND 0.47 Cadmium ND 0.23 " Chromium 310 0.47 " Coball 55 0.47 Copper 45 0.93 Lead 9.5 0.47 Nlolvbdenum 0.68 0.47 " Nickel 430 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 70 1.9 Zinc 69 1.9 " Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) Surrogate: 4-Bronw luorohen_ene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPI1 Motor Oil (('23-('40) Surrogate: o-Telphem'1 7.8 5.0 mg'kg 1 BIE0095 05,05121 12:58 EPA8015M 1013„ (39- 157) 220 10 mg/kg 1 BIE0062 05/05/2121:51 EPA8015M ND 50 " " " 11 84 '1, (65 - 136) 11" 11 N-02, N-03 N-02 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID : SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by: Lab ID : 2102742-03 Field Data: NA Analyte Result R1, Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mb'kg 1000 B I F'0101 0/05/21 1 "-4� 1 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 " Bromoform ND 12 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 12 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-C'hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibrontoethane(FiDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobenzene ND 1.2 1,4-I)ichlorobenzenc ND 1.2 Dichlorodifluoronuthane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 ],I-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 " cis-1,3-Dichloropropene ND 1.2 " trans-1,3-Dichloropropene ND 1.2 " Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805925-3376 Page 10 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by : Lab ID : 2102742-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B1 E0101 05/05/21 17:51 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 " Methylene chloride ND 1.2 " Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-1•etrachloroethane ND 12 " 1,1,2,2-1'etrachloroethane ND 1.2 " Tetrachloroethcne WCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 " 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroetliane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Dibromofluororuethanc 93 `S, ( 74 - 122) " Surrogate: Tohrene-d8 94 % (65. 128 ) Surrogate: 4-Branu/hu»uhen_enc 88 `%b ( 75- 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Z102742 Orcutt CA, 93457 Project Manager. Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: SE Corner Sampled: 05/04/21 14:45 Matrix: Solid Sampled by: Lab ID : 2102742-04 Field Data: NA Analyte Result RL units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B I E0098 05/05/21 12:17 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B 1 E0102 05/06/21 13:49 EPA 601(1B Arsenic 5.0 1.9 " Barium 180 0.92 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 46 0.46 Cobalt 14 0.46 Copper 41 0.92 Lead 13 0.46 Molybdenum ND 0.46 Nickel 85 0.46 " Scicnium ND 1.8 Silvcr ND 0.46 Thallium 1.9 0.92 Vanadium 39 1.8 " zinc 57 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 5.6 4.4 mg/kg 1 BIE0095 05/05/21 13:24 EPA 8015M D-04 Surrogate. 4-Bronro/luoroheri--ene 108 % (39 - 157) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 190 10 mg/kg I B I E0062 05/05/21 22:15 EPA 8015M TPI I Motor Oil (C23-('40) ND 50 " " " " Surrogate: o-Terphe-W 85 %b (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376_ Page 12 of 37 KEC Pacific Petroleum California P. 0. Box 2646 Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. Project: Pacific Petroleum Project Number: Natural Healing Center Project Manager: Clarence Reynolds WO & Reported: 210z742 05/06/2021 17:25 Analytical Report for Sample ID : SE Corner Sampled: 05/04/21 14:45 Matrix: Solid Sampled by: Lab ID: 2102742-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgtkg 1000 B1E0101 05/05/2118:18 FPA8260B f Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzcne ND 1.2 " Chloroethane ND 1.2 Chlorofonn ND 1.2 C'hloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 " Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobenzenc ND 1.2 " IA-Dichlorobenzene ND 1.2 Dichloroditluoromethane ND 1.2 " 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 " " trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 " 1, 1 -Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 " trans-1,3-Dichloropropene ND 1.2 Ethylbenzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Pox 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportI Analytical Sample ID: SE Corner Sampled: 05/04/21 14:45 Matrix: Solid Sampled by: Lab ID : 2102742-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 l lexachlorobutadiene ND 1.2 mg/kg 1000 B I E0101 05/05/21 18:18 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND L2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 " 1,1,1,2-Tetrachloroethane ND 1.2 " 1,1,2,2-Tetrachloroetbanc ND 1.2 Tctrachloroctllene (PCE) ND 1.2 " Toluene ND 1.2 " 1,2,3-Trichlorobenzcne ND 1.2 1,2,4-Trichlorobenzene ND 1.2 " 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 " Xylcncs (total) ND 1.2 Surrogate: Dihromolluoromedutne 98 % (74 - 122) " Surrogate: Toluene-d8 96 % (65 - 128) " Surrogate: 4-Bromo/ltan•ohcu_cme 90 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical for Sample ID : Center Sampled: 05/04/21 14:50 Matrix : Solid Sampled by : Lab ID: 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.086 mg/kg 1 B I E0098 05/05/21 12:19 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 E0102 05/06/21 13:52 EPA 601013 Arsenic 7.0 1.9 " Barium 140 0.96 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 72 0.48 N-02 Cobalt 22 0.48 " Copper 78 0.96 Lead )5 0.48 Molybdenum 0.99 0.48 Nickel 160 0.48 " Selenium ND 1.9 " Silver ND 0.49 Thallium 1.3 0.96 " Vanadium 62 1.9 Zinc 80 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 7.7 4.8 mgAg 1 B 1 E0095 05/05/21 13:49 EPA 8015M D-04 Surrogate: d-Bromo/Inoroben_ene 106 3f, (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 350 10 mg'kg 1 B 1 E0062 05/05/21 22:38 EPA 8015M TPII Motor Oil (C23-C40) ND 50 Surrogate: o-Tciphenrl 861", (65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX (805) 925-3376 Page 15 of 37 C A 06MOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: Center Sampled: 05/04/21 14:50 Matrix : Solid Sampled by: Lab ID : 2102742-05 Field Data: NA Analjtta Result RL Units Dilution Batch Analyzed Method Noles Volatile Organic Compounds by GC/MS R-07 Benzene ND I.Z mg'kg Itttlll BIFitlitl 05 (t5 '1 I H af, i P•% H i lilt Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 C'hlorobenzcnc ND 1.2 Chlorocthanc ND 1.2 " Chloroform ND 1.2 Chloromelhane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 " Dibromocliloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 " Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzenc ND 12 Dichlorodifluoromethane ND 1.2 l,l-I)ichloroethane ND 1.2 1,2-Dichloroethene ND 1.2 1,1-Dichloroethene ND 1.2 cis- 1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane NI) L2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis- 1.3 -Dichloropropene ND 1.2 trans-1,3-Dichloropropcne ND 1.2 " Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 37 :0:E Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. Project: Pacific Petroleum Project Number: Natural Healing Center Project Manager: Clarence Reynolds WO & Reported: 2102742 05/06/2021 17:25 Analytical Report for Samples Sample ID: Center Sampled: 05/04/21 14:50 Matrix : Solid Sampled by : Lab ID : 2102742-05 Field Data: NA Analyte` Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 I I exachlorobutadiene ND 1.2 mgtkg 1000 B1E0101 05/05/21 18:46 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 . 1,1,1,2-1'etracliloroethane ND 1.2 1,1,2,2-Tetracliloroethane ND 1.2 " Tctrachlomcthcne (PCE) ND 1.2 Toluene ND 1.2 " 1,2,3-Trichlorobenzene ND 1.2 " 1,24-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 " 1,2.3-Trichloropropane ND 1.2 " 1,24-Trimethylbenzene ND 1.2 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Uibrom(i luoromethane 94 ' o ( 74 - 12 2) " Surrogate: Toluent,48 95 7& (65 - 128 ) Surrogate: 4-Bronuq/luoroben_ene 88 ;<b ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain ofcustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. 0. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Total Metals by CN7AA - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0098 - EPA 7471A Preparation: EPA 7471A Prep 05/05/21 08:00 Blank (B1E0098-BLK1) Analyzed: 05/05/21 11:40 Mercury ND 0.10 mg/kg LCS (B1E0098-BS1) Analyzed: 05/05/21 11:35 Mercury 0.902 0.10 mg/kg 0.833 96 85-115 LCS Dup (B1E0098-BSD1) Analyzed: 05/05/21 11:37 Mercury 0.831 0.10 mg/kg 0.833 100 85-115 4 20 Duplicate (B1E0098-DUPl) Source: 2102717-01 Analyzed: 05/05/21 11:44 Mercury 0.0262 0.10 mg/kg 0.0394 40 20 QR-04 Matrix Spike (B1E0098-MS1) Source: 2102717-01 Analyzed: 05/05/21 11:46 Mercury 0.836 0.097 mg!kg 0.812 0.0394 98 75-125 Matrix Spike Dup (B1E0098-MSDl) Source: 2102717-01 Analyzed: 05/05/21 11:48 Mercury 0.938 0.098 mg/kg 0.814 0.0394 98 75-125 0.3 20 Post Spike (B1E0098-PS1) Source: 2102717-01 Analyzed: 05/05/21 11:50 Mercury 5.22 ug/L 5.00 0.256 99 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805' 925-3376 Page 18 of 37 C A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 TotalControl Analyte Result RL Units Spike Source °,RFC " OREC' RPl) RPf) Ne%s Level Result Limits Limit Batch BIE0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Blank (B1E0102-BLKI) Analyzed: 05/06/21 13:12 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 " Thallium ND 1.0 " Vanadium ND 2.0 " Zinc ND 2.0 LCS (B1E0102-BSI) Analyzed: 05/06/21 12:50 Antimony 99.2 2.5 mg/kg 100 99 80-120 Arsenic 99.8 2.0 100 100 80-120 Barium 102 1.0 100 102 80-120 Beryllium 96.5 0.50 100 96 80-120 Cadmium 101 0.25 100 101 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 102 0.50 100 102 80-120 Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium 97.7 2.0 100 98 80-120 Silver 4.81 0.50 5.00 96 80-120 Thallium 104 LO 100 104 80-120 Vanadium 98.6 2.0 100 99 80-120 Zinc WI 2.0 100 101 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 t 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 LCS Dup (B1E0102-BSDl) Analyzed: 05/06/21 12:52 Antimony 99,8 2.5 mg/kg 100 100 80-120 0.6 20 Arsenic 102 2.0 100 102 80-120 2 20 Barium 103 1.0 100 103 80-120 1 20 Beryllium 97.2 0.50 100 97 80-120 0.8 20 Cadmium 102 0.25 l00 102 80-120 0.9 20 Chromium 103 0.50 100 103 80-120 0.6 20 Cobalt 103 0.50 100 103 80-120 0.6 20 Cropper 103 1.0 100 103 80-120 0.6 20 Lead 103 0.50 100 103 80-120 0.5 20 Molybdenum 99.6 0.50 100 100 80-120 2 20 Nickel 103 0.50 100 103 80-120 0.6 20 Selenium 100 2.0 100 100 80-120 3 20 Silver 4.89 0.50 5.00 98 80-120 2 20 Thallium 105 LO 100 105 80-120 2 20 Vanadium 98.9 2.0 100 99 80-120 0.4 20 Zinc 102 2.0 100 102 80-120 0.6 20 Duplicate (B1E0102-DUPl) Source: 2102717-02 Analyzed: 05/06/21 13:17 Antimony ND 2.4 mg/kg ND 20 Arsenic 7.55 1.9 8.39 10 20 Barium 92.7 0.95 97.2 5 20 Beryllium 0.657 0.48 0.691 5 20 Cadmium ND 0.24 ND 20 Chromium 16.8 0.48 16.2 4 20 Cobalt 7.71 0.48 8.09 5 20 Copper 18.7 0.95 19.7 5 20 Lead 11.1 0.48 11.8 6 20 Molybdenum 1.43 0.49 1.58 10 20 Nickel 22.9 0.48 19.7 15 20 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.95 ND 20 Vanadium 32.2 1.9 32.7 2 20 Zinc 60.1 1.9 64.4 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: J805925-3376 Page 20 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcun CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Control Analvte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Matrix Spike (B1E0102-MS1) Source: 2102717-02 Analyzed: 05/06/21 12:55 Antimony 26.4 2.5 mg/kg 99.2 ND 27 10-116 Arsenic 105 2.0 99.2 8.39 98 77-121 Barium 193 0.99 99.2 97.2 97 30-169 Beryllium 93.6 0.50 99.2 0.69.1 94 86-I11 Cadmium 93.6 0.25 99.2 ND 94 81-112 Chromium 118 0.50 99.2 16.2 103 75-129 Cobalt 102 0.50 99.2 8.09 94 71-121 Copper 119 0.99 99.2 19.7 100 68-135 Lead 105 0.50 99.2 11.8 94 72-121 Molybdenum 89.4 0.50 " 99.2 1.58 89 70-112 Nickel 114 0.50 99.2 19.7 95 73-121 Selenium 89.8 2.0 99.2 ND 91 76-116 Silver 4.31 0.50 4.96 ND 87 54-132 Thallium 89.0 0.99 99.2 ND 90 64-120 Vanadium 130 2.0 99.2 32.7 98 78-124 Zinc 158 2.0 99.2 64.4 94 50-143 Matrix Spike Dup (B1E0102-MSD1) Source: 2102717-02 Analyzed: 05/06/21 12:57 Antimony 29.7 2.4 mg'kg 94.4 ND 31 10-I16 12 20 Arsenic 103 1.9 " 94.4 8.39 101 77-121 2 20 Barium 182 0.94 " 94.4 97.2 89 30-169 6 20 Beryllium 91.6 0.47 94.4 0.691 96 86-111 2 20 Cadmium 91.5 0.24 94A ND 97 81-112 2 20 Chromium 113 0.47 94.4 16.2 103 75-129 4 20 Cobalt 99.2 0.47 94.4 8.09 96 71-121 3 20 Copper 114 0.94 94.4 19.7 100 68-135 4 20 Lead 102 0.47 94.4 11.8 96 72-121 3 20 Molybdenum 88.9 0.47 " 94.4 1.58 92 70-112 0.6 20 Nickel 111 0.47 1.94.4 19.7 96 73-121 3 20 Selenium 88.7 1.9 94.4 ND 94 76-116 1 20 Silver 4.23 0.47 4.72 ND 90 54-132 2 20 Thallium 87.0 0-94 94.4 ND 92 64-120 2 20 Vanadium 126 1.9 94.4 32.7 98 78-124 4 20 Zinc 153 1.9 94.4 64.4 94 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Total Metals by 'Control Analv_ to Result Rl. Units Spike Source %REC °,oREC RPI2 RPD Notes Level Result Limits Limit Batch BlE0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Post Spike (B1E0102-PS1) Source: 2102717-02 Analyzed: 05/06/21 13:00 Antimony 1.95 mg/L 2.00 -0.0338 98 75-125 Arsenic 2.25 2.00 0.171 104 75-125 Barium 3.97 2.00 1.98 99 75-125 Beryllium 1.97 2.00 0.0141 98 75-125 Cadmium 1.97 2.00 -0.0215 99 75-125 Chromium 2.42 2.00 0.330 104 75-125 Cobalt 2.15 2.00 0.165 99 75-125 Copper 2.51 2.00 0.401 105 75-125 Lead 2.20 2.00 0.240 98 75-125 Molybdenum 2.02 2.00 0.0322 99 75-125 Nickel 2.48 2.00 0.403 104 75-125 Selenium 1.96 2.00 -0.0744 98 75-125 Silver 0.0946 0.100 -0.00744 95 75-125 Thallium 1.88 2.00 -0.0732 94 75-125 Vanadium 2.71 2.00 0.668 102 75-125 Zinc 3.25 2.00 1.31 97 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 -- Page 22 of 37 Oilfield Environmental & compliance, Inc. Pacific Pettoleum California Project: Pacific Petroleum WO & Reported: P O Box 2646 Project Plumber: Natural Healing Center 2102742 Orcuti CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile1 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO095 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/05/21 06:24 Blank (BIE0095-BLK1) Analyzed: 05/05/21 09:00 TPH Gasoline W5-02) ND 0.50 mg/kg Surrogate:4-Bromo/luorohenzene 0.134 110.124 ]OR 39-157 LCS (B1E0095-BSI) Analyzed: 05/05/21 08:09 TPH Gasoline (C5-C12) 0.917 0.50 mg/kg 0.992 92 M-139 Surrogate' 4-Bromolluorohen:e1le 0.158 .' 0.124 127 39-157 LCS Dup (B1E0095-BSDI) Analyzed: 05/05/21 08:34 TPII Gasoline (C5-Cl2) 1.03 0.50 mg/kg 0.994 103 68-139 11 20 Surrogate:4-Bromo/luorohen_ene 0.157 110.124 127 39-157 Duplicate (B1E0095-DUP1) Source: 2102652-01 Analyzed: 05/05/21 09:59 TPH Gasoline (C5-C12) ND 5.2 mg/kg ND 20 Surrogate:4-Bromolliurohenzene 1.30 111.30 100 39-157 Matrix Spike (B1EO095-MS1) Source: 2102652-01 Analyzed: 05/05/21 14:41 TPH Gasoline (('5-('12) 7.97 4.9 mg/kg 9.80 ND 81 10-171 Surrogale: 4-Bromolluorohen_ene 1.40 1.23 115 39-157 Matrix Spike Dup (BIE0095-MSDI) Source: 2102652-01 Analyzed: 05/05/21 15:07 TPH Gasoline (C54'12) 8.18 5.2 mg/kg 10.4 ND 78 10-171 3 20 Surrogate.' 4-Brnmolluorohenreue 1.40 111.30 107 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 21.02742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Semi-Volatile1 - Quality Control Analyte Result RL Units Spike Source %RE(' %REC RPD RPD Notes Level Result Limits Limit Batch BlEO062 - EPA 8015M Preparation: EPA 3550C 05/05/21 10:31 Blank (B1E0062-BLK1) Analyzed: 05/05/21 17:58 TPH Diesel (C13-C22) ND 10 mg/kg TPH Motor Oil (C'23-C40) ND 50 " Surrogate: o-Tcrphenrl 37.8 " 49.9 76 65-136 LCS (BIE0062-BSI) Analyzed: 05/05/21 17:12 TPH Diesel (C13-C22) 411 10 mg/kg 500 82 72-115 TPH Motor Oil (('23-C40) 467 50 500 93 74-126 Surrogate: o-Tcrphent,l 400 50.0 80 65-136 LCS Dup (B1E0062-BSD1) Analyzed: 05/05/21 17:35 TPH Diesel (C13-C22) 433 10 mg/kg 499 87 72-115 5 20 TPH Motor Oil (C23-C40) 493 50 499 99 74-126 6 20 Surrogate: o-TcrphvnYl 41.1 49.9 82 65-136 Duplicate (B1E0062-DUPl) Source: 2102648-01 Analyzed: 05/05/21 21:27 TPH Diesel (('13-C22) 35.5 10 mg/kg 34.6 2 20 D-04 TPH Motor Oil (('23-C40) 71.2 50 65.4 8 20 D-04 Surrogate: o-Terphen'1 53.6 49.8 108 65-136 Matrix Spike (B1E0062-MS1) Source: 2102648-01 Analyzed: 05/05/21 21:51 TPH Diesel (('13-C22) 731 10 mg/kg 499 34.6 140 46-147 TPH Motor Oil (('23-C40) 559 50 499 65.4 99 35-171 Surrogate: o-Terphenrl 44.1 49.9 88 65-136 Matrix Spike Dup (B1E0062-MSD1) Source: 2102648-01 Analyzed: 05/05/21 22:15 TPH Diesel (C'13-C'22) 502 10 mg/kg 499 34.6 106 46-147 26 20 QR-02 TPH Motor Oil (C23-C40) 485 50 499 65.4 84 35-171 14 20 Surrogate: o-Tcrpher14 41.3 49.9 83 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 24 of 37 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcun CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 CompoundsVolatile Organic Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO101- EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (BlE0101-BLK1) Analyzed: 05/05/21 13:17 Benzene ND 0.25 mg/kg Bromobenzene NI) 0.25 Bromochloromcthanc ND 0.25 Bromodichloromethane ND 0.25 " Bmmoform ND 0.25 " Bromomethane NI) 0.25 " n-Butylbenzene ND 0.25 sec-Butylbenzene NI) 0.25 " tort -Butyl benzene ND 0.25 Carbon tetrachloride NI) 025 " Chlorobenzene NI) 025 C'hloroethane NI) 0.25 Chloroform ND 0.25 Chloromethane NI) 0.25 2-Chlorotoluene ND 025 4-Chlorotoluene ND 0.25 " Dibromochloromethane ND 0.25 1,2-Dibromo-3-chloropropane ND 0.25 1,2-Dibromoethane (FDB) ND 025 " Dibrtttnomcthane ND 0.25 1,2-r)iehlorobenzene ND 025 " 13-Dichlorobenzenc ND 0.25 1,4-Dichlorobenzene ND 0.25 Dichlorodifluoromcthanc ND 0.25 " 1, 1 -Dichloroethane ND 025 1,2-Dichlorocthane ND 0.25 " 1, 1 -Dichloroethene NI) 0.25 " cis-1.2-Dichloroethene ND 0.25 " trans-1,2-Dichloroethene ND 0.25 1,2-Dichloropropane ND 0.25 1,3-Dichloropropene NI) 0.25 22-Dichloropropanc ND 0.25 " 1, 1 -Dichloropropene NI) 0.25 " cis- 1.3-Dichloropropene ND 0.25 " trans- l,3-Dichloropropene ND 025 Fthylbenzene NU 0.25 " Ilexachlorobutadiene ND 025 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene Ni) 025 " h9ethylene chloride ND 0.25 Naphthalene NI) 025 n-Propylbenzene N1) 025 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: R O. Box 2(Y46 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank(B1E0101-BLKI) Analyzed:05/05/2) 13:17 Styrene ND 0.25 mg/kg 1, 1, 1,2-Tetrachloroethane ND 0.25 1,1,2,2-1'ctrachloroethanc ND 0.25 Tetrachloroethene (PCE) ND 0.25 Toluene ND 0.25 " 1,2,3-Trichlorobenzene ND 0.25 " 1,2,4-1'richlorobenzene ND 0.25 1, 1, 1 -Trichloroethane ND 0.25 1,1,2-Trichloroethane ND 0.25 " Triehloroethene (TC'E) ND 0.25 Trichlorofluoromethane ND 0.25 " 1,2,3-Trichloropropane ND 0.25 1,2,4-Trimethylbenzene ND 0.25 " 1,3,5-Trimethylbenzene ND 0.25 Vinyl chloride ND 0.25 Xylenes (total) ND 0.25 Surrogate: Dibroniglluoromethane 0.0468 0.0496 94 74-122 Surrogate: Toluene-db' 0.0462 0.0496 93 65-128 Surrogate:4-Bromolluorohen_ene 0.0431 0,0496 87 75-127 LCS (B1E0101-BS1) Analyzed: 05/05/21 12:22 Benzene 2.30 0.25 nigkg 1.99 116 70-131 Bromobenzene 1.97 0.25 1.99 99 74-130 BromochlOrOmCthanc 1.85 0.25 1.99 93 64-133 Bromodichloromethane 1.99 0.25 1.99 100 69-137 Bromofornn 1.74 0.25 1.99 88 55-132 Bromomethane 1.64 0.25 1.99 83 10-142 n-Butylbenzene 2.58 0.25 1.99 130 64-156 sec-Butylbenzene 2.53 0.25 1.99 127 75-155 tort-Butylbenzene 2.32 0.25 1.99 117 74-144 Carbon tetrachloride 2.18 0,25 1.99 110 67-135 Chlorobenzene 2.17 0.25 1.99 109 73-134 Chloroethane 1.83 0.25 1.99 92 10-167 Chloroform 2.13 0.25 1.99 107 69-124 C'hloromethane 2.32 0.25 1.99 117 34-136 2-Chlorotoluene 2.14 0.25 1.99 107 75-135 4-Chlorotoluene 2.14 0.25 1.99 108 70-138 Dibromochloromethane 1.99 0.25 1.99 100 67-135 1,2-Dibromo-3-chloropropanc 1.99 0.25 1.99 100 41-149 1,2-Dibromoethane (EDB) 1.92 0.25 1.99 97 68-131 Dihromomcthanc 1.48 0.25 1.99 74 61-140 1,2-Dichlorobenzene 2.07 0.25 1.99 104 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 -- Page 26 of 37 C A 06-M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2.646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ControlVolatile Organic Coinpounds by GC/N1S - Quality Analyte Result RL Units Spike Source %RE(' %REC RPD RPD Notes Level Result Limits Limit Batch BIE0101- EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS (B1E0101-BS1) Analyzed: 05/05/21 12:22 1,3-Dichlorobenzcne 2.17 0.25 mglkg 1.99 109 76-138 1,4-Dichlorobenzene 2.14 0.25 1.99 108 72-132 Dichlorodifluoromcthanc 1.31 0.25 1.99 66 10-155 I,1-Dichloroethane 2.33 0.25 1.99 117 63-139 1,2-Dichloroethane 2.06 0.25 1.99 104 64-126 1,1-Dichloroethene 2.77 0.25 1.99 139 52-167 cis-1.2-Dichloroethene 2.07 0.25 1.99 104 70-135 trans-1,2-Dichloroethene 2.43 0.25 1.99 122 67-147 1.2-Dichloropropane 2.05 0.25 1.99 103 68-131 1,3-Dichloropropane 2.04 0.25 1.99 103 64-128 2,2-Dichloropropane 2.31 0.25 1.99 116 63-154 1,1-Dichloropropene 2.22 0.25 1.99 112 68-139 cis-1,3-Dichloropropene 2.09 0.25 1.99 105 72-134 trans-1,3-Dichloropropene 2.26 0.25 1.99 114 69-132 Ethylbenzene 2.46 0.25 1.99 124 68-136 1lexachlorobutadiene 2.20 0.25 1.99 111 72-199 4-Isopropyl Toluene 2.39 0.25 1.99 120 74-150 Isopropylbenzene 2.41 0.25 1.99 121 71-149 Methylene chloride 2.57 0.25 1.99 129 51-127 QA1-08 Naphthalene 1.99 0.25 1.99 100 57-158 n-Propylbenzene 2.27 0.25 1.99 114 70-143 Styrene 2.25 0.25 1.99 113 68-138 1,1,1,2-Tetrachloroethane 1.92 0.25 1.99 97 76-130 1,1,2,2-Tetrachlorocihane 2.09 0.25 1.99 105 60-136 Telrachloroelhene(PCE) 2.09 0.25 1.99 105 73-139 Toluene 2.18 0.25 1.99 110 72-128 1,2,3-Trichlorobenzene 1.74 0.25 1.99 88 61-166 1.2,4-Trichlorobenzene 1.85 0.25 1.99 93 71-158 1,13-Trichloroethane 2.24 0.25 1.99 113 71-135 1,1.2-Trichloroethane 2.07 0.25 1.99 104 64-132 Trichloroethene(TCE) 1.92 0.25 1.99 97 74-139 Trichlorofluoromethane 1.74 0.25 1.99 87 30-156 1,2,3-Trichloropropane 2.01 0.25 1.99 101 67-123 1,2.4-Trimethylbenzene 2.52 0.25 1,99 127 68-134 1,3,5-Trimethylbenzene 2.37 0.25 1.99 119 71-140 Vinyl chloride 2.46 0.25 1.99 124 43-144 Xylenes (total) 7.54 0.25 5.96 126 69-138 Surrogate: Dibromolluoromethane 0.0485 0.0497 98 74-122 Surrogate: Touene-d8 0.0471 0.0497 95 65-128 Surrogate:4-Brontolluoroben_rne 0.0467 ().(1497 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported P. O. Box 2646 Project Number: Naturaf Healing Center 2102742 Orcutt CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 VolatileCompounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Lintit Batch BIE0101- EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1EO101-BSD1) Analyzed: 05/05/21 12:49 Benzene 2.25 0.25 mg/kg 1.99 113 70-131 2 20 Bromobenzene 1.93 0.25 1.99 97 74-130 2 20 Bromochloromcthane 1.85 0.25 1.99 93 64-133 0 20 Bromodichloromethane 2.00 0.25 1.99 101 69-137 0.5 20 Bromoform 1.81 0.25 1.99 91 55-132 3 20 Bromomethane 1.48 0.25 1.99 75 10-142 10 20 n-Butylbenzene 2.57 0.25 1.99 129 64-156 0.2 20 sec-Butylbenzene 2.51 0.25 1,99 126 75-155 O.s 20 tert-Butylbenzene 2.34 0.25 1.99 118 74-144 1 20 Carbon tetrachloride 2.12 0.25 1.99 107 67-135 3 20 Chlorobenzene 2.20 0.25 1.99 110 73-134 1 20 Chloroethane 1.75 0.25 1.99 88 10-107 4 20 Chlorofonn 2.10 0.25 1.99 106 69-124 1 20 Chloromethane 2.15 0.25 1.99 108 34-136 8 20 2-Chlorotoluene 2.15 0.25 1.99 108 75-135 0.6 20 4-Chlorotoluene 2.15 0.25 1.99 108 70-138 0.5 20 Dibromochloromethane 1.94 0.25 1.99 98 67-135 2 20 1,2-Dibromo-3-chloropropane 1.89 0.25 1.99 95 41-149 5 20 1,2-Dibromoethane (EDB) 1.96 0.25 1.99 99 68-131 2 20 Dibromomcthanc 1.52 0.25 1.99 76 61-140 3 20 1,2-Dichlorobenzene 2.12 0.25 1.99 107 76-136 2 20 1,3-Dichlorobenzene 2.17 0.25 1.99 109 76-138 (1 20 1,4-Dichlorobenzene 2.21 0.25 1.99 Ill 72-132 3 20 Dichlorodifluorontcthanc 1.31 0.25 1.99 66 10-155 0.2 20 1,1-Dichloroethane 2.30 0.25 1.99 116 63-139 1 20 1,2-Dichloroethane 2.09 0.25 1.99 105 64-126 2 20 1, 1 -Dichloroethene 2.55 0.25 1.99 128 52-167 8 20 cis-1,2-Dichloroethene 2.01 0.25 1.99 101 70-135 3 20 tans-1,2-Dichloroethene 2.37 0.25 1.99 119 67-147 2 20 1.2-Dichloropropane 2.07 0.25 1.99 104 68-131 0.8 20 1,3-Dichloropropane 2.02 0.25 1.99 102 64-128 1 20 2,2-Dichloropropane 2.25 0.25 1.99 113 63-154 3 20 ),I-Dichloropropene 2.20 0.25 1.99 ill 68-138 1 20 cis-1,3-Dichloropropene 2.06 0.25 1.99 103 72-134 2 20 trans-1,3-Dichloropropene 2.25 0.25 1.99 113 69-132 0.8 20 F;thylbenzene 2.47 0.25 1.99 124 68-136 0.2 20 Ilexachlorobutadiene 2.25 0.25 1.99 113 72-198 2 20 4-Isopropyl Toluene 2.42 0.25 1.99 122 74-150 1 20 Isopropylbenzene 2.36 0.25 1.99 119 71-149 2 20 Methylene chloride 2.45 0.25 1.99 123 51-127 5 20 Naphthalene 2.00 0.25 1.99 101 57-158 0.9 20 n-Propylbenzene 2.29 0.25 1.99 115 70-143 0.9 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 28 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Bolt 2646 Project Number: Natural Healing Center 2102742 Orcurt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Compounds by G C/NJS - Qnality Control Analyte Result RL Units Spike Source %REC " 4REC RPD RPD Notes Level Result Limits Limit Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSD1) Analyzed: 05/05/21 12:49 Styrene 2.26 0.25 mg/kg 1.99 114 68-138 0.4 20 1,1,1,2-Tetrachlorocthane 1.96 0.25 1.99 99 76-130 2 20 1,1,2,2-1'ctrachloroethanc 2.08 0.25 1,99 105 60-136 0.2 20 Teirachloroethene (PCE) 2.07 0.25 " 1.99 104 73-138 1 20 Toluene 2.21 0.25 1.99 111 72-128 1 20 1,2,3-Trichlorobenzene 1.87 0.25 1.99 94 61-166 7 20 1,2,4-1'richlorobenzene 1.89 0.25 1.99 95 71-158 2 20 1,1,1-Trichloroethane 2.17 0.25 1.99 109 71-135 3 20 1,1,2-Trichloroethane 2.16 0.25 1.99 108 64-132 4 20 Trichloroethene (TCE) L89 0.25 1.99 95 74-139 1 20 Trichlorofluoromethane 1.59 0.25 1.99 79 30-156 10 20 1,2,3-Trichloropropane 1.90 0.25 1.99 95 67-123 6 20 1,14-Trimethylbenzene 2.60 0.25 1.99 131 68-134 3 20 1,3,5-Trimethy]benzene 2.38 0.25 1.99 120 71-140 0.6 20 Vinyl chloride 2.27 0.25 1.99 114 43-144 8 20 Xylenes (total) 7.47 0.25 5.96 125 69-138 0.9 20 Surrogate: UibroinuJluoromrthan(, 0,0486 0.0497 98 74-122 Surrogate: Toluene-d8 0.0467 0.0497 94 65-128 Serrogate:4-Bromo/luoroben_ene 0.0459 0.0497 92 75-121 Duplicate (B1E0101-DUPl) Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 Benzene ND 1.3 mg/kg ND 20 Bromobenzene ND 1.3 ND 20 Bromochloromcthanc ND 1.3 ND 20 Bromodichloromethane ND 1.3 ND 20 Bromotbrm ND 1.3 " ND 20 Bromomethane ND 1.3 ND 20 n-Butylbenzene ND 1.3 ND 20 sec-Butylbenzene ND 1.3 ND 20 tort-Butylbenzene ND 1.3 ND 20 Carbon tetrachloride ND 1.3 ND 20 Chlorobenzene ND 1.3 ND 20 Chloroethane ND 1.3 ND 20 Chlorofonn ND 1.3 ND 20 Chloromethane ND 1.3 ND 20 2-Chlorotoluene ND 1.3 ND 20 4-Chlorotoluene ND 1.3 ND 20 Dibromochloromethanc ND 1.3 ND 20 1,2-Dibrotno-3-chloropropane ND 1.3 " ND 20 1,2-Dibrontoethane (EDB) ND 1.3 ND 20 Dibromomcthanc ND 1.3 ND 20 1,2-Dichlorobenzene ND 1.3 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: R O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Analyte Result RL Units Spike Source %REC 'oREC RPD RPD Notes F Level Result Limits Limit Batch BlE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Duplicate (B1E0101-DUPI) Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 1,3-Dichlorobenzene ND 1.3 mg/kg ND 20 1,4-Dichlorobenzene ND 1.3 ND 20 Dichlorodifluoromethanc ND 1.3 ND 20 ],I-Dichloroethane NI) 1.3 ND 20 1,2-Dichloroethane ND 1.3 NI) 20 1,1-Dichloroethene ND 1.3 ND 20 cis-1,2-Dichloroethene ND 1.3 ND 20 trans-1,2-Dichloroethene ND 1.3 ND 20 1,2-Dichloropropane ND 1.3 ND 20 1,3-Dichloropropane ND 1.3 ND 20 2,2-Dichloropropane ND 1.3 ND 20 1,1-Dichloropropene ND 1.3 ND 20 cis- I .3-Dichloropropene ND 1.3 ND 20 trans-1,3-Dichloropropene ND 1.3 ND 20 Ethylbenzene ND 1.3 ND 20 Hexachlorobutadiene ND 1.3 ND 20 4-Isopropyl Toluene ND 1.3 ND 20 Isopropylbenzene ND 1.3 ND 20 Methylene chloride ND 1.3 ND 20 Naphthalene ND 1.3 ND 20 n-Propylbenzene NI) 1.3 ND 20 Styrene ND 1.3 NI) 20 1, 1, 1,2-Tetrachloroethane ND 1.3 ND 20 1,1,2,2-Tetrachloroethane ND 1.3 ND 20 Tetrachloroethane (PCE) ND 1.3 ND 20 Toluene 0.572 1.3 ND 20 A-01 1,2,3-Trichlorobenzene ND 1.3 ND 20 1,24-Trichlorobenzene ND 1.3 ND 20 1, 1, 1 -Trichloroethane NI) 1.3 ND 20 1,1,2-Trichloroethane ND 1.3 ND 20 Trichloroethene (TCE) NI) 1.3 ND 20 Trichlorofluoromethane ND 1.3 ND 20 1,2,3-Trichloropropane ND 1.3 ND 20 1,2,4-Trimethylbenzene ND 1.3 NI) 20 1,3,5-Trimethylbenzene ND 1.3 ND 20 Vinyl chloride ND 1.3 ND 20 Xylenes (total) NI) 1.3 ND 20 Surrogate: Dibronu ffituromethane 0.0467 0.0502 93 74-122 Surrogate: Tolnene-d8 0.0475 0.0502 95 65-128 Surrogate: 4-Bromgfhwrohen ene 0.0442 0.0502 88 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 37 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Repotted: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC °aREC RPD RPD Notes Level Result Limits Limit Batch BlEO101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 lliatrix Spike (HICO101-NIS1) Source: 2102742-02 Analyzed:05/05.121 20:08 Benzene 11.1 1.3 tsty'tkg 10.0 ND 111 37-145 Bromobenzene 9.57 1.3 10.0 NI) 96 29-147 Bromochloromethanc 9.29 1.3 10.0 NI) 93 40-145 Bromodichloromethane 10.2 L) 10.0 ND 102 39-153 Bromotorm 9.14 13 10.0 NI) 91 32-143 Bromomethane 12.1 1_3 10'0 ND 121 10-141 n-Butylbenzene 12.3 1.3 10.0 NI) 123 10-16-1 sec-Butylbenzene 12.5 1.3 10.0 ND 125 14-168 tert-Butylbenzene 11.8 1.3 10.0 ND 118 21-159 Carbon tetrachloride 10.4 1.3 10.0 ND 104 28-148 Chlorobenzene 10.6 1.3 10.0 NI) 106 32-148 Chloroethane 11.0 1.3 10.0 ND 110 I1-166 Chloroform 10.3 1.3 10.0 ND 103 40-139 Chloromethane 9.86 1.3 10.0 ND 98 18-135 2-C'hlorotoluene 10.7 1.3 10.0 NI) 107 25-151 4-Chlorotoluene 10.7 1.3 10.0 ND 106 22-150 Dibromochloromethane 9.53 1.3 10.0 ND 95 40-147 1,2-Dibromo-3-chloropropane 9.97 1.3 10.0 NI) 100 25-158 1,2-Dibromoethane (EDB) 9,29 1.3 10.0 NI) 93 38-147 Dibromomcthane 7.54 1.3 10.0 NI) 75 39-150 1,2-Dichlorobenzene 10.6 1.3 10.0 NI) 106 24-154 1,3-Dichlorobc117cnc 10.9 1.3 10.0 ND 108 21-153 1,4-Dichlorobenzene 10.6 1.3 10.0 NI) 106 21-146 Dichloroditluoromcthanc 5.88 1.3 10.0 NI) 59 10-149 L I-Dichloroethane 11.2 1.3 10.0 ND 112 34-151 12-Dichloroethenc 10.1 1.3 10.0 N1) 100 40-137 1,1-Dichloroethene 11.8 1.3 10.0 ND 118 21-172 cis-1.2-Dichloroethene 9.65 1.3 10.0 ND 96 38-147 trans-1,2-Dichloroethene 11.3 1.3 10.0 ND 112 30-100 1,2-Dichloropropane 10.4 1.3 10.0 NI) 104 39-146 1,3-Dichloropropane 10.2 1.3 10.0 ND 102 39-141 2.2-Dichloropropane 9.32 1.3 10.0 ND 93 26-149 1, 1 -Dichloropropene 10.7 1.3 10.0 ND 106 28-150 cis- 1.3-Dichloropropene 9.97 1.3 10.0 NI) 100 34-149 trans- l,3-Dichloropropene 10.7 1.3 10.0 NI) 107 36-143 lithylbenzene 11.5 1.3 10.0 ND 115 23-150 Ilexachlorobutadiene ILL 1.3 10.0 ND 111 10-192 4-Isopropyl Toluene 11.7 1.3 10.0 ND 117 11-165 Isopropylbenzene 11.2 1.3 10.0 NI) 112 17-166 Mohylene chloride 12.0 1.3 10.0 ND 120 28-135 Naphthalene 12.0 1.3 10.0 ND 120 10-174 n-Propylbenzene 11.3 1.3 10.0 NI) 113 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www,oecusa.com FAX: 805 925-3376 Page 31 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Conipounds by GONIS - Quality Control Analyze Result Rl, Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1) Source: 2102742-02 Analyzed: 05/05/21 20:08 Styrene 10.8 1.3 mgrkg 10.0 ND 108 24-154 1, 1, 1,2-Tetrachloroethane 9.48 1.3 10.0 ND 95 38-149 1,1,2,2-1'ctrachloroethanc 11.0 1.3 10.0 ND 110 22-164 Tetrachloroethene(PCE) 9.82 1.3 10.0 ND 98 25-153 Toluene 10.7 1.3 10.0 ND 107 26-149 1,2,3-Trichlorobenzene 10.2 1.3 10.0 ND 101 10-163 1,2,4-Trichlorobenzene 9.97 1.3 10.0 ND 99 10-162 1, 1, 1 -Trichloroethane 10.6 1.3 10.0 ND 106 34-149 1,1.2-Trichloroethane 9.74 1.3 10.0 ND 97 25-175 Trichloroethene (TCE) 9.32 1.3 10.0 ND 93 25-170 Trichlorofluoromethane 10.8 1.3 10.0 ND 107 19-155 1,2,3-Trichloropropane 10.3 1.3 10.0 ND 103 32-165 1,2,4-Trimethylbenzene 12.6 1.3 10.0 ND 126 15-150 1,3.5-Trim ethy]benzene 11.7 1.3 10.0 ND 117 10-158 Vinyl chloride 10.9 1.3 10.0 ND 108 22-148 Xylenes(total) 35.6 1.3 30.1 ND 118 22-153 Surrogate. Dibrvn o luoromethane 0.0473 0.0501 94 74-122 Surrogate: Toluene-d8 0.0469 0.0501 94 65-128 Surrogate:4-Bromn/hrorohenzene 0.0453 0.0501 90 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 37 OEC Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. Protect: Pacific Petroleum Project Number: Natural Healing Center Project Manager: Clarence Reynolds I WO & Reported: 21412742 05/06/2021 17:25 nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OFC, CA -FLAP 8015 Diesel & Motor Oil Fist EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA-ELAP Total Metals by ICP 601013 Total Antimony EPA 6010B Solid OEC, CA-ELAP 601 OB Total Arsenic EPA 601013 Solid OEC. CA -FLAP 6010B Total Barium EPA 601013 Solid OEC, CA-ELAP 6010B Total Beryllium EPA 6010B Solid OEC. CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 601 OB Total Chromium EPA 601013 Solid OEC, CA -FLAP 6010B Total Cobalt EPA 6010B Solid OEC. CA-ELAP 601013 Total Copper EPA 6010B Solid OEC_ CA-ELAP 601013 Total Lead EPA 601 OB Solid OEC. CA-ELAP 601 OB Total Molybdenum EPA 601 OB Solid OEC, CA-ELAP 6010B Total Nickel EPA 6010B Solid OEC, CA -FLAP 6010B Total Selenium EPA 6010B Solid OFC, CA-ELAP 6010B Total Silver EPA 601 OB Solid OEC. CA-ELAP 6010B Total Thallium EPA 6010B Solid OEC. CA-ELAP 6010B Total Vanadium EPA 6010B Solid OEC. CA -FLAP 6010B Total Zinc EPA 601013 Solid OEC, CA-ELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC. CA-ELAP Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid 0EC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OFC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project number: Natural Healing Center 2102742 Orcutt CA., 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Notes and Definitions Qualifier Definition MDl. Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference A-01 Potential carryover from previous high leveled sample. D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC N-03 Analyte concentration above 20x TCLP. QM-()S The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out -Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 34 of 37 File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0511.D Operator BNT Acquired 5 May 2021 12:06 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-01@ Misc Info : 1@B1E0095 GRO SO Vial Number: 11 Response_ GOME0511.D\FID1A 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 Time 0.00 1.00 2.00 3.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0512.D Operator BNT Acquired 5 May 2021 12:32 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-02@ Misc Info : 1@B1E0095 GRO SO Vial Number: 12 GOME0512.D\FID1A 90000 60000 40000j 35000 20000 l . - - . Y,- - r -.. - - - — . t rT-- 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 . -: -= 1 --I. - I • , 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0513.D Operator BNT Acquired 5 May 2021 12:58 pm using AcgMethod GASBTEXE.M Instrument GC7 -• Sample Name: 2102742-03@ Misc Info : 1@B1E0095 GRO SO Vial Number: 13 GOME0513.D\FID1A 75000 70000 -' 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 1 4 1� `. T 7-7j 0.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0514.D Operator BNT Acquired 5 May 2021 1:24 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-04@ Misc Info : 1@B1E0095 GRO SO Vial Number: 14 Response_ 80000- 75000 40000 35000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 G0ME0514.DT1D1A I 4.00 5.00 6.00 7.00 8.00 9.00 M1 �Y• 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0515.D Operator BNT Acquired 5 May 2021 1:49 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-05@ Misc Info : 1@B1E0095 GRO SO Vial Number: 15 Response- GOME0515.D\FID1A 75000 r. 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 15000 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 P � ^^^ �N' A V 1.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 r-I U 0 x a H 0 4 +-) N U C] O� (N U) LO �j X a O N (Q r lD / v O r O N N W to LO r o • • Cq LO I— CJ� O O H / O H H 1 N N N >� 0LO C' /Cn Lr) O X� Ln N H N .. .. .. .. .. .. .. 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N u n n 0 0 0 0 0 0 0 0 0 �f n o n 0 r 0 0 0 0 0 0 0 0 0 0 0 0 0 w t t t t t + O O O O O O O O O C O O O O O O O O LO -t m N r CDO CD 0 N r r r r r m 00 n (00 L M N E r-I U O x a p O a) U Q � • G M U1 N O W � a O N r Cl N ri W LO (n -I O a) (n 6l CJ O O M / O N N N >-I O (n 'r N r--I I` / to Ln C7 0 .. '3 I ri cU lO pa' to N rI M 41 a) C (Ti O Q u '0 a) z w & 1-) �4 a) H (Z •r{ �4 ri ri a) it V) E U) (a •ri 04 U r(d —' •ri rt40 XC hI(n X> 0 co O v O N t1) O O LO O W ei O CO O O N O O. v O M O t0 M O (M C. N M o' 0 ri 0 0 N O (0 N O N O N N O O N O W n n o O o 0 0 0 0 0 0 yF— O O O O O O O 0 O O O O O O O O N + + + + + + + O O O O O O O O O C y (D y N N N N O O O O O 0 O O O O d to of M N O O O O O O O O O 0 CD Vl r- m co O n (0 0 Lo V M N E_ �-I U r-I O x a H zs O �11- U is Ll G OD ill lM Ln O 04 O LO N lO / O - O O Lr) O W Ln ri (?) O N / O O N N ,+ >1 LO �w / to C9 o In c-i (E) OD N M c ro O a �-0 mzw a~ 0 (1) d-) F4 ro •1-i N4 Nb;:1"ro 04 cqb •�-I 04 U G r0 -rl •rl 2 U Q LL 6 CO LO O W 2 O m t6 C _O> �F r � I-- O O O r- ti r- O O O O O O O O O O O O O O O O O O O O O y C t t t t t + O O O O O O O O O O O O O O O O O M CV O O OD O M CD CDN CD m co to o N � CV [i N O V N FN N O O fV N E 1- 2 U Q LL_ 6 O O W O m r1 � U to 0 x a H O a) U U tS C] � O U) Ir Ln O W f�, O 00 N / O r-I O O N � W U O p� LO ri u O N LO / O O 1-1 N I N N >I >,Ln C' / (n C) .. 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C n�U 0o a c o o p E C c Vi Li. 3 Z 0 N x .L+ R 4 e _ m M :37' � sX r t a tn Y coK D a,c - E0 co R M LO p Y L fl -- m a _ t N Cy aY, d E U E lV tnn U F x w c� 1'- ►= -j m V y o n 75 N z J Q U w IL w S. § � § § k � k 000000 f ■■■■O■ t ¢ƒemu - £ co § ® . e = a ° 7 7 ) k 0 L 2 CDK 8 2 ; ) $ 0 o I @ § 2 § � / � < � o k 7 s § ) �) k \ 2 2 _ _ a 0 w 3 § k } IV 2 I) I # Ef {kcc\w¢ k k o o u Q o m d } { \ \ ca - ] f 2 ƒ k < CO < O O L) p -0 Ch r kt § �D CD )$ # _k\ cA CD w Jƒ )) < 0 k ° - % J.,)2 J a. O o c c -0_ 2 m = _ LD & 4 § § a§ 7 t) k p e k § - \ < E 0 E 6 2 3 3 r a® 3 0 CL } r k k\ k c a a >) k% E a s-< °/ 2 _ it = G E k 0 3 0 ) CD _ _ w ) w E \cO// 2 �OOo O k J »■ O O 2 o A 3 y \ t \ � 7 S § E 2 n U N NI 04 N O N N C m E Ll E O m c `o U w a� z m N m a` x v •o v v v v v v v _� o 0 U 0 U o U 0 U 0 U 0 U 0 U 0 U 0 U c c c c c Y Y Y 3 Y 3 Y 3 3 e0 co 00 00 c0 - E Q rn 0 CDrn rn a, rn O v_ v ` v . S LL LL LL LL LL LL U.LL LL LL 0 .Q Q 0 > Q Q Q Q > Q m N O N O N O N O N O c m > _m > m > _m > m > C N E N O E N E N N E N N C E N U � N N� cU O O U Q m N N M m 'V lla LLi m v 'n. 3 d c O O N O U N m > i M O a L a X m r c 0 U m 0 ai a E 0 Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102508 Pacific Petroleum California P. O. Box 2646 Report Date: May 03, 2021 16:36 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 23, 2021 13:40 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin0oect California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 w" W.oecusa.com FAX: (805) 925-3376 Page 1 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Suminary Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bin 2094-A 2102508-01 Solid Solid 04/23/2021 11:00 04/23/2021 13:40 Bin 2094-B 2102508-02 Solid Solid 04/23/2021 11:05 04/23/2021 13:40 Bin 2094-C 2102508-03 Solid Solid 04/23/2021 11:10 04/23/2021 13:40 Bin 20340-A 2102508-04 Solid Solid 04/23/2021 11:15 04/23/2021 13:40 Bin 20340-B 2102508-05 Solid Solid 04/23/2021 11:20 04/23/2021 13:40 Bin 20340-C 2102508-06 Solid Solid 04/23/2021 11:25 04/23/2021 13:40 Bin 20158-A 2102508-07 Solid Solid 04/23/2021 11:30 04/23/2021 13:40 Bin 20158-B 2102508-08 Solid Solid 04/23/2021 11:35 04/23/2021 13:40 Bin 20158-C 2102508-09 Solid Solid 04/23/2021 11:40 04/23/2021 13:40 Bin 2088-A 2102508-10 Solid Solid 04/23/2021 11:45 04/23/2021 13:40 Bin 2088-B 2102508-11 Solid Solid 04/23/2021 11:50 04/23/2021 13:40 Bin 2088-C 2102508-12 Solid Solid 04/23/2021 11:55 04/23/2021 13:40 Bin 20376-A 2102508-13 Solid Solid 04/23/2021 12:00 04/23/2021 13:40 Bin 20376-B 2102508-14 Solid Solid 04/23/2021 12:05 04/23/2021 13:40 Bin 20376-C 2102508-15 Solid Solid 04/23/2021 12:10 04/23/2021 13:40 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 BatchSainple -- Analysis Batch ID Preparation Date/Time *** DEFAULT GENERAL METHOD *** Asbestos Bulk PLM-(non-soil& Asphalt)(sub) OEC Admin Services Chroinatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B ID0766 04/27/2021 07:10 STLC Metals by ICP 6010B STLC B 1 D0916 04/30,,2021 10:33 STLC Metals Extraction STLC Metals Extraction B1D0838 04/28/2021 12:44 TCLP Metals by ICP 601013 WIT B I D0919 04/3012021 10:49 - TCLP Metals Extraction TCLP Metals Extraction B 1D0839 04/28/2021 12:48 Total Metals by CVAA Mercury Total EPA 7471A B1D0711 04/26/2021 09:00 Total Metals by ICP 601013 Total B 1 D0734 04/26/2021 07:37 Volatile Organic Compounds by GUMS 8260B Full List B 1 D0650 04/23/2021 12:1 1 Volatile Organic TPH by GC/FID 8015 TPll-Gasoline B I D0692 04/23/2021 14:16 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by : Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.095 0.094 mg/kg 1 B1D0711 04/26/21 14:53 EPA7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I D0734 04/26/21 13:51 EPA 6010B Arsenic 7.4 1.9 Barium 690 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 64 0.48 N-02 Cobalt 14 0.48 -- • Copper 260 0.97 " " " " " N-02 Lead 2400 0.48 N-01, N-03 Molvbdenum 2.0 0.48 Nickel 94 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 31 1.9 Zinc 1300 1.9 STLC Metals by ICP Chromium 0.28 0.10 mg/L 2 Bl D0916 05/03/21 12:58 STI.C/FPA 6010B Copper 1.6 0.10 TCLP Metals by ICP Lead 2.0 0.050 mg/L 1 B 1 D0919 05/03/21 14:09 EPA 1311 /I?PA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 4 of 94 Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Sample 1D : Sin 2094-A Matrix,- Solid Lab ID: 2102508-01 Analyte Volatile Organic TPH by GC/FID TPH Gasoline (C'5-C 22) Surrogate: 4-B1o17oIluorobetrene Semi -Volatile Organic TPH by GC/FID TPH Diesel tC13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Tetphenrl Oilfield Environmental & Compliance, Inc. Project: Pacific Petroleum Project Number: Natural Healing Cen[er Projec[ Manager: Clarence Reynolds Result Rl- Units Dilution Batch Analyzed ND 4.9 mglkg 1 B I D0692 04/23/2 114:32 94"/„ (39-157) ND 10 mg1kg1 97 50 „ 11 84% (65-136) BID0766 0412712115:24 BYO & Reported: 2! OZ +118 05/03/2021 1616 Sampled : 04/23/21 11:00 Sampled by: Field Data: NA Method Notes EPA 8015M R-07 EPA 8015M The results in this report apply to the samples analyzed in accordance with the chain ofcustody document. This analytical California ELAP Certificate # 2438 re Port m ust be reproduced in 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.comlreports us entirety. TEL: (805) 922-4772 ww["'.oecusa.com FAX; 805 925-3376 Page 5 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.051 mg/kg 1 B1D0050 04/23/21 17:17 EPA8260B Bromobenzene ND 0.051 Bromochloroinethane ND 0.051 Bromodichloromethane ND 0.051 Bromoform ND 0.051 Bromoniethane ND 0.051 n-Butylbenzene ND 0.051 " sec-Butylbenzene ND 0.051 tort-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobcnzenc ND 0.051 Chlorocthanc ND 0.051 Chloroform ND 0.051 Chloromethane ND 0.051 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND 0.051 Dibromochlorontethane ND 0.051 " 12-Dibronio-3-chloropropane ND 0.051 1,2-Dibronioethane (EDB) ND 0.051 Dibromomethane ND 0.051 1,2-Dichlorobenzene ND 0.051 1.3-Dichlorobenzene ND 0.051 1,4-Dichlorobenzene ND 0.051 Dichlorodifluoromcthanc ND 0.051 1,1-Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 ],I-Dichloroethene ND 0.051 cis-1,2-Dichloroethene ND 0.051 " trans-1,2-Dichloroethene ND 0.051 1,2-Dichloropropane ND 0.051 1.3-Dichoropropane ND 0.051 2,2-Dichloropropane ND 0.051 1,1-Dichloropropene ND 0.051 cis-] 3-Dichloropropene ND 0.051 trans- l,3-Dichloropropene ND 0.051 Ethylbcnzcne ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: i 805) 925-3376 Page 6 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID : 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlombutadiene ND 0.051 ing/kg 1 BID0650 04/23/21 17:17 EPA8200B ' 4-Isopropyl Toluene ND 0.051 Isopropylbenzene ND 0.051 Methylene chloride ND 0.051 Naphthalene ND 0.051 n-Propylbenzene ND 0.051 Styrene ND 0.051 1, 1, 1,2-Tetrachloroethane ND 0.051 1.1 .2,2-Tetrachloroethane ND 0.051 Tetrachlorocthenc (PCE) ND 0.051 Toluene ND 0.051 1,2,3-Trichlorobenzenc ND 0.051 1,2,4-Trichlorobenzene ND 0.051 1,1,t-Trichloroethane ND 0.051 1,12-Trichloroethane ND 0.051 Trichloroethene (TCE) ND 0.051 " Trichlorolluoromethane ND 0.051 1.2.3-Trichloropropane ND 0.051 1,24-Trimethylbenzene ND 0.051 1,3.5-Trimethylhenzene ND 0.051 Vinyl chloride ND 0.051 Xylencs (total) ND 0.051 Surrogate: Dihromuilnoromethane 98 % (74 - 122) Surrogate: Toluene-dS 95 % ( 65 - 12S ) " Surrogate: 4-Bronro/1uoroben_eue 89 IN, ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B1D0711 04/26/21 15:02 EPA7471A Total Metals by ICP Antimony ND 2.4 mgIg 1 B 1 D0734 04/26/21 13:54 EPA 6010B Arsenic 7.6 1.9 Barium 220 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 100 0.48 N-02, N-03 Cobalt 15 0.49 Copper 61 0.97 Lead 320 0.48 N-02, N-03 Molvbdenum 1.6 0.48 Nickel 130 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 38 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium 0.29 0.10 mil- 2 B1D0916 05/03/2113:00 STLC/EPA6010B Lead 20 0.10 N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L I B 1 D0919 05/03/21 14:26 EPA 1311 /EPA 6010B Lead 0.31 0.050 " "11" " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: 1871-1i 925-3376 Page 8 of 94 ( A W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GOOD TPH Gasoline (C5-('12) ND 4.8 mg/kg 1 BID0692 04/23/21 14:58 EPA 8015M R-07 Surrogate: 4-Bromo/luorohen::ene 99 N (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 16 10 mg/kg 1 BID0766 04/27/21 15:24 EPA 8015M D-06 TP11 Motor Oil (C23-C40) 150 50 "11 11 11" Surrogate: o-kiphent'l 80 (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 9 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.049 mg/kg 1 B1D0650 04/23/21 17:45 EPA 8260B '^ Broniobenzene ND 0.049 Bromochloromethane ND 0.049 Bromodichloromethane ND 0.049 Bromoform ND 0.049 Bromomethane ND 0.049 n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 " Carbon tetrachloride ND 0.049 Chlorobenzene ND 0.049 Chloroethanc ND 0.049 Chloroform ND 0.049 Chloromethane ND 0.049 " 2-Chlorotoluene ND 0.049 4-C'hlorotoluene ND 0.049 Dibromochloromethane ND 0.049 1.2-Dibromo-3-chloropropane ND 0.049 1,2-Dibrontoethane (EDB) ND 0.049 Dibroinomethane ND 0.049 " 1,2-Dichlorobenzenc ND 0.049 1,3-Dichlorobenzenc ND 0.049 1,4-Dichlorobenzenc ND 0.049 Dichlorodifluoromcthanc ND 0.049 1,1-Dichloroethane ND 0.049 1,2-Dichloroethane ND 0.049 1,1-Dichloroethene ND 0.049 " cis-1,2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 1,2-Dichloropropane ND 0,049 13-Dichloropropane ND 0.049 2,2-Dichloropropane ND 0.049 I,I-Dichloropropene ND 0.049 cis-l3-Dichloropropene ND 0.049 ' trans-1,3-Dichloropropene ND 0.049 Ethylbenzene ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 2094-C Sampled: 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID: 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA NlercurN 0.17 0.098 mg/kg I BID0711 04/26/21 15:04 EPA7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I D0734 04/26/21 14:05 EPA 601 OB --• Arsenic 7.7 2.0 Barium 280 1.0 Beryllium ND 0.50 — Cadmium ND 0.25 Chromium 52 0.50 N-02 Cobalt 10 0.50 Copper 79 1.0 Lead 270 0.50 " " " " " N-02, N-03 Molvbdenum 1.1 0.50 Nickel 69 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 34 2.0 Zinc 370 2.0 " STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 B 1 D0916 05/03/21 13:03 STLC/EPA 601 OB - Lead 22 0.10 " " " N_07 TCLP Metals by ICP Lead 0.11 0.050 mg/L 1 B 1 D0919 05/03/21 14:29 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-C Sampled: 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.8 mg/kg 1 BID0092 04/23/21 15:24 EPA 8015M R-07 Surrogate: 4-Bromo/luorobenzene 93 % (39 - 157) , Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 B1D0766 04/27/21 15:47 EPA 8015M TPH Motor Oil (C23-C40) 220 50 Surrogate: o-Terphe pl 79 % (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.049 mgtkg 1 Bl D0650 04/23/21 18:12 EPA 8260B Bromobenzene ND 0.049 Bromochloromethane ND 0.049 Bro nodichloromethane ND 0.049 Bromofonn ND 0.049 " Bromomethane ND 0.049 " n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 Carbon tetrachloride ND 0.049 Chlorobenzcnc ND 0.049 " Chloroethane ND 0.049 Chloroform ND 0.049 Chloroniethane ND 0.049 2-Chlorotoluene ND 0.049 4-Chlorotoluene ND 0.049 " Dibromochloromethane ND 0.049 _. 1,2-Dibromo-3-chloropropane ND 0.049 12-Dibrontoethane (EDB) ND 0.049 " Dibromomethane ND 0.049 12-Dichlorobenzene ND 0.049 1,3-Dichlorobenzene ND 0.049 1,4-Dichlorobenzenc ND 0.049 Dichloroditluoromcthanc ND 0.049 - l,l-Dichloroethane ND 0.049 1,2-Dichloroethane ND 0.049 1,1-Dichloroethene ND 0.049 cis-1.2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 12-Dichloropropane ND 0.049 " 1,3-Dichloropropane ND 0.049 - , 22-Dichloropropane ND 0.049 1, 1 -Dichloropropene ND 0.049 cis- 1,3-Dichloropropane ND 0.049 trans-1,3-Dichloropropanc ND 0.049 F.thylbenzene ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 14 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID: 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Volatile Organic Compounds by GC/MS (Continued) R-07 llexachlorobutadiene ND 0.049 mg/kg 1 BID0050 04/23/21 18:12 F•PA8260B 4-Isopropyl Toluene ND 0.049 " Isopropylbenzene ND 0.049 Methylene chloride ND 0.049 " — • Naphthalene ND 0.049 n-Propylbenzene ND 0.049 " Styrene ND 0.049 1,1,1,2-1'etracliloroethane ND 0.049 " 1,1.2,2=Cetrachloroethane ND 0.049 Tctrachloroethcnc (PCE) ND 0.049 " Toluene ND 0.049 " 1,2,3-Trichlorobenzenc ND 0.049 " 1,2,4-Trichlorobenzene ND 0.049 " 1,1,1-Trichloroethane ND 0.049 1,1,2-Trichloroethane ND 0.049 " Trichloroethene (TCE) ND 0.049 " Trichlorofluoromethane ND 0.049 " 1,2,3-Trichloropropane ND 0.049 " 1,2.4-Trimethylbenzene ND 0.049 1,3,5-Triniethylbenzene ND 0.049 Vinyl chloride ND 0.049 Xylencs (total) ND 0.049 " Surrogate: Dibronigfluormnethane 97 '% ( 74 122 ) Surrogate. Toluene-d8 96 %", ( 65 128 ) Surrogate: 4-Bromojl11o1ohe71_rne 92 IN ( 75 121) ' The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Drcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples I Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Nlercurc 0.13 0.087 mg/kg 1 BID0711 04/26/21 15:06 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1 D0734 04/26/21 14:07 EPA 6010B Arsenic 7.3 2.0 Barium 230 0.98 " Beryllium ND 0.49 Cadmium ND 0.25 Chromium 58 0.49 " " " " " N-02 Cobalt 12 0.49 Copper 63 0.98 Lead 390 0.49 N-02, N-03 MolOdenum 2.1 0.49 Nickel 69 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 35 2.0 Zinc 530 2.0 " STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 BID0916 05/03/21 13:05 STI.C/EPA6010B — Lead 14 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/l. 1 B1 D0919 05/03/21 14:31 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: i802 925-3376 Page 16 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by : Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C2) ND 5.2 mgtkg 1 BID0692 04/23/21 15:50 EPA 8015M R-07 Surrogate: 4-Brom0/luorohen ene 99 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID -, TPH Diesel (C13-C22) ND 10 mg/kg 1 B1D0766 04/27/21 15:47 EPA 8015M TPH Motor Oil (C23-C40) 170 50 Surrogate: o-Tetphenrl 86'> (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain ofcustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by : Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.051 mg/kg 1 BID0650 04/23/21 18:40 EPA8260B Bmniobenzene ND 0.051 Bromochloromethane ND 0.051 Bromodichloromethane ND 0.051 Brotnoform ND 0.051 Bromomethane ND 0.051 n-Butvibenzene ND 0.051 sec-Butylbenzeue ND 0.051 tert-Butylbenzeue ND 0.051 Carbon tetrachloride ND 0.051 Chlorobcnzcne ND 0.051 Chlorocthanc ND 0.051 " Chloroform ND 0.051 Chloromethane ND 0.051 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND t1.051 Dibromochloromethane ND 0.051 " 1.2-Dibronro-3-chloropropane ND 0.051 1,24Dibromoethane (EDB) ND 0.051 Dibromomethane ND 0.051 12-Diehlorobenzene ND 0.051 - 1,3-Diehlorobenzene ND 0.051 IA-Diehlorobenzene ND 0.051 Dichlorodifluoromethane ND 0.051 " l,l-Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 1,1-Dichloroethene ND 0.051 cis-1,2-Dichloroethene ND 0.051 trans-1,2-Dichloroethene ND 0.051 1,2-Dichloropropane ND 0.051 " 13-Dichloropropane ND 0.051 " 2,2-Dichloropropane ND 0.051 I,I-Diehloropropene ND 0.051 " cis-1.3-Diehloropropene ND 0.051 ' trans-1,3-Diehloropropene ND 0.051 lahylbenzene ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 18 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by : Lab ID: 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.051 mg/kg 1 BID0650 04/23/21 18:40 EPA8260B 4-Isopropyl Toluene ND 0.051 Isopropylbenzene ND 0.051 Methylene chloride ND 0.051 Naphthalene ND 0.051 " n-Propylbenzene ND 0.051 Styrene ND 0.051 1, 1, 1.2-Tetrachloroethane ND 0.051 1.1,2,2-Tetrachloroethane ND 0.051 Tctrachlorocthcnc (PCE) ND 0.051 Toluene ND 0.051 1,2,3-Trichlorobenzene ND 0.051 1,2,4-Trichlorobenzene ND 0.051 1,1,1-Trichloroethane ND 0.051 " 1.1,2-Trichloroethane ND 0.051 Trichloroethene (TICE) ND 0.051 Trichlorofluoromethane ND 0.051 ,. 1.2,3-Trichloropropane ND 0.051 1.2,4-Trimethylbenzene ND 0.051 " 1.3.5-Trimethylbenzene ND 0.051 Vinyl chloride ND 0.051 Xylencs (total) ND 0.051 Surrogate: Uihromglluorontcthane 98 % (74 - 122 ) Surrogate Toluene-d8 97 "/. (65 - 128 ) Surrogate 4-BronutPuboroben-ene 92 5n (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.00cusa.com FAX: 805 925-3376 Page 19 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-B Sampled : 04/23/21 11:20 ' Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Nlercur% 0.095 0.091 mg kg 1 BID0711 04/26/21 15:08 EPA 7471A Total Metals by ICP Antimony ND 2.5 ing/kg 1 BID0734 04/26/2114:10 EPA 6010B Arsenic 10 2.0 Barium 240 0.98 " Bervllium ND 0.49 Cadmium ND 0.25 Chromium 50 0.49 N-02 Cobalt 11 0.49 Copper 54 0.98 Lead 800 0.49 " " " " " N-02, N-03 Molybdenum 0.77 0.49 Nickel 79 0.49 Selenium ND 2.0 Silvcr ND 0.49 Thallium ND 0.98 " Vanadium 37 2.0 Zinc 350 2.0 STLC Metals by ICP Chromium 0.29 0.10 ni./I, 2 B1D0916 05/03/2113:08 STLC/EPA6010B Lead 120 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.23 0.050 mg/L 1 B I D0919 05/03/21 14:34 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 .vvw.oecusa.com FAX: 1805) 925-3376 Page 20 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by : Lab ID: 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mgrkg 1 B1D0092 04/23/21 16:16 EPA 8015M R-07 Surrogate: 4-Bromolluoroben_ene 99 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 37 10 mg/kg 1 BID0766 04/27/21 16:09 EPA 8015M D-06 TPH Motor Oil (C23-C40) 280 50 Surrogutc o-kiphenYl 86 N, (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Saniples Sample ID : Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 0.047 mg!kg I B1D0650 04/23/21 19:07 EPA 8200B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 " Brorrolorm ND 0.047 " Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 C'hlorobenzcne ND 0.047 C:hloroethanc ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 " 4-C'hlorotoluene ND 0.047 " Dibromochlorotnethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 1,2-Dibromocthane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 " 1,4-Dichlorobenzene ND 0.047 Dichloroditluorometbanc ND 0.047 1,1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1, 1 -Dichloroethene ND 0.047 cis- I .2-Dichloroethene ND 0.047 " trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 I.1-Dichloropropaue ND 0.047 cis-1.3-Dichloropropanc ND 0.047 trans-1,3-Dichlompropene ND 0.047 " Etliylbcnzcne ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples 0 Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by : Lab ID: 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 0.047 mg/kg 1 BID0650 04/23/21 19:07 EPA 8260B 4-Isopropyl Toluene ND 0,047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 " 1,1,12-Tetrachloroethane ND 0.047 " 1.1,2,2-Tetrachloroethane ND 0.047 " Tetrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 - 1,2,3-Triehlorobenzenc ND 0.047 1,2,4-Trichi orobenzene ND 0.047 1, 1, 1 -Tricliloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 1,2,3-Trichloropropane ND 0.047 1.2,4-Trimethylbenzene ND 0.047 1,3.5-Trimethylben7ene ND 0.047 Vinyl chloride ND 0.047 Xylcncs (total) NU 0.047 Sunwgute: Dihromolluoronre thane 98 `/ (74 - 122) " Surrogate: Toluene -A 96'% (65 - 128) " Surrogate: 4-Brunw/l:roroheuceue 91 IN (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID: 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 B1D0711 04/26/2115:10 EPA 7471A Total Metals by ICP Antimony ND 2.4 mglkg I B1D0734 04/26/21 14:13 EPA 6010B �. Arsenic 11 2.0 Barium 340 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 50 0.49 N-02 Cobalt 14 0.49 r, Copper 230 0.98 Lead 1200 0.49 N-01, N-03 Nlolvbdennm 1.7 0.49 Nickel 73 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 32 2.0 Zinc 1000 2.0 STLC Metals by ICP Chromium 0.32 0.10 mg/L 2 BID0916 05103'2113:11 STLC/EPA6010B TCLP Metals by ICP Lead 0.84 0.050 mg/l. 1 B 1 D0919 05/03/21 1436 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mg/kg 1 BID0692 04/23/21 16:42 EPA 8015M R-07 Surrogate. 4-BromoJluoroben_ene 96 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 29 10 mg/kg I BID0766 04/27/2116:09 EPA8015M D-06 TPH Motor Oil (C23-C40) 150 50 11 11 11" 11 Surrogate: o-Teiphen l 83 % (65- 136) " 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by : Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.050 mg/kg 1 B1 D0650 04/23/21 19:35 EPA 8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 Bromoform ND 0.050 Bronioniethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0A50 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobenzenc ND 0.050 Chlorocthane ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 4-Chlorotoluene ND 0.050 " Dibromuchloromethane ND 0.050 1.2-Dibromo-3-chloropropane ND 0.050 1,2-Dibromoethane (EDB) ND 0.050 Dibromomethane ND 0.050 1.2-Dichlorobenzene ND 0.050 1.3-Dichlorobenzene ND 0.050 IA-Dichlorobenzene ND 0.050 Dichlorodifluorrmtethanc ND 0.0.50 1,1-Dichloroethene ND 0.050 1,2-Dichloroetliane ND 0.050 1,1-Dichloroethene ND 0.050 cis- 1.2-Dichloroethene ND 0.050 " trans-l.2-Dichloroethene ND 0,050 " 12-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 22-Dichloropropane ND 0.050 1,1-Dichloropropene ND 0.050 cis-1.3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 Fthylbcnzenc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 94 WAL Oilfield Environmental &Compliance, Inc. I(. �i W.� Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20340-C Sampled : 04/23/21 11:25 Matrix: Solid Sampled by Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.050 mg/kg 1 B1D0650 04/23/21 19:35 EPA8260B 4-Isopropyl Toluene ND 0.050 lsopropylbenzene ND 0.050 Methylene chloride ND 0.050 �. Naphthalene ND 0.050 n-Piopylbenzene ND 0.050 Styrene ND 0.050 1,1.1,2-Tetrachloroethane ND 0.050 " 1.1.2,2-Tetrachloroethane ND 0.050 Torachlorocthcne (ICE) ND 0.050 Toluene ND 0.050 1,2,3-Trielilorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1,1,1-Trichloroethane ND 0.050 — 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorolluoromethane ND 0.050 1,2,3-Trichloropropane ND 0.050 1,2,4-Trimethylbenzene ND 0.050 1,3,5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 " Surrogate: Dibromo/luoromethane 98% (74 - 122) " Surrogate: Toluene-dS 95 % ( 65. 128 ) " Surrogate: 4-Bromo/luoroben_ene 90 % (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 27 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID: 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.11 0.092 mg/kg 1 B1 D0711 04/26/21 15:12 EPA 7471 A Total Metals by ICP Antimony 5.9 2.5 mg/kg 1 BID0734 04/26/2114:16 EPA 6010B �• Arsenic 8.5 2.0 " Barium 260 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 65 0.49 N-02 Cobalt 11 0.49 Copper 77 0.98 Lead 530 0.49 " " " " " N-02 N-03 Molybdenum 1.2 0.49 " Nickel 91 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 34 2.0 Zinc 780 2.0 STLC Metals by ICP Chromium 0.59 0.10 mg%L 2 B1 D0916 05/03/21 13:21 STLC/EPA 6010B Lead 17 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.12 0.050 mg/L 1 BID0919 05/03/21 14:39 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by : Lab ID: 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 5.1 ing/kg I BID0692 04/23/21 17:08 EPA 8015M R-07 Surrogate: 4-Bromofluorobenzene 98'%h (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 38 10 mg/kg I BID0766 04/27/21 16:32 EPA 8015M TPH Motor Oil (C23-C40) 150 50 Surrogate: o-Zeiphenyl 86 (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by : Lab ID: 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.045 mgllcg 1 BID0650 04/23/21 20:02 EPA 8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 Bromoform ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 " Chloroethanc ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorololuene ND 0.045 Dibrornochloromethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 1,2-Dibronioethane (ED13) ND 0.045 Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 13-Dichlorobenzene ND 0.045 " IA-Dichlorobenzene ND 0.045 DichlorodiFluoromethane ND 0.045 1, 1 -Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 1,1-Dichloroethene ND 0.045 " cis- 1.2-Diehl oroethene ND 0.045 " trans- l,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 13-Dichloropropane ND 0.045 2,2-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis-1.3-Dichloropropene ND 0.045 trans-1,3-Dichloropropene ND 0.045 Ethylbenzene ND 0.045 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 30 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 " Matrix: Solid Sampled by : Lab ID: 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg/kg 1 BID0650 04/23/21 20:02 EPA 8260B — 4-Isopropyl Toluene ND 0.045 " Isopropylbenzene ND 0.045 " Methylene chloride ND 0.045 " r , Naphthalene ND 0.045 " n-Propylbenzene ND 0.045 " Styrene ND 0.045 " 1, 1, 1.2-Tetrachloroethane ND 0.045 " I.I.2,2-Tetrachloroethane ND 0.045 " Tetrachloroethane (PC E) ND 0.045 " Toluene ND 0.045 ' 1,2,3-Trichlorobenzcne ND 0.045 1,2,4-Trichlorobenzene ND 0.045 " 1,1,1-Trichloroethane ND 0.045 " 1,1,2-Tricliloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 " Trichlorolluoromethane ND 0.045 1,2,3-Trichloropropane ND 0.045 " 1,24-Trimethylbenzene ND 0.045 " 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 " - Xylencs (total) ND 0.045 " Surrogate: Dihrouwfluor<nnethane 96 %, (74 - 122) " Surrogate" Toluene-d8 97 "4, (65 - 128) Surrogate: 4-BrnmoJluorohen-ene 93 % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.12 0.090 mg!kg 1 Bl D0711 04/26/21 15:14 EPA 7471 A Total Metals by ICP Antinionv ND 2.5 mg/kg 1 BID0734 04/26/21 14:19 EPA 6010B Arsenic 6.5 2.0 " Barium 270 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 86 0.49 N-02 Cobalt 25 0.49 Copper 60 0.99 Lead 190 0.49 N-02, N-03 Molybdenum 1.0 0.49 " Nickel 170 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 35 2.0 "Zinc 380 2.0 STLC Metals by ICP Chromium 0.34 0.10 mg/l. 2 B I D0916 05/03/21 13:23 STLC/FPA 6010B Lead 13 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.29 0.050 mg/L 1 B 1 D0919 05/03/21 14:41 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 32 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples i Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by : Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-02) ND 5.0 mg/kg I BID0692 04/23/21 17:34 EPA 8015M R-07 Surrogate: 4-BromgJluorohen_ene 89 IN (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 93 40 mg/kg 4 B 1 D0766 04/28/21 15:31 EPA 8015M D-06 TPH Motor Oil (C23-C40) 320 200 11 11 11" 11 Surrogate: o-k1phenYl 84 (65- 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 o f 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by : Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.047 mglkg I B1D0650 04/23/21 20:30 EPA 8260B ^ Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromoform ND 0.047 " Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzcnc ND 0.047 Chlorocthanc ND 0.047 Chlorofonn ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 12-Dibromo-3-chloropropane ND 0.047 1,2-Dibromoethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 1,4-Dichlorobenzene ND 0.047 Dichlorodifluoromcilhane ND 0.047 y I,1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 - cis- 1,2-Dichloroethene ND 0.047 trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1,1-Dichloropropene ND 0.047 cis-1.3-Dichloropropene ND 0.047 trans-1,3-Dichloropropene ND 0.047 Ethylbcnzene ND 0.047 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: [805) 925-3376 Page 34 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.047 mg/kg 1 Bl D0650 04/23/21 20:30 EPA 8200B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1, 1, 1,2-Tetrachloroethane ND 0.047 " I.1.2.2-Tetrachloroethane ND 0.047 " Tetrachlorocthcne WE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzene ND 0.047 1,2,4-Trichlorobenzene ND 0.047 1,1,1-Trichloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 " Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 1.2.3-Trichloropropane ND 0.047 1,24-TrimethAbenzene ND 0.047 1,3,5-Trinrethylbenzenc ND 0.047 Vinyl chloride ND 0.047 Xylencs (total) ND 0.047 Surrogate: Dihrolnolluoromethanc 95 174- 122) " Surrogate: Toluene-dS 96 % ( 65 - 12,4) " Surrogate: 4-Bromo/htoroheu:ene 871b (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by : Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mgfkg 1 BID0711 04/26/2115:16 EPA 7471A Total Metals by ICP Antimony 38 2.5 mg/kg I B I D0734 04/26/21 14:22 EPA 601 OB Arsenic 13 2.0 Barium 610 0.99 Beryllium ND 0.49 r' Cadmium ND 0.25 Chromium 63 0.49 N-02 Cobalt 19 0.49 Copper 78 0.99 Lead 8000 49 100 04/26/2114:50 N-01, N-03 Molybdenum 1.8 0.49 l 04/26/21 14:22 " Nickel 110 0.49 Selenium ND 2.0 Silver ND 0.49 "—' Thallium ND 0.99 Vanadium 39 2.0 Zinc 2100 2.0 STLC Metals by ICP Chromium 0.27 0.10 m,/L 2 B 1 D0916 05 /03/21 13:26 STLC/EPA 601 OB TCLP Metals by ICP Lead 0.054 0.050 mg/L 1 B 1 D0919 05/03/21 14:44 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 94 C A 6m: Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report foi- Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by : Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mgukg 1 B1D0692 04/23/21 18:00 EPA 9015M R-07 Surrogate: 4-BromoJluorobenrene 97 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 39 10 mg/kg 1 BID0766 04/27/21 16:32 EPA8015M D-06 TPH Motor Oil (C23-C40) 110 50 1. 11 11" 11 Surrogate: o-Tetphemd 75 % (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 37 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.052 mgikg 1 B1 D0650 04/23/21 23:41 EPA 8260B Bromobenzene ND 0.052 Bromochloromethane ND 0.052 Bromodichloromethane ND 0.052 Bromofonn ND 0.052 Bromomethane ND 0.052 n-Butylbenzene ND 0.052 " sec-Butylbenzene ND 0.052 tert-Butylbenzene ND 0.052 Carbon tetrachloride ND 0.052 Chlorobenzenc ND 0.052 Chloroethanc ND 0.052 Chloroform ND 0.052 Chloromethane ND 0.052 2-Chlorotoluene ND 0.052 " 4-C.'hlorotoluene ND 0.052 " Dibromochloromethane ND 0.052 1,2-Dibromo-3-chloropropane ND 0.052 1,2-Dibromoethane (P.DB) ND 0.052 Dibromomethane ND 0.052 1,2-Dichlorobenzene ND 0.052 13-Dichlorobenzene ND 0.052 1,4-Dichlorobenzene ND 0.052 Dichloroditluoromethane ND 0.052 I,I-Dichloroethane ND 0.052 1,2-Dichloroethane ND 0.052 1, 1 -Dichloroethene ND 0.052 cis-I,2-Dichloroethene ND 0,052 trans-1,2-Dichloroethene ND 0.052 12-Dichloropropane ND 0.052 1,3-Dichloropropane ND 0.052 2.2-Dichloropropane ND 0.052 1,1-Dichloropropane ND 0.052 cis-1,3-Dichloropropanc ND 0.052 trans-1,3-Dichloropropcnc ND 0.052 Ethylbcnzcne ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria. CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by : Lab ID: 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.052 mgtkg 1 BID0650 04/23/2123:41 EPA8260B 4-Isopropyl Toluene ND 0.052 lsopropylbenzene ND 0.052 Methylene chloride ND 0.052 Naphthalene ND 0.052 " n-Propylbenzene ND 0.052 Styrene ND 0.052 L1,1,2-Tetrachloroethane ND 0.052 1.1,22-Tetrachloroethane ND 0.052 Tctrachloroethcne (PCE) ND 0.052 Toluene ND 0.052 1,2,3-Trichlorobenzene ND 0.052 1,24-Trichlorobenzene ND 0.052 1,1,1-Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 Triehloroethene (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 1.2,3-Trichloropropane ND 0.052 12,4-Trimethylbenzene ND 0.052 " 13,5-Trimethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylcnes (total) ND 0.052 Surrogate: Dihronuolluoromethane 971% 174 - 122 ) Surrogate: Toluene-d8 97' (65 - 128 ) Surrogate: 4-Brvnmlluoruheur_ene 91 % (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.19 0.088 mg/kg 1 BID0711 04/26/21 15:18 EPA 7471A Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt ._ Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc STLC Metals by ICP Lead TCLP Metals by ICP Lead ND 2.5 mg/kg 1 B I D0734 04/26/21 14:25 EPA 6010B 9.0 2.0 380 1.0 ND 0.50 1.3 0.25 44 0.50 13 0.50 36 1.0 360 0.50 0.73 0.50 71 0.50 ND 2.0 ND 0.50 ND 1.0 35 2.0 780 2.0 N-02, N-03 12 0.10 me/L 2 B 1 D0916 05/03/21 13:28 STLC/EPA 6010B N-117 0.092 0.050 mg/L 1 BI D0919 05/03/21 14:46 EPA 1311 /I PA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 2088-A Sampled: 04/23/21 11:45 " Matrix: Solid Sampled by: Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 4.6 mg/kg 1 B1D0692 04/23/21 18:26 EPA 8015M R-07 Surrogate: 4-Bromu/laorobenzene 98 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 21 10 nig/kg 1 BID0766 04/27/21 16:54 EPA 8015M D-06 TPII Motor Oil (C23-C40) 140 50 11 11 11 11° Surrogate: o-kiphenrl 80 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805 9) 25-3376 Page 41 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled : 04/23/21 11:45 Matrix: Solid Sampled by : Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.052 mg/kg 1 BID0650 04/24/21 00:08 EPA 8260B Bromobenzene ND 0.052 Bromochloromethane ND 0.052 Brarnodichloromethane ND 0.052 Bromofonn ND 0.052 Bromomethane ND 0.052 n-Butylbenzene ND 0.052 sec-Butylbenzene ND 0.052 tert-Butylbenzene ND 0.052 Carbon tetrachloride ND 0.052 " Chlorobenzene ND 0.052 " Chlorocthanc ND 0.052 Chloroform ND 0.052 Chloromethane ND 0.052 2-Chlorotoluene ND 0.052 4-Chlorotoluene ND 0.052 Dibromochloromethane ND 0.052 1,2-Dibromo-3-chloropropane ND 0.052 1,2-Dibromoethane (EDB) ND 0.052 " Dibromomethane ND 0.052 1.2-Dichlorobenzene ND 0.052 " 1,3-Dichlorobcnzene ND 0.052 1,4-Dichlorobcnzenc ND 0.052 Dichlorodifluoromethane ND 0.052 I,I-Dichloroethane ND 0.052 1,2-Dichloroethane ND 0.052 1, 1 -Dichloroethene ND 0.052 cis -L2-Dichloroethene ND 0.052 trans-1,2-Dichloroethene ND 0.052 1,2-Dichloropropane ND 0.052 1,3-Dichloropropane ND 0.052 2,2-Dichloropropane ND 0.052 " 1,1-Dichloropropane ND 0.052 cis-1.3-Dichloropropenc ND 0.052 trans-1,3-Dichloropropenc ND 0.052 Ethylbenzene ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of eustodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 94 WAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2088-A Sampled : 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID : 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 flexachlorobutadiene ND 0.052 mgtkg 1 BID0650 04/24/2100:08 EPA8260B 4-Isopropyl Toluene ND 0.052 Isopropylbenzene ND 0.052 Methylene chloride ND 0.052 " Naphthalene ND 0.052 " n-Propylbenzene ND 0.052 Styrene ND 0.052 1. 1, 1,2-Tetrachloroethane ND 0.052 .— 1,1,2.2-Tetrachloroethane ND 0.052 Tctrachlorocthcnc (PCE) ND 0.052 Toluene ND 0.052 1,2.3-Trichlorobenzene ND 0.052 1,2.4-Trichlorobenzene ND 0.052 1, 1, 1 -Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 Trichloroethene (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 " 1,2.3-Trichloropropane ND 0.052 1,2,4-Triniethylbenzene ND 0.052 1.3,5-Trimethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylenes (total) ND 0.052 " Surrogate: Dihromghuoromethane 97 ` o (74 - 122) Surrogate: Toluene-d8 96(65 - L8) Surrogate: 4-BronwJluoroben-ene 90 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.11 0.099 mg/kg 1 BID0711 04/26/21 15:20 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:28 EPA 6010B Arsenic 15 2.0 Barium 270 0.98 Beryllium ND 0.49 Cadmium 1.4 0.25 Chromium 130 0.49 N-02, N-03 Cobalt 16 0.49 Copper 68 0.98 Lead 440 0.49 " " " " N-02, N-03 - , 111olvbdenum 1.2 0.49 " Nickel 120 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 38 2.0 Zinc 1400 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/L 2 BID0916 05/03/21 13:31 STLC/EPA6010B Lead 14 0.10 " " " " " N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BID0919 05/03/2114:49 EPA 1311/EPA6010B Lead 0.27 0.050 " " " " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 44 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by : Lab ID : 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.6 mgfkg 1 BID0692 04/23/21 20:35 EPA 8015M R-07 r Surrogate: 4-Bromofrorohen:ene 97 "/., (39 - 157) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 17 10 mg/kg 1 BID0766 04/27/21 16:54 EPA 8015M D-06 TPH Motor Oil (C23-C40) 87 50 Surrogate: o-TeiphenYl 74 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 8051 925-3376 Page 45 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples I Sample ID : Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mg/kg 1 BID0650 04/24/21 00:35 EPA 8260B Brotnobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 Bronrofortn ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbeuzene ND 0.045 tort-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobcnzenc ND 0,045 Chlorocthanc ND 0.045 Chlorotbrm ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 " 1,2-Dibromo-3-chloropropane ND 0.045 " 1,2-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 " 1,2-Dichlorobenzene ND 0.045 " 1.3-Dichloroben7ene ND 0.045 1,4-Dichlorobenzene ND 0.045 " Dichlorodifluoromethane ND 0.045 1, 1 -Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 LI-Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 " trans-1,2-Dichloroethene ND 0.045 " 12-Dichloropropane ND 0.045 13-Dichloropropane ND 0.045 22-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis- 1.3-Dicliloropropenc ND 0.045 " trans-1,3-Dichloropropene ND 0.045 Ethylbenzenc ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 46 of 94 IrO-E-qC Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report foi- Samples Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID : 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 llexachlorobutadiene ND 0.045 mg/kg 1 BID0650 04/24/2100:35 EPA8200B 4-tsopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 " Naphthalene ND 0.045 n-Propylbenzene ND 0.045 Styrene ND 0.045 1.1.1,2-Tetrachloroethane ND 0.045 1,1,2.2-Tetrachloroethane ND 0.045 Tctrachlorocthcnc (PCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1,1,1-Trichlomethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0,045 Trichlorofluoromethane ND 0.045 1,2,3-Trichloropropane ND 0.045 1,2,4-Triniethylbenzene ND 0.045 " 1,3,5-Trnuethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: Uihromulluorumrthane 97' ; (74 - 122 ) Surrogate: Toluene-dg 95 / (65 - 128 ) Surrogate: 90 "/o ( 75. 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.096 mg/kg 1 B1 D0711 04/26/21 15:30 EPA 7471 A Antimony ND 2.5 mg/kg 1 BID0734 04/26/21 14:31 EPA 6010B Arsenic 13 2.0 " Barium 300 0.99 Beryllium ND 0.49 Cadmium 19 0.25 N-02 Chromium 56 0.49 N-02 Cobalt 17 0.49 Copper 1100 0.99 " " " " " N-02 Lead 390 0.49 " " " " N-02, N-03 Molvbdenum 1.1 0.49 Nickel 100 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 34 2.0 Zinc 660 2.0 STLC Metals by ICP Cadmium 0.088 0.050 mg/L 2 BID0916 05/03/2113:34 STI.C/EPA6010B Chromium 0.24 ().10 11" " " 11 Copper 0.69 0.10 Lead 10 0.10 " " " " " N-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8051 925-3376 Page 48 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes TCLP Metals by ICP Lead 0.085 0.050 mg/1- 1 B1D0919 05/03/21 14:59 EPA 1311 /EPA 601013 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: 4-81-omo/luo1-oben:7ene Semi -Volatile Organic TPH by GC/FID TPA Diesel (03-C22) TPH Motor Oil (C23-C40) Sun•ogate: o-Tecphen l ND 4.8 mg/kg 1 B I D0692 04/23/21 21:01 EPA 8015M R-07 96%, (39-157) 11" 20 10 mg/kg 1 B 1 D0766 04/27/21 17:17 EPA 8015M D-06 130 50 78% (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 49 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Sampled by : Matrix: Solid Field Data: NA Lab ID: 2102508-12 -Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.045 mglkg I BID0650 04/2412101:02 EPA8260B Bromobenzene ND 0.045 Bromocliloromethane ND 0.045 Bromodichloromethane ND 0.045 " Bromoform ND 0.045 " Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 " Chlorobenzenc ND 0.045 Chloroethane ND 0.045 " Chloroform ND 0.045 Chlommethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 " 1.2-Dibronio-3-chloropropane ND 0.045 " 1,2-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 1,2-Diclilorobenzene ND 0.045 I.3-Dichlorobcnzcnc ND 0.045 1,4-Dichlorobcnzcnc ND 0.045 Dichlorodithtoromethanc ND 0.045 1,1-Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 1, 1 -Dichloroethene ND 0.045 cis-1,2-Dichloroethene NO 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1,3-Dichloropropane ND 0.045 2,2-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis-1,3-Dichloropropcnc ND 0.045 trans-1,3-Dichloropropcnc ND 0.045 Ethylbenzene ND 0.045 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by: Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg/kg 1 B 1 D0650 04/24/21 01:02 EPA 8260B 4-Isopropyl Toluene ND 0.045 Isopropylbeuzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 " n-Propylbenzene ND 0.045 Styrene ND 0.045 1,1.1.2-Tetrachloroethane ND 0.045 1,1,2,2-Tetrachloroetliane ND 0.045 1'etrachloroethcne (PCE) ND 0.045 Toluene ND 0.045 1,2,3-Trichlorobenzcne ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1, 1, 1 -Trichloroethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 " Trichlorotluoromethane ND 0,045 " 1,2.3-Trichloropropane ND 0.045 1,24-Trimethylbenzene ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylcnes (total) ND 0.045 Surrogate: Dibromgfluoromethane 95 ' (74 - 122) " Surrogate: Toluene-d8 98 3,, (65- 128) " Surrogate: 4-Bromoflaorohen_enc 88 Y. (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report t Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 BID0711 04/26/21 15:32 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/21 14:41 EPA 6010B Arsenic 7.0 2.0 " Barium 360 1.0 " Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium 48 0.50 " Cobalt 10 0.50 " Copper 620 1.0 N-02 Lead 940 0.50 N-02, N-0 3 Molybdenum 1.4 0.50 " Nickel 66 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 " Vanadium 34 2.0 " Zinc 610 2.0 " STLC Metals by ICP Copper 2.4 0.10 mg/L 2 BID0916 05/03/2113:36 STLC/EPA6010B Lead 51 0.10 N-07 TCLP Metals by ICP Lead 4.7 0.050 mgil- 1 B l D0919 05/03/21 15:01 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 52 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 5.2 mg1g l BID0692 04/23/21 21:27 EPA 8015M R-07 ^ Surrogate: 4-BromgJluorobenzene 92 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 12 10 mg/kg 1 BID0766 04/27/21 17:17 EPA 8015M D-06 TPH Motor Oil (C23-C40) 67 50 Surrogate: o-kiphen l 73 X (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria. CA 93454 www.oecusa.com FAX: (805) 925-3376 r raw Page 53 of 94 C A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.050 mg/kg 1 BID0li50 04/24/21 01:29 EPA 8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 " Bromodichloromethane ND 0.050 -. Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 " sec-Butylbenzene r ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobenzene ND 0.050 " 7 Chlorocthane ND 0.050 Chloroform ND 0.050 " Chloromethane ND 0.050 " 2-Chlorotoluene ND 0.050 " 4-Chlorotoluene ND 0.050 Dibromochloromethane ND 0.050 " . 1,2-Dibronu>-3-chloropropane ND 0.050 " 12-Dibromoethane (EDB) ND 0.050 " Dibromomethane ND 0.050 1,2-Dichlorobenzene NO, 0.050 " O-Dichlorobenzenc ND 0.050 14-Dichlorobenzenc ND 0.050 " Dichlorodilluoromethane ND 0.050 1,1-Dichloroethane ND 0.050 " 1,2-Dichloroethane ND 0.050 " 1,1-Dichloroethene ND 0.050 " cis-1.2-Dichloroethene ND 0.050 mans-1,2-Dichloroethene ND 0.050 " 12-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 2,2-Dichloropropane ND 0.050 " 1,1-Dichloropropene ND 0.050 cis- 1.3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 Fthylbenzene ND 0.050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 54 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID: 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 0.050 mg/kg 1 BID0650 04/24/21 01:29 EPA 8260B —' 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 " —. Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1, 1, 1,2-Tetrachloroethane ND 0.050 1,1.2,2-Tetrachloroethane ND 0.050 Tetrachloroethane (PCE) ND 0.050 Toluene ND 0.050 1,2,3-Trichlorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorofluoromethanc ND 0,050 " _ 1,2,3-Trichloropropane ND 0.050 1,2,4-Trimethylbenzene ND 0.050 1,3,5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: I)ibromglhmromcthmze 96 % (74 - 122 ) Surrogate: Toluene-dS 96 (65 - 128 ) Surrogate: 4-&vmol7uoroben_ene 69 %, ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805' 925-3376 Page 55 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID : Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.20 0.097 mg/kg 1 B 1 D0711 04/26/21 15:34 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B ID0734 04/26/21 14:44 EPA 6010B Arsenic 6.7 2.0 Barium 440 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 73 0.50 N-02 Cobalt 9.4 0.50 Copper 57 0.99 Lead 2000 0.50 N-01 N-03 Nlolvbdenum 2.5 0.50 Nickel 68 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 30 2.0 Zinc 770 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/L 2 B 1 D0916 05/03/21 13:39 STLC/EPA 6010B TCLP Metals by ICP Lead 0.99 0.050 mg/L 1 BID0919 05/03/21 15:04 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 56 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report -- Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 5.1 mg, kg 1 Bl D0692 04/23/21 21:53 EPA 8015M R-07 Surrogate: 4-Bromo/luorohenzene 96 "/r, (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mg/kg 1 B1D0766 04/28/21 15:08 EPA 8015M TPH Motor Oil (C23-C40) 64 50 11 11 11 11 1. Surrogate: o-Teiphen.vl 79 /n (65 - 136) " --I The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 57 of 94 r A 61rcra Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by : Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg. kg 1 BI D0650 04/24/21 01:57 EPA 8260B -' Bromobenzene ND 0.047 " Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromofonn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 .- tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobcnzene ND 0.047 Chlorocthanc ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 -- 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 1,2-Dibronnoethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzcne ND 0.047 1,3-Dichlorobenzcnc NI) 0.047 1,4-Dichlorobenzcnc ND 0.047 Dichlorodifluoromethane ND 0.047 I,l-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 cis-1.2-Dichloroethene ND 0.047 " trans-1,2-Dichloroethene ND 0.047 " 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 " 2.2-Dichloropropane ND 0.047 1. 1 -Dichloropropene ND 0.047 cis-1.3-Dichloropropanc ND 0.047 trans-O-Dichloropropane ND 0.047 Ethylbcnzene ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 58 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by : Lab ID: 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 11 exach I orobutadi en e ND 0.047 mg/kg 1 BID0650 04/24/21 01:57 EPA 8260B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 " Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1,1,1,2-1-etrachloroethane ND 0.047 1,1,2,2-Tetrachloroethane ND 0.047 Tetrachlorocthanc (PCE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzcnc ND 0.047 1,2,4-Trichlorobenzene ND 0.047 1,1,1-Trichloroethane ND 0.047 1.1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 1,2.3-Trichloropropane ND 0.047 L2.4-Trimethylbenzene ND 0.047 1,3,5-Triniethylbenzene ND 0.047 Vinyl chloride ND 0.047 " Xylcncs (total) NU 0.047 Surrogate: Dibromolluoromethane 97'N (74- 122) " Surrogate: Toluene-dS 96 % (65 - 128) " Surrogate: 4-Broinof toroben_ene 91 % (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 59 of 94 fA A MW Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 - ' Matrix: Solid Sampled by: Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg I B 1 D0711 04/26/21 15:36 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 Bl D0734 04/26/21 14:47 EPA 6010B Arsenic 5.6 1.9 " Barium 320 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 49 0.49 Cobalt 10 0.48 ^ Copper 41 0.97 Lead 440 0.48 " " " " N-02, N-03 Dlolvbdenum 0.80 0.48 Nickel 68 0.48 Selenium ND 1.9 Silver ND 0.48 ' Thallium ND 0.97 Vanadium 38 1.9 Zinc 580 1.9 STLC Metals by ICP Lead 40 0.10 mg/L 2 BID0916 05/03/21 13:41 STLC/EPA6010B N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/1- 1 B1D0919 05/03/21 15:06 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 - Matrix: Solid Sampled by : Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.6 mg/kg I BID0692 04/23/21 22:18 EPA 8015M R-07 Surrogate: 4-Bmmo/luorohenzene 94 `% (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 140 20 mg/kg 2 B1D0766 04/28/21 16:38 EPA 8015M D-06 TPH Motor Oil (C23-C40) 360 100 Surrogate: o-Tegphen l 120 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 61 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg/kg 1 B1D0650 04/24/2102:24 EPA8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 " Bromotorm ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 " tent-Butylbenzene ND 0.047 " Carbon tetrachloride ND 0.047 Chlorobenzenc ND 0.047 Chloroethanc ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 1,2-Dibrontoethane (ED13) ND 0.047 Dibroutomethane ND 0.047 1.2-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 " 14-Dichlorobenzenc ND 0.047 Dichloroditluoromethane ND 0.047 1,1-Dichloroethane ND 0.047 12-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 cis- 1.2-Dichloroethene ND 0.047 " trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 2.2-Dichloropropane ND 0.047 1.1-Dichloropropane ND 0.047 cis- 1.3-Dichloropropenc ND 0.047 trans-1,3-Dichloropropcnc ND 0.047 Ethylbcnzenc ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 62 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlombutadiene ND 0.047 ing/kg 1 B1D0650 04/24/2102:24 EPA9260B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 " Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1,1.1,2-Tetrachloroethane ND 0.047 1,1.2.2-Tetrachloroethane ND 0.047 Tetrachloroctlicne (PCE) ND 0.047 " Toluene ND 0.047 " 1,2,3-Triclilorobenzene ND 0.047 1,2,4-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 " 1,2.3-Trichloropropane ND 0.047 1,2,4-1'rimethylbenzene ND 0.047 13.5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 Xylcnes (total) ND 0.047 Surrogate: Dibromolhroromethane 95 44, ( 74- 122) Surrogate: Toluene-dg 97 % ( 65 - 128) " Surrogate: 4-Bromolhioroben_ene 92 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacLisa.com FAX: 805) 925-3376 Page 63 q f 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 1636 Total Metals by CVAA - Quality Control IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes —1 Level Result Limits Limit J Batch BlD0711 -EPA 7471A Preparation: EPA 7471A Pre1 Blank (B1D0711-BLK1) Mercury ND LCS (BlD0711-BSI) Mercury 0.803 LCS Dup (BlD0711-BSD1) Mercury 0.765 Duplicate (BlD0711-DUPl) Source: 2102489-02 Mercury 0.0432 Matrix Spike (B1D0711-MS1) Source: 2102489-02 Mercury 0.943 Matrix Spike Dup (BlD0711-MSDI) Source: 2102489-02 Mercury 0.673 Post Spike (B1D0711-PS1) Source: 2102489-02 Mercury 5.23 04/26/21 09:00 Analyzed: 04/26/21 14:37 0.10 mg/kg Analyzed: 04/26/21 14:31 0.10 mg!kg 0.833 Analyzed: 04/26/21 14:33 0.10 mg/kg 0.833 Analyzed: 04/26/21 14:45 0.099 mg/kg 0.0418 Analyzed: 04/26/21 14:47 0.090 mg/kg 0.746 0.0418 Analyzed: 04/26/21 14:49 0.087 mg/kg 0.723 0.0418 Analyzed: 04/26/21 14:51 ug/I. 5.00 0.273 96 85-115 92 85-115 5 20 3 20 107 75-125 87 75-125 22 20 QR-02 99 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 64 of 94 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes --• Level Result Limits Limit Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Blank (B1D0734-BLK1) Analyzed: 04/26/21 13:29 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 " "-' Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " - - Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 " LCS (BlD0734-BS1) Analyzed: 04/26/21 13:04 Antimony 97.0 2.5 mg/kg 100 97 80-120 Arsenic 100 2.0 100 100 80-120 Barium 93.5 1.0 100 94 80-120 Beryllium 99.0 0.50 100 99 80-120 Cadmium 99.2 0.25 100 99 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 100 0.50 100 100 80-120 Copper 104 1.0 100 104 80-120 Lead 99.4 0.50 100 99 80-120 Molybdenum 98.4 0.50 100 99 80-120 Nickel 102 0.50 100 102 80-120 Selenium 101 2.0 100 101 80-120 Silver 5.04 0.50 5.00 101 80-120 Thallium 108 1.0 100 108 80-120 Vanadium 99.8 2.0 100 100 80-120 Zinc 97.0 2.0 100 97 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 65 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 - LCS Dup (BlD0734-BSDI) Analyzed: 04/26/21 13:06 Antimony 97.8 2.5 mg/kg 100 98 80-120 0.8 20 Arsenic 101 2.0 100 101 80-120 0.7 20 Barium 93.6 1.0 100 94 80-120 0.2 20 Beryllium 98.6 0.50 100 99 80-120 0.4 20 Cadmium 99.5 0.25 100 100 80-120 0.3 20 Chromium 103 0.50 100 103 80-120 0.9 20 Cobalt 101 0.50 100 101 80-120 0.3 20 Copper 104 1.0 100 104 80-120 0.9 20 Lead 99.8 0.50 100 100 80-120 0.3 20 Molybdenum 99.4 0.50 100 99 80-120 0.9 20 Nickel 102 0.50 100 102 80-120 0.4 20 Selenium 101 2.0 100 101 80-120 0.1 20 Silver 5.04 0.50 5.00 101 80-120 0.1 20 Thallium 108 1.0 100 108 80-120 0.5 20 Vanadium 100 2.0 100 100 80-120 0.4 20 Zinc 97.4 2.0 100 97 80-120 0.4 20 Duplicate (BlD0734-DUPI) Source: 2102489-01 Analyzed: 04/26/21 13:35 - Antimony ND 2.5 mg/kg ND 20 Arsenic 5.86 2.0 6.40 9 20 Barium 87.5 0.99 72.5 19 20 Beryllium 0.369 0.49 0.419 12 20 Cadmium ND 0.25 ND 20 Chromium 20.3 0.49 22.2 9 20 Cobalt 6.53 0.49 6.95 6 20 Copper 18.4 0.99 21.5 16 20 Lcad 5.52 0.49 6.10 10 20 Molybdenum 1.50 0.49 2.18 37 20 (1P..-t;�l Nickel 25.9 0.49 30.4 16 20 Selenium ND 2.0 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.99 ND 20 - Vanadium 18.9 2.0 20.6 9 20 Zinc 49.7 2.0 53.8 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 11805 925-3376 Page 66 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 tControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 �. Matrix Spike (BlD0734-MSI) Source: 2102489-01 Analyzed: 04/26/21 13:08 Antimony 30.5 2.5 mg/kg 98.3 ND 31 10-116 Arsenic 102 2.0 98.3 6.40 97 77-121 Barium 159 0.98 98.3 72.5 88 30-169 Beryllium 93.2 0.49 99.3 0.419 94 86-111 Cadmium 90.1 0.25 98.3 ND 92 81-112 Chromium 124 0.49 98.3 22.2 103 75-129 Cobalt 95.3 0.49 98.3 6.95 93 71-121 - Copper 123 0.98 98.3 21.5 103 68-135 Lead 95.5 0.49 98.3 6.10 91 72-121 Molybdenum 87.8 0.49 99.3 2.18 97 70-112 - Nickel 122 0.49 98.3 30.4 93 73-121 Selenium 91.6 2.0 98.3 ND 93 76-116 Silver 4.59 0.49 4.92 ND 93 54-132 Thallium 94.7 0.98 98.3 ND 96 64-120 Vanadium 117 2.0 98.3 20.6 98 78-124 Zinc 142 2.0 99.3 53.8 89 50-143 Matrix Spike Dup (B1D0734-MSD1) Source: 2102489-01 Analyzed: 04/26/21 13:11 Antimony 28.7 2.4 mg/kg 97.7 ND 29 10-116 6 20 Arsenic 99.5 2.0 97.7 6.40 95 77-121 2 20 Barium 173 0.98 97.7 72.5 103 30-169 9 20 Beryllium 90.5 0.49 97.7 0.419 92 86-111 3 20 Cadmium 96.7 0.24 97.7 ND 89 81-112 4 20 Chromium 120 0.49 97.7 22.2 100 75-129 3 20 Cobalt 95.5 0.49 97.7 6.95 91 71-121 3 20 Copper 120 0.98 97.7 21.5 101 68-135 3 20 Lead 92.4 0.49 97.7 6.10 88 72-121 3 20 Molybdenum 85.4 0.49 97.7 2.19 85 70-112 3 20 Nickel 121 0.49 97.7 30.4 92 73-121 1 20 Selenium 87.5 2.0 97.7 ND 90 76-116 5 20 Silver 4.44 0.49 4.88 ND 91 54-132 3 20 Thallium 90.3 0.98 97.7 ND 92 64-120 5 20 Vanadium 115 2.0 97.7 20.6 96 78-124 2 20 Zinc 141 2.0 97.7 53.8 89 50-143 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 67 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Post Spike (BlD0734-PSI) Source: 2102489-01 Analyzed: 04/26/21 13:14 Antimony 1.85 mg/l. 2.00 -0.00714 93 75-125 Arsenic 2.15 2.00 0.129 101 75-125 Barium 3.34 2.00 1.46 94 75-125 Beryllium 1.96 2.00 0.00843 97 75-125 Cadmium 1.88 2.00 -0.0200 94 75-125 Chromium 2.46 2.00 0.448 100 75-125 Cobalt 2.05 2.00 0.140 96 75-125 Copper 2.56 2.00 0.433 106 75-125 Lead 2.01 2.00 0.123 94 75-125 Molybdenum 1.97 2.00 0.0439 96 75-125 - • Nickel 2.55 2.00 0.613 97 75-125 Selenium 1.96 2.00 -0.0375 98 75-125 Silver 0.0965 0.100 -0.00476 96 75-125 Thallium 1.98 2.00 -0.0435 99 75-125 Vanadium 2.41 2.00 0.410 100 75-125 Zinc 2.96 2.00 1.08 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 68 of 94 i A WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0916 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:33 Blank (BlD0916-BLKI) Analyzed: 05/03/21 12:22 Cadmium ND 0.025 mg/L Chromium ND 0.050 " Copper ND 0.050 " Lead ND 0.050 " LCS (B1D0916-BS1) Analyzed: 05/03/21 12:35 Cadmium 9.62 0.025 mg/L 10.0 96 80-120 Chromium 9.56 0.050 10.0 96 80-120 Copper 9.66 0.050 10.0 97 80-120 Lead 9.70 0.050 10.0 97 80-120 LCS Dup (BlD0916-BSD1) Analyzed: 05/03/21 12:37 Cadmium 9.68 0.025 mg/L 10.0 97 80-120 0.6 20 Chromium 9.59 0.050 10.0 96 80-120 0.3 20 Copper 9.70 0.050 10.0 97 80-120 0.4 20 Lead 9.78 0.050 10.0 98 80-120 0.9 20 Duplicate (B1D0916-DUP1) Source: 2102467-01 Analyzed: 05/03/21 12:53 Cadmium ND 0.050 mg/L ND 20 Chromium 0.0860 0.10 0.111 25 20 QR-04 Copper 1.53 0.10 1.76 14 20 Lead 0.773 0.10 0.930 18 20 Leach Fluid Blank (B1D0916-LBK1) Analyzed: 05/03/21 12:25 Cadmium ND 0.050 mg/L Chromium ND 0.10 Copper ND 0.10 " Lead ND 0.10 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 69 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 TCLP Metals by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0919 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:49 Blank (B1D0919-BLKI) Analyzed: 05/03/21 13:54 Chromium ND 0.050 mg/1. Lead ND 0.050 " LCS (B1D0919-BS1) Analyzed: 05/03/21 14:02 Chromium 9.42 0.050 mg/L 10.0 94 80-120 Lead 9.97 0.050 1.10.0 100 80-120 LCS Dup (B1D0919-BSD1) Analyzed: 05/03/21 14:04 Chromium 9.35 0.050 mg/L 10.0 94 80-120 0.7 20 Lead 9.82 0.050 1110.0 98 80-120 2 20 Duplicate (B1D0919-DUPl) Source: 2102508-01 Analyzed: 05/03/21 14:11 Chromium ND 0.050 mg/L ND 20 Lead 1.60 0.050 112.02 24 20 QR-04 _ Leach Fluid Blank (BlD0919-LBK1) Analyzed: 05/03/21 13:57 Chromium ND 0.050 mg/L Lead ND 0.050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:_(8051925-3376 Page 70 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes - Level Result Limits Limit Batch BID0692 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 04/23/21 08:32 . Blank (BlD0692-BLKI) Analyzed: 04/23/21 10:26 TPH Gasoline (C5-02) ND 0.50 mg/kg Surrogate: 4-Bromof uorohenzene 0.128 110.125 103 39-157 LCS (B1D0692-BS1) Analyzed: 04/23/21 09:34 TPH Gasoline (C5-C12) 1.07 0.50 mg/kg 1.00 107 68-139 Surogate:4-Bronmlluorobenzene 0.146 110.126 116 39-157 • LCS Dup (B1D0692-BSDl) Analyzed: 04/23/21 10:00 TPH Gasoline (C5-C12) 1.05 0.49 mg/kg 0.988 106 68-139 2 20 Surrogate:4-Bromgfluorohenzene 0.150 0.124 121 39-157 - Duplicate (BlD0692-DUPl) Source: 2102433-01RE1 Analyzed: 04/23/21 22:44 TPH Gasoline (C5-('12) ND 4.8 mg/kg ND 20 Surrogate:4-Bromolluorohenzene 1.18 111.20 98 39-157 Matrix Spike (B1D0692-MS1) Source: 2102433-01RE1 Analyzed: 04/23/21 23:10 TPH Gasoline (('5-C12) 8.79 4.9 mg/kg 9.80 ND 90 10-171 Surrogatc:4-Bromolluorohenzene 1.34 111.23 109 39-157 Matrix Spike Dup (B1D0692-MSDl) Source: 2102433-01RE1 Analyzed: 04/23/21 23:36 TPH Gasoline (C5-C12) 8.26 4.4 mg/kg 9.77 ND 94 10-171 6 20 Surrogate.4-Bromolhmrohencene 1.29 111.10 118 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 71 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Semi -Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RP i Notes Level Result Limits Limit Batch BlD0766 - EPA 8015M Preparation: EPA 3550C 04/27/21 07:10 Blank (BlD0766-BLKI) Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22) ND 10 nig/kg TPH Motor Oil (C23-C40) ND 50 " Surrogate: o-TeiphenYl 41.9 " 49.8 84 65-136 LCS (BlD0766-BS1) Analyzed: 04/27/21 13:53 TPH Diesel (C13-C22) 420 10 ingtkg 499 84 72-115 TPH Motor Oil (C23-C40) 404 50 499 81 74-126 Surrozate: o-Terphenvl 43A 49.9 86 65-136 LCS Dup (B1D0766-BSDl) Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22) 420 10 mg/kg 500 84 72-115 0.2 20 TPH Motor Oil (C23-C40) 402 50 500 80 74-126 0.5 20 Surrogate: o-Teiphemd 42.3 50.0 85 65-136 Duplicate (B1D0766-DUPl) Source: 2102489-01 Analyzed: 04/27/21 15:02 TPH Diesel (C13-C22) ND 9.9 mg/kg ND 20 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Teiphent•1 38.9 49.6 78 65-136 Matrix Spike (BlD0766-MSI) Source: 2102489-01 Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22) 430 9.9 mg/kg 497 ND 86 46-147 TPH Motor Oil (C23-C40) 418 50 497 ND 84 35-171 Surrogate: o-Teiphen.rl 40.2 49.7 81 65-136 Matrix Spike Dup (BlD0766-MSD1) Source: 2102489-01 Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22) 480 10 mg/kg 499 ND 96 46-147 11 20 TPH Motor Oil (C23-C40) 429 50 499 ND 86 35-171 3 20 Surrogate: o-Teipheni'l 44.5 49.9 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 72 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (BlD0650-BLK1) Analyzed: 04/23/21 16:50 Styrene ND 0.0050 mg/kg 1, 1, 1,2-Tetrachloroethane ND 0.0050 " 1,1,2,2-Tetrachloroethane ND 0.0050 " Tetrachloroethene (PCE) ND 0,0050 " Toluene ND 0.0050 " 1,2.3-Trichlorobenzene ND 0.0050 " 1,2,4-Trichlorobenzene ND 0.0050 1,1..1-Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2,3-Trichloropropane ND 0.0050 12,4-Trimethylbenzene ND 0.0050 " 1,3,5-Trimethylbenzene ND 0.0050 " Vinvl chloride ND 0.0050 Xylenes (total) ND 0.0050 " Surrogate: Dibronw/luorumethane 0.0484 0.0498 97 74-122 Surrogate: Toluene-d8 0.0479 0.0498 96 65-128 Surrogate 4-Bromo/luorohen.ene 0.0453 0.0498 91 75-121 LCS (BlD0650-BSI) Analyzed: 04/23/21 14:31 Benzene 0.0389 0.0050 mg/kg 0.0390 98 70-131 Bromobenzene 0.0369 0.0050 0,0396 93 74-130 Brontochloromethanc 0.0351 0.0050 0.0396 89 64-133 Bromodichloromethane 0.0368 0.0050 0.0396 93 69-137 Bromotirrm 0.0337 0.0050 0.0396 85 55-132 Bromomethane 0.0397 0.0050 0.0396 100 10-142 ❑-Butylbenzene 0.0440 0.0050 0.0396 Ill 64-156 sec-Butylbenzene 0.0465 0.0050 0.0396 117 75-155 tert-Butylbenzene 0.0438 0.0050 0.0396 110 74-144 Carbon tetrachloride 0.0396 0.0050 0.0390 100 67-135 Chlorobenzene 0.0399 0.0050 0.0396 101 73-134 Chloroethane 0.0366 0.0050 0.0390 92 10-167 Chloroform 0.0371 0.0050 0.0396 94 69-124 C'hloromethane 0.0280 0.0050 0.0396 72 34-136 2-Chlorotohiene 0.0421 0.0050 0.0396 106 75-135 4-Chlorotoluene 0.0420 0.0050 0.0396 106 70-138 Dibromochloromethane 0.0370 0.0050 0.0396 93 67-135 1,2-Dibromo-3-chloropropane 0.0368 0.0050 0.0396 93 41-149 1,2-Dibromoethane (EDB) 0.0365 0.0050 0.0396 92 68-131 Dibromomcthanc 0.0322 0.0050 0.0396 81 61-140 1,2-Diclilorobenzene 0.0409 0.0050 0.0396 103 76-130 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 74 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS (BlD0650-BS1) Analyzed: 04/23/21 14:31 1,3-Dichlorobenzcne 0.0427 0.0050 mgtkg 0.0396 108 76-138 1,4-Dichlorobenzene 0.0410 0.0050 0.0396 104 72-132 Dichloroditluoromcthane 0.0196 0.0050 0.0396 50 10-155 l,l-Dichloroethane 0.0399 0.0050 0.0396 101 63-139 1,2-Dichlorocthane 0.0359 0.0050 0.0396 91 64-126 I,1-Dichloroethene 0,0435 0.0050 0.0396 110 52-167 cis-1.2-Dichloroethene 0.0380 0.0050 0.0396 96 70-135 trans-1,2-Dichloroethene 0.0421 0.0050 0.0396 106 67-147 1,2-Dichloropropane 0.0368 0.0050 0.0396 93 68-131 13-Dichloropropane 0.0359 0.0050 0.0396 91 64-128 2,2-Dichloropropane 0.0404 0.0050 0.0396 102 63-154 13-Diehloropropene 0.0386 0.0050 0.0390 97 68-138 cis-1.3-Diehloropropene 0.0376 0.0050 0.0396 95 72-134 trans-1,3-Diehloropropene 0.0385 0.0050 0,039(, 97 69-132 Ethylbenzene 0.0404 0.0050 0.0396 102 68-136 11exachlorobutadiene 0.0446 0.0050 0.0396 113 72-198 4-Isopropyl Toluene 0.0439 0.0050 0.0396 111 74-150 lsopropylbenzene 0.0429 0.0050 0.0396 108 71-149 Niethylene chloride 0.0402 0.0050 0.0396 102 51-127 Naphthalene 0.0436 0.0050 0.0396 110 57-158 n-Propylbenzene 0.0435 0.0050 0.0396 110 70-143 Styrene 0.0412 0.0050 0.0396 104 68-138 1, 1, 1,2-Tetrachloroethane 0.0373 0.0050 0.0396 94 76-130 1,1,2,2-Tctrachlorocthanc 0.0407 0.0050 0.0396 103 60-136 Tetrachloroethene(PCE) 0.0381 0.0050 0.0396 96 73-138 Toluene 0.0371 0.0050 0.0396 94 72-128 1,2,3-Trichlorobenzene 0.0390 0.0050 0.0396 98 61-166 1,2,4-Trichlorobenzene 0.0406 0.0050 0.0396 103 71-158 1. 1, 1 -Trichloroethane 0.0389 0.0050 0.0396 98 71-135 1,1,2-1'richloroethane 0.0341 0.0050 0.0396 86 64-132 Trichloroethene(TCE) 0.0374 0.0050 0.0396 94 74-139 Trichlorofluoromethaue 0.0379 0,0050 0.0396 96 30-156 1,2,3-Trichloropropane 0.0383 0.0050 0.0396 97 67-123 12,4-Trimethylbenzene 0.0419 0.0050 0.0396 106 68-134 1,3,5-Trimethylbenzene 0.0440 0.0050 0.0396 Ill 71-140 Vinyl chloride 0.0352 0,0050 0.0396 89 43-144 Xylenes (total) 0.122 0.0050 0.119 102 69-138 Surrogate: L)ibrunto/ittorontelhttn(, 00490 0.0495 99 74-133 Surrogate: Tt,luene-dX 0.0475 0.049.5 96 65-128 Surrogates' 4-Brnnu,jhtnruhett.une 0.0476 0.0495 96 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: ; 805) 925-3376 Page 75 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatilepo by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 -•- LCS Dup (B1D0650-BSD1) Analyzed: 04/23/21 14:59 Styrene 0.0437 0.0050 mgtkg 0.0398 110 68-138 6 20 1, 1, 1,2-Tetrachloroethane 0.0395 0.0050 0.0398 99 76-130 6 20 1,1,2,2-Tetrachlorocthanc 0.0415 0.0050 0.0398 104 60-136 2 20 Tetrachloroethene (PCE) 0.0400 0.0050 0.0398 100 73-138 5 20 TOIUCIIC 0.0399 0.0050 0.0398 100 72-128 7 20 1,2,3-Trichlorobenzene 0.0432 0.0050 0.0398 109 61-166 10 20 1,2,4-1'richlorobenzene 0.0439 0.0050 0.0398 110 71-158 8 20 1, 1, 1 -Trichloroethane 0.0415 0.0050 0.0398 104 71-135 6 20 1,1,2-Trichloroethane 0.0377 0.0050 0.0398 95 64-132 10 20 Trichloroethene (TCE) 0.0396 0.0050 0.0398 99 74-139 6 20 'Irichlorofluoromethane 0.0412 0.0050 0.0398 104 30-156 9 20 1,2,3-Trichloropropane 0.0381 0.0050 0.0398 96 67-123 0.6 20 12.4-Trim ethyl benzene 0.0448 0.0050 0.0398 113 68-134 7 20 1.3,5-Trimethyl benzene 0.0461 0.0050 0.0398 116 71-140 5 20 Vinyl chloride 0.0371 0.0050 0.0398 93 43-144 5 20 Xylenes (total) 0.128 0.0050 0.119 108 69-138 5 20 Surrogate: Dibromolluoromethanc 0.0504 0.0497 101 74-122 Surrogate: Toluene-d8 0.0476 0.0497 96 65-128 Surrogate 4-Bromo/hiorobenzene 0.0475 0.0497 96 75-121 Duplicate (B1D0650-DUP1.) Source: 2102489-01 Analyzed: 04/24/21 03:18 Benzene ND 0.0050 mg/kg ND 20 Bromobenz_ene ND 0.0050 ND 20 Brontochloromethanc ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 ' Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tent-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1.2-Dibronio-3-chloropropane ND 0.0050 ND 20 1,2-Dibronioethane (EDB) ND 0.0050 ND 20 Dibromomethanc ND 0.0050 ND 20 12-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl lent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 77 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Conipounds by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Duplicate (B1D0650-DUPI) Source: 2102489-01 Analyzed: 04/24/21 03:18 1,3-Dichlorobenzene ND 0.0050 mg/kg NI) 20 IA-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromethanc ND 0.0050 ND 20 1,1-Dichloroethane ND 0.0050 ND 20 1,2-Dichloroethanc ND 0.0050 ND 20 1, 1 -Dichloroethene ND 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1.2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1, 1 -Dichloropropene ND 0.0050 ND 20 cis-1,3-Dichloropropene ND 0.0050 NI) 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 Ethylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Nlethylene chloride ND 0.0050 " ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene NI) 0.0050 ND 20 Styrene ND 0.0050 ND 20 1, 1, 1,2-Tetrachloroethane ND 0.0050 ND 20 1,1,2,2-Tctrachlorocthanc ND 0.0050 ND 20 Tetrachloroethene WCE) NI) 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,24-Trichlorobenzene ND 0.0050 ND 20 I,1,1-Trichloroethane NI) 0.0050 ND 20 1, 1 .2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorofluoronrethane ND 0.0050 " ND 20 1,2,3-Trichloropropane NI) 0.0050 ND 20 1,24-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibrotno/ltiorumc,thune 0.0479 0.0496 97 74-122 Surrogate: Tiduene-dN 0.0485 0.0496 98 65-128 Surrogate: 4-Bronioguorohen_ene 0.0452 0.0496 91 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 78 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic CompoundsQuality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 -• Matrix Spike (BlD0650-MS1) Source: 2102489-02 Analyzed: 04/24/21 04:12 Benzene 0.0404 0.0050 mglkg 0.0402 ND 101 37-145 Bromobenzene 0.0359 0,0050 0.0402 ND 89 29-147 Bromochloromcthanc 0.0367 0.0050 0.0402 ND 91 40-145 Bromodichloromethane 0.0384 0.0050 0.0402 ND 96 39-153 Bromotorm 0.0332 0.0050 0.0402 ND 83 32-143 Bromomethane 0.0467 0.0050 0.0402 ND 116 10-141 - n-Butylbenzene 0.0324 0.0050 0.0402 ND 81 10-162 sec-Butylbenzene 0.0408 0.0050 0.0402 ND 102 14-168 tert-Butylbenzene 0.0388 0.0050 0.0402 ND 97 21-159 Carbon tetrachloride 0.0380 0.0050 0.0402 ND 95 28-148 - Chlorobenzene 0.0384 0.0050 0.0402 ND 96 32-148 Chloroethane 0.0502 0.0050 0.0402 ND 125 11-166 Chloroform 0.0400 0.0050 0.0402 ND 100 40-139 Chloromethane 0.0350 0.0050 0.0402 ND 87 18-135 .-. 2-Chlorotoluene 0.0362 0.0050 0.0402 ND 90 25-151 4-Chlorotoluene 0.0363 0.0050 0.0402 ND 90 22-150 Dibromochloromethane 0.0359 0.0050 0.0402 ND 89 40-147 1,2-1)ibromo-3-chloropropane 0.0390 0.0050 0.0402 ND 97 25-158 1,2-Dibromoethane (F.DB) 0.0369 0,0050 0.0402 ND 92 38-147 Dibronxancthanc 0.0319 0.0050 0.0402 ND 79 39-150 1,2-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 24-154 1,3-Dichlorobenzene 0.0369 0.0050 0.0402 ND 92 21-153 1,4-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 21-146 Dichloroditluorontcthane 0.0188 0.0050 0.0402 ND 47 10-149 1,1-Dichloroethane 0.0420 0,0050 0.0402 ND 105 34-151 1,2-Dichlorocthane 0.0400 0.0050 0.0402 ND 100 40-137 13-Dichloroethene 0.0449 0.0050 0.0402 ND 112 21-172 cis-1.2-1)ichloroethene 0.0385 0.0050 0.0402 ND 96 38-147 trans- l,2-Dichloroethene 0.0409 0.0050 0.0402 ND 102 30-160 1,2-Dichloropropane 0.0397 0.0050 0.0402 ND 99 39-146 1,3-Dichloropropane 0.0396 0.0050 0.0402 ND 99 39-141 2,2-Dichloropropane 0.0280 0.0050 0,0402 ND 70 26-149 1. 1 -Dichloropropene 0.0385 0.0050 0.0402 ND 96 28-150 cis-1.3-Dichloropropene 0.0371 0.0050 0.0402 ND 92 34-149 trans-1,3-Dichloropropene 0.0384 0.0050 0.0402 ND 96 36-143 Ftylbenzene 0.0397 0.0050 0.0402 0.00290 92 23-150 Ilexachlorobutadiene 0.0313 0.0050 0.0402 ND 78 10-192 4-Isopropyl Toluene 0.0385 0.0050 0.0402 0.00290 89 11-165 Isopropylbenzene 0.0406 0.0050 0.0402 0.00202 96 17-166 - Nlethylene chloride 0.0456 0.0050 0.0402 ND 114 28-135 Naphthalene 0.0441 0.0050 0.0402 0.00948 86 10-174 n-Propylbenzenc 0.0393 0.0050 0.0402 0.00310 90 16-156 The results In this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 79 of 94 661�N Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GC/MS - Quality Control knalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (BlD0650-MSI) Source: 2102489-02 Analyzed: 04/24/21 04:12 Styrene 0.0397 0.0050 mg/kg 0.0402 ND 96 24-154 1,1,1,2-Tetrachloroethane 0.0367 0.0050 0.0402 ND 91 38-149 1,1,2,2-Tetrachloroethane 0.0387 0.0050 0.0402 ND 96 22-164 Tetrachloroethane (PCE) 0.0349 0.0050 0.0402 ND 87 25-153 Toluene 0.0376 0.0050 0.0402 ND 94 26-149 1,23-Trichlorobenzene 0.0323 0.0050 0.0402 ND 80 10-163 1,2,4-Trichlorobenzene 0.0323 0.0050 0.0402 ND 81 10-162 1, 1, 1 -Trichloroethane 0.0387 0.0050 0.0402 ND 96 34-149 1, 1,2-Trich loroethane 0.0397 0.0050 0.0402 ND 99 25-175 Trichloroethene (TCE) 0.0386 0.0050 0.0402 ND 96 25-170 Trichlorofluoromethane 0.0487 0.0050 0.0402 ND 121 19-155 1,2,3-Trichloropropane 0.0403 0.0050 0.0402 ND 100 32-165 1,2.4-Trimethylbenzene 0.0466 0.0050 0.0402 0.0183 70 15-150 1,3,5-Triin ethyl benzene 0.0413 0.0050 0.0402 0.00496 90 10-158 Vinyl chloride 0.0446 0.0050 0.0402 ND 111 22-148 Xylenes (total) 0.130 0.0050 0.120 0.0173 93 22-153 Surrogate: Dibrvmof itorumcthane' 0.0487 " 0.0502 97 74.122 Surrogate: Tohrene-A 0.0484 0.0502 96 65-128 Surrogate:4-Bromofluorohenzene 0.0474 0.0502 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 80 of 94 M A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sampleid Summary ualysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 9015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals by ICP 601013 STLC Cadmium STLC/EPA 6010B Water OEC, CA-ELAP 6010B STLC Chromium STLC/EPA 601013 Water OEC, CA-ELAP 601013 STLC Copper STLC/EPA 601013 Water OEC, CA-ELAP 601013 STLC Lead STLC/EPA 601013 Water OEC. CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601013 TCLP Chromium EPA 1311/EPA 6010B Water OEC, CA-ELAP 601013 TCLP Lead EPA 1311%EPA 601013 Water OF.C, CA-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA -FLAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 81 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method Summary (Continued) _., nalysis Method Matrix Laboratory & Certification Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA -FLAP Total Metals by ICP 6010B Total Antimony 6010B Total Arsenic 6010B Total Barium 6010B Total Beryllium 6010B Total Cadmium 6010B Total Chromium 601013Total Cobalt 6010B Total Copper 6010B Total Lead 6010B Total Molybdenum 6010B Total Nickel 6010B Total Selenium 6010B Total Silver - • 601OB Total Thallium 601 OB Total Vanadium 6010B Total Zinc EPA 6010B Solid OEC, CA -FLAP EPA 6010B Solid OEC, CA-ELAP EPA 6010B Solid OEC, CA-ELAP EPA 6010B Solid OEC, CA-ELAP EPA 6010B Solid OEC, CA-ELAP EPA 6010B Solid OEC. CA-ELAP EPA 6010B Solid OEC, CA-E.LAP EPA 601 OB Solid OEC, CA -FLAP EPA 601 OB Solid OEC, CA-ELAP EPA 6010B Solid OEC, CA-ELAP EPA 6010B Solid OEC, CA-ELAP EPA 6010B Solid OEC, CA-ELAP EPA 601 OB Solid OEC. CA-ELAP EPA 601OB Solid OEC, CA-ELAP EPA 601 OB Solid OEC, CA -FLAP EPA 6010B Solid OEC. CA-ELAP Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 82 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EI'A 8015M Solid OEC, CA-ELAP 8015 TPI I -Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OE.C_ Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPI I -Gasoline EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-E.LAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAY 8015 TPH-Gasoline EPA 8015M Solid OEC', Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC:, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 83 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-01 Analyte concentration exceeds TTLC. N-02 Analyte concentration below TTLC but above I Ox S'PLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-03 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8051, 925-3376 Page 84 of 94 EMSL Analytical, Inc. 464 McCormick Street San Leandro, CA 94577 Tel/Fax: (510) 895-3675 / (510) 895-3680 http://www.EMSL.com / sanleandrolab@emsl.com Attention: Shahanaz Parvin Oilfield Environmental and Compliance 307 Roemer Way Suite 300 Santa Maria, CA 93454-1105 Project: 2102508 EMSL Order: 092105912 Customer ID: OILF50 Customer PO: 2102508 Project ID: Phone: (805) 922-4772 Fax: (805) 925-3376 Received Date: 04/26/2021 8:45 AM Analysis Date: 04/26/2021 Collected Date: 04/23/2021 Test Report: Asbestos Analysis of Bulk Materials via EPA 600IR-931116 Method using Polarized Light Microscopy Non -Asbestos Asbestos Sample Description Appearance % Fibrous % Non -Fibrous % Type 2102508-16 Tan 50% Quartz None Detected Non -Fibrous 50% Non -fibrous (Other) 092105912-0001 Homogeneous _ 2102508-17 Gray 50% Quartz None Detected Non -Fibrous 40% Ca Carbonate 092105912-0002 Homogeneous 10% Non -fibrous iOther. Analyst(s) Gavin Lee (2) Cecilia Yu, Laboratory Manager or Other Approved Signatory EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 "Interim Method") but augmented with procedures outlined in the 1993 ("final") version of the method. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non -friable organically bound materials present a problem matrix and therefore EMSL recommends gravimetric reduction prior to analysis. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Estimation of uncertainty is available on request. Samples analyzed by EMSL Analytical, Inc San Leandro, CA NVLAP Lab Code 101048-3, WA C884 Initial report from: 04/26/2021 13:36:56 ASB PLM 0008 0001 - 1.78 Printed: 4/26/2021 1:36 PM Page 1 of 1 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2314.D Operator EW Acquired 23 Apr 2021 2:32 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-01@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 14 Response_ 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2314.DT1D1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2315.D Operator EW Acquired 23 Apr 2021 2:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-02@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 15 80000 ` 75000 70000 65000 60000 55000 500001 45000 40000 35000 f 30000 25000 20000 15000 I 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 GOMD2315.D\FID1A r.00 8.00 9.00 1 0.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2316.D Operator EW Acquired 23 Apr 2021 3:24 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-03@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 16 Response_ 95000 90000 I 85000; i 80000. 75000 70000 65000 60000• 550001 50000i 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2316.D\FID1A I I• _ 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 - File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2317.D Operator : EW Acquired : 23 Apr 2021 3:50 pm using AcgMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-04@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 17 Response 1 900001 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2317.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2318.D Operator EW Acquired 23 Apr 2021 4:16 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-05@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 18 Response_ 95000{ 90000 85000 80000 75000i 60000 55000 50000 i 40000 35000 30000 25000 20000 15000 10000 5000 G0MD2318.DT1D1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2319.D Operator EW Acquired 23 Apr 2021 4:42 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-06@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 19 Response_ 90000 85000 80000 75000+ l 70000� 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2319.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2320.D Operator EW Acquired 23 Apr 2021 5:08 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-07@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 20 Response_ GOMD2320.D\FID1A 95000 90000 85000 80000 45000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2321.D Operator EW Acquired 23 Apr 2021 5:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-08@1:10 PREP Misc Info : 1@BlD0692 GRO Solid Vial Number: 21 Response_ 85000! 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 I 10000 GOMD2321.D\FID1A 5000 I 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2322.D Operator EW Acquired 23 Apr 2021 6:00 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-09@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 22 Resr 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 I 30000 25000 20000 15000 10000 5000 GOMD2322.DT1D1A - I i I 1 1 1-7 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2323.D Operator EW Acquired 23 Apr 2021 6:26 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-10@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 23 GOMD2323.D\FID1A 75000 70000 65000 60000 55000 50000 45000 40000 I 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2328.D Operator EW Acquired 23 Apr 2021 8:35 pm using AcgMethod GASBTEXE.M Instrument GC7 .� Sample Name: 2102508-11@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 28 Response_ I 90000i 850001 80000 75000� I 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2328.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2330.D Operator EW Acquired 23 Apr 2021 9:27 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-13@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 30 Response_ I 95000, I 90000 I 1 85000 65000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.0( GOMD2330.D\FID1A 10 12.00 r 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2331.D Operator EW Acquired 23 Apr 2021 9:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-14@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 31 Response_ 90000 850001 800001 75000 i 50000 45000 40000 35000 ~ 30000 25000 20000 15000 10000 GOMD2331.D\FID1A Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 �j File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2332.D Operator EW Acquired 23 Apr 2021 10:18 pm using AcgMethod GASBTEXE.M Instrument GC7 .-• Sample Name: 2102508-15@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 32 Response_ 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000- 25000 20000 15000- 10000 5000- 1 Time 0.00 1.00 2.00 3.00 GOMD2332.D\FID1A 1.00 12.00 13.00 14.00 n ! 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Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: I*dA6 Ia,"), Meredith Sprister, Business Director msprister@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Revision i Previous Report Reason for Revision 2102032 04/07/2021 16:45 Complete report. Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Sump Trench W 2102032-01 Solid Solid 04/06/2021 10:25 04/06/2021 11:30 Sump Trench Pile 2102032-02 Solid Solid 04/06/2021 10:26 04/06/2021 11:30 Sump Trench Bottom 2102032-03 Solid Solid 04/06/2021 10:30 04/06/2021 11:30 Fire Trench Bottoms 2102032-04 Solid Solid 04/06/2021 10:36 04/06/2021 11:30 Fire Trench W 2102032-05 Solid Solid 04/06/2021 10:38 04/06/2021 11:30 Fire Trench E 2102032-06 Solid Solid 04/06/2021 10:40 04/06/2021 11:30 BatchSample Analysis Batch ID Preparation Date/Time STLC Metals by ICP 6010B STLC B 1 D0494 04/ 16/2021 15:40 STLC Metals Extraction STLC Metals Extraction BlD0313 04/12/2021 14:18 TCLP Metals by ICP 6010B TCLP B 1 D0495 04/16/2021 15:41 TCLP Metals Extraction TCLP Metals Extraction B 1 D0312 04112/2021 14:17 Total Metals by CNAA MercuryTotal EPA 7471 A B 1 D0153 04/07/2021 07:54 Total :Metals by ICP 601 OB Total B 1 D0123 04/06/2021 12:15 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 20 a A bincra Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 04/06/21 10:25 ' Matrix: Solid Sampled by : Lab ID : 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.097 0.091 mg%kg 1 B 1 D0153 04/07/21 14:55 EPA 7471 A Total Metals by ICP Antimony 7.5 2.3 mg/kg 1 B I D0123 04/07/21 13:25 EPA 6010B Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 N-02, N-03 Molybdenum 2.0 0.46 Nickel 98 0.46 Selenium ND 1.9 Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 Zinc 410 1.9 " STLC Metals by ICP Chromium 0.70 0.10 mg/L 2 B1D0494 04/19'2112:57 STLC/EPA6010B - Lead 3.6 0.10 " " " " " TCLP Metals by ICP Lead 0.23 0.050 mgi'L I BID0495 04/19/2114:01 EPA 1311/EPA601OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID : Sump Trench Pile Sampled: 04/06/21 10:26 Matrix: Solid Sampled by : Lab ID: 2102032-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.12 0.094 mg/kg 1 B1D0153 04/07/21 14:57 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BID0123 04/07/2113:28 EPA 6010B Arsenic 7.4 1.9 Barium 280 0.95 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 12 0.47 Copper 38 0.95 Lead 180 0.47 N-02, N-03 Molybdenum 1.2 0.47 Nickel 78 0.47 " Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 37 1.9 Zinc 250 1.9 STLC Metals by ICP Chromium 0.39 0.10 mg/L 2 BID0494 04/19/2113:00 STI.C"F.PA6010B Lead 15 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.086 0.050 mg/l. 1 B I D0495 04/19/21 14:04 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalytical t Sample ID: Sump Trench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by : Lab ID: 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg I B 1 DOI 53 04/07/21 14:59 EPA 7471 A Total Metals by ICP Antimony 2.5 2.4 mg/kg 1 B 1 D0123 04/07/21 13:31 EPA 601 OB Arsenic 7.0 1.9 " Barium 230 0.97 Beryllium ND 0.48 " Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.48 " Copper 72 0.97 Lead 140 0.48 N-02 N-03 Nlolvbdenum 1.1 0.48 Nickel 190 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 34 1.9 Zinc 560 1.9 " STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 B I D0494 04/19/21 13:02 STLC/EPA 601 OB . Lead 7.6 0.10 " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 nrg/l, 1 B 1 D0495 04/19/21 14:06 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID : Fire Trench Bottoms Sampled: 04/06/21 10:36 Matrix: Solid Sampled by: Lab ID : 2102032-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg/kg 1 B1D0153 04/07/21 15:01 EPA 7471A Total Metals by ICP Antimony ND 2.3 mgtkg 1 BID0123 04/07/2113:34 EPA6010B Arsenic 6.6 1.8 Barium 220 0.91 Beryllium 0.63 0.46 Cadmium ND 0.23 Chromium 52 0.46 Cobalt 18 0.46 Copper 26 0.91 Lead 9.4 0.46 Molybdenum 0.46 0.46 Nickel 110 0.46 Selenium ND 1.8 Silver ND 0.46 Thallium ND 0.91 Vanadium 34 1.8 Zinc 28 1.8 STLC Metals by ICP Chromium ND 0.10 mg/L 2 B1D0494 04/19/2113:13 STLC/EPA601t1B N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report Sample ID: Fire Trench W Sampled: 04/06/21 10:38 " Matrix: Solid Sampled by : Lab ID : 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.13 0.096 mg/kg 1 B 1 D0153 04/07/21 15:04 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1 D0123 04/07/21 13:37 EPA 6010B r Arsenic 4.8 1.9 Barium 130 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 41 0.48 Cobalt 9.0 0.48 Copper 22 0.96 Lead 27 0.48 Molvbdenum 1.1 0.48 " Nickel 50 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 34 L9 " Zinc 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report t Sample ID : Fire Trench E Sampled: 04/06/21 10:40 Matrix: Solid Sampled by : Lab ID : 2102032-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.12 0.094 mg/kg 1 B1D0153 04/07/21 15:06 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg!kg 1 B1D0123 04/07/2113:17 EPA 6010B Arsenic 6.4 1.9 Barium 170 0.94 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 49 0.47 Cobalt 12 0.47 Copper 26 0.94 Lead 32 0.47 Molybdenum 1.2 0.47 Nickel 73 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.94 Vanadium 36 1.9 Zinc 64 1.9 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0153 -EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 _ Blank (B1D0153-BLK1) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg/kg LCS (B1D0153-BSI) Analyzed: 04/07/21 13:07 -.. Mercury 0.809 0.10 mgIg 0.833 97 85-115 LCS Dup (BID0153-BSD1) Analyzed: 04/07/21 13:09 Mercury 0.799 0.10 mg/kg 0.833 96 85-115 1 20 Duplicate (B1D0153-DUPl) Source: 2101942-01 Analyzed: 04/07/21 13:17 Mercury 0.0118 0.087 mg/kg 0.0145 21 20 QR-04 Matrix Spike (B1D0153-MS1) Source: 2101942-01 Analyzed: 04/07/21 13:19 Mercury 0.904 0.097 mg/kg 0.809 0.0145 98 75-125 Matrix Spike Dup (B1D0153-MSD1) Source: 2101942-01 Analyzed: 04/07/21 13:21 Mercury 0.776 0.092 mg/kg 0.765 0.0145 100 75-125 4 20 Post Spike (B1D0153-PS1) Source: 2101942-01 Analyzed: 04/07/21 13:23 Mercury 5.16 ug/l. 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Blank (B1D0123-BLKI) Analyzed: 04/07/21 12:48 Antimony ND 2.5 mg1kg Arsenic ND 2.0 " Barium ND 1.0 " Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1 A Lead ND 0.50 Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 " Vanadium ND 2.0 Zinc ND 2.0 LCS (B1D0123-BS1) Analyzed: 04/07/21 12:53 Antimony 97.5 2.5 mg/kg 100 98 80-120 Arsenic 100 2.0 100 100 80-120 Barium 103 LO 100 103 80-120 Beryllium 100 0.50 100 100 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 100 0.50 100 100 80-120 Cobalt 102 0.50 100 102 80-120 Copper 98.3 1.0 100 98 80-120 Lead 102 0.50 100 102 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium 99.8 2.0 100 100 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 1.0 100 102 80-120 Vanadium 96.7 2.0 100 97 80-120 Zinc 102 2.0 100 102 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 ..rvw.oecusa.com FAX: (805) 925-3376 Page 10 of 20 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 -EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 . LCS Dup (BIDO123-BSDl) Analyzed: 04/07/21 12:56 Antimony 100 2.5 mgAg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 1.0 100 105 80-120 2 20 - Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 SO-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 50-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 101 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 SO-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 1.0 100 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 100 104 80-120 2 20 Duplicate (B1DO123-DUPl) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mgikg 1.40 20 Arsenic 5.99 1.9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 ND 20 Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 -+ Copper 26.5 0.97 26.5 0.2 20 Lead 28.1 0.48 32.0 13 20 Molybdenum 56.4 0.49 1.20 192 20 QR-04 Nickel 68.5 0.48 73.4 7 20 F Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 Vanadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of 20 WIL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Totalby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Matrix Spike (B1D0123-MS1) Source: 2102032-06 Analyzed: 04/07/21 12:58 Antimony 37.4 2.4 mg/kg 97.7 1.40 37 10-116 Arsenic 101 2.0 97.7 6.36 97 77-121 Barium 250 0.98 97.7 169 83 30-169 Beryllium 94.0 0.49 97.7 0.395 96 86-111 Cadmium 90.0 0.24 97.7 ND 92 81-112 Chromium 144 0.49 97.7 48.9 98 75-129 Cobalt 102 0.49 97.7 11.8 92 71-121 Copper 122 0.98 97.7 26.5 98 68-135 Lead 120 0.49 97.7 32.0 90 72-121 Molybdenum 87.1 0.49 97.7 1.20 88 70-112 Nickel 156 0.49 97.7 73.4 85 73-121 Selenium 91.5 2.0 97.7 ND 94 76-116 Silver 4.87 0.49 4.88 ND 100 54-132 Thallium 85.3 0.98 97.7 ND 87 64-120 Vanadium 131 2.0 97.7 36.2 97 78-124 Zinc 163 2.0 97.7 64.5 100 50-143 Matrix Spike Dup (B1D0123-MSD1) Source: 2102032-06 Analyzed: 04/07/21 13:01 Antimony 38.1 2.5 mg/kg 98.3 1.40 37 10-116 2 20 Arsenic 108 2.0 98.3 6.36 103 77-121 6 20 Barium 263 0.98 98.3 169 96 30-169 5 20 Beryllium 97.9 0.49 98.3 0.395 99 86-111 4 20 Cadmium 94.3 0.25 98.3 ND 96 81-112 5 20 Chromium 156 0.49 98.3 48.9 109 75-129 8 20 Cobalt 106 0.49 98.3 11.8 96 71-121 4 20 Copper 130 0.98 98.3 26.5 105 68-135 6 20 Lead 126 0.49 98.3 32.0 95 72-121 4 20 Molybdenum 91.2 0.49 98.3 1.20 91 70-112 5 20 Nickel 167 0.49 98.3 73.4 95 73-121 7 20 Selenium 96.0 2.0 98.3 ND 98 76-116 5 20 Silver 4.99 0.49 4.92 ND 102 54-132 2 20 Thallium 89.8 0.98 98.3 ND 91 64-120 5 20 _ Vanadium 137 2.0 98.3 36.2 102 78-124 4 20 Zinc 167 2.0 98.3 64.5 104 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 12 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by 1CP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PS1) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.98 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.558 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 vanadium 2.68 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.30 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 STLC Metals by ICP - Quality Control ialyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0494 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 10:40 Blank (B1D0494-BLK1) Analyzed: 04/19/21 12:12 Chromium ND 0.050 mg/l. Lead ND 0.050 " LCS (B1D0494-BSI) Analyzed: 04/19/21 12:23 Chromium 9.69 0.050 mg/L 10.0 97 80-120 Lead 9.80 0.050 1110.0 98 80-120 LCS Dup (B1D0494-BSDI) Analyzed: 04/19/21 12:25 Chromium 9.72 0.050 mg/L 10.0 97 80-120 Lead 9.71 0.050 1110.0 97 80-120 Duplicate (BlD0494-DUPI) Source: 2101759-01 Analyzed: 04/19/21 12:46 Chromium 120 0.050 mg/L 112 Lead 54.3 0.050 1151.6 Leach Fluid Blank (BlD0494-LBKI) Analyzed: 04/19/21 12:15 Chromium ND 0.10 mg/L Lead ND 0.10 " Leach Fluid Blank (B1D0494-LBK2) Analyzed: 04/19/21 12:17 Chromium ND 0.10 mg/L Lead ND 0.10 " Matrix Spike (B1D0494-MS1) Source: 2101759-01 Analyzed: 04/19/21 12:28 Chromium 116 0.10 mg/L 10.0 112 42 89-115 Lead 59.4 0.10 1.10.0 51.6 78 86-114 Matrix Spike Dup (BlD0494-MSD1) Source: 2101759-01 Analyzed: 04/19/21 12:38 Chromium 134 0.10 mg/L 10.0 112 214 89-115 Lead 68.2 0.10 1110.0 51.6 166 86-114 0.3 20 1 20 6 20 5 20 QN1-4X QN1-4a 14 20 QN14a 14 20 QN14X The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TCLP Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (BlD0495-BLK1) Analyzed: 04/19/21 13:46 Lcad ND 0.050 mg/L LCS (B1D0495-BS1) Analyzed: 04/19/21 13:26 Lcad 9.76 0.050 mg/L 10.O LCS Dup (B1D0495-BSDl) Analyzed: 04/19/21 13:28 Lead 9.71 0.050 mg/L 10.0 Duplicate (B1D0495-DUPl) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lead ND 0.050 mg/[. Leach Fluid Blank (B1D0495-LBKl) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/1. Leach Fluid Blank (BlD0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/I. Matrix Spike (BlD0495-MSI) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lcad 10.1 0.050 mg/L 10.0 Matrix Spike Dup (BlD0495-MSD1) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lead 9.94 0.050 mg/I, 10.0 98 80-120 97 80-120 0.5 20 ND 20 ND 101 86-114 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Sample Method Summary nalysis Method Matrix Laboratory & Certification STLC Metals by ICP 601013 STLC Chromium S'I'LC/EPA 601013 Water OEC. CA -FLAP 601013 STLC lead STLC/EPA 601013 Water OEC, CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601013TCLP Lead EPA 1311/EPA 6010B Water OEC, CA-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, C A-ELAP Total Metals by ICP 601013 Total Antimony EPA 601013 Solid OEC, CA -FLAP 601013 Total Arsenic EPA 601013 Solid OEC, CA-ELAP 601013 Total Barium EPA 601013 Solid OEC, CA-ELAP 6010B Total Beryllium EPA 601013 Solid OEC. CA-ELAP 0010B Total Cadmium EPA 601013 Solid OEC, CA-ELAP 6010B Total Chromium EPA 601013 Solid OEC, CA-ELAP 601013 Total Cobalt EPA 601013 Solid OEC, CA-ELAP 001013 Total Copper EPA 601013 Solid OEC, CA-ELAP 601013 Total Lead EPA 601013 Solid OEC, CA-ELAP 601013 Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 601013 Total Nickel EPA 6010B Solid OEC, CA -FLAP 601013 Total Selenium EPA 601013 Solid OEC. CA-ELAP 601OB Total Silver EPA 601013 Solid OEC, CA-ELAP 601013 Total "I'hallium EPA 6010B Solid OEC, CA-ELAP 6010B Total Vanadium EPA 001013 Solid OEC, CA-ELAP 601013 Total Zinc EPA 6010B Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCI.P. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 time, or greater the spike concentration. The QC batch was accepted based on LCS and or LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 20 XQ� » J C a E U �H� SPHOS PSNOSIO 1e101 G O G ZBOS / Mos L 4114R1Osi bu v U s DOUB' SDOAS a C wme OWOJ-dHl rn E m *pWnS I OPIURAO eApaeaa F- m > oa e z $ +• 1911 Ilnd SO9Z9 Z A ❑ A: Cu cU� d SPnew " ZZ eall Is, c� d d oC m r m m `` w eCL19 m 9 a : a n aIf a - ~ ❑ ❑❑ C 13 U a 06 Z❑':: � o0 o ca o C z u q®eyq O O O❑ F m } x = ■❑ ` r c` a E C 10 0 y0 .. N o «eEWp � V o� G '� n=ry H as�- W L 31 ❑❑ �. d c° o F E E Q 3 O a a� E s a A� �� O W N C C C +r •r. 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Box 2646 Report Date: April 06, 2021 16:03 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Centers, 2600 Broad St. Enclosed is an analytical report for the above referenced project. The samples included in this report were received on March 25, 2021 15:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: '*GiI.�J Meredith Sprister, Business Director msprister@occusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Revision Previous Report Reason for Revision 2101841 03/26/2021 17:07 Complete report. nle Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Tank N Wall 2101841-01 Solid Solid 03/25/2021 11:15 03/25/2021 15:00 Tank S Wall 2101841-02 Solid Solid 03/25/2021 11:20 03/25/2021 15:00 Tank E Wall 2101841-03 Solid Solid 03/25/2021 11:25 03/25/2021 15:00 Tank W Wall 2101841-04 Solid Solid 03/25/2021 11:30 03/25/2021 15:00 ' Tank Bottom E. End 2101841-05 Solid Solid 03/25/2021 11:05 03/25/2021 15:00 Tank Bottom W. End 2101841-06 Solid Solid 03/25/2021 11:10 03/25/2021 15:00 Sump Trench W 2101841-07 Solid Solid 03/25/2021 11:35 03/25/2021 15:00 Sump Trench S 2101841-08 Solid Solid 03/25/2021 11:38 03/25/2021 15:00 Control 2101841-09 Solid Solid 03/25/202111:00 03/25/2021 15:00 Soil Pile N 2101841-10 Solid Solid 03/25/2021 11:40 03/25/2021 15:00 Soil Pile S 2101841-11 Solid Solid 03/25/2021 11:45 03/25/2021 15:00 Soil Pile W 2101841-12 Solid Solid 03/25/2021 11:50 03/25/2021 15:00 Soil Pile E 2101841-13 Solid Solid 03/25/2021 12:10 03/25/2021 15:00 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 e Page 2 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 BatchSample Analysis Batch ID Preparation Date/Time Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B1(`0798 03/25/2021 17:29 STLC Metals by ICP 601013 STLC BID0007 04/01/2021 09:01 STLC Metals Extraction STLC Metals Extraction B I C 0891 03/302021 10:02 TCLP Metals by ICP 601013TCLP B I D0112 04/06/2021 10:26 TCLP Metals Extraction TCLP Metals Extraction B I C0898 03/30/2021 12:22 Total Metals by CVAA Mercury Total EPA 7471 A B 1('0807 03/26.'2021 07:43 Total Metals by ICP 6010B Total B1 C0810 03/26/2021 08:36 Volatile Organic Compounds by GUMS 826013 Full List BIC0815 03/26/2021 09:17 8260B Full List B I C0817 03/26,12021 11:40 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B1('0802 03/26;2021 05:22 8015 TPH-Gasoline B 1('0804 03/26/2021 05:26 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805i 925-3376 Page 3 of 79 ---v Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg,kg 1 B 1('0807 03/26/21 14:37 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg,kg 1 BI('0810 03/26/21 13:30 FPA601OB Arsenic 8.9 2.0 Barium 150 0.98 Bervllium 0.61 0.49 Cadmium ND 0.24 Chromium 51 0.49 N-02 Cobalt 17 0.49 Copper 28 0.98 Lead 9.1 0.49 Molvbdenum 2.6 0.49 " Nickel 76 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 39 2.0 Zinc 32 2.0 " STLC Metals by ICP Chromium 0.13 (1.10 mg/l. 2 BID0007 04/01/2) 14:45 STI.C/EPA601OB Volatile Organic TPH by GC/FID TPH Gasoline (C5-C2) ND 4.9 mg/kg 1 BIC0802 03/26/21 10:47 EPA 9015M R-07 Surrogate" d-BromoJluoroben::ene 103 % (31 - 168 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 ,,,,ww.oecusa.com FAX: 805 925-3376 Page 4 of 79 C A W6M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Heating Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (Cl3-C22) ND 10 mg'Rg 1 BIC0798 03/26/21 07:48 EPA 8015M TPII Motor Oil (('23-C40) ND 50 " Surrogate: o-Tei phen.rl 107 % (65 - 133) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mgtkg 1000 B I C0815 03/2621 11:52 EPA 8260B r Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichlorornethane ND 1.2 - Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 r sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcne ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 " Dibromochloromethanc ND 1.2 _ 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibrontoethane (EDB) ND 1.2 Dibrotuomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichloroben7ene ND 1.2 Dichlorodithwromiethane ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 -. cis-1.2-Dichloroethene ND 1.2 trans-l.2-Dichloroethene ND 1.2 " 12-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 - trans-1,3-Dichloropropene ND 1.2 Ethylbcnzcnc ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:1805) 925-3376 Page 6 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlombutadiene ND 1.2 mgtkg 1000 BIC0815 03/26'21 11:52 EPA926013 4-Isopropyl Toluene ND 1.2 Nopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1,13,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 Tetrachloroctliene (PCE) ND 1.2 Tolucnc ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 " I.1,1-Trichlometliane ND 1.2 1,1.2-Trichloroethane ND 1.2 IYiehloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1.24-Trimethylbenzene ND 1.2 13,5-Trinrethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromu/luorome thane 97 ` o ( 75 - 122 ) Surrogate: Toluene-db' 92% (66 - 12S) " Surrogate: 4-Bromollooroben_ene 92 "i,, ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.coniWeports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.086 mglkg 1 B 1('0807 03/20/21 14:39 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg: kg 1 B I COX 10 03/26/21 13:33 EPA 601 OB Arsenic 4.1 2.0 Barium 11 0.98 Beryllium ND 0.49 Cadmitan ND 0.24 Chromium 9.0 0.49 Cobalt 1.4 0.49 Copper 3.5 0.99 Lead 2.5 0.49 Molybdenum 3.3 0.49 Nickel 6.8 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 6.3 2.0 Zinc 9.7 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) Surrogate: 4-Bromq lnoroben:�cne Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-('22) TPH Motor Oil (('23-C40) Surrogate: o-Terphent'1 ND 4.5 mg/kg I B I C0802 03/26'21 11:13 EPA 8015M R-07 103` (31-168) 11" 11 ND 10 mg'kg 1 B I C0798 03/26/21 10:07 EPA 8015M ND 50 " " " " 11 10 11b (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgncg 1000 B1C'0815 03/26/21 12:17 FPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzene ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 " 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzenc ND 1.2 1,3-Dichlorobenzenc ND 1.2 1,4-Dichlorobenzenc ND 1.2 Dichlorodifluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1.1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 " trans-1,3-Dichloropropene ND 1.2 Fthylbcnzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Rcstdt RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene NI) 1.2 mg/kg 1000 B1C0815 03/26/21 12:17 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1.2-Tetrachloroethane NI) 1.2 I.1,2,2-Tetrachloroethane ND 1.2 'Forachlorocthcnc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2.4-Trichlorobenzene ND 1.2 1,1.1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane NI) 1.2 _ 1,23-Trichloropropane NI) 1.2 1,2.4-Trimethylbenzene ND 1.2 1.3.5-Trimethylbenzene NI) 1.2 vinvl chloride NI) 1.2 Xylencs (total) ND 1.2 Surrogate: Dihrornolluoromethanc 92 "„ (75 - 122) Surrogate: Toluene-dS 8-4 ( 66 - 128/ Surrogate: 4-13rumu1luuruherr_enc 92 "/„ (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 79 ( , � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg 1 B 1 C0907 03/26/21 14:41 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BIC 0810 03/26/21 13:36 EPA 6010B Arsenic 4.2 1.9 Barium 140 0.95 Bervllium 0.51 0.47 Cadmium ND 0.24 Chromium 52 0.47 Cobalt 16 0.47 Copper 23 0.95 Lead 7.0 0.47 Molybdenum ND 0.47 Nickel 72 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 33 1.9 " Zinc 20 1.9 " STLC Metals by ICP Chromium ND 0.10 ma/L 2 BID0007 04/01/21 14:48 STLC/EPA 6010B Volatile Organic TPH by GC/FID N-02 TPH Gasoline (C'5-C12) ND 4.6 mg/kg 1 BIC0802 03/26,'2111:39 EPA8015M R-07 Surrogate: 4-Bromo/lttorobell:Cne 104 `� (31 - 168) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 210184 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (('13-C22) ND 9.9 mg/kg 1 B1C0798 03/26/21 08:02 IIPA 8015M TPiI Motor Oil (C23-C40) ND 50 1. 11 11" 1. Surrogate: o-Teiphenpl 108 �-" (05 -133) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 79 r- Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg�kg 1000 B1C0815 03/26/21 12:43 ITA8260B Bromobenzene ND 1.2 Bromoehloromethane ND 1.2 Bromodichloromethanc ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 n-BuMbenzene ND 1.2 sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzene ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibrorno-3-chloropropane ND 1.2 1,2-Dibrotnoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzcnc ND 1.2 1,4-Dichlorobcnzcnc ND 1.2 Dichlorodifluoromcthanc ND 1.2 " Ll-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND L2 " 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I,1-Dichloropropane ND 1.2 " cis-1,3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 lithylbenzcne ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusaxom FAX: '805 925-3376 Page 13 of 79 r� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 1.2 mg/kg 1000 B1('0815 03/26/2112:43 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1.1,1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 lctrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobcn7cne ND 1.2 " 1,2,4-Trichloroben7ene ND 1.2 " 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichlomethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethanc ND 1.2 1,2.3-Trichloropropane ND 1.2 1,14-Trimethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride NI) 1.2 Xylencs (total) ND 1.2 Surrogate: Dibrcmtolluoromethone 92 rn ( 75 - Ill ) Surrogate: Toluene-d8 95 %, (66 - 128) " Surrogate. 90'Yo (76-122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Report! Analytical t Sample ID : Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg 1 B 1 C0807 03/26/21 14:44 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mgIg 1 B1C0810 03/26/21 13:38 EPA601013 - Arsenic 2.6 1.8 " Barium 5.8 0.92 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 6.9 0.46 " Cobalt 0.92 0.46 Copper 1.9 0.92 Lead 3.7 0.46 Molybdenum 2.6 0.46 - - Nickel 4.1 0.46 Selenium ND 1.8 Silver ND 0.46 " Thallium ND 0.92 Vanadium 4.6 1.8 "Zinc 6.8 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: 4-Brennq lnorohenzene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Tcrl)henYl 35 5.1 mg'kg 1 B 1 C0802 03/26/21 12:05 EPA 8015M 148"11, (31-168) 11 " 11 17 9.9 mglkg 1 72 50 " " 107S, (65-133) BIC0798 03/2621 11:03 EPA 8015M D-04 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID : Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BIC 0815 03/26/21 13:08 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofortn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobcnzenc ND 1.2 Chlorocthane ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropanc ND 1.2 1.2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-1)ichlorobenzene ND 1.2 13-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodilluoromethane ND 1.2 1. 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1. 1 -Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " I.3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1,1-Dichloropropane ND 1.2 cis- l3-Dichloropropenc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethvlbcnzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 79 rt ALMM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mg'kg I B 1('0807 03/26/21 14:46 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B 1('0810 03/26/21 13:41 EPA 6010B - • Arsenic 5.4 1.9 Barium 32 0.93 Beryllium ND 0.47 _ Cadmium ND 0.23 Chromium 15 0.47 " Cobalt 4.3 0.47 _ . Copper 11 0.93 Lead 8.3 0.47 Molybdenum 2.9 0.47 " _ Nickel 19 0.47 Selenium ND 1.9 Silver ND 0.47 _ Thallium ND 0.93 Vanadium 13 1.9 Zinc 19 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 35 4.9 mg/kg I BIC0802 03/26/21 12:31 FPA 8015M Surrogate: 4-Bromo/hrorohenzene 145 i'i, (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Terphem-1 11 10 mgIg 110 50 " " 106 `%, (65 - 133 ) B I C0798 0312621 11:31 EPA 8015M D-04 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical i Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R417 Benzene ND 1.2 mglkg 1000 B1('0815 03/26/21 13:34 EPA826013 Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chlorocthane ND 1.2 Chlomfonn ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 " 12-Dibromoethane (ED13) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 I.3-Dichlorobenzene ND 1.2 I A-Dichlorobenzene ND 1.2 Dichlorodifluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 12-Dichloroethane ND 1.2 l,1-Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 12-Dichloropropane ND 1.2 1,3-Dichoropropane ND 1.2 " 22-Dichloropropane ND 1.2 1.1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 11 exach lorobutadi ene ND 1.2 mg!kg 1000 B1('0815 03/26/21 13:34 EPA8200B 4-Isopropyl Toloene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1.2-Tetrachloroethane ND 1.2 1.1.2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 " Toluene ND 1.2 1,2,3-Trichloroben7cne ND 1.2 1.2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroetliene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 " 1,24-Trimethylbenzene ND 1.2 1,3,5-Tritnethylbeuzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Uihromofluoromethaue 95 40 ( 75 - 122) Surrogate: Toluene-dS 86 N, (66 - 128) Smrogute: d Brnnmllmruhen_cue 94 "i, (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 79 r A i rr w4ra Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical t Sample ID : Tank Bottom W. End Sampled: 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mglkg I B I C0807 03/26/21 14:48 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B1C0810 03/26/2113:44 EPA 601OB - Arsenic ND 2.0 Barium 9.9 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 8.0 0.49 Cobalt 1.2 0.49 Copper 1.6 0.98 Lead 3.4 0.49 Molybdenum 1.1 0.49 " Nickel 4.7 0.49 " Selenium ND 2.0 Silvcr ND 0.49 _ Thallium ND 0.98 Vanadium 5.9 2.0 Zinc 7.9 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: 4-BromnJhroroben_ene Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) TPH Motor Oil (C23-('40) Surrogate: o-Tetphen.vl 6.1 4.5 mgtkg 1 B1C0804 03/26/21 10:55 EPA 8015M 1O8 1�1; (31 - 168) 11 " 11 ND 9.9 mg!kg 1 BIC0798 03/26/21 10:21 EPA 9015M ND 50 " " " " " 106% (65-133) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report most be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 79 .( , Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by : Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GONIS R-07 Benzene ND 1.2 mg/kg 1000 BIC0815 03/26/21 13:59 EPA 8260B Bromobenzene ND 1.2 " Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Brotnofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcne ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 - ' 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-I)ichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 I A-Dichlorobenzene ND 1.2 Dichlorodilluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dicliloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 12-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I,1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 " trans- l,3-Dichloropropene ND 1.2 Etylbenzene ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 22 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by : Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg!kg 1000 BIC0815 03/26/2113:59 EPA8200B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2=retrachloroethane ND 1.2 Tetrachloroctliene (PCE) ND 1.2 Toluene ND 1.2 L2,3-Trichlorobenzcnc ND 1.2 1,2,4-Trichloroben7ene ND 1.2 1.1. 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 " Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3,5-Triniethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromofluororncthanc� 93 %) ( 75 - 122) Surrogate: Toluene-db' 88 ':', (66 - 128 ) 11 Surrogate: 4-Brumniluuruheu_ene 94 `%" ( 76 - 122) 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 23 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analvtical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by : Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg/kg 1 BIC0807 03/26/21 14:54 EPA 7471A Total Metals by ICP Antimony 8.2 2.4 mg/kg 1 B 1 C0810 03/26/21 13:47 EPA 601 OB Arsenic 8.9 1.9 " Barium 260 0.96 Beryllium ND 0.48 — Cadmium ND 0.24 Chromium 55 0.48 " N-02 Cobalt 12 0.48 — • Copper 120 0.96 Lead 550 0.48 " " " " " N-02 N-03 Molybdenum 1.1 0.48 Nickel 150 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 33 1.9 Zinc 720 1.9 STLC Metals by ICP Chromium 0.34 0.10 mg/l. 2 B I D0007 04/01 /21 14:40 STI.C/EPA 601 OB Lead 56 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.25 0.050 mg/l. 1 B 1 DO 112 04/06/21 12:18 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl1ent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: f805 925-3376 Page 24 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (('5-('12) ND 4.9 mg/kg 1 BIC0804 03/26'21 11:52 EPA 8015M R-07 ,-. Surrogate: 4-Bromo/laorohenzene 100 /, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 71 40 mg/kg 4 BIC0798 03/26'21 11:59 EPA 8015M D-04 TP11 Motor Oil (C23-C40) 520 200 1. 11 11 11D-04 Surrogate: o-Terphenrl 108 % (65 - 133) " " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples W Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg%kg 1000 B 1 C0815 03/26/21 14:25 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromotnethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 Chloroethanc ND 1.2 Chlorof'onn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (ED13) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 1,4-Dich1orobcn7cnc ND 1.2 Dichloroditluoromethanc ND 1.2 " 1,1-Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 " 1,1-Dichloroethene ND 1.2 cis-L2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropanc ND 1.2 13-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-13-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.eom FAX: 805 925-3376 Page 26 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical i Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Iiexachlorobutadiene ND 1.2 mg/kg 1000 BIC0815 03/26/21 14:25 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1.1.1.2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcnc (PCE.) ND 1.2 TOIUcnC ND 1.2 12,3-Trichlorobcn7ene ND 1.2 1,2,4-Trichloroben7ene ND 1.2 1. 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 L2.3-Trichloropropane ND 1.2 " 1.24-Trimethvlbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 " Surrogate: Uibronu{lltunynilc4haue 97 "i ( 75 - 122 ) Surrogate: Toluene-d,N 90 % ( 66.- 128 ) Surrogate: 4-Bronw. luo oben_ene NR'."' ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 Www.oecusa.com FAX: (805) 925-3376 Page 27 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mg/kg 1 BIC0807 03/26/2114:56 EPA 7471A Total Metals by ICP Antimony ND 2.4 mgkg 1 BIC0810 03/26/21 13:50 EPA 601OB Arsenic 4.1 1.9 Barium 180 0.96 Beryllium 0.53 OAS Cadmium ND 0.24 Chromium 78 0.48 N-02 Cobalt 16 0.48 Copper 31 0.96 Lead 37 0.48 Molybdenum ND 0.48 Nickel 100 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 47 1.9 Zinc 69 1.9 STLC Metals by ICP Chromium 0.25 0.10 mg/L 2 BID0007 04/01/21 14:51 STLC/EPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 4.7 mg/kg 1 BIC0804 03/26/21 12:20 EPA 9015M R-07 Surrogate: 4-Bromo/htoruhen_ene 107 ifi (31 - 168) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: (805) 925-3376 Page 28 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 27 9.9 r TPH Motor Oil (C23-C40) 610 50 Surrogate: o-TerphenYl 107 mgIg 1 B1('0798 03/26/21 13:02 I:PA8015M D-06 (65-133) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of 79 WI AL'114" aral'a Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0050 mg%kg 1 B I C0817 03/26/21 13:46 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodiehloromethane ND 0.0050 Brontoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 " Chloroethane ND 0.0050 Chloroform ND 0.0050 Chlorontethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-C'hlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1.2-Dibronio-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (EDB) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzenc ND 0.0050 13-Dichlorobenzenc ND 0.0050 1.4-Dichlorobenzenc ND 0.0050 Dichlorodifluoromcthanc ND 0.0050 I,1-Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 22-Dichloropropane ND 0.0050 I,1-Dichloropropene ND 0.0050 cis-1.3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 " Ethylbenzcne ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 30 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) 11exachIorobutadiene ND 0.0050 mg�kg 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " Styrene ND 0.0050 " 1. 1, 1,2-Tetrachloroethane ND 0.0050 " 1,1.2.2-1'etracliloroethane ND 0.0050 " TetrachloroelllCnC(PC:E) ND 0.0050 Toluene ND 0.0050 " 1,2,3-Trichlorobenzcnc ND 0.0050 " 1.2,4-Trichlorobenzene ND 0.0050 " 1, 1, 1 -Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 " Trichlorotluoromethane ND 0.0050 " 123-Trichloropropane ND 0.0050 12.4=rrimethylbenzene ND 0.0050 " 13,5-Trinrethylbenzene ND 0.0050 " Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 " Surrogate: Uihromu/luoromethanc 94 % ( 75 - 122 ) Surrogate: Toluenc,48 89 `';' ( 66 - 128 ) Surrogate: 4-Bromo/luorohen_ene 89 4;, ( 76 - 122 ) I B 1('0817 03/26/21 13:46 EPA 8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.14 0.095 mg!kg 1 B 1 C0807 03/26/21 14:58 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BIC0810 03/26/21 13:52 EPA 6010B — • Arsenic 5.9 1.9 " " " " Barium 170 0.97 " Bervllium 0.50 0.49 "^ Cadmium ND 0.24 Chromium 41 0.49 Cobalt 16 0.49 Copper 27 0.97 Lead 10 0.49 Molybdenum ND 0.49 —• Nickel 38 0.49 Selenium ND 1.9 Silver ND 0.49 Thallium ND 0.97 Vanadium 33 1.9 " Zinc 27 1.9 " Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.7 mglkg I BIC0804 03/26/2112:49 EPA8015M R-07 Surrogate: 4-Bronw la(mhenzene 96 % ( 31 - 168) 11 11" Semi -Volatile Organic TPH by GC/FID TPH Diesel (CI3-C22) ND 10 mg/kg I BIC0798 03.126/21 10:49 EPA 8015M ]'PH Motor Oil (C23-C40) 85 50 " " " " " Surrogate: o-Teihhenvl 105 io (65 - 133) 11" " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 805 925-3376 Page 32 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 BIC0817 03/26/21 14:44 EPA9260B Bromobenzene ND 0.0050 Brornochkxomethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tent-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzcnc ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 C'hloromethane ND 0.0050 " 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (ED13) ND 0.0050 " Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 I A-Dichlorobenzene ND 0.0050 Dichlorodifluoronethane ND 0.0050 " 1,1-1)ichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1.2-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 2,2-Dictiloropropaue ND 0,0050 " 1,1-Dichloropropene ND 0.0050 " cis- 1,3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 " Ethylbcnzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID : Control Sampled : 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method votes Volatile Organic Compounds by GUMS (Continued) Ilexachlorobutadiene ND 0.0050 mg'kg 1 BIC0817 03/26/2114:44 IPA8200B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1, 1, 1,2-Tetrachloroethane ND 0.0050 " 1,1,2.2-Tetrachlorocthane ND 0.0050 7ctrachlorocthcnc (PCE) ND 0.00.50 Toluene ND 0.0050 1,2,3-Trichlorobcn7cnc ND 0.0050 1,2,4-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethane (TCE) ND 0.0050 Trichlorolluoromethane ND 0.0050 1.2.3-Trichloropropane ND 0.0050 1,2,4-Trimethylbenzene ND 0.0050 " 1.3.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 X_vlencs (total) ND 0.0050 Surrogate:1)ihrunw/lrununuthmrr 93's, (75-122) " Surrogate: Toluene-d8 95 ' i, (66. 1 28) " Surrogate: 4-Bromofluorohe,t_ene 98 9s, ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 34 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Soil Pile N Sampled: 03/25/21 11:40 Matrix : Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7 Notes Total Metals by CVAA Mercury ND 0.099 mglkg 1 B 1 C0807 03/26/21 15:00 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I BIC0810 03/26/2113:55 EPA 6010B Arsenic 3.6 2.0 Barium 13 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 11 0.50 Cobalt 1.9 0.50 " ^, Copper 5.3 1.0 " Lead 4.3 0.50 Molybdenum 2.5 0.50 �. Nickel 9.0 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND LO Vanadium 8.4 2.0 Zinc 8.8 2.0 ' Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) 42 4.9 mg/kg 1 BIC0804 03/26,121 13:17 EPA 8015M Surrogate: 4-Bromufhroroheuzene 196 io (31 - 168) S-02 Semi -Volatile Organic TPH by GGFID TPII Diesel (C13-C22) ND 9.9 mg/kg 1 BIC0798 03/26/21 10:35 EPA 8015M TPH Motor Oil (C23-C40) 52 50 " " " " " Surrogate: o-Teipherml lllh'%;, (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Sampled by : Matrix: Solid Field Data: NA Lab ID : 2101841-10 Analyte Result RL Units Dilution Batch Analyzed Method 'Fates Volatile Organic Compounds by GUMS R-07 Benzene ND 0.045 mglkg 1 B1('0817 03/26/21 12:49 EPA8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 Broniofarm ND 0.045 Bromomethane ND 0.045 n-Bulvibenzene 0.22 0.045 " see-Butylbenzene 0.11 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 Chloroethane ND 0.045 Chloroform ND 0.045 C'hloromcthanc ND 0.045 2-C'hlorutoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 1,2-Dibromo-3-chloropropanc ND 0.045 1.2-Dibromoethane (EDB) ND 0.045 Dibromoniethane ND 0.045 " 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobenzene ND 0.045 1.4-Dichlorobenzene ND 0.045 Dichlurodilluoromelltane ND 0.045 1,1-Dichlorocthanc ND 0.045 1,2-Dichloroethene ND 0.045 1, 1 -Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloroprupane ND 0.045 1.3-Dichloroprupane ND 0.045 2.2-Dichloroprupane ND 0.045 1,1-Dichloroprupene ND 0.045 cis-1.3-I)ichloropropene ND 0.045 trans-1,3-Nchloropropene ND 0045 " Ethylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Sample ID : Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg.lkg 1 B1('0817 03/26/2) 12:49 EPA9260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 ., Naphthalene ND 0.045 n-Propylbenzene 0.15 0.045 " Styrene ND 0.045 1, 1, 1.2-Tetrachloroethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachloroethene (PCE) ND 0.045 " Toluene ND 0.045 1,23-Trichlorobenzene ND 0.045 1,2.4-Trichlorobenzene ND 0.045 1,1.1-Trichloroethane ND 0.045 1,1.2-Trichlorocthane ND 0.045 Trichloroethene (7'CE) ND 0.045 " Trichlorotluoromethane ND 0.045 - 1,23-Trichloropropanc ND 0.045 " 1,2.4-Trimethylbenzene ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: Dibranzojluoromethanc• 92 75 - 122) Surrogate: luluc'nc-ds 47'%b ( 66 - 128 ) Surrogute: 4-Bromolhiorobenzene 99 % (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101941 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical t MEMO Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID: 2101841-11 Field Data: NA Anaiyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mg/kg 1 B 1('0807 03/26/2) 15:02 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mglkg I B 1 C0910 03/26/21 14:06 EPA 6010B Arsenic 4.5 2.0 " Barium 47 H) Beryllium ND 0.50 Cadmium f ND 0.25 Chromium 18 0.50 Cobalt 3.6 0.50 Copper 9.8 H) Lead 16 0.50 Molybdenum 2.1 0.50 Nickel 36 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 " " Vanadium 15 2.0 Zinc 29 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4A mgIg 1 BIC0804 03/20/21 13:46 EPA 8015M R-47 Srn ragcge: 4-Brom,/luorohen-cne 100 11 o (31 - 168) Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-C22) ND 10 mglkg 1 B1('0798 03/26/21 12:27 EPA 8015M TPH Motor Oil (C23-C40) 260 50 " " " Srn•rugale: o-K'J phem'1 108,16 (65 - 1.33) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 38 of 79 6 ' Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0049 mg%kg I B 1 C0817 03/26/21 15:13 EPA 826013 Bromobenzene ND 0.0049 Bromochloromethane ND 0.0049 Bromodichloromethane ND 0.0049 • Bromoform ND 0.0049 Bromomethane ND 0.0049 " n-Butvlbenzene ND 0.0049 sec-Butylbenzene ND 0.0049 tort-Butylbenzene ND 0.0049 Carbon tetrachloride ND 0.0049 Chlorobenzcnc ND 0.0049 " Chloroethane ND 0.0049 Chloroform NT) 0.0049 Chloromethane ND 0.0049 - 2-Chlorotoluenc ND 0.0049 4-Chlorotoluene ND 0.0049 Dibroinochloromethane ND 0.0049 1.2-Dibronio-3-chloropropane ND 0.0049 " 1,2-Dibrontoethane (EDB) ND 0.0049 Dibromomethane ND 0.0049 12-Dichloroben7ene ND 0.0049 - 1.3-Dichlorobenzene ND 0.0049 14-Dichlorobenzene ND 0.0049 Dichlorodifluoromcthanc ND 0.0049 I,I-Dichloroethane ND 0.0049 1,2-Dichloroethane ND 0.0049 LI-Dichloroethene ND 0.0049 . - cis-1.2-Dichloroethene ND 0.0049 " trans-1,2-Dichloroethene ND 0.0049 " 1,2-Dichloropropane ND 0.0049 13-Dichloropropane ND 0.0049 22-Dichloropropane ND 0.0049 1, 1 -Dichloropropene ND 0.0049 cis-L3-Dichloropropene ND 0.0049 trans-1,3-Dichloropropene ND 0.0049 Ethylbcnzenc ND 0.0049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 _ www.oecusa.com FAX: (805) 925-3376 Page 39 of 79 G A M, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Ilexachlornbutadiene ND 0.0049 mg%kg 1 B1('0817 03/26/21 15:13 17PA8260B 4-Isopropyl Toluene ND 0.0049 " Isopropylbenzene ND 0.0049 Methylene chloride ND 0.0049 _. Naphthalene ND 0.0049 n-Propylbenzene ND 0.0049 Styrene ND 0.0049 " 1,1,1,2-1'etrachloroethane ND 0.0049 1,1,2.2-Tetrachloroethane ND 0.0049 Tetrachlorocthcne 1PCE) ND 0.0049 Toluene ND 0.0049 - 1,2,3-Trichlorobenzene ND 0.0049 1,14-Trichloroben7ene ND 0.0049 1,1,1-Trichloroethane ND 0.0049 - 1,1,2-Trichloroethane ND 0.0049 Trichloroethene (TCE) ND 0.0049 Trichlorofluoromethane ND 0.0049 1,23-Trichloropropane NI) 0.0049 1.2,4-Trimethylbenzene ND 0.0049 1,35-Trimethylbenzene ND 0.0049 Vinyl chloride ND 0.0049 Xylenes(total) ND 0.0049 Surrogate: Dihrunrulhun w,rrtlur», 91 In' ( 75 - 122 ) Surrogate: Toluene-dS 95 "„ ( 66 - 128 ) Surrogate: 4-Bro»roJlaurohrn_cnr 97 N,, ( 76- 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mg -kg 1 BIC0807 03/26/21 15:04 FPA7471A Total Metals by ICP Antimony ND 2.3 mgtkg 1 BIC0810 03/26/21 14:09 EPA 6010B Arsenic 5.6 1.9 Barium 23 0.93 Beryllium ND 0.47 - Cadmium ND 0.23 Chromium 14 0.47 Cobalt 2.5 0.47 Copper 6.8 (1.93 Lead 73 0.47 Molybdenum 3.7 0.47 Nickel 11 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 15 1.9 " Zinc 15 1.9 Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) ND 4.7 mglkg 1 BIC0804 03/26/21 14:14 EPA 8015M R-07 Surrogate: 4-Bronm/1noroben_cne 103 %, (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 9.9 mg`kg 1 B1('0798 0312621 11:17 EPA 8015M - 'TPH Motor Oil (C23-C40) 75 50 " "11" U-04 Surrogate: o-liv-phe•md 1117%& (65 - 133 I The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805] 925-3376 Page 41 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0050 mglkg 1 BIC0817 03/26/21 15:43 EPA8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Brornodichloromethane ND 0.0050 Bromoform ND 0.0050 " Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzcnc ND 0.0050 Chloroethanc ND 0.0050 Chlorotbnn ND 0,0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 " Dibromochloromethanc ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (E )B) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 " 1,4-Dichlorobenzene ND 0.0050 Dichlorodilluoromethanc ND 0.0050 1,1-Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 13-Dichloropropane ND 0.0050 22-Dichloropropane ND 1L0050 LI-Dichloropropene ND 0.0050 cis- 1.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 I-'thylbcnzcnc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecLisa .corn FAX: 805) 925-3376 Page 42 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 I Analytical Report for Samples Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.090 mgtkg 1 B 1 C0807 03/26/21 1.5:06 EPA 7471 A Antimony ND 2.4 mgikg 1 BIC0810 03/26�21 14:11 EPA 6010B Arsenic 2.0 1.9 Barium 5.5 0.96 Beryllium ND 0.48 r• Cadmium ND 0.24 Chromium 6.4 0.49 Cobalt 0.76 0.48 _.. Copper 1.8 0.96 Lead 3.7 0.48 Molybdenum 1.6 0.48 Nickel 3.9 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 5.2 1.9 Zinc 5.2 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) ND 4.9 mg/kg 1 B I C0804 03/26/21 14:42 EPA 8015M R-07 Surrogate: 4-Bronv) luorobc•n_cne 102 % (.31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-('22) ND 10 mg`kg 1 B1C0798 03/26 21 11:45 EPA 8015M TP11 Motor Oil (C23-C40) 120 50 " " " " " Surrogate: o-Tcgphcnr( 107 ;'o (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by : Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 BIC 0817 03/26/21 16:12 EPA 8260B �Broinobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 - Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butvlbenzene ND 0.0050 r sec-Butylbenzene ND 0.0050 " tort-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobcnzenc ND 0.0050 Chloroetbane ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0,0050 " DibromochIorometbane ND 0.0050 �. 1,2-Dibromo-3-chloropropane ND 0.0050 1.2-Dibromoethane (ED13) ND 0.0050 Dibromomethane ND 0.0050 12-Dichlorobenzene ND 0.0050 1.3-Dichlorobcnzene ND 0.0050 1,4-Dichlorobcnzcnc ND 0.0050 Dichlorodilluoromethane ND 0.0050 1, 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 l,l-Dichloroethene ND 0.0050 cis- 1,2-Dichloroetlien e ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 12-Dichloropropane ND 0.0050 " 1.3-Dichloropropane ND 0.0050 " 22-Dichloropropane ND 0.0050 1. 1 -Dichloropropene ND 0.0050 cis- 1.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Ethylbenzcnc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 45 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by : Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) llexachlorobutadiene ND 0.0050 mgtkg 1 BIC0817 03/26/2110:12 EPA8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " Styrene ND 0.0050 1,1.12-TetrachIoroethatie ND 0.0050 1.12,2-Tetrachloroethane ND 0.0050 Tetrachlorocthene (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobcnzenc ND 0.0050 1,2,4-Trichlorobenzene ND 0.0050 1,1,1-Trichloroethane ND 0.0050 I.1,2-Trichloroethane ND 0.0050 Trichloroethene (TC'E) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2,3-Trichloropropane ND 0.0050 " 12,4-Trimethylbenzene ND 0.0050 13,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: Dibronu{fluoromethane 91 % ( 75 - 122 ) Surrogate: Toluene-ds 95 /, ( 66- 128 ) Surrogate: 4-BromoJluoroben_ene 97 4,, ( 76- 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 805 925-3376 Page 46 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlCO807 - EPA 7471A Preparation: EPA 7471A Prep 03/26/21 07:43 Blank (B1C0807-BLK1) Analyzed: 03/26/21 13:21 Mercury ND 0.10 mg/kg LCS (BlC0807-BS1) Analyzed: 03/26/21 13:17 N4crcury 0.792 0.10 mg/kg 0.833 95 85-115 LCS Dup (BlC0807-BSDI) Analyzed: 03/26/21 13:19 Mercury 0.783 0.10 mg/kg 0.833 94 85-115 1 20 Duplicate (BlC0807-DUPI) Source: 2101842-02 Analyzed: 03/26/21 13:25 Mercury 0.0556 0.096 mg/kg 0.0554 0.3 20 Matrix Spike (B1C0807-MSl) Source: 2101842-02 Analyzed: 03/26/21 13:27 Mercury 0.855 0.096 mg/kg 0.796 0.0554 100 75-125 Matrix Spike Dup (B1C0807-MSD1) Source: 2101842-02 Analyzed: 03/26/21 13:29 Mercury 0.750 0.087 mg/kg 0.727 0.0554 96 75-125 13 20 Post Spike (B1C0807-PSI) Source: 2101842-02 Analyzed: 03/26/21 13:31 Mercury 5.17 ug/L 5.00 0.347 97 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 'Fotal Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Blank (B1C0810-BLK1) Analyzed: 03/26/21 12:16 Antimony ND 2.5 mg1kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 Cobalt ND 0.50 " Copper ND 1.0 Lead ND 0.50 " Molybdenum ND 0.50 Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 LCS (BlC0810-BSI) Analyzed: 03/26/21 12:40 Antimony 100 2.5 mg!kg 100 100 80-120 Arsenic WI 2.0 100 101 80-120 Barium 102 1.0 100 102 80-120 Beryllium 103 0.50 100 103 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 103 0.50 100 103 80-120 Cobalt 103 0.50 100 103 80-120 " Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 100 0.50 100 100 80-120 Nickel 103 0.50 100 103 80-120 Selenium 100 2.0 100 100 80-120 Silver 5.06 0.50 5.00 101 80-120 Thallium 104 1.0 100 104 80-120 - Vanadium 100 2.0 100 100 80-120 Zinc 103 2.0 100 103 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: {805) 925-3376 EM Page 48 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Matrix Spike (B1C0810-MS1) Source: 2101840-03 Analyzed: 03/26/21 12:45 Antimony 49.8 2.4 mg/kg 97.6 ND 51 10-116 Arsenic 100 2.0 97.6 3.12 100 77-121 Barium 196 0.98 97.6 116 82 30-169 Beryllium 98.3 0.49 97.6 ND 101 96-111 Cadmium 93.4 0.24 97.6 ND 96 81-112 Chromium 113 0.49 97.6 17.6 97 75-129 .._ Cobalt 96.4 0.49 97.6 4.26 94 71-121 Copper 106 0.98 97.6 8.79 100 68-135 Lead 98.5 0.49 97.6 5.56 95 72-121 Molybdenum 89.8 0.49 97.6 1.27 91 70-112 ' Nickel 111 0.49 97.6 23.4 90 73-121 Selenium 94.7 2.0 97.6 ND 97 76-Ilo Silver 4.74 0.49 4.88 ND 97 54-132 Thallium 91.2 0.98 97.6 ND 93 64-120 Vanadium 112 2.0 97.6 15.4 99 78-124 Zinc 122 2.0 97.6 29.6 95 50-143 Matrix Spike Dup (B1C0810-MSD1) Source: 2101840-03 Analyzed: 03/26/21 12:55 Antimony 48.3 2.5 mg/kg 98.0 ND 49 10-116 3 20 Arsenic 102 2.0 98.0 3.12 101 77-121 1 20 Barium 203 0.98 98.0 llli 89 30-169 4 20 - Bervllium 99.4 0.49 98.0 ND 101 86-111 1 20 Cadmium 95.0 0.25 98.0 ND 97 81-112 2 20 Chromium 117 0.49 98.0 17.6 101 75-129 4 20 Cobalt 98.2 0.49 98.0 4.26 96 71-121 2 20 Copper 110 0.98 98.0 8.79 103 68-135 3 20 Lead 100 0.49 98.0 5.56 97 72-121 2 20 Molybdenum 91.3 0.49 98.0 1.27 92 70-112 2 20 Nickel 113 0.49 98.0 23.4 92 73-121 2 20 Selenium 96.4 2.0 98.0 ND 98 76-116 2 20 Silver 4.89 0.49 4.90 ND 100 54-132 3 20 Thallium 93.1 0 98 98.0 ND 95 64-120 2 20 Vanadium 115 2.0 98.0 15.4 102 78-124 3 20 Zinc 124 2.0 98.0 29.6 96 50-143 1 20 The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 Www.oecusa.com FAX: 805 925-3376 Page 50 of 79 -("9�3�00 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total' - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Post Spike (B1C0810-PS1) Source: 2101840-03 Analyzed: 03/26/21 12:58 Antimony 1.97 mg/L 2.00 0.0203 98 75-125 Arsenic 2.08 2.00 0.0657 101 75-125 Barium 4.38 2.00 2.43 97 75-125 Beryllium 1.99 2.00 0.00456 99 75-125 Cadmium 1.89 2.00 -0.00476 94 75-125 Chromium 2.37 2.00 0.370 100 75-125 Cobalt 1.97 2.00 0.0898 94 75-125 Copper 2.25 2.00 0.185 103 75-125 Lead 2.02 2.00 0.117 95 75-125 Molybdenum 1.98 2.00 0.0268 98 75-125 Nickel 2.37 2.00 0.492 94 75-125 Selenium 1.97 2.00 0.000298 98 75-125 Silver 0.0974 0.100 -0.00288 97 75-125 Thallium 1.88 2.00 -0.0363 94 75-125 ~ Vanadium 2.30 2.00 0.324 99 75-125 Zinc 2.50 2.00 0.023 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAK: %805) 925-3376 Page 51 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 STLC Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0007 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/01/21 09:01 Blank (B1D0007-BLKI) Analyzed: 04/01/21 14:11 Chromium ND 0.050 111g/1. Lead ND 0.050 " LCS (B1D0007-BSI) Analyzed: 04/01/21 14:24 Chromium 9.98 0.050 mg/L 10.0 100 80-120 Lcad 10.0 0.050 1110.0 100 80-120 LCS Dup (B1D0007-BSD1) Analyzed: 04/01/21 14:27 Chromium 9.89 0.050 mg/L 10.0 99 80-120 0.9 20 Lead 9.90 0.050 1110.0 99 80-120 2 20 Duplicate (B1D0007-DUPl) Source: 2101841-07 Analyzed: 04/01/21 14:42 Chromium 0.341 0.10 mg/L 0.342 0.3 20 Lead 58.7 0.10 1156.1 4 20 Leach Fluid Blank (B1D0007-LBK1) Analyzed: 04/01/21 14:13 Chromium ND 0.10 mg/L Lead ND 0.10 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cI!ent.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 52 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 i Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0112 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/06/21 10:26 Blank (B1D0112-BLKI) Analyzed: 04/06/21 12:08 Lcad ND 0.050 mg/L LCS (B1D0112-BSI) Analyzed: 04/06/21 12:13 ' Lead 9.64 0.050 mg/L 10.0 96 80-120 LCS Dup (B1D0112-BSD1) Analyzed: 04/06/21 12:16 Lcad 9.78 0.050 mg/L 10.0 98 80-120 1 20 Duplicate (B1D0112-DUP1) Source: 2101841-07 Analyzed: 04/06/21 12:21 Lead 0.242 0.050 mg/l. 0.246 2 20 Leach Fluid Blank (B1D0112-LBKI) Analyzed: 04/06/21 12:11 Lcad ND 0.050 mg/L The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 53 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic TPH by 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0802 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:22 Blank (BlC0802-BLKI) Analyzed: 03/26/21 08:30 TPI I Gasoline (C5-(' 12) ND 0.50 mg/kg Surrogate:4-Bromo/luorohensene 0.127 " 0.125 101 31-168 LCS (B1C0802-BS1) Analyzed: 03/26/21 06:59 TPII Gasoline (C5-C12) 1.01 0.50 mg/kg 1.00 WI 62-151 Surrogate:4-Bronto/laorohenzeni, 0.152 " 0.125 121 31-168 LCS Dup (B1C0802-BSDI) Analyzed: 03/26/21 07:25 TPHGasoline (C5-C12) 0.958 0.50 mg/kg 0.996 96 62-151 5 20 Surrogate: 4-13ronmlluorohen- ne 0.142 0.125 114 31-168 Duplicate (B1C0802-DUPI) Source: 2101840-01 Analyzed: 03/26/21 09:29 TPH Gasoline (('5-('12) ND 0.50 mg/kg ND 20 Surrogate:4-Bronin/luorobenzenc 0.131 " 0.124 105 31-16S Matrix Spike (BlC0802-MS1) Source: 2101836-04 Analyzed: 03/26/21 16:07 TPH Gasoline (C'5-C12) 0.989 0.50 mg/kg 1.00 ND 99 10-166 Surrogate:4-BromoJlumt)henrene 0.146 " 0126 116 31-168 Matrix Spike Dup (BIC0802-MSD1) Source: 2101836-04 Analyzed: 03/26/21 16:33 TPH Gasoline (C5-('l2) 0.971 0.50 mg/kg 0.992 ND 98 10-I66 2 20 Surrogate: 4-Brotnoluorohenzene 0.149 0.124 120 31-168 Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Blank (Bl C0804-BLK1) Analyzed: 03/26/21 10:27 TPH Gasoline (C'5-('12) ND 0.50 nig/kg Surrogate:4-BromgPuborohenzene 0.133 110.125 107 31-168 LCS (B1C0804-BSI) Analyzed: 03/26/21 09:30 TPH Gasoline (('5-('12) 1.24 0.50 mg/kg 0.998 124 62-151 Surrogate:4-Bromolbtorohc.tizene 0.147 110.125 118 31-168 LCS Dup (B1C0804-BSD1) Analyzed: 03/26/21 09:59 TPH Gasoline (C5-('121 1.32 0.50 mg/kg 0.998 132 62-151 7 20 Szrrogate:4-Bromollttorohen_ene 0.164 0.125 131 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 wvvw.oecusa.com FAX: (805) 925-3376 Page 54 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Semi -Volatile Organic TPH by 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0798 - EPA 8015M Preparation: EPA 3550C 03/25/21 17:29 Blank (B1C0798-BLK1) Analyzed: 03/26/21 07:35 TPII Diescl (C13-C22) ND 10 mg/kg TPII Motor Oil (C'23-C'40) ND 50 " Surrogate: o-Telphel(1-1 53.7 1149.8 /08 65-133 LCS (BlC0798-BSI) Analyzed: 03/26/21 07:07 TPH Diesel (C13-C22) 508 9.9 mgtkg 496 102 77-114 TPH Motor Oil (('23-C40) 549 50 496 111 76-128 Surrogate: o-Tcq)henyl 50.7 49.6 102 65-133 LCS Dup (BlC0798-BSDI) Analyzed: 03/26/21 07:21 TPII Diesel (CI3-C22) 501 9.9 mg/kg 497 101 77-114 1 20 TPH Motor Oil (C'23-C40) 557 50 497 112 76-128 2 20 Surrogate: o-TerphenYl 53.5 49.7 108 65-133 Duplicate (BlC0798-DUPl) Source: 2101840-01 Analyzed: 03/26/21 08:44 TPH Diesel (C13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) 43.1 50 44.8 4 20 Surrogate. o-Teiphern•l 53.4 49.8 107 65-133 Matrix Spike (BlC0798-MS1) Source: 2101840-01 Analyzed: 03/26/21 13:48 TPH Dicscl (C13-('22) 507 9.9 mg!kg 497 ND 102 45-149 TPH Motor Oil (('23-C40) 556 50 497 44.8 103 34-175 - Surrogate: o-Tecphen•l 55.9 49.7 113 65-133 Matrix Spike Dup (B1C0798-MSD1) Source: 2101840-01 Analyzed: 03/26/21 14:02 TPH Diesel (CI 488 10 mg'kg 499 ND 98 45-149 4 20 • TPII Motor Oil (('23-C40) 548 50 499 44.8 101 34-175 1 20 Surrogate: o-Tc,lphenrl 552 49.9 111 65-133 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 56 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 - Blank (B1C0815-BLK1) Analyzed: 03/26/21 11:26 Benzene ND 0.25 mg!kg Bromobenzene ND 0.25 " Bromochloromethanc ND 0.25 " ^ Bromodichloromethane ND 0.25 " Bromofurm ND 0.25 " Bromotnethane ND 0.25 �. n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 " Carbon tetrachloride ND 0.25 " Chlorobenzene ND 0.25 Chloroethane ND 0.25 Chloroform ND 0.25 " Chloromethane ND 0.25 _ 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene ND 0.25 Dibromochloromethane ND 0.25 " 1,2-Dibromo-3-chloropropane ND 0.25 1,2-Dibromoethane (EDB) ND 0.25 " Dibromomcthanc ND 0.25 1,2-Dichlorobenzenc ND 0.25 " -' 0-Dichlorobenzenc ND 0.25 1,4-Dichlorobenzene ND 0.25 " Dichloroditluoromethane ND 0.25 " 1,1-Dichloroethane ND 0.25 1,2-Dichloroethane ND 0.25 1,1-Dichloroethene ND 0.25 " cis-1,2-Dichloroethene ND 0.25 • trans-1,2-Dichloroethene ND 0.25 1,2-Dichloropropane ND 0.25 1,3-Dichloropropane ND 0.25 " 12-Dichloropropane ND 0.25 1,1-Dichloropropene ND 0.25 " cis- 1.3 -Dichloropropene ND 0.25 " trans-1,3-Dichloropropene ND 025 Ethylbenzenc ND 0.25 " Hexachlorobutadiene ND 0.25 " 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 " Methylene chloride ND 0.25 " Naphthalene ND 0.25 n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 57 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Coinpounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 �• Blank(B1C0815-BLKI) Analyzed: 03/26/21 11:26 Styrene ND 0.25 mgrkg 1,1,1,2-Tetrachloroethane ND 0.25 1,1.2,2-1'ctrachlorocthane ND 0.25 Tetrachloroethene 1PCE) ND 0.25 " Toluene ND 0.25 " 1,2,3-Trichlorobenzene ND 0.25 " ,.. 1,2.4-•Trichlorobenzene ND 0.25 " 1, 1, 1 -Trichloroethane ND 0.25 1,1,2-Trichloroethane ND 0.25 " Trichloroethene (TC'E) ND 0.25 Trichlorotluoromethane ND 0.25 1,2,3-Triehloropropane ND 0.25 1,24-Trimethylbenzene ND 0.25 " 1,3,5-Trimethylbenzene ND 0.25 Vinv] chloride ND 0.25 " Xylenes (total) ND 0.25 " Surrogate: Uihrvunq/luurrmtethunr 0.0445 0.0498 89 75-122 - Surrogate: Toluene-d8 0.0455 0.0498 91 66-128 Sm•ro ate: 4-Bromo/hroroben_enr 0.0479 0.0498 96 76-122 LCS (B1C0815-BSI) Analyzed: 03/26/21 09:44 - Benzene 1.80 0.25 mg kg 1.99 91 75-131 Bromobenzene 1.97 0.25 1.99 99 75-136 Bromochloromcthanc 1.67 0.25 1.99 84 70-135 Bromodichloromethane 1.84 0.25 1.99 93 76-137 Bromofonn 1.68 0.25 1.99 85 55-139 Bromonrethane 1.49 0.25 1.99 75 10-157 u-Butylbenzene 2.38 0.25 1.99 120 62-166 sec-Butylbenzene 2.50 0.25 1.99 126 72-167 tort-Butylbenzene 2.33 0.25 1.99 117 69-158 Carbon tetrachloride 1.77 0.25 1.99 89 70-140 C'hlorobenzene 1.94 0.25 1.99 98 76-137 - * Chloroethane 2.09 0.25 1.99 105 10-164 C'hlorotbrm 1.80 0.25 1.99 91 75-123 Chloromethane 1.73 0.25 1.99 87 26-146 2-Chlorotoluene 2.11 0.25 1.99 106 73-145 4-C'hlorutoluene 2.13 0.25 1.99 107 67-151 Dibromochloromethane 1.80 0.25 1.99 90 68-144 12-Dibromo-3-chloropropane 1.63 0.25 1.99 82 45-148 1,2-Dibromoethane (EDB) 1.80 0.25 1.99 91 73-134 Dibromomethanc 1.66 0.25 1.99 84 70-140 1,2-Dichlorobenzene 2.15 0.25 1.99 108 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 58 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic CompoundsQuality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS (BlC0815-BS1) Analyzed: 03/26/21 09:44 1,3-Dichlorobenzenc 2.19 0.25 mg/kg 1.99 110 76-146 1,4-Dichlorobenzene 2.10 0.25 1.99 106 72-140 Dichloroditluoromcthanc 1.73 0.25 1.99 87 10-166 1, 1 -Dichloroethane 1.82 0.25 1.99 92 65-139 1,2-Dichlorocthanc 1.90 0.25 1.99 90 67-125 1,1-Dichloroethene 2.05 0.25 1.99 103 54-168 cis-1,2-Dichloroethene 1.80 0.25 1.99 91 74-135 trans-1,2-Dichloroethene 1.98 0.25 1.99 100 68-149 1,2-Dichloropropane 1.77 0.25 1.99 89 74-130 1.3-Dichloropropane 1.83 0.25 1.99 92 68-130 " 2,2-Dichloropropane 1.95 0.25 1.99 98 33-187 1,1-Dichloropropene 1.95 0.25 " 1.99 98 71-140 cis-1,3-Dichloropropene 1.79 0.25 1.99 90 78-135 trans-1,3-Dichloropropene 1.90 0.25 1.99 96 70-137 -- Ethylbenzene 1.93 0.25 1.99 97 69-143 Hexachlorobuladiene 3.12 0.25 1.99 157 69-203 4-Isopropyl Toluene 2.38 0.25 1.99 120 74-154 Isopropylbenzene 2.11 0.25 1.99 106 72-157 Methylene chloride 1.75 0.25 1.99 88 49-129 Naphthalene 1.84 0.25 1.99 93 61-158 n-Propylbenzene 2.17 0.25 1.99 109 69-147 Styrenc 1.92 0.25 1.99 97 71-144 1,1,1,2-Tetrachlorocthane 1.92 0.25 1.99 97 78-132 1,1,2,2-'I'ctracltloroethanc 1.90 0.25 1.99 96 64-138 Tetrachloroethene(PCE) 2.09 0.25 1.99 105 74-145 Tolucnc 1.82 0.25 1.99 92 76-131 1,2,3-Trichlorobenzene 2.11 0.25 1.99 106 63-170 1,2,4-Trichlorobenzene 2.20 0.25 1.99 1 W 71-165 - 1,1,1-Trichloroethane 1.97 0.25 1.99 99 74-137 1,1,2-Trichloroethane 1.82 0.25 1.99 91 68-134 Trichloroethene (TCE) 1.94 0.25 1.99 98 79-139 Trichlorotluoromethane 2.20 0.25 1.99 111 32-154 L2,3-Trichloropropane 1.77 0.25 1.99 89 69-125 L2.4-Trimethylbenzene 2.14 0.25 1.99 108 67-144 1,3.5-Trimethylben7ene 2.17 0.25 1.99 109 66-154 _ Vinyl chloride 2.27 0.25 1.99 114 39-150 Xylenes (total) 5.95 0.25 5.96 100 71-147 Surrogate: Dibrontgiluurumcthune 0.0496 0.0497 100 75-122 Surrogate: Toluene-ds 0.0462 0.0497 93 06-128 Surrogate: d-Bromol/uorohen_ene 0.0451 0.0497 91 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 59 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Coinpounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (B1CO815-BSDI) Analyzed: 03/26/21 10:09 Benzene 1.87 0.25 mg -kg 2.00 94 75-131 4 20 Bromobenzene 2.02 0.25 2.00 101 75-136 2 20 Bromochloromethanc 1.69 0.25 2.00 85 70-135 2 20 Bromodichloromethane 1.93 0.25 2.00 97 76-137 5 20 Bromol'orm 1.80 0.25 2.00 90 55-139 7 20 Bromomethane 1.21 0.25 2.00 61 10-157 20 20 n-Butylbenzene 2.45 0.25 2.00 123 62-166 3 20 sec-Butylbenzene 2.48 0.25 2.00 124 72-167 0.9 20 tert-Butylbenzene 2.39 0.25 2.00 119 69-158 2 20 Carbon tetrachloride 1.87 0.25 2.00 94 70-140 6 20 Chlorobenzene 2.07 0.25 2.00 104 76-137 7 20 Chloroethane 2.21 0.25 2.00 111 10-164 6 20 Chloroform 1.81 0.25 2.00 90 75-123 0.4 20 Chloromethane 1.82 0.25 2.00 91 26-146 5 20 2-Chlorotoluene 2.26 0.25 2.00 113 73-145 7 20 4-Chlorotoluene 2.25 0.25 2.00 112 67-151 5 20 Dibromuchloromethane 1.97 0.25 2.00 98 68-144 9 20 1,2-1)ibromo-3-chloropropane 1.84 0.25 2.00 92 45-148 12 20 1.2-Dibromoethane (L^DB) 1.98 0.25 2.00 99 73-134 9 20 Dibromomethunc 1.75 0.25 2.00 87 70-140 5 20 1,2-Dichlorobenzene 2.18 0.25 2.00 109 78-142 1 20 0-Dichlorobenzene 2.30 0.25 2.00 115 76-146 5 20 1,4-Dichlorobenzene 2.06 0.25 2.00 103 72-140 2 20 DichlorodiFluoroniethanc 1.73 0.25 2.00 86 10-166 0.1 20 1.1-Diehloroethene 1.95 0.25 2.00 98 65-139 7 20 1.2-Dichloroethanc 1.93 0.25 2.00 96 67-125 7 20 1.1-Diehloroethene 2.07 0.25 2.00 103 54-168 O16 20 cis-12-Diehloroethene 1.86 0.25 2.00 93 74-I35 4 20 trans-1,2-Diehloroethene 2.11 0.25 2.00 105 68-149 6 20 1,2-Dichloropropane 1.82 0.25 2.00 91 74-130 3 20 1,3-Dichloropropane 1.84 0.25 2.00 92 68-130 0.6 20 2,2-Dichloropropane 1.94 0.25 2.00 97 33-187 0.4 20 1,1-Dichloropropene 2.04 0.25 2.00 102 71-140 5 20 cis- 1,3-Dichloropropene 1.80 0.25 2.00 90 78-135 0.5 20 trans-1,3-Dichloropropene 1.94 0.25 2.00 97 70-137 2 20 Ethvlbenzene 2.06 0.25 2.00 103 69-143 6 20 1iexachlorobutadiene 3.30 0.25 2.00 165 69-203 6 20 4-Isopropyl Toluene 2.42 0.25 2.00 121 74-154 2 20 Isopropylbenzene 2.19 0.25 2.00 109 72-157 3 20 A'lethylene chloride 1.87 0.25 2.00 94 49-129 7 20 Naphthalene 2.04 0.25 2.00 102 61-158 1O 20 n-Propylbenzene 2.30 0.25 2.00 115 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilepi Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 - LCS Dup (B1C0815-BSDl) Analyzed: 03/26/21 10:09 Styrene 2.06 0.25 mg/kg 2.00 103 71-144 7 20 1,1,1.2-Tetrachloroethane 2.04 0.25 2.00 102 78-132 6 20 1,1,2,2-Tetrachloroethane 2.02 0.25 2.00 101 64-138 6 20 Tetrachloroethene(PCE) 2.18 0.25 2.00 109 74-148 4 20 TOInC11C 1.91 0.25 " 2.00 96 76-131 5 20 1,2,3-Trichlorobenzene 2.36 0.25 2.00 118 63-170 12 20 12,4-Trichlorobenzene 2.37 0.25 2.00 118 71-165 7 20 1,1,1-Trichloroethane 1.98 025 2.00 99 74-137 0.8 20 1.1,2-Trichloroethane 1.92 0.25 2.00 96 68-134 6 20 Trichloroethene (TCE) 1.92 025 2.00 96 79-139 0,9 20 �- Trichlorolluoromethane 2.15 (1,25 2.00 107 32-154 3 20 1,2,3-Trichloropropane 1.78 0.25 2.00 89 69-125 0.3 20 1.2.4-Trimethylbenzene 2.19 0.25 2.00 110 67-144 2 20 1,3,5-Trimethylbenzene 2.24 0.25 2.00 112 66-154 3 20 Vinyl chloride 2.22 0.25 2.00 111 39-150 2 20 Xylenes (total) 6.14 0.25 6.00 102 71-147 3 20 Surrogate: Uibronrolluoromcthtrttc 0, 04 92 0.0500 98 75-122 Surrogate: Tohtene-d8 0.0452 0.0500 90 66-128 Surrogate • 4-Broniglluornhenrent• 0.0464 0,0500 93 76-122 Duplicate (B1C0815-DUPl) Source: 2101841-07 Analyzed: 03/26/21 14:51 - Benzene ND 1.2 mg/kg ND 20 Bromobenzene ND 1.2 ND 20 Bromochloromethanc ND 1.2 ND 20 Bromodichloromethane ND 1.2 ND 20 Bromoform ND 1.2 " ND 20 Bromomethane ND 1.2 ND 20 n-1utylbenzene ND 1.2 ND 20 sec-Butylbenzene ND 1.2 ND 20 tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzeue ND 1.2 ND 20 Chloroethane ND 1.2 ND 20 Chloroform ND 1.2 ND 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 - 4-Chlorotoluene ND 1.2 ND 20 Dibromochloromethane ND 1.2 ND 20 1,2-Dibmmo-3-chloropropane ND 1.2 ND 20 _ 1,2-Dibromoethane (EDI3) ND 1.2 ND 20 Dibromomethanc ND 1.2 ND 20 1,2-Dichlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 61 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Duplicate (B1C0815-DUPI) Source: 2101841-07 Analyzed: 03/26/21 14:51 1,3-Dichlorobenzcne ND 1.2 mgIg ND 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichlorodilluoromethanc ND 1.2 ND 20 1,1-Dichloroethene ND 1.2 ND 20 1,2-Dichloroethane ND 1.2 " ND 20 1, 1 -Dichloroethene ND 1.2 ND 20 cis-1,2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropane ND 1.2 ND 20 0-Dichloropropane ND 1.2 ND 20 2.2-Dichloropropane ND 1.2 ND 20 l,l-Dichloropropene ND 1.2 ND 20 cis-1.3-Dichloropropene ND 1.2 ND 20 trans-1,3-Dichloropropene ND 1.2 ND 20 1?thvlbenzene ND 1.2 ND 20 Ilexachlorobutadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 Isopropylbenzene ND 1.2 ND 20 Nlethylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 ND 20 n-Propylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1,1,1,2-Tetrachloroethane ND 1.2 ND 20 1,1,2,2-Tetrachloroethane ND 1.2 ND 20 Tetrachloroethane (PCE) ND 1.2 ND 20 Tolucnc ND 1.2 ND 20 1,23-Trichlorobenzene ND L2 ND 20 1,2,4-Trichlorobenzene ND 1.2 ND 20 1, 1, 1 -Trichloroethane ND 1.2 ND 20 1.1,2-Trichloroethane ND 1.2 ND 20 Trichloroethenc (TCE) ND 1.2 ND 20 Trichlorotluoromethane ND 1.2 ND 20 1,23-Trichloropropane ND 1.2 ND 20 1.2,4-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 ND 20 Vinyl chloride ND 1.2 ND 20 X_ylenes (total) ND 1.2 ND 20 Surrogate: 11.0468 0.0494 95 75-122 Surrogate: Toluene-dN 0.0455 0. 04 94 92 66-128 Surrogate: 4-Bromolhrorohen_enc 0.0466 0.0494 94 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: l805 925-3376 Page 62 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatileOrganic CompoundsQuality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (B1C0815-MSI) Source: 2101841-04 Analyzed: 03/26/21 18:41 Benzene 8.51 1.2 mg/kg 9.92 ND 86 36-146 Bromobenzene 8.76 1.2 9.92 ND 88 28-152 Bromochloromcthanc 8.53 1.2 9.92 ND 86 43-146 Bromodichloromethane 8.97 1.2 9.92 ND 90 43-153 Bromofonn 8.44 1.2 9.92 ND 85 26-151 Bromomethane 4.77 1.2 9.92 ND 48 10-158 n-Butylbenzene 8.02 1.2 992 0.499 76 10-171 sec-Butylbenzene 9.66 1.2 9.92 ND 97 10-170 tert-Butylbenzene 9.42 1.2 9,92 ND 95 19-168 Carbon tetrachloride 8.16 1.2 9.92 ND 82 29-151 Chlorobenzeue 8.93 1.2 9.92 ND 90 31-151 Chloroethane 10.4 1.2 9.92 ND 105 13-160 Chloroform 9.01 1.2 992 ND 91 44-137 Chloromethane 7.13 1.2 9.92 ND 72 10-144 2-Chlorotoluene 8.99 1.2 9.92 ND 91 24-158 4-Chlorotoluene 8.51 1.2 9.92 ND 86 19-160 Dibroinochloromethane 9.48 1.2 9.92 ND 96 40-153 1,2-Dibromo-3-chloropropane 9.07 1.2 9.92 ND 91 21-164 1,2-Dibromoethane (EDB) 9.81 1.2 9.92 ND 99 41-148 Dibromomcthane 8.47 1.2 9.92 ND 85 45-158 1,2-Dichlorobenzene 9.26 1.2 9.92 ND 93 24-158 0-Dichlorobenzene 8.93 1.2 9.92 ND 90 19-160 1,4-Dichlorobenzene 8.53 1.2 9.92 ND 86 20-152 Dichlorodifluoromcthanc 6.47 1.2 9.92 ND 65 10-153 1.1-Dichloroethane 8.67 1.2 9.92 ND 87 35-148 1,2-Dichlorocthane 9.37 1.2 9.92 ND 94 42-132 1, 1 -Dichloroethene 8.72 1.2 992 ND 88 18-174 cis-12-Dichloroethene 8.62 1.2 9.92 ND 87 41-146 trans-1,2-Dichloroethene 9.52 1.2 9.92 ND 96 27-161 1,2-Dichloropropane 8.67 1.2 9.92 ND 87 42-145 13-Dichloropropane 9.17 1.2 9.92 ND 92 42-141 2.2-Dichloropropane 8.42 1.2 9.92 ND 85 10-166 1,1-Dichloropropene 8.71 1.2 9.92 ND 88 28-151 cis-1,3-Dichloropropene 8.40 1.2 9.92 ND 85 38-148 trans-1,3-Dichloropropene 9.73 1.2 9.92 ND 98 36-144 Ethylbenzene 8.85 1.2 9.92 ND 89 16-162 1lexachlorobutadienc 8.06 1.2 9.92 ND 87 10-193 4-Isopropyl Toluene 8.50 1.2 9.92 ND 86 11-167 isopropylbenzene 9.00 1.2 9.92 NI) 91 13-174 Methylene chloride 8.75 1.2 9.92 ND 88 30-131 Naphthalene 9.21 1.2 9.92 ND 93 10-178 n-Propylbenzene 8.74 1.2 9.92 ND 88 12-160 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX [805 925-3376 Page 63 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (BlC0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Styrene 8.91 1.2 mgIg 9.92 ND 89 23-160 1,1,1,2-Tetrachloroethane 9.93 1.2 9.92 ND 100 36-152 1,1,2,2-Tetrachlorocthane 9.13 1.2 9.92 ND 92 19-175 Tetrachloroethene (PCE) 8.53 1.2 9.92 ND 86 23-162 Toluene 8.41 1.2 9.92 ND 85 26-152 1,23-Trichlorobenzene 8.62 1.2 9.92 ND 87 10-168 1,2,4-Trichlorobenzene 9.22 1.2 9.92 ND 83 10-170 1, 1, 1 -Trichloroethane 9.36 1.2 9.92 ND 94 36-150 1,1,2-Trichloroethane 9.70 1.2 9.92 ND 98 25-179 Trichloroethene (TC'E) 8.55 1.2 9.92 ND 86 29-167 Trichlorofluoromethane 8.61 1.2 9.92 ND 87 15-156 1,2,3-Trichloropropane 8.96 1.2 9.92 ND 90 26-177 1.2,4-Trimethylbenzene 9.51 1.2 9.92 ND 86 14-157 1.3,5-Trimethylbenzene 8.70 1.2 9.92 ND 88 10-167 Vinyl chloride 9.41 1.2 9.92 ND 95 14-154 Xylenes (total) 26.2 1.2 29.8 ND 88 21-162 Surrogate: Dibromolluoromethanc 0.0487 0.0496 98 75-122 Surrogate: Toluene-dN 0.0457 0.0496 92 66-128 Surrogate: 4-Bromol7uorohenzene 0.0458 0.0496 92 76-122 Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (B1C0817-BLKl) Analyzed: 03/26/21 12:18 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " Bromochloromethane ND 0.0050 " Bromodiehloromethane ND 0.0050 " Brornoform ND 0.0050 " Bromomethane ND 0.0050 " n-Butylbenzcne ND 0.0050 " sec-Butylbenzcne ND 0.0050 tert-Butylbenzcne ND 0.0050 " Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0,0050 " Chloroethane ND 0.0050 " Chloroform ND 0.0050 " Chloromethane ND 0.0050 " 2-C'hlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 " Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (F.DB) ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: t805, 925-3376 Page 64 of 79 ,(W A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet piControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (B1C0817-BLK1) Analyzed: 03/26/21 12:18 Dibromomcthane ND 0.0050 mg/kg 1,2-Dichlorobenzene ND 0.0050 " 1.3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene NI) 0,0050 " Dichlorodif7uoromcthane ND 0.0050 1,1-Dichloroethane ND 0.0050 " 12-Dichloroethane ND 0.0050 l,l-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " 1,2-Dichloropropane NI) 0.0050 " 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 1, 1 -Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Fthylbenzene ND 0.0050 " Ilexachlorobutadiene ND 0.0050 " 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzcnc ND 0.0050 Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 Styrene ND 0.0050 " 1,1,1,2-Tetrachloroethane NI) 0.0050 " 1,1,2,2-Tetrachlorocthane ND 0.0050 " Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 1.2.3-Trichlorobenzene ND 0.0050 1,2.4-Trichlorobenzene NI) 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 " 7richlorotluoromethane ND 0.0050 " 1,2.3-Trichloropropane ND 0.0050 " 1,2.4-Trimethylbenzene ND 0.0050 " 1.3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylenes (total) ND 0.0050 Surrogate: Dibromolluoromethane 0.0459 0. 04 95 93 75-122 Surrogate: Toluene-d8 0.0472 0.0495 95 66-128 Surrogate:4-Bromo/luorohenzeue 0.0483 0.0495 98 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 65 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilei poby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (BlC0817-BSI) Analyzed: 03/26/21 10:22 Benzene 0.0342 0.0050 mg/kg 0.0398 86 75-131 Bromobenzene 0.0367 0.0050 0.0398 92 75-136 Bromochloromcthane 0.0328 0.0050 0.0398 82 70-135 Bromodichloromethane 0.0334 0.0050 0.0399 84 76-137 Bromoform 0.0369 0.0050 0.0398 93 55-139 Bromomethane 0.0230 0.0050 0.0398 58 10-157 n-Butylbenzene 0.0396 0.0050 0.0398 99 62-166 sec-Butylbenzene 0.0452 0.0050 0.0398 114 72-167 tert-Butylbenzene 0,0427 0.0050 0.0398 108 69-158 Carbon tetrachloride 0.0348 0.0050 0.0398 87 70-140 Chlorobenzene 0.0374 0.0050 0.0398 94 76-137 Chloroethane 0.0413 0.0050 0.0398 104 10-164 Chloroform 0.0323 0.0050 0.0398 81 75-123 Chloromethane 0.0324 0,0050 0.0398 82 26-146 2-Chlorotoluene 0.0396 0.0050 0.0398 100 73-145 4-Chlorotoluene 0.0405 0.0050 0.0398 102 67-151 Dibroroochloromethane 0.0371 0.0050 0.0398 93 68-144 1,2-Dibromo-3-chloropropane 0.0355 0.0050 0.0398 89 45-148 1,2-Dibrornoethane (EDB) 0.0369 0.0050 0.0398 93 73-134 Dibromomethane 0.0328 0.0050 0.0398 82 70-140 1,2-Dichlorobenzene 0.0402 0.0050 0.0398 101 78-142 - 1,3-Dichlorobenzene 0.0406 0.0050 0.0398 102 76-146 1,4-Dichlorobenzene 0.0388 0.0050 0.0398 97 72-140 Dichlorodifluoromcthane 0.0375 0.0050 0.0398 94 10-166 ],I-Dichloroethane 0.0342 0.0050 0.0398 86 65-139 12-Dichloroethane 0.0336 0.0050 0.0398 84 67-125 1,1-Dichloroethene 0.0360 0.0050 0.0398 90 54-168 cis-1,_-Dichloroethene 0.0346 0.0050 0.0398 87 74-135 trans-1,2-Dichloroethene 0.0375 0.0050 0.0398 94 68-149 1,2-Dichloropropane 0.0336 0.0050 0.0398 84 74-130 1,3-Dichloropropane 0.0356 0.0050 0.0398 90 68-130 2.2-Dichloropropane 0.0394 0.0050 0.0398 99 33-187 1, 1 -Dichloropropene 0.0350 0.0050 0.0398 88 71-140 cis-1.3-Dichloropropene 0.0349 0.0050 0.0398 88 78-135 trans-1,3-Dichloropropene 0.0393 0.0050 0.0398 99 70-137 Ethylbenzene 0.0379 0.0050 0.0398 95 69-143 Hexachlorobutadiene 0.0480 0.0050 0.0398 121 69-203 4-Isopropyl Toluene 0.0438 0,0050 0.0398 110 74-154 lsopropylbenzene 0.0408 0.0050 0.0398 102 72-157 Nlethylene chloride 0,0320 0.0050 0.0398 80 49-129 Naphthalene 0.0429 0.0050 0.0398 108 61-158 n-Propylbenzene 0.0417 0.0050 0.0398 105 69-147 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 66 of 79 i A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (B1C0817-BS1) Analyzed: 03/26/21 10:22 Styrene 0.0394 0.0050 mg/kg 0.0398 97 71-144 1, 1, 1,2-Tetrachloroethane 0.0379 0.0050 0.0398 95 78-132 1,1,2,2-Tetrachlorocthane 0.0390 0.0050 0.0398 98 64-138 Tetrachloroethene (PCE) 0.0386 0.0050 0.0398 97 74-149 Toluene 0.0330 0.0050 0.0398 83 76-131 1,2,3-Trichlorobenzene 0.0434 0.0050 0.0398 109 63-170 1,2,4-Trichlorobenzene 0.0433 0.0050 0.0398 109 71-165 1, 1, 1 -Trichloroethane 0.0349 0.0050 0.0399 88 74-137 1,1,2-Trichloroethane 0.0364 0.0050 0.0398 92 68-134 Triehloroethene (TCE) 0.0344 0.0050 0.0398 86 79-139 Trichlorofluoromethane 0.0382 0.0050 0.0398 96 32-154 1,2,3-Trichlompropane 0.0367 0.0050 0.0398 92 69-125 1,24-Trimethylbenzene 0.0390 0.0050 0.0398 98 67-144 1,3,5-Trimethylbenzene 0.0409 0.0050 0.0398 103 66-154 Vinyl chloride 0.0373 0.0050 0.0399 94 39-150 Xylenes(total) 0.115 0.0050 0.119 97 71-147 Surrogate: Dibromolluoromethane 0.0474 0.0497 95 75-122 Surrogate: TbIttene-dS 0.0478 0.0497 96 66-128 Sur•rogate:4-Bromolluorohelizem, 0.0490 0.0497 99 76-122 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 Benzene 0.0353 0.0050 mg/kg 0.0398 89 75-131 3 20 Bromobenzene 0.0390 0.0050 0.0399 98 75-136 6 20 Bromochloromethanc 0.0339 0.0050 0.0398 85 70-135 3 20 Bromodichloromethane 0.0349 0.0050 0.0398 88 76-137 4 20 Bromoform 0.0390 0.0050 0.0398 98 55-139 6 20 Bromomethane 0.0259 0.0050 0.0398 65 10-157 12 20 n-Butylbenzene 0.0425 0.0050 0.0398 107 62-166 7 20 sec-Butylbenzene 0.0487 0.0050 0.0398 122 72-167 7 20 tert-Butylbenzene 0.0459 0.0050 0.0398 115 69-158 7 20 Carbon tetrachloride 0.0363 0.0050 0.0398 91 70-140 4 20 Chlorobenzene 0.0396 0.0050 0.0398 99 76-137 6 20 Chloroethane 0.0404 0.0050 0.0398 101 10-164 2 20 Chloroform 0.0339 0.0050 0.0399 85 75-123 5 20 Chloromethane 0.0344 0.0050 0.0398 86 26-146 6 20 2-Chlorotoluene 0.0425 0.0050 0.0398 107 73-145 7 20 4-Chlorotoluene 0.0431 0.0050 0.0398 108 67-151 6 20 Dibromoehloromethane 0.0391 0.0050 0.0398 98 68-144 5 20 1.2-Dibromo-3-chloropropanc 0.0367 0.0050 0.0398 92 45-148 3 20 1,2-Dibromoethane (EDB) 0.0387 0.0050 0.0398 97 73-134 5 20 Dibromon ethanc 0.0337 0.0050 0.0398 85 70-140 3 20 1,2-Dichlorobenzene 0.0426 0.0050 0.0398 107 78-142 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 67 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilei pi Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 1,3-Dichlorobenzenc 0.0435 0.0050 mg/kg 0.0398 109 76-146 7 20 1,4-Dichlorobenzene 0.0413 0.0050 0.0398 104 72-140 6 20 Diehl orodi11uoromethane 0.0383 0.0050 0.0398 96 10-166 2 20 1,1-Dichloroethane 0.0354 0.0050 0.0398 89 65-139 4 20 1,2-Dichlorocthane 0.0346 0.0050 0.0398 87 67-125 3 20 1, 1 -Dichloroethene 0.0372 0.0050 0.0398 93 54-169 3 20 cis-1,2-Dichloroethene 0.0359 0.0050 0.0398 90 74-135 4 20 trans-1,2-Dichloroethene 0.0389 0.0050 0.0399 98 68-149 4 20 1,2-Dichloropropane 0.0350 0.0050 0.0398 88 74-130 4 20 1,3-Dichloropropane 0.0372 0.0050 0.0398 93 68-130 4 20 2,2-Dichloropropane 0.0403 0.0050 0.0398 101 33-187 2 20 1,1-Dichloropropene 0.0365 0.0050 0.0398 91 71-140 4 20 cis-1.3-Dichloropropene 0.0362 0.0050 0.0398 91 78-135 4 20 trans- l,3-Dichloropropene 0.0415 0.0050 0.0399 104 70-137 5 20 ' Ethylbenzene 0.0402 0.0050 0.0398 101 69-143 6 20 Hexachlorobutadiene 0.0509 0.0050 0.0398 128 69-203 6 20 4-Isopropyl Toluene 0.0471 0.0050 0.0399 118 74-154 7 20 Isopropylbenzene 0.0437 0.0050 0.0398 110 72-157 7 20 Nlethylene chloride 0.0333 0.0050 0.0398 84 49-129 4 20 Naphthalene 0.0453 0.0050 0.0398 114 61-158 6 20 n-Propylbenzene 0.0443 0.0050 0.0398 111 69-147 6 20 -• Styrene 0.0410 0.0050 0.0398 103 71-144 6 20 1,1,1,2-Tetraehloroethane 0.0402 0.0050 0.0398 101 78-132 6 20 1,1,2,2-Tetrachlorocthane 0.0407 0.0050 0.0398 102 64-138 4 20 Tetrachloroethene (PCE) 0.0412 0.0050 0.0398 103 74-148 6 20 Toluene 0.0349 0.0050 0.0398 88 76-131 6 20 1,2,3-Trichlorobenzene 0.0459 0.0050 0.0398 115 63-170 6 20 12,4-Trichlorobenzene 0.,0448 0.0050 0.0398 112 71-165 4 20 1,1,1-Triehloroethane 0.0365 0.0050 0.0398 92 74-137 5 20 1,1,2-Trichloroethane 0.0386 0.0050 0.0398 97 68-134 6 20 Trichloroethene(TCE) 0.0365 0.0050 0.0399 92 79-139 6 20 Trichlorofluoromethane 0.0398 0.0050 0.0398 100 32-154 4 20 ' 1,2,3-Trichloropropane 0.0384 0.0050 0.0398 96 69-125 5 20 12,4-Trintethylbenzene 0.0422 0.0050 0.0398 106 67-144 8 20 1,3,5-Trimethylbenzene 0.0437 0.0050 0.0398 110 66-154 7 20 Vinyl chloride 0.0382 0.0050 0.0398 96 39-150 2 20 Xylenes (total) 0.123 0.0050 0.120 103 71-147 7 20 Surrogate: DihrorngPuborontethcnte 0.0467 0.0498 94 75-122 Surrogate: Toluene-d8 0.0473 0.0498 95 66-128 - Surrogate:4-Bromglluorohenrene 0.0495 0.0498 99 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 68 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilei poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPl) Source: 2101841-08 Analyzed: 03/26/21 14:15 Benzene ND 0.0050 mgikg ND 20 Bromobenzene ND 0,0050 " ND 20 Bromochloromcthane ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromotbnn ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chlommethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibromomcthane ND 0.0050 ND 20 1,2-Diclilorobenzene ND 0.0050 ND 20 1,3-Dichlorobenzenc ND 0.0050 ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromethane ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 1,2-Dichlorocthanc ND 0.0050 ND 20 1,1-Dichloroethene ND 0.0050 ND 20 cis-1.2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1,1-Dichloropropene ND 0.0050 ND 20 cis-1.3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 r-thylbenzene ND 0,0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 " ND 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 69 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 Styrene ND 0.0050 mg/kg ND 20 1,1,1,2-Tetrachloroethane ND 0.0050 ND 20 1,1,2.2-Tetrachloroethanc ND 0.0050 ND 20 Tetrachloroethene WCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2.4-Trichloroben7ene ND 0.0050 ND 20 _ 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1 .12-Trichloroethane ND 0.0050 ND 20 Tricbloroethene (TCE) ND 0.0050 ND 20 Triclilorotluoromethane ND 0.0050 ND 20 L2,3-Trichloropropane ND 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0,0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: 0.0460 0.0496 93 75-122 _ Surrogate: Toluene-ds 0.0472 0.0496 95 66-128 Surrogate 4-Bron:oJ7uorobeuzene 0.0480 0.0496 97 76-122 Matrix Spike (B1C0817-MS1) Source: 2101841-12 Analyzed: 03/26/21 20:05 Benzene 0.0322 0.0050 mgIg 0.0399 ND 81 36-146 Bromobenzene 0.0319 0.0050 0.0399 ND 80 28-152 Bromochloromethanc 0.0323 0.0050 0.0399 ND 81 43-146 Bromodiehloroinethane 0.0322 0.0050 0.0399 ND 81 43-153 Bromoform 0.0376 0.0050 0.0399 ND 94 26-151 Bromomethanc 0.0290 0.0050 0.0399 ND 73 10-159 n-Butylbenzene 0.0242 0.0050 0.0399 ND 61 10-171 sec-Butylbenzene 0.0324 0.0050 0.0399 ND 81 10-176 tert-Butylbenzene 0.0335 0.0050 0.0399 ND 84 19-168 Carbon tetrachloride 0.0322 0.0050 0.0399 ND 81 29-151 Chlorobenzene 0.0337 0.0050 0.0399 ND 84 31-151 C'hloroethane 0.0346 0.0050 0.0399 ND 87 13-160 Chloroform 0.0316 0.0050 0.0399 ND 79 44-137 Chloromethane 0.0329 0.0050 0.0399 ND 82 10-144 2-Chlorotoluene 0.0335 0.0050 0.0399 ND 84 24-15S " 4-Chlorotoluene 0.0330 0.0050 0.0399 ND 83 19-160 Dibrornochloromethane 0.0370 0.0050 0.0399 ND 93 40-153 1,2-Dibromo-3-chloropropane 0.0333 0.0050 0.0399 ND 84 21-164 1,2-Dibromoethane (EDB) 0.0366 0.0050 0.0399 ND 92 41-148 Dibromomcthane 0.0315 0.0050 0.0399 ND 79 45-158 1,2-Dichlorobenzene 0.0325 0.0050 0,0399 ND 82 24-158 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 70 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analyte Volatile Organic Compounds by GUMS - Quality Control Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Matrix Spike (BlC0817-MSI) Source: 2101841-12 Analyzed: 03/26/21 20:05 1,3-Dichlorobenzene 0.0321 0.0050 mgIg 0.0399 ND 80 19-160 14-Dichlorobenzene 0.0305 0.0050 0.0399 ND 76 20-152 Dichlorodilluoromcthane 0.0373 0.0050 0.0399 ND 93 10-153 1, 1 -Dichloroethane 0.0332 0.0050 0.0399 ND 83 35-148 1.2-Dichlorocthene 0.0321 0.0050 0.0399 ND 80 42-132 1,1-Dichloroethene 0.0345 0.0050 0.0399 ND 86 18-174 cis-1,2-Dichloroethene 0.0335 0.0050 0.0399 ND 84 41-146 trans-1,2-Dichloroethene 0.0354 0.0050 0.0399 ND 89 27-161 1.2-Dichloropropane 0.0321 0.0050 0.0399 ND 80 42-145 1,3-Dichloropropane 0.0358 0.0050 0.0399 ND 90 42-141 2,2-Dichloropropane 0.0344 0.0050 0.0399 ND 86 10-I66 I,1-Dichloropropene 0.0321 0.0050 0.0399 ND 80 28-151 cis- 1,3 -Dichloropropene 0,0320 0.0050 0.0399 ND 80 38-148 trans-1,3-Dichloropropene 0.0376 0.0050 0.0399 ND 94 36-144 Ethylbenzene 0.0324 0.0050 0.0399 ND 81 16-162 Hexachlorobutadiene 0.0223 0.0050 0.0399 ND 56 10-193 4-Isopropyl Toluene 0.0300 0.0050 0.0399 ND 75 11-167 Isopropylbenzene 0.0328 0.0050 0.0399 ND 82 13-174 Wthylene chloride 0.0310 0.0050 0.0399 ND 78 30-131 Naphthalene 0.0314 0.0050 0.0399 ND 79 10-178 n-Propylbenzene 0.0325 0.0050 0.0399 ND 81 12-160 Styrene 0.0336 0.0050 0.0399 ND 84 23-160 1, 1, 1.2-Tetrachloroethane 0.0368 0.0050 0.0399 ND 92 36-152 1,1,2,2-Tctrachloroethanc 0,0365 0.0050 0.0399 ND 91 19-175 Telrachloroelhene WCE) 0.0339 0.0050 " 0.0399 ND 85 23-162 Toluene 0.0291 0.0050 0.0399 ND 73 26-152 1,2,3-Trichlorobenzene 0.0262 0.0050 0.0399 ND 66 10-168 1,14-Trichlorobenzene 0.0257 0.0050 0.0399 ND 64 10-170 l,l,l-Trichloroethane 0.0334 0.0050 0.0399 ND 84 36-150 1,1,2-Trichloroethone 0.0304 0.0050 0.0399 ND 91 25-179 Trichloroethane (TCE) 0.0338 0.0050 0.0399 ND 85 29-167 Trichlorofluoromethane 0.0379 0.0050 0.0399 ND 95 15-156 1,23-Trichloropropane 0.0376 0.0050 0.0399 ND 94 26-177 1,2.4-Trimethylbenzene 0.0309 0.0050 0.0399 ND 77 14-157 1,3,5-Trimethylbenzene 0.0323 0.0050 0.0399 ND 81 10-167 Vinyl chloride 0.0368 0.0050 0,0399 ND 92 14-154 Xylenes (total) 0.0983 0.0050 0.120 ND 82 21-162 Surrogate: Dibromolluoromohane 0.0459 0.0499 92 75-122 Surrogate: Toluene-d8 0.0473 0.0499 95 66-128 Su•rogate:4-Bromoguorohell:01" 0.0486 0.0499 97 76-I22 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 71 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sampleod Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC_ Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC- CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal STLC Metals by ICP 001013 STLC Chromium STLC/EPA 601013 Water OEC. CA-ELAP 6010B STLC Lead STLOEPA 6010B Water OEC. CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC. Internal TCLP Metals by ICP 601013 TCLP Lead EPA 1311/EPA 601 OB Water OEC, CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 72 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) 5knalysis Method Matrix Laboratory & Certification Total Metals by ICP 601 OB Total Antimony EPA 601 OB Solid OEC, CA -FLAP 601 OB Total Arsenic EPA 601 OB Solid OEC, CA-ELAP 001 OB Total Barium EPA 001OB Solid OEC, CA-ELAP 601 OB Total Beryllium EPA 601 OB Solid OEC, CA-ELAP 601013 Total Cadmium EPA 601OB Solid OEC, CA-ELAP 601 OB Total Chromium EiPA 601 OB Solid OEC, CA-ELAP 6010B Total Cobalt EPA 601OB Solid OEC, CA-ELAP 6010B Total Copper EPA 601 OB Solid OEC. CA-ELAP 6010B Total Lead EPA 601 OB Solid OF,C, CA-ELAP 601 OB Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 601 OB Total Nickel EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Selenium EPA 601 OB Solid OEC, CA-ELAP 601013 Total Sih er EPA 601 OB Solid OFC, CA-ELAP 6010B Total Thallium EPA 601 OB Solid OEC, CA-ELAP 6010B Total Vanadium F,PA 601 OB Solid OEC, CA-ELAP 601 OB Total Zinc EPA 601 OB Solid OF,C, CA-ELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC. CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comVeports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: :805) 925-3376 Page 73 of 79 --I Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPII-Gasolinc EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC Internal 8015 TPH-Gasoline EPA 8015M Solid OEC_ CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, C A-ELAP 8015 TPH-Gasolinc EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 74 of 79 Im W AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 NotesDefinitions Qualifier Definition MDL. Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. D-06 Results in the diesel organics range are primarily due to overlap from a heaNy oil range product. N-02 Analyte concentration below TTLC but above 1 Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-03 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits duc to matrix interference. QC batch accepted based on LCS and or LCSD recovery and/or RPD values. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. S-02 The surrogate recovery for this sample cannot be accurately quantified due to interference from coeluting organic compounds present in the sample extract. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. 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N z O p U U) Q W a N APPENDIX E Statement of Qualifications STATEMENT OF QUALIFICATIONS Buena Resources, Inc. is a locally owned and operated full -service environmental company providing environmental consulting, field services and analytical services. Our environmental professionals are experienced in Phase I assessment, Phase II subsurface investigations and Phase III remediation. Our staff consists of professional engineers and environmental technicians. Personnel are OSHA 40 hour trained to perform environmental work when hazardous chemicals are involved. Clients for whom we've performed our services include major oil company, large utilities, industrial facilities, lending institutions, real estate developers and property owners and sellers. The following professionals performed work related to this project: Mr. Daniel Ringstmeyer is a Registered Professional Engineer, Colorado and California, Registered Environmental Assessor, Certified OSHA 40-Hour Trained worker, 8-Hour Trained Haz-mat Supervisor and a licensed California General Engineering Contractor. Mr. Ringstmeyer holds a Bachelors of Science in civil engineering from the South Dakota State University. He is the Founder/Owner and Principal Engineer of Buena Resources, Inc. and CIRRUS Environmental, Inc. He is the Principle Engineer responsible for all work performed by the environmental consulting/contracting firm. Mr. Ringstmeyer has conducted Phase I ESA assessments, Phase II subsurface investigations and Phase III remediation projects for sites throughout California and Mexico. He has designed and managed many successful remediation projects utilizing soil vapor extraction/thermal oxidation, bioremediation, groundwater pump and treat, and carbon adsorption throughout California and Mexico including the closure of a large Class I TSD Landfill facility. He has also directly been responsible for the closure of several idled oil fields and illegal agriculture landfills.