Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
Closure Report for 2600 Broad Street
Closure Report Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA June 17, 2021 Prepared For: Mr. John Hochleutner Pacific Petroleum California, Inc. 1615 Betteravia Road Santa Maria, CA 93268 Prepared By: Buena Resources, Inc. P.O. Box 2040 Santa Maria, CA 93457-2040 Diesel Tank & Contaminated Soil Removal 2600 Broad Street San Luis Obispo, CA TABLE OF CONTENTS 1.0 Excavation: 2.0 Soil Sampling of the Excavation: 3.0 Discussion of Results: 4.0 Conclusions: Appendix A Site Maps & Figures Appendix B Lab Summary Spreadsheets Appendix C Site Photographs Appendix D Laboratory & Chain of Custody Reports Appendix E Statement of Qualifications 2 2-3 3-4 4 General Contractor License #841453 Buenaresources P.O Box 2040 Santa Mai ia, CA 93457-2040 P: (805) 34b-1766 F: (805) 346-1767 June 17, 2021 Ms. Molly Brown, Fire Inspector III City of San Luis Obispo Fire Department 2160 Santa Barbara Avenue San Luis Obispo, CA 93401-5240 Subject: Fuel Tank Removal and Soil Removal from a Site located at 2600 Broad Street in San Luis Obispo, CA Dear Molly: Buena Resources, Inc. has prepared this Closure Report to summarize the work performed and the laboratory results at the above site. Pacific Petroleum of California was engaged by Natural Healing Center to remove an existing diesel tank from this site, which had been closed at some point in the past by filling with cement. The diesel tank was estimated to be 4'-dia. by 8' long in size. The excavation related to that tank site was 8' x 8' by 8' deep. A second excavation located adjacent to the tank removal was 12' x 12' by 12' deep. Once the tank was removed, the underlying soils were found to have been impacted. Impacted soil was noted below the tank, in the excavation bottom and on the sides of the excavation. Soil believed to be impacted from the diesel tank was removed and placed into 10 cyd. bins. A total of 64.51 tons of Cal Haz lead impacted and hydrocarbon impacted soil was removed and shipped to Waste Management's Kettleman Hills Class I TSD facility. Buenaresources A State Certified Small & WBE Business BUENARESOURCES EXCAVATION: The area to the west and below the tanks were found to have been impacted by the diesel fuel along with Chromium, Nickel and Lead. All elevated metals above the SLTC testing threshold were tested, with all the Chromium and Nickel samples found to be below the Title 22 STLC (soluble) hazardous thresholds. Lead, however, did exceed the Title 22 threshold and would be considered California hazardous material. Additional testing by TCLP RCRA method all reported levels below the RCRA threshold. The underlying soils under this site has a band of Serpentine, which is likely accountable for the reported Chromium and Nickel levels. This greenish material is very hard and, in this case, weathered with cracks. The diesel fuel appears to have migrated into these cracks requiring these underlying soils to be impacted requiring removal. The last samples taken in on June 4tn were all below the Region II ESLs for all hydrocarbon ranges and meet the closure criteria established for this site. The depth of this excavation was approximately 12' and 12' x 12' in size. The excavations are shown in Appendix A as Figure 1. 2.0 SOIL SAMPLING OF THE EXCAVATION 2.1 Soil Sampling Plan Samples were taken from the excavation sides and bottom. All soil samples were analyzed for full range hydrocarbons (gasoline, diesel and motor oil ranges) by EPA method 8015, Volatile Organic Compounds by EPA method 8260b and CAM metals. Each sample was sealed, labeled, placed in a cooler with ice and shipped to the laboratory. Analyses were completed according to the various methods specified according to SW-846 guidelines. Action levels used at this site were the Regional Water Quality Control -Region II ESLs (Environmental Screening Levels) for residential soils. Buena. A State Certified Small & WBE Business 2 BUENARESOURCES 2.2 Sampling Maintenance and Security Upon collection, the sample containers were labeled in accordance with EPA protocols and chilled pending transportation to OEC, a State certified analytical laboratory located in Santa Maria, California following chain -of -custody procedures. All samples were recorded on Chain -of - Custody forms in ink and transferred to the laboratory according to EPA SW-846 protocol. Any changes or corrections were made by drawing a line through the error and initialing and dating the correction, then entering the correct information. 3.0 DISCUSSION OF RESULTS: Samples were taken at four wall locations and at two bottom of excavation locations below the tank. In addition, seven trench and four soil piles were initially sampled and were found to have lead at levels considered Cal Haz for STLC Lead. The soils in the five bins were also sampled to confirm the contaminates were hazardous. All five bins reported STLC lead at levels which exceeded the Title 22 guidelines for hazardous waste thresholds and were subsequently shipped as Cal Haz STLC Lead impacted soils to Waste Management's Kettleman Hill's TSD facility. The samples taken on May 5tn reported elevated diesel levels in three of the six samples. Those areas were further excavated with the final sampling on June 3rd reporting all bottom samples below the Region II ESL action levels for residential soils. All of the samples taken at the excavation sites reported no volatile organic compounds to at least the method detection limit (MDL) with the exception of the Soil Pile North Sample. The Soil Pile North sample reported n- Butylbenzene at 0.2 mg/kg, sec -Butyl benzene at 0.11 mg/kg and n-Propylbenzene at 0.15 mg/kg. All later samples taken after additional material had been removed were below the MDL for all Method 8260b compounds. The CAMs reported nine samples with elevated chromium and six with elevated nickel levels requiring additional STLC testing to determine if the material was hazardous. The STLC levels were all below the California Title 22 hazardous thresholds for both the chromium and nickel and is not considered hazardous. Buenaresources A State Certified Small & WBE Business 3 BUENARESOURCES It is important to note that elevated levels of these two metals are common in the Serpentine material found in this area. The reported TTLC levels were at levels high enough to require further STLC testing. All of those STLC results were well below Title 22 regulated STLC metal levels and likely would be considered typical background values for this area. 4.0 CONCLUSIONS: The one cement filled diesel tank was successfully removed by PPC and shipped to WM McKittrick Landfill facility for landfilling. Impacted soil from the fuel and lead was discovered below the tank and adjacent to the tank location and was subsequently removed. A total of 64.52 tons of Cal Haz STLC lead impacted soil was removed and shipped to Waste Management's Kettleman Hills TSD facility. This material also reported elevated diesel range hydrocarbons in the side slopes and bottom which was removed and included with the material shipped to Kettleman Hills. Based on the above reported results, it is our opinion that there is no further work required at this site due to the fuel contamination from the removed tank. We recommend that this site be closed and backfilled. Thank you for the opportunity to be of service. If you have any questions, please contact this office at (805) 346-1766. Sincerely, Buena Resources, Inc. gc-,o .112 Daniel P. Ringstmeyer, P.E. (043540) Owner/Engineer Buenaresources A State Certified Small & WBE Business 4 APPENDIX A Site Maps & Figures VICINITY MAP 41 hop. o 0 0- E I U 'tiighland Dr Slack St; 101 E Foothill Blvd cp,�,o Real ,�Ceta Dr Santa E� O Rosa Park San Luis 9M 13Dbispo v 2028„�o3A � U] 1 �S ��'r 2600 Broad St, San L.. 2o2A,_.., lac o 0 2600 Broad St 20; QO San Luis Obispo, CA High St 93401 Sobtff Laguna Lake Park 201 `T.j 4 � :l�l �cr � �2008 �j yPrado Rd 1 Tank Farm Rd I m n 200A r 3 _Slnsi r Park _'3t c V t Southwood ❑r 227 Damon -Garcia Sports Fields �at�lc Farm Rd San Luis Obispo +CoMcGhesney Field Ra Evans Rd Islay Hill Park 0 rni 0.5 1 1.5� Copyright© and (P) 1988-2012 Microsoft Corporation and/or its suppliers. All rights reserved. http://wvw .microsoft.conVstreets/ Certain mapping and direction data© 2012 NAVrEQ. All rights reserved. The Data for areas of Canada includes information taken with permission from Canadian authorities, including: © Her Majesty the Queen in Right of Canada, © Queen's Printer for Ontario. NAVTEQ and NAVTEQ ON BOARD are trademarks of NAVTEQ. ©2012 Tele Atlas North America, i All rights reserved. Tele Atlas and Tele Atlas North America are trademarks ofTeleAtlas, Inc. © 2012 by Applied Geographic Solutions. All rights reserved. Portions ©Copyright 2012 by Woodall Publications Corp. All rights reserved. 2 z� io 0 �cn V Z > map Q Q } m U N O Q v m w m a C o o K = O( W oww3 n N Imo 0 0 W W O N U W Z N Q O NW O . O Z 0 0 � ow�~ Q J z maw W O U > V l w> N ¢ O ¢ U N S z w n o W rO 0 S O= w H m O te ro= w Z O = p a 'Woo Z a Z z 7 ID0 0 H 30 xx p �az-5 �00 (n ins NN� Q N Z Z O O G0 HQ rzJZ< Qp�N Z ;� 0 M 0 0 mo N OO W/y/�� w, Q roWN 7 M, OUZOU W 'Oa MO'M 6� c0 M N N Zl\\W\ W s2 1 Z ' O F > Q W O N r/ M �p M m r M � N N O M N � Z W W r- i U Z Z H Q p U �o w a j H p Q v) wQ0 W O U O (n m J Y cDz Z (o< Q NUl F `s a E �E5 191 ta 7 g 00 ?� IN WWMA McKittrick Waste Treatment Site Reprint 56533 Hwy 58 W. Ticket# 156247 WASTE MANAGEMENT MCKittrick, CA, 93251 Ph: (661) 762-7366 Customer Name PACIFICPETRO PACIFIC PETROLEU Carrier Pacific Petroleum Pacific Petroleum Ticket Date 05/13/2021 Vehicle# PPC 570 Volume Payment Type Credit Account Container Manual Ticket# Driver Ryan Hauling Ticket# Check# Route North Billing # 0001772 State Waste Code Gen EPA ID Manifest PPC 2021-000473 Destination Grid LF PO Profile 647907CA (FORMER FUEL TANK) Generator 144-NATURAL SANLUISOBISPO 2600 NATURAL HEALING CENTER (2600 BROAD ST) Time Scale Operator Inbound Gross 39760 lb In 05/13/2021 09:33:05 INBOUND Dcarmical Tare 29540 lb Out 05/13/2021 12:49:25 OUTBOUND Dcarmical Net 10220 lb Tons 5.11 Comments Truck was held up pending paperwork corrections Receiving: Mon -Thu Drums 7-3, Liquids & Roll -offs 7-4, End Dumps 7-5 Product LD% Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------------------- 1 SpwasteSolidOth-Cu 100 1.00 Yards SANLUISOBI 2 EVF-P-Standard Env 100 SANLUISOBI 3 FUEL -Fuel Surcharg 100 SANLUISOBI 4 RCR-P-Regulatory C 100 % SANLUISOBI 5 WWM-P-Waste Water 100 SANLUISOBI 6 HARD2HANDLE-Hard T 100 1 Load SANLUISOBI Total Tax Total Ticket Driver's Signature C an Hills Landfill Reprint 3 Skyline -Road, P.O. Box 471 Ticket# 55260 Ke*4awmmA ErjaA, 93239 Ticket Date 05/24/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667316JJK Grid B18 Volume Yards Carrier CAD981164312 Driver Arturo Vehicle # G249 Vehicle License 9F36934 Container # 4NP7786 Container License 4NP7786 Time Scale Operator In 05/24/2021 11:46 MANUAL WT A. Ortega Gross 75320 lb* Out 05/24/2021 12:41 A. Ortega Tare 44320 lb* * Manual Weight Net 31000 lb Tons 15.50 Comments Inbound Product Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------- 1 NONH DISP-TONS-Non 100 15.50 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 - SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Drivers Signature L qAjp7nb Pase print or type. (Form des Hell for use on Nuts Itch) typewnter.) N/9 y, Page 101 3 Emrg eency Response Frrn� 1. Generator ID Number e UNIFORM HAZARDOUS WASTE MANIFEST _ _ -- Generators Saz Address l"di"e 5 Generator's Name and Ma7ing Address Ger,era'orsProne 8. Transporter t Company Name 7, Transporter 2 Company Name 8 DesnatedFaciit/NameandSiteAddress g R Phone:' 9b.0 SDOTDescopMr,(,n durbngProperShippingName, Hazanl Class, ID Numt aand Padong Group V any)) Form Approved. OMB No.2050.0039 ManifestTracki Number 0156�7316 JJK urg address) i. EPA ID Number U S. EPA ID Number 19. Con sires 11. Total 12 UM 13 Waste Codes No Type OZ., WLNd. 30 3, I 1x 4. —1 14. Special handlinglnsWcuonsamAdditiaiallnfcrmaE-0n and to IieaMe intemationa'. and naEonal gpvemmenrd mgulatrons. if export srupmxsm and I an d^_ Pdmary 15. GENERA70R'510FFEROR'SCERTIFlCATION; IherebydecWrethatthewntentsofthisconsigmnerdarefu8yandaccuratelydesrnlg vemmat�ove n thepropers511 egname. mearedasmtoPm�• marked and labeled'placarded. am are in aEI respells m proper wndieon br bansport armrLrg aPF Exporter I urbty tlat the wrtlents dthis t»ns'gnmerd conform W the terms o1lha attached EPAAdarwrleagmenr of Consent sma;anu N generator) wrtiy dot Ne waste minirt oat on sra anent den4:zd» 49 CFR 262.27(a) (N I am a la ge quan ty gene eta) a (b) (rf I am a is We 19I' Da/ yea Sigrature Generators'O1lerors Printedlfyp^_d Name 16. ke rr:sbonal Shi^ ❑ Exoon from U 5. Pcr. of snay'ex,t — — — -- �Impo IoUS Date feanrgUS. Transporter sgnavre t� exports �7) 17.. Transporter Acknowledgment 01 Receipt of Matenals r'lhr. Da+r Ba' SignaW2 �, /� f I Tran34+` 1 PrgtedTyped is r ! ;I S 12 y P 24 18. D saepan y �^� 1 Ga. Discrepancy Indipuon Space ❑ U Resdue ❑ Partal Reject ,on ❑Full Rejerwa^ Quantity ❑Type Mardfest Ref°rence NcmoEr' U.S EPA ID Number t8b Aeemate FaaldY(or Generator; 7 U W I FadlVs Phone: Month Day 0 19. Hazardous Waste Report Management Method Codes (i z., wiles fa iazardous waste treatment, disposal. and repydirg systems) 0-1 2 3 e 20, DesignatedOwmRr or OperaNr Certiikaudn of receipt of hazardous materials covered by the man'rfest ex, p; as rued in It m 18a {onN Day -year Pnntad/Tyced ;nary G rE TINATi: STATE EPA Form870 22(Rev 3-05)Pre'riousedil�sare Obsolete. DEz.r'''[E1'raCl iTY"Oa C man Hills Landfill Reprint 3 Sk�yline;Road, P.O. Box 471 Ticket# 55489 Keft4,1wm&fA yuiErftA, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667317JJK Grid B18 Volume Yards Carrier CAD981164312 Driver Vehicle # G1076 Vehicle License 9F18973 Container # 4NC6734 Container License 4NC6734 Time Scale Operator In 05/28/2021 10:45 MANUAL WT A. Ortega Gross 71860 lb* Out 05/28/2021 12:25 A. Ortega Tare 43720 lb* * Manual Weight Net 28140 lb Tons 14.07 Comments Inbound Product Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------- 1 NONH DISP-TONS-Non 100 14.07 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 SANLUISOBI 4 FUEL -Fuel Surcharg 100 SANLUISOBI 5 RCR-P-Regulatory C 100 SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature fm 5&(0/gF1g173. TAL Sao -1/qW—k73'1 Please print or type. (Form designed for use on eMe (124tal) typewrller.) Form Annmvpr! OMA Nn 9AgW 10 F UNIFORM HAZAROMS 1. Generaror ID Number 2. Page 1 of 13 Emergency Response Phone 4. Manifest Tracking Number „ C man Hills Landfill Reprint 3 Skyline :Road, P.O. Box 471 Ticket# 55500 Ke6&0Pwm&vkr0idiqwErfiA, 93239 Ticket Date 05/28/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667318JJK Grid B18 Volume Yards Carrier CAD981164312 Driver JUAN Vehicle # 65424M1 Vehicle License 65424M1 Container # Container License Time Scale Operator In 05/28/2021 12:43 MANUAL WT A. Ortega Gross 46680 lb* Inbound Out 05/28/2021 14:02 A. Ortega Tare 32740 lb* * Manual Weight Net 13940 lb Tons 6.97 Comments REPLACEMENT TICKET FOR TICKET # 55490 Product Qty UOM Rate Tax Amount Origin 1 ------------------------------------------------------------------------------- CALH DISP-TONS-Cal 100 6.97 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 SANLUISOBI 4 FUEL -Fuel Surcharg 100 SANLUISOBI 5 RCR-P-Regulatory C 100 SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature Hfq- 6542ynv,j §- se pnnt n type. (Form designed f0r use on elite (12-p dch) r °wdlec) UNIFORM HAZARDOUS 1 Generalcr ID Number WASTE MANIFEST 2 s. Gem Wes Name and wiling Address - i. iranspater 1 Company Name Transporter 2 Company Name Response Phone 4. Man'rfest T roan Approved, OMB No. 2050-0039 - 015 6N7 318 JJK :Address (8 dAterent than mailing address) FaaitysPfnrle '`-r ;'_ _ 9a W U.S. DOT Desap' fndeting Proper Stopping Name, Hazard Class. ID Number. 10. Containers HM and Pig Group (4 any)) 11, TOW 12. Unit 1 _ NO. Type Quantity WtNd, 13. Waste Codes �} Yt )k:rjE __- == 20 4. 14. Special HartAirg fnsbuctions and Additimnal Irdomation — - r 15 GE►IERATOR'SfOFF"'S CERTMATION: I hereby declare that the contents of this cansgrl mt are fulty and accurately described above by the Proper stopping name, and are classified, padeage a tec and IabeledYo!acardad. and are h al aspects u grope condition transport according to apptirable memaba�and national governmental regulations. ke Exporter Off* hat the comae ds of dus consignment conform to he terms of the attached EPA export shipment and I am the Primary low* mat tlm • re rtrad uzation s element dentifi�d in 40 CFR 262.27 a d I am a I Ackncudedgr ant of C sent f) (' large quantity generator) a (bi . I am a 44 qua general:.- =rw ![� e Y. / Signature Day >114 7� ts.lnternetional snipmar,rs ❑ Import to U.S ❑ Export from U.S, Port of enbyrexil: _ T-sDorlersgnalum (fur exports ooty): Date leaving U.S: — — — — 17. TransporwA mowlaogrme t of Reagpr of MaWials 18. Disaapar~y - 1aa. Dweipansy kdication Space ❑ Quantity ❑TYce ❑Residue Manifest Refs ~ 150. ARemate Fadifty (or Generalorl _J J �IF.WsPh. .1 19, Hazardous Waste Repod Management Method Codes (i.e.. codes for hazardous waste treatment, di sposal, and recycling systems) 1 13Z 2 7- 20. Designated Facility Owner or Operate: Certification of receipt of hazardous mater1* covered by the man'dest except as ed in kern 18a -tud. YPed Signature r trAL,'e �n1rLk",AJ 512111� Month + Day JJ I I ❑ Partial Rejection ❑ Ful Rejection U.S. EPA ID Number Month Day 4 EPA Foram 8700.22 Rev. 3-05) Previous edbons are obsolete 0ESirt 7 FACILIT E INATIO i STATE (IF REQUIRED) C man Hills Landfill Reprint 3 Skyl.ine$Road, P.O. Box 471 Ticket# 55678 Kebh 1wm&me EriA, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667326JJK Grid B18 Volume Yards Carrier CAD981164312 Driver Vehicle # G1072 Vehicle License 5375SITZ Container # Container License Time Scale Operator In 06/04/2021 12:03 MANUAL WT A. Ortega Gross 68100 lb* Out 06/04/2021 13:38 A. Ortega Tare 45140 lb* * Manual Weight Net 22960 lb Tons 11.48 Comments Inbound Product Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------- 1 CALH DISP-TONS-Cal 100 11.48 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 - SANLUISOBI 4 FUEL -Fuel Surcharg 100 - SANLUISOBI 5 RCR-P-Regulatory C 100 % SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Drivers Signature +„ "' ', Form Approved. OMB No. 2050.0039 Please print a type. (Form des grr4 use on elite (12-pitch) typewriter.) 4. Ma hMe:tTradw g Number UNIFORM HAZARDOUS tT ID Number 2. Page 1 of 3. Emergency Response Phone (� JJ K 1 WASTE MANIFEST p tit311MINI 1 8x.Qi"-IQLgi 1015667326 5. Generators Name and Matting Address . C watots Site Address (tdrftemmi than mailing addressi ,uHL SLO 908 HUSTON ST 284A BF;;=.O ST GRO'VER BEACH. Ck 934-K US 5 Linea UHii" o, G. x"Gn US GeneratorsPthone:T-4-:•.� h1=t U.S. EPA ID Number 6. Transporter 1 Cw4)arry Name Pam Petroleum 0�v,11c. CACo5l164312 7. Transporter 2 Company Name U.S. EPA ID Number 8. Designated Facility Name and Site Address GHEMICALUl.ASTE MAivrtGEMEraT.FN, U.S. EPA ID Number C .,,4`t;- m51 OLD SKr LINE ROAG KEfn. wN CITY, CP. 93239 US Fall" s Pf one, 55t i6 9711 ga. 9b. U.S. DOT Description (mduding Proper Shipping Name. Hazard Class. ID Number, 10. Containers 11. Total 12. Unit 13, Waste Codes HM and Packing Group (N any)) No. Type 0uan11y WL'M 1 X 1. R4, UN3477, EM.11RpMMEMf4LL, t+,AZaRDOil'S Sr1BSTA!uCr 3OL G /� GH j ----- u 2 y u 1 I 3. 14. Special tiaating Insbucha s and Additional Inlammation �� I� 5 Z 1� G tY:ear m,appropnale PPE 24 Haur,�mergesq Re-o rse ;� tom? 925-'?N7 Prole 1Y CA61992C a GENERaw SIQFFEROR'S CERTIFICATION: 1 hereby declare Brat the contents of this consignment are fully and accurately descn above by the proper shipping name. and are classified, pac w*, in for trarsportaaarding to applicable international and national gave mnental regulations. If export shipment and I am the Primary marked and labeledlplacarded. and are m all respects proper condition Eporter, I certify that the conW% of this oors went w tom to the terms of the attached EPAAdohowledgment of Consent I w* drat the waste mmomation statement identined in 40 CFR 262.27(a) (rf I am a large quantity generator) or (b) Cd I an a anan -sly generator) is true. GrsRlnted/TYped�� �l Month Day Year 1vl 0(/� +� �0 16, International Shipments ❑ Import to U.S. ❑ Export flan U.S Port or erdryleAt = Transporter signature(exports only): Date leaving U.S.: 4Y 17.TrahsporterAcluvfedgmentofReceiptofMaWials Transporter 1 PrmledTyped Name Signature Month Day Year UA rj A LI ?u aTransporter 2 Pninte0yped Name Month Day Yeas F 18.Disaepancy 18a. Discrepancy Indication Space ❑ Quantity Type ❑ Residue ❑ Partal Rejection ❑ Full Rejection Manifest Reference Numbs: 18b. Atemate Facility (or Gerwator) U S. EPA ID Number J U LL I Fadtity's Phone: Month Day Yex I k. Sombre of Alternate Facility (or Gerherdtar) N 19, Hazardous West- Report Managemem Memco woes p.e, w 1 3. 4 2.. N\32 20. Designated Facility Owner or Operator: Cati6mbon of receipt of hazardous materials covered by the manifest except as noted in flan 18a Abr�i Day YeaPiritedlTyped PrimedTyped Name Signature � tin y�.ti t'I �a LI EPA Form 8700-22(Rev.3-05i Previous edition a't ^s, ate. DESIGNATED FACILITY TO GENERATOR STATE (IF REQUIRED) C Tan Hells Landfill Reprint 3 Skyline,Road, P.O. Box 471 Ticket# 55679 Ke*A0wm&4A eNBA, 93239 Ticket Date 06/04/2021 Ph: (559) 386-9711 Customer PACIFIC PETROLEUM CALI PACIFIC PETROLEUM Billing # 0000172 1547 E BETTERAVIA RD Payment Type Credit Account SANTA MARIA, CA, 93454 Profile CA619920 Generator 144-NHCSLO NHC SLO (2640 BROAD ST) Origin County SAN LUIS OBISPO Manifest 015667327JJK Grid B18 Volume Yards Carrier CAD981164312 Driver JAVIER Vehicle # G383 Vehicle License 65425M1 Container # 4ND3836 Container License 4ND3836 Time Scale Operator In 06/04/2021 11:44 MANUAL WT A. Ortega Gross 77000 lb* Out 06/04/2021 13:31 A. Ortega Tare 44020 lb* * Manual Weight Net 32980 lb Tons 16.49 Comments Inbound Product Qty UOM Rate Tax Amount Origin ------------------------------------------------------------------------------- 1 CALH DISP-TONS-Cal 100 16.49 Tons SANLUISOBI 2 MFE-e-Manifest (La 100 1.00 Each SANLUISOBI 3 EVF-P-Standard Env 100 SANLUISOBI 4 FUEL -Fuel Surcharg 100 SANLUISOBI 5 RCR-P-Regulatory C 100 SANLUISOBI 6 WWM-P-Waste Water 100 o SANLUISOBI Total Tax Total Ticket Driver's Signature i-353- NND3 Form Approved. OMB No. 205M39 Wease pant or type. tram cesgrrea nor usn u h —1 1. Gehceretor ® 2. Page 1 of 3. EmergencY Response Phone UNIFORM HAZARDOUS ,, 4. ManNestTrackirg Number 01566737 JJK WASTE MANIFEST A .1, __ , ?: {..:,n.".19d= 5. Ceneraor s.Name, and"Address Generators Site Address (a itmerem than mailing address) NHC SLO 9f36 HUSTON ST Bq l V' GROVER. BEACH, C- VW3 3 h'a SAN LUIS WSPO, Cp S,3A01 US Generators Phone: ::. _ l . IQ' 6. Transporter 1 Company Name U.S. EPA ID Number Pacl9. Petroleum CA., Inc GA,D9811643t2 7. Transporter 2 Carpany Name U.S. EPA ID Number 8. Designated Facility NaMe and Site Address GHEM;CAl u'dASTE MAIJkGEMENT, I1eC U.S. EPA ID Number CAT000646117 3Sf1 OLD SKYLINE ROAD KETTLENIA.N CIrf, CA 93239 US F s Phone: 559-*Q711 9a. 9b. U.S. DOT Descr ption (including Proper Shipping Name, Hazard Class, ID Number, 10. Coma hers 11 Total 12, Unit 13. Waste Codes No. Type Group and packing p (t any)) Duartily NRNd. X gar t' PO, UN3O77, ENVIRCMENTi A Y HAZARDOUS SUPSTAUCE SOLD N O.S. LEAD Q Cs1 �� Y t81 I 2 LU { 3. i 4. -I-� 14 Special Handling Instructions and Additional Information [3�N$ Zbf4t} wear ON appropriate PPE 21 Hour Emergency Response #i X6) 9 194% 103,39 Ptorde R CA51M 15, RNERATOR'SIDFFEROR'S CERTIMATM: 1 heratiy declare that the coments of this consignment are fully and acaaately described above by the proper shipping name, and are classified, packaged, marked and Iabeledlplacarded, and are In all respects n proper oxiJilion for transpor according to applicable international and natbnal governmental regulations. If expos shipment and I am the Primary Exporter, I certify that the contents of this catsignment conform o the tames of the attached EPAAckrawledgment of Consent. I certify that the waste minimization statement idenft in 40 CFR 28P 27(a) Id I am a large quantity generator) or (b) p am a ;,het .antly generator) is U. ix V�JOAerors Pnnted(Typed Nan; Signature r ( Mai Day year f o `J7 M�t��V F/ 8G a U F1 in colStpmeMs �Irrw1.U.S. ❑ Fxpont from U.S Port of enirylexit — -- — — Z Trarspatsr signature (for a"Is only): Date leaving U.S. fZ 17. Transporter Acknowledgment Of RMV Of Materials Month Day Year Transporter 1 Printedl'ryped Name Signature J- G.100(541 Z Transporter 2 P W W Ty—P R rile Signature Mamh Day Yea 18. Discrepancy 18a. Discrepancy Indication Spam meaty Type ❑ Residue ❑ Partial Rejection ❑ Fug Rejection Manifest Reference Number: 181b. Alternate Fadtry (a Generator) J_ U.S. EPA ID Number r� ra+. FadWsPhone- 18c. Sgret re ofAtemate Facility (of Generator) Month Day Year a z h19 Hazardous Waste Report Management Method Codes Cie., codes for hazardous waste treatment, disposal, and recyding systems) C 1. 77 2. 3. 4. 20. Designated Facility Owner or Opera: Ceri Bmtwn of rmip(of haz&*w materials covered by the manifest except as noted in hem tao Atdod'rypeci Name Signature Month Day Yea EPA Foan8700-i2-(Rev.3-05) Previoused(tau30a obsolete DESIGNATEV FACILITY T^ GENERATOR STATE (IF REQUIRED) APPENDIX B Lab Summary Spreadsheets c o a, dac op�k d• J •--I N �..� .-1 000014 00 J V1 H W C O V r4 � 0000 NO 0000 0 � Lo y_jj Vf W N GW>1 F _LO to O� n ZZ � 000 N 6 N 0 M N l0 N 0 N N 0 0 p O D O O c, 25 D O 0 0 0 0 � J In `n O 0 n 0 N N O N CD Io N O O 0 i a00 M N Q u N 'i Gt v°vi Dl p v N v v r;°OoLnr-IWooOV O N .--I M O N o00voo�Ins � d' N e-I a,3 OC. O Em m N O N � H (aiO N O O M O d' N M 00 r, N n 00 M Ol �' Q1 01 to W V V In ri OV OV ^ a-i 00 � O� V O O� LD V O V O 0 m Y d bD Eb 000 C Y o \04 I O H 3 m O m aV o O > c C 0. E O, _ E _ co a u T v L— c0 'LO L C i N m sOO R i 2 S S t00 Q Q cL6 [D m U U U U 3 Z to in H N 0- a N E E 0 U c o a d°C 0�� O: J ri N ri 0000-4 0100 .1 N to W C E O kn Vf W VI GJ! N M M O O O O DN O O LO O Q LO O N0 0 0 0 0 N 0 N 0 N J 'n LO 0 N O N N O N `n N 0 `O O O i 000 M N U) Q U u u C) N Ln 0O 0) Ln N CD M N �n d' 00 p Ol '1 W Ol O Ln a-i l, O p -1-1 N V v v ,--� O ai co "I v Q O O v m m N O M Vl o O a N O 0) O a, 01 01 O O a' Ol O n NO Oal N N y N v 0 0 `""� d' N 0 0 r�-i V Ov Ov l� O O O V m Q N M O N 00 Ol O N O Vl m a1 N l�D O Ln Cl O N O Ln 11 N a4 v u rV vcFNoor -I 00r-I v 00 OO v v v v v 'm u CA M O O M Ln a1 O �n N O a i tD Ol � i j O�� � 1� Ln 000 ~ N M y V V t0 N 0 p� N a1 ri O� v 0 ,1 Vl 00 O O as r v Ca m C N _ 0 m m O M� 00 ' N n N M 0) p N p O 00 lD ^ O O ri M H C ^^ O V a1 V N V N O O Vl ri O rj V O O O O O q co Q m M N O Ln N Ln a-i O Ol a� u'f N O a --I 1� -4 O1 p^ al � 00 cn N N O CD p ri N M Ln V V M N O O _j N CI' a-i 0 0 -4 v pv pv lO f, 0 0 V V m N C W N O N .D O 00 ct N O 01 Ol M 0 O T 0l a1 N O O w N V lD N O O aNI a1 M 00 0 0 .�� V O O O 0 0 .;v V V V V O m W V Lfl a-1 N^ t N ri M M N lD r-Iv�o�`n ll " Cl lD lD O O 3 v v v v �noo "'��00 Oo 0 0 m c w m -V �i �i E m 04 0: � to — m y p m 4 a, E E jU O O Yz o O au o > p E ' on� a -0 ? E m Ls UZ i 'O C7 2 2 S G lO CL C i m 0) a m L -0 o Q O v O u N > N C O ra u d J U J U J 0 i H H H r4 Z V Q Q cm m U U U U J Z N I- > N O F Qq m E N w V1 CN O O m m Co mga `o 19 J c o a, °C po t tD Ix J rl N r-I rl 00� 00 J V1 H W C O O w 00 00 WU L M N N W IA > J aJ F- O O n O N N O M N � O I- N O N ci N V D Ln O LO O n O D N O CD CDO LO T p N 0 O 0 N 0 0 to 0 n 0 N 0 0 � O co N M V) Q C n ID 00 O KT O fV N 00 f� Ln rl 00 p M .-� N tD O 00 U V V V rl 0 0 '" I v E tD O O N M O Kt kD N l0 1-I M p tf1 00 ct M 0) i., 1-1 V V V " p p� rl �t ei � O 00 V O r1 M U) WLn H w O. m O 00 00 �' N Ln O t0 � 01 O 01 H u ^ N V rl N N 6 O O� rl v 0 0 0 N V v 0 V N N� CtD p Ip LO 0 N i� o0 O Vl n rl Ol V y V r1 O O rl N M lD O N v rl l0 t.f) Wm O v z a c 0 01 p O m 00 O In N a0 a)� r I � pn � m o0 u r1 0) V V V n r4 6 6 ai M .� O O^ V O O mt l0 3 v v o v v v z en Y aJ bn 00 C Y E m tor_ C0 c C= o E N 7 r a, O _ o ° u ++ E E au E E ._+ u mv O O QJ O 0 0 u > C 'O i 2 2 2 0- 9.0 L u C Q i Q m co a1 m M U t U O U O U J Z (n iN L f— m i C IV H H co Q U u � o a N �V! -0 W O L J ^O V W �+ I..L cu L N m O m O O l0 N c O d oo� D: J rl N kD ei 0No-1 00 J N Nf W c O '00 U 0 0 O tD O M O N SDI 00 c .N-I N r-I -1 CA Vf W VI 0J>! H M Lc) O� O OOD N C-1 O LO N LO I� N O N O N- M O N D O O p 0 O 0 0 0 0 0 0 O 0 0 O 0 0 O O O O O = J to � O n N QO N O N O N O N O N N N N Cl) l0 Q U U 06 pl CV*4 oo M Oi � l 00 00O 01 1 O0 N 11 O N Vl V m M rl 'D c; p 0 0,�VV ei OO � N O O O V V V V m 00 00 11 M N lN O D1 'IT c; t1 0 tD 00 In NlD O N e Cl) O 01� O I00N m m N V m O V yN V V O V V V m O O m a co p toM Ln 01 In O rn In N 1 1-0 1 I c:) Ln Ol a, o0 m CD^ 00 � , N V In o0 N O V O V -I 0.vO V O V O O V CO u O laNY L'iNlO O p N-cr - -.N M O 0) m Ot 00 O CO 0�0 mN V O V M ,-1 0 V O E C m O � m O. M IV I� n p O �: N 0 O Ln ri .q �n p ^ 0) n q� 01 O �Ln m N i N E N M N O V r1 N p O 0 V O M f0 H c m V 0 a O M N O O r1 M M It In N 00 fV M - aMi r'I O 0) 00 Ol In m N N Ln V� V^ N O O In p M 0 N o O V O O m� 0 O C V O V V V V V m u Of 00 p p V1 ^ O O In In N N O M O ei M O o In a' O N i r4 V N 0 n N O O In r1 r, N e^-I 0 rl tD V O V M m 0 ' fV ri � V m 00 ' M 00 0)� lD O N c)ne p 00 r- 00 ND O M NO O l l Om V OV � O V VV m a N 0,p r1 �D ri O p N a> mO `4 O O M OM 00 N N C V V V V p V 0 V N O V V V ii O rl m Y N 0) =tw \ \ M to E E cu fp = 00 E E \ o0 E 7 \ W p0 to r_ _7 E (u E E, w L o �; u a+ c E E 3 E E m ° CL p_ t0 :i+ v O O E >= 3 E p +� m Q -p L 0 T Y C - m U O U s U O C7 a C G L •N v v O u > f0 J J J a J LU �' 2 o_ 2 o 2 D 10 N Q - Q Q m N m m U t U O U O U Z to in F- > N F- F- F- U U 2 F- H H 00 U in v� v1 F- H L E _ E N N In N p >. M N i N aI O *' a d lL6 Q O co J c o a, o cn 00 L e-I 0000 —1-1 0 J Vf V1 W C O toO O O O O O O tD � N 00 (A Vf W V1 j J O � 000 N LO N O M N 0 f-- N CDJ~ U')l17 N— � In In N \ O O O p 0 OLO 0 OO 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0 0 IO J S O uO H O O N 00 0 N O N 0 N tO O 4 N O N O N O O N N F Cl) 0 Q u v O W O N 0CD � N al O r-I o a --I Ol 00 m 00 i i O i N N V r4 M O V V1 m Ov Ov O O v O o Ln O C lG m p Ln N I, O N 00 � �n O M O O m N i i i N V V O V l0 0 0 01 0 O N V n O O C V 00 C Q m nO O V1 .ry O N O L( O i O ri LD V M O V OVmLo �V vv vvv w, F d m O. E u H N 00 d' O O q Ln N m O 01 O n O O to O o CD N Q1 O N i Ln 00 O v N O v r-I M O r-I to I -I r-I ri M `� V O O m lWD O O O ;p V V V 00 m 00 L LI1 M O O Q1 M O m N Ln O t\ N O ct �^-I 00 O N V ^O N O rl mm ,� aW-I lD v p a I V O �O O O CD v v CO Q co O a-i N N O N Ol 00Lq O OV C/1 q �' .m-I M lD a�i I� ^ O O O M 00 N CV .--I O v M .--I M O O V v v ^ O co 00 Y \ lv OO to \ 0\O OA C toE \ OD � Ei es E zto E m c v m •E y o w o .' E E o (te, E E E o Q- -o E "p o -a 7 f0 H fp 0) O 1 O > O C C O E u o + L L ` "♦:j j., Y i_ L C U Q O U J f6 U'AO L S ca OJ 'O (7 0 C }, L I L >Z ca OJ O u > M O UU U UaaC 2 2 2 W C a L a m m ..0 U O U U Ou Z N to F- 7 N N N V) N S H H 00 U m C Np co O N co O U m ++ CO Boa O J C ho O OLO O O lDtD r-I J J LY Ln C E 0 0 0 CDp W V rN N aO-I N 00 O i�,.� J J kn W Vf LA GJ>I F O O � � O 000 U') O N O O N � t 2 t` N O 0 Q O In N D 0 :z 0 0 0 0 0 0 0 0 p 0 0 0 0 0 O- 0 Ot 0 O O O m J = O O L� 0 0 0 N 0 L O N� 0 N LLO N 00 N O O F Q F� 0 co N M LO 3 � O N N Q1 p 00 v N 0 0 cn 00 .--1 O Q? � 0 M p Ln CL N Ln v o6 o6 N O O ei aN-I U, p -i v OV OV n p p 7 N M c W 3 Q1 p N O 01 N N lD Cr .--I n IT al 0) 01 V Oi 0 0� i e-1 M � �-I � v 0 0 Ln I� p V V V V V m Y H m c LLJ NJ O H O N M N n V' M N m M r-I M O D Q1 Ql . n Ct M cn M 01 C M `-q O M p p e j d .-i pp O N I V p p h co V V V V V V V d Q. H ra H io 3 Ln n N N M l0 00 v N 0) cn 01 I� 0 O .--i T 01 LO 00 v v N Ln O O �O O r4 i N Ct V c;O 1 l0 LA 3 m 3 lD Q1 p N N O, j N N w M N 0) n v N n O M 0 O p V V V -4 O OV Ln . I N^ 0 0^ V O O M N V V W 3 Ln M Q1 N v, Ln Ln O M 00 m v 00 Ql M 1, V r-iV V v 0 0 Q1 ri M N M 6 v 0 0 6 M Y Hv V vV g H 3 Ql O O N v 01 C. N 1� pp CO lD tD O 13) co Q1 N -ber-I Ln V V v 00 e0-L D O -4 N 01 p N I� v O O M trl O F- V V V V Z Y bo N 0\0 bA c= c cc E \ \ E W E E y o,cc0 0 U ate+ c E j_ A m N = O vaJJ U cu OO E C E c � UJ O (7 O > m c VJO 0=1 U Q Q [o GJ m mLO U U U UO J Z Ln n H> N NU HCLN L m E r E p M 7 N i, CY) N O U f0 M C d O f6 J C O O O rn 00 rO r-I -1 J J H W {A C m C) ON k.0 p O lD CD U e-i N W � fV 00 J J Nf W V1 VI j J J~ LO u)O O n 0`00 N N O M N r- \ N O u) 6 6O O N o O O N 0 O O O O N 2 Q LO O n N M o N O U H n^ O Ln Q. O N 00 t0 00 p� 00 O cn O CO W Oi n Oi Ln N V N O V p p I- r-I m M p V p p 0 O H V V O O p a1 O N t0 I� O 00 O1 M n C v00 Qo �vi�oo�rAC,4 pm �ppmN u v d Z N N Q N ri rN-I l0 m Lq N - O1 M . CD L!1 . VQ1 . 00 C n. 0 0 0 v m O O `'� r-i Ln 1. 6 N V O v W o0 E C v O V V V V m H O N H N a O O T Q V1 ^ O t!'1 u1 N 00 -O 00 LO ^ 0 �--� W O O Ln Ln-I V Zo01 r4 O V� C p p ri m Q1 -4 O ni M V O V ra N O V V H 3 ^ O? 0 O m lO ry� d' N �n 00 M I� �--I V' Q1 V1 to a _ Cn ^ O N V Ln N O O `'{ N LO 1l OV M `i V O O V V O V V V V H W CD Q? O O O� Q Lfl 00 d' N � 'D 00 I� O Ol 00 �o Cl N N a y r-IV O u N u1 0 0 k0 0 r-� M o ri c» V O O u1 Ln HO rNI v v V v v Y N on \ 00 0 C w C m -V � N N C C N N E E E w C £ N � 4-1 (D o s°C� .� N U �� -a w T 1 C 7 E O 7 m O � +. m O cC L p E u .O 7 7 •>„ 7 .E m O. -a i T _ C 3 t6 U i+ vi I 'O C7 o 3 m u a + �, L L v O L O- m a, o Y u y y > u c� C == 2 t0 c N w c O Q Q to CO N [O ca U L U 0 O U O U O J 2 2 Z N in F- IV F- U i H H H 00 N L M nCl) ' i 1 ry'ArW' L N i C� C E N M :3 O !n N (O L O N O M Qa O f6 J c d 4) Oo�k o 0No-1 00a-i J Vf H W C O ba V M r4 00 to r-I H V1 W VI OJT! H tp O n 000 U)Lo N O M N f� N O N M V 0 V) Lo 0 0 N O Lo O N ll� O In N 0 Lo N 2 O^ 00 N Cl) N N O Q U W F O N m N l0 N N M Ol d' 01 W d N l0 e^-I 0 0 a --I N M O r4 ^ `� V O O M l0 •- V V V V V li 3 00 M 00 N .-i N t, w cn � N 0 0� N N -4 V1 O O M l0 0) L V ri v V C5 V V V LL 0 m M lfl N Lo N N 00 k-0 � 01 O , r Ql 00 V w N C5 O V1 a-1 N Ol 0 0 v p Ov M N L V 0) LL O. E Om H In O ry W 00 N a) N ^ O 0 e-I 4 Q1 m O 1.0 N O HCL N^ 0 0 r-I 0 •--i r-I V O O 0^ E 3 H as a L d: O r N N 00 O v N 00 Q1 � m^ O 0) m0 V1 00 flv^ N Oo OV in .- m r 00 ^ V O O^ N 00 E v 3 H 3 f' Ln cl' O N ^ O ^ cn q N 00 0)00 Ot O ^ O m N O- E I� 0i N O V O V LO M 0 Q) V O V O v m O m p 7 H V Y \ O) O0 E 00 m bn C w Y E \ \ 0 O w o E a 3 E E O L O U �O O "p E C E E ru f6 N 0) U � 7 -_ 7 '� E '' L t.. U N '� L U M J f6 J H O C� C C C N •% �' "a -0 Q t�0 v O u > — _ O U U a 0 CL CL a- LO v Q L Q m m w m l6 U L U O U O U y J c G c G Z 0) N (n s H N N F _ coN APPENDIX C Site Photographs - West Wall & Excavation Floor. . � � • ,� � ., �- -'` �� .fir—��. ^ram. :. .�. � � . �.. v �~ .:.T � �.� Ar;, V •, •ram•: r.. rr Y VIP 4.111 Lox .� _� � -X� y"• r,'�:� � _ � .- sir � ~t•� M�'� 1'4, • .. F �. � '� -r err- .� ��• ��-..� - �'r �: w.+ +. JYZI r�, r Ve Ile ICI' tny� r • '�r - .+wx -_ _ ,tit � •�,� tk:7 pp, I - 'd e di 7 Excavation Floor. 40. 4F AV, A i East Wall. East and South Wall fo Aft Ik )1% "el gr • _� •tea r" •1 - 1 .�` ` R _ ' - •~5 r �" � �w �/ � ■ WA _ w.�rrf� s 1+ � ry. �;�.. -ram � . • .{ ..,„��-��;�,�Rr!`,�-�r � :ar.=- Sir' 11 Jw " •rr - r+tea � -j �,. f � .'_ _ ..�.�,'1. . f _ - yL.�/ �L}��''�_ � � �� .'. - ',1 � ,' � i � , {ice ., J_ ti. • � � � ', � • t APPENDIX D Laboratory Reports & Chain of Custody Forms Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2103479 Pacific Petroleum California P. O. Box 2646 Report Date: June 09, 2021 16:44 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com This laboratory is accredited in accordance with the recognised International Standard ISO/IEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-1AF Communiaue dated Apri12017) 307 Roemer Way, Suite 300 .��'t�tl�ltl`'/�. client.oec.com\reports Santa Maria, CA 93454 www.oecusa.com o Main: (805) 922-4772 PJLA TNI 2016 & ISO/IEC 17025:2017 Fax: (805) 925-3376 :j ���.�� 'Msao9 CA-ELAP 2438, TNI 02666 Accreditation N99137 Page 1 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom East @ 12' 2103479-01 Solid Solid 06/03/2021 11:50 06/04/2021 12:50 Bottom West @ 12' 2103479-02 Solid Solid 06/03/2021 11:55 06/04/2021 12:50 Sample Batch Preparation Summary Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatoerams Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List BIF0145 06/04/2021 16:24 STLC Metals by ICP 6010E STLC 131F0261 06/09/2021 08:56 STLC Metals Extraction STLC Metals Extraction B 1 F0229 06/07/2021 16:29 Total Metals by CVAA Mercury Total EPA 7471A B1F0194 06/07/2021 07:40 Total Metals by ICP 6010B Total B 1 F0197 06/07/2021 08:26 Volatile Organic Compounds by GC/MS 8260B Full List B I F0146 06/04/2021 12:21 Volatile Organic TPH by GC/F1D 8015 'ITH-Gasoline B 1 F0154 06/04/2021 10:34 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mg!kg 1 BIF0194 06/07/21 16:25 EPA 7471A Total Metals by ICP Antimony ND 2.3 mgtkg 1 B 1 F0197 06/07/21 14:12 EPA 601 OB Arsenic 5.6 1.9 " Barium 120 0.93 " Beryllium ND 0.47 Cadmium ND 0.23 Chromium 73 0.47 " Cobalt 18 0.47 " Copper 47 0.93 " Lead 8.2 0.47 " Molvbdenum ND 0.47 " Nickel 130 0.47 " Selenium ND 1.9 Silver ND 0.47 " Thallium ND 0.93 " Vanadium 49 1.9 " Zinc 65 1.9 " STLC Metals by ICP Chromium ND 0.020 mg/E, 2 BIF0261 06/09/21 14:34 STI.C/EPA 601 OB Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.5 mg/kg 1 BIF0154 06/04/21 17:01 EPA 8015M Surrogate: 4-BromoJluorohenzene 92 N, (39 - 157) 11 " 11 N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-C22) ND 10 TPH Motor Oil (('23-C40) ND 50 Surrogate: o-TeiphettrJ N7 mgtkg 1 B 1 F0145 06/05/21 12:12 EPA 8015M (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 4 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kg I BI F0146 06/04/21 16:16 EPA 8260B Bromobenzene ND 0.050 " Bmmocliloromethane ND 0.050 Bromodichloromethane ND 0.050 Bromofurm ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 " Chlorobenzcnc ND 0.050 Chloroethanc ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-C6lorotoluene ND 0.050 4-C'hlorotoluene ND 0.050 " Dibromochloromethane ND 0.050 1.2-Dibromo-3-chloropropane ND 0.050 1,2-Dibromoethane (EDB) ND 0.050 Dibromomethane ND 0.050 1,2-Dichlorobenzene ND 0.050 1,3-Dichlorobenzene ND 0.050 1,4-Dichlorobenzene ND 0.050 Dichloroditluoromethane ND 0.050 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 I,1-Dichloroethene ND 0.050 cis-1,2-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 1,3-Dichloropropane ND 0.050 2.2-Dichloropropane ND 0.050 1, 1 -Dichloropropene ND 0.050 cis- 1.3-Dichloropropene ND 0.050 " trans-l.3-Dichloropropene ND 0.00 F.thylbenzenc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCHI CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 wrww.oecusa.com FAX: (805) 925-3376 Page 5 of 32 (MOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.050 mg/kg 1 BIF0146 06/04/21 16:16 EPA8260B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1, 1, 1,2-Tetrachloroethane ND 0.050 1,1,2.2-1'etrachloroethane ND 0.050 Tctrachlorocthcnc IPCE) ND 0,050 Toluene ND 0,050 1,2,3-Trichlorobcn7cnc ND 0.050 1,2,4-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorofluoromethane ND 0.050 " 1,2.3-Trichloropropane ND 0.050 1,24-77inrethylbenzene ND 0.050 " 1,3,5-Trimethylbenzene ND 0.050 " Vinyl chloride ND 0.050 " Xylenes (total) ND 0.050 Surrogate: Dihrowno/lnoromethatur 103 %, ( 74 - 122 ) Surrogate: Tohuene-db' 99 % (65 - 12Y) Surrogate: 4-Bromo/luo •ohen_ene l05 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 6 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID: Bottom West @ 12' Sampled : 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg I B 1 F(1194 06/07/21 16:27 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I BIF0197 06/07/21 14:15 EPA 6010B Arsenic 7.4 1.9 Barium 160 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 51 0.49 Cobalt 14 0.48 Copper 63 0.96 Lead 8.9 0.48 Molybdenum 0.57 0.48 Nickel 88 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 " Vanadium 52 1.9 Zinc 71 1.9 STLC Metals by ICP Chromium ND 0.020 mg/L 2 B IF0261 06/09/2) 14:37 STLC/EPA 6010B Volatile Organic TPH by GUND TPil Gasoline (C5-('12) ND 4.4 uig.tkg 1 BIF0154 06/04/21 17:29 EPA 8015M Surrogate: 4-Brotng1luoroben_ene 95 (39 - 157) 11" 11 N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C 13-('22) ND 9.9 TP11 Motor Oil (C23-C40) ND 50 Surrogate: o-Teipheni'l 90 mg/kg l B 1 F0145 06/05/21 12:34 EPA 8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID : Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.048 mgtkg 1 B 1 F0146 06/04/21 15:48 EPA 8260B Bromobenzene ND 0.048 " Bromochloromethane ND 0.048 Bromodichloromethane ND 0.048 Bromoform ND 0.048 " Bromomethane ND 0.048 n-Butylbenzene ND 0.048 " sec-Butylbenzene ND 0.048 tert-Butylbenzene ND 0.048 Carbon tetrachloride ND 0.048 Chlorobenzene ND 0.048 " Chloroethane ND 0.048 Chloroform ND 0.048 Chloromethane ND 0.048 2-Chlorotoluene ND 0.048 4-Chlorotoluene ND 0,048 " Dibromochloromethane ND 0.048 1.2-Dibromo-3-chloropropane ND 0.048 1,2-Dibronioethane (EDB) ND 0.048 Dibromomethane ND 0.048 1,2-Dichlorobenzenc ND 0.048 1.3-Dichlorobenzenc ND 0.048 I A-Dichlorobenzenc ND 0.048 DichlorodiFluoromcthane ND 0.048 1,1-Dichloroethane ND 0.048 12-Dichloroethane ND 0.048 1, 1 -Dichloroethene ND 0.048 cis-1,2-Dichloroethene ND 0.048 " trans-1,2-Dichloroethene ND 0.048 1,2-Dichloropropane ND 0.048 1,3-Dichloropropane ND 0.048 22-Dichloropropane ND 0.048 1, 1 -Dichloropropene ND 0.048 cis- 1.3-Dichloropropene ND 0.048 trans-1,3-Dichloropropene ND 0.048 Ethylbenzi ne ND 0.048 CCHI The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Anal a Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 0.048 mg/kg 1 BIF0146 06/04/21 15:48 FPA8200B 4-1sopropyl Toluene ND 0.048 Isopropylbenzene ND 0.048 Methylene chloride ND 0.048 Naphthalene ND 0.048 n-Propylbenzene ND 0.048 Styrene ND 0.048 1, 1, 1,2-Tetrachloroethane ND 0.048 1,1,2,2-Tetrachloroethanc ND 0.048 Tctrachlorocthcnc (PC[,") ND 0.048 Toluene ND 0.048 1,2,3-Trichloroben7ene ND 0.048 1,2,4-Triehlorobenzene ND 0.048 1,1,1-Trichloroethane ND 0.048 1,1,2-Trichloroethane ND 0.048 Trichloroethane (TCE) ND 0.048 Trichlorotluoromethane ND 0.048 1.2,3-Trichloropropane ND 0.048 1.2,4-Trimethylbenzene ND 0.048 1.3,5- rimethylbenzenc ND 0.048 Vinyl chloride ND 0.048 Xylcncs (total) ND 0.048 Surrogate: Dibronwlluorowethane 104 ` (74 - 122) " Surrogate: Toluene-d8 102 / (65 - 128) " Sm'rogate: 4-Brumn/luuruhen_ene 104 ``/n (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805 925-3376 Page 10 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by CN7AA - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0194 - EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (Bl F0194-BLKI) Analyzed: 06/07/21 12:49 Mercury ND 0.10 mg/kg LCS (B1F0194-BS1) Analyzed: 06/07/21 12:53 Mercury 0.782 0.10 mg/kg 0.833 94 85-115 LCS Dup (B1F0194-BSD1) Analyzed: 06/07/21 13:30 Mercury 0.859 0.10 mg/kg 0.833 103 85-115 9 20 Duplicate (B1F0194-DUP1) Source: 2103489-02 Analyzed: 06/07/21 13:34 Mercury ND 0.097 mglkg ND 20 Matrix Spike (B1F0194-MS1) Source: 2103489-02 Analyzed: 06/07/21 13:37 Mercury 0.827 0.091 mg/kg 0.755 ND 110 75-125 Matrix Spike Dup (B1F0194-MSDI) Source: 2103489-02 Analyzed: 06/07/21 13:39 Mercury 0.839 0.089 mgJkg 0.742 ND 113 75-125 1 20 Post Spike (B1F0194-PSI) Source: 2103489-02 Analyzed: 06/07/21 13:41 Mercury 5.52 ug/L 25.0 0.00199 22 85-115 Ql, 02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 32 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLK1) Analyzed: 06/07/21 13:30 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND LO " Lead ND 0.50 Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 " Thallium ND LO Vanadium ND 2.0 Zinc ND 2.0 LCS (B1F0197-BSI) Analyzed: 06/07/21 13:35 Antimony 92.0 2.5 mgtkg 100 92 80-120 Arsenic 97.2 2.0 100 97 80-120 Barium 99.6 1.0 100 100 80-120 Beryllium 95.1 0.50 100 95 80-120 Cadmium 98.2 0.25 100 98 80-120 Chromium 98.8 0.50 100 99 80-120 Cobalt 99.2 0.50 100 99 80-120 Copper 98.2 1.0 100 98 80-120 Lead 100 0.50 100 100 80-120 Molvbdenum 96.0 0.50 100 96 80-120 Nickcl 99.6 0.50 100 100 80-120 Selenium 96.4 2.0 100 96 80-120 Silver 4.92 0.50 5.00 98 80-120 Thallium 100 1.0 100 100 80-120 Vanadium 96.6 2.0 100 97 80-120 Zinc 98.6 2.0 100 99 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 w vw.oecusa.com FAX: 8051 925-3376 Page 12 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ControlTotal Metals by ICP - Quality AnaIyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSD1) Analyzed: 06/07/21 13:37 Antimony 94.8 2.5 mg/kg 100 95 80-120 3 20 Arsenic 98.8 2.0 100 99 80-120 2 20 Barium 101 1.0 100 101 80-120 1 20 Beryllium 96.5 0.50 100 96 80-120 l 20 Cadmium 99.2 0.25 100 99 80-120 1 20 Chromium 100 0.50 100 100 80-120 1 20 Cobalt 100 0.50 100 100 80-120 l 20 Copper 99.8 1.0 100 100 80-120 2 20 Lead 101 0.50 100 101 80-120 1 20 Molybdenum 98.2 0.50 100 98 80-120 2 20 Nickel 101 0.50 100 101 80-120 1 20 Selenium 97.8 2.0 100 98 80-120 1 20 Silver 4.93 0.50 5.00 99 80-120 0.1 20 Thallium 102 1.0 100 102 80-120 1 20 Vanadium 98.0 2.0 100 98 80-120 I 20 Zinc 99.8 2.0 100 100 80-120 1 20 Duplicate (B1F0197-DUPI) Source: 2103489-01 Analyzed: 06/07/21 13:52 Antimony ND 2.4 mg/kg ND 20 Arsenic 1.22 1.9 ND 20 Barium 21.0 0.97 22.9 8 20 Beryllium ND 0.49 " ND 20 Cadmium ND 0.24 ND 20 Chromium 1.94 0.49 2.02 4 20 Cobalt 1.40 0.49 1.78 24 20 QR-04 Copper 1.33 0.97 1.40 5 20 Lead 1.23 0.49 1.40 13 20 Molvbdenutn ND 0.49 ND 20 Nickc] 1.31 0.49 1.34 2 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 3.80 1.9 4.18 8 20 Zinc 4.32 1.9 4.51 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:; 805 925-3376 Page 13 of 32 -4mv AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ControlTotal Metals by JCP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MS1) Source: 2103489-01 Analyzed: 06/07/21 13:40 Antimony 70.3 2.3 mg/kg 93.4 ND 75 10-116 Arsenic 93.3 1.9 93.4 ND 100 77-121 Barium 119 0.93 93.4 22.9 102 30-169 Beryllium 90.1 0.47 93.4 ND 96 86-111 Cadmium 91.8 0.23 93.4 ND 98 81-112 Chromium 96.8 0.47 93.4 2.02 102 75-129 Cobalt 94.2 0.47 93.4 1.78 99 71-121 Copper 96.2 0.93 93.4 1.40 102 68-135 Lead 94.4 0.47 93.4 1.40 100 72-121 Molybdenum 88.2 0.47 93.4 ND 94 70-112 Nickel 95.2 0.47 93.4 1.34 101 73-121 Selenium 90.1 1.9 93.4 ND 97 76-116 Silver 4.56 0.47 4.67 ND 98 54-132 Thallium 92.3 0.93 93.4 ND 99 64-120 Vanadium 96.5 1.9 93.4 4.18 99 78-124 Zinc 98.0 1.9 93.4 4.51 100 50-143 Matrix Spike Dup (B1F0197-MSD1) Source: 2103489-01 Analyzed: 06/07/21 13:42 Antimony 70.4 2.4 mg/kg 95.8 ND 73 10-116 Q1 20 Arsenic 94.3 1.9 95.8 ND 98 77-121 1 20 Barium 116 0.96 95.8 22.9 97 30-169 3 20 Beryllium 91.2 0.48 95.8 ND 95 86-I11 1 20 Cadmium 92.3 0.24 95.8 ND 96 81-112 0.6 20 Chromium 97.6 0.48 95.8 2.02 100 75-129 0.8 20 Cobalt 94.7 0.48 95.8 1.78 97 71-121 0.6 20 Copper 96.9 0.96 95.8 1.40 100 68-135 0.7 20 Lead 94.9 0.48 95.8 1.40 98 72-121 0.6 20 Molybdenum 88.6 0.48 95.9 ND 93 70-112 0.5 20 Nickel 95.5 0.48 95.8 1.34 98 73-121 0.3 20 Selenium 91.2 1.9 95.8 ND 95 76-116 1 20 Silver 4.64 0.48 4.79 ND 97 54-132 2 20 Thallium 93.1 0.96 95.9 ND 97 64-120 0.9 20 Vanadium 97.2 1.9 95.8 4.18 97 78-124 0.7 20 Zinc 103 L9 95.9 4.51 103 50-143 5 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 32 ( A WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PS1) Source: 2103489-01 Analyzed: 06/07/21 13:45 Antimony 2.03 mg/L 2.00 0.00248 101 75-125 Arsenic 2.04 2.00 0.0178 101 75-125 Barium 2.50 2.00 0.460 102 75-125 Beryllium 1.96 2.00 0.00219 98 75-125 Cadmium 2.00 2.00 -0.00308 100 75-125 Chromium 2.07 2.00 0.0408 101 75-125 Cobalt 2.06 2.00 0.0359 101 75-125 Copper 2.06 2.00 0.0293 102 75-125 Lead 2.07 2.00 0.0283 102 75-125 Molybdenum 2.01 2.00 -0.00109 101 75-125 Nickel 2.06 2.00 0.0271 102 75-125 Selenium 199 2.00 -0.0103 99 75-125 Silver 0.0945 0.100 -0.00169 94 75-125 Thallium 2.03 2.00 -0.00407 101 75-125 Vanadium 2.08 2.00 0.0842 100 75-125 Zinc 2.10 2.00 0.0909 MI 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 STLC Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0261 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (B1F0261-BLK1) Analyzed: 06/09/21 13:50 Chromium ND 0.010 mg/L LCS (B1F0261-BSI) Analyzed: 06/09/21 14:17 Chromium 10.1 0.010 mg/l, 10.0 LCS Dup (B1F0261-BSDI) Analyzed: 06/09/21 14:19 Chromium 10.2 0.010 mg/L 10.0 Duplicate (BlF0261-DUPl) Source: 2103218-01 Analyzed: 06/09/21 14:27 Chromium 1.22 0.020 mg/L 1.22 Leach Fluid Blank (B1F0261-LBKI) Analyzed: 06/09/21 13:52 Chromium ND 0.020 mg/L Leach Fluid Blank (B1F0261-LBK2) Analyzed: 06/09/21 13:55 Chromium ND 0.020 mJL Leach Fluid Blank (BlF0261-LBK3) Analyzed: 06/09/21 13:58 Chromium ND 0.020 mg/L 101 80-120 102 80-120 0.5 20 0.08 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLKl) Analyzed: 06/04/21 12:45 TPH Gasoline (C5-('12) ND 0.49 mg/kg Surrogate:4-Bromo/luorobenzene 0.107 " 0.123 87 39-157 LCS (B1F0154-BS1) Analyzed: 06/04/21 11:48 TPH Gasoline (('5-C 12) 1.38 0.50 mg/kg 0.999 139 68-139 Surrogate 4-Bromulluorohenzene 0.158 110.125 126 39-157 LCS Dup (B1F0154-BSD1) Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12) 1.29 0.50 mg/kg 1.00 128 68-139 7 20 Surrogate:4-Bromq/luorohenzene 0.146 0.125 116 39-157 Duplicate (B1F0154-DUPl) Source: 2103455-02RE1 Analyzed: 06/04/21 15:35 TPH Gasoline (('5-('12) ND 0.50 mg/kg 0.113 20 Surrogate:4-Bromolluorohenzene 0.113 " 0.124 92 39-157 Matrix Spike (B1F0154-MS1) Source: 2103429-02 Analyzed: 06/04/21 19:23 TPH Gasoline (('5-C12) 0.905 0.49 mg/kg 0.973 ND 93 10-171 Surrogate:4-Bromnlluoroben_ene 0.132 110.122 109 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 17 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Semi-Volatile1 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) Analyzed: 06/04/21 11:45 TPII Diesel (C13-('22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 " Surrogate: o-Teiphenrl 41.5 1150.0 83 65-136 LCS (B1F0145-BSI) Analyzed: 06/04/21 11:45 TPH Diesel (('13-C22) 434 10 mg/kg 499 87 72-115 TPH Motor Oil (('23-C40) 420 50 499 84 74-126 Surrogate. o-Teiphenyl 45.8 49.9 92 65-136 LCS Dup (B1F0145-BSD1) Analyzed: 06/04/21 12:07 TPH Diesel (C13-C22) 444 10 mg/kg 499 89 72-115 2 20 TPI1 Motor Oil (C23-C40) 441 50 499 88 74-126 5 20 Surrogate: o-TciphenYl 46.7 49.9 94 65-136 Duplicate (B1F0145-DUPl) Source: 2103472-01 Analyzed: 06/04/21 16:23 TPH Diesel (C13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Teiphem,l 40.5 49.9 81 65-136 Matrix Spike (111170145-MSI) Source: 2103472-01 Analyzed: 06/04/21 15:37 TPH Diesel (C13-('22) 452 10 mg/kg 498 ND 91 46-147 TPH Motor Oil (C23-C40) 500 50 498 ND 100 35-171 Surrogate: o-Teiphenrnl 41.6 49.8 84 65-136 Matrix Spike Dup (B1F0145-MSD1) Source: 2103472-01 Analyzed: 06/04/21 16:00 TPH Diesel (('.13-C22) 496 10 mg/kg 498 ND 100 46-147 9 20 TPH Motor Oil (C23-C40) 517 50 498 ND 104 35-171 3 20 Surrogate: o-T,iphenyl 44.0 49.8 88 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX- [805; 925-3376 c Page 18 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLKI) Analyzed: 06/04/21 11:32 Benzene ND 0.0050 mg/kg Bromobenzene NI) 0.0050 " Bromochlorotnethanc ND 0.0050 " Bromodichloromethane NJ) 0.0050 Bromoform ND 0.0050 Bromomethane ND 0.0050 " n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 " Carbon tetrachloride NI) 0.0050 Chlorobenzene ND 0.0050 " Chloroethane ND 0.0050 " Chloroform N1.) 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorot0luene ND 0.0050 Dibromochloromethane ND 0.0050 1,2-Dibromo-3-chloropropane ND 0.0050 1.2-Dibromoethane (F.DB) ND 0.0050 " Dibromomcthane ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " 0-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 " Dichloroditluoromcthane ND 0.0050 1,1-Dichloroethene ND 0.0050 " 1,2-Dichloroethanc ND 0.0050 1, 1 -Dichloroethene ND 0.0050 " cis-L2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene NI) 0.0050 1,2-Dichloropropane NI) 0.0050 " 1,3-Dichloropropane ND 0.0050 " 2,2-Dichloropropane ND 0.0050 " 1, 1 -Dichloropropene ND 0.0050 " cis- I3-Dichloropropene ND 0.0050 " trans- l,3-Dichloropropene ND 0.0050 " Ethylbenzene ND 0,0050 Hexachlorobutadiene ND 0.0050 4-Isopropyl Toluene N1) 0.0050 Isopropylbenzene ND 0.0050 " Nlethylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene NI) 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCHI CA-ELAP 2438, TN102666 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 o f 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes ILevel Result Limits Limit Batch BIF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLKI) Analyzed: 06/04/21 11:32 Styrene ND 0.0050 mgtkg 1, 1, 1,2-Tetrachloroethane ND 0A050 1,1.2,2-Tctrachlorocthanc ND 0.0050 Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 1,2.3-Trichlorobenzene ND 0.0050 " 1,2,4-1'richlorobenzene ND 0.0050 " 1, 1, 1 -Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 " Trichloroethane (TCE) ND 0.0050 " Trichlorofluoromethane ND 0.0050 " 1,2,3-Trichloropropane ND 0.0050 " 1.2,4-Trimethylbenzene ND 0.0050 1,3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 " Surrogate: Dibronrgiluoromethane 0.0516 0.0498 104 74-122 Surrogate: Toluene-d8 0.0503 0.0498 101 65-128 Surrogate:4-Bronto/luorohen_ene 0.0529 0.0498 106 75-121 LCS (B1F0146-BS1) Analyzed: 06/04/21 09:47 Benzene 0.0406 0.0050 mg/kg 0.0398 102 70-131 Brontobenzene 0.0466 0.0050 0.0398 117 74-130 Bromochloronicthanc 0.0399 0.0050 0.0398 100 64-133 Bromodichloromethane 0.0445 0.0050 0.0399 112 69-137 Bromotbrm 0.0447 0.0050 0.0398 112 55-132 Bromomethane 0.0407 0.0050 0.0398 102 10-142 n-Butylbenzene 0.0476 0.0050 0.0398 120 64-156 sec-Butylbenzene 0.0493 0.0050 0.0398 124 75-155 tert-Butylbenzene 0.0492 0.0050 0.0398 121 74-144 Carbon tetrachloride 0.0442 0.0050 0.0399 111 67-135 Chlorobenzene 0.0445 0.0050 0.0398 112 73-134 Chloroethane 0.0390 0.0050 0.0399 98 10-167 Chlorofonn 0,0412 0.0050 0.0398 104 69-124 Chloromethane 0.0297 0.0050 0.0398 75 34-136 2-Chlorotohiene 0.0454 0.0050 0.0398 114 75-135 4-ChlorotolLien e 0.0460 0.0050 0.0398 116 70-138 Dibronx>chloromethane 0.0439 0.0050 0.0398 110 67-135 1,2-Dibromo-3-chloropropane 0.0435 0.0050 0.0398 109 41-149 1,2-Dibromoethane (EDB) 0.0409 0.0050 0.0398 103 68-131 Dibronwmcthanc 0.0433 0.0050 0.0398 109 61-140 1,2-Dichlorobenzene 0.0458 0.0050 0.0398 115 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BSI) Analyzed: 06/04/21 09:47 13-Dichlorobenzenc 0.0462 0.0050 mg/kg 0.0398 116 76-138 1,4-Dichlorobenzene 0.0457 0.0050 0.0398 115 72-132 Dichlorodifluoromcthanc 0.0210 0.0050 0.0398 53 10-155 I,l-Dichloroethane 0.0389 0.0050 0.0398 98 63-139 1,2-Dichloroethane 0.0416 0.0050 0.0398 104 64-126 l,l-Dichloroethene 0.0342 0.0050 0.0398 86 52-167 cis-L2-Dichloroethene 0.0401 0.0050 0,0398 101 70-135 trans-1,2-Dichloroethene 0.0392 0.0050 0.0398 99 67-147 1.2-Dichloropropane 0.0406 0.0050 0.0398 102 68-131 1,3-Dichloropropane 0.0405 0.0050 0.0398 102 64-128 2,2-Dichloropropane 0.0432 0.0050 0.0398 109 63-154 1,1-Dichloropropene 0.0393 0.0050 0.0398 99 68-138 cis-1.3-Dichloropropene 0.0416 0.0050 0.0398 105 72-134 trans-1,3-Dichloropropene 0.0437 0.0050 0.0398 110 69-132 Ethylbenzene 0.0449 0.0050 " 0.0398 113 68-136 Ilexachlorobutadiene 0.0540 0.0050 0.0398 137 72-198 4-Isopropyl Toluene 0.0504 0.0050 0.0398 127 74-150 Isopropylbenzene 0.0473 0.0050 0.0398 119 71-149 Methylene chloride 0.0346 0.0050 0.0398 87 51-127 Naphthalene 0.0482 0.0050 0.0398 121 57-158 n-Propylbenzene 0.0474 0.0050 0.0398 119 70-143 Styrene 0.0456 0.0050 0.0398 115 68-138 1, 1, 1,2-Tetrachloroethanc 0.0459 0.0050 0.0398 115 76-130 1,1,2,2-1'etrachlorocthanc 0.0399 0.0050 0.0398 100 60-136 Tetrachloroethene(PCE) 0.0443 0.0050 0.0399 111 73-135 Toluene 0.0430 0.0050 0.0398 108 72-128 1,2,3-Triclilorobenzene 0.0507 0.0050 0.0399 127 61-166 1,2.4-Trichlorobenzene 0.0502 0.0050 0.0398 126 71-158 1,1.1-Trichloroethane 0.0424 0.0050 0.0398 107 71-135 1,1.2-Trichloroethane 0.0414 0.0050 0.0398 104 64-132 Trichloroethene (TCE) 0.0442 0.0050 0.0398 111 74-139 Trichlorofluoromethane 0.0429 0.0050 0.0398 108 30-156 1,2,3-Trichloropropane 0.0452 0.0050 0.0398 114 67-123 1,2.4-Trimethylbenzene 0.0454 0.0050 O10398 114 68-134 13,5-Trimethylbenzene 0.0461 0.0050 0.0398 116 71-140 Vinyl chloride 0.0326 0.0050 0.0398 82 43-144 Xylenes (total) 0.133 0.0050 0.119 112 69-138 Surrogate: Dibronu)lluoromethattc, 0.0525 0.0497 106 74-122 Surrogate: Toluene-dS 0.0517 0.0497 104 65-128 Surrogate:4-BromoJlnorobenfene 0.0530 0.0497 107 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCFH CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 21 of 32 044M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSDI) Analyzed: 06/04/21 10:13 Benzene 0.0423 0.0050 mgikg 0.0400 106 70-131 4 20 Bromobenzene 0.0498 0.0050 0.0400 124 74-130 7 20 Bromochloromcthanc 0.0412 0.0050 0.0400 103 64-133 3 20 Bromodichloromethane 0.0455 0.0050 0.0400 114 69-137 2 20 Bromotorm 0.0458 0.0050 0.0400 115 55-132 2 20 Bromomethane 0.0391 0.0050 0.0400 98 10-142 4 20 n-Butylbenzene 0.0476 0.0050 0.0400 119 64-156 0.1 20 sec-Butylbenzene 0.0508 0.0050 0.0400 127 75-155 3 20 tert-Butylbenzene 0.0496 0.0050 0.0400 124 74-144 3 20 Carbon tetrachloride 0.0456 0.0050 0.0400 114 67-135 3 20 Chlorobenzene 0.0457 0.0050 0.0400 114 73-134 3 20 Chloroethane 0.0394 0.0050 0.0400 98 10-167 1 20 Chloroform 0.0421 0.0050 0.0400 105 69-124 2 20 Chloromethane 0.0308 0.0050 0.0400 77 34-136 4 20 2-Chlorotoluene 0.0452 0.0050 0.0400 113 75-135 0.4 20 4-Chlorotoluene 0.0468 0.0050 0.0400 117 70-138 2 20 Dibromochloromethane 0.0463 0.0050 0.0400 116 67-135 5 20 1,2-Dibronui-3-chloropropane 0.0461 0.0050 0.0400 115 41-149 6 20 1,2-Dibromoethane (EDB) 0.0422 0.0050 0.0400 105 68-131 3 20 Dibromomcthanc 0.0459 0.0050 0.0400 115 61-140 6 20 1,2-Dichlorobenzene 0.0472 0,0050 0.0400 118 76-136 3 20 1,3-Dichlorobenzene 0.0499 0.0050 0.0400 122 76-138 6 20 1,4-Dichlorobenzene 0.0472 0.0050 0.0400 118 72-132 3 20 Dichloroditluoromethanc 0.0228 0.0050 0.0400 57 10-155 8 20 1.1-Dichloroethene 0.0405 0.0050 0.0400 101 63-139 4 20 1,2-Dichlorocthane 0.0425 0.0050 0.0400 106 64-126 2 20 I,1-Dichloroethene 0.0347 0.0050 0.0400 87 52-167 2 20 cis-1,2-Dichloroethene 0.0420 0.0050 0.0400 105 70-135 5 20 trans-1,2-Dichloroethene 0.0401 0.0050 0.0400 100 67-147 2 20 1,2-Dichloropropane 0.0430 0.0050 0.0400 107 68-131 6 20 1,3-Dichloropropane 0.0426 0.0050 0.0400 106 64-128 5 20 22-Dichloropropane 0.0446 0.0050 0.0400 111 63-154 3 20 1, 1 -Dichloropropene 0.0406 0.0050 0.0400 102 68-138 3 20 cis-1.3-Dichloropropene 0.0434 0.0050 0.0400 108 72-134 4 20 trans-1,3-Dichloropropene 0.0454 0.0050 0.0400 114 69-132 4 20 Ethvlbenzene 0.0470 0.0050 0.0400 Hs s 68-136 5 20 Hexachlorobutadiene 0.0549 0.0050 0.0400 137 72-198 0.5 20 4-Isopropyl Toluene 0.0514 0.0050 0.0400 128 74-150 2 20 Isopropylbenzene 0.0499 0.0050 0.0400 125 71-149 5 20 Methylene chloride 0.0360 0.0050 0.0400 90 51-127 4 20 Naphthalene 0.0511 0.0050 0.0400 128 57-158 6 20 n-Propylbenzene 0.0466 0.0050 0.0400 116 70-143 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. CCFH CA-ELAP 2438, TN102666 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic CompoundsQuality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSDl) Analyzed: 06/04/21 10:13 Styrene 0.0479 0.0050 mg/kg 0.0400 120 68-138 5 20 1,1.1,2-Tetrachloroethane 0.0490 0.0050 0.0400 123 76-130 7 20 1,1,2,2-Tetrachloroethane 0.0417 0.0050 0.0400 104 60-136 5 20 Tetrachloroethane (PCE) 0.0454 0.0050 0.0400 114 73-138 3 20 Toluene 0.0439 0.0050 0.0400 110 72-128 2 20 1,2,3-Triclilorobenzene 0.0520 0.0050 0.0400 130 61-166 3 20 1,2.4-Trichloroben7ene 0.0512 0.0050 0.0400 128 71-158 2 20 1, 1, 1 -Trichloroethane 0.0432 0.0050 0.0400 108 71-135 2 20 1.1,2-Trichloroethane 0.0448 0.0050 0.0400 112 64-132 8 20 Trichloroethene (TCE) 0.0448 0.0050 0.0400 112 74-139 1 20 Trichlorofluoromethane 0.0430 0.0050 0.0400 107 30-156 0.1 20 1,2,3-Trichloropropane 0.0463 0.0050 0.0400 116 67-123 3 20 1.2,4-Trimethylbenzene 0.0459 0.0050 0.0400 115 68-134 1 20 1,3,5-Trim ethyl benzene 0.0465 0.0050 0.0400 116 71-140 0.9 20 Vinyl chloride 0.0338 0.0050 0.0410 84 43-144 3 20 Xylenes (total) 0.139 0.0050 0.120 116 69-138 4 20 Surrogate: Dibranu)%hror,tntt•thttnt, 0.0519 0.0500 104 74-122 Surrogate: Tohtene-d8 0.0510 0.0500 102 65-128 Surrogate:4-Bromofluorohen_eue 0.0530 0.0500 106 75-121 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 IS1oHS Benzene ND 0.0050 mgIg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromcthanc ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 test-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-1)ibromo-3-chloropropanc ND 0.0050 ND 20 1,2-Dibromoethane (EDI3) ND 0.0050 ND 20 Dibromomcthanc ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 23 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilet poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate (B1F0146-DUPl) Source: 2103474-01 Analyzed: 06/04/21 15:22 ISloovS 1,3-Dichlorobenzene ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 DichIorodi11uoromethane ND 0.0050 " ND 20 CCHI 1, 1 -Dichloroethane ND 0.0050 ND 20 1,2-Dichloroethane ND 0.0050 ND 20 I,1-Dichloroethene ND 0.0050 ND 20 cis-1.2-Dichloroethene ND 0.0050 ND 20 trans-l.2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1, 1 -Dichloropropene ND 0.0050 ND 20 cis-1,3-Dichloropropene ND 0.0050 ND 20 trans- l,3-Dichloropropene ND 0.0050 ND 20 Iithylbenzene ND 0.0050 ND 20 1lexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane ND 0.0050 ND 20 1,1.2,2-Tetrachloroethane ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,23-Trichlorobenzene ND 0.0050 ND 20 1.2,4-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1.12-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TC'E) ND 0.0050 ND 20 Trichlorofluoromethane ND 0.0050 ND 20 1,2,3-Trichloropropane ND 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1,3.5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibromo luoromcthane 0.0538 0.0498 108 74-122 Surrogate. Tohiene-d8 0.0509 0.0498 102 05-128 Surrogate:4-Bromglluorohenaene 0.0506 0.0498 102 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cllent. oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 24 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sampleod Summary alysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELARNELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP,NF.LAP STLC Metals by ICP 601013 STLC Chromium STLC/EPA 6010E Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Water OEC. Internal Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, Internal Total Metals by ICP 6010B Total Antimony EPA 601013 Solid OEC, CA-ELAPNELAP 6010B Total Arsenic EPA 6010B Solid OEC, CA-ELARNELAP 6010E Total Barium EPA 6010B Solid OEC, CA-1LARNELAP 6010B Total Beryllium EPA 6010B Solid OEC, CA-ELAP,NEI,AP 6010E Total Cadmium EPA 6010B Solid OEC, CA-ELARNELAP 6010E Total Chromium EI'A 6010B Solid OEC, CA-F.LAP,NELAP 601013 Total Cobalt EPA 6010E Solid OFC, CA-ELAPNELAP 601013 Total Copper EPA 6010B Solid OEC, CA-ELAPNELAP 601013 Total Lead EPA 6010E Solid OEC, CA-ELAPNELAP 601013Total Molybdenum EPA 6010E Solid OEC, CA-ELAPNELAP 001013 Total Nickel EPA 6010E Solid OF(-, CA-F.LAP,NF.LAP 601011 Total Selenium EPA 6010E Solid OEC, CA-ELARNELAP 6010B Total Silver EPA 6010E Solid OEC, CA-ELARNELAP 6010B Total Thallium EPA 6010E Solid OEC, CA-ELARNELAP 6010B Total Vanadium EPA 601013 Solid OEC, CA-ELAPNELAP 6010E Total Zinc EPA 601013 Solid OEC. CA-ELARNELAP Volatile Organic Compounds by GUMS 8200B Full List EPA 8260B Solid OF,C, CA-ELARNELAP 8260B Full List EPA 8260B Solid OK, Internal Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Notes and Definitions DefinitionQualifier MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference CCF11 The CCV for this analyte failed high. Results for this analyte may be biased high. CCHI The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. 1SIowS The internal standard associated with this sample fails the method criteria on the lo" side. Results may be biased high. N-02 Analyte concentration below TTLC but above 1 Ox STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805J 925-3376 Page 26 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 27 of 32 a x U 0 Q x a N EH Ln O O Ga 4 O N W � � U N Q,' LO O tT to f C. ri / U7 r1 � z ,~ a 04 � / N to Q A G Q' N O q 44 r-i fYl [x] O O x N I U � Ca C �n h n -ice o U U O N H N S4 +-J F N C ro O A O N Z C C J-> }l 71 ro -ri �4 r-i N i-i C 4--) 04 U —4 •ri a U C ro •rI -rt Ga0FCHU) O 0 0 O 0 0 O 0 0 u-� O 0 0 00 0 0 00 O U- p- o O Ln I la co O lfi ui O O Lo O U� f O Lq l O I IO O (M O M O N O O N O I � 0 0 O to O I_ f- I, fl O O O O O O o O O 4)IF—� O O O O O O O O O O O O O O O w C + y + y + N + N + N + N O O O O O O O O O O O O O O O O 0 0 O a LO It M N 0 O O O O O O N vl e- O W O ti co O Ln V f+7 N E i= Q 0 LL V O LL 2 O C] W Ey c W � I O Q f-+ U x O c3 Gl O rl +� N a) o is I'D U o r.4 N h �:l N ¢a f2a O a) N ri i E Ln o L / r-I ,-I O O W N I x rn a ��� x h U M .. .. .. .. .. .. .. � u +-> a) c (a o �-A-0 a)zw a °4 75 H Z JO-) a) N � N S-i � +-> 04 U r n --1 a) zs U)co (0°O •ri U 1~ N •rl •rl N 1-40FZ,HCO > ry O O O O O O O O O O O O O O 0 O 0 0 0 0 0 0 o O 0 0 0 0 0 0 0 o O 0 0 0 0 0 0 0 0 0 0 0 0 0OLO O�LO M Na0 r nco CO ' M N O 0 v 0 0 M 0 N LO O N O O O O to O O O O O O O O O O 00 O O 00 0 r O O t` 0 tD O O O O LO O O O U) 0 0 CM O Cl) O to N O O N O to 0 0 0 0 0 0 0 0 0 U) Ea x U 0 Q x • a <r FI o O 1-4 X: 4-) C. N / ts' ,H U LO O �3) l0 i O i / ill z e x a / C LO Q M C N O q H Ga / rl ri PO [x] O O x N I U r- La C LID t` co �3 G / C7 0 Lo H NJ N UUO N11-1 N N +) I~ N C ro O A o a)Ez a a JJ u 7 N H Z ro -,A �4 N f4 a 4-) L1a U -1 N b m F co ro -�I ¢. U C ro •� •� Cia O F�4 H CO X 0 0 0 0 -o 0 0 p f � 0 0 0) 1 p �un ro 0 0 00 fo �o 0 n 0 u� 'o 0 LO O ui 0 0 LO 0 Lq v to O r O ri f I O I O M O tq N O IF O cV 0 d p 'o O 0 I- N. n N- I-- i�- 0 0 0 o O O O O O �-t- o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 y c + am + + d (D + a) + m + + o o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 a O M N O O O O O O O O N d y ! a- O 00 I` O N V M O N E ►3 x Q w H � W � I O rG f- 4 C7 x O TS C1 O / -C� r 4-) N N O b" � U o r� � Zs N S~ h � N ¢ 04 O N -0 N 61 S -H / (N Ra'- 0 H in o U) � H Gl O / N N W N I in P �v Ga x hUMr-I / C7 o W p;c -1 (2)i.n U C4 N i H .. .. .. .. .. .. .. N S4 +� N a (0 0 .Q sa-0 N2w P 40-3 � � N H z b -,1 s4 H ri N O" V) m (0 •.-i 04 U (d •ri -.-I C 4 0 ICC ua ro 0 O d N CD 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 a00 r On (0 co LO � to 7 V M M N N to O 0 U 1 LL 0 1 Z TQ i U 9 CC) 0 rn N O X LL E m •� li') N a±L G3 p0 4. maif .0 rn �z U u�� Cd �C� .@ a � c ^ A 9 O +J t h m � N "a a d U E E E0 m u 'o m O h N V rcm= N sPlloS t�1 Penlosl0 J%O.L AjInlsoLoO C C � Me I VMS 80d / iged pj 3 /1111Uello8l g Ui O o 3OZZ9-93OAS a c N W9L08OWQ°J dNl O z y CIO = a n ,o = � y, a epUlnS / eplueAO DApaeaa E F- d iII m d 4 Z vc N y = d N isll Ilod 809Z9 0 z w L _ o U air sielaw ZZ epil a U CO 4 x m _ T J � m m V 1 1 0 G d m m 0 o a N do Or CL E e c Na .5 m m N g 00 00 nil- ❑ r c u � a H E E ❑ ❑; o 131m: �:a °❑r z 0 C m T %may o 0 .�+ o o � C is m m❑ a m G Z W) G Ki Z V N m L x ■ ❑ } i r n cc N _ 0_ u c c o a d E d 3 00 e qe E es m 3 3 a v o m m in CO % in va n 0 p in ❑ ❑ m coCL m rA w a y E ¢aS m, Q Q rr m 9 � •. � ,c c c .r adi E U E E_ � N z 0 H u or H z J a C] w C. N z 76. E z ? G ■ O § 0 i / f mammon 7 7 \� \ 2 ±_± o ) } 2 `) E K cc 0 2 C £ o ® o © _ 0 o. ° ) 7 0 - §) k `a) z z a : - { a a E -0 CD 7 k*t CU) - ` Q e & = » 0 -Fu.9 2 $ a CD o f 2 » R } k ) 2$ f 2 D CD® ^ | a K 3 a 7 / a { { / \)) \ \ r § & J g r 0 § M _ ƒ jƒ = � f � 7 k 2 � a) & k & ! �) S [ © CD 7 k \ $ CCU k k § J § k) \ ƒ \ & 5 @ a & z a c 7 2 0 E ] c}] 2 e o ° o £ 1$LL k*S/ § % E k §® § k= e / 0 E 3 t E 6 0 2\« ®o) LL d ca $ƒ § > CD0 7 7 / 0 2 k 0> - \\ i E )) j J CD \ k s) o) E 0( ^ E J J J w ƒ / t ) § $ f g& f t w o ) c« m m Q § z § G / 0 o$ § Q f ;« � CL ( E S k E 2 S. 9. M � O a L D_ axi a E U d O N O. E m N V 0 M U LL 0 z a C) F co 0 u-;, N LO X L t■- ti /m ■■■■1 LO N V � L o C ■ a'e 0 0 a.at� j= U «i C: m u Hco L7 � in LD Cb x 0 m a e `c Q A '0a 0-. c m c a a u G a J a ro c v E_ E E::ti: m•'�� o' U�rnx sP11oS rJy penlOslO lelol /41MsCLUoO- 000 ZBOB r V"08 s::> �.. 80d r 49ed ,. /41114Et1u01' �..LA. O o OOUB SODAS a � W9609OW09-dHl Z OpIllnS / eplueA:) enl;aeea c� y F- E > Z L > s[ I Ilnd 909ZB Z �_ Q t ❑ 3 slineW - ZZ s1111 ace x m 1 a❑ m Z' CL 0. < to U aE <CEl o F El o V � � ❑ in a a°i N F E E❑ [] Q In H ~ z ..,. Q o x ❑:� Z w O r F � 6 C Ec �a a o❑�� �N Z V O O C 8 'S ❑ } 0 x a a ffi O � d CD 'O w a Qj m a0 8 P.6 E N s .. InL C C d O a O a V L- et m I i ❑❑ L d Q1 Lti CD Z'Lti E N N ql E g C ° c C m 9 E61 a c c c m a U v� U F d E U 3 E J ?p o xwUN-� 6 Z O U U) a U w a m LZ O M U LL O 1 Z a U 9 00 O N rn L" M Li - cc cD Cb m N a FC ^ 9 C (O 11 a a a U U AIL � co E E m o V c E co E c a ,�= o N SPlIOS M PGAJOs1019io1 A41AISOuOD m m m u m io O D D ZSOS / VMS 80d / 194d y n folgellual ul O p DOLES "SODAS m YIS60SOWOO-dHl y 0 z L, � 22 7 CZ5 o d E ,o w aPUInS ! ePlueAO aAltaeaa m f- _ E @ Z y 39I1 I1n3 809Z9 J z N q= L p a +: ' U p SIe3eW " ZZ ORIl W c .c ❑ L � J D U m m m c m p m +"' u 9 > p E1 00 ❑ ❑ O N e U r N m m $L o^ m C) E E❑ ❑.' N f Z.Q �n O U 00 X. ° y � sTi cc d . -0 a� m+ accG am+ r c Z m h x ❑ } p w cc C o c 3 o `O E p m m d ate+ n c a m C a 0 ar K N w C N •Q O ama N40 t 6 G ' lam! 4 m V G a p D cn L ' �� a O L o OO w U y 1 ca D ❑❑ m m m � N m m m N a a, viuOt Q 2 E E iO ;5 ��C Q G d E U E E '�° � l oc x" CL CL V d M t 6i z 0 U Q U w a U) Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2103212 Pacific Petroleum California P. O. Box 2646 Report Date: May 28, 2021 10:05 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 24, 2021 13:05 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: W W., �ou 1,�,�� Shahnaz Parvin, Project Manager sparvin a)oecusa.com California ELAP Certification # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 922-4772 www.oecusa.com FAX: (805) 925-3376 Page I of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom West Center 2103212-01 Solid Solid 05/24/2021 11:20 05/24/2021 13:05 Bottom East Center 2103212-02 Solid Solid 05/24/2021 11:25 05/24/2021 13:05 Bin 20339-A 2103212-03 Solid Solid 05/24/2021 11:30 05/24/2021 13:05 Bin 20339-B 2103212-04 Solid Solid 05/24/2021 11:35 05/24/2021 13:05 Bin 20339-C 2103212-05 Solid Bin 20144-A 2103212-06 Solid Bin 20144-B 2103212-07 Solid Bin 20144-C 2103212-08 Solid Solid 05/24/202111:40 05/24/2021 13:05 Solid 05/24/202111:45 05/24/2021 13:05 Solid 05/24/202111:50 05/24/2021 13:05 Solid 05/24/202111:55 05/24/2021 13:05 Sample Batch Preparation Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List BIE0696 05/25/2021 08:55 STLC !Metals Extraction STLC Metals Extraction Bl E0743 05/261'2021 08:58 TCLP Metals by 1CP 6010B TCLP BIE0794 05/27/2021 10:55 TCLP Metals Extraction TCLP Metals Extraction B I E0744 05/26/2021 09:03 Total Metals by CVAA Mercury Total EPA 7471 A B I E0694 05/25/2021 07:50 Total Metals by ICP 6010B Total B I E0693 05/25/2021 07:26 Volatile Organic Compounds by GC/MS 8260B Full List B1F.0697 05/25/2021 09:00 Volatile Organic TPH by GC/F1D 8015 TPH-Gasoline BIE0737 05/26,12021 06:59 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical t Sample ID : Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.22 0.093 mgtkg 1 B 1 E0694 05/25/21 14:04 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg I B 1 E0693 05/25/21 14:18 EPA 6010B Arsenic 7.0 1.9 Barium 560 0.96 Beryllium ND 0.48 " Cadmium ND 0.24 Chromium 120 0.48 Cobalt 21 0.48 Copper 43 0.96 Lead 7.3 0.48 Nlolvbdenum 0.62 0.48 Nickel 160 0.48 Selenium ND 1.9 Silvcr ND 0.48 Thallium ND 0.96 Vanadium 46 1.9 Zinc 56 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/I, 1 B 1 E0794 05/27/21 19:15 EPA 1311 /EPA 601 OB Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 0.50 mg/kg 1 BIE0737 05/26/21 13:56 EPA 8015M Surrogate: 4-Br0nrofluorohen_ene 101 � (39 - 157) N-02, N-03 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 57 i A Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical.Report Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH DieselW13-C22) 51 10 mgIg 1 BIE0696 05/25/2114:26 EPA8015M TPH Motor Oil (C23-C40) ND 50 11 11 11" 11 Surrogate: o-kiphenrl 90 % (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom West Center Sampled : 05/24/21 11:20 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mg!kg 1000 B I E0697 05/25/21 15:16 EPA 9260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzenc ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chlorocihane ND 1.2 Chlorofonn ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 12-Dibronw-3-chloropropane ND 1.2 1,2-Dibrontoethane (EDB) ND 1.2 " Dibromomethaue ND 1.2 1,2-Dichlorobenzene ND 1.2 " 1,3-Dichlorobenzene ND 1.2 1.4-Dichlorobenzene ND 1.2 Dichlorodifluoromcthane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1.1-Dichloroethene ND 1-2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1.2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1.1-Dichloropropane ND 1.2 " cis- I .3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report i Sample ID: Bottom West Center Sampled: 05/24/21 11:20 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Wexachlorobutadiene ND 1.2 mg!kg 1000 BIE0697 05/25/2115:16 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 " 1,1,1,2-1'etrachloroethane ND 1.2 1.1,2,2-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 " Toluene ND 1.2 1,2,3-Trichlorobenzcnc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 " Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 " 1,2,4-Trimethylbenzene ND 1.2 " 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dihrontglhtoromedmne 101 Y" (74 - 122 ) Surrogate: Toluene-dS 102 % (65 - 128 ) Surrogaty: 4-Bromollaoroheir-ene 97 (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bottom East Center Sampled : 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mg/kg 1 BIE0694 05/25/21 14:06 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg.'kg 1 BIE0693 05/25/21 14:21 EPA 601OB Arsenic 6.6 1.9 Barium 220 0.96 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 120 0.49 Cobalt 19 0.48 Copper 39 0.96 " Lead 8.3 0.48 Molybdenum ND 0.48 Nickel 150 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 51 1.9 " Zinc 62 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/L I B I E0794 05/27/21 19:17 EPA 131 VEPA 601 OB Volatile Organic TPH by GC/FID N-02, N-03 TPI I Gasoline (C5-C 12) 2.2 0.50 mg/kg I BIE0737 05/26/2115:34 EPA8015M D-04 Surrogute: d-Bromofluoroben_ene lld''lo (39- 157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (03-C22) 330 10 TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Terphenld 108 mglkg 1 B1 E0696 05/25/21 14:03 EPA 8015M ( 65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mgtkg 1000 B I E0697 05/25/21 15:43 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromofonn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzene ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 12-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 " 1,2-Dichlorobenzene ND 1.2 13-Dichlorobenzenc ND 1.2 I A-Dichlorobenzenc ND 1.2 DichlorodiFluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 " cis-1,2-Dichloroethane ND 1.2 trans-1,2-Dichloroethane ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropane ND 1.2 cis-13-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbcnzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 57 DIOR Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bottom East Center Sampled: 05/24/21 11:25 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tetrachloroethcne (PCE) ND 1.2 Toluene ND 1.2 1,2.3-Trichlorobenzcnc ND 1.2 1,2.4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (WE) ND 1.2 Triehlorotluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,24-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate. Dibromolluoromethane 10/ 1 Surrogate: Toluene-d8 102 :a Surrogate: 4-Bromolluorohen_ene 96 ,% mglkg 1000 (74-122) ( 65 - 128 ) (75-121) B 1 E(1697 05/25/21 15:43 F.PA 8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mgtkg 1 B 1 E0694 05/25/21 14:08 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1 E0693 05/25/21 14:24 EPA 6010B Arsenic 5.1 2.0 Barium 230 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 Cobalt 21 0.49 Copper 47 0.99 " Lead 11 0.49 Molvbdenum 0.74 0.49 " Nickel 190 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 62 2.0 Zinc 72 2.0 TCLP Metals by ICP Chromium ND 0.050 nig/L I BIE0794 05/27/21 19:20 EPA 13I1/EPA6010B Volatile Organic TPH by GC/FID N-02, N-03 ITH Gasoline (C5-C12) 4.2 0.50 mg/kg I BIE0737 05/26/21 16:26 EPA8015M 1)-04 Surrogate: 4-Bronwfrorohenzene 118 Y" (39 - 157) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportI Analytical t Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by : Clarence Reynolds Lab ID: 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Teiphenyl 350 10 mg/kg 1 BIE0696 05/25/2115:12 EPA8015M 55 50 11 11 11 11° 1/2% (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 12 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B I E0697 05/25'21 16:11 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromcthane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcnc ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibrontoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodiiluoromcthanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 12 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-33T& Page 13 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-A Sampled: 05/24/21 11:30 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 11exachlorobutadiene ND 1.2 mg/kg 1000 BIE0697 05/25/21 10:11 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 " Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1,1.2.2-Tetrachloroethane ND 1.2 Tctrachlorocthcnc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzcnc ND 1.2 12,4-Trichlorobenzene ND 1.2 1.1,1-Trichloroethatie ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (WE) ND 1.2 Trichlorotluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Triniethylbenzene ND 1.2 13.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 Surrogate: Dibromolluorocnethune 102 % ( 74 - 122 ) Surrogate: Toluene-d$ 103 i', (65. 128) " Surrogate: 4-Bron:ulluorohen_ene 97 % (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by : Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mPtkg 1 B 1 E0694 05/25/21 14:10 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mglkg I B I E0693 05/25/21 14:26 EPA 601 OB Arsenic 10 1.9 Barium 290 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 710 0.48 N-02 N-03 Cobalt 47 0.48 Copper 52 0.96 " Lead 13 0.48 Molybdenum 1.2 0.48 Nickel 1900 0.48 " N-02 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 77 1.9 Zinc 83 1.9 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 B I E0794 05/27/21 19:23 EPA 1311 /EPA 6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 0.76 0.50 mg/kg 1 Bl E0737 05/26/21 17:18 EPA 8015M D-04 Surrogate: 4-BrumoJ7noruhencene 101 ?1 (39- 157) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805; 925-3376 Page 15 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPI1 Diesel (C13-C22) III i Motor Oil (C23-C40) Surrogate: o-Tcuphenrl 71 10 mg!kg I Q 1 E0696 05/25/21 13:41 EPA 8015M ND 50 1. 11 11" 1. 106% (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-B Sampled : 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mgtkg 1000 B1 E0697 05/25/21 16:38 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethane ND 1.2 Chlorotbnn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibronioethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 1,4-Dichlorobcnzenc ND 1.2 Dichlorodit7uoromethane ND 1.2 I,1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 I,I-Dichloroethene ND 1-2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1. 1 -Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-0-Dichloropropene ND 1.2 Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples I Sample ID: Bin 20339-B Sampled: 05/24/21 11:35 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 I lexachlorobutadiene ND 1.2 mg/kg 1000 B 1 E0697 05/25/21 16:38 FPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcnc (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichloroben7cnc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluorontethane ND 1.2 " 1,2,3-Trichloropropane ND 1.2 1,14-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibromolluorornethane 100 (74 - 122) Surrogute: Toluenc-d8 101 % ( 65 - 128 ) Surrogate: 4-BruntuJlaurnhcu_ene 97 (75- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 18 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 1.4 0.092 mg/kg 1 B l E0694 05/25/21 14:12 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg l B 1 E0693 05/25/21 14:13 EPA 601 OB Arsenic 6.1 2.0 Barium 220 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 140 0.50 Cobalt 21 0.50 Copper 46 H) Lead 19 0.50 1llolvbdenum 0.57 0.50 " Nickel 180 0.50 Selenium ND 2.0 Silvcr ND 0.50 Thallium ND 1.0 Vanadium 54 2.0 Zinc 87 2.0 TCLP Metals by ICP Chromium Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: 4-B ro m o f U to ro b en z en e ND 0.050 mg/l. 1 BIF0794 05/27/2 1 19:25 EPA 1311 /EPA 601 OB 2.3 0.50 mg/kg 1 Bl E0737 05/26/21 19:53 EPA 8015M 107% (39-157) N-02, N-03 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 57 r A 61RO Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples M Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 390 10 TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Tci-phenpl 105 mg/kg 1 B 1 E0696 05/25/21 14:49 EPA 8015M (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 e Page 20 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.3 mg!kg 1000 B 1 E0697 05/25/21 17:05 EPA 8260B Bromobenzene ND 1.3 Bromochloromethane ND 1.3 Bromodichloromethane ND 1.3 Bratnoform ND 1.3 Bromomethane ND 1.3 n-Butylbenzene ND 1.3 sec-Butylbenzene ND 1.3 tert-Butylbenzene ND 1.3 Carbon tetrachloride ND 1.3 Chlorobcnzcne ND 1.3 Chlorocthanc ND 1.3 Chloroform ND 1.3 Chloromethane ND 1.3 2-Chlorotoluene ND 1.3 4-C'hlorotoluene ND 1.3 Dibromochloromethane ND 1.3 1.2-Dibronto-3-chloropropane ND 1.3 1.2-Dibromoethane (EDB) ND 1.3 Dibromomethane ND 1.3 1,2-Dichlorobenzene ND IS " 1,3-Dichlorobenzene ND 1.3 1,4-Dichlorobenzene ND 1.3 Dichloroditluoromelhane ND 1.3 1,1-Dichloroethane ND 1.3 1,2-Dichloroethane ND 1.3 1, 1 -Dichloroethene ND 1.3 cis-1.2-Dichloroethene ND 1.3 " trans-1,2-Dichloroethene ND 1.3 " 12-Dichloropropane ND 1.3 13-Dichloropropane ND 1.3 2,2-Dichloropropane ND 1.3 1,1-Dichloropropene ND 1.3 cis- I.3-Dichloropropene ND 1.3 trans- l,3-Dichloropropene ND 1.3 Ethylbcnunc ND 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20339-C Sampled: 05/24/21 11:40 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlombutadiene ND 1.3 4-Isopropyl Toluene ND 1.3 Isopropylbenzene ND 1.3 Methylene chloride ND 1.3 Naphthalene ND 1.3 n-Propylbenzene ND 1.3 Styrene ND 1.3 1, 1, 1.2-1'etrachloroethane ND 1.3 1,1,2,2-Tetrachloroethane ND 1.3 Tetrachloroethanc (PCE) ND 1.3 Toluene ND 1.3 1,2,3-Trichlorobenzcne ND 1.3 1,2,4-Trichlorobenzene ND 1.3 1, 1. 1 -Trichloroethane ND 1.3 1,1,2-Trichloroethane ND 1.3 Trichloroethene (WE) ND 1.3 Trichlorofluoromethane ND 1.3 1,2,3-Trichloropropane ND 1.3 1,2,4-Triniethylbenzene ND 1.3 1,3.5-Triniethylbenzene ND 1.3 Vinyl chloride ND 1.3 Xylcncs (total) ND 1.3 Surrogate: Dibromolluoromethanr 102 4;, .Surrogate: Toluene-d8 102 Surrngotc: 4-Bronw/luoroben_ene 98 Y. mg/kg 1000 (74-122) (65-128) ( 7-5- 121 ) BIE0697 05/25/21 17:05 EPA 8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Nlercun 0.23 0.093 mgrkg 1 B 1 E0694 05/25/21 14:14 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I BI E0693 05/25/21 14:37 EPA 60111B Arsenic 4.9 2.0 Barium 230 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 150 0.50 Cobalt 25 0.50 " Copper 49 0.99 Lead 41 0.50 Nlolvbdenum 0.69 0.50 Nickel 190 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 0.99 Vanadium 60 2.0 Zinc 82 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/l. 1 B 1 E0794 05/27/21 19:28 EPA 1311 /EPA 601 OB N-02, N-03 Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12) 1.5 0.50 mg/kg 1 B1 E0737 05/26/21 20:45 EPA 8015M D-04 Surrogute: 4-Bromglluoroben_ene 115 5b (39 - 157 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl1ent.oee.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 57 Oilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPA by GC/FID TPH Diesel (C13-C22) 370 10 'TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Teiphenil 102 0 mg'kg 1 B 1 E0696 05/25/21 14:49 EPA 8015M (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 24 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B I E0697 05/25/21 17:33 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND L2 Bromoform ND 1.2 Brotnomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzcnc ND 1.2 Chlorocthanc ND 1.2 Chlorofor n ND 1.2 Chloromethane ND 12 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1.2-Dibronloethane(EDB) ND 1.2 Dibronunuethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND L2 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis- 1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis- 1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-A Sampled: 05/24/21 11:45 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mgtkg 1000 B I F0697 05/25/21 17:33 EPA 8260B 4-Isopropyl Toluene ND 1.2 lsopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene 2.8 1.2 " n-Propylbenzcnc ND 1.2 " Styrene ND 1.2 1,1,1,2-TetrachlUioetllaIle ND 1.2 1,1,2,2-Tetracliloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2_4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TC'E) ND 1.2 Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropanc ND 1.2 1,2,4-Trimethylbenzene ND 1.2 " 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dihrrnnglluoromethane 99 °s, ( 74 - 122) " Surrogate: Toluene-cI8 102 % (65. 128 ) Surrogate: 4-Bromrl7norohen::ene 96 % ( 75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.19 0.093 mgtkg 1 B I E0694 05/25/21 14:16 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I E0693 05/25/21 14:40 EPA 6010E Arsenic 4.6 2.0 Barium 180 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 150 0.49 Cobalt 19 0.49 Copper 40 0.99 Lead 24 0.49 Molybdenum ND 0.49 Nickel 150 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 50 2.0 Zinc 77 2.0 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BIE0794 05/27/2119:30 EPA 1311/EPA601i1B Volatile Organic TPH by GC/FID N-02, N-03 TPH Gasoline (C5-('12) 2.2 0.50 mg/kg 1 BIE0737 05/26/21 21:36 EPA 8015M D-04 Surrogate: 4-Bromo/hrorobenzene I0IR `% (39 - 1 7 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical t Sample ID : Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 320 9.9 TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Teiphemd 95 `%) mglkg I B I E0696 05/25/21 15:12 EPA 8015M ( 65 - 136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 28 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg!kg 1000 B I E0697 05/25/21 18:00 EPA 8200B Bromobenzene ND 1.2 Broniochloromethane ND 1.2 Bromodichloromethane ND 1.2 Broniolorm ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1,2 sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibrouro-3-chloropropane ND 1.2 1,2-Dibronioethane (EDB) ND 1.2 Dibromoniethane ND 1.2 1.2-Dichlorobenzene ND 1.2 13-Dichlorobcnzcnc ND 1.2 1,4-Dichlorobcnzcnc ND 1.2 Dichlorodilhioromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 " 1,2-Diehloropropane ND 1.2 L3-Diehloropropane ND 1.2 2.2-Diehloropropane ND 1.2 I.l-Dichloropropene ND L2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-B Sampled: 05/24/21 11:50 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachi orobutadiene ND 1.2 mg/kg 1000 B1 F0697 05/25/21 18:00 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene 2.3 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 Tetrachloroethene (PCE) ND 1.2 Toluene ND 1.2 1,23-Trichlorobenzene ND 1.2 1,24-Trichlorobenzene ND 1.2 " 1,1.l-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 1,2,3-Trichloropropanc ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dibromo/luorome thane 100 % ( 74 - 12 2) " Surrogate: 7oluene-d8 102 ;'o (' 65 - 128 ) Surrogate: d-Bromq/lnavben_eue 98 %, (75- 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 n___ 2n _rcv Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mg1kg 1 B 1 E.0694 05/25/21 14:18 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I E0693 0.5/25/21 14:42 EPA 601 OB Arsenic 5.0 2.0 Barium 140 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 160 0.49 Cobalt 23 0.49 Copper 45 0.98 Lead 14 0.49 Molybdenum ND 0.49 Nickel 190 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 50 2.0 Zinc 71 10 TCLP Metals by ICP Chromium ND 0.050 mg/L I BIE0794 05/27/2119:40 EPA 1311 /EPA 601013 Volatile Organic TPH by GC/FID N-02, N-03 TPH Gasoline(('S-('12) 2.1 0.49 mg/kg 1 BIE0737 05/26/2122:28 EPA 8015M D-04 Surrogate:4-Bromoflaoroben_c1le 119ib (39-157) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 57 WAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ReportAnalytical Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID: 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 560 10 TPH Motor Oil (C23-C40) ND 50 Surrogate: o-Teiphem,l 120 "Y,, mg!kg 1 B 1 E0696 05/25/21 14:26 EPA 8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report for Samples Sample ID : Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mgtkg 1000 B 1 E0697 05/25/21 18:28 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromofortn ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbeuzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethanc ND 1.2 Chlorofonn ND 1.2 Chloroniethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 12-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (ED13) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Diehlorobcnzene ND 1.2 1,4-Diehlorobcnzcnc ND 1.2 Dichloroditluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1.2-Dichloroethane ND 1.2 ],I-Dichloroethene ND 1.2 cis- I .2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND L2 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 1.1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 " Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Analytical Report foi- Samples Sample ID: Bin 20144-C Sampled: 05/24/21 11:55 Matrix: Solid Sampled by: Clarence Reynolds Lab ID : 2103212-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg'kg 1000 B I E0697 05/25/21 18:28 EPA 8200B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-1'etracliloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tetrachlorocthenc WE) ND 1.2 Tolucnc ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,2.4-Trimethylbenzene ND 1.2 1,3,5-Trimethylbenzene NJ) 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 " Surrogate: Dihrouwlluoromethame 99 %> ( 74 - 122) " Surrogate: Toluene-dS 101 % (65 - 12S) " Surrogate: 4-Bronui/luorobenzeue 96 % ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0694 - EPA 7471A Preparation: EPA 7471A Prep 05/25/21 07:50 Blank (BlE0694-BLK1) Analyzed: 05/25/21 13:31 Mercury ND 0.10 tngrkg LCS (BlE0694-BSI) Analyzed: 05/25/21 13:27 Mercury 0.840 0.10 mg/kg 0.833 101 85-115 LCS Dup (B1E0694-BSD1) Analyzed: 05/25/21 13:29 Mercury 0.849 0.10 mglkg 0.833 102 85-115 1 20 Duplicate (B1E0694-DUP1) Source: 2103193-05 Analyzed: 05/25/21 13:47 Mercury 0.216 0.18 ing/kg 1.87 159 20 QR-04 Matrix Spike (B1E0694-MSI) Source: 2103193-05 Analyzed: 05/25/21 13:51 Mercury 1.04 0.093 mg/kg 0.776 1.87 NR 75-125 Q11-07 Matrix Spike Dup (BlE0694-MSD1) Source: 2103193-05 Analyzed: 05/25/21 13:53 Mercury 1.68 0.090 mg/kg 0.751 1.87 NR 75-125 47 20 QNI-07. QR-04 Post Spike (BlE0694-PS1) Source: 2103193-02 Analyzed: 05/25/21 15:19 Mercury 5.28 ug/I. 5.00 0.114 103 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 35 of57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by 1CP - Quality Contl•ol I Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Blank (BlE0693-BLK1) Analyzed: 05/25/21 14:02 Antimony ND 2.5 mg�kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1.0 Lead ND 0.50 Molybdenum ND 0.50 Nickel ND 0.50 Selenium ND 2.0 " Silver ND 0.50 Thallium ND I O Vanadium ND 2.0 " Zinc ND 2.0 LCS (BlE0693-BSI) Analyzed: 05/25/21 14:45 Antimony 99.7 2.5 mgIg 100 100 80-120 Arsenic 99.6 2.0 100 100 80-120 Barium 102 LO 100 102 80-120 Beryllium 98.2 0.50 100 98 80-120 Cadmium 100 0.25 100 100 80-120 Chromium 99.5 0.50 100 100 80-120 Cobalt 101 0.50 100 101 80-120 Copper 101 1.0 100 101 80-120 Lead 102 0.50 100 102 80-120 Molybdenum 97.8 0.50 100 98 80-120 Nickel 101 0.50 100 101 80-120 Selenium 99A 2.0 100 99 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 H) 100 102 80-120 Vanadium 97.6 2.0 100 98 80-120 Zinc 100 2.0 100 100 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 ControlTotal Metals by 1CP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 LCS Dup (B1E0693-BSD1) Analyzed: 05/25/21 14:47 Antimony 100 2.5 mg/kg 100 100 80-120 0.5 20 Arsenic 99.7 2.0 100 100 80-120 0.1 20 Barium 101 1.0 100 101 80-120 0.05 20 Beryllium 98.5 0.50 100 98 80-120 0.3 20 Cadmium 100 0.25 100 100 80-120 0.2 20 Chromium 99.4 0.50 100 99 80-120 0.2 20 Cobalt 101 0.50 100 101 80-120 0.05 20 Copper 100 1.0 100 100 80-120 0.2 20 Lead 102 0.50 100 102 80-120 0.1 20 Molybdenum 98.4 0.50 100 98 80-120 0.6 20 Nickel 102 0.50 100 102 80-120 0.1 20 Selenium 100 2.0 100 100 80-120 1 20 Silver 4.96 0.50 5.00 99 80-120 0 20 Thallium 102 1.0 100 102 80-120 0.4 20 Vanadium 97.0 2.0 100 97 80-120 0.7 20 Zinc 100 2.0 100 100 80-120 0.2 20 Duplicate (BlE0693-DUPI) Source: 2103212-05 Analyzed: 05/25/21 14:15 Antimony ND 2.4 mg/kg ND 20 Arsenic 5.18 1.9 6.10 16 20 Barium 205 0.97 218 6 20 Beryllium 0.409 0.49 0.435 6 20 Cadmium ND 0.24 ND 20 Chromium 154 0.49 144 7 20 Cobalt 22.3 0.49 20.9 6 20 Copper 48.8 0.97 46.3 5 20 Lead 17.9 0.49 19.3 8 20 Molybdenum 0.510 0.49 0.574 12 20 Nickel 196 0.49 179 9 20 Selenium ND 1.9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 52.3 1.9 54.0 3 20 Zinc 69.6 1.9 87.4 23 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 57 CAOilfield Environmental & Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by Control Analyte Result RL Units Spike Source %REC °/oREC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Matrix Spike (B1E0693-MS1) Source: 2103212-05 Analyzed: 05/25/21 13:50 Antimony 13.1 2.4 mg/kg 97.9 ND 13 10-116 Arsenic 101 2.0 97.9 6.10 96 77-121 Barium 226 0.98 97.9 218 8 30-169 QM-07 Beryllium 95.2 0.49 97.9 0.435 97 86-I11 Cadmium 90.0 024 97.9 ND 92 81-112 Chrontiutn 218 0.49 97.9 144 76 75-129 Cobalt 109 0.49 97.9 20.9 90 71-121 Copper 146 0.99 97.9 46.3 102 68-135 Lead 107 0.49 97.9 19.3 90 72-121 Molybdenum 35.0 0.49 97.9 0.574 35 70-112 QIN1-07 Nickel 230 0.49 97.9 179 52 73-121 QD14)7 Selenium 85.9 2.0 97.9 ND 88 76-116 Silver 4.79 0.49 4.90 ND 98 54-132 Thallium 85.9 0.98 97.9 ND 88 64-120 Vanadium 138 2.0 97.9 54.0 86 78-124 Zinc 162 2.0 97.9 87.4 77 50-143 Matrix Spike Dup (B1E0693-MSD1) Source: 2103212-05 Analyzed: 05/25/21 13:52 Antimony 9.34 2.4 tng%kg 95.8 ND 10 10-116 33 20 QR-02 Arsenic 96.6 1.9 95.8 6.10 95 77-121 4 20 Barium 295 0.96 95.8 218 80 30-169 26 20 QR-02 Beryllium 91.2 0.48 95.8 0.435 95 86-I11 4 20 Cadmium 85.1 0.24 95.8 ND 89 81-112 6 20 Chromium 271 0.48 95.8 144 133 75-129 22 20 QD1-07, QR-04 Cobalt 113 0.48 95.8 20.9 96 71-121 3 20 Copper 140 0.96 95.8 46.3 97 68-135 4 20 I -cad 104 0.48 95.8 19.3 88 72-121 3 20 Molybdenum 32.4 0.48 95.8 0.574 33 70-112 8 20 QNI-07 Nickel 319 0.48 95.8 179 146 73-121 32 20 QM-07, QR-04 Selenium 79.5 1.9 95.8 ND 83 76-116 8 20 Silver 4.59 0.48 4.79 ND 96 54-132 4 20 Thallium 79.5 0.96 95.9 ND 83 64-120 8 20 Vanadium 147 1.9 95.8 54.0 97 78-124 6 20 Zinc 158 1.9 95.8 87.4 74 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Post Spike (B1E0693-PS1) Source: 2103212-05 Analyzed: 05/25/21 14:08 Antimony 1.99 mg/L 2.00 0.00347 99 75-125 Arsenic 2.07 2.00 0.121 98 75-125 Barium 6.39 2.00 4.34 103 75-125 Beryllium 1.96 2.00 0.00863 98 75-125 Cadmium 1.83 2.00 -0.0417 91 75-125 Chromium 4.75 2.00 2.85 95 75-125 Cobalt 2.27 2.00 0.414 93 75-125 Copper 2.88 2.00 0.919 98 75-125 Lead 2.24 2.00 0.384 93 75-125 Molybdenum 1.97 2.00 0.0114 98 75-125 Nickel 5.42 2.00 3.56 93 75-125 Selenium 1.80 2.00 -0.120 90 75-125 Silver 0.0954 0.100 -0.00119 95 75-125 Thallium 1.78 2.00 -0.0164 89 75-125 Vanadium 3.01 2.00 1.07 97 75-125 Zinc 3.61 2.00 1.74 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cI!ent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 39 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 i Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0794 -EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 05/27/21 10:55 Blank (BlE0794-BLKI) Analyzed: 05/27/21 18:35 Chromium ND 0.050 mg/L LCS (BlE0794-BS1) Analyzed: 05/27/21 18:20 Chromium 10.0 0.050 mg/L 10.0 LCS Dup (BlE0794-BSDI) Analyzed: 05/27/21 18:22 Chromium 9.84 0.050 mg/L 10.0 Duplicate (B1E0794-DUPl) Source: 2102854-01 Analyzed: 05/27/21 18:52 Chromium ND 0.050 mg/L Leach Fluid Blank (BlE0794-LBKI) Analyzed: 05/27/21 18:37 Chromium ND 0.050 mg/L Leach Fluid Blank (BlE0794-LBK2) Analyzed: 05/27/21 18:40 Chromium ND 0.050 mg/L Leach Fluid Blank (BlE0794-LBK3) Analyzed: 05/27/21 18:42 Chromium ND 0.050 mg/L Matrix Spike (BlE0794-MS1) Source: 2102854-01 Analyzed: 05/27/21 18:25 Chromium 10.2 0.050 mg/L 10.0 Matrix Spike Dup (B1E0794-MSD1) Source: 2102854-01 Analyzed: 05/27/21 18:45 Chromium 10.2 0.050 mg/l. 10.0 100 80-120 98 80-120 2 20 ND 20 ND 102 82-119 ND 102 82-119 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 ^- 1. _ram., Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0737 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/26/21 06:59 Blank (Bl E0737-BLKl) Analyzed: 05/26/21 10:49 TPII Gasoline (('5-C12) ND 0.50 mg/kg Surogate:4-Broma/luorobenccne 11.12E " 0.125 102 39-157 LCS (BlE0737-BS1) Analyzed: 05/26/21 09:57 TPII Gasoline (CS-('12) 1.08 0.50 mg/kg 0.994 108 68-139 Surrogate:4-Bromofluorohen_ene 0.146 " 0.124 117 39-157 LCS Dup (BlE0737-BSDI) Analyzed: 05/26/21 10:23 TPH Gasoline (C5-C12) 1.20 0.50 mg/kg 0.998 120 68-139 11 20 .Surrogate:4-Bromo/luorohenzene 0.154 0.125 123 39-1.57 Duplicate (BlE0737-DUPI) Source: 2103210-01RE1 Analyzed: 05/26/21 13:04 TPH Gasoline (C5-C12) ND 0.49 mg/kg ND 20 Surrogate:4-Bromgfhu>rohenzene 0.120 " 0.122 99 39-157 Matrix Spike (B1E0737-MS1) Source: 2103210-01RE1 Analyzed: 05/26/21 23:45 TPH Gasoline (('5-('12) 0.868 0.48 mg'kg 0.967 ND 90 10-171 Surrogate:4-Bromolluoroben:enc. 0.142 " 0.121 117 39-157 Matrix Spike Dup (B1E0737-MSDl) Source: 2103210-01RE1 Analyzed: 05/27/21 00:11 TPII Gasoline (('5-C12) 0.911 0.50 mg/kg 0.998 ND 91 10-171 5 20 Surrogate: 4-Brontof uorohenzene 0.149 " 0.125 119 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 I)--- i/ t -f s7 rA &WIA rpw M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Semi-Volatile1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0696 - EPA 8015M Preparation: EPA 3550C 05/25/21 08:55 Blank (BlE0696-BLK1) Analyzed: 05/25/21 13:41 TPH Dicscl (('13-C22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 " Surrogate: o-Teiphen.0 43.3 " 50.0 87 65-136 LCS (BlE0696-BS1) Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22) 512 10 mg/kg 499 103 72-115 TP11 Motor Oil (('23-C40) 473 50 499 95 74-126 Surrogate. o-Teipl(wyl 49.9 49.9 101) 65-136 LCS Dup (BlE0696-BSD1) Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22) 487 10 mg/kg 500 97 72-115 5 20 TPH Motor Oil (C23-C'40) 459 50 500 92 74-126 3 20 Surrogate: o-Teiphcind 48.7 50.0 97 65-136 Duplicate (BlE0696-DUPl) Source: 2103212-01 Analyzed: 05/25/21 14:03 TPH Diesel (Cl 3-C22) 35.5 9.9 mg/kg 50.9 36 20 QR-06 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Teiphegrl 42.6 49.7 86 65-136 Matrix Spike (B1E0696-MS1) Source: 2103212-01 Analyzed: 05/25/21 12:55 TPH Diesel (('13-C22) 500 10 mg/kg 498 50.9 90 46-147 TPH Motor Oil (('23-C40) 432 50 498 ND 87 35-171 Surrogate: o-TeiphenYl 44.5 49.8 89 6.5-136 Matrix Spike Dup (B1E0696-MSDl) Source: 2103212-01 Analyzed: 05/25/21 13:18 TPH Diesel (('13-C22) 497 9.9 mg'kg 497 50.9 90 46-147 0.6 20 TPH Motor oil (('23-('40) 432 50 497 ND 87 35-171 0.2 20 Surrogate: o-Teiphenvl 44.3 49.7 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 42 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1) Analyzed: 05/25/21 13:26 Benzene ND 0.25 mgAg Bromobenzene ND 0.25 " Bromochloromcthanc ND 0.25 Bromodichloromethane ND 0.25 Bromofbnn ND 0.25 Bromomethane NI) 0.25 n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 tert-Butyl benzene ND 0.25 Carbon tetrachloride ND 0-25 Chlorobenzene ND 0.25 " Chloroethane ND 0.25 " Chloroform ND 0.25 " Chloromethane ND 0.25 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene NI) 0.25 " Dibromochloromethane ND 0.25 " 1,2-1)ibromo-3-chloropropane ND 0.25 1,2-Dibromoethane (EDB) ND 0.25 Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0,25 1,3-Dichlorobenzene ND 0.25 " IA-Dichlorobenzene ND 0.25 " Dichloroditluoronethanc ND 0.25 " I,1-Dichloroethane ND 0.25 1,2-Dichlorocthanc ND 0.25 " 1,1-Dichloroethene ND 0.25 " cis-1 2-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 1,2-Dichloropropane ND 0.25 " 1,3-Dicliloropropane ND 0.25 2,2-Dicliloropropane ND 0.25 " l,l-Dichloropropenc ND 0.25 cis- 1.3-Dichlompropene ND 0.25 " trans-1,3-Dichloropropenc ND 0.25 " Ethvlbenzene ND 0.25 " Ilexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 Methylene chloride ND 0,25 Naphthalene ND 0.25 n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Kim-' Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA,93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by GC/n1S - Quality Control IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLKI) Analyzed: 05/25/21 13:26 Styrene ND 0.25 mg/kg 1, 1, 1 .2-Tetrachloroethane ND 0.25 " I.1,2.2-Tetrachloroethane ND 0.25 Tetrachloroethane (PCE) ND 0.25 " Toluene ND 0.25 " 1,2.3-Trichlorobenzene ND 0.25 1,2A-Trichlorobenzene ND 0.25 " 1, 1, 1 -Trichloroethane ND 0.25 1,1.2-Trichloroethane ND 0.25 " Trichlomethene (TCE) ND 0.25 " Trichlorotluoromethane ND 0.25 1,2,3-Trichloropropane ND 0.25 1,2.4-Trinrethylbenzene ND 0.25 1.3.5-Trimethylben7ene ND 0.25 Vinyl chloride ND 0.25 Xylenes (total) ND 0.25 Surrogate: Dibrornolluoromc•thmic, 0.0496 0.0500 99 74-122 Surrogate: Toluene-d8 0.0507 0.0500 101 65-128 Surogale:4-Bromolluorahenrene 0.0482 0.0500 96 75-121 LCS (B1E0697-BSI) Analyzed: 05/25/21 11:37 Benzene 1.80 0.25 mg/kg 1.98 91 70-131 Bromobenzene 2.09 0.25 1.99 105 74-130 Bromochloromcthane 1.77 0.25 1.98 89 64-133 Bromodichloromethane 2.12 0.25 1.99 107 69-137 Bromotixm 2.09 0.25 1.98 105 55-132 Bromoniethane 1.51 0.25 1.98 76 10-142 n-Butylbenzene 2.47 0.25 1.98 125 64-156 sec-Butylbenzene 2.46 0-25 1.99 124 75-155 tert-Butylbenzene 2.34 0.25 1.98 118 74-144 Carbon tetrachloride 1.70 0.25 1.98 86 67-135 Chlombenzene 2.08 0.25 1.98 105 73-134 Chloroethane 1.65 0.25 1.98 83 10-167 Chloroform 2.01 0.25 1.98 WI 69-124 C'hloromethane 2.46 0.25 1.98 124 34-136 2-Chlorotoluene 2.16 0.25 1,98 109 75-135 4-Chlorotoluene 2.30 0.25 1.98 116 70-138 Dibromochloromethane 2.01 0.25 1.98 102 67-135 1.2-Dibromo-3-chloropropanc 2.45 0.25 1.98 124 41-149 1,2-Dibromoethane (EDB) 1.98 0.25 1.98 100 68-131 Dibromomcthanc 1.92 0.25 1.98 97 61-140 1,2-Diclilorobenzene 2.20 0.25 1.98 111 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 44 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds by GUMS - Quality Control l nalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS (B1E0697-BSI) Analyzed: 05/25/21 11:37 1,3-Dichlorobenzene 2.30 0.25 mgtkg 1.98 116 76-138 14-Dichlorobenzene 2.23 0.25 1.98 112 72-132 Dichloroditluorontethanc 1.51 0.25 1.98 76 10-155 1, 1 -Dichloroethane 1.90 0.25 1.98 96 63-139 1,2-Dichloroethane 2.04 0.25 1.98 103 64-126 I,I-Dichloroethene 1.79 0.25 1.98 90 52-167 cis-1 2-Dichloroethene 1.84 0.25 1.98 93 70-135 trans-1,2-Dichloroethene 1.69 0.25 1.98 85 67-147 1,2-Dieliloropropaue 3.19 0.25 1.98 161 68-131 1,3-Dichloropropane 1.91 0.25 1.99 96 64-128 2.2-Dichloropropane 2.11 0.25 1.98 107 63-154 I,1-Dichloropropene 1.82 0.25 1.98 92 68-139 cis-1,3-Dichloropropene 2.08 0.25 1.98 105 72-134 trans-1,3-Dichloropropene 2.10 0.25 1.98 109 69-132 Ethylbenzene 1.92 0.25 1.98 97 68-136 1lexachlorobutadiene 2.24 0.25 1.98 113 72-198 4-Isopropyl Toluene 2.40 0.25 1.98 121 74-150 lsopropylbenzene 2.21 0.25 1.99 112 71-149 Methylene chloride 1.81 0.25 1.98 91 51-127 Naphthalene 2.29 0.25 1.98 116 57-158 n-Propylbenzene 2.29 0.25 1.98 116 70-143 Styrene 2.47 0.25 1.98 124 68-138 1,1,1,2-Tetrachloroethane 2.10 0.25 1.98 106 76-130 1,1,2,2=retrachloroethane 2.18 0.25 1.98 110 60-136 Tetrachloroelhene(PCE) 1.79 0.25 1,99 91 73-138 Toluene 1.99 0.25 1.98 101 72-128 1,2,3-Trichlorobenzene 2.47 0.25 1.98 125 61-166 L2,4-Trichlorobenzene 2.43 0-25 1.98 123 71-158 1, 1, 1 -Trichloroethane 1.92 0.25 1.98 97 71-135 1,1,2-Trichloroethane 2.23 0.2.5 1.98 113 64-132 Trichloroethane (TCE) 1.87 0.25 1.98 94 74-139 Trichlorofluoromethane 2.69 0.25 1.98 136 30-156 1,2,3-Trichloropropane 2.05 0.25 1.98 104 67-123 1,24-Trimethylbenzene 2.31 0.25 1.98 117 68-134 1,3.5-Trimethylbenzene 2.27 0.25 1.99 114 71-140 Vinyl chloride 2.14 0.25 1.98 108 43-144 Xylenes(total) 6.81 0.25 5.94 115 69-138 Surrogate: Dihromolhioromcthauc 11.0512 0.0495 103 74-122 Surrogate:7bluene-d8 0.0516 0.0495 104 65-128 Surrogate:4-Bromolluorohen_ene 0.0467 0.0495 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. QnB-08 California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 45 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 IVolatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSDI) Analyzed: 05/25/21 12:04 Benzene 1.74 0.25 mg/kg 1.99 87 70-131 3 20 Bromobenzene 2.08 0.25 1.99 104 74-130 0.4 20 Bromochloromethanc 1.69 0.25 1.99 85 64-133 5 20 Bromodichloromethane 2.14 0.25 1.99 107 69-137 0.8 20 Bromofonn 2.06 0.25 1,99 103 55-132 1 20 Bromomethane 1.50 0.25 1.99 75 10-142 1 20 u-Butylbenzene 2.33 0.25 1.99 117 64-156 6 20 sec-Butylbenzene 2.25 0.25 1.99 113 75-155 9 20 tert-Butylbenzene 2.17 0.25 1.99 109 74-144 8 20 Carbon tetrachloride 1.60 0.25 1.99 80 67-135 6 20 Chlorobenzene 2.07 0.25 1.99 104 73-134 0.3 20 Chloroethane 1.70 0.25 1.99 85 10-167 3 20 Chloroform 1.93 0.25 1.99 97 69-124 4 20 Chloromethane 2.10 0.25 1.99 108 34-136 13 20 2-Chlorotoluene 2.05 0.25 1.99 103 75-135 5 20 4-Chlorotoluene 2.15 0.25 1.99 108 70-138 7 20 Dibronwchloromethane 2.11 0.25 1.99 106 67-135 5 20 1,2-Dibromo-3-chloropropane 2.68 0.25 1.99 135 41-149 9 20 1,2-Dibromocthane (EDB) 2.01 0.25 1.99 101 68-131 1 20 Dibromomethanc 1.92 0.25 1.99 96 61-140 0.08 20 1,2-Dichlorobenzene 2.20 0.25 1.99 110 76-136 0.4 20 1.3-Dichlorobenzene 2.15 0.25 1.99 108 76-138 7 20 1,4-Diclilorobenzene 2.13 0.25 1.99 107 72-132 5 20 Dichlorodifluoroiucthane 1.50 0.25 1.99 75 10-155 0.5 20 1, 1 -Dichloroethane 1.83 0.25 1.99 92 63-139 4 20 1,2-Dichlorocthanc 2.01 0.25 1.99 101 64-126 2 20 1, 1 -Dichloroethene 1.73 0.25 1.99 87 52-167 4 20 cis-1.2-Dichloroethene 1.71 0.25 1.99 86 70-135 8 20 trans- l,2-Dichloroethene 1.64 0.25 1.99 82 67-147 3 20 1,2-Dichloropropane 1.94 0.25 1.99 97 68-131 49 20 1,3-Dichloropropane 2.05 0.25 1.99 103 64-128 7 20 2,2-Dichloropropane 2.00 0.25 1.99 100 63-154 5 20 1,1-Dichloropropene 1.75 0.25 1.99 88 68-138 4 20 cis-1.3-Dichloropropene 1.98 0.25 1.99 100 72-134 5 20 trans-1,3-Dichloropropene 2.25 0.25 1.99 113 69-132 4 20 Ethylbenzene 2.05 0.25 1.99 103 68-136 7 20 HexachIorobutadiene 2.12 0.25 1.99 107 72-198 5 20 4-Isopropyl Toluene 2.23 0.25 1.99 112 74-150 7 20 lsopropylbenzene 2.24 0.25 1.99 112 71-149 1 20 Methylene chloride 1.79 0.25 1.99 90 51-127 1 20 Naphthalene 2.10 0.25 1.99 106 57-158 8 20 n-Propylbenzene 2.12 0.25 1.99 106 70-143 8 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSDI) Analyzed: 05/25/21 12:04 Styrene 2.23 0.25 mg/kg 1.99 112 68-138 10 20 1, 1, 1,2-Tetrachloroethane 2.18 0.25 1.99 109 76-130 3 20 1,12.2-Tetrachloroethanc 2.11 0.25 1.99 106 60-136 3 20 Tetrachloroethene(PCE) 1.81 0.25 1.99 91 73-138 0.8 20 Toluene 1.83 0.25 1.99 92 72-128 9 20 1,2,3-Trichlorobenzene 2.32 0.25 1.99 116 61-166 6 20 1,2,4-1'richlorobenzene 2.35 0.25 1.99 118 71-158 3 20 1, 1, 1 -Trichloroethane 1.86 0.25 1.99 93 71-135 3 20 1,12-Trichloroethane 2.18 0.25 1.99 109 64-132 2 20 Trichloroethene (TCE) 1.82 0.25 1.99 91 74-139 3 20 Trichlorofluoromethane 2.59 0.25 1.99 130 30-156 4 20 1,2,3-Trichloropropane 1.96 0.25 1.99 98 67-123 5 20 1.2.4-Trimethylbenzene 2.16 0.25 1.99 108 68-134 7 20 1,3,5-Trimethylbenzene 2.13 0.25 1.99 107 71-140 6 20 Vinyl chloride 2.12 0.25 1.99 107 43-144 0.6 20 Xylenes(total) 6.17 0.25 5.98 103 69-138 10 20 Surrogate: Dibroinolluoromethane 0.0512 0.0498 103 74-122 Surrogate. Toluene-d8 0.0510 I1.0498 102 65-128 Surrogate: 4-Bromq luorohenzene 0.0499 0.0498 100 75-121 Duplicate (B1E0697-DUPI) Source: 2103210-01 Analyzed: 05/25/21 14:48 Benzene ND 1.2 mgtkg ND 20 Bromobenzene ND 1.2 ND 20 Bromochloromcthane ND 1.2 ND 20 Broniodichloromethane ND 1.2 ND 20 Bromoform ND 1.2 ND 20 Bromomethane ND 1.2 ND 20 n-Butylbenzene ND 12 ND 20 sec-Butylbenzene ND 1.2 ND 20 tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzene ND 1.2 ND 20 Chloroethane ND 1.2 ND 20 Chloroform ND L2 ND 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 4-Chlorotoluene ND 1.2 ND 20 Dibromochloromethanc ND 1.2 ND 20 I2-Dibromo-3-chloropropanc ND 1.2 ND 20 1,2-Dibromoethane (EDB) ND 1.2 ND 20 Dibromomethanc ND 1.2 ND 20 1,2-Dichlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 47 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilet ptControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Duplicate (B1E0697-DUPl) Source: 2103210-01 Analyzed: 05/25/21 14:48 1,3-Dichlorobenzene ND 1.2 mg/kg NI) 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichlorodifluoromcthanc ND 1.2 ND 20 1,1-Dichloroethane ND 1.2 ND 20 1,2-Dichloroethane ND 1.2 " ND 20 1,1-Dichloroethene ND 1.2 ND 20 cis-1,2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropaue ND 1.2 ND 20 1,3-Dichloropropaue ND 1.2 ND 20 2.2-Dichloropropaue ND 1.2 ND 20 1,1-Dichloropropene ND 1.2 ND 20 cis- 1,3 -Dichloropropene ND 1.2 ND 20 trans-1,3-Dichloropropene NI) 1.2 NI) 20 Ethylbenzene ND 1.2 ND 20 1lexachlorobutadiene ND 1.2 " ND 20 4-Isopropyl Toluene ND 1.2 NI) 20 Isopropylbenzene ND 1.2 ND 20 methylene chloride ND 1.2 NI) 20 Naphthalene NI) 1.2 ND 20 n-Propylbenzene ND 1.2 NI) 20 Styrene ND 1.2 NI) 20 1,1,12-Tetrachloroethane ND 1.2 NI) 20 1,1,2,2-Tetrachlorocthanc ND 1.2 ND 20 Tetrachloroethene WC'E) ND 1.2 ND 20 Toluene ND 1.2 ND 20 1,2,3-Trichlorobenzene ND 1.2 ND 20 1,24-Trichlorobenzene ND 1.2 NI) 20 1,1,1-Trichloroethane NI) 1.2 ND 20 1,12-Trichloroethane ND 1.2 ND 20 Trichloroethene (WE) ND 1.2 ND 20 Trichlorofluoromethane NL) 1.2 ND 20 1,2,3-Trichloropropane ND 1.2 ND 20 1,24-Trimethylbenzene NI) 1.2 ND 20 1,3.5-Trimethylbenzeue NI) 1.2 ND 20 Vinyl chloride NI) 1.2 ND 20 Xylenes (total) ND 1.2 NI) 20 Surrogate. Uihronwlhtoromcthatt(• 0.0503 0.0494 102 74-122 Surrogate:7ohiene-d8 0.0514 0.0494 104 65-128 Surrogate: 4-Bromollaorohenzuat, 0.0478 0.0494 97 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805% 925-3376 Page 48 of 57 I(. �9 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilepo Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1) Source: 2103212-01 Analyzed: 05/25/21 19:22 Benzene 9.97 1.2 mg/kg 9.94 ND 90 37-145 Bromobenzene 11.0 1.2 9.94 ND 111 29-147 Bromochloromethane 9.22 1.2 9.94 ND 93 40-145 Bromodichloromethane 10.9 1.2 9,94 ND 110 39-153 Bromoform 10.7 12 9.94 ND 108 32-143 Bromomethane 10.3 1.2 9.94 ND 104 10-141 u-Butylbenzene 11.6 12 9.94 ND 117 10-162 sec-Butylbenzene 12.2 1.2 9.94 ND 123 14-168 tert-Butylbenzene 11.8 1.2 9.94 ND 119 21-159 Carbon tetrachloride 8.48 1.2 9.94 ND 85 28-148 Chlorobenzene 10.9 1.2 9.94 ND 110 32-148 Chloroethane 12.6 1.2 9.94 ND 127 11-106 Chloroform 9.94 1.2 9.94 ND 100 40-139 Chloromethane 10.4 1.2 9.94 ND 105 18-135 2-Chlorotoluene 10.8 1.2 9.94 ND 108 25-151 4-Chlorotoluene 11.3 1.2 9.94 ND 114 22-150 Dibromochloromethane 10.2 1.2 9.94 ND 103 40-147 1,2-Dibromo-3-chloropropane 12.4 1.2 9.94 ND 125 25-158 1,2-Dibromoethane (EDB) 10.1 1.2 9.94 ND 102 38-147 Dibromomctbanc 9,74 1.2 9.94 ND 98 39-150 1,2-Dichlorobenzene 11.4 1.2 9.94 ND 115 24-154 1,3-Dichlorobenzene 11.3 1.2 9.94 ND 114 21-153 1,4-Dichlorobenzene 10.9 1.2 9.94 ND 110 21-146 Dichlorodifluoromcthanc 6.32 1.2 9.94 ND 64 10-149 1, 1 -Dichloroethane 9.32 1.2 9.94 ND 94 34-151 1,2-Dichloroethane 9.93 1.2 9.94 ND 100 40-137 1, 1 -Dichloroethene 7.41 1.2 9.94 ND 74 21-172 cis-1,2-Dichloroethene 8.87 1.2 9.94 ND 89 38-147 trans-1,2-Dichloroethene 8.06 1.2 9.94 ND 81 30-160 12-Dichloropropane 10.0 1.2 9.94 ND 101 39-146 1,3-Dichloropropane 9.84 1.2 9.94 ND 99 39-141 2,2-Dichloropropane 9.05 1.2 9.94 ND 91 26-149 1, 1 -Dichloropropene 9.03 1.2 9.94 ND 91 28-150 cis- 1,3-Dichloropropene 9.92 1.2 9.94 ND 100 34-149 trans-1,3-Dichloropropene 11.0 1.2 9.94 ND 111 36-143 Ethylbcnzene 10.8 1.2 9.94 ND 109 23-150 Hexachlorobutadiene 11.4 1.2 9.94 ND 115 10-192 4-Isopropyl Toluene 11.9 1.2 9.94 ND 120 11-165 Isopropylbenzene 11.7 1.2 9.94 ND I18 17-166 Nlethylene chloride 8.61 1.2 9.94 ND 87 28-135 Naphthalene 12.4 1.2 9.94 ND 124 10-174 n-Propylbenzene 11.3 1.2 9.94 ND 114 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Volatilepi by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (BlE0697-MS1) Source: 2103212-01 Analyzed: 05/25/21 19:22 Styrene 11.5 1.2 mg/kg 9.94 ND 116 24-154 1,1,1,2-Tetrachloroethane 11.1 1.2 9.94 ND 111 38-149 1,1,2,2-Tctrachloroethanc 10.7 1.2 9.94 ND 107 22-164 Tetrachloroethene (PCE) 9.37 1.2 9.94 ND 94 25-153 Toluene 10.4 1.2 9.94 ND 105 26-149 1,2,3-Trichlorobenzene 12.7 1.2 9.94 ND 128 10-163 1,2.4-1'richlorobenzene 12.4 1.2 994 ND 124 10-162 1, 1, 1 -Trichloroethane 9.87 1.2 9.94 ND 99 34-149 1,1,2-Trichloroethane 11.3 1.2 994 ND 113 25-175 Trichloroethene (TCE) 9.24 1.2 9.94 ND 93 25-170 Trichlorofluoromethane 12.0 1.2 9.94 ND 121 19-155 1,2,3-Trichloropropane 9.81 1.2 9.94 ND 99 32-165 1,2,4-Trimethylbenzene 11.7 1.2 9.94 ND 118 15-150 1,3,5-Trimethylbenzene 11.4 1.2 9.94 ND 114 10-158 Vinyl chloride 11.2 1.2 9.94 ND 112 22-148 Xylenes (total) 32.3 1.2 29.8 ND 108 22-153 Surrogate. Uibromo/luoromethanc. 0.0508 0.0497 /02 74-122 Surrogate' Toluene-d8 0.0509 0.0497 102 05-I28 Su•rogate:4-Bromoguorohen--ene 0.0499 0.0497 100 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Method Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OFC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015,M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601013 TCLP Chromium EPA 131 IiEPA 601013 Water OEC, CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA -FLAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA-ELAP Total Metals by ICP 601013Total Antimony EPA 6010B Solid OEC, CA-ELAP 601013 Total Arsenic EPA 601013 Solid OEC, CA-ELAP 601013 Total Barium EPA 601013 Solid OEC, CA-ELAP 601013 Total Beryllium EPA 601013 Solid OEC, CA-ELAP 601 OB Total Cadmium EPA 601013 Solid OEC, CA-ELAP 001013 Total Chromium EPA 601013 Solid OEC, CA-ELAP 601013 Total Cobalt EPA 601013 Solid OEC. CA-ELAP 6010B 'Total Copper EPA 601013 Solid OEC, CA-ELAP 6010B Total Lead EPA 601013 Solid OEC, CA-ELAP 601011 Total Molybdenum EPA 601013 Solid OEC, CA-ELAP 6010B Total Nickel EPA 601013 Solid OEC, CA-IiLAP 601013 Total Selenium EPA 601013 Solid OEC, CA -FLAP 6010B Total Silver EPA 601013 Solid OEC, CA-ELAP 601013Total Thallium EPA 601013 Solid OEC_ CA-ELAP 601013 Total Vanadium EPA 601013 Solid OFC, CA-ELAP 601013 Total Zinc EPA 601013 Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Sample Method Summary t nalysis Method Matrix Laboratory & Certification Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC, CA -FLAP Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, Intemal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasolinc EPA 8015M Solid OEC, CA-ELAP 8015 TPI1-Gasoline EPA 8015M Solid OEC, lntemal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-E.LAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OE,C, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 52 of 57 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103212 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/28/2021 10:05 Notes and Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery and4x RPD values. QM -OR The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however. both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. QR-00 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to non -homogenous sample matrix. QC batch accepted based on LCS and/or LCSD recovery and/or RPD values. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out -Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 53 of 57 �4 U 0 x a E-i '0 O 4 N O" L U M LS L N -rl O W � / Q4 CO (N l0 l0 LO N O1 N I'D LT) N O o W N r R) 7+ N rl O O N I / N >1Lo -1 Ey ro 1 N rG 5 U M Gl a C7 0 / Ln -i � o UN NriM C (0 O-Q O a)z s 4-) �4 ro-rA �4-A N i-i ;� J-L 04 U � r-d N b m E u? ro .HP,U5:;ro-,i-.-I Ga0H(nX> 0 + N co (D o + (D •-- r- O + 0) F- 0 + N Cl) •- r- O + N N rn o + N n 0 + N `- 0 0 O O O 0)00 0 0 O O O 0 0 O O O r- 0 0 O O O CO O 0 O O O LA 0 0 O O O 'ITM o 0 O O O O 0 0 0 Cl 0 O O O O N of 0 0 0 O 0 0 0 0 0 0 _ Ln of 0 -o O _ Ln 00 •o _O OD 0 0 -o F O O pC) S O O E C•j O N O -O N O O O O File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2612.D Operator RR Acquired 26 May 2021 1:56 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-01RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 12 Response_ i 85000! 800001 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 i 0.00 1.00 2.00 3.00 4.00 5.00 6.00 GOME2612.D\FID1A 7.00 8.00 9.00 1 0.00 11.00 12.00 13.00 14.00 0 V) 0 0 0 d C. -Gn of 0 -o a> 0 co 0 0 00 0 0 0 0 Go 2 U m o N O LL o N Gn L N Ln W O m p _O cu L6 >� C U o 'n a H ,{ -0 CD o 0 f C] 41 rn LO N b-- M LO U N FC - O� CD w M / U) U � � as U) N H � j N M Ili O a) p N •• 110 1O Ln N O N o W � o N ri U U� N N O O N 1 / N >1L H 00 FC U M G1 a C7 0 / LO 1— UN (Nr-iN p .. .. .. .. .. .. p N i4 4-) E a) rl(ooQ �4 zw F O a) �:5 1- n P� � n r` r- � 0 0 0 0 0 0 0 0 0 11 i4 �l H Z N O O O O O + O O O + + 0 O O O o O O O 0 O 0 O 0 O 0 O 0 (tl i+ a) + a) + 0) + a) a) a� d o 0 0 00 0 0 0 N + fZ U -1 o GO Gn � M N O CD O CD O 0 O O O r-1 a) CS' Ul E U] (0 N r- �- 0 O SD O ^ GO O 0 a 0 N O --1 P? U l (0 -H -rI Cz40<,HWX> N Ix File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2614.D Operator RR Acquired 26 May 2021 3:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-02RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 14 Response_ 110000 105000 100000 95000 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOME2614.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 x U 0 x a CH Z7 O Ll +� N Ln M it Ln U (N a W 0 U � W C1. � N N L() i Ol N •• � In M O o W N r FJ j N co FG O O N 1 / N F:4 ,7y Lo r-I H (0-1N FG U M NJ M U N N 1 M 4 C (0 O ,Q u4 mzw -P Fed a NH z M-11 �-i-4 v �4 ;�+-) R+U i r-A a) 01 U) E U) (o -rq Q U C (0 -rj -H 440 HU)X> 2 U m N lL 0 LO M N N W 2 O m m O7 lq 1�- p- n r- � 1- � O O O O O O O O O yO O 0 O O O O O O O O O O O O O t. + + + + + + O O O O O O O O O C m (D m 4) m a) a) 0 0 0 0 0 0 0 O 0 o n o In Cl) N OO CD O OOO O O O co a) aD � to LO m N ix r I O 1 O O lf) O O O O O IO r O O • O aD O O 00 O O O O o 0 O CO O 0 LO O O LO 0 0 0 0 v O ri 0 0 ri 0 0 N O O N 0 LO O O O O File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2616.D Operator RR Acquired 26 May 2021 4:26 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-03RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 16 Response 8500(y. 70000 65000 60000 550001 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOME2616.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 0 0 0 0 0 p 0 p m Co O of 0 00 0 p OD p r` 0 0 0 U o 00 N 0 O LL_ O 0 (O n N In O N W O m O (0 O x Lf) U .-I O O x U? a H O o L +� (13 b � N FG �# Cl) O P7 -H O Cl) / U) U � cW E 0 ¢ N N N C O tf) r CD o W pq N '-I (2) 0 "r � N d FC,' O O / N to -A O H r0 rl N Q FC £UM Ca a c7 0 / Ln -q�--) U-) UN NrIN +-) s j r- N O Q �4 (1)zw F J O N rl 'z, I n n n n r n r n o 0 0 0 0 0 0 0 0 J-) S4 N H a) O O O O O + O + ClO O + + O O O O O O O O O O CD O O O O O f0 ., i }4 ,-I t O t N t N + N N N N N O O O O O O O O O N }4 71 J-) Qa U r-I n 0 0 0 0 0 0 0 0 0 -i t3' m t~ m ro � � r to Lo "T M N •ri Qa U (CS -rl -ri [= 0FGHcn > NCDCO F— File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2618.D Operator RR Acquired 26 May 2021 5:18 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-04RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 18 Response 85000 80000 75000 70000 65000, 6000J 55000 50000 45000 40000 35000 30000 I 25000 20000 15000 10000 GOME2618.DT1D1A 5000 0.00 T 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 U r-I O x a 41 O 41 N M b LO U N r•G o G W •rl / U] U � co (N 0) Q0 N QQ uO N O O W � W N rl CJ N Lr) Q O O $ N I / N L ri E- c0 . 1 N F�4 X U M G1 a 0 0 /XLO H -i U N N r CO .. .. .. .. .. .. .. N �+ 4 m r- m o q �4 NZ4-1 4-) S�-I � m H 2 ro -ri SA r N $-I 71 4J U r ri N b" in rz U] (0 .'A Q U �: (0 -" -rl 44 0 a H U) x 2 U am N LL is M Cl) N W 2 O m m C m �i1 n r� n P- r- r- O O 0 N N N N N N O 0 O � Cl) stCN O O Q N 0 0 0 0 0 0 0 0 o 0 0 0 0 0 f- CO LO V M N 0 0 0 0 0 0 ai 0 0 0 0 co O -O N o O 0 I File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2624.D Operator RR Acquired 26 May 2021 7:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-05RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 24 Response_ I 85000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOME2624.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 f � h: A.P.. 9.00 10.00 11.00 12.00 13.00 14.00 X U 0 x a E-i '0 O 4 m U �1 U M iT N -rl W co x �l / 04 v� N 6l %D N •• � U-) N O o W W N rl C�J � N � Q O O � N I / N to r-I E-H (a —i N < U M C] a U o T) r-I aU N •• UN NrIM .. .. .. .. .. .. .. (1) �4 (0 O S� s4 (1)z4-4 F� Oa)E r-� 4) }-I �l (1) H z ro •rl M r- a) �4 �l 4 ¢ U r-I co U) ro •� �. U c ro -r� •rl wog NI O O 0 O O 0 0 (00 n Lc)It N N 0 0 0 0 0 0 rn of 0 0 of 0 Lq 00 0 _o 00 0 r` 0 _o 0 Lq 0 -o �.c> 7 C' 0 u'> ri O 0 Cl) 0 N O 0 N 0 O O O O I- r- O O O O O O O O O O O O O O O O O O O 0 + + 0 0 0 0 o O O 0 O 0 CD O O O O O O O O O 00 O M N m N 0 r- f00 LO 'T i- File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2626.D Operator RR Acquired 26 May 2021 8:45 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-06RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 26 Response 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOME2626.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 I 9.00 1 II' Ih 3.00 11.00 12.00 13, 00 14.00 U 0 x a E1 O �11- Gl O Ln f N H W m x :� 0 W / p, C rl N N LO r T N ko LO M O O W Ip N rl 7-+ N t� FC O O � N I / N Ln ri E1 ro rl N r� UM C] a 0 0 /:Ell H c.-) �w UN NrIM .. .. .. .. .. .. .. N �4 +) N rl rt O Q �-4 N Z w 4-L f4 �l N H rz (0 -,1 f 4 r-� N S4 :1 +-) Q1 U r-I r-I N b" m rz co « 1 04 a ro-H LV 0FGHM > S U Q 0 LL O L`C N W 2 O m N O tq 0 0 0 0 'o 0 0) 0 _o . of O co 0 _o 00 0 •o _0 0 �o _o cc O O O LO LO v O O O UC O r r r r r r r o 0 0 0 0 0 0 0 0 0 o O o 0 0 0 0 0 O O o 0 0 0 0 + + t + + + + O O O O O O O O O N N co N N Cl) N N N N O O O O O O O O O O O O O O O O •- `- O m O 00 r to Lli V M N File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2628.D Operator RR Acquired 26 May 2021 9:36 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-07RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 28 GOME2628.D\FID1A 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 I 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 k U 1-1 x a H 0 Q � M 3 Ln U N FG W o � pq -r-I U � 0, u) N N Ln N O O W � fA N rl NJ N 00 Q' O O / N Ln r-i H 0 —i (N G1 .a C7 0 / in rHC--)m CJ N N r N .. .. .. .. .. .. .. N }4 -P i N rl N O �4 N 44 � !-) 14 7� N H Z ro-H �,-� N V m E O -I Q U � (0-r-I -r-I x U m N 0 LL co N W 2 O in <6 C O CA U) o C + o CD d N n n n n n n n O O O O O Cl 0 O O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 + + + + + + + 0 O 0 0 0 0 o O o d d a) d d d d o 0 0 0 0 0 0 C. 0 t0 Ui V M N e- O O O O CD O O O O O r r •- r r r m 00 n to Lf) V Cl) N File C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2630.D Operator RR Acquired 26 May 2021 10:28 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2103212-08RE1@ Misc Info : 1@BlE0737 GRO Solid Vial Number: 30 Response_ 850J i 80000, 750001 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 G0ME2630.DT1D1A 10000 I�Ji I 5000 of 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 9 E 141— Cc: 0 a. at� rn 0? LL . cu sj� m it - m co m d a: A 0 S E 0 j u) cc 2 t: 0 E m 0 3 E c -i 0 �- V,4 SPIIOS PGAJOSJO IVIO.L f4JAISOMOO m m zBoo I Mos 80d i 169d C QN 0 o OOLES SOOAS O z y W9080WOO-dHi z cc C ap1jinS (D cc OPIUBAO SM308H E > z do N Isil jjn:j qoqZs X. 'K 0 co C4 z .11new ZZ 81111 X m 72 o In M (D r E::4): 0 M ..C. u) A. Ir E m OV 00 00 1� DO 9 t eq E u 00 0 z 0 12 S c m 0 fu :-c x V-4 .E m El -a . N m a.A: u 0 C .0 kP E 'Ua C C', P r_E U-1 CL IN 0 C4 th m E M ILI r 10 0 ins p r. in El El to In m .0 m c) C) CL E cr cr cr m E cc cz w1w u P -i d: 0 ti 0 u 0 \ \ S _j � - e ) 1 E ° k ) Q \ R a f (L \ 0um - LO § ) ƒ / ) \ \ � � } § ) ) Ef �� cc a) § c a a E )f < m o OCO « ƒfI % $ $ ) ) ƒ �/ ECD / / ] \ G�\__ L)f»/\ q 3 # ) E G G 3 3 § k k \ k u /�ƒ\ ] f £ _ ) o 3: 0 ! 0 $ 2 m o > o I D E k*«\�\ _0 3 o I2c\ ° k ^ j § a 3 § J 7 « M M 2 o « \ \ \ \ \ / s o. R N C N E 1I1kULLLLLLLkULH E O U a� c 0 U� n� N N N N d c v Li? 0 U 0 U 0 N 0 U 0 U 0 U 0 0 w 0 co U N c c c c c c c c Y Y_ Y_ Y_ Y_ Y_ Y_ Y _ @ M Q O� @ Q O� m Q o� @ Q O m R _ Q O @ 3 _ Q O @ 3 _ Q 0 @ 3 Q O > > > , > , > , > >CO, > N N N @ N N N N N @ N @ N @ N N N E v 0 v y v 0 S LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL C O a Q Q Q Q Q Q Q Q IDN N O N N O N N O N N O N N O N N O N N O ((no N O c > _@ > m > _@ > _@ > m > @ > @ > _m C N E N E N N N E N E N E N E O U O a0 o N O O o N O O o N 0 a0 0 N O aD o N O c0 O N O 00 o N O c0 O N cU U Q OO Q m Q Q m Q 00 d<.. H;-� 00 uc<.o II-W MM��n O .I O O O O O O O mm C � 0 0N JIN 171 co LO N LO 0 cc U- L: a a a Avo m!; a J -i J a U a a a U me U H N 1�J p C N J N U U U U U U V 1- I- F m u U J J J U U J J U U J U y= U) U) � J N — V T N sPIPS PenloslO Idol Lo A)IMsaJOO « « 0 C 0 zoos VMS n 80d Used p. m lNIH4�lusl � O o DOM? saOAS a C ^t O y = W9tW8 OWa9 • dHl z '� a r. o d > oa ePUms 1 eplueRO enpoeea N !- i tip Z �a + w y is! 1 U�d 809Z8 i� %` .� �C o u N CIA Z soneW - ZZ sau c .°3 U m Cy Q a� m m Y a m m m r LIP ~ m cr > > o m 7 D! m m n A3 00 N Q tb 10 c 00 4 ❑ ❑ rJ Q m ci m °c ❑ .. CE Z ? 12 6 r oo � rt b N❑ �' +°+ � C Z U G O w:a .� D x a� ■❑ d - 7J C, m at U y n u 0 Y 78 b 0 v m 3 �n m m sy 03 > a a. O 00 U U 6. 11 El to Co m > > > m E .. to v 0'a '� g c a, o- m m E m c c c m U i t"n V F R c4 H w U U .- � i= a d 3F7 N" 6 Z 0 F- U U) d U w n. rn Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2103479 Pacific Petroleum California P. O. Box 2646 Report Date: June 09, 2021 16:44 Orcutt, CA 93457 Project: Pacific Petroleum Number: NHC SLO, 2640 Broad Street Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com This laboratory is accredited in accordance with the recognised International Standard ISOAEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-IAF Communique dated April 2017) 307 Roemer Way, Suite 300 ��\/��� client.oec.com\reports Santa Maria, CA 93454 www.oecusa.com Main: (805) 922-4772 FAA TNI 2016 & ISO/lEC 17025:2017 Fax: (805) 925-3376 : ���\.�� �esao8 CA-ELAP 2438, TNI 02666 Accreditation #99137 D- -- 7 ,.P10 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Sununary Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bottom East @ 12' 2103479-01 Solid Solid 06/03/2021 11:50 06/04/2021 12:50 Bottom West @ 12' 2103479-02 Solid Solid 06/03/2021 11:55 06/04/2021 12:50 Sample Batch ' p. Analysis Batch ID Preparation Date/Time OEC Admin Services Chromatograms Semi -Volatile Organic T,PH by GC/F1D 8015 Diesel & Motor Oil List BIF0145 06I04/2021 16:24 STLC Metals by ICP 601013 STLC B I F0261 06/09/2021 08:56 STLC Metals Extraction STLC Metals Extraction B 1 F0229 06/07/2021 16:29 Total Metals by CVAA Mercury Total EPA 7471A B 1 F0194 06i07/2021 07:40 Total Metals by ICP 601013 Total B I F0197 06/07/2021 08:26 Volatile Organic Compounds by GC/MS 8200B Full List B 1 F0146 06/04/2021 12:21 Volatile Organic TPH by GC/FID 8015 TPH-Gasolinc B I F0154 06/04/2021 10:34 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples 0 Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.087 mg/kg 1 BIF0194 06/07/21 16:25 EPA 7471A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B 1 F0197 06/07/21 14:12 EPA 6010B Arsenic 5.6 1.9 Barium 120 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 73 0.47 Cobalt 18 0.47 Copper 47 0.93 Lead 8.2 0.47 Molvbdenum ND 0.47 Nickel 130 0.47 Selenium ND 1.9 Silver ND 0.47 " Thallium ND 0.93 Vanadium 49 1.9 Zinc 65 1.9 STLC Metals by ICP Chromium ND 0.020 mg/l. 2 B 1 F0261 06/09/21 14:34 STI.C/I?PA 601 OB Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.5 mg/kg 1 BIF'0154 06/04/21 17:01 EPA 8015M Surrogate: 4-Bromo/luorohen_ene 92% (39 - 157) " " N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data.: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 mg/kg TPH Motor Oil (C23-('40) ND 50 " Surrogate: o-Tetrhen.11 87 % (65 - 136 ) BIF0145 06/05/21 12:12 EPA8015M The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kg 1 BIF0146 06/04/21 16:16 EPA8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0,050 Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobcnzene ND 0.050 " Chloroethane ND 0.050 Chlorotorm ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 " 4-Chlorotoluene ND 0.050 " Dibromochloromethane ND 0.050 1,2-Dibromo-3-chloropropane ND 0.050 1,2-Dibrotnoethane (EDB) ND 0.050 Dibromomethane ND 0.050 1,2-Dichlorobenzene ND 0.050 1,3-Dichlorobcnzcnc ND 0.050 " 1,4-Dichlorobcn7cnc ND 0.050 Dichloroditluoromcthanc ND 0.050 1, 1 -Dichloroethane ND 0.050 " 12-Dichloroethane ND 0.050 LI-Dichloroethene ND 0.050 cis-1,2-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 13-Dichloropropane ND 0.050 2,2-Dich1oropropane ND 0.050 1, 1 -Dichloropropene ND 0.050 cis-1,3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 F.1hylbenzcne ND 0.050 COP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 5 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NEC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID: Bottom East @ 12' Sampled: 06/03/21 11:50 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.050 mglkg 1 BIF0146 06/04/2116:16 EPA8260B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1, 1, 1,2-Tetrachloroethane ND 0.050 1,L2,2-Tetrachloroethane ND 0.050 Tetrachlorocthcne (PCE) ND 0.050 TolUCnc ND 0.050 1,23-Trichlorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.050 L1,1-Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 Trichlorolltwromethane ND 0.050 1,23-Trichloropropane ND 0.050 L2.4-7rimethylbenzene ND 0.050 1,3.5-71'rimethytbenzene ND 0.050 Vinyl chloride ND 0.050 " Xylencs (total) ND 0.050 Surrogate: Dihromolluoromethane 103 (74 - 122) Surrogale: Toluene-d8 99 (65 - 128 ) Surrogate: 4-Bromollaorohen_ene 105 '% (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg I BIF0194 06/07/21 16:27 EPA 747]A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I F0197 06/07/21 14:15 EPA 601(IB Arsenic 7.4 1.9 Barium 160 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 51 0.48 Cobalt 14 0.48 Copper 63 0.96 Lead 8.9 0.48 Molybdenum 0.57 0.48 Nickel 88 0.48 Selenium ND 1.9 Silver ND 0.49 Thallium ND 0.96 Vanadium 52 1.9 Zinc 71 1.9 STLC Metals by ICP Chromium ND 0.020 mg/L 2 B I F0261 06/09/21 14:37 STLC/EPA 6010B Volatile Organic TPH by GC/FID TPFIGasoline (C5-('12) ND 4.4 uig./kg 1 BIF0154 06/04/21 17:29 EPA8015M Surrogutc: d-BromoJlrwroben_ene 95 Y" (.39- 157) N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-C22) ND 9.9 mglkg 1 BIF0145 06/05/21 12:34 EPA 8015M TPH Motor Oil (('23-C40) ND 50 11 11 1. 11'. Sunvgate: o-Teiphen-Vl 90 Y" (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 C A 16MOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 ReportAnalytical Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID: 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.048 mglkg 1 BIF0146 06/04/21 15:48 EPA8260B Bromobenzene ND 0.048 " Bromochloromethane ND 0.048 Bromodichloromethane ND 0.048 " Broniofonn ND 0.048 Bromomethane ND 0.048 " n-Butylbenzene ND 0.048 sec-Butylbenzene ND 0.048 tert-Butyl benzene ND 0.048 " Carbon tetrachloride ND 0.048 Chlorobcnzcnc ND 0.048 Chloroethane ND 0.048 Chlorofonn ND 0.048 Chloromethane ND 0.048 2-Chlorotoluene ND 0.048 " 4-Chlorotoluene ND 0.048 Dibromochloromethane ND 0.048 " 1,2-Dibronio-3-chloropropane ND 0.048 " 1,2-Dibrontoethane (EDB) ND 0.048 " Dibromomethane ND 0.048 1,2-Dichlorobenzene ND 0.048 1.3-Dichlorobenzene ND 0.048 1,4-Dichlorobenzene ND 0.048 " Dichlorodifluoromethanc ND 0.048 " 1, 1 -Dichloroethane ND 0.048 1,2-Dichloroethane ND 0.048 1,1-Dichloroethene ND 0.048 cis-1.2-Dichloroethene ND 0.048 trans-1,2-Dichloroethene ND 0.048 1,2-Diehloropropane ND 0.048 1,3-Diehloropropane ND 0.048 2,2-Diehloropropane ND 0.048 1, 1 -Dichloropropene ND 0.048 cis-1.3-Dichloropropene ND 0.048 " trans-1,3-1)ichloropropene ND 0.048 Ethylbcnzene ND 0.048 CC111 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Analytical Report for Samples Sample ID: Bottom West @ 12' Sampled: 06/03/21 11:55 Matrix: Solid Sampled by: C Reynolds Lab ID : 2103479-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Iexachlorobutadiene ND 0.048 mglkg I B l F0146 06/04/21 15:48 EPA 8260B 4-Isopropyl Toluene ND 0.048 lsopropylbenzene ND 0.048 Methylene chloride ND 0.048 Naphthalene ND 0.048 n-Propylbenzene ND 0.048 Styrene ND 0.048 1,1,1.2-Tetrachloroethane ND 0.048 1,1,2,2-Tetrachloroethane ND 0.048 " Tetrachlorocthcnc (PCE) ND 0.048 Toluene ND 0.048 1,23-Trichlorobenzene ND 0.048 1,2.4-Trichloroben7ene ND 0.048 1. 1, 1 -Trichloroethane ND 0.049 1,1,2-Trichloroethane ND 0.048 Trichloroethene (WE) ND 0.048 Trichlorofluoromethane ND 0.048 1.2,3-Trichloropropane ND 0.048 1,2,4-Trimethylbenzene ND 0.048 13,5-Trimethylbenzene ND 0.048 Vinyl chloride ND 0.048 Xylcnes (total) ND 0.048 Surrogate: Dibronuillaoromethane 104 N, ( 74. 122 ) Surrogate: Tolueuc48 1 02 3b (65. 1 LN) Surrogate: d-Bronto)lttoroben_ene 104 % ( 75. 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-E LAP 2438, TN102666 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Pnoe In"f32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO194 - EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (B1F0194-BLK1) Analyzed: 06/07/21 12:49 Mercury ND 0.10 mg/kg LCS (B1F0194-BS1) Analyzed: 06/07/21 12:53 Mercury 0.782 0.10 mg%kg 0.833 94 85-115 LCS Dup (B1F0194-BSD1) Mercury Duplicate (B1F0194-DUPl) Mercury Matrix Spike (B1F0194-MSI) Mercury 0.859 Source:2103489-02 ND Source:2103489-02 0.927 Matrix Spike Dup (B1F0194-MSD1) Source: 2103489-02 Mercury 0.839 Post Spike (B1F0194-PSI) Source: 2103489-02 Mercury 5.52 Analyzed: 06/07/21 13:30 0.10 mg/kg 0.833 103 85-115 9 20 Analyzed: 06/07/21 13:34 0.097 mg/kg ND 20 Analyzed: 06/07/21 13:37 0.091 mg'kg 0.755 ND 110 75-125 Analyzed: 06/07/21 13:39 0.089 mg/kg 0.742 ND 113 75-125 1 20 Analyzed: 06/07/21 13 :41 ug/L 25.0 0.00199 22 85-115 QL-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIlent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page I 1 of 32 r A 6M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLK1) Analyzed: 06/07/21 13:30 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 " Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 Nickel ND 0.50 Selenium ND 2.0 ' Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 Zinc ND 2.0 " LCS (B1FO197-BS1) Analyzed: 06/07/21 13:35 Antimony 92.0 2.5 mgtkg 100 92 80-120 Arsenic 97.2 2.0 100 97 80-120 Barium 99.6 1.0 100 100 80-120 Beryllium 95.1 0.50 100 95 80-120 Cadmium 98.2 0.25 100 98 80-120 Chromium 98.8 0.50 100 99 80-120 Cobalt 99.2 0.50 100 99 80-120 Copper 98.2 1.0 100 98 80-120 Lead 100 0.50 100 100 80-120 Molvbdenum 96.0 0.50 100 96 80-120 Nickel 99.0 0.50 100 100 80-120 Selenium 96.4 2.0 100 96 80-120 Silver 4.92 0.50 5.00 98 80-120 Thallium 100 LO 100 100 80-120 Vanadium 96.6 2.0 100 97 80-120 Zinc 98.6 2.0 100 99 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSD1) Analyzed: 06/07/21 13:37 Antimony 94.8 2.5 mg/kg 100 95 80-120 3 20 Arsenic 98.8 2.0 100 99 80-120 2 20 Barium 101 1.0 100 101 80-120 1 20 Beryllium 96.5 0.50 100 96 80-120 1 20 Cadmium 99.2 0.25 100 99 80-120 1 20 Chromium 100 0.50 100 100 80-120 1 20 Cobalt 100 0.50 100 100 80-120 1 20 Copper 99.8 1.0 100 100 80-120 2 20 Lead 101 0.50 100 101 80-120 1 20 Molybdenum 98.2 0.50 100 98 80-120 2 20 Nickel 101 0.50 100 101 80-120 1 20 Selenium 97.8 2.0 100 98 80-120 1 20 Silver 4.93 0.50 5.00 99 80-120 0.1 20 Thallium 102 1.0 100 102 80-120 1 20 Vanadium 98.0 2.0 100 98 80-120 1 20 Zinc 99.8 2.0 100 100 80-120 1 20 Duplicate (B1F0197-DUPl) Source: 2103489-01 Analyzed: 06/07/21 13:52 Antimony ND 2.4 mg/kg ND 20 Arsenic 1.22 1.9 ND 20 Barium 21.0 0.97 22.9 8 20 Beryllium ND 0.49 ND 20 Cadmium ND 0.24 ND 20 Chromium 1.94 0.49 2.02 4 20 Cobalt 1.40 0.49 1.78 24 20 QR-04 Copper 1.33 0.97 1.40 5 20 Lead 1.23 0.49 1.40 13 20 Molybdenum ND 0.49 ND 20 Nickel 1.31 0.49 134 2 20 Selenium ND L9 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.97 ND 20 Vanadium 3.80 1.9 4.18 8 20 Zinc 4.32 1.9 4.51 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MS1) Source: 2103489-01 Analyzed: 06/07/21 13:40 Antimony 70.3 2.3 mg/kg 93.4 ND 75 10-116 Arsenic 93.3 1.9 93.4 ND 100 77-121 Barium 119 0.93 93.4 22.9 102 30-169 Beryllium 90.1 0.47 93.4 ND 96 96-1 t I Cadmium 91.8 0.23 93.4 ND 98 81-112 Chromium 96.8 0.47 93.4 2.02 102 75-129 Cobalt 94.2 0.47 93.4 1.78 99 71-121 Copper 96.2 0.93 93.4 1.40 102 68-135 Lead 94.4 0.47 93.4 1.40 100 72-121 Molybdenum 88.2 0.47 93.4 ND 94 70-112 Nickel 95.2 0.47 93.4 1.34 101 73-121 Selenium 90.1 1.9 93.4 ND 97 76-116 Silver 4.56 0.47 4.67 ND 98 54-t32 Thallium 92.3 0.93 93.4 ND 99 64-120 Vanadium 96.5 1.9 93.4 4.18 99 78-124 Zinc 98.0 L9 93.4 4.51 100 50-143 Matrix Spike Dup (B1F0197-MSD1) Source: 2103489-01 Analyzed: 06/07/21 13:42 Antimony 70.4 2.4 mg"kg 95.8 ND 73 10-116 0.1 20 Arsenic 94.3 1.9 95.8 ND 98 77-121 1 20 Barium 116 0.96 95.8 22.9 97 30-169 3 20 Beryllium 91.2 0.48 95.8 ND 95 86-I11 t 20 Cadmium 92.3 0.24 95.8 ND 96 81-112 0.6 20 Chromium 97.6 0.48 95.8 2.02 100 75-129 0.8 20 Cobalt 94.7 0.48 95.8 1.78 97 71-121 0.6 20 Copper 96.9 0.96 95.8 1.40 100 68-135 0.7 20 Lead 94.9 0.48 95.8 1.40 98 72-121 0.6 20 Molvbdenum 88.6 0.48 95.9 ND 93 70-112 0.5 20 Nickel 95.5 0.48 95.8 1.34 98 73-121 0.3 20 Selenium 91.2 1.9 95.8 ND 95 76-116 1 20 Silver 4.04 0.48 4.79 ND 97 54-132 2 20 Thallium 93.1 0.96 95.8 ND 97 64-120 0.9 20 Vanadium 97.2 1.9 95.8 4.18 97 78-124 0.7 20 Zinc 103 1.9 95.8 4.51 103 50-143 5 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Total Metals by ICP - Quality Control lnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PSI) Source: 2103489-01 Analyzed: 06/07/21 13:45 Antimony 2.03 mg/L 2.00 0.00248 101 75-125 Arsenic 2.04 2.00 0.0179 101 75-125 Barium 2.50 2.00 0.460 102 75-125 Beryllium 1.96 2.00 0.00218 98 75-125 Cadmium 2.00 2.00 -0.00308 100 75-125 Chromium 2.07 2.00 0.0408 101 75-125 Cobalt 2.00 2.00 0.0359 101 75-125 Copper 2.06 2.00 0.0283 102 75-125 Lead 2.07 2.00 0.0283 102 75-125 Molybdenum 2.01 2.00 -0.00109 101 75-125 Nickel 2.06 2.00 0.0271 102 75-125 Selenium 1.99 2.00 -0.0103 99 75-125 Silver 0.0945 0.100 -0.00169 94 75-125 Thallium 2.03 2.00 -0.00407 101 75-125 Vanadium 2.08 2.00 0.0842 100 75-125 Zinc 2.10 2.00 0.0909 101 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 STLC Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIF0261 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (BlF0261-BLKI) Chromium LCS (B1F0261-BS1) Chromium LCS Dup (BlF0261-BSD1) Chromium Duplicate (BlF0261-DUPI) Chromium Leach Fluid Blank (BlF0261-LBK1) Chromium Leach Fluid Blank (B1F0261-LBK2) Chromium Leach Fluid Blank (B1F0261-LBK3) Chromium Analyzed: 06/09/21 13:50 ND 0.010 ma/L Analyzed: 06/09/21 14:17 10.1 0.010 mg/L 10.0 Analyzed: 06/09/21 14:19 10.2 0.010 mg/L 10.0 Source:2103218-01 Analyzed: 06/09/21 14:27 1.22 0.020 mg/l. 1.22 Analyzed: 06/09/21 13:52 ND 0.020 mg/L Analyzed: 06/09/21 13:55 ND 0.020 mg/l. Analyzed: 06/09/21 13: 5 8 ND 0.020 mg/l. 101 80-120 102 80-120 0.5 20 0.08 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Pnan 16 of?7 &M*�, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLKI) Analyzed: 06/04/21 12:45 TPH Gasoline (C5-C12) ND 0.49 mg/kg Surrogate. 4-Bromolluorohenfene 0.107 " 0.123 87 39-157 LCS (B1F0154-BS1) Analyzed: 06/04/21 11:48 TP11Gasoline (0-C12) 1.38 0.50 mg/kg 0.998 138 68-139 San'rogate:4-Bromulluorohcn.-cne 0.158 " 0.125 126 39-157 LCS Dup (B1F0154-BSDI) Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12) 1.29 0.50 mg/kg 1.00 128 68-139 7 20 Surrogate:4-Bromnhnorohen_ene 0.146 0.125 116 39-157 Duplicate (B1F0154-DUPl) Source: 2103455-02RE1 Analyzed: 06/04/21 15:35 TPH Gasoline (C 5-C12) ND 0.50 mg/kg 0.113 20 Surrogate:4-Bromolhrorobenzene 0.113 110.124 92 39-157 Matrix Spike (B1F0154-MS1) Source: 2103429-02 Analyzed: 06/04/21 19:23 TPH Gasoline (C5-('12) 0.905 0.49 mg/kg 0.973 ND 93 10-171 Surrogate:4-Broniolloorohcnrene 0.132 " 0.122 109 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103475 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Semi-Volatileby 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLKI) Analyzed: 06/04/21 11:45 TPH Diesel (C13-C'22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 1. Surrogate: o-Terpher.rl 41.5 1150.0 83 65-136 LCS (B1F0145-BSI) Analyzed: 06/04/21 11:45 TPH Diesel (C'13-C22) 434 10 mgrkg 499 87 72-115 TPII Motor Oil (C23-C40) 420 50 499 84 74-126 Surrogate: o-Terphenyl 45.8 49.9 92 65-136 LCS Dup (B1F0145-BSD1) Analyzed: 06/04/21 12:07 TPH Diesel (C13-C22) 444 10 mg/kg 499 89 72-115 2 20 TPI I Motor Oil (C23-C40) 441 50 499 88 74-126 5 20 Surrogute: o-Terphern.l 46.7 49.9 94 65-136 Duplicate (B1F0145-DUPI) Source: 2103472-01 Analyzed: 06/04/21 16:23 TPH Diesel (C'13-('22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) ND 50 ND 20 Surrogate: o-Terphenyl 40.5 49.9 81 65-136 Matrix Spike (B1F0145-MS1) Source: 2103472-01 Analyzed: 06/04/21 15:37 TPH Diesel (CI 452 10 mg/kg 498 ND 91 46-147 TPH Motor Oil (C23-C40) 500 50 498 ND 100 35-171 Surrogate: o-Terphenvl 41.6 49.8 84 65-136 Matrix Spike Dup (B1F0145-MSD1) Source: 2103472-01 Analyzed: 06/04/21 16:00 TPH Diesel (C13-C'22) 496 10 mg/kg 498 ND 100 46-147 9 20 TPH Motor Oil (('23-C40) 517 50 498 ND 104 35-171 3 20 Surrogate• o-Terphen},l 44.0 49.8 88 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatilepi i by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1) Analyzed: 06/04/21 11:32 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " Bromochloromethane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 Bromoniethane ND 0.0050 " n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 " Chlorobenzene ND 0.0050 " Chloroethane ND 0.0050 " Chloroform ND 0.0050 " Chloromethane ND 0.0050 " 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1,2-Dibromo-3-chloropropane ND 0.0050 " 1,2-Dibromoethane (EDB) ND 0.0050 Dibromomcthane ND 0.0050 1,2-I)ichlorobenzene ND 0.0050 " 1,3-Dichlorobenzenc ND 0.0050 " 1,4-Dichlorobenzene ND 0.0050 Dichlorodifluoromethane ND 0.0050 CCHI 1,1-Dichloroethene ND 0.0050 1,2-Dichlorocthanc ND 0.0050 I,1-Dichloroethene ND 0.0050 " cis-1.2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 " 1.2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 1, 1 -Dichloropropene ND 0.0050 cis-1.3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 F,thylbenzene ND 0.0050 " Hexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 " Isopropyl6enzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzenc ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 o f 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GUMS - Quality Control J IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1) Analyzed: 06/04/21 11:32 Styrene ND 0.0050 mgtkg 1,1.1,2-Tetrachloroethane ND 0.0050 1,1,2,2-Tetrachloroethanc ND 0.0050 " Tetrachloroethene (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Tiichlorobenzene ND 0.0050 1,2,4-Trichloroben7ene ND 0.0050 1,1,1-Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorolluoromethane ND 0.0050 " 1,2.3-Trichloropropane ND 0.0050 " 1,2,4-Trimethylbenzene ND 0.0050 " 1,3,5-Trim ethyl benzene ND 0.0050 Vinyl chloride ND 0.0050 " Xylenes (total) ND 0.0050 Surrogate: Dihronwlluoromethane 0.0 16 0.049N 104 74-122 Surrogate_ Toluene-dN 0.0503 0.0498 101 05-128 Su•rogate:4-BromoJluorohenzene 0.0529 0.0498 106 75-121 LCS (B1F0146-BSI) Analyzed: 06/04/21 09:47 Benzene 0.0406 0.0050 mglkg 0.0398 102 70-131 Bromobenzene 0.0466 0.0050 0.0399 117 74-130 Bronx>chloromethane 0.0399 0.0050 0.0398 100 64-133 Bromodichloromethane 0.0445 0.0050 0.0398 112 69-137 Bromoform 0.0447 0.0050 0.0398 112 55-132 Bromomethane 0.0407 0.0050 0.0399 102 10-142 n-Butylbcnzene 0.0476 0.0050 0.0398 120 64-156 sec-Butylbenzene 0.0493 0.0(150 0.0398 124 75-155 tert-Butylbenzene 0.0482 0.0050 0.0398 121 74-144 Carbon tetrachloride 0.0442 0.0050 0.0398 111 67-135 Chlorobenzene 0.0445 0.0050 0.0398 112 73-134 C'hloroethane 0.0390 0.0050 0.0398 98 10-167 Chloroform 0.0412 0.0050 0.0398 104 69-124 C hloromethane 0.0297 0.0050 0.0398 75 34-136 2-Chlorotoluene 0.0454 0.0050 0.0398 114 75-135 4-Chlorotoluene 0.0460 0.(1050 0.0398 116 70-138 Dibromochloronrethane 0.0439 0.0050 0.0398 110 67-135 1,2-Dibromo-3-chloropropanc 0.0435 0.0050 0.0398 109 41-149 12-Dibronroethane (EDB) 0.0409 0.0050 0.0398 103 68-131 Dibronwmethane 0.0433 0.0050 0.0398 109 61-140 12-Dichlorobenzene 0.0458 0.0050 0.0398 115 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 20 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Z103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Coinpounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BSI) Analyzed: 06/04/21 09:47 1,3-Dichlorobenzene 0.0462 0.0050 mg/kg 0.0398 116 76-138 IA-Dichlorobenzene 0.0457 0.0050 0.0398 115 72-132 Dichlorodiiluoromethanc 0.0210 0.0050 0.0398 53 10-155 1,1-Dichloroethane 0.0389 0.0050 0.0398 98 63-139 1,2-Dichlorocthanc 0.0416 0.0050 0.0398 104 64-126 1, 1 -Dichloroethene 0.0342 0.0050 0.0398 86 52-167 cis-1,2-Dichloroethene 0.0401 0.0050 0.0398 101 70-135 trans-1,2-Dichloroethene 0.0392 0.0050 0.0399 99 67-147 1,2-Dichloropropane 0.0406 0.0050 0.0398 102 68-131 1,3-Dichloropropane 0.0405 0.0050 0.0398 102 64-128 2,2-Dichloropropane 0.0432 0,0050 0.0398 109 63-154 I,1-Dichloropropene 0.0393 0.0050 0.0398 99 68-138 cis-1.3-Dichloropropene 0.0416 0.0050 0.0398 105 72-134 trans-1,3-Dichloropropene 0.0437 0.0050 0.0398 110 69-132 Ethylbenzene 0.0449 0.0050 0.0398 113 68-136 Ilexachlorobutadiene 0.0546 0.0050 0.0399 137 72-198 4-Isopropyl Toluene 0.0504 0,0050 0.0398 127 74-150 Isupropylbenzene 0.0473 0.0050 0.0398 119 71-149 Methylene chloride 0.0346 0.0050 0.0398 87 51-127 Naphthalene 0.0482 0.0050 0.0398 121 57-158 n-Propylbenzene 0.0474 0.0050 0.0398 119 70-143 Styrene 0.0456 0.0050 0.0398 115 68-138 1,1,1,2-Tetrachloroethane 0.0459 0.0050 0.0398 115 76-130 1,1,2,2-Tetrachloroethanc 0.0399 0.0050 0.0398 too 60-136 Tetrachloroethene (PCE) 0.0443 0.0050 0.0399 111 73-139 Toluene 0.0430 0.0050 0.0398 108 72-128 1,2,3-Tiichlorobenzene 0.0507 0.0050 0.0398 127 61-166 1,2,4-Trichlorobenzene 0.0502 0.0050 0.0398 126 71-158 1,1,1-Trichlorocthane 0.0424 0.0050 0.0398 107 71-135 1,1,2-Trichlorocthane 0.0414 0.0050 0.0398 104 64-132 Trichloroethene (TCE) 0.0442 0.0050 0.0398 111 74-139 Trichlorotluoromethane 0.0429 0.0050 0.0398 108 30-156 1,2,3-Trichloropropane 0.0452 0.0050 0.0398 114 67-123 1,24-Trimethylbenzene 0.0454 0.0050 0.0398 114 68-134 1,3,5-Trimethylbenzene 0.0401 0.0050 0.0398 116 71-140 Vinyl chloride 0.0326 0.0050 0.0398 82 43-144 Xylenes (total) 0.133 0.0050 0.119 112 69-138 Surrogate: Dihnnnglluoninicihone 0.0525 0.0497 106 74-122 Surrogate. 7bluene-d8 0.0517 0.0497 104 65-128 Surrogate:4-Bronto/luoroben_c°nc 0.0530 0.0497 107 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CCFH CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 32 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes l Level Result Limits Limit Batch BlFO146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSDI) Analyzed: 06/04/21 10:13 Benzene 0.0423 0.0050 mg/kg 0.0400 106 70-131 4 20 Bromobenzene 0,0498 0.0050 0.0400 124 74-130 7 20 Bromochloromcthanc 0.0412 0.0050 0.0400 103 64-133 3 20 Bromodichloromethane 0.0455 0.0050 0.0400 114 69-137 2 20 Bromoform 0.0458 0.0050 0.0400 115 55-132 2 20 Bromomethane 0.0391 0.0050 0.0400 98 10-142 4 20 n-Butylbenzene 0.0476 0.0050 0.0400 119 64-156 0.1 20 sec-Butylbenzene 0.0508 0.0050 0.0400 127 75-155 3 20 test-Butylbenzene 0.0496 0.0050 0.0400 124 74-144 3 20 Carbon tetrachloride 0.0456 0.0050 0.0400 114 67-135 3 20 Chlorobenzene 0.0457 0.0050 0.0400 114 73-134 3 20 Chloroethane 0.0394 0.0050 0.0400 98 10-167 1 20 Chloroform 0,0421 0.0050 0.0400 105 69-124 2 20 Chloromethane 0.0308 0.0050 0.0400 77 34-136 4 20 2-Chlorotoluene 0.0452 0.0050 0.0400 113 75-135 0.4 20 4-01101-0101uene 0.0468 0.0050 0.0400 117 70-138 2 20 Dibromochlorontethane 0.0463 0.0050 0.0410 116 67-135 5 20 1,2-Dibromo-3-chloropropane 0.0461 0.0050 0.0400 115 41-149 6 20 1,2-Dibromoethane(EDB) 0.0422 0.0050 0,0400 105 68-131 3 20 Dibrrmumrcthanc 0.0459 0.0050 0.0400 115 61-140 6 20 1,2-Dichlorobenzene 0.0472 0,0050 0.0400 118 76-136 3 20 1,3-Dichlorobenzene 0.0489 0.0050 0.0400 122 76-138 6 20 1,4-Dichlorobenzene 0.0472 0.0050 0.0400 118 72-132 3 20 Dichloroditluoromethane 0,0229 0.0050 0.0400 57 10-155 8 20 1,1-Dichloroethane 0.0405 0.0050 0.0400 WI 63-139 4 20 1,2-Dichloroethane 0.0425 0.0050 0.0400 106 64-126 2 20 1, 1 -Dichloroethene 0.0347 0.0050 0.0400 87 52-167 2 20 cis-1,2-Dichloroethene 0.0420 0.0050 0.0400 105 70-135 5 20 trans-1,2-Dichloroethene 0.0401 0.0050 0.0400 100 67-147 2 20 1,2-Dichloropropane 0.0430 0.0050 0.0400 107 68-131 6 20 13-Dichloropropane 0.0426 0.0050 0.0400 106 64-128 5 20 2,2-Dichloropropane 0.0446 0.0050 0.0400 111 63-154 3 20 I,1-Dichloropropene 0.0406 0.0050 0.0400 102 68-138 3 20 cis-1,3-Dichloropropene 0.0434 0.0050 0.0400 108 72-134 4 20 trans- l,3-Dichloropropene 0.0454 0.0050 0.0400 114 69-132 4 20 Ethvlbenzene 0.0470 0.0050 0.0400 118 68-136 5 20 11exachlorobutadione 0.0549 0.0050 0.0400 137 72-198 0.5 20 4-Isopropyl Toluene 0.0514 0.0050 0.0400 128 74-150 2 20 Isopropylbenzene 0.0499 0.0050 0.0400 125 71-149 5 20 Methylene chloride 0.0360 0.0050 0.0400 90 51-127 4 20 Naphthalene 0.0511 0.0050 0.0400 128 57-158 6 20 n-Propylbenzene 0.0466 0.0050 0.0400 116 70-143 2 20 CCFH The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) Analyzed: 06/04/21 10:13 Styrene 0.0479 0.0050 mg/kg 0.0400 120 68-138 5 20 1, 1, 1,2-Tetrachloroethane 0.0490 0.0050 0.0400 123 76-130 7 20 1.1,2,2-Tetrachloroethane 0.0417 0.0050 0.0400 104 60-136 5 20 Tetrachloroethane IPCE) 0.0454 0.0050 0.0400 114 73-138 3 20 Toluene 0.0439 0.0050 0.0400 110 72-128 2 20 1,2,3-Trichlorobenzene 0.0520 0.0050 0.0400 130 61-166 3 20 1,2.4-Trichlorobenzene 0.0512 0.0050 0.0400 128 71-158 2 20 1,1,1-Trichloroethane 0.0432 0-0050 0.0400 108 71-135 2 20 1,1,2-Trichloroethane 0.0448 0.0050 0.0400 112 64-132 8 20 Trichloroethene (TCE) 0.0448 0.0050 0.0400 112 74-139 1 20 Ti ichlorotluoromethane 0.0430 0.0050 0.0400 107 30-156 0.1 20 1,2.3-Trichloropropane 0.0463 09050 0.0400 116 67-123 3 20 1,2.4-Trimethylbenzene 0.0459 0.0050 0.0400 115 68-134 1 20 1,3,5-Trimethyl benzene 0.0465 0.0050 0.0400 116 71-140 0.9 20 Vinyl chloride 0.0338 0.0050 0.0400 84 43-144 3 20 Xylenes (total) 0.139 0.0050 0.120 116 69-138 4 20 Surrogate: Dibiotuglhtoromethcruc 0.0519 0.0500 104 74-122 Surrogate: Toluene-dh' 0.0510 0.0500 102 65-128 S'urrogale:4-Bromolluorohen_ene 0.0530 0.0500 106 75-121 Duplicate (B1F0146-DUPI) Source: 2103474-01 Analyzed: 06/04/21 15:22 IShcH S Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromcthane ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromoform ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 u-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0 00.50 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND O.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropanc ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibromomcthane ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: cIlent.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 66T�N Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlF0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate (B1F0146-DUPI) Source: 2103474-01 Analyzed: 06/04/21 15:22 IS1OHS 13-Dichlorobenzene ND 0.0050 mgtkg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromcthanc ND 0.0050 ND 20 CCHI LI-Dichloroethane NI) 0.0050 ND 20 1.2-Dichloroethane ND 0.0050 ND 20 I,l-Dichloroethene NJ) 0.0050 ND 20 cis-L2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 13-Dicliloropropaoe ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1,1-Dichloropropene ND 0.0050 ND 20 cis-L3-Dichloropropene ND 0.0050 ND 20 trans-0-Dichloropropene ND 0.0050 ND 20 Ethvlbenzene NI) 0.0050 NI) 20 Hexachlorobuladiene ND 0.0050 NI) 20 4-Isopropyl Toluene NI) 0.0050 NI) 20 Isopropylhenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1,1,1,2-Tetrachlorocthane NI) 0.0050 ND 20 1,1,2,2-Tetrachlorocthanc ND 0.0050 ND 20 Tetrachloroethene IPCE) ND 0.0050 ND 20 TOILICnc ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1 .24-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane NI) 0.0050 ND 20 Trichloroethane (TCE) ND 0.0050 ND 20 Trichlorofluoromethane ND 0.0050 ND 20 1,2,3-Trichloropropane NI) 0.0050 ND 20 1,2A-Trimethylbenzene ND 0.0050 NI) 20 1,3,5-Trimethylbenzene ND 0.00.50 NI) 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibrotnq/litorotitethttttt, 0.0538 0-0498 108 74-122 Surrogate: Tduene-dS 0.0509 0.0498 102 65-128 Surrogate:4-Bromo/luotnben�ene 0.0506 0.0498 102 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 Sample Method Summary Fnalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAPNELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OF,C, CA-ELAPNELAP STLC Metals by ICP 601013 STLC Chromium STLC/EPA 6010E Solid OEC, Internal STLC Metals Extraction STLC Metals Extraction STLC Water OEC, Internal Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, Internal Total Metals by ICP 601013 Total Antimony EPA 6010E Solid OEC. CA-ELAP,NELAP 6010E Total Arsenic EPA 601013 Solid OEC, CA-ELAPNELAP 6010B Total Barium EPA 6010B Solid OEC, CA-ELAPNELAP 6010B Total Beryllium EPA 601013 Solid OEC, CA-ELAPNELAP 601013 Total Cadmium EPA 6010B Solid OEC, CA-ELAPNELAP 601013 Total Chromium EPA 6010E Solid OEC, CA-ELAPNELAP 601013 Total Cobalt EPA 6010E Solid OEC, CA-ELAPNELAP 001013 Total Copper EPA 601013 Solid OEC, CA-ELAPNELAP 601013 Total Lead EPA 601013 Solid OEC, CA-ELAPNELAP 601013"I'otal Molybdenum EPA 601013 Solid OEC, CA-ELAP.NF.LAP 601013 Total Nickel EPA 6010E Solid OEC, CA-LLAP,NELAP 601013 Total Selenium EPA 6010E Solid OEC, CA-ELAP,NELAP 6010E Total Silver EPA 6010B Solid OEC, CA-ELAP.NELAP 601013 Total Thallium EPA 6010B Solid OEC. CA-FLAPNELAP 6010E Total Vanadium EPA 6010B Solid OEC. CA-ELAPNELAP 6010E Total Zinc EPA 601013 Solid OEC, CA-ELAPNELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA-ELAPNELAP 8260B Full List EPA 8200B Solid OEC, Internal Volatile Organic TPH by GC/FID 8015'IP1-1-6asoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: +.805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: NHC SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 NotesDefinitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference CCFI-I The CCV for this analyte failed high. Results for this analyte may be biased high. CCHI The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. ISIowS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above 1 Ox STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below statc,Iederal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 32 C A OOM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: N14C SLO, 2640 Broad Street 2103479 Orcutt CA, 93457 Project Manager: Clarence Reynolds 06/09/2021 16:44 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. CA-ELAP 2438, TN102666 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 32 a x U 0 r x a (Ij E-E Ln Ti O O Ga X 4-) O (3) rl U LO O Z3 QO f O i / Cn r-I �l N z t~ a w / N Ln N O Ll � Cu W O O x N I U � a Ln l- h U M n o CiUO (N-1-1 a) Sa 4-) F N cm0.Q 0 a)rl p J, �A �l a) H `Zi (0 -ri l4 r-I a) is P 4-) 04 I a) trU) 6 m (0 C=40F4HCo X > 0 Lq 0 O 0 Iq 0 0 0 0 0 of 0 0 of 0 00 0 0 ro 0 0 O rr O LO Lfi O CO O O O Cf) 0 Lq v O - O • O Cl) O O M O N O O N IO I� 0 O C7 o 0 0 0 o o 0 0 o O 0 O o 0 N + 0 N + N + N + + N + + fU o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O l0 '7 M N O O O O O y N 000 N COO Lo V M N E H Q LL O LL 2 0 q W • H d' PQ � I O FG Ga CD x O q 0 -1 J- ) N a) O t5 Q U O a' � ZT N C h � N 04 ¢ O a) N r iI / O 04 H LO o q.. O W N I x rn a ��� x h U M O • • P4 .. .. .. .. .. .. .. a) � J-) = a) c (1 0 �4-0 a)zw r O(1)E 5:� 1�5 .4J �4 ;� v 1-I Z 00 ro-� �,� CD n ao -1 a) of U) V) •r-i Q, U rd -rl -ri N G.+Or.0> � O O O O O O o O O O O O O O O O O 0 O O O 0 O 0 0 O O O 0 O o O O O 0 o O O O O O O O O O O O O co LO 0n On co Cop LO � � M M N N - 0 iC) io M 0 i N O O (V O O O O Lq O O O O -- O LO 0 O - O 0 O U� W O I O W - O O r- Lo O ' n O (O O O co O to Lo LO O O O O O co 0 O M O N O 0 N 0 O O O 0 O 0 0 37 x U 0 Q x a � H to 0 0 x 4-) o Iv .-I U N a' to O is O H / U] rl � N z r z a / 31 Ln a M ';T H •• � Q rl Lu / r-I � P7 W O O x N I U cl, Q to I` �-i ;T hU(n / C7 0 -1 vUN U U o N r +I � N rl ro 0-0 0 � z a J-) P ro-H u-i U S-I a 1) 04 U rl �vtsmu�ro •ri � U C, ro •ri -rl Ci404 HCn}.> N a) N a) N 0 N N O O 00. (O to V m N O O N e- O co O O 0 O O O 00 0 0 0 0 0 0 0 � (fl to a M N � 0 0 0 0 0 0 0 0 O 0 0 M 0 co 0 0 co 0 r 0 0 i 0 co 0 0 to O m ui O O to O to v to I)+ o v 0 to ri 0 O M O N O O fV O f U� O 0 0 0 0 E F ►3 X C] W • H Ln LQ � I G a w O C] 0 N a) IT O T) Q0 U o rG � ZS N ti~ h � N 04 04 N Ol �4 -H / N O. --I r� 0 H Ln G U) �l • • O / N N O G G' W N I LO x rn� w ���w x hU,—I LO U fYi N .-I r-I .. .. .. .. .. .. .. a) �1 z(a0� u-0 a)zw FZ 0 a) E~ C ;� l) F4 �l a) H Zi (0 -,-1 i4 H (1)�4a4-)0,U-1 —Aa)I1wsUnro -'1 04 U r- (d •ri -rl Ga0FCHU) � Q O o O o 0 0 0 0 o O 0 0 0 o O 0 a) o O O O o 0 0 0 0 O O o o O o 0 c CD o O� O 0 0 0 o O O CD CD0 N 0 O 0 O O 000 Q n co COO Ln LO V V M M N Nry 0 M O i o _M 0 N i O i O I O O O O Cn O O O O O 0) O O O O 00 O O OD O U[ O ti CO O O O Cn Cn O 0 U) C. LO O O V 0 ri O O M Cl LO N O 0 N O CA 0 0 0 0 0 0 0 NIN 9 C Lh N LO X R LL ti N (� S. o 0 � CLIOLU tl s cd m N f O m c x m 3 � F m „ c � E E E N o F- O m O F W "= N o PI{ S �-- M PexIOS1O Idol ,971AISQMOO ai R m m ai m G G O Vice I V"08 A 83d I lsed .. . A1ilmn1O81 : O o OORS SOOAS a WSWBOWO°J-dHl y 0 Z L h ° m c " epUlnS . I OPIURAC) SAIJOeea 1 CD E z N w islllin.1809ze 0 U N Vl L L ❑ sleteW - LZ still a v� t:i C Q r1 _ o J ro M m m p Q 'a i v > o r m CL cmi V U N a f =a N m v ma N ¢ N 411 C 00 m ►= h d C oo � 0 Z:N U L e r d U U oo c J3 •10 E c CI � 61 ro QI m❑ � •pp aE o ", Z U — h CD L a N � OQ O a E •—gyp � c . ON a N Ed 0�3 13 N ii p- ru 'Q m u !. p M f+ 7 Q\ C i C N 10 N \ t CO o V L � C as G O c 'e�j ii. A. O Do U V too U Q vy ❑❑ m m m L m dl 0 N b Q C o O F O O~ r• —� 1-3 N a 3 y c m E W o— E o R A c c c a We c a U F m s °' cii V �; Q U 6i z 0 U z J Q Q W I1 C4 S. \ $ Q I` e ) _ E \ $ § } \ a ° z CL \ \ \ \ } C11 t U k � E 2 � \ / 0 k } cck k k a)0 ) f < m { ) c & - I % $ \ ) ƒ } 0 Eca / ƒ i\M 0 U) § ƒ « # v 0 A t ] U G 0 G 3 § k k k k � E top m ? £ _ ) 0j ! o 7 2 m o ± s 2 = « = Q a f Cc2 k\ o ` £ 2 a \ ° k ^ ] ( a 3 & 3 / « c # 0000w 0 0 0 0 0/ F ccC _ k � S)\ kk �GL CD ) ƒ t § _ [ \ e ) ® 2 *_ / ko� E 2 E _ m E t D § \ 7 LL 0 ] / \ o # o � ) $ 7 7] I a 2 k± \ j < \ ) k J J J CD w d U 61 d1l Cl) O W. j J oc0 � o ON -1 a j O U Q' � O n t a (D c E U N O R a E y 0 F- U 1 0 1 Z TQ i U R, co C u7 N uj cu LL c rAO A ro 7 h b � a E pJ E E R C m b y u U c .O. E mu2 0 '� x sPlloS M PeAIoSIO MO.L 141nlscwoD m m « is « m O A G Me I VMS 8Dd / lsed ti /4111QepuB1 on Q a1 OOZZO sDOAS Q ° W9WOOWC3V dHl xy z L = J £ ° " ePU1nS I oplusAo GAtlOaea ° 1 co 4 1s1l tlnd 809Z8 J o d N ♦a co A L c Z ❑ sleleW - ZZ 01111 CL.��aQ x o a❑ d) cu m ;, ;, �`' c o ro m m m $ b•.a. C U u sr = a01 x m MID E : j: m y L W oo ❑ •� Q :�. 4 g. N a- £ E Ch N ~ ~ ❑ ❑ to lC \y 2:'."1 — 1 N 4 m a O O y c_ .0« N.:H « « b.•. �. « o 0 7 c Z V U 0 G❑ to E::: f L Y C C, G'. ° N E b •.,v, N c d CL o a k N ai uo tO GI E ..+ Q, c o, p ❑❑ m m m L Ql a m a m a m W N 'O ai C CL S y i .0 c G O >✓ a Q w o L F° i o Q L m (� > Q > cr 7 CT N E` E U E E m c c c d w W U 6 Z O r V Z 0 M C) V. O 1 Q Z U X Oo 0 In N CS) LO cc - N lica N c „ m d rn N E E E0. ro m m C J d u c 1= 1- 1= i7 • [7 E E m QJI.., N In U o 0 N SPlIOS M POAIOSIO Mol ANAISOLOO m m m m m m C 0 G zoos V Ms 8Od 1 iaad .� y i A3lIIgS31u81 0 o OORS SOOAS WS308OW0'J dNl xy 0 z � rnaPU1nS " [E. j; io I SPIUVAD aAgOaaa E i in ayi Z u 1911 IIOd 808z8 J Z . L. m - U 0 Q sIS3s1V - zZ aRll c 0 o E❑$- ;� m ti ro m m `' $ � 0 � m > > C C m V U N d N V CL x°a 00 iW N Q. 4 00 ❑❑ .= vI c ' ai m g ON al 1 F E E❑ Cl, U o 00 ro c ❑ 1 z :r m 0 m > r m': ci 1 K °° E a a)G U m m❑ N Z U (D p 6 r g c6 �` o m $ cc u y u C: 0 'O Y E to N ° o m u U c a c o U) {ar C ON C O A C CD i C E C p O y 4 ` CQ C OS s. - O O6 G 0 y 1 (>3 pr 0. DD U U -i w In N O y ❑❑ m m m y 01 m m m N$ n E i� '90 CL E n S C m Q O s F F O Q I- m a c Q N� a c d EO U r%) U F„@ cx w U, U E I- i= cc a Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102742 Pacific Petroleum California P. O. Box 2646 Report Date: May 06, 2021 17:25 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 05, 2021 08:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page I of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA. 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by: Lab ID : 2102742-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mg/kg 1 B1E0098 05'05121 12:11 E.PA7471A Total Metals by ICP Antimony ND 2.5 mglkg 1 Bl E0102 05/06/21 13:33 EPA 6010B Arsenic 7.8 2.0 Barium 120 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 44 0.50 Cobalt 18 0.50 Copper 36 0.99 Lead 16 0.50 Molybdenum ND 0.50 Nickel 71 0.50 Selenium ND 2.0 Silver ND 0.50 " Thallium ND 0.99 Vanadium 43 2.0 " Zinc 68 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 1.9 4.4 mglkg 1 BIE0095 05/0.5/21 12:06 EPA 8015M 0-04 Surrogate: 4-Bromofluorobenccne I O9 '%11 (39 -Liz) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 490 10 mgIg 1 B1 E0062 05/05/21 19:52 EPA 8015M TPH Motor Oil (('23-C40) ND 50 11 " " " Srarrogate: o-7egphenYl 89 % (65 - 136) 11" " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 ReportAnalytical Sample ID: NW Corner Sampled: 05/04/21 14:30 Matrix: Solid Sampled by : Lab ID : 2102742-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.3 mg/kg 1000 B 1 F,0101 05/05/21 16:56 EPA 826013 4-Isopropyl Toluene ND 1.3 Isopropylbenzene ND 1.3 Methylene chloride ND 1.3 " Naphthalene ND 1.3 n-Propylbenzene ND 1.3 Styrene ND 1.3 1. 1. 1,2-Tetrachloroethane ND 1.3 1.1,2.2-Tetrachloroethane ND 1.3 Tctrachlorocthcnc (1'CE) ND 1.3 Toluene ND 1.3 1,2,3-Trichlorobenzcne ND 1.3 1,2,4-Trichlorobenzene ND 1.3 1, 1, 1 -Trichloroethane ND 1.3 1,1,2-Trichloroethane ND 1.3 Trichloroethene (TCE) ND 1.3 Trichlorofluoromethane ND 1.3 1,2.3-Tricliloropropane ND 1.3 " 1,2,4-Trimethylbenzene ND 1.3 " 1.3,5-Trimethylbenzene ND 1.3 Vinyl chloride ND 1.3 Xylenes (total) ND 1.3 " Surrogate: Dibromolzuoromethmtc 95 %1 ( 74- 122) " Surrogate: Toluene-a'S 95 Yo (65 - 128 ) Surrogate: 4-BromnJhuoroben-ene 90 ye, ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: W5) 925-3376 Page 5 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : NE Corner Sampled: 05/04/21 14:35 Matrix: Solid Sampled by : Lab ID : 2102742-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 Bl E0101 05/05/21 17:24 EPA 8260B Brontobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromoform ND 1.2 " Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzene ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 12-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoetliane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 " 13-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 " Dichlorodilluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 " cis-1,2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis- 1.3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 " Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 WiV Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by: Lab ID : 2102742-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B 1 E0098 05/05/21 12:15 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B1 E0102 05/06/21 13:46 EPA 601 OB Arsenic 4.5 1.9 Barium 200 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 310 0.47 N-02, N-03 Cobalt 55 0.47 Copper 45 0.93 Lead 9.5 0.47 " Molvbdenum 0.68 0.47 Nickel 430 0.47 " " " " " N-02 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 70 1.9 "Zinc 69 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 7.8 5.0 urg/kg 1 B IE0095 05,05121 12:58 EPA 8015M D-04 Surrogate: 4-Bromo/luorohenzene 101 '% (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 220 10 mg/kg 1 BIE0062 05/05/21 21:51 EPA 8015M TPH Motor Oil (C23-('40) ND 50 " " " " " Surrogate: o-Te/phenYl 84 %, (65 - 136) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 WK Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID : SW Corner Sampled: 05/04/21 14:40 Matrix: Solid Sampled by : Lab ID : 2102742-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Net Volatile Organic Compounds by GC/MS (Continued) R-07 flex achlorobutadiene ND 1.2 mg/kg 1000 Bl E0101 05/05/21 17:51 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 " 7'ctrachlorocthene (PCE) ND 1.2 Toluene ND 1.2 12,3-Trichlorobenzenc ND 1.2 " 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 12,4-77iniethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate. Dihroutgfluoroneetltatee 93,111, ( 74 - 122 ) 11 Surrogate. Toluene-dS 94 (65 - 12S) Surrogate: 4-Bronup lnorohelt:vne 88 °ib (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: SE Corner Sampled: 05/04/21 14:45 Matrix: Solid Sampled by: Lab ID : 2102742-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B1 E0101 05/05/21 18:18 FPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzene ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 14-Dichlorobenzene ND 1.2 Dichloroditluoromethane ND 1.2 1,1-Dichloroethane ND 12 1,2-Dichloroethatte ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 vans-1,2-Dichloroethene ND 1.2 " I.2-Dichloropropane ND 1.2 " 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1,3-Dichloropropcnc ND 1.2 trans-1,3-Dichloropropcnc ND 1.2 Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report for Samples Sample ID: Center Sampled : 05/04/21 14:50 Matrix: Solid Sampled by : Lab ID : 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.086 mgfkg 1 B1 F.0098 05/05/21 12:19 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B l E0102 05/06/21 13:52 EPA 601 OB Arsenic 7.0 1.9 Barium 140 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 72 0.48 Cobalt 22 0.48 Copper 78 0.96 Lead 15 0.48 " Molybdenum 0.99 0.48 " Nickel 160 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium 1.3 0.96 Vanadium 62 1.9 Zinc 80 1.9 N-02 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 7.7 4.8 mg/kg I BIE0095 05/05/21 13:49 EPA 8015M D-04 Surrogate. 4-Bromofhrorobenacne 106 o (39 - 157) 11 11" Semi -Volatile Organic TPH by GC/FID TPH Diesel(C13-C22) 350 10 mg/kg I BIE0062 05/05/21 22:38 EPA8015M TPH Motor Oil (C23-C40) ND 50 " Surrogate: o-TerphenYl 86 % (65 - 136) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analytical Report Sample ID : Center Sampled: 05/04/21 14:50 Matrix: Solid Sampled by: Lab ID : 2102742-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg,ncg 1000 B I E010I 05/05/21 18:46 EPA 8260E 4-Isopropyl Toluene ND 1.2 " Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcnc (PCE) ND 1.2 Tolucnc ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 " 1,2.3-Trichloropropane ND 1.2 " 12.4-Trimethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate. Dibromglluoromethane 94 (74-122) " Surrogate: Toluene-dS 95 Yo (65 - 12S) Surrogate. 4-8ronmfluorohen_ene RR % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: i8051 925-3376 Page 17 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Blank (B1E0102-BLK1) Analyzed: 05/06/21 13:12 Antimony ND 2.5 mg/kg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 Molybdenum ND 0.50 " Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 " Vanadium ND 2.0 " Zinc ND 2.0 LCS (B1E0102-BS1) Analyzed: 05/06/21 12:50 Antimony 99.2 2.5 mg%kg 100 99 80-120 Arsenic 99.8 2.0 100 100 80-120 Barium 102 1.0 100 102 80-120 Beryllium 96.5 0.50 100 96 80-120 Cadmium 101 0.25 100 101 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 102 0.50 100 102 80-120 Copper 103 1.0 100 103 80-120 Lcad 103 0.50 100 103 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium 97.7 2.0 100 98 80-120 Silver 4.81 0.50 5.00 96 80-120 Thallium 104 1.0 100 104 80-120 Vanadium 98.6 2.0 100 99 80-120 Zinc 101 2.0 100 101 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Total Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Matrix Spike (B1E0102-MSI) Source: 2102717-02 Analyzed: 05/06/21 12:55 Antimony 26.4 2.5 mg/kg 99.2 ND 27 10-116 Arsenic 105 2.0 99.2 8.39 98 77-121 Barium 193 0.99 99.2 97.2 97 30-169 Beryllium 93.6 0.50 99.2 0.691 94 86-I11 Cadmium 93.6 0.25 99.2 ND 94 81-112 Chromium 118 0.50 99.2 16.2 103 75-129 Cobalt 102 0.50 99.2 8.09 94 71-121 Copper 119 0.99 99.2 19.7 100 68-135 Lead 105 0.50 99.2 11.8 94 72-121 Molybdenum 89.4 0.50 99.2 1.59 89 70-112 Nickel 114 0.50 99.2 19.7 95 73-121 Selenium 89.8 2.0 99.2 ND 91 76-116 Silver 4.31 0.50 4.96 ND 87 54-132 Thallium 89.0 0.99 99.2 ND 90 64-120 Vanadium 130 2.0 99.2 32.7 98 78-124 Zinc 158 2.0 99.2 64.4 94 50-143 Matrix Spike Dup (B1E0102-MSD1) Source: 2102717-02 Analyzed: 05/06/21 12:57 Antimony 29.7 2.4 mg/kg 94.4 ND 31 10-116 12 20 Arsenic 103 1.9 94.4 8.39 101 77-121 2 20 Barium 182 0.94 94.4 97.2 89 30-169 6 20 Beryllium 91.6 0.47 94.4 0.691 96 86-111 2 20 Cadmium 91.5 0.24 94.4 ND 97 81-112 2 20 Chromium 113 0.47 94.4 16.2 103 75-129 4 20 Cobalt 99.2 0.47 94.4 8.09 96 71-121 3 20 Copper 114 0.94 94.4 19.7 100 68-135 4 20 Lead 102 0.47 94.4 11.8 96 72-121 3 20 Molybdenum 88.9 0.47 94.4 1.58 92 70-112 0.6 20 Nickel 111 0.47 94.4 19.7 96 73-121 3 20 Selenium 88.7 1.9 94.4 ND 94 76-116 1 20 Silver 4.23 0.47 4.72 ND 90 54-132 2 20 Thallium 87.0 0.94 94.4 ND 92 64-120 2 20 Vanadium 120 1.9 94.4 32.7 98 78-124 4 20 Zinc 153 1.9 94.4 64.4 94 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile1 - Quality Control Analyze Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlEO095 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/05/21 06:24 Blank (BIE0095-BLK1) Analyzed: 05/05/21 09:00 TPH Gasoline (C5-Cl2) ND 0.50 mg/kg Surrogate:4-Bromgfluorohenzene 0.134 0.124 108 39-157 LCS (B1E0095-BSI) Analyzed: 05/05/21 08:09 TPH Gasoline (C5-C12) 0.917 0.50 mg/kg 0.992 92 68-139 Surrogate:4-Bromolluoroben_ene 0.158 110.124 127 39-157 LCS Dup (BIE0095-BSD1) Analyzed: 05/05/21 08:34 TPH Gasoline (C5-C12) 1.03 0.50 mg/kg 0.994 103 68-139 11 20 Surrogate:4-Bromofluorohenzene 0.157 0.124 127 39-157 Duplicate (B1E0095-DUPI) Source: 2102652-01 Analyzed: 05/05/21 09:59 TPH Gasoline (('5-C12) ND 5.2 mg/kg ND 20 Surrogate:4-Bromofluorohenzene 1.30 " 1.30 100 39-157 Matrix Spike (B1E0095-MS1) Source: 2102652-01 Analyzed: 05/05/21 14:41 TPH Gasoline (C5-C12) 7.97 4.9 mg/kg 9.80 ND 81 10-171 Surrogate:4-Bromgfhtoroben:enc 1.40 111.23 115 39-157 Matrix Spike Dup (B1E0095-MSD1) Source: 2102652-01 Analyzed: 05/05/21 15:07 TPH Gasoline (C5-02) 8.18 5.2 mg/kg 10.4 ND 78 10-171 3 20 Surrogate:4-Brrnnofluorohenzene 7.40 " 1.30 107 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0101- EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (BI E0101-BLK1) Analyzed: 05/05/21 13:17 Benzene ND 0.25 mgikg Bromobenzene NI) 0.25 BromochIoromethane ND 0.25 " Bromodichloromethane ND 0.25 " Bromofomi ND 0.25 Bromomethane NI) 0.25 " n-Butylbenzene ND 0.25 sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 Carbon tetrachloride NI) 0.25 Chlorobenzene ND 0.25 " Chloroethane NI) 0.25 Chloroform ND 0.25 " Chloromethane ND 0.25 " 2-Chlorotoluene ND 0.25 4-Chlorotoluene ND 0.25 " Dibromochloromethane ND 0.25 1,2-Dibromo-3-chloropropane ND 0.25 " 12-Dibronioethane (EDB) ND 0.25 Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0.25 1.3-Dichlorobenzene ND 0.25 " 1,4-Dicllorobenzene NI) 0.25 " Dichloroditluoromcthanc ND 0.25 1,1-Dichloroethene NI) 0.25 L2-Dichlorocthane ND 0.25 l,l-Dichloroethene ND 0.25 " cis-1,2-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 1.2-Dichloropropane ND 0.25 1,3-Dichloropropane NI) 0.25 2.2-Dichloropropane NI) 0.25 " 1, 1 -Dichloropropene ND 0.25 cis-1.3-Dichloropropene ND 0.25 " trans-l.3-Dichloropropene ND 0.25 " Ethylbcnzene NI) 0.25 " I►exachlorobutadiene NI) 0.25 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 Methylene chloride NI) 0.25 " Naphthalene ND 0.25 " n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0101- EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS (BIE0101-BSI) Analyzed: 05/05/21 12:22 1,3-Dichlorobenzene 2.17 0.25 mglkg 1.99 109 76-138 1,4-Dichlorobenzene 2.14 0.25 1.99 108 72-132 Dichlorodifluoromcthane 1.31 0.25 1.99 66 10-155 1, 1 -Dichloroethane 2.33 0.25 1.99 117 63-139 1.2-Dichlorocthanc 2.06 0.25 1.99 104 64-126 1, 1 -Dichloroethene 2.77 0.25 1.99 139 52-167 cis-1 2-Dichloroethene 2.07 0.25 1.99 104 70-135 trans-1,2-Dichloroethene 2.43 0.25 1.99 122 67-147 1.2-Dichloropropane 2.05 0.25 1.99 103 68-131 1,3-Dichloropropane 2.04 0.25 1.99 103 64-128 2,2-Dichloropropane 2.31 0.25 1.99 116 63-154 1,1-Dichloropropene 2.22 0.25 1.99 112 68-138 cis- 1,3-Dichloropropene 2.09 0.25 1.99 105 72-134 trans-1,3-Dichloropropene 2.26 0.25 1.99 114 69-132 Ethylbenzene 2.46 0.25 1.99 124 68-136 1lexachlorobutadiene 2.20 0.25 1.99 Ill 72-198 4-Isopropyl Toluene 2.39 0.25 1.99 120 74-150 Isopropylbenzene 2.41 0.25 1.99 121 71-149 Methylene chloride 2.57 0.25 1.99 129 51-127 Naphthalene 1.99 0.25 1.99 100 57-158 n-Propylbenzene 2.27 0.25 1.99 114 70-143 Styrene 2.25 0.25 1.99 113 68-138 1, 1, 1,2-Tetrachloroethane 1.92 0.25 1.99 97 76-130 1,1,2,2=1'etrachlorocthane 2.09 0.25 1.99 105 60-136 Telrachloroelhene(PCE) 2.09 0.25 1.99 105 73-138 Toluene 2.19 0.25 1.99 110 72-129 L2,3-Trichlorobenzene 1.74 0.25 1.99 88 61-166 1.2,4-Trichlorobenzene 1.85 0.25 1.99 93 71-158 1, 1, 1 -Trichloroethane 2.24 0.25 1.99 113 71-135 1,1,2-Trichloroethane 2.07 0.25 1.99 104 64-132 Trichloroethene (TCE) 1.92 0.25 1.99 97 74-139 Trichlorofluoromethane 1.74 0.25 1.99 87 30-156 1,2,3-Trichloropropane 2.01 0.25 1.99 1 W 67-123 L2.=4-Trimethylbenzene 2.52 0.25 1.99 127 08-134 1.3,5-Trimethylbenzene 2.37 0.25 1.99 119 71-140 Vinyl chloride 2.46 0.25 1.99 124 43-144 Xylenes (total) 7.54 0.25 5.96 126 69-138 Surrogate: DibronuoJluorome>the1ne, 0.0485 0.0497 98 74-122 Surrogate: Tbheene-d8 0.0471 0.0497 9.5 65-128 Surrogate:4-BromoJluoroben::ene 0.0467 0.0497 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. QNI-08 California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSD1) Analyzed: 05/05/21 12:49 Styrene 2.26 0.25 mg/kg 1.99 114 68-138 0.4 20 1,1,1,2-Tetrachloroethane 1.96 0.25 1.99 99 76-130 2 20 1,1,2,2-I'ctracliloroethane 2.09 0.25 1.99 105 60-136 0.2 20 Tetraehloroethene (PCE) 2.07 0.25 1.99 104 73-138 1 20 TOIne11C 2.21 0.25 " 1.99 111 72-128 1 20 1,2,3-Trichlorobenzene 1.87 0.25 1.99 94 61-166 7 20 1,2,4-Trielilorobenzene 1.89 0.25 1.99 95 71-158 2 20 1,1,1-Trichloroethane 2.17 0.25 1.99 109 71-135 3 20 1,1,2-Trichloroethane 2.16 0.25 1.99 108 64-132 4 20 Trichloroethene (TCE) 1.89 0.25 1.99 95 74-139 1 20 Trichlorofluoronnethane 1.58 0.25 1.99 79 30-156 10 20 1,23-Trichloropropane 1.90 0.25 1.99 95 67-123 6 20 1,2,4-Trimethylbenzene 2.60 0.25 1.99 131 68-134 3 20 1,3,5-Trimethylbenzene 2.38 0.25 1.99 120 71-140 0.6 20 Vinyl chloride 2.27 0.25 1.99 114 43-144 8 20 Xylenes (total) 7.47 0.25 5.96 125 69-138 0.9 20 Surrogate: Dibromofluoromethane 0.0486 0.0497 98 74-122 Surrogate: Toluene-d8 0.0467 0.0497 94 65-128 Surrogate:4-Bromofluorohen_ene 0.0459 0.0497 92 75-121 Duplicate (B1E0101-DUPI) Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 Benzene ND 1.3 mg/kg ND 20 Bromobenzene ND 1.3 ND 20 Bromochloromcthane ND 1.3 ND 20 Bromodichloromethane ND 1.3 ND 20 Bromoform ND 1.3 ND 20 Bromomethane ND 1.3 ND 20 n-Butylbenzene ND 1.3 ND 20 sec-Butylbenzene ND 1.3 ND 20 tert-Butylbenzene ND 1.3 ND 20 Carbon tetrachloride NJ) 1.3 ND 20 Chlorobenzene NI) 1.3 ND 20 Chloroethane ND 1.3 ND 20 Chloroform ND 1.3 ND 20 Chloromethane ND 1.3 ND 20 2-Chlorotoluene ND 1.3 NI) 20 4-Chlorotoluene ND 1.3 ND 20 Dibromochloromethane ND 1.3 ND 20 1,2-Dibromo-3-chloropropane ND 1.3 ND 20 1,2-Dibromoethane (EDB) ND 1.3 ND 20 Dibromomethane ND 1.3 ND 20 1,2-Dichlorobenzene NI) 1.3 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 29 of37 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Volatile Organic Compounds by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlE0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MSl) Source: 2102742-02 Analyzed: 05/05/21 20:08 Benzene 11.1 1.3 ing/kg 10.0 ND 111 37-145 Bromobenzene 9.57 1.3 10.0 ND 96 29-147 Bromochloromcthanc 9.29 1.3 10.0 ND 93 40-145 Bromodichloromethane 10.2 1.3 10.0 ND 102 39-153 Bromoform 9.14 1.3 10.0 ND 91 32-143 Bromomethane 12.1 1.3 10.0 ND 121 10-141 n-Butylbenzene 12.3 1.3 10.0 ND 123 10-162 sec-Butylbenzene 12.5 1.3 10.0 ND 125 14-168 tert-Butylbenzene 11.8 1.3 10.0 ND Its 21-159 Carbon tetrachloride 10.4 1.3 10.0 ND 104 28-148 Chlorobenzene 10.6 1.3 10.0 ND 106 32-148 Chloroethane 11.0 1.3 10.0 ND Ito 11-166 Chloroform 10.3 1.3 10.0 ND 103 40-139 Chloromethane 9.86 1.3 10.0 ND 98 18-135 2-Chlorotoluene 10.7 1.3 10.0 ND 107 25-151 4-Chlorotoluene 10.7 1.3 10.0 ND 106 22-150 Dibromochloromethane 9.53 1.3 10.0 ND 95 40-147 1,2-Dibronio-3-ch1oropropane 9.97 1.3 10.0 ND 100 25-158 1,2-Dibromoethane (EDB) 9.29 1.3 10.0 ND 93 38-147 Dibromomethane 7.54 1.3 10.0 ND 75 39-150 1,2-Dichlorobenzene 10.6 1.3 10.0 ND 106 24-154 1,3-Dichlorobenzene 10.9 1.3 10.0 ND 108 21-153 IA-Dichlorobenzene 10.6 1.3 10.0 ND 106 21-146 Dichlorodifluoromethane 5.88 1.3 10.0 ND 59 10-149 1,1-Dichloroethane 11.2 1.3 10.0 ND 112 34-151 1,2-Dichlorocthanc 10.1 1.3 10.0 ND 100 40-137 LI-Dichloroethene 11.8 1.3 10.0 ND its 21-172 cis-1.2-Di chloroethene 9.65 1.3 10.0 ND 96 38-147 trans- l,2-Dichloroethene 11.3 1.3 10.0 ND 112 30-160 12-Dichloropropane 10.4 1.3 10.0 ND 104 39-146 1,3-Dichloropropane 10.2 1.3 10.0 ND 102 39-141 2,2-Dichloropropane 9.32 1.3 10.0 ND 93 26-149 1, 1 -Dichloropropene 10.7 1.3 10.0 ND 106 28-150 cis-1,3-Dichloropropene 9.97 1.3 10.0 ND 100 34-149 trans-1,3-Dichloropropene 10.7 1.3 10.0 ND 107 36-143 Elhylbenzene 11.5 1.3 10.0 ND 115 23-150 Ilexachlorobutadiene 11.1 1.3 10.0 ND 111 10-192 4-Isopropyl Toluene 11.7 1.3 10.0 ND 117 11-165 Isopropylbenzene 11.2 1.3 10.0 ND 112 17-166 Methylene chloride 12.0 1.3 10.0 ND 120 28-135 Naphthalene 12.0 1.3 10.0 ND 120 10-174 n-Propylbenzene 11.3 1.3 10.0 ND 113 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 37 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102742 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/06/2021 17:25 Sample Method Summary analysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC, CA-ELAP Total Metals by ICP 601 OB Total Antimony EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Arsenic EPA 6010B Solid OEC, CA -FLAP 6010B Total Barium EPA 60I013 Solid OEC, CA-ELAP 6010E Total Beryllium EPA 6010B Solid OEC. CA-ELAP 6010B Total Cadmium EPA 601013 Solid OEC, CA-ELAP 601013 Total Chromium EPA 601 OB Solid OEC, CA-ELAP 6010E Total Cobalt EPA 601OB Solid OEC, CA-ELAP 601 OB Total Copper EPA 6010B Solid OEC_ CA-ELAP 601013 Total Lead EPA 601 OB Solid OEC, CA-EI.AP 601 OB Total Molybdenum EPA 601 OB Solid OEC, CA-ELAP 60108 Total Nickel EPA 6010B Solid OEC. CA-ELAP 60108 total Selenium EPA 6010B Solid OEC, CA-ELAP 601013 Total Siher EPA 601013 Solid OEC. CA-ELAP 601013 Total Thallium EPA 601OB Solid OEC, CA-ELAP 6010B Total Vanadium EPA 6010B Solid OEC. CA-ELAI' 601 OB Total Zinc EPA 6010E Solid OEC, CA-EL.AP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPII-Gasoline 8015 'ITH-Gasoline 8015 TPI I-Gasol ine Solid OEC. CA-ELAP EPA 8015M Solid OEC, Internal EPA 8015M Solid OEC, CA-ELAP EPA 80I5M Solid OEC. Internal EPA 8015M Solid OEC, CA-ELAP EPA 8015M Solid OF.C, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.corn FAX: 805 925-3376 Page 33 of 37 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0511.D Operator BNT Acquired 5 May 2021 12:06 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-01@ Misc Info : 1@B1E0095 GRO SO Vial Number: 11 Response_ 85000I 80000 75000 70000 65000 60000 55000 50000 45000 40000 1 1 GOME0511.D\FID1A Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0513.D Operator BNT Acquired 5 May 2021 12:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-03@ Misc Info : 1@B1E0095 GRO SO Vial Number: 13 Response 95000, 90000 85000` E 45000 40000 i 30000+ 25000 20000 15000 10000 GOME0513.D\FID1A 5000: Time 0.00 1.00 2.60 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.0 10 3.00 14.00 File C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0515.D Operator BNT Acquired 5 May 2021 1:49 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102742-05@ Misc Info : 1@B1E0095 GRO SO Vial Number: 15 Response_ 850001 75000 70000 65000 60000 55000; i 50000 45000 40000 35000 30000 25000 20000 15000 i 10000 5000I Time 0.00 1.00 2.00 GOME0515.D\FID1A it 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 _ 5 O O O SSS O Cl) O W U � Cl) Q O � M LL 0 Y � M LO �j W Lo 2 O 6 m 0 M CM m H N U � M ,-I a { N [� ri O 1 ,L M N � o � i M U G] t3l N M U� M Ln N O W o X W O N N co O l0 / (M O r O Lr) N ri ui rn e) O O N N / O N N N 7+ OLn ';T ` N N r-I r- y. % in Ln C7 O M • • '� I r-I CJ C N l ai Lf) N r-I M O r. (d O 4 S4 'd q) Z 4-4 O N E r. 75n n n n n n o 0 0 0 0 0 0 0 0 a.J (ll H ,7 N 0 O O O O O O O O O O O O O CD O O O O O O -a �� t N + N + 0) + + N N + O N O O O O O O O O O O O U r-1 O O O O O O O O O N H a)J d LO v m N 000 On (00 LLO OV m N E_ -rl Qa U (", f0 -ri -r-I N 2 U d 0 LL O co Cl) Ln 0 w 0 m � rn U iA 0 x a H 23 0 l� N o CS' U Ca � -rl rb U) M Ln O W 04 O Ln N [Q rl lfl / O -I O O N O p� Ln CJ O N / O O - N I N N >+ >r Ln 'i' N / Cn C7 O • • ',� Ln rl vU 00 >C R O (N 1-1 M +) N cro0� �4 zs (1) z 44 O-1 H S4 � N +Z N O N N 14 :1 +-) 0, C) 0 rl N O" tl) b Lo •ri 04 U G r0 •ri -ri N Ga 0 rG cn 1. I-- f` n r- O O o O 0 o O O 0 0 0 0 O O O 0 o O o 0 0 0 0 + + + + + O o 0 o O o 0 0 0 N N N N O o O O o O o O O Cl) N O O O O O O O O O O co n to U) It M N 0 _0 ri O O N O (O N O V N O N N I O 0 N l OR 1V E F- O U / LL. O 1 Z zt O Ul) CV Lo 0 ii LL ~ c tV 4 p aaV E E E E t 0 V = 9PIIOS PeA109101e101 ai Gi m f4lAlSOLoO a io 0 G O Q Z9091 V"Oe a 80d I ised V o� ltlp9 mu81 en sr e Q � U x_ a OOLZB sOOAS C4 L �° N WSW8OW00 dHl z n = .a ". 0 CL E o ePUlnS IePlueRO enPOeea ai W w c d v M C N y isll lln� 809ZB o z i w U a�i sleieW - ZZ enu a rn U O d t� o j a m w m d b 7 4 U C R it a' m . - A i a (/) CI N < �+ N ❑❑ = m g: h�� F ❑ ry;.2 H H z y 33 �o 0 0 0❑8' vi LL C. z V a e • +��tt ❑ x 3 R C� cc o U ' o m m M T' N t 04 o �3 a , o y a P r o d E @ R tn L C C p 0 a 0 s. d m at t W a 0 y ❑❑ m m m � u�Ci m.o.. E i m a - - - ai 0 U I- z J g U w a CO 91, a 1:/ f�- o. R N C (D EL L UUU E O U a) c 0 U� a� N N N x c c c c c Y >Y Y Y Y co O W coO N O N O) 'a N 0) '6 N 0 N O N m a)N O) O) N m N O O v 2 L- lL LL. a:lL LL lL LL i LL 0 .Q oQ Q a a Q a) n O w 0 m O v) O N O c m> m> m> m> m> (7 J U J U' J C9 J C9 J .2 O O O 0 E 0 N O O O O O O U , N N V N V Nr N HC-II J�1-50020— m Hc<-� M o 0 0 0 0 0 0 0 Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102508 Pacific Petroleum California P. O. Box 2646 Report Date: May 03, 2021 16:36 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 23, 2021 13:40 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Shahnaz Parvin, Project Manager sparvin@oecusa.com California ELAP Certification # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 922-4772 www.oecusa.com FAX: (805) 925-3376 Page 1 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Bin 2094-A 2102508-01 Solid Solid 04/23/2021 11:00 04/23/2021 13:40 Bin 2094-B 2102508-02 Solid Solid 04/23/2021 11:05 04/23/2021 13:40 Bin 2094-C 2102508-03 Solid Solid 04/23/2021 11:10 04/23/2021 13:40 Bin 20340-A 2102508-04 Solid Solid 04/23/2021 11:15 04/23/2021 13:40 Bin 20340-B 2102508-05 Solid Solid 04/23/2021 11:20 04/23/2021 13:40 Bin 20340-C 2102508-06 Solid Solid 04/23/2021 11:25 04/23/2021 13:40 Bin 20158-A 2102508-07 Solid Solid 04/23/2021 11:30 04/23/2021 13:40 Bin 20158-B 2102508-08 Solid Solid 04/23/2021 11:35 04/23/2021 13:40 Bin 20158-C 2102508-09 Solid Solid 04/23/2021 11:40 04/23/2021 13:40 Bin 2088-A 2102508-10 Solid Solid 04/23/2021 11:45 04/23/2021 13:40 Bin 2088-B 2102508-11 Solid Solid 04/23/2021 11:50 04/23/2021 13:40 Bin 2088-C 2102508-12 Solid Solid 04/23/2021 11:55 04/23/2021 13:40 Bin 20376-A 2102508-13 Solid Solid 04/23/2021 12:00 04/23/2021 13:40 Bin 20376-B 2102508-14 Solid Solid 04/23/2021 12:05 04/23/2021 13:40 Bin 20376-C 2102508-15 Solid Solid 04/23/2021 12:10 04/23/2021 13:40 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 94 AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analysis Batch ID Preparation Date/Time *** DEFAULT GENERAL METHOD *** Asbestos Bulk PLM-(non-soil& Asphalt)(sub) OEC Admin Services Chromatograms Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List BID0766 04/27/2021 07:10 STLC Metals by ICP 601 OB STLC 131 D0916 04/30,12021 10:33 STLC Metals Extraction STLC Metals Extraction BID0838 04/28/2021 12:44 TCLP Metals by ICP 601 OB TCLP B 1 D0919 04/30/2021 10:49 TCLP Metals Extraction TCLP Metals Extraction B I D0839 04/28/2021 12:48 Total Metals by CVAA Mercury Total EPA 7471 A B ID0711 04/26/2021 09:00 Total Metals by ICP 601 OB Total B 1 D0734 04/26/2021 07:37 Volatile Organic Compounds by GUMS 8260B Full List BID0650 04/23/2021 12:11 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B I D0692 04/23/2021 14:16 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 8054 925-3376 Page 3 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Alercury 0.095 0.094 mg/kg I B 1 D0711 04/26/21 14:53 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I D0734 04/261/21 13:51 EPA 601 OB Arsenic 7.4 1.9 Barium 690 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 64 0.48 Cobalt 14 0.48 Copper 260 0.97 Lead 2400 0.49 N-02 N-02 N-01, N-03 Molvbdenum 2.0 0.48 Nickel 94 0.48 " Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 31 1.9 "Zinc 1300 1.9 STLC Metals by ICP Chromium 0.28 0.10 mg/L 2 B 1 D0916 05/03/21 12:58 STLC/FPA 601 OB Copper 1.6 11 0.10 " " " " TCLP Metals by ICP Lead 2.0 0.050 mg/L 1 BID0919 05/03/21 14:09 EPA 1311 /EPA 601 OB The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID: 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND Surrogate: 4-Bromo/laoroben:ene Semi -Volatile Organic TPH by GC/FID 4.9 mglkg 1 B 1 D0692 04/23/21 14:32 EPA 8015M R-07 94/ (39-157) 11 " 11 TPH Diesel (C 3-C.22) ND 10 TPH Motor Oil (C 23-C40) 97 50 Surrogate: o-Terphenyl 84 "/„ mg/kg 1 BID0766 04/27/2115:24 EPA8015M (65-136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by : Lab ID : 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.051 mg/kg 1 BID0650 04/23/21 17:17 EPA 8260B Bromobenzene ND 0.051 Bromochloromethane ND 0.051 Bromodichloromethane ND 0.051 Bromoform ND 0.051 Bromomethane ND 0.051 " n-Butylbenzene ND 0.051 sec-Butylbenzene ND 0.051 tort-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobcnzene ND 0.051 Chlorocthane ND 0.051 Chloroform ND 0.051 Chloromethane ND 0.051 2-Chlorotoluene ND 0.051 4-Chlorotoluene ND 0.051 Dibromochloromethane ND 0.051 1,2-Dibronio-3-chloropropane ND 0.051 1.2-Dibrontoethane (EDB) ND 0.051 Dibromomethane ND 0.051 1,2-Dichlorobenzene ND 0.051 " I.3-Dichlorobenzene ND 0.051 1,4-Dichlorobenzene ND 0.051 Dichloroditluoromethane ND 0.051 1, 1 -Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 LI-Dichloroethene ND 0.051 cis-1,2-Dichloroethene ND 0.051 trans-1,2-Dichloroethene ND 0.051 1,2-Dichloropropane ND 0.051 " 13-Dichloropropane ND 0.051 2,2-Dichloropropane ND 0.051 1, 1 -Dichloropropene ND 0.051 cis-l3-Dichloropropane ND 0.051 trans- l,3-Dichloropropane ND 0.051 Ethylbenzene ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-A Sampled: 04/23/21 11:00 Matrix: Solid Sampled by: Lab ID : 2102508-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.051 mg/kg 4-Isopropyl Toluene ND 0.051 Isopropylbenzene ND 0.051 Methylene chloride ND 0.051 " Naphthalene ND 0.051 n-Propylbenzene ND 0.051 " Styrene ND 0.051 1,1,1,2-Tetrachloroethane ND 0.051 " 1.1.2,2-Tetrachloroethane ND 0.051 " "Tctrachloroethane (PCE) ND 0.051 " Toluene ND 0.051 1,2,3-Trichlorobenzene ND 0.051 " 1,2,4-Trichlorobenzene ND 0.051 1, 1, 1 -Trichloroethane ND 0.051 " 1,1,2-Trichloroetliane ND 0.051 " Trichloroethene (WE) ND 0.051 " Trichlorolluoromethane ND 0.051 " 1.2.3-Trichloropropane ND 0.051 " 1,2,4-1-rinrethylbenzene ND 0.051 " 1,3,5-Triniethylbenzene ND 0.051 Vinyl chloride ND 0.051 " Xylencs(total) ND 0.051 " Surrogate: Dihrwnullvoevuuctheroe 98 `; , ( 74 - 122 ) Surrogate: Toluene-d8 95 % (65 - 128 ) Surrogate: 4-Broniolluorobenzene 89 � ( 75 - 121) B1D0650 04/23/21 17:17 EPA8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Total Metals by CVAA Mercury ND 0.093 mg/kg 1 B1D0711 04/26/21 15:02 EPA 7471A Total Metals by ICP Antimony ND 2.4 mgtkg 1 BID0734 04/26/2113:54 EPA 6010B Arsenic 7.6 1.9 Barium 220 097 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 100 0.48 N-02, N-03 Cobalt 15 0.48 Copper 61 0.97 Lead 320 0.48 " " " " " N-02 N-03 Molvbdenum 1.6 0.48 Nickel 130 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 38 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium 0.29 0.10 nigiL 2 BID0916 05/03/21 13:00 S'rLC/EPA601013 Lead 20 0.10 N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BID0919 05/03/2114:26 EPA 1311/EPA6010B Lead 0.31 0.050 " " " " 1. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.8 mg/kg 1 BID0692 04/23/21 14:58 EPA 8015M R-07 Surrogate: 4-Bromu/luorohen:ene 99 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel W13-C22) 16 10 mg/kg 1 BID0766 04/27/21 15:24 EPA 8015M D-06 TPH Motor Oil (C23-C40) 150 50 11 11 11" 11 Surrogate: o-Teiphenrl 80 Y" (65 - 136 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 I Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by: Lab ID: 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.049 mg/kg I BID0650 04/23/21 17:45 BPA8260B Bromobenzene ND 0.049 Bromochloromethane ND 0.049 Bromodichloromethane ND 0.049 Bromoform ND 0.049 " Bromomethane ND 0.049 " n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 " Carbon tetrachloride ND 0.049 Chlorobenzenc ND 0.049 Chlorocthanc ND 0.049 Chloroform ND 0.049 Chloromethane ND 0.049 2-Chlorotohiene ND 0.049 4-Chlorotoluene ND 0.049 Dibromochloromethane ND 0.049 " 1,2-Dibromo-3-chloropropane ND 0.049 I.2-Dibromoethane (EDB) ND 0.049 Dibromomethane ND 0.049 1,2-1)ichlorobenzene ND 0.049 1,3-Dichlorobcnzcnc ND 0.049 " 1,4-Dichlorobcn7cnc ND 0.049 Dichloroditluoromethane ND 0.049 1, 1 -Dichloroethane ND 0.049 1,2-Dichloroethane ND 0.049 1,1-Dichloroethene ND (1.049 " cis-1,2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 " 1,2-Dichloropropane ND 0.049 1,3-Dichloropropane ND 0.049 2,2-Dichloropropane ND 0.049 1, 1 -Dichloropropene ND 0.049 cis-1,3-Dichloropropene ND 0.049 trans-1,3-Dichloropropene ND 0.049 Etylbenzene ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 94 r A i A L! MMS!! Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-B Sampled: 04/23/21 11:05 Matrix: Solid Sampled by : Lab ID : 2102508-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 llexachlorobutadiene ND 0.049 mg/kg 1 BID0650 04/23/21 17:45 EPA 8260B 4-Isopropyl Toluene ND 0.049 Isopropylbenzene ND 0.049 Methylene chloride ND 0.049 " Naphthalene ND 0.049 n-Propylbenzene ND 0.049 Styrene ND 0.049 1,1,1,2-Tetrachloroethane ND 0.049 1,1,2,2-Tetrachloroetliane ND 0.049 Tctrachlorocthcnc (PCE) ND 0.049 Toluene ND 0.049 1,23-Trichlorobenzene ND 0.049 1,24-Trichlorobenzene ND 0.049 " 1, 1, 1 -Trichloroethane ND 0.049 1,1,2-Trichloroethane ND 0.049 Trichloroethene (TCE) ND 0.049 Trichlorofluoromethane ND 0.049 " 1,23-Trichloropropane ND 0.049 " 1,2,4-Trimethylbenzene ND 0.049 " 13.5-Trimethylbenzene ND 0.049 Vinyl chloride ND 0.049 Xylenes (total) ND 0.049 Surrogate: Dibromolluoromethane 95 ° ; ( 74 - 122 ) Surrogate: Toluene-d8 96'X, (65- 128 ) Surrogate. 4-Brouno1luorohen_ene 90 IN ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of 94 6M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.17 0.098 mg/kg I B1D0711 04/26/21 15:04 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1 D0734 04/26/21 14:05 EPA 6010B Arsenic 7.7 2.0 Barium 280 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 52 0.50 N-02 Cobalt 10 0.50 Copper 79 1.0 Lead 270 0.50 " " " " " N-02 N-03 Nlolybdenum 1.1 0.50 Nickel 69 0.50 " Selenium ND 2.0 Silvcr ND 0.50 " Thallium ND 1.0 Vanadium 34 2.0 "Zinc 370 2.0 STLC Metals by ICP Chromium 0.24 0-10 mg/L 2 B 1 D0916 05/03/21 13:03 STLC/EPA 6010B Lead 22 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.11 0.050 mg/L 1 B 1 D0919 05/03/21 14:29 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 12 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH (tasoline (C5-C12) ND Surrogate: 4-Bromofluorohen_ene Semi -Volatile Organic TPH by GC/FID 4.8 ing/kg 1 BID0692 04/23/2115:24 EPA8015M R-07 93'% (39-157) TPH Diesel (C13-C22) ND 10 TPH Motor Oil (C23-C40) 220 50 Surrogate: o-Terphep•1 79 % mg/kg 1 B 1 D0766 04/27/21 15:47 EPA 8015M (65-136) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled : 04/23/21 11:10 Matrix: Solid Sampled by: Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.049 mg/kg 1 B1 D0650 04/23/21 18:12 EPA 8260B Bromobenzene ND 0.049 Bromochloromethane ND 0.049 Bromodichloromethane ND 0.049 Bromofonn ND 0.049 Bromomethane ND 0.049 " n-Butylbenzene ND 0.049 sec-Butylbenzene ND 0.049 tert-Butylbenzene ND 0.049 Carbon tetrachloride ND 0.049 Chlorobenzene ND 0.049 Chlorocthanc ND 0.049 Chloroform ND 0.049 " Chloromethane ND 0.049 2-Chlorotoluene ND 0.049 4-Chlorotoluene ND 0.049 Dibromochloromethanc ND 0.049 1,2-Dibronro-3-chloropropane Ni) 0.049 1,2-Dibromoethane (FDB) ND 0.049 Dibromomethane ND 0.049 1.2-Dichlorobenzene ND 0.049 1,3-Dichloroben7ene ND 0.049 1,4-Dichlorobcn7cnc ND 0.049 Dichloroditluoromcthane ND 0.049 I,1-Dichloroethane ND 0.049 1,2-Dichloroethane ND 0.049 I,1-Dichloroethene ND 0.049 cis-L2-Dichloroethene ND 0.049 trans-1,2-Dichloroethene ND 0.049 1,2-Dichloropropane ND 0.049 13-Dichloropropane ND 0.049 2,2-Dichloropropane ND 0.049 I,l-Dichloropropene ND 0.049 cis-1,3-Dichloropropene ND 0.049 trans-1,3-Dichloropropene ND 0.049 Ethylbenzcnc ND 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2094-C Sampled: 04/23/21 11:10 Matrix: Solid Sampled by : Lab ID : 2102508-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 0.049 mg/kg 1 BID0650 04/23/21 18:12 EPA9260B 4-Isopropyl Toluene ND 0.049 Isopropylbenzene ND 0.049 Methylene chloride ND 0.049 Naphthalene ND 0.049 n-Propylbenzene ND 0.049 Styrene ND 0.049 1,1,1,2-Tetrachloroethane ND 0.049 1,1,2,2-Tetrachloroethane ND 0.049 Tctrachlorocthenc (PCE) ND 0.049 Toluene ND 0.049 1,2,3-Trichlorobenzene ND 0.049 1,2,4-Trichlorobenzene ND 0.049 1,1,1-Trichloroethane ND 0.049 1,1,2-Trichloroethane ND 0.049 Trichloroethene (TCE) ND 0.049 Trichlorotluoromethane ND 0.049 " 1,2.3-Trichloropropane ND 0.049 1,2.4-Trimethylbenzene ND 0.049 1,3,5-Trimethylbenzene ND 0.049 Vinyl chloride ND 0.049 Xylenes (total) ND 0.049 Surrogates Dibroinolluorome thane 97 % t 74 • 122 ) Surrogate: Toluene-dg 96 % ( 65 - 128 ) Suriwgate: 4-Brmao/luorolemene 92 4 i ( 75: 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 02508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA MercurN 0.13 0.087 mg1kg 1 B 1 D0711 04/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I B I D0734 04/26/21 14:07 EPA 6010B Arsenic 7.3 2.0 Barium 230 0.98 Beryllium ND 0.49 " Cadmium ND 0.25 Chromium 58 0.49 N-02 Cobalt 12 0.49 Copper 63 0.98 Lead 390 0.49 N-02 N-03 Molvbdenum 2.1 0.49 Nickel 69 0.49 Selenium ND 2.0 " Silver ND 0.49 Thallium ND 0.98 Vanadium 35 2.0 Zinc 530 2.0 STLC Metals by ICP Chromium 0.24 0.10 mg/L 2 B1D0916 05/03/2113:05 STLC/EPA6010B Lead 14 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/I, 1 B 1 D0919 05/03/21 14:31 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID : Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by : Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-(' 12) ND Surrogate: 4-Brom o/l noro hen_ en e Semi -Volatile Organic TPH by GUND 5.2 mg/kg I B1D0692 04/23/21 15:50 EPA8015M R-07 99`i, (39-157) " TPH Diesel (C13-C22) ND 10 TPH Motor Oil (C23-C40) 170 50 Surrogate: o-Teiphenrl 86 %£, uig/kg I B1 D0766 04/27/21 15:47 EPA 8015M (65-136) " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Pnaa 17 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 0.051 mg/kg 1 B I D0650 04/23/21 18:40 EPA 9260B Bromobenzene ND 0.051 Bromochloromethane ND 0.051 Bromodichloromethane ND 0.051 Bromoform ND 0.051 Bromomethane ND 0.051 n-Butylbenzene ND 0.051 sec-Butylbenzene ND 0.051 test-Butylbenzene ND 0.051 Carbon tetrachloride ND 0.051 Chlorobenzene ND 0.051 Chloroethanc ND 0.051 Chlorotornn ND 0.051 Chloromethane ND 0.051 2-Chlorotoluene ND 0.051 4-C'hlorotoluene ND 0.051 Dibromochloromethane ND 0.051 1.2-Dibromo-3-chloropropane ND 0,051 1,2-Dibromoethane (E.DB) ND 0.051 Dibromomethane ND 0.051 1,2-Dichlorobcn7ene ND 0.051 1,3-Dichlorobcnzenc ND 0.051 1,4-Dichlorobcnzenc ND 0.051 Dichlorodilluoromethanc ND 0.051 l,l-Dichloroethane ND 0.051 1,2-Dichloroethane ND 0.051 I,1-Dichloroethene ND 0.051 cis-1,2-Dichloroethene ND 0.051 trans-1,2-Dichloroethene ND 0.051 1,2-Dichloropropane ND 0.051 1.3-Dichloropropane ND 0.051 22-Dichloropropane ND 0.051 1.1-Dichloropropane ND 0.051 cis-1.3-Dichloropropenc ND 0.051 trans-1,3-Dichloropropcnc ND 0.051 I':thylbenzene ND 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 18 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-A Sampled: 04/23/21 11:15 Matrix: Solid Sampled by: Lab ID : 2102508-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.051 mglkg 1 BID0650 04/23/21 18:40 F.PA 8260B 4-Isopropyl Toluene ND 0.051 Isopropylbenzene ND 0.051 " Methylene chloride ND 0.051 Naphthalene ND 0.051 " n-Propylbenzene ND 0.051 " Stvrene ND 0.051 1,1.1,2-Tetrachloroethane ND 0.051 1.1,2,2-Tetrachloroethanc ND 0.051 Tctrachloroethene (PCE) ND 0.051 Toluene ND 0.051 1,2,3-Trichi orobenzenc ND 0.051 1,2,4-Trichlorobenzene ND 0.051 1,1,1-Trichloroelhane ND 0.051 1,1,2-Trichloroethane ND 0051 Trichloroethene (TCE) ND 0.051 Trichlorofluoromethane ND 0.051 1.2,3-Trichloropropane ND 0.051 1,2,4-Trimethylbenzene ND 0.051 " 1,3,5-Trimethylbenzene ND 0.051 Vinyl chloride ND 0.051 Xylencs (total) ND 0.051 " Surrogate: Dibromotluoromethanc 98 "/., ( 74 - 122 ) Surrogate. Toluene-d$ 97 % (65 - 128 ) Surrogate: 4-Broaw/luoroheuccne 92 ( 7-5- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report foi- Samples Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID: 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.095 0.091 mg/kg 1 BID0711 04/26/21 15:08 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1D0734 04/26/21 14:10 EPA 60I OB Arsenic 10 2.0 Barium 240 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 50 0.49 N-02 Cobalt 11 0.49 Copper 54 0.98 Lead 800 0.49 " " " N-02, N-03 Molybdenum 0.77 0.49 Nickel 79 0.49 " Selenium ND 2.0 Silvcr ND 0.49 Thallium ND 0.98 Vanadium 37 2.0 "Zinc 350 2.0 STLC Metals by ICP Chromium 0.29 0.10 mg/L 2 B 1 D0916 05/03/21 13:08 STLC/EPA 6010B Lead 120 U.10 N-07 TCLP Metals by ICP Lead 0.23 0.050 m,/L I B I D0919 05/03/21 14:34 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 20 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-02) ND Surrogate: 4-Bromo/luorohenzene Semi -Volatile Organic TPH by GC/FID 5.0 mg/kg 1 B 1 D0692 04/23/21 16:16 EPA 8015M R-07 99% (39-157) TPH Diesel (C13-C22) 37 10 TPH Motor Oil (C23-C40) 280 50 Surrogate: o-TciphenYl 86 N, mg/kg 1 B 1 D0766 04/27/21 16:09 EPA 8015M (65-136) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. P-06 California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 21 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg/kg 1 B I D0650 04/23/21 19:07 FPA 8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromoforn ND 0.047 Bromotnethane ND 0.047 n-Butylbenzene ND 0.047 " sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzene ND 0.047 C:hlorocthane ND 0.047 Chloroform ND 0.047 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 " 1,2-Dibromo-3-chloropropane ND 0.047 12-Dibromoethane (EDB) ND 0.047 Dibromomethane ND 0.047 12-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 1,4-Dichlorobcwenc ND 0.047 Dichlorodifluoromcthane ND 0.047 1,1-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 cis-1,2-Dichloroethene ND 0,047 trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 13-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1. 1 -Dichloropropene ND 0.047 cis-1.3-Dichloropropcnc ND 0.047 trans-1,3-Dichloropropcnc ND 0.047 Ethylbenzene ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 22 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Report Sample ID: Bin 20340-B Sampled: 04/23/21 11:20 Matrix: Solid Sampled by: Lab ID : 2102508-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.047 mgtkg 1 BID0650 04/23/21 19:07 EPA 8260B 4-Isopropyl Toluene ND 0.047 " " " " " Isopropylbenzene ND 0.047 " Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1, 1, 1,2-Tetrachloroethane ND 0.047 1,1,12-Tetrachloroethane ND 0.047 Tetrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobcnzenc ND 0.047 1,24-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 Trichloroethane (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 1,2.3-Trichloropropane ND 0.047 L2,4-Trimethylbenzene ND 0.047 1,3.5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 Xylencs (total) ND 0.047 Surrogate: Dihromolluoromethane 98 % (74 - 122) 11 Surrogate: Toluene-dS 96 / (65 - 128) 11" Surrogate: 4-Brom0/hiorohcn_ene 91 IN (75 - 121 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 23 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury - ND 0.091 mg/kg 1 Bl D0711 04/26/21 15:10 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1 D0734 04/26/21 14:13 EPA 6010B Arsenic 11 2.0 Barium 340 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 50 0.49 N-02 Cobalt 14 0.49 Copper 230 0.98 Lead 1200 0.49 " " " " " N-01, N-03 Nlolvbdenum 1.7 0.49 Nickel 73 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 32 2.0 " Zinc 1000 2.0 STLC Metals by ICP Chromium 0.32 0.10 mg/L 2 BID0916 05/03'2113:11 STLC/EPA6010B TCLP Metals by ICP Lead 0.84 0.050 mg/L 1 B 1 D0919 05/03/21 14:36 EPA 1311 /FPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 24 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-C Sampled : 04/23/21 11:25 Matrix: Solid Sampled by : Lab ID: 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 5.0 mg!kg 1 BID0692 04/23/21 16:42 EPA 8015M R-07 Surrogate: 4-Bromofhtoroben_ene 96 (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 29 10 ing/kg 1 B1 D0766 04/27/21 16:09 EPA 9015M D-06 TPH Motor Oil (C23-C40) 150 50 11 11 11" 11 Surrogate: o-Kvphenrl 83 % (65 - 136) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples I Sample ID: Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by: Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.050 mg/kg 1 BID0650 04/23/21 19:35 EPA8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 Bromoform ND 0.050 Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tert-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobenzcnc ND 0.050 Chloroethane ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 " 4-Chlorotoluene ND 0.050 " Dibromochloromethane ND 0.050 1,2-Dibromo-3-chloropropane ND 0.050 1,2-Dibromoethane (EDB) ND 0.050 Dibromomethane ND 0.050 12-Dichlorobenzene ND 0.050 1.3-Dichlorobenzene ND 0.050 1,4-Dichlorobenzene ND 0.050 Dichloroditluoromethanc ND 0.050 1,1-Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 LI-Dichloroethene ND 0.050 cis-1,2-Dichloroethene ND 0.050 trans- I .2-Dichloroethene ND 0.050 1,2-Dichloropropane ND 0.050 1.3-Dichloropropane ND 0.050 " 2.2-Dichloropropane ND 0.050 1.1-Dichloropropene ND 0.050 cis-1.3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 " Lthylbenzene ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Pnvn 26 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20340-C Sampled: 04/23/21 11:25 Matrix: Solid Sampled by : Lab ID : 2102508-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 77 Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.050 mgtkg 1 B I D0650 04/23/21 19:35 EPA 8260B 4-Isopropyl Toluene ND 0.050 lsopropylbenzene ND 0.050 Methylene chloride ND 0.050 Naphthalene ND 0.050 n-Propylbenzene ND 0.050 Styrene ND 0.050 1, 1, 1,2-Tetrachloroethane ND 0.050 1.1,2,2-1'etrachloroethane ND 0.050 Tctrachlorocthcne (ICE) ND 0.050 Tolucnc ND 0.050 1,2,3-Trichlorobenzene ND 0.050 1,2,4-Trichlorobenzene ND 0.0510 1,1,1-Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethene (TCE) ND 0.050 " Trichlorotluoromethane ND 0.050 1,2.3-Trichloropropane ND 0.050 1.24-Triniethylbenzene ND 0.050 1,3.5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Dibromoffitoromethane 98 io (74 - 122) " Sin•rogate: Toluene-d8 95 % ( 65 - 128) Surrogate: 4-Brom(!1luoroberr_cene 90 Y. (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 27 094 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical t Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID: 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Nates Total Metals by CVAA Mercury 0.11 0.092 mg/kg 1 B 1 D0711 04/26/21 15:12 EPA 7471 A Total Metals by ICP Antimony 5.9 2.5 mg/kg 1 BID0734 04/26/2114:16 EPA 6010B Arsenic 8.5 2.0 Barium 260 0.98 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 65 0.49 N-02 Cobalt 11 0.49 Copper 77 0.98 Lead 530 0.49 " " " " " N-02 N-03 Molybdenum 1.2 0.49 Nickel 91 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 34 2.0 " Zinc 780 2.0 STLC Metals by ICP Chromium 0.59 0.10 mg/L 2 BID0916 05/03/2113:21 STLC/EPA6010B Lead 17 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.12 0.050 mg/L I B 1 D0919 05/03/21 14:39 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 28 of 94 C A 16-M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) ND Surrogate 4-Bromq/I1orohen_ene Semi -Volatile Organic TPH by GC/FID 5.1 mg/kg I B1D0692 04/23/21 17:08 EPA 8015M R-07 98%, (39-157) TPH Diesel (C13-C22) 38 10 TPH Motor Oil (C23-C40) 150 50 Surrogate o-kiphenrl 86 %, mg/kg 1 B 1 D0766 04/27/21 16:32 EPA 8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 29 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by: Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mg/kg 1 B1D0650 04/23/2120:02 EPA8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 " Bromodichloromethane ND 0.045 Bromofonn ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobcnzene ND 0.045 " Chloroethane ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 " 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 1,2-DibromocIlia ne (EDB) ND 0.045 Dibromomethanc ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichloroben7cnc ND 0.045 1,4-Dichlorobenzcnc ND 0.045 DichlorodiFluoromcthane ND 0.045 1. 1 -Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 l,l-Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1,3-Dichloropropane ND 0.045 2,2-Dichloropropane ND 0.045 1,1-Dichloropropene ND 0.045 " cis-1,3-Dichloropropene ND 0.045 " trans-1,3-Dichloropropene ND 0.045 " Ethylbcnzene ND 0.045 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Pane 30 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples I Sample ID : Bin 20158-A Sampled: 04/23/21 11:30 Matrix: Solid Sampled by : Lab ID : 2102508-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg/kg 1 BID0650 04/23/2120:02 EPA8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene ND 0.045 Styrene NI) 0.045 1.1,1.2-1'ehachloroethane ND 0.045 1.L2,2-Tetrachloroethane ND 0.045 'I'ctrachlorocthcne (PCE) ND 0.045 " Toluene ND 0.045 1,2,3-Triehlorobenzcne ND 0.045 " 1,2,4-Trichlorobenzene ND 0.045 " 1, 1, 1 -Trichloroethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 Trichlorolluoromethane ND 0.045 1,23-Trichloropropane ND 0.045 1,2,4-1'rimethylbenzene ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate. Dibromolluoromrethane 96'' (74- 122) " Surrogate: Tollfene-d8 97 "rb (65. 128 ) Sm•rogute: 4-Bromolluaroben_ene 93 (75- 121 ) The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID: 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Alercur) 0.12 0.090 mg/kg I Bl D0711 04/26/21 15:14 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B 1 D0734 04/26/21 14:19 EPA 60108 Arsenic 6.5 2.0 Barium 270 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 86 0.49 Cobalt 25 0.49 Copper 60 0.99 Lead 190 0.49 Molybdenum 1.0 0.49 Nickel 170 0.49 " Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 35 2.0 "Zinc 380 2.0 STLC Metals by ICP Chromium Lead TCLP Metals by ICP N-02 N-02, N-03 034 0.10 mg/L 2 B 1 D0916 05/03/21 13:23 STLC/EPA 6010B 13 0.10 " " " "11N-07 Lead 0.29 0.050 mg/l, I B 1 D0919 05/03/21 14:41 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 94 aw TAL =3& 6ya Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 5.0 mg/kg 1 B1D0692 04/23/21 17:34 EPA 8015M R-07 Surrogate: 4-Bromn/hmroben_ene 89 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 93 40 mg/kg 4 B1D0766 04/28/21 15:31 EPA 8015M D-06 TPH Motor Oil (C23-C40) 320 200 '. Surrogate: o-Teiphenvd 84 %, (65 - 136) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 94 WA im, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20158-B Sampled : 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mgIg 1 B1D0650 04/23/2120:30 EPA8260B Bromobenzene ND 0.047 " Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromofonn ND 0.047 " Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzene ND 0.047 Chloroethanc ND 0.047 Chlorofonn ND 0.047 Chloromethane ND 0.047 " 2-Chlorotoluene ND 0.047 4-C'hlorololuene ND 0.047 Dibromochloromethane ND 0.047 " 1,2-Dibromo-3-chloropropane ND 0.047 1,2-Dibromoethane (EDB) ND 0.047 Dibromomethane ND 0.047 1,2-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 1,4-Dichlorobenzene ND 0.047 " Dichlorodifluoromethane ND 0.047 1, 1 -Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 i,l-Dichloroethene ND 0.047 cis-1,2-Dichloroethene ND 0.047 trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 11.047 1,3-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 1, 1 -Dichloropropene ND 0.047 cis-1.3-Dichloropropene ND 0.047 trans-1,3-Dichloropropene ND 0.047 Ethylbenzene ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 34 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report foi- Samples Sample ID : Bin 20158-B Sampled: 04/23/21 11:35 Matrix: Solid Sampled by: Lab ID : 2102508-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.047 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1. 1, 1,2-Tetrachloroethane ND 0.047 1.1,2,2=I'etrachloroethane ND 0.047 Tetrachloroethene (PCE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzene ND 0.047 1,2,4-Trichlorobenzene ND 0.047 1,1,1-Trichloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 Triehloroethene (TCE) ND 0.047 TrichloroFluoromethane ND 0.047 1,2,3-Trichloropropane ND 0.047 1,2,4-1'rimethylbenzene ND 0.047 1,3,5-Trimethylbenzene ND 0.047 Vinyl chloride ND 0.047 Xylenes (total) ND 0.047 Surrogate: Dihrangfluoromethane 95 Surrogate: Toluene -A 96 Surrogate. 4-Br0n11)/luorohencene 87 mg/kg I BID0650 04/23/2120:30 EPA8260B ( 74 - 122) (65-128) (75-121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.aecusaXorn FAX: (805) 925-3376 Page 35 of94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mgtkg 1 B 1 D0711 04/26/21 15:16 EPA 7471 A Total Metals by ICP Antimony 38 2.5 mg/kg 1 B 1 D0734 04/26/21 14:22 EPA 6010B Arsenic 13 2.0 Barium 610 0.99 Beryllium ND 0.49 Cadmium ND 0.25 Chromium 63 0.49 Cobalt 19 0.49 Copper 78 0.99 Lead 8000 49 100 04/26/2114:50 Molybdenum 1.8 0.49 1 04/26/21 14:22 Nickel 110 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 Vanadium 39 2.0 Zinc 2100 2.0 " STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 B 1 D0916 05/03/21 13:26 STLC/EPA 6010B TCLP Metals by ICP Lead 0.054 0.050 mg/L I BID0919 05/03/21 14:44 EPA 1311/EPA6010B N-02 N-01, N-03 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 36 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 I Analytical Report for Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND Surrogate•4-Bromn/luurohen_ene Semi -Volatile Organic TPH by GC/FID 5.0 mg/kg 1 BID0692 04/23/21 18:00 EPA 8015M R-07 97% (39-157) 11 11" TPH Diesel (03-C22) 39 10 TPH Motor Oil (C23-C40) 110 50 Sttrrogutc: o-Teiphemd 75 Yo mglkg 1 BID0766 04/27/2116:32 EPA8015M (65-136) 11° 11 D-06 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Pnav 27nf9d Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 0.052 mgikg 1 BID0650 04/23/21 23:41 EPA 8260B Bromobenzene ND 0.052 Bromochloromethane ND 0.052 Brotnodichloromethane ND 0.052 " Brorroform ND 0.052 " Bromomethane ND 0.052 " n-Butylbenzene ND 0.052 " sec-Butylbenzene ND 0.052 " tert-Butylbenzene ND 0.052 " Carbon tetrachloride ND 0.052 " Chlorobcnzcnc ND 0.052 " Chlorocthanc ND 0.052 " Chloroform ND 0.052 Chloromethane ND 0.052 2-Chlorotoluene ND 0.052 " 4-Clilorotoluene ND 0.052 " Dibromochloromethane ND 0.052 " 1,2-Dibromo-3-chloropropane ND 0.052 " 1,2-Dibrontoethane (EDB) ND 0.052 " Dibromomethane ND 0.052 " 1,2-Dichlorobenzene ND 0.052 1.3-Dichlorobenzene ND 0.052 " 14-Dichlorobenzene ND 0.052 Dichlorodifluoromcthanc ND 0.052 " 1,1-Dichloroethene ND 0.052 1,2-Dichloroethane ND 0.052 1,1-Dichloroethene ND 0.052 " cis-1,2-Dichloroethene ND 0.052 " trans-1,2-Dichloroethene ND 0.052 " 1,2-Dichloropropane ND 0.052 " 1,3-Dich1oropropane ND 0.052 2,2-Dichloropropane ND 0.052 1, 1 -Dichloropropene ND 0.052 cis-L3-Dichloropropene ND 0.052 " trans-1,3-Dichloropropene ND 0.052 Ethylbcnzcne ND 0.052 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 r Page 38 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20158-C Sampled: 04/23/21 11:40 Matrix: Solid Sampled by: Lab ID : 2102508-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS (Continued) R-07 Hexachlorobutadiene ND 0.052 mg/kg I B I D0650 04/23/21 23:41 EPA 8260B 4-Isopropyl Toluene ND 0.052 Isopropylbenzene ND 0.052 " Methylene chloride ND 0.052 Naphthalene ND 0.052 n-Propylbenzene ND 0.052 Styrene ND 0.052 1.1,1,2-Tetrachloroethane ND 0.052 1.1,2,2-1'etrachloroethane ND 0.052 Tctrachlorocthcnc(PCE) ND 0.052 Toluene ND 0.052 1,2,3-Trichlorobenzene ND 0.052 1,2.4-Trichlorobenzene ND 0.052 1,1,1-Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 Trichloroethene (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 1.2,3-Trichloropropane ND 0.052 1,2,4-Trimethylbenzene ND 0.052 1,3,5-Trimethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylencs (total) ND 0.052 Surrogate: Dibromolluoromethanc 97'N (74- 122) " Surrogate: Toluene-d8 97 `,'o (65 - 128) " Surrogate: 4-Bromq/luo oben_ene 91 %, (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entiret} California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.19 0.088 mg/kg 1 BID0711 04/20/21 15:18 EPA 747]A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I D0734 04/26/21 14:25 EPA 6010B Arsenic 9.0 2.0 Barium 380 1.0 Beryllium ND 0.50 Cadmium 1.3 0.25 Chromium 44 0.50 " Cobalt 13 0.50 Copper 36 1.0 Lead 360 0.50 Molvbdenum 0.73 0.50 Nickel 71 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 35 2.0 Zinc 780 2.0 N-02, N-03 STLC Metals by ICP Lead 12 0.10 mg/L 2 B1D0916 05/03/2113:28 STLC/EPA6010B N-07 TCLP Metals by ICP Lead 0.092 0.050 mg/L I B1D0919 05/03/2114:46 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 40 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report t Sample ID : Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID : 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPII Gasoline (C5-C 12) ND 4.6 mgtkg 1 B1D0692 04/23/21 18:26 EPA 8015M R-07 Surrogate: 4-Bromgfluoroben:ene 98 % (39 - 157) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (03-C22) 21 10 mg/kg 1 BID0766 04/27/21 16:54 EPA 8015M D-06 TPII Motor Oil (C23-C40) 140 50 11 11" Surrogate: o-kiphenrl 80 % (65 - 136 ) 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 41 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID : 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.052 mg/kg 1 B 1 D0650 04/24/21 00:08 EPA 8260B Bromobenzene ND 0.052 " Brontochloromethane ND 0.052 " Bromodichloromethane ND 0.052 Bromofonn ND 0.052 Bromomethane ND 0.052 n-Butylbenzene ND 0.052 sec-Butylbenzene ND 0.052 tert-Butylbenzene ND 0.052 Carbon tetrachloride ND 0.052 Chlorobenzenc ND 0.052 Chloroethane ND 0.052 Chloroform ND 0.052 Chloromethane ND 0.052 2-Chlorotoluene ND 0.052 4-Chlorotoluene ND 0.052 " Dibromochloromethane ND 0.052 1,2-Dibromo-3-chloropropane ND 0.052 " 1,2-Dibronioethane (EDB) ND 0.052 Dibromomethane ND 0.052 1,2-Dichlorobenzene ND 0.052 " 1,3-Dichlorobenzene ND 0.052 1,4-Dichlorobenzene ND 0.052 Dichlorodifluoromethane ND 0.052 l,l-Dichloroethane ND 0.052 1,2-Dichloroethane ND 0.052 1, 1 -Dichloroethene ND 0.052 cis-1.2-Dichloroethene ND 0.052 trans-1,2-Dichloroethene ND 0.052 12-Dichloropropane ND 0.052 1,3-Dichloropropane ND 0.052 2.2-Dichloropropane ND 0.052 1, 1 -Dichloropropene ND 0.052 cis-1.3-Dichloropropene ND 0.052 " trans- l,3-Dichloropropene ND 0.052 Ethyl benzene ND 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl1ent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805)_925-3376 Page 42 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-A Sampled: 04/23/21 11:45 Matrix: Solid Sampled by: Lab ID: 2102508-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.052 mglkg 1 BID0650 04/24/2100:08 EPA8260B 4-Isopropyl Toluene ND 0.052 Isopropylbenzene ND 0.052 Methylene chloride ND 0.052 Naphthalene ND 0.052 n-Propylbenzene ND 0.052 Styrene ND 0.052 1, 1, 1,2-Tetrachloroethane ND 0.052 1,1,2,2-1'etrachloroethane ND 0.052 Torachloroethenc (PCE) ND 0.052 Toluene ND 0.052 1,2,3-Trichlorobenzene ND 0.052 1,2.4-Trichlorobenzene ND 0.052 1, 1, 1 -Trichloroethane ND 0.052 1,1,2-Trichloroethane ND 0.052 Trichloroethene (TCE) ND 0.052 Trichlorofluoromethane ND 0.052 1,2,3-Trichloropropane ND 0.052 1,2,4-Triniethylbenzene ND 0.052 1,3,5-Trimethylbenzene ND 0.052 Vinyl chloride ND 0.052 Xylenes (total) ND 0.052 Surrogate: Dibromolhroromethane 97 % (74 - 122) " Surrogate: Toluene-dg 96'%, (65 - 125' ) Surrogate: 4-Bronw luorohen_ene 90 Y. (75- 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 43 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA ltlercury 0.11 0.099 mg/kg 1 B1 D0711 04/26/21 15:20 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BID0734 04/26/2114:28 EPA 6010B Arsenic 15 2.0 Barium 270 0.98 Beryllium ND 0.49 Cadmium 1.4 0.25 Chromium 130 0.49 N-02, N-03 Cobalt 16 0.49 " Copper 68 0.98 Lead 440 0.49 N-02, N-03 Molybdenum 1.2 0.49 Nickel 120 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 38 2.0 Zinc 1400 2.0 STLC Metals by ICP Chromium 0.23 0.10 mg/L 2 B1D0916 05/03/21 13:31 STLC/EPA6010B Lead 14 0.10 " " " " N-07 TCLP Metals by ICP Chromium ND 0.050 mg/L 1 BID0919 05/03/21 14:49 EPA 1311/EPA6010B Lead 0.27 0.050 " " " " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.corn FAX: 805 925-3376 Page 44 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.6 mgfkg 1 BID0692 04/23/21 20:35 EPA 8015M R-07 Surrogate: 4-Bromo/laorobenzene 97 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 17 10 mg/kg I B1D0766 04/27/21 16:54 EPA 8015M D-06 TPH Motor Oil (C23-C40) 87 50 " "11" Surrogate: o-Tcthhenl,l 74 'X. (65 - 136) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 45 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mg/kg 1 B1 D0650 04/24/21 00:35 EPA 8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethane ND 0.045 " Broniofonn ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 test-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobcnzcne ND 0.045 Chlorocthanc ND 0.045 Chlorofonn ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochloromethane ND 0.045 " 1,2-Dibromo-3-chloropropane ND 0.045 1,2-Dibromoetliane (EDB) ND 0.045 Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobenzene ND 0.045 14-Dichlorobenzene ND 0.045 Dichloroditluoromethane ND 0.045 1,1-Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 LI-Dichloroethane ND 0.045 cis- 1.2-Dichloroethene ND 0.045 trans-1,2-Dichloroethane ND 0.045 1,2-Dieliloropropane ND 0.045 1,3-Dichloropropane ND 0.045 " 2.2-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis-1,3-Dichloropropane ND 0.045 trans-1,3-Dichloropropanc ND 0.045 Ethylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 46 of 94 r A &7M Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2088-B Sampled: 04/23/21 11:50 Matrix: Solid Sampled by: Lab ID: 2102508-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlombutadiene ND 0.045 mg/kg 1 BID0650 04/24/2100:35 EPA8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene ND 0.045 Styrene ND 0.045 1,1,1,2-Tetrachloroethane ND 0.045 11,2.2-Tetrachloroethane ND 0.045 Tctrachlorocthenc WCE) ND 0.045 Toluene ND 0.045 " 1,23-Trichlorobenzenc ND 0.045 1,14-Trichlorobenzene ND 0.045 1, 1, 1 -Trichloroethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 Trichlorofluoromethane ND 0.045 1,2,3-Tricliloropropane ND 0.045 1,2,4-1'riniethylbenzene ND 0.045 1,3,5=rrimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: DihronwlLmromethane 97 4„ (74 - 122 ) Surrogate: Toluene-(18 95 % ( 65 - 128) " Surrogate: 4-Bromofluorohencene 90 io ( 75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805 925-3376 Page 47 of 94 M A WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by: Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mglkg 1 B1D0711 04/26/21 15:30 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 BI D0734 04/26/21 14:31 EPA 601 OB Arsenic 13 2.0 Barium 300 0.99 Beryllium ND 0.49 Cadmium 19 0.25 Chromium 56 0.49 Cobalt 17 0.49 Copper 1100 0.99 Lead 390 0.49 " Molybdenum 1.1 0.49 Nickel 100 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.99 " Vanadium 34 2.0 Zinc 660 2.0 STLC Metals by ICP N-02 N-02 N-02 N-02, N-03 Cadmium 0.088 0.050 tng/L 2 BID0916 05/03/21 13:34 STI.CtEPA6010B Chromium 0.24 O.10 " " " " " Copper 0.69 0.10 " Lead 10 0.10 " " " " " N-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 48 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by: Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes TCLP Metals by ICP Lead Volatile Organic TPH by GC/FID 0.085 0.050 mg/L 1 B1D0919 05/03/21 14:59 EPA 1311/EPA6010B TPH Gasoline (C5-C12) ND 4.8 mg/kg 1 BID0692 04/23/21 21:01 EPA 8015M R-07 Surrogate: 4-Brom(? luorobenrene 96 % (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 20 10 mg/kg 1 B1D0766 04/27/21 17:17 EPA 8015M D-06 TPH Motor Oil (C23-C40) 130 50 11 11 1, 1111 Surrogate: o-Terpherrvl 78 %, 11 (65 - 136) " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by: Lab ID: 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mgtkg 1 B 1 D0650 04/24121 01:02 EPA 8260B Bromobenzene ND 0.045 Bromocbloromethane ND 0.045 Bromodichloromethane ND 0.045 Bromoform ND 0.045 Bromomethane ND 0.045 n-Butylbenzene ND 0.045 sec-Butylbenzene ND 0.045 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzcnc ND 0.045 Chloroethane ND 0.045 Chloroform ND 0,045 Chlorotnethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 Dibromochlorotnethane ND 0.045 1.2-Dibronto-3-chloropropane ND 0.045 12-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 12-Dichlorobenzene ND 0.045 1.3-Dichlorobenzcnc ND 0.045 1,4-Dichlorobcn7enc ND 0.045 Dichlorodifluoromethane ND 0.045 l,l-Dichloroethane ND 0.045 1,2-Dichloroethane ND 0.045 1, 1 -Dichloroethene ND 0.045 cis-1.2-Dichloroethene ND 0.045 " trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 1,3-Dichloropropame ND 0.045 22-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis- 1,3-Dichloropropene ND 0.045 trans-1,3-Dichloropropene ND 0.045 Ethylbenzcnc ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 50 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Sarnples Sample ID: Bin 2088-C Sampled: 04/23/21 11:55 Matrix: Solid Sampled by : Lab ID : 2102508-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.045 mg/kg I BID0650 04/24/21 01:02 EPA 8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene ND 0.045 Styrene ND 0.045 1.1.1,2-1'etrachloroethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0.045 " 7'etraclilorocthene (PCE) ND 0.045 " Toluene ND 0.045 1,2,3-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1,1,1-Trichloroethane ND 0.045 " 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCE) ND 0.045 Trichlorofluoroniethane ND 0,045 1,2.3-Trichloropropane ND 0,045 1,2,4-Triniethylbenzene ND 0.045 13,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 " Surrogate: DihrumuJhroronrethune 95 '/ ( 74 - 122) Surrogate: Trhtene-d8 981,% (65 - 128) " Surrogate: 4-BramoJluorohen_ene 88 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 for Samples I Analytical Report Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by : Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg1kg 1 B1D0711 04/26/21 15:32 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg 1 Bl D0734 04/26/21 14:41 EPA 6010B Arsenic 7.0 2.0 Barium 360 LO Beryllium ND 0.50 Cadmium ND 0.25 Chromium 48 0.50 Cobalt 10 0.50 Copper 620 1.0 Lead 940 0.50 N-02 N-02, N-03 Dlolvbdenum 1.4 0.50 Nickel 66 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 34 2.0 Zinc 610 2.0 STLC Metals by ICP Copper 2.4 0.10 mg/L 2 BID0916 05/03/2113:36 STLC/EPA6010B Lead 51 0.10 " " " " " N-07 TCLP Metals by ICP Lead 4.7 0.050 mgiL 1 BID0919 05/03/2115:01 EPA 1311/E.PA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805} 925-3378 Page 52 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples I Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by : Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (('5-C12) ND 5.2 mg/kg I B1D0692 04/23/21 21:27 EPA 8015M R-07 Surrogate: 4-Brotn #htorohensene 92 Yo (39 - 157 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 12 10 mg/kg l TPH Motor Oil (C23-C40) 67 50 11" Surrogate: o-Terphemd 73 Y. (65- 136 ) BID0766 04/27/2117:17 EPA8015M D-06 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 53 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report Sample ID : Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 0.050 mg/kg 1 BID0650 04/24/21 01:29 EPA 8260B Bromobenzene ND 0.050 Bromochloromethane ND 0.050 Bromodichloromethane ND 0.050 Bromoform ND 0.050 " Bromomethane ND 0.050 n-Butylbenzene ND 0.050 sec-Butylbenzene ND 0.050 tort-Butylbenzene ND 0.050 Carbon tetrachloride ND 0.050 Chlorobcnzene ND 0.050 Chloroethanc ND 0.050 Chloroform ND 0.050 Chloromethane ND 0.050 2-Chlorotoluene ND 0.050 4-Chlorotoluene ND 0.050 Dibromochloromethane ND 0.050 1,2-Dibromo-3-chloropropane ND 0.050 " 1,2-Dibromoethane (EDB) ND 0.050 Dibromomethane ND 0.050 1.2-Dichlorobenzene ND 0.050 1,3-Dichlorobcnzcnc ND 0.050 1,4-Dichlorobcn7cnc ND 0.050 Dichloroditluoromethane ND 0.050 1, 1 -Dichloroethane ND 0.050 1,2-Dichloroethane ND 0.050 1,1-Dichloroethene ND 0.050 cis-1.2-Dichloroethene ND 0.050 trans-1,2-Dichloroethene ND 0.050 1.2-Dichloropropane ND 0.050 1.3-Dichloropropane ND 0.050 22-Dichloropropane ND 0.050 1.1-Dichloropmpene ND 0.050 cis-1.3-Dichloropropene ND 0.050 trans-1,3-Dichloropropene ND 0.050 Ethylbcnzcnc ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 54 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-A Sampled: 04/23/21 12:00 Matrix: Solid Sampled by: Lab ID : 2102508-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 11exachlorobutadiene ND 0.050 mg!kg 1 BID0650 04/24/21 01:29 EPA 8260B 4-Isopropyl Toluene ND 0.050 Isopropylbenzene ND 0.050 " Methylene chloride ND 0.050 " Naphthalene ND 0.050 " n-Propylbenzene ND 0.050 " Styrene ND 0.050 " 1, 1, 1,2-Tetrachloroethane ND 0.050 1,1.2,2-Tetrachloroethane ND 0.050 " Tctrachlorocthcne (PC E) ND 0.050 Toluene ND 0.050 1,2,3-Trichlorobenzene ND 0.050 1,2A-Trichlorobenzene ND 0.050 1, 1, 1 -Trichloroethane ND 0.050 1,1,2-Trichloroethane ND 0.050 Trichloroethane (TCE) ND 0.050 Trichlorotluoromethane ND 0.050 1,2,3-Trichloropropane ND 0.050 12,4-Trimethylbenzene ND 0.050 1,3,5-Trimethylbenzene ND 0.050 Vinyl chloride ND 0.050 Xylenes (total) ND 0.050 Surrogate: Dibron:ulhior(;methaac 96 % ( 74 - 722 ) Surrogate: Toluene-dR 96 M, (65 - 128 ) Surrogate: 4-Bronwfhtorohen_cne 89 % (75 - 121) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 55 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID : Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID: 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercun 0.20 0.097 mg/kg 1 B 1 D0711 04/26/21 15:34 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mglkg 1 BID0734 04/26/2114:44 EPA6010B Arsenic 6.7 2.0 Barium 440 0.99 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 73 0.50 N-02 Cobalt 9.4 0.50 Copper 57 0.99 Lead 2000 0.50 " " " " " N-01, N-03 Molybdenum 2.5 0.50 Nickel 68 0.50 Selenium ND 2.0 Silvcr NU 0.50 Thallimn ND 0.99 Vanadium 30 2.0 Zinc 770 2.0 " STLC Metals by ICP Chromium 41.23 0.10 mg/l. 2 B1D0916 05/03/21 13:39 STLC/E.PA6010B TCLP Metals by ICP Lead 0.99 0.050 mg/L 1 B I D0919 05/03/21 15:04 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusA.com FAX: 805 925-3376 Page 56 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by : Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND Surrogate: 4-Bromn%l uorohen_ene Semi -Volatile Organic TPH by GC/FID 5.1 mglkg 1 BID0692 04/23/2 1 21:53 EPA8015M R-07 96% (39-157) TPH Diesel (C13-C22) ND 10 TPH Motor Oil (C23-C40) 64 50 Surrogate: o-Teiphenurl 79'% mg/kg 1 B1D0766 04/28/2115:08 EPA8015M (65-136) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 57 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 0.047 mg.!'kg 1 BID0650 04/24/21 01:57 FPA 8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromofonn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzene ND 0.047 Chlorocthanc ND 0.047 Chloroform ND 0A47 Chloromethane ND 0.047 2-Chlorotoluene ND 0.047 4-Chlorotoluene ND 0.047 Dibromochloromelhane ND 0.047 1.2-Dibromo-3-chloropropane ND 0.047 1,2-Dibromoethane (FDB) ND 0.047 Dibromomethane ND 0.047 12-Dichlorobenzene ND 0.047 1,3-Dichlorobenzene ND 0.047 1,4-Dichlorobenzene ND 0.047 Dichloroditluoromcthanc ND 0.047 l,l-Dichloroethane ND 0.047 1,2-Dichloroethane ND 0.047 1,1-Dichloroethene ND 0.047 cis-1.2-Dichloroethene ND 0.047 trans-1,2-Dichloroethene ND 0.047 1,2-Dichloropropane ND 0.047 1,3-Dichloropropane ND 0.047 2,2-Dichloropropane ND 0.047 I,1-Dichloropropene ND 0.047 cis- 1.3-Dichloropropcne ND 0.047 trans-1,3-Dichloropropanc ND 0.047 Fthylbcnzene ND 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 58 of 94 - (.. �i M�� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-B Sampled: 04/23/21 12:05 Matrix: Solid Sampled by: Lab ID : 2102508-14 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 11exachIorobutadiene ND 0.047 mg/kg 1 B1D0650 04/24/21 01:57 EPA 8260B 4-Isopropyl Toluene ND 0.047 Isopropylbenzene ND 0.047 Methylene chloride ND 0.047 Naphthalene ND 0.047 " n-Propylbenzene ND 0.047 Styrene ND 0.047 1, 1, 1,2-Tetrachloroethane ND 0.047 1,1,2,2-Tetrachloroethane ND 0.047 Tetrachlorocthcne (PCE) ND 0.047 Toluene ND 0.047 1,2,3-Trichlorobenzene ND 0.047 1,2,4-Trichlorobenzene ND 0.047 " 1, 1, 1 -Trichloroethane ND 0.047 1.1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromelhane ND 0.047 1,2.3-Trichloropropane NI) 0.047 1,2,4-Trimethylbenzene NI) 0.047 1,3,5-Trimethylbenzene NI) 0.047 Vinyl chloride ND 0.047 Xylencs (total) ND 0.047 Surrogate: Uibromo/luoromethane 97 % (74 - 122 ) Surrogate: Toluene-dS 96 % (65 - 118 ) Surrogate: 4-Bronm/ltuu•oben_cne 91 % (75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 59 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by : Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg kg I B 1 D071 1 04/26/21 15:36 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgikg 1 B1 D0734 04/26/21 14:47 EPA 6010B Arsenic 5.6 1.9 " Barium 320 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 49 0.49 " Cobalt 10 0.48 Copper 41 0.97 Lead 440 0.48 " " " " " N-02 N-0.3 111olvbdenum 0.80 0.49 " Nickel 68 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 38 1.9 Zinc 580 1.9 STLC Metals by ICP Lead 40 0.10 mg/L 2 BID0916 05/03/2113:41 STLC/EPA6010B N-07 TCLP Metals by ICP Lead 0.20 0.050 mg/I. I B I D0919 05/03/21 15:06 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 94 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportAnalytical Sample ID: Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID : 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) ND Surrogate: 4-Bromo/luorohen_ene Semi -Volatile Organic TPH by GC/FID 4.6 mg/kg 1 B 1 D0692 04/23/21 22:18 EPA 8015M R-07 94, (39-157) TPH Diesel (03-C22) 140 20 TPII Motor Oil (C23-C40) 360 100 Surrogate: o-Teiphen.11 120 ', mg/kg 2 B1 D0766 04/28/21 16:38 EPA 8015M (65-136) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. D-06 California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 61 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analytical Report for Samples Sample ID : Bin 20376-C Sampled : 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.047 mg'kg I B 1 D0650 04/24/21 02:24 EPA 8260B Bromobenzene ND 0.047 Bromochloromethane ND 0.047 Bromodichloromethane ND 0.047 Bromofonn ND 0.047 Bromomethane ND 0.047 n-Butylbenzene ND 0.047 sec-Butylbenzene ND 0.047 tert-Butylbenzene ND 0.047 Carbon tetrachloride ND 0.047 Chlorobenzene ND 0.047 Chloroethanc ND 0.047 Chlorotbnn ND 0.047 " Chloromethane ND 0.047 2-Chlorotoluene ND 0-047 4-Chlorotoluene ND 0.047 Dibromochloromethane ND 0.047 1,2-Dibromo-3-chloropropane ND 0.047 1.2-Dibronnethane (EDB) ND 0.047 Dibromomethane ND 0.047 1.2-Dichlorobenzene ND 0.047 13-Dichlorobenzene ND 0.047 1,44)ichlorobenzene ND 0.047 Dichlorodifluoromethane ND 0.047 1,1-Dichloroethane ND 0.047 " 1,2-Dichloroethane ND 0.047 1, 1 -Dichloroethene ND 0.047 cis-L2-Dichloroethene ND 0.047 trans-1,2-Dichloroethene ND 0.047 1.2-Dichloropropane ND 0.047 13-1)ichloropropane ND 0.047 2,24Dichloropropane ND 0.047 1,1-Dichloropropene ND 0.047 cis-1.3-Dichloropropcnc ND 0.047 trans-1,3-Dichloropropcnc ND 0.047 E^'thylbenzene ND 0.047 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 62 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ReportI Analytical t Sample ID : Bin 20376-C Sampled: 04/23/21 12:10 Matrix: Solid Sampled by: Lab ID: 2102508-15 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 0.047 mg/kg 1 B 1 D0650 04/24/21 02:24 EPA 8260B 4-Isopropyl Toluene ND 0.047 lsopropylbenzene ND 0.047 Methylene chloride ND 0,047 Naphthalene ND 0.047 n-Propylbenzene ND 0.047 Styrene ND 0.047 1.1,1,2-Tetrachloroethane ND 0.047 1,1,2,2=Tetrachloroethane ND 0.047 Tctrachlorocthcnc IPCE) ND 0.047 Toluene ND 0.047 1,2.3-Trichlorobenzenc ND 0.047 1,2,4-Trichlorobenzene ND 0.047 1, 1, 1 -Trichloroethane ND 0.047 1,1,2-Trichloroethane ND 0.047 Trichloroethene (TCE) ND 0.047 Trichlorofluoromethane ND 0.047 1,2,3-Trichloropropane ND 0.047 1.2,4-TrimethyIbenzene ND 0.047 1,3.5-TrimethyIbenzene ND 0.047 Vinyl chloride ND 0.047 Xylcnes (total) ND 0.047 Surrogate: Dihromglhrorvnretlronc 95 4, (74 - 122) Surrogate: Toluene-d8 97 % ( 65 - 128 ) Surrogate: 4-Bromo11uorohen_ene 92 % ( 75 - 121) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 63 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total Metals by CVAA - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1D0711 - EPA 7471A Preparation: EPA 7471A Prep 04/26/21 09:00 Blank (BlD0711-BLKI) Analyzed: 04/26/21 14:37 Mercury ND 0.10 mg/kg LCS (BlD0711-BS1) Analyzed: 04/26/21 14:31 Mercury 0.803 0.10 mg/kg 0.833 96 85-115 LCS Dup (BlD0711-BSDI) Analyzed: 04/26/21 14:33 Mercury 0.765 0.10 mg/kg 0.833 92 85-115 5 20 Duplicate (BlD0711-DUPI) Source: 2102489-02 Analyzed: 04/26/21 14:45 Mercury 0.0432 0.099 mg/kg 0.0418 3 20 Matrix Spike (BlD0711-MSI) Source: 2102489-02 Analyzed: 04/26/21 14:47 Mercury 0.943 0.090 mg/kg 0.746 0.0418 107 75-125 Matrix Spike Dup (BlD0711-MSD1) Source: 2102489-02 Analyzed: 04/26/21 14:49 Mercury 0.673 0.087 mg/kg 0.723 0.0418 87 75-125 22 20 QR-02 Post Spike (B1D0711-PSI) Source: 2102489-02 Analyzed: 04/26/21 14:51 Mercury 5.23 ug/L 5.00 0.273 99 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 64 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: R O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total'Control Analyte Result RL Units Spike Source %REC %REC RPD "MDNotes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Blank (BlD0734-BLK1) Analyzed: 04/26/21 13:29 Antimony ND 2.5 mgfkg Arsenic ND 2.0 " Barium ND 1.0 " Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 " Thallium ND 1.0 " Vanadium ND 2.0 Zinc ND 2.0 LCS (BlD0734-BS1) Analyzed: 04/26/21 13:04 Antimony 97.0 2.5 mg,'kg 100 97 80-120 Arsenic 100 2.0 100 100 80-120 Barium 93.5 1.0 100 94 80-120 Beryllium 99.0 0.50 100 99 80-120 Cadmium 99.2 0.25 100 99 80-120 Chromium 102 0.50 100 102 80-120 Cobalt 100 0.50 100 100 80-120 Copper 104 1.0 100 104 80-120 Lead 99.4 0.50 100 99 80-120 Molybdenum 98.4 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-120 Selenium 101 2.0 100 101 80-120 Silver 5.04 0.50 5.00 101 80-120 Thallium 108 1.0 100 108 80-120 Vanadium 99.8 2.0 100 100 80-120 Zinc 97.0 2.0 100 97 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3375 Page 65 of 94 161*4yOilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total' Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 LCS Dup (B1D0734-BSD1) Analyzed: 04/26/21 13:06 Antimony 97.8 2.5 mgIg 100 98 80-120 0.8 20 Arsenic 101 2.0 100 101 80-120 0.7 20 Barium 93.6 1.0 100 94 80-120 0.2 20 Beryllium 98.6 0.50 100 99 80-120 0.4 20 Cadmium 99.5 0.25 100 100 80-120 0.3 20 Chromium 103 0.50 100 103 80-120 0.8 20 Cobalt 101 0.50 100 101 80-120 0.3 20 Copper 104 1.0 100 104 80-120 0.8 20 Lead 99.9 0.50 100 100 80-120 0.3 20 Molybdenum 99.4 0.50 100 99 80-120 0.9 20 Nickel 102 0.50 100 102 80-120 0.4 20 Selenium 101 2.0 100 101 80-120 0.1 20 Silver 5.04 0.50 5.00 101 80-120 0.1 20 Thallium 108 1.0 100 108 80-120 0.5 20 Vanadium 100 2.0 100 100 80-120 0.4 20 Zinc 97.4 2.0 100 97 80-120 0.4 20 Duplicate (BlD0734-DUPl) Source: 2102489-01 Analyzed: 04/26/21 13:35 Antimony ND 2.5 mg/kg ND 20 Arsenic 5.86 2.0 6.40 9 20 Barium 87.5 0.99 72.5 19 20 Beryllium 0.369 0.49 0.419 12 20 Cadmium ND 0.25 ND 20 Chromium 20.3 0.49 22.2 9 20 Cobalt 6.53 0.49 6.95 6 20 Copper 18.4 0.99 21.5 16 20 Lead 5.52 0.49 6.10 10 20 Molybdenum 1.50 0.49 2.18 37 20 QR-04 Nickel 25.9 0.49 30.4 16 20 Selenium ND 2.0 ND 20 Silver ND 0.49 ND 20 Thallium ND 0.99 ND 20 Vanadium 19.9 2.0 20.6 9 20 Zinc 49.7 2.0 53.8 8 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 66 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Matrix Spike (B1D0734-MSI) Source: 2102489-01 Analyzed: 04/26/21 13:08 Antimony 30.5 2.5 mg/kg 98.3 ND 31 10-116 Arsenic 102 2.0 98.3 6.40 97 77-121 Barium 159 0.98 98.3 72.5 88 30-169 Beryllium 93.2 0.49 98.3 0.419 94 86-111 Cadmium 90.1 0.25 98.3 ND 92 81-112 Chromium 124 0.49 98.3 22.2 103 75-129 Cobalt 98.3 0.49 98.3 6.95 93 71-121 Copper 123 098 98.3 21.5 103 68-135 Lead 95.5 0.49 98.3 6.10 91 72-121 Molybdenum 87.8 0.49 99.3 2.18 87 70-112 Nickel 122 0.49 98.3 30.4 93 73-121 Selenium 91.6 2.0 98.3 ND 93 76-116 Silver 4.59 0.49 4.92 ND 93 54-132 Thallium 94.7 0.98 98.3 ND 96 64-120 Vanadium 117 2.0 98.3 20.6 98 78-124 Zinc 142 2.0 98.3 53.8 89 50-143 Matrix Spike Dup (BlD0734-MSD1) Source: 2102489-01 Analyzed: 04/26/21 13:11 Antimony 28.7 2.4 mg/kg 97.7 ND 29 10-116 6 20 Arsenic 99.5 2.0 97.7 6.40 95 77-121 2 20 Barium 173 0.98 97.7 72.5 103 30-169 9 20 Beryllium 90.5 0.49 97.7 0.419 92 86-111 3 20 Cadmium 96.7 0.24 97.7 ND 89 81-112 4 20 Chromium 120 0.49 97.7 22.2 100 75-129 3 20 Cobalt 95.5 0.49 97.7 6.95 91 71-121 3 20 Copper 120 0.98 97.7 21.5 101 68-135 3 20 Lead 92.4 0.49 97.7 6.10 88 72-121 3 20 Molybdenum 85.4 0.49 97.7 2.19 85 70-112 3 20 Nickel 121 0.49 97.7 30.4 92 73-121 1 20 Selenium 87.5 2.0 97.7 ND 90 76-116 5 20 Silver 4.44 0.49 4.88 ND 91 54-132 3 20 Thallium 90.3 0.98 97.7 ND 92 64-120 5 20 Vanadium 115 2.0 97.7 20.6 96 78-124 2 20 Zinc 141 2.0 97.7 53.8 89 50-143 0.6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: ciient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 67 of 94 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Total Metals by ' Control Analyte Result RL. Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Post Spike (BlD0734-PSI) Source: 2102489-01 Analyzed: 04/26/21 13:14 Antimony 1.95 mg/l. 2.00 -0.00714 93 75-125 Arsenic 2.15 2.00 0.129 101 75-125 Barium 3.34 2.00 1.46 94 75-125 Beryllium 1.96 2.00 0.00943 97 75-125 Cadmium 1.88 2.00 -0.0200 94 75-125 Chromium 2.46 2.00 0.448 100 75-125 Cobalt 2.05 2.00 0.140 96 75-125 Copper 2.56 2.00 0.433 106 75-125 Lead 2.01 2.00 0.123 94 75-125 Molybdenum 1.97 2.00 0.0438 96 75-125 Nickel 2.55 2.00 0.613 97 75-125 Selenium 1.96 2.00 -0.0375 98 75-125 Silver 0.0965 0.100 -0.00476 96 75-125 Thallium 1.98 2.00 -0.0435 99 75-125 Vanadium 2.41 2.00 0.416 100 75-125 Zinc 2.96 2.00 1.08 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 68 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0916 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:33 Blank (BlD0916-BLKI) Analyzed: 05/03/21 12:22 Cadmium ND 0.025 mg/L Chromium ND 0.050 " Copper ND 0.050 " Lead ND 0.050 LCS (BlD0916-BS1) Analyzed: 05/03/21 12:35 Cadmium 9.62 0.025 mg/L 10.0 96 80-120 Chromium 9.56 0.050 10.0 96 80-120 Copper 9.66 0.050 10.0 97 80-120 Lead 9.70 0.050 10.0 97 80-120 LCS Dup (BlD0916-BSD1) Analyzed: 05/03/21 12:37 Cadmium 9.68 0.025 mg/L 10.0 97 80-120 0.6 20 Chromium 9.59 0.050 10.0 96 80-120 0.3 20 Copper 9.70 0.050 10.0 97 80-120 0.4 20 Lead 9.78 0.050 10.0 98 80-120 0.9 20 Duplicate (B1D0916-DUPl) Source: 2102467-01 Analyzed: 05/03/21 12:53 Cadmium ND 0.050 mg/L ND 20 Chromium 0.0960 0.10 0.111 25 20 Copper 1.53 0.10 1.76 14 20 Lead 0.773 0.10 0.930 18 20 Leach Fluid Blank (BlD0916-LBK1) Analyzed: 05/03/21 12:25 Cadmium ND 0.050 niWl- Chromium ND 0.10 " Copper ND 0.10 " Lead ND 0.10 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 69 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 TCLP Metals by ICP Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0919 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:49 Blank (BlD0919-BLKI) Analyzed: 05/03/21 13:54 Chromium ND 0.050 mg/L Lead ND 0.050 11 LCS (BlD0919-BSI) Analyzed: 05/03/21 14:02 Chromium 9.42 0.050 mg/L 10.0 94 80-120 Lead 9.97 0.050 1.10.0 100 80-120 LCS Dup (BlD0919-BSD1) Analyzed: 05/03/21 14:04 Chromium 9.35 0.050 mg/L 10.0 94 80-120 0.7 20 Lead 9.82 0.050 1110.0 98 80-120 2 20 Duplicate (BlD0919-DUPl) Source: 2102508-01 Analyzed: 05/03/21 14:11 Chromium ND 0.050 mg/L ND 20 Lead 1.60 0.050 112.02 24 20 QR-04 Leach Fluid Blank (BlD0919-LBKI) Analyzed: 05/03/21 13:57 Chromium ND 0.050 mg/L Lead ND 0.050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 70 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0692 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 04/23/21 08:32 Blank (BlD0692-BLK1) Analyzed: 04/23/21 10:26 TPH Gasoline (('5-C12) ND 0.50 mg/kg Surrogate:4-Bromg/htorobcnccne 0.128 110.125 103 39-157 LCS (B1D0692-BSl) Analyzed: 04/23/21 09:34 TPH Gasoline (('5-C12) 1.07 0.50 mg/kg 1.00 107 68-139 Surrogate. 4-Broinq luorohcii Gene 0.146 110.126 116 39-157 LCS Dup (BlD0692-BSD1) Analyzed: 04/23/21 10:00 TPH Gasoline (C5-C12) 1.05 0.49 mg/kg 0.988 106 68-139 2 20 Surrogate:4-Bromglluorohenzene 0.150 110.124 121 39-157 Duplicate (BlD0692-DUPl) Source: 2102433-01RE1 Analyzed: 04/23/21 22:44 TPH Gasoline (C5-('12) ND 4.8 mg!kg ND 20 Surrogate:4-Bromgl1noohenzene 1.18 111.20 98 39-157 Matrix Spike (B1D0692-MS1) Source: 2102433-01RE1 Analyzed: 04/23/21 23:10 TPH Gasoline (C5-('l2) 8.79 4.9 mg/kg 9.80 ND 90 10-171 Surrogatc:4-Bromolluorobenrenc 1.34 111.23 109 39-157 Matrix Spike Dup (BlD0692-MSD1) Source: 2102433-01RE1 Analyzed: 04/23/21 23:36 TPII Gasoline (C5-C12) 8.26 4.4 mg/kg 9.77 ND 94 10-171 6 20 Surrogate: 4-Broniq luorohenzene 1.29 111.10 118 39-157 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 71 of 94 '( , �E W—� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Serni-Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0766 - EPA 8015M Preparation: EPA 3550C 04/27/21 07:10 Blank (B1D0766-BLK1) Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22) ND 10 mg/kg TPH Motor Oil (C'23-C40) ND 50 " Surrogate: o-Teipherrnl 41.9 49.8 84 65-136 LCS (BlD0766-BSI) Analyzed: 04/27/21 13:53 TPH Diesel (C13-C22) 420 10 mg/kg 499 84 72-115 TPH Motor Oil (C23-C40) 404 50 499 81 74-126 Surrogate: o-Teiphen-vl 43.0 49.9 86 65-136 LCS Dup (BlD0766-BSDI) Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22) 420 10 mg/kg 500 84 72-115 0.2 20 TPH Motor Oil (C 23-C40) 402 50 500 80 74-126 0.5 20 Surrogate: o-TeiphenYl 42.3 50.0 85 65-136 Duplicate (BlD0766-DUPl) Source: 2102489-01 Analyzed: 04/27/21 15:02 TPH Diesel (CI3-C22) ND 9.9 mg/kg ND 20 TPH Motor Oil (C23-C40) ND 50 ND 20 Surrogate: o-Teiphen.Vl 38.9 49.6 78 65-136 Matrix Spike (B1D0766-MSl) Source: 2102489-01 Analyzed: 04/27/21 14:17 TPH Diesel (Cl 3-('22) 430 9.9 mg/kg 497 ND 86 46-147 TPH Motor Oil (C23-C40) 418 50 497 ND 84 35-171 Surrogate: o-Teiphen.vl 40.2 49.7 81 65-136 Matrix Spike Dup (BID0766-MSD1) Source: 2102489-01 Analyzed: 04/27/21 14:40 TPH Diesel (CI3-C22) 480 10 mg/kg 499 ND 96 46-147 11 20 TPH Motor Oil (C23-C40) 429 50 499 ND 86 35-171 3 20 Surrogate: o-Teaphenrl 44.5 49.9 89 65-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: (80511925-3376 Page 72 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Batch BID0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (BlD0650-BLKI) Analyzed: 04/23/21 16:50 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " Bromochloromcthane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromofonn ND 0.0050 " Bronioniethane ND 0.0050 " n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 " Chloroform ND 0.0050 " Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 " Dibromochloromethane ND 0.0050 1,2-I)ibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (EDB) ND 0.0050 " Dibromoniethanc ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " 1.3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 Dichlorodithtoromethane ND 0.0050 1,1-Dichloroethene ND 0.0050 1,2-Dichlorocthanc ND 0.0050 13-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 trans-1.2-Dichloroethene ND 0.0050 " 12-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 1,1-Dichloropropene ND 0.0050 " cis-1.3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethvlbenzene ND 0.0050 " 1lexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: {805 925-3376 Page 73 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (BlD0650-BLK1) Analyzed: 04/23/21 16:50 Styrene ND 0.0050 mg/kg 1,1,1,2-Tetrachloroethane ND 0.0050 " 1,1,2,2-Tetrachloroethane ND 0.0050 " Teirachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 " 1,2,3-Trichlorobenzene ND 0.0050 " L2,4-Trichlorobenzene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.0050 " 1,1,2=frichlorocthane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2,3-Trichloropropane ND 0.0050 12,4-Trimethylbenzene ND 0.0050 " 1.3,5-Trimethylbenzene ND 0.0050 " V'invl chloride ND 0.0050 " Xylenes (total) ND 0.0050 " Surrogate: Dibromolluorome thane 0.0484 0.0498 97 74-122 Surrogate. Toluene-d8 0.0479 0.0498 96 65-128 Surrogate: 4-BromoJluorobenzerne 0.0453 0.0498 91 75-121 LCS (B1D0650-BSI) Analyzed: 04/23/21 14:31 Benzene 0.0389 0.0050 mg1kg 0.0396 98 70-131 Bromobenzene 0.0369 0.0050 0.0396 93 74-130 Bromochloromethanc 0.0351 0.0050 0.0396 89 64-133 Bromodichloromethane 0.0368 0.0050 0.0396 93 69-137 Bromoform 0.0337 0.0050 0.0396 85 55-132 Bromomethane 0.0397 0.0050 0.0396 100 10-142 n-Butylbenzene 0.0440 0.0050 0.0396 Ill 64-156 sec-Butylbenzene 0.0465 0.0050 0.0396 117 75-155 tert-Butylbenzene 0.0438 0.0050 0.0396 110 74-144 Carbon tetrachloride 0.0396 0.0050 0.0396 100 67-135 Chlorobenzene 0.0399 0.0050 0.0396 WI 73-134 Chloroethane 0,0366 0.0050 0.0396 92 10-167 Chloroform 0.0371 0.0050 0.0396 94 69-124 Chloromethane 0.0286 0.0050 0.0396 72 34-136 2-Chlorotoluene 0.0421 0.0050 0,0396 106 75-135 4-Chlorotoluene 0.0420 0.0050 0.0396 106 70-138 Dibronwchloromethane 0.0370 0.0050 0.0396 93 67-135 1,2-Dibromo-3-chloropropane 0.0368 0.0050 0.0396 93 41-149 1,2-Dibromoethane (EDB) 0.0365 0.0050 0.0396 92 68-131 Dibromomethanc 0.0322 0.0050 0.0396 81 61-140 1,2-Dichlorobenzene 0.0409 0.0050 0.0396 103 76-136 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWw.oecusa.cam FAX: (805) 925-3376 Page 74 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS (BlD0650-BS1) Analyzed: 04/23/21 14:31 1,3-Dichlorobenzene 0.0427 0.0050 mglkg 0.0396 108 76-138 IA-Dichlorobenzene 0.0410 0.0050 0.0396 104 72-132 Dichlorodifluoromethanc 0.0196 0.0050 0.0396 50 10-155 1,1-Dichloroethane 0,0399 0.0050 0.0396 101 63-139 1,2-Dichloroethene 0.0359 0.0050 0.0396 91 64-126 1,1-Dichloroethene 0.0435 0.0050 0.0396 110 52-167 cis- I .2-Dichloroethene 0.0380 0.0050 0.0396 96 70-135 trans-1,2-Dichloroethene 0.0421 0.0050 0.0396 106 67-147 1,2-Dichloropropane 0.0368 0.0050 0.0396 93 68-131 1,3-Dichloropropane 0.0359 0.0050 0.0396 91 64-128 2,2-Dichloropropane 0.0404 0.0050 0.0396 102 63-154 LI-Dichloropropene 0A386 0.0050 0.0390 97 68-138 cis- I3-Dichloropropene 0.0376 0.0050 0.0396 95 72-134 trans-1,3-Dichloropropene 0.0385 0.0050 0.0396 97 69-132 Ethylbenzene 0.0404 0.0050 0.0396 102 68-136 Ilexachlorobutadiene 0.0446 0.0050 0.0396 113 72-198 4-Isopropyl Toluene 0.0439 0.0050 0.0396 111 74-150 Isopropylbenzene 0.0429 0.0050 0.0396 108 71-149 Methylene chloride 0.0402 0.0050 0.0396 102 51-127 Naphthalene 0.0436 0.0050 0.0396 110 57-158 n-Propylbenzene 0.0435 0.0050 0.0396 110 70-143 Styrene 0.0412 0.0050 0.0396 104 68-138 1,1,1,2-Tetrachloroethane 0.0373 0.0050 " 0.0396 94 76-130 1,1,2,2-Tctrachlorocthanc 0.0407 0.0050 0.0396 103 60-136 Tetrachloroelhene(PCE) 0.0381 0.0050 0,0396 96 73-138 Toluene 0.0371 0.0050 0.0396 94 72-128 1,2,3-Trichlorobenzene 0.0390 0.0050 0.0396 98 61-166 1,24-Trichlorobenzene 0.0406 0.0050 0.0396 103 71-158 1.1,1-Trichloroethane 0.0389 0.0050 0.0396 98 71-135 1,1,2-Trichloroethane 0.0341 0.0050 0.0396 86 64-132 Trichloroethene(TCE) 0.0374 0.0050 0.0396 94 74-139 Trichlorofluoromethane 0.0379 0.0050 0.0396 96 30-156 1,2,3-Trichloropropane 0.0383 0.0050 0.0396 97 67-123 1,24-Trimethylbenzene 0.0419 0.0050 0.0396 106 68-134 1,3,5-Trimethylbenzene 0.0440 0.0050 0.0396 111 71-140 Vinyl chloride 0.0352 0.0050 0.0396 89 43-144 Xylenes(total) 0.122 0.0050 0.119 102 69-138 Surrogate: Dibromolluoromethune 0.0490 0.0495 99 74-122 Surrogute:7uluene-d8 0.0475 0.0495 96 65-128 Sm•rogate:4-Bromolluorohencene 0.0476 0.0495 96 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 75 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (B1D0650-BSD1) Analyzed: 04/23/21 14:59 Benzene 0.0417 0.0050 mg/kg 0.0398 105 70-131 7 20 Bromobenzene 0.0394 0.0050 0.0398 99 74-130 6 20 Bromochloromcthane 0.0377 0.0050 0.0398 95 64-133 7 20 Bromodichloromethane 0.0392 0.0050 0.0398 98 69-137 6 20 Bromoform 0.0363 0.0050 0.0398 91 55-132 8 20 Bromomethane 0.0416 0.0050 0.0398 105 10-142 5 20 n-Butylbenzene 0.0475 0.0050 0.0398 120 64-156 8 20 sec-Butylbenzene 0.0493 0.0050 0.0399 124 75-155 6 20 tert-Butylbenzene 0.0464 0.0050 0.0398 117 74-144 6 20 Carbon tetrachloride 0.0418 0.0050 0.0398 105 67-135 5 20 Chlorobenzene 0.0420 0.0050 0.0398 106 73-134 5 20 Chloroethane 0.0394 0.0050 0.0398 99 10-167 7 20 Chloroform 0.0392 0.0050 0.0398 99 69-124 5 20 Chloromethane 0.0302 0.0050 0.0398 76 34-136 5 20 2-Chlorotoluene 0.0435 0.0050 0.0398 109 75-135 3 20 4-Chlorotoluene 0.0431 0.0050 0.0398 108 70-138 3 20 Dibromochloromethane 0.0397 0.0050 0.0398 100 67-135 7 20 1,2-Dibronuo-3-chloropropane 0.0410 0.0050 0.0398 103 41-149 11 20 1,2-Dibrontoethane (EDB) 0.0388 0.0050 0.0398 98 68-131 6 20 Dibromomethane 0.0334 0.0050 0.0398 84 61-140 4 20 1,2-Dichlorobenzene 0.0429 0.0050 0.0398 ]08 76-136 5 20 1.3-Dichlorobenzene 0.0444 0.0050 0.0398 112 76-138 4 20 1,4-Dichlorobenzene 0.0436 0.0050 0.0398 110 72-132 6 20 Dichloroditluoromcthane 0.0206 0.0050 0.0398 52 10-155 5 20 1, 1 -Dichloroethane 0.0424 0.0050 0.0399 107 63-139 6 20 1,2-Dichloroethane 0.0395 0.0050 0.0399 99 64-126 10 20 1, 1 -Dichloroethene 0.0446 0.0050 0.0399 112 52-167 2 20 cis- 1,2-Dichloroethene 0.0413 0.0050 0.0398 104 70-135 8 20 trans-1,2-Dichloroethene 0.0447 0.0050 0.0398 112 67-147 6 20 1,2-Dichloropropane 0.0401 0.0050 0.0398 101 68-131 9 20 1,3-Dichloropropane 0.0383 0.0050 0.0398 96 64-128 6 20 2,2-Dichloropropane 0.0436 0.0050 0.0398 110 63-154 8 20 1, 1 -Dichloropropene 0.0416 0.0050 0.0398 105 68-138 8 20 cis- 1,3-Dichloropropene 0.0407 0.0050 0.0398 102 72-134 8 20 trans- I .3-Dichloropropene 0.0414 0.0050 0.0398 104 69-132 7 20 Ethylbenzene 0.0422 0.0050 0,0398 106 68-136 4 20 Ilexachlorobutadiene 0.0478 0.0050 0.0398 120 72-198 7 20 4-Isopropyl Toluene 0.0465 0.0050 0.0398 117 74-150 6 20 Isopropylbenzene 0.0461 0.0050 0.0398 116 71-149 7 20 Methylene chloride 0.0427 0.0050 0.0398 108 51-127 6 20 Naphthalene 0.0454 0.0050 0.0398 114 57-158 4 20 n-Propylbenzene 0.0460 0.0050 0.0398 116 70-143 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX_(805) 925-3376 Page 76 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GUMS - Quality Control �nalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (BlD0650-BSDI) Analyzed: 04/23/21 14:59 Styrene 0.0437 0.0050 mg/kg 0.0398 110 68-138 6 20 1,1,1,2-Tetrachlorocthane 0.0395 0.0050 0.0398 99 76-130 6 20 1,1,2,2-Tetrachlorocthanc 0.0415 0.0050 0.0398 104 60-136 2 20 Tetrachloroethene (PCE) 0.0400 0.0050 0.0398 100 73-139 5 20 Toluene 0.0399 0.0050 0.0398 100 72-128 7 20 1,2,3-Trichlorobenzenc 0.0432 0.0050 0.0398 109 61-166 10 20 1,2,4-1'richlorobenzene 0.0439 0.0050 0.0398 110 71-158 8 20 1,1,1-Trichloroethane 0.0415 0.0050 0.0398 104 71-135 6 20 1,1,2-Trichloroethane 0.0377 0.0050 0.0398 95 64-132 10 20 Trichloroethene (TCE) 0.0396 0.0050 0M398 99 74-139 6 20 Trichlorofluoromethane 0.0412 0.0050 0.0398 104 30-156 9 20 1,2,3-Trichloropropane 0.0381 0.0050 0,0398 96 67-123 0.6 20 1,14 Triinethylbenzene 0.0448 0.0050 0.0398 113 68-134 7 20 1,3,5-Trimethylben7ene 0.0461 0.0050 0.0398 116 71-140 5 20 Vinyl chloride 0.0371 0.0050 0.0398 93 43-144 5 20 Xylenes (total) 0.128 0.0050 0.119 108 69-138 5 20 Surrogate: Dibromo/luorumeiltunc 0.0504 0.0497 1111 74-122 Surrogate: Toluene-d8 0.0476 0.0497 96 65-128 Surrogate:4-Bramo/luorohersene 0.0475 0.0497 96 75-121 Duplicate (BlD0650-DUPI) Source: 2102489-01 Analyzed: 04/24/21 03:18 Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0,0050 ND 20 Bromochloromclhanc ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromofonn ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochhxomethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane ND 0.0050 ND 20 1,2-Dibrontoetliane (EDB) ND 0.0050 ND 20 Dibromomethane ND 0.0050 ND 20 1.2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oectrsa.corn FAX: (805) 925-3376 Page 77 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GUMS - Quality Control J �nalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Duplicate (BlD0650-DUPl) Source: 2102489-01 Analyzed: 04/24/21 03:18 1,3-Dichlorobenzcnc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromcthane ND 0.0050 ND 20 l,l-Dichloroethane ND 0.0050 ND 20 1,2-Dichloroethane ND 0.0050 ND 20 1, 1 -Dichloroethene ND 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroetlene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane ND 0.0050 ND 20 1,1-Dichloropropene ND 0.0050 ND 20 cis-1,3-Dichloropropene ND 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 Ethylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane ND 0.0050 ND 20 1,1,2,2-Tetrachloroethane ND 0.0050 ND 20 Tetrachloroethene WCE) ND 0.0050 " ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1.24-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane ND 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethane ND 0.0050 ND 20 1,2,3-Trichloropropane ND 0.0050 ND 20 L2,4-Trimethylbenzene ND 0.0050 ND 20 1,3,5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: Dibromolluorome.thane 0.0479 0.0490 97 74-122 Surrogate: Toluene-d8 0.0485 0.0496 98 65-128 Sm•rogate:4-Bromollnmrrbencene 0.0452 0.0496 91 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 78 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (B1D0650-MS1) Source: 2102489-02 Analyzed: 04/24/21 04:12 Benzene 0.0404 0.0050 mg/kg 0.0402 ND 101 37-145 Bromobenzene 0.0359 0.0050 0.0402 ND 89 29-147 Bromochloromethanc 0.0367 0.0050 0.0402 ND 91 40-145 Bromodichloromethane 0.0384 0.0050 0.0402 ND 96 39-153 Bromoform 0.0332 0.0050 0.0402 ND 83 32-143 Bromomethane 0.0467 0.0050 0.0402 ND 116 10-141 n-Butylbenzene 0.0324 0.0050 0.0402 ND 81 10-162 sec-Butylbenzene 0.0408 0.0050 0.0402 ND 102 14-168 tert-Butylbenzene 0.0388 0.0050 0.0402 ND 97 21-159 Carbon tetrachloride 0.0380 0.0050 0.0402 ND 95 28-148 Chlorobenzene 0.0394 0.0050 0.0402 ND 96 32-148 Chloroethane 0.0502 0.0050 0.0402 ND 125 11-166 Chloroform 0.0400 0.0050 0.0402 ND 100 40-139 Chloromethane 0.0350 0.0050 0.0402 ND 87 18-135 2-Chlorotoluene 0.0362 0.0050 0.0402 ND 90 25451 4-Chlorotoluene 0.0363 0.0050 0.0402 ND 90 22-150 Dibromochloromethanc 0.0359 0.0050 0.0402 ND 89 40-147 1,2-Dibromo-3-chloropropane 0.0390 0.0050 0.0402 ND 97 25-158 1,2-Dibromoethane (EDB) 0.0369 0.0050 0.0402 ND 92 38-147 Dibromomcthane 0.0319 0.0050 0.0402 ND 79 39-150 1 .2-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 24-154 1,3-Dichlorobenzene 0.0369 0.0050 0.0402 ND 92 21-153 1,4-Dichlorobenzene 0.0362 0.0050 0.0402 ND 90 21-146 DichlorodiFluoromcthanc 0.0188 0.0050 0.0402 ND 47 10-149 I,1-Dichloroethene 0.0420 0.0050 0.0402 ND 105 34-151 1,2-Dichloroethane 0.0400 0.0050 0.0402 ND 100 40-137 1, 1 -Dichloroethene 0.0449 0.0050 0.0402 ND 112 21-172 cis-1.2-Dichloroethene 0.0385 0.0050 0.0402 ND 96 38-147 trans-1,2-Dichloroethene 0.0409 0.0050 0.0402 ND 102 30-160 1,2-Dichloropropane 0.0397 0.0050 0.0402 ND 99 39-146 1,3-Dichloropropane 0.0396 0.0050 0.0402 ND 99 39-141 2,2-Dichloropropane 0.0280 0.0050 0.0402 ND 70 26449 1, 1 -Dichloropropene 0.0385 0.0050 0.0402 ND 96 28-150 cis-1,3-Dichloropropene 0.0371 0.0050 0.0402 ND 92 34-149 trans-1,3-Dichloropropene 0.0384 0.0050 0.0402 ND 96 36-143 Ethylbenzene 0.0397 0.0050 0.0402 0.00290 92 23-150 Flexachlorobutadiene 0.0313 0.0050 0,0402 ND 78 10-192 4-Isopropyl Toluene 0.0385 0.0050 0.0402 0.00290 89 11-165 Isopmpylbenzene 0.0406 0.0050 0.0402 0.00202 96 17-166 Nlethylene chloride 0.0456 0.0050 0.0402 ND 114 28-135 Naphthalene 0.0441 0.0050 0.0402 0.00948 86 10-174 n-Propylbenzene 0.0393 0.0050 0,0402 0.00310 90 16-156 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comWeports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 79 of 94 r A a WMQ Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Volatile Organic Compounds by GC/NlS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (BlD0650-MSI) Source: 2102489-02 Analyzed: 04/24/21 04:12 Styrene 0.0387 0.0050 mg/kg 0.0402 ND 96 24-154 1,1,1,2-Tetrachloroethane 0.0367 0.0050 0.0402 ND 91 38-149 1,1,2,2-Tetrachloroethane 0.0387 0.0050 0.0402 ND 96 22-164 Tetrachloroethene (PCE) 0.0349 0.0050 0.0402 ND 87 25-153 Toluene 0.0376 0.0050 0.0402 ND 94 26-149 1,2.3-Trichlorobenzene 0.0323 0.0050 0.0402 ND 80 10-163 1,24-Trichloroben7ene 0.0323 0.0050 0.0402 ND 81 10-162 1,1,1-Trichloroethane 0.0387 0.0050 0.0402 ND 96 34-149 1,1.2-Trichloroethane 0.0397 0.0050 0.0402 ND 99 25-175 Trichloroethene (TCE) 0.0386 0.0050 0.0402 ND 96 25-170 Trichlorofluoroniethane 0.0487 0.0050 0.0402 ND 121 19-155 1,2,3-Trichloropropane 0.0403 0.0050 0.0402 ND 100 32-165 1,2,4-Trimethylbenzene 0.0466 0.0050 0.0402 0.0183 70 15-150 1,3,5-Trimethylbenzene 0.0413 0.0050 0.0402 0.00496 90 10-158 Vinyl chloride 0.0446 0.0050 0.0402 ND 111 22-148 Xylenes (total) 0.130 0.0050 0.120 0.0173 93 22-153 Surrogate: Dibronurfluoromethane 0.0487 0.0502 97 74-122 Surrogate: Toluene-d8 0.0484 0.0502 96 05-128 Surrogate: 4-Bromol7norobenzene 0.0474 0.0502 94 75-121 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 80 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OF,C, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List F13A 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals by ICP 601013 STLC Cadmium STLC/EPA 601013 Water OEC, CA-ELAP 6010B STLC Chromium STLC/EPA 601013 Water OEC, CA-ELAP 601013 STLC Copper STLC/EPA 601013 Water OEC, CA-ELAP 601013 STLC Lead STLC/EPA 6010B Water OEC, CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 6010B TCLP Chromium EPA 1311/EPA 601013 Water OEC, CA-ELAP 601013TCLP Lead EPA 1311/EPA 601013 Water OEC, CA-P LAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA -FLAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 81 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Total Metals by CVAA Mercury Total EPA 7471A EPA 7471A Solid OEC. CA-ELAP Total Metals by ICP 6010B Total Antimony EPA 601013 Solid OEC, CA -FLAP 601013 Total Arsenic EPA 601013 Solid OEC, CA-ELAP 6010B Total Barium EPA 6010B Solid OEC. CA-ELAP 601013 Total Beryllium EPA 6010B Solid OEC, CA-ELAP 6010B Total Cadmium EPA 6010B Solid OEC, CA-ELAP 601013 Total Chromium EPA 601013 Solid OEC, CA-ELAP 6010B Total Cobalt EPA 6010B Solid OEC, CA-ELAP 601013 Total Cropper EPA 601013 Solid OEC, CA-ELAP 6010B Total Lead EPA 6010B Solid OEC, CA-ELAP 6010B Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 6010B Total Nickel EPA 601013 Solid OEC. CA -FLAP 6010B Total Selenium EPA 6010B Solid OEC. CA-ELAP 601013 Total Silver EPA 6010B Solid OEC. CA -FLAP 601013Total Thallium EPA 601013 Solid OEC, CA-ELAP 0010B Total Vanadium EPA 601013 Solid OEC, CA-ELAP 6010B Total Zinc EPA 601013 Solid OEC. CA-ELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC, CA -FLAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 82 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Sample Method i nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA -FLAP 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasolinc EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH -Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 83 of 94 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102508 Orcutt CA, 93457 Project Manager: Clarence Reynolds 05/03/2021 16:36 Notes and Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-01 Analyte concentration exceeds TTLC. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 84 of 94 EMSL Analytical, Inc. 464 McCormick Street San Leandro, CA 94577 Tel/Fax: (510) 895-3675 / (510) 895-3680 http://www.EMSL.com / sanleandrolab@emsl.com Attention: Shahanaz Parvin Oilfield Environmental and Compliance 307 Roemer Way Suite 300 Santa Maria, CA 93454-1105 Project: 2102508 EMSL Order: 092105912 Customer ID: OILF50 Customer PO: 2102508 Project ID: Phone: (805) 922-4772 Fax: (805) 925-3376 Received Date: 04/26/2021 8:45 AM Analysis Date: 04/26/2021 Collected Date: 04/23/2021 Test Report: Asbestos Analysis of Bulk Materials via EPA 600IR-931116 Method using Polarized Light Microscopy Non -Asbestos Asbestos Sample Description Appearance % Fibrous % Non -Fibrous % Type 2102508-16 Tan 50% Quartz None Detected Non -Fibrous 50% Non -fibrous (Other) 092105912-0001 Homogeneous 2102508-17 Gray 50% Quartz None Detected Non -Fibrous 40% Ca Carbonate 092105912-0002 Homo: ieneous 10% Non -fibrous (Other) Analyst(s) Gavin Lee (2) Cecilia Yu, Laboratory Manager or Other Approved Signatory EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 "Interim Method") but augmented with procedures outlined in the 1993 ("final") version of the method. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non -friable organically bound materials present a problem matrix and therefore EMSL recommends gravimetric reduction prior to analysis. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Estimation of uncertainty is available on request. Samples analyzed by EMSL Analytical, Inc San Leandro, CA NVLAP Lab Code 101048-3, WA C884 Initial report from: 04/26/2021 13:36:56 4St3 PLM 0008 0001 - 1.78 Printed: 4/26/2021 1:36 PM Page 1 of 1 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2314.D Operator EW Acquired 23 Apr 2021 2:32 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-01@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 14 Response_ GOMD2314.D\FID1A 90000. 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2315.D Operator EW Acquired 23 Apr 2021 2:58 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-02@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 15 Response_ 85000 80000 75000 70000 650001 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2315.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 1.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2316.D Operator EW Acquired 23 Apr 2021 3:24 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-03@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 16 GOMD2316.D\FID1A 95000 90000 85000 80000 45000 40000 30000 1 10000 5000 Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2317.D Operator EW Acquired 23 Apr 2021 3:50 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-04@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 17 Response_ 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2317.D\FID1A - Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2318.D Operator EW Acquired 23 Apr 2021 4:16 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-05@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 18 GOMD2318.D\FID1A 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 i Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2319.D Operator EW Acquired 23 Apr 2021 4:42 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-06@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 19 Response_ 90000 85000 80000 i 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2319.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2320.D Operator EW Acquired 23 Apr 2021 5:08 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-07@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 20 GOMD2320.D\FID1A 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 I Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2321.D Operator EW Acquired 23 Apr 2021 5:34 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-08@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 21 Response_ 85000 f 80000 75000 70000 65000 60000 55000 50000 45000 40000 20000• 15000 10000 5000 Time 0.00 I 1.00 2.00 3.00 4.00 5.00 6.00 GOMD2321.D\FID1A 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2322.D Operator EW Acquired 23 Apr 2021 6:00 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-09@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 22 90000 85000 80000 75000 700001 65000i 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 i Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 GOMD2322.D\FID1A 7.00 .�'r 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2323.D Operator EW Acquired 23 Apr 2021 6:26 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-10@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 23 Response 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 i 20000 15000 10000 5000 GOMD2323.D\FID1A Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2328.D Operator EW Acquired 23 Apr 2021 8:35 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-11@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 28 Response 90000 85000 80000 75000 70000 650001 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 GOMD2328.D\FID1A 5000 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2329.D Operator EW Acquired 23 Apr 2021 9:01 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-12@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 29 Response 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 5000 GOMD2329.D\FID1A 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2330.D Operator EW Acquired 23 Apr 2021 9:27 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-13@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 30 Response_ 95000 900001 85000 80000 75000 70000 650001 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 f 10000 GOMD2330.D\FID1A 5000 h i� �� Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2331.D Operator EW Acquired 23 Apr 2021 9:53 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-14@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 31 GOMD2331.D\FID1A 90000 85000 60000 55000 50000 45000 40000 I i 35000- i 30000 25000 20000 15000 10000 5000 :. -- _I , , . - ; Time 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 File C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2332.D Operator EW Acquired 23 Apr 2021 10:18 pm using AcgMethod GASBTEXE.M Instrument GC7 Sample Name: 2102508-15@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 32 GOMD2332.D\FID1A 90000 85000 80000 75000 70000 65000 60000 55000 50000 45000 40000 35000 30000 25000 20000 15000 10000 r^00 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 W m 0. L N .Vdin 45OQ aa.t� Q 7= V cd to w QD a K x� as O � U sPlloS ""Nosh mot RilMsouoJ m o G G G ZSOHIVIVOO Bad I issd:: . e M11Qnu01 U = c OOM saOAS a o O 111141,02 OWOO' dHl zCL "7 10 a w o spWnS I eplus>:O anpassa FE OC Cq �+� � as1l llnd 809ZB � rr' p ii o ❑ G�i V) U (� a d p4 qn-W - ZZ dill a( .0 ❑ Ix m ` g r � � E E ❑ C U # Z❑} O all al 3� _ p p P a a O O b 1rp}] C R u q c- 0 El cc a •� �N $ c U U F 04 W U U ►- J C' 7. O F� U N z J Q W a U) X � G O �►�' V rc in S R� oP110S Poo-loo1010101 A41AIS-00 G O O Z909 J V 16909 .�L+ 8�d I food C u U UH = Q 5a � U 001z9 o00AS 10119 Will OWU£1- dMl Omt a u i, eTi w opWnS 1 splumAD oAp000a 1'- � Z $ y � m 12 d O loll lied 809L9 X }( � R Z � N L O � � oioi•W - zz olllt }( � � "\ a n U Ct d p4 =� � r �D _C 1 � - g �Y OD 0 CIO U O0 3I " �+ Z❑❑❑ 8 _ u ft $ c V p .nr � W N = V w x C DD L r ae O i r C $ + n a b pG c 1' CL JE � r: m m � U� I ii v 2 J Q U U.1 CL 0 'V.: y Q � « / z t ) } z O Duo \ / f ■■■■O■ § ~CD Dq t D\ ƒ } I c 7 ƒ \ K 3 0 7 0 off o° o e 7 0°- ) z z 2 § \ �; _ 2 } o ft0& �_ / 2 ) ) § } a 2 k a p e I I a 2 a J / /k�� 0 , L { / c { E 3 d) ) ) 2 @ G & & 9 / 0 2 a n £ \ CD § ) r � f _ m <2 `k &fk _ � . § $ C s &�_)#� k \ / \ f \ k M @ a / z CL a / J ) ) \ \7 ow ƒ\0)Bo ` $ ) �% =$>{)E /ƒ/ %- \ \ [// \ o G m ,)- -0 a) ° o� 2 § ) \ c ■ ) ) o < ) \ ) in au)) \$ k k ) (� k J J J w > -^ m ® - ■ O j \ \ \ \ \ m o o \ / \ 0 IL 2■ o o U v ■ � ,It a s N C N E E O U a> 0 U� O 1 Z N N d a` c v v v v v o 0 o a o v v o v o v v v v v o 17g vA o� aA o n11tn n ). �0 °0cic°o°n <on i0n CCn iv ((i(l0i .i U C U C _ @ oQ O Q 0 @ 3 Q 0 O Q o O Q 0 O Q 0 O 3 Q 0 O Q o O Q o O Q 0 O 3 Q o N 3 Q o O 3 Q o N 3 oQ O 3 Q 0 �. a > > > > > > > >a N N a0 N a0a000a0a0aoc0Dc0N N N N N N O N N NN N N y N <A N N N O) N y N O o N N O O N N N m N N N <T o N N O o,v_ d O O N O O O N O N OO v N O O 3 N OD1 N N OOu NOJJ01 v_ a� m v y y v y a y m d d ddLL uO LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL lL W W 0 .n U N N N Q N Q N Q N Q N Q Q Q N Q Q Q NQ Q Q N Q ¢ NQ N N O N O N o N O N O N O N O N O N O N O N O N mNN m > > > > > > > > > > > >c > m > m > m J C� J J C7 +m„ C N E N N E N N E N N N E N E N N N E N N E N O U O V O N O V O N O O N O O N O ar O N O O N O O N 0 V 0 N O O N 14,1 O N O O N O O N O 7 O N 0 0 N O V O N LL O RQ m Q m Q m Q m Q m Q m Q m Q m Q m Q m Q m Q m Q m Q m Q m Q Q 0 0 N 0 N 0 M 0 M 0 V 0 d' 0 0 0 O 0 O 0 0 0 M 0 W 0 O 0 O 0 O O e- N N M M V t0 CO r m a L D_ I N moj O m O N� U U J cn nab o (D a CL l E f6 N x� c E t 0 sP110S P•NosIO 1"01 4AI-0 G G C Z9081VF908 y Bad I Issd U AMllQsUuBl ec c d OOM * SOOAS v U a m 0Q W9F08 OWOO' dHt X Z � i COD u >, a °pUj°S ! eplusAO sepassa m F- E ;* 4>t d x +�+ 'Z I911 Nnd 809Z8 X o z may+ . ir-4 ❑ a` v0 Q G� O p d "On ZZ *11 j( m aW❑ T 9 o m m . g C {i O 4 O ® N N a C N < r N ❑ ❑ U � s Qt 3 '� M 'h z ❑':: El z U w ❑ x x 4c h _ 3 C a 5 i v° C . t~v N V R C E _pi o ❑ ❑ m ae m c d E. c oa °< EN W > > > y a a Q ai z 0 V 0' y Q U W a U) 4 G A L V m cao sPlloS PsMasIG Rlol in O G zoo WON sod 1 lssd u U LI °; S a' � U x aocte MAS L R C ma QWUO - dH Nil; ma z w a a „ v T N s0YM8 1 squsA:D sArtossa c F" E " $ o 4s11 1ind E09ZB X r ` j� z a ++ r�O O Y \ sips" - ZZ owl ri vi C� G d o4 } a i❑ C • o CL v ID d: C x g ❑ Q r a G g �r vi ra 3 n = Q a o 333 [DO s K a I " 3 a N u m C E N 7 N aLe t n �.. da ❑ m m �t a T i ,J ► i >, $ 9t >o d F~ E a x� N c c m U I—F In z O v z g w a Q W1 N '0 >4 0 c 00 M Vy C GY X 6Z.. i-i7 [•� z 7 Q o 00 a p co V C E U y .Q L d �C E 0 14 Cd n. u 0 fItei ti U Kt tfj � c. 0 co C �. U yA O i a U �a " a V E c, z :2 o *. W C V Li. E 0 rn b .O N N .0 � G N � L Q { O N c ,a y� c T N 7 f 0. n C4 �JJ L `U a fn N � � Os N pp, r C O Pr c N Page 91 of 94 1 91 rn E m N O ut s COL. Cot a �• U U�4 � Co�rt c tb as d a: n �t ppIL U U CL U n C) U CJJ U wav v a a a a a 0- F E E E m " 0 U U U cL cj a F 1= F a O 3IJ- F U F F � F U F U h U tJ S ;n 0 U 1 00 1 (n co (n co co In $pit" PeNoWa INol O O O z909IY4909 Y p o DOtz9-$30AS :a M°9409 onoo - dHl Z opNlnS I oPIuVAO *Aa-*S a .a vs d S, t- pp a>1 Cq � "I isll Und 809z9 X X o Z �y+ ff, •lases zz *Fill � � o v� GJ C7 d a ai .a In ca M72 $ h O CL - ! t V t i I I I O 61 O N C E a N < Lr 00CD g - � U 3 p n •I z C a Y � oo 3 b z(i o to a��3 a Q �. x V-7 w C Ch a a E [ rl `wj O O «cam ❑❑ C ` ° p° I d E Ormay In k n « F 'a Q y y E m E .0 N o�C Oo awv�� Z 0 V M H N Z g W Cl. rn 9 N rn E.m N .U�L its o mom �• U S�L G � tCO S Ulu to 4 cs a a a � E x Syt a J F a s a �- o co M a�! a-c6 U d U J H > -0 O » d �% »�» t U U U 0- mNm F F F ao F. mC J J U J J -J Un Un Un m sPlloS "MoslO Inol RilMswroa 7s w a G C O zoos I V t606 y 80d 1 lssd U U DOM * SOOAS ' O W9 L06 OWOO - dHl X "� CL zs as sPWnS 1 oplu*Ao oAp"*N m F E Z 3 w a d mi 11ne1 806E6 o := c ; d ❑ sln.w zz ona x as s m mB�F a q q .. s ❑ Q E o . 00 �� E — o u Y 3 zv g E a ❑❑ x App U ig CL _ d i m 6-11 f N a. a e 7 E !2 !3 E a S IL to c c c ig W. 3 r 11, r 1 a u z � o 0 00 r. tnC. c U cu A U ar 'o C CL E 0 U lSf U y V �.O •c M � M Q U 47 •�+ O yr 00 O C V 0.' °'d �2 Oii CN � r� s r"• !n M Q w ¢ V as o U c ot avi O r% t%l C. 0- U z a 0 d N _ N id .c d L � try � N c L v i W .r N fi d ? N Page 94 of 94 r-4 6 Analytical Report 4 (4. "i�) 3��Y� Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director msprister@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 A "MJL M Va Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Revision Previous Report Reason for Revision 2102032 04/07/2021 16:45 Complete report. Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Sump Trench W 2102032-01 Solid Solid 04/06/2021 10:25 04/06/2021 11:30 Sump Trench Pile 2102032-02 Solid Solid 04/06/2021 10:26 04/06/2021 11:30 Sump Trench Bottom 2102032-03 Solid Solid 04/06/2021 10:30 04/06/2021 11:30 Fire Trench Bottoms 2102032-04 Solid Solid 04/06/2021 10:36 04/06/2021 11:30 Fire Trench W 2102032-05 Solid Solid 04/06/2021 10:38 04/06/2021 11:30 Fire Trench E 2102032-06 Solid Solid 04/06/2021 10:40 04/06/2021 11:30 BatchSample Analysis Batch ID Preparation Date/Time STLC Metals by ICP 6010B STLC B1D0494 04/16,2021 15:40 STLC Metals Extraction STLC Metals Extraction BID0313 04/12/2021 14:18 TCLP Metals by ICP 6010E TCLP B I D0495 04/16/2021 15:41 TCLP Metals Extraction TCLP Metals Extraction B 1 D0312 04! 12/2021 14:17 Total metals by CVAA Mercury Total EPA7471A BID0153 04/07/2021 07:54 Total .Metals by ICP 6010B Total B I D0123 04/062021 12:15 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Sample ID: Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by : Lab ID: 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.097 0.091 mg/kg 1 BID0153 04/07/21 14:55 EPA 7471A Total Metals by ICP Antimony 7.5 2.3 mg/kg 1 BID0123 04/07/21 13:25 EPA 6010B Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 " " " " " N-02 N-03 Molybdenum 2.0 0.46 Nickel 98 0.46 Selenium ND 1.9 Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium 0.70 0.10 mg/L 2 BID0494 04/19/2112:57 STLC/EPA6010B Lead 3.6 0.10 TCLP Metals by ICP Lead 0.23 0.050 mg/L I BID0495 04/19/21 14:01 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA93454 www.oecusa.com FAX: e805F 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Sump Trench Pile Sampled: 04/06/21 10:26 Matrix: Solid Sampled by : Lab ID: 2102032-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Alercury 0.12 0.094 mg/kg 1 B1D0153 04/07/21 14:57 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B1D0123 04/07/2113:28 EPA 6010B Arsenic 7.4 19 " Barium 280 0.95 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 12 0.47 Copper 38 0.95 Lead 180 0.47 " " " " " N-02, N-03 Alolybdenum 1.2 0.47 Nickel 78 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 37 1.9 Zinc 250 1.9 STLC Metals by ICP Chromium 0.39 0.10 mg/L 2 B1D0494 04/19/2113:00 STLC/EPA6010B Lead 15 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.086 0.050 mg/I. 1 Bl D0495 04/19/21 14:04 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (85) 925-3376 Page 4 of 20 walft Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalytical i Sample ID: Sump Trench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by : Lab ID : 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg I BID0153 04/07/21 14:59 EPA7471A Total Metals by ICP Antimony 2.5 2.4 mg/kg 1 B1 D0123 04/07/21 13:31 EPA 601 OB Arsenic 7.0 1.9 Barium 230 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.48 Copper 72 0.97 Lead 140 0.49 " " " " " N-02, N-03 INolvbdenum 1.1 0.48 Nickel 190 0.49 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 34 1.9 Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 BID0494 04/19/21 13:02 STLC/EPA6010B Lead 7.6 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 mg/L I B I D0495 04/19/21 14:06 EPA 1311 /EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalytical Sample ID: Fire Trench Bottoms Sampled: 04/06/21 10:36 Matrix: Solid Sampled by : Lab ID : 2102032-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg/kg 1 B1 DO153 04/07/21 15:01 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg,kg 1 B1 D0123 04/07/21 13:34 EPA 6010B Arsenic 6.6 1.8 Barium 220 0.91 Beryllium 0.63 0.46 Cadmium ND 0.23 Chromium 52 0.46 Cobalt 18 0.46 Copper 26 0.91 Lead 9.4 0.46 Molybdenum 0.46 0.46 Nickel 110 0.46 Selenium ND 1.8 Silver ND 0.46 Thallium ND 0.91 Vanadium 34 1.8 Zinc 28 1.8 STLC Metals by ICP Chromium ND 0.10 mg/L 2 B1 D0494 04/19/21 13:13 STLC/FPA 6010B N-02 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID: Fire Trench W Sampled: 04/06/21 10:38 Matrix: Solid Sampled by: Lab ID : 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc 0.13 0.096 mg/kg I BID0153 04/07/21 15:04 EPA 7471A ND 2.4 mg/kg 1 B ID0123 04/07/21 13:37 EPA 6010B 4.8 1.9 130 0.96 ND 0.48 ND 0.24 41 0.48 9.0 0.48 22 0.96 27 0.49 Ll 0.48 50 0.48 ND 1.9 ND 0.48 ND 0.96 34 1.9 " 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805)_ 925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalytical Sample ID : Fire Trench E Sampled: 04/06/21 10:40 Matrix: Solid Sampled by: Lab ID : 2102032-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercurc 0.12 0.094 mg/kg 1 B 1 D0153 04/07/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I D0123 04/07/21 13:17 EPA 6010B Arsenic 6.4 1.9 Barium 170 0.94 Beryllium ND 0.47 Cadmium ND 0.24 Chromium 49 0.47 Cobalt 12 0.47 Copper 26 0.94 Lead 32 0.47 Molybdenum 1.2 0.47 Nickel 73 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.94 Vanadium 36 1.9 Zinc 64 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 8 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes `i Level Result Limits Limit Batch BlDO153 - EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 Blank (B1D0153-BLKl) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg/kg LCS (B1D0153-BS1) Analyzed: 04/07/21 13:07 Mercury 0.809 0.10 mglkg 0.833 97 85-115 LCS Dup (B1D0153-BSDl) Mercury Duplicate (B1D0153-DUPl) Mercury Matrix Spike (B1D0153-MSl) Mercury Matrix Spike Dup (B1D0153-MSD1) Mercury Post Spike (B1D0153-PS1) Mercury Analyzed: 04/07/21 13:09 0.799 0.10 mg/kg 0.833 Source:2101942-01 Analyzed: 04/07/21 13:17 0.0118 0.087 mg/kg 0.0145 Source:2101942-01 Analyzed: 04/07/21 13:19 0.804 0.097 mg/kg 0.809 0.0145 Source:2101942-01 Analyzed: 04/07/21 13:21 0.776 0.092 mg/kg 0.765 0.0145 96 85-115 1 20 21 20 QR-04 98 75-125 100 75-125 4 20 Source:2101942-01 Analyzed: 04/07/21 13:23 5.16 ug/l, 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Blank (B1D0123-BLK1) Analyzed: 04/07/21 12:48 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 Copper ND 1.0 " Lead ND 0.50 Molybdenum ND 0.50 Nickel ND 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 LCS (B1D0123-BS1) Analyzed: 04/07/21 12:53 Antimony 97.5 2.5 mg/kg 100 98 80-120 Arsenic 100 2.0 100 100 80-120 Barium 103 1.0 100 103 80-120 Beryllium 100 0.50 100 100 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 100 0.50 100 100 80-120 Cobalt 102 0.50 100 102 80-120 Copper 98.3 1.0 100 98 80-120 Lead 102 0.50 100 102 80-120 Molybdenum 98.1 0.50 100 98 80-120 Nickel 102 0.50 100 102 80-t20 Selenium 99.8 2.0 100 100 80-120 Silver 4.96 0.50 5.00 99 80-120 Thallium 102 1.0 100 102 80-120 Vanadium 96.7 2.0 " 100 97 80-120 Zinc 102 2.0 100 102 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by ' Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSDI) Analyzed: 04/07/21 12:56 Antimony 100 2.5 mbrkg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 1.0 100 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 80-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 101 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 LO 100 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 100 104 80-120 2 20 Duplicate (B1D0123-DUPI) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mg -kg 1.40 20 Arsenic 5.99 1.9 6.36 6 ?(I Barium 159 0.97 " 169 6 2(1 Bervllium 0.372 0.48 0.395 6 !it Cadmium ND 0.24 ND 21) Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 Copper 26.5 0.97 26.5 �0 Lead 28.1 0.48 32.0 13 20 Molybdenum 56.4 0.48 1.20 1 k)2 Itt 11R-04 Nickel 68.5 0.48 73.4 ?0 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 Vanadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page ll of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ControlTotal Metals by ICP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Matrix Spike (B1D0123-MS1) Source: 2102032-06 Analyzed: 04/07/21 12:58 Antimony 37.4 2.4 mg1kg 97.7 1.40 37 10-116 Arsenic 101 2.0 97.7 6.36 97 77-121 Barium 250 0.98 97.7 169 83 30-169 Beryllium 94.0 0.49 97.7 0.395 96 S6-111 Cadmium 90.0 0.24 97.7 ND 92 81-112 Chromium 144 0.49 97.7 48.9 98 75-129 Cobalt 102 0.49 97.7 11.8 92 71-121 Copper 122 0.98 97.7 26.5 98 68-135 Lead 120 0.49 97.7 32.0 90 72-121 Molybdenum 87.1 0.49 97.7 1.20 88 70-112 Nickel 156 0.49 97.7 73.4 85 73-121 Selenium 91.5 2.0 97.7 ND 94 76-116 Silver 4.87 0.49 4.88 ND 100 54-132 Thallium 85.3 0.98 97.7 ND 87 64-120 Vanadium 131 2.0 97.7 36.2 97 78-124 Zinc 163 2.0 97.7 64.5 100 50-143 Matrix Spike Dup (B1D0123-MSD1) Source: 2102032-06 Analyzed: 04/07/21 13:01 Antimony 38.1 2.5 mgfkg 98.3 1.40 37 10-116 2 20 Arsenic 108 2.0 98.3 6.30 103 77-121 6 20 Barium 263 0.98 98.3 169 96 30-169 5 20 Beryllium 97.9 0.49 98.3 0.395 99 86-111 4 20 Cadmium 94.3 0.25 98.3 ND 96 81-112 5 20 Chromium 156 0.49 98.3 48.9 109 75-129 8 20 Cobalt 106 0.49 98.3 11.8 96 71-121 4 20 Copper 130 0.98 98.3 26.5 105 68-135 6 20 Lead 126 0.49 98.3 32.0 95 72-121 4 20 Molybdenum 91.2 0.49 99.3 1.20 91 70-112 5 20 Nickel 167 0.49 98.3 73.4 95 73-121 7 20 Selenium 96.0 2.0 98.3 ND 98 76-116 5 20 Silver 4.99 0.49 4.92 ND 102 54-132 2 20 Thallium 89.8 0.98 98.3 ND 91 64-120 5 20 Vanadium 137 2.0 98.3 36.2 102 78-124 4 20 Zinc 167 2.0 99.3 64.5 104 50-143 3 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.,oecusa.com FAX: (805) 925-3376 Page 12 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Totalby Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BID0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PSI) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.88 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.559 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Motybdemnn 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 Vanadium 2.68 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of20 r A M W& TAL M �rQ Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 STLC Metals by ICP - Quality Control enalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0494 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 10:40 Blank (B1D0494-BLK1) Analyzed: 04/19/21 12:12 Chromium ND 0.050 mg/l. Lead ND 0.050 11 LCS (B1D0494-BS1) Analyzed: 04/19/21 12:23 Chromium 9.69 0.050 mg/L 10.0 97 80-120 Lead 9.80 0.050 1110.0 98 80-120 LCS Dup (B1D0494-BSDl) Analyzed: 04/19/21 12:25 Chromium 9.72 0.050 mg/L 10.0 97 80-120 0.3 20 Lead 9.71 0.050 1110.0 97 80-120 1 20 Duplicate (BlD0494-DUPI) Source: 2101759-01 Analyzed: 04/19/21 12:46 Chromium 120 0.050 mg/L 112 6 20 Lead 54.3 0.050 1151.6 5 20 Leach Fluid Blank (BlD0494-LBK1) Analyzed: 04/19/21 12:15 Chromium ND 0.10 mg/L Lead ND 0.10 " Leach Fluid Blank (B1D0494-LBK2) Analyzed: 04/19/21 12:17 Chromium ND 0.10 mg/L Lead ND 0.10 " Matrix Spike (B1D0494-MS1) Source: 2101759-01 Analyzed: 04/19/21 12:28 Chromium 116 0.10 mg/L 10.0 112 42 89-115 QN14X Lead 59.4 0.10 1110.0 51.6 78 86-114 Qn'I-4X Matrix Spike Dup (B1D0494-MSDl) Source: 2101759-01 Analyzed: 04/19/21 12:38 Chromium 134 0.10 mg/L 10.0 112 214 89-115 14 20 QNI-4X Lead 68.2 0.10 1110.0 51.6 166 86-114 14 20 QN14X The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 14 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (BlD0495-BLKI) Analyzed: 04/19/21 13:46 Lead ND 0.050 mg/L LCS (BlD0495-BSI) Analyzed: 04/19/21 13:26 Lead 9.70 0.050 mg/I. 10.0 LCS Dup (BlD0495-BSDI) Analyzed: 04/19/21 13:28 Lead 9.71 0.050 mg/L 10.0 Duplicate (BlD0495-DUPI) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lead ND 0.050 mg/L Leach Fluid Blank (B1D0495-LBKI) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/L Leach Fluid Blank (B1D0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/L Matrix Spike (B1D0495-MSI) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lead WA 0.050 mg/I. 10.O Matrix Spike Dup (B1D0495-MSDI) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lcad 9.84 0.050 mg/L 10.0 98 80-120 97 80-120 0.5 20 ND 20 ND 101 86-114 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 I Sample Method Summary nalysis Method Matrix Laboratory & Certification STLC Metals by ICP 6010B STLC Chromium STLC/EI'A 601013 Water OEC_ CA -FLAP 601013 STLC Lcad STLC/EPA 601013 Water OEC, CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC, Internal TCLP Metals by ICP 601013 TCLP Lead EPA 1311/EPA 601OB Water OEC, C A-ELAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury'rotal EPA 7471 A EPA 7471A Solid OEC',CA-ELAP Total Metals by ICP 601013 Total Antimony EPA 601013 Solid OEC, CA-ELAP 601013 Total Arsenic EPA 001013 Solid OEC. CA-ELAP 001013 Total Barium EPA 6010B Solid OEC, CA-ELAP 601013 Total Beryllium EPA 601013 Solid OEC. CA-EL.AP 601 OB Total Cadmium EPA 601OB Solid OEC, CA-ELAP 601013 Total Chromium EPA 601 OB Solid OEC, CA-ELAP 601013 Total Cobalt EPA 601013 Solid OEC, CA-ELAP 601013 Total Copper EPA 601013 Solid OEC, CA -FLAP 001013 Total Lead EPA 601013 Solid OEC. CA-ELAP 001 OB Total Molybdenum EPA 601013 Solid OEC, CA-ELAP 601013 Total Nickel EPA 601013 Solid OEC, CA-EL.AP 601013 Total Selenium EPA 601 OB Solid OEC. CA-ELAP 601013Total Silver EPA 601013 Solid OEC, CA-ELAP 6010B Total Thallium EPA 601 OB Solid OEC, CA-ELAP 601 OB Total Vanadium EPA 601 OB Solid OEC, CA-ELAP 6010I3 Total Zinc EPA 601OB Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 16 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Notes and Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above 1 Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and!or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and or LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 20 x�C f a � a a OE s m V V F F � o N V 0: fPIIOS pfNOfIU 11401 a ro G G C Z8081V1,808 L u 80d I I"d d >wlliQfiluel �A G �+ OOLZB-fOOAS1 a L E 82 111191,08 0W00, clHl � o "•7 a m i, *pWnS 1 oplumAo eApaffa F' E > Ci Z ifl� Ilnd 809Z9 Z ❑ sinew ZZOmi a❑ T ED � v $ o n Ix 0. E 19 en �= g. � ❑p U 4 ro N OLl ;. r U Z C d C � aaamff ❑ Cl } %VI . Oel?r y N � O' a+ ` a s t; vi ❑ ❑CL g E. A N C C C E E N 3 0 > \ ( 0 cli CL . 0 w 2 a § � - e ) - E } $ E k } 6 m z z § : 2 ® ) ( ( \ ) ) b z - / m R z z O f ) ] A - Z \ $ 7 z ) } / moo 0 E / f f \ � o b \ _ /f, 0 0 t ] E o J 3 $ « z z ) § k k \ k U ■ > ■ > » » a > E mc )\ 3 _ ± 0 j 2 a o - ! _ ] @ 2) = E a § 2 §*{/<\ o ® m Z / & 0 = 2 m t ' k ^ ] $ a 3 § 3 72: D E E 3 3 g E 3 0 0 0 0$ 2 ƒ 2CL _ < � S ) / -alp a) a)r E $ i 2 7kj \ \ m 13 < { gE-$ 2E' { }�{]J\\ § 0�[2eu 2 � \ < E » - s 0 0/ f 2 a 0 7 Lt o i # _ ; o k)$eeEf%§ ) § A < I S £ S J ) ) w o O CL \ E j 2 E 2 a V. tll N E E O U IdHLLLL a� c 0 U� N LL x - v v v v v v � c°n tin c c c c c c Y >Y Y >Y >Y Y Co Co 0o a0 co co N L N CD N rn N m N rn N rn N rn o � ;v_ v v ;g -o 2 LL LL LL LL LL LL .Q N C t/1 UJ f6 N N f0 V1 N W N N @ tll to (6 Vl tll (6 C Ucoo N N N N N N a°o. co co aoo aoo oU c 0 pPlI o U Q 0 0 A a a M d wis U�UJUU U � ai E •JU E UF-OF-UF- �U U mto HVF-UOP v y X Un X cn X Un X sPi1oS PsAIosIO INOI .1 ,WAI-00 R !s G G O 80d Bead a � U � f11114g1uD1 C N OOR9 - 800AS d `.0 U a % W9 08 OWO`J - dHI L O N z w = 3 ra a m L1 o a epnS 1 amus60 eApaeey F- a z u ++ , isn Ilnd 809Z8 Zo }y+ N CQ A. w iia U tt,,�� O� d x .� OG e elgaw zz mt } ,c ❑ � h a m m a �1 c O m m v c f� a N I . < gOP CL E S N a ro S g oiS � 4 g ^ P F ❑ ❑.� U c n Z ? O G w o- � O 0 v 3 3 N E. z a a o° Sp ■❑ m. r x .' a C', n V _ c c = o mC3 15 $ CL 14 c eta aq, El El m m m �v ii e c a N c c c e e c . { � rig U F" PG E W V U E 3 F- F .0 CV tx Z Z � S 2 6i z O F= U M z V W a rn Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: 1�qw�4 A�-) Meredith Sprister, Business Director msprister@occusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analvtical Report for Samples Sample ID : Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by: Lab ID : 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.097 0.091 mg1kg 1 B 1 D0153 04/07/21 14:55 EPA 7471 A Total Metals by ICP Antimonv 7.5 2.3 mg/kg 1 B 1 D0123 04/07/21 13:25 EPA 6010B Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 " " " " " N-02, N-03 Molybdenum 2.0 0.46 Nickel 98 0.46 Selenium ND 1.9 Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 " Zinc 410 1.9 STLC Metals by ICP Chromium 0.70 0.10 mg/L 2 BID0494 04!19/21 12:57 STLC/EPA6010B Lead 3.6 0.10 TCLP Metals by ICP Lead 0.23 0.050 mg/L 1 BID0495 04/19/21 14:01 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples Sample ID : Sump bench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by : Lab ID: 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.093 mg/kg I Bl D0153 04/07/21 14:59 EPA 7471 A Total Metals by ICP Antimonv 2.5 2.4 mg/kg 1 131 DO123 04/07/21 13:31 EPA 6010B Arsenic 7.0 1.9 Barium 230 0.97 Beryllium ND OAS Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.49 Copper 72 0.97 Lead 140 0.48 " " " " " N-02, N-03 Molvbdenum 1.1 0.48 Nickel 190 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 34 1.9 Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 mg/L 2 B1D0494 04/19/2113:02 STLC/F.PA6010B Lead 7.6 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 mg/L I B 1 D0495 04/19/21 14:06 EPA 131 1/EPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportI Analytical Sample ID: Fire Trench W Sampled: 04/06/21 10:38 Matrix: Solid Sampled by : Lab ID: 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.13 0.096 mg/kg 1 BID0153 04/07/21 15:04 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg I B I D0123 04/07/21 13:37 EPA 6010B Arsenic 4.8 1.9 Barium 130 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 41 0.48 Cobalt 9.0 0.49 " Copper 22 096 Lead 27 0.49 " Nlolvbdenum 1.1 0.48 Nickel 50 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 34 1.9 Zinc 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Wav, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by CVAA - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0153 -EPA 7471A Preparation: EPA 7471A Pre Blank (B1D0153-BLK1) Mercury ND LCS (B1D0153-BS1) Mercury 0.809 LCS Dup (B1D0153-BSD1) Mercury 0.799 Duplicate (B1D0153-DUPI) Source: 2101942-01 Mercury 0.0118 Matrix Spike (B1D0153-MS1) Source: 2101942-01 Mercury 0.904 Matrix Spike Dup (B1D0153-MSD1) Source: 2101942-01 Mercury 0.776 Post Spike (B1D0153-PS1) Source: 2101942-01 Mercury 5.16 04/07/21 07:54 Analyzed: 04/07/21 13:13 0.10 mg/kg Analyzed: 04/07/21 13 : 07 0.10 mglkg 0.833 97 85-115 Analyzed: 04/07/21 13 :09 0.10 mg/kg 0.833 96 85-115 1 20 Analyzed: 04/07/21 13 :17 0.087 mglkg 0.0145 21 20 QR-04 Analyzed: 04/07/21 13:19 0.097 mg/kg 0.809 0.0145 98 75-125 Analyzed: 04/07/21 13:21 0.092 mg/kg 0.765 0.0145 100 75-125 4 20 Analyzed: 04/07/21 13:23 ug/I. 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.aecusa.com FAX: 805 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 -EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSDl) Analyzed: 04/07/21 12:56 Antimony 100 2.5 ntgIg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 1.0 100 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 80-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 101 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 1.0 100 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 100 104 80-120 2 20 Duplicate (B1D0123-DUPl) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mgfkg 1.40 20 Arsenic 5.99 L9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 ND 20 Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 Copper 26.5 0.97 26.5 0.2 20 Lead 28.1 0.48 32.0 13 20 Molybdenum 56.4 0.48 1.20 192 20 Nickel 68.5 0.48 73.4 7 20 Selenium ND L9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 Vanadium 35.4 L9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 QR-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of 20 I(. �i W� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by lCP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PS1) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/l. 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.88 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.558 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 Vanadium 2.68 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oectisa.com FAX: (805) 925-3376 Page 13 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 TCLP Metals by ' Control �Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (BID0495-BLK1) Analyzed: 04/19/21 13:46 Lead ND 0.050 mg/l. LCS (BlD0495-BS1) Analyzed: 04/19/21 13:26 Lead 9.76 0.050 mg/L 10.0 98 80-120 LCS Dup (BlD0495-BSD1) Analyzed: 04/19/21 13:28 Lcad 9.71 0.050 mg/I. 10.0 97 80-120 0.5 20 Duplicate (BlD0495-DUPl) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lead ND 0.050 mg/L ND 20 Leach Fluid Blank (BlD0495-LBKI) Analyzed: 04/19/21 13:48 Lead ND 0.050 mg/L Leach Fluid Blank (BlD0495-LBK2) Analyzed: 04/19/21 13:51 Lead ND 0.050 mg/L Matrix Spike (B1D0495-MS1) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lead 10.1 0.050 mg/L 10.0 ND 101 86-114 Matrix Spike Dup (BlD0495-MSDI) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lead 9.84 0.050 mg/I. 10.0 NI) 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Notes and Definitions Q-alifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPI) Relative Percent Difference N-02 Analyte concentration below TTLC but above lox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and or LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 17 of 20 @ 6. \ ) 0 \C\ - e m _ E CD \ \� E k ! f , § \ \ k \ \ } � � k \ � \ / 0 k } a \ { { ° ) 0- 0 E 2 O 7 A O � � ) &f= \ ) $ ) (L ) J ■, 0 OD C ca $ / Co abA ? § I « 3 y 0 0 t \ E O ■ 0 3 3 < 2 k ) & k k IL k 0 ■ ■ ■ » a > > > » /w 00 ca 3 } f 3 = a A 2 , \ $(D k f § k�{/<j 0 0C) SM 0 I G 2 \ a G 0§ 3 Q_(D C o m /\\\§\ 2 \ \& < a)0 /2 —�i (D ( x E $ S E § ' a 0 x ƒ 0 E { ] J { ° ) } \) k ] S c ® E § G - e 0 0 e a® 0 0 7 7 � 0 k« J ID )] � � \ of J af w �m ■ � , Cts rn E,m , N wl. ia .o 0 O mom aa.t�► � rn C6 a a � tip m co ci �i� VUUUU U fE E TO LOP Cn� �� v y+ Xfn Xcn X(n X :pllOS psAIOsla IMOl ZBOO I V"O9 L « 8Od / lssd W U, �itUQsWu6i fm e d iif a DOUR •sOOAS L a � � N MOM OWOV - dWl Z = O clq a m o �i'a `a spWns I OplusllO sApassa ►- L jn yN Isn Iind 809Zi Z 0. (A U Q d OG ZZ still } a ❑ a m m r o am w a a fY E . d x oiS ❑❑ _ U U IC n z ❑ �. a N O O L C t F ca LD } C �❑ x 2 040. t� C A _ m U g C � q c a m a < E� a a v � a mE � N A N � � o .. a a n rJ r l t� D ❑❑ O l m a m a CL co Q a, a. o F- v to EE C C C U 1 1--- M 0 H U t- z 5 W a Analytical Report Oilfield Environmental &Compliance, Inc. Clarence Reynolds OEC Work Order: 2102032 Pacific Petroleum California P. O. Box 2646 Report Date: April 19, 2021 16:46 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Center Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 06, 2021 11:30 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: O Meredith Sprister, Business Director mspristcr@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Drcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 ReportAnalytical Sample ID : Sump Trench W Sampled: 04/06/21 10:25 Matrix: Solid Sampled by: Lab ID: 2102032-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Alercury 0.097 0.091 mg/kg 1 B1D0153 04/07/2114:55 EPA 7471A Total Metals by ICP Antimonv 7.5 2.3 nig/kg I B1D0123 04/07/2113:25 EPA 6010B Arsenic 9.4 1.9 Barium 200 0.93 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 52 0.46 N-02 Cobalt 14 0.46 Copper 67 0.93 Lead 380 0.46 " " " " " N-02 N-03 Molybdenum 2.0 0.46 Nickel 98 0.46 Selenium ND 1.9 Silver ND 0.46 Thallium ND 0.93 Vanadium 31 1.9 Zinc 410 1.9 STLC Metals by ICP Chromium 0.70 0.10 mg/L 2 BID0494 04/19/21 12:57 STLC/EPA 6010B Lead 3.6 0.10 TCLP Metals by ICP Lead 0.23 0.050 mg/L 1 BID0495 04/19/2114:01 EPA 1311/EPA60111B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805. 925-3376 Page 3 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Samples I Sample ID : Sump Trench Bottom Sampled: 04/06/21 10:30 Matrix: Solid Sampled by: Lab ID : 2102032-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Not Total Metals by CVAA Mercury ND 0.093 mg/kg 1 BID0153 04/07/2114:59 EPA 7471A Total Metals by ICP Antimony 2.5 2.4 mg/kg 1 BID0123 04/07/2113:31 EPA 6010B Arsenic 7.0 1.9 " Barium 230 0.97 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 58 0.48 N-02 Cobalt 19 0.49 " Copper 72 0.97 Lead 140 0.48 " " " " " N-02, N-03 Molybdenum 1.1 0.48 " Nickel 190 0.48 " Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.97 Vanadium 34 1.9 Zinc 560 1.9 STLC Metals by ICP Chromium 0.27 0.10 nig/l. 2 BID0494 04/19/21 13:02 STLC/EPA6010B Lead 7.6 0.10 " " " " " N-07 TCLP Metals by ICP Lead 0.10 0.050 mg/l. 1 B 1 D0495 04/ 19/2) 14:06 EPA 1311 /E.PA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: {805) 925-3376 Page 5 of 20 r&WA.L" Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Analytical Report for Saniples Sample ID : Fire Trench W Sampled: 04/06/21 10:38 Matrix: Solid Sampled by : Lab ID : 2102032-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.13 0.096 mgfcg 1 B1D0153 04/07/21 15:04 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BID0123 04/07/2113:37 EPA 6010B Arsenic 4.8 1.9 Barium 130 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 41 0.48 Cobalt 9.0 0.48 Copper 22 0.96 Lead 27 0.48 Molvbdenum 1.1 0.48 Nickel 50 0.49 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 34 19 Zinc 62 1.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0153 -EPA 7471A Preparation: EPA 7471A Prep 04/07/21 07:54 Blank (B1D0153-BLK1) Analyzed: 04/07/21 13:13 Mercury ND 0.10 mg leg LCS (B1D0153-BS1) Analyzed: 04/07/21 13:07 Mercury 0.809 0.10 mglkg 0.833 97 85-115 LCS Dup (B1D0153-BSDI) Analyzed: 04/07/21 13:09 Mercury 0.799 0.10 mg/kg 0.833 96 85-115 1 20 Duplicate (B1D0153-DUPI) Source: 2101942-01 Analyzed: 04/07/21 13:17 Mercury 0.0119 0.087 mg/kg 0.0145 21 20 QR-04 Matrix Spike (B1D0153-MSI) Source: 2101942-01 Analyzed: 04/07/21 13:19 Mercury 0.904 0.097 mg/kg 0.809 0.0145 98 75-125 Matrix Spike Dup (B1D0153-MSD1) Source: 2101942-01 Analyzed: 04/07/21 13:21 Mercury 0.776 0.092 mg/kg 0.765 0.0145 100 75-125 4 20 Post Spike (B1D0153-PSI) Source: 2101942-01 Analyzed: 04/07/21 13:23 Mercury 5.16 ug/L 5.00 0.0886 101 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 LCS Dup (B1D0123-BSD1) Analyzed: 04/07/21 12:56 Antimony 100 2.5 mg/kg 100 100 80-120 3 20 Arsenic 103 2.0 100 103 80-120 2 20 Barium 105 1.0 100 105 80-120 2 20 Beryllium 102 0.50 100 102 80-120 2 20 Cadmium 104 0.25 100 104 80-120 2 20 Chromium 102 0.50 100 102 80-120 2 20 Cobalt 104 0.50 100 104 80-120 2 20 Copper 100 1.0 100 100 80-120 2 20 Lead 104 0.50 100 104 80-120 2 20 Molybdenum 101 0.50 100 WI 80-120 3 20 Nickel 104 0.50 100 104 80-120 2 20 Selenium 102 2.0 100 102 80-120 2 20 Silver 5.02 0.50 5.00 100 80-120 1 20 Thallium 105 H) 100 105 80-120 2 20 Vanadium 98.6 2.0 100 99 80-120 2 20 Zinc 104 2.0 100 104 80-120 2 20 Duplicate (B1D0123-DUPl) Source: 2102032-06 Analyzed: 04/07/21 13:20 Antimony ND 2.4 mg/kg 1.40 20 Arsenic 5.99 L9 6.36 6 20 Barium 159 0.97 169 6 20 Beryllium 0.372 0.48 0.395 6 20 Cadmium ND 0.24 ND 20 Chromium 53.2 0.48 48.9 8 20 Cobalt 12.7 0.48 11.8 8 20 Copper 26.5 0.97 26.5 0.2 20 Lead 28.1 0.48 32.0 13 20 Ivlolvbdenum 56.4 0.48 1.20 192 20 QR-04 Nickel 68.5 0.48 73.4 7 20 Selenium ND 1.9 ND 20 Silver ND 0.48 ND 20 Thallium ND 0.97 ND 20 Vanadium 35.4 1.9 36.2 2 20 Zinc 69.4 1.9 64.5 7 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0123 - EPA 6010B Preparation: EPA 3050B 04/06/21 12:15 Post Spike (B1D0123-PSI) Source: 2102032-06 Analyzed: 04/07/21 13:04 Antimony 2.04 mg/L 2.00 0.0296 100 75-125 Arsenic 2.17 2.00 0.134 102 75-125 Barium 5.57 2.00 3.55 101 75-125 Beryllium 1.96 2.00 0.00833 98 75-125 Cadmium 1.88 2.00 -0.0199 94 75-125 Chromium 2.94 2.00 1.03 95 75-125 Cobalt 2.16 2.00 0.248 96 75-125 Copper 2.58 2.00 0.558 101 75-125 Lead 2.58 2.00 0.675 95 75-125 Molybdenum 1.98 2.00 0.0253 98 75-125 Nickel 3.45 2.00 1.55 95 75-125 Selenium 1.97 2.00 -0.0445 99 75-125 Silver 0.0972 0.100 -0.00308 97 75-125 Thallium 1.84 2.00 -0.0477 92 75-125 Vanadium 2.69 2.00 0.763 96 75-125 Zinc 3.23 2.00 1.36 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0495 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/16/21 15:41 Blank (BlD0495-BLKI) Analyzed: 04/19/21 13:46 Lcad ND 0.050 mg/L LCS (BlD0495-BSl) Analyzed: 04/19/21 13:26 Lead 9.76 0.050 mg/L 10.0 98 80-120 LCS Dup (BlD0495-BSDI) Analyzed: 04/19/21 13:28 Lcad 9.71 0.050 mg/L 10.0 97 80-120 0.5 20 Duplicate (B1D0495-DUPl) Source: 2101934-01 Analyzed: 04/19/21 13:56 Lcad ND 0.050 mg/L ND 20 Leach Fluid Blank (B1D0495-LBK1) Analyzed: 04/19/21 13:48 Lcad ND 0.050 mg/L Leach Fluid Blank (B1D0495-LBK2) Analyzed: 04/19/21 13:51 Lcad ND 0.050 mg/L Matrix Spike (B1D0495-MSl) Source: 2101934-01 Analyzed: 04/19/21 13:31 Lcad 10.1 0.050 111g/1. 10.0 ND 101 86-114 Matrix Spike Dup (BlD0495-MSDI) Source: 2101934-01 Analyzed: 04/19/21 13:33 Lcad 9.84 0.050 mg/L 10.0 ND 98 86-114 2 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 15 of 20 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Center 2102032 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/19/2021 16:46 Notes and Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantization Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater the spike concentration. The QC batch was accepted based on LCS and or LCSD recoveries within the acceptance limits. QR-04 The RPD exceeded the QC control limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 20 @ < § z ) ; O 0 O ■ O § 0 i / ƒ gnomon § 7 $ 2 ± ) \ _* £ ` k k 0 k e o 0 CD 2 m # = / ) § 7 ° `; @ m $ £ ) z z , § 8 ; ` - /�\ 2 ) \ k ) 2 \ \ L) s, M -0E ± f 0 z z 7 2)) ƒ{ 2 ! � - - § 3 3 f / aLD 7 $ \ /)) 0 / § § A R / ƒ ) 0 0 ƒ C \ 0 0 \ ? ) © a7 ) cc/ u - ° k A - & [ r k s o a 2£ k 7 S$; ) j ( k \ & f \ z / § § { § \ \ ° 27 CD 2 % £ 7 L < E ] a { E k & Lj f 6 d§ 2 2 0 d # / f & 2 2 \ ] t ± 2 / $ _ I DE § ) \ ) t ) R /) /)) § \) E t � G A §) J ) w - � 2 0 0 g? . d \ \ ) \ ) \ k \ Z E \ a § z ■ O■ 3 o m u § «« 4 k k E j ) ( a a pis �UUUUU E HU o �U HU JuJ CJE ~1 CO F- F21 Xu)Xu)I rplws paAIOa1O Inol AtlMsouoO ii e W C G G Egos / Y Me ,q L 8Od /3sad si 12 aluai+lua OOZZO • aOOAS �+ U a J -j O N w2m OWO°J•dHl z = o o a a *pWnS I aplurAD aAparaa I !' E mi Z .+ 1sn Ilnd 809ZO Z . N T A ca i aw+ w UU= X slrlaW ZZ Owl m ,c ❑ T � n C C. 1 a E N Q c m O z 011 V 4 s a a d � � � � Q ❑.Q U y� U T 0 Z z CI a D NA Ii � F aci ca c E� ao.1 o e rig ly 3 $ N Z U co �❑ 4: } q x i C, U = c g e g � o � .� � � o N � oc a c` rn c R CC L h CIS0 L �3 El m 1 2ap ti� N ui c E. CQH�m • N� �'c n a�A -pg- cm&.;E GL 6 z 0 H L7 Z U w IL rn Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2101841 Pacific Petroleum California P. O. Box 2646 Report Date: April 06, 2021 16:03 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Centers, 2600 Broad St. Enclosed is an analytical report for the above referenced project. The samples included in this report were received on March 25, 2021 15:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director msprister@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Revision History Previous Report Reason for Revision 2101841 03/26/2021 17:07 Complete report. Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Tank N Wall 2101841-01 Solid Solid 03/25/2021 11:15 03/25/2021 15:00 Tank S Wall 2101841-02 Solid Solid 03/25/2021 11:20 03/25/2021 15:00 Tank E Wall 2101841-03 Solid Solid 03/25/2021 11:25 03/25/2021 15:00 Tank W Wall 2101841-04 Solid Solid 03/25/2021 11:30 03/25/2021 15:00 Tank Bottom E End 2101841-05 Solid Solid 03/25/2021 11:05 03/25/2021 15:00 Tank Bottom W. End 2101841-06 Solid Solid 03/25/2021 11:10 03/25/2021 15:00 Sump Trench W 2101841-07 Solid Solid 03/25/2021 11:35 03/25/2021 15:00 Sump Trench S 2101841-08 Solid Solid 03/25/2021 11:38 03/25/2021 15:00 Control 2101841-09 Solid Solid 03/25/202111:00 03/25/2021 15:00 Soil Pile N 2101841-10 Solid Solid 03/25/2021 11:40 03/25/2021 15:00 Soil Pile S 2101841-11 Solid Solid 03/25/2021 11:45 03/25/2021 15:00 Soil Pile W 2101841-12 Solid Solid 03/25/2021 11:50 03/25/2021 15:00 Soil Pile E 2101841-13 Solid Solid 03/25/2021 12:10 03/25/2021 15:00 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX:_(805J 925-3376 Page 2 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Batch Preparation Analysis Batch ID Preparation Date/Time Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List B1('0798 03/25/2021 17:29 STLC Metals by ICP 6010B STLC BID0007 04/01/2021 09:01 STLC Metals Extraction STLC Metals Extraction B 1('0891 03/30i2021 10:02 TCLP Metals by ICP 601013 TCLP B 1 D01 12 04/06/2021 10:26 TCLP Metals Extraction TCLP Metals Extraction B 1 C0898 03/30/2021 12:22 Total Metals by CVAA Mercury Total EPA 7471 A B I C0807 03/26/2021 07:43 Total Metals by ICP 6010B Total B 1 C'0810 03/26/2021 08:36 Volatile Organic Compounds by GUMS 826013 Full List BIC0815 03/26/2021 09:17 8260B Full List B 1 C0817 03/26/2021 11:40 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline B1('0802 03/26/2021 05:22 8015 TPH-Gasoline BIC0804 03/26/2021 05:26 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by : Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mgtkg 1 B 1('0807 03/26/21 14:37 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgrkg 1 B1('0810 03/26/21 13:30 EPA 601OB Arsenic 8.9 2.0 Barium 150 0.98 Bervllium 0.61 0.49 " Cadmium ND 0.24 Chromium 51 0.49 N-02 Cobalt 17 0.49 Copper 28 0.98 Lead 9.1 0.49 Molybdenum 2.6 0.49 Nickel 76 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 39 2.0 Zinc 32 2.0 STLC Metals by ICP Chromium 0.13 (l.1() mg%1. 2 B1D0007 04/01/21 14:45 STLCILPA6010B Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.9 mg/kg I BIC'0802 03/26/21 10:47 EPA 8015M R-117 Surrogate: 4-Bromglluoroben:ene 103 3b (31 - 168) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805 925-3376 Page 4 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 77:Note] Semi -Volatile Organic TPH by GC/FID TPII Diesel (Cl 3-C22) ND 10 TPH Motor Oil (C23-C40) ND 50 Surrogate o-Terphem•1 107 `ib mg/kg I BIC0798 03/26/2107:48 GPA8015M (65-133) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID : Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mglkg 1000 BIC0815 03/2621 11:52 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 C hlorobenzcnc ND 1.2 Chloroethane ND 1.2 Chloroform ND L2 Chloroniethane ND 1.2 2-Chlorotolnene ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 " 1.2-Dibronioethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichloroben7ene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichloroben7ene ND 1.2 Dichlorodifluoro nethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND 1.2 " cis-L2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 " 2.2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 " cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbcnzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 6 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Heating Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank N Wall Sampled : 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mgrkg 1000 B1('0815 03/262111:52 EPA826013 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 1, 1, 1 .2-Tetrachloroethane ND 1.2 1.1.2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcnc (PC E) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzenc ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1. 1, 1 -Trichloroethane ND 1.2 1,12-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorotluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND L2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surr(Igate: 1)ibronwlhrurrmrethane 97 ; ( 75 - 122 ) Surrogate: Toluene-dN 92'% ( 66 - 128 ) Surrogate: 4-Brunurlltrurubcu_c>uc 92 40 ( 76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 7 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.086 mgtkg 1 BIC0807 03/20/2114:39 EPA 7471A Total Metals by ICP Antimony ND 2.4 mg`kg 1 B I C 0810 03/26/21 13:33 EPA 6010B Arsenic 4.1 2.0 Barium 11 0.98 Beryllium ND 0.49 Cadmium ND 024 Chromium 9.0 0.49 Cobalt 1.4 0.49 Copper 3.5 0.98 Lead 2.5 0.49 Molybdenum 3.3 0.49 Nickel 6.8 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 6.3 2.0 Zinc 9.7 2.0 Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12') ND 4.5 mg/kg I BIC0802 03/26`21 11:13 EPA 8015M R-07 Surrogate: 4-BromoJhmroben_ene 103 "o (31 - 168) " 11 Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 10 mgIg I B1C0798 03/26/21 10:07 EPA 8015M TPH Motor Oil (('23-C40) ND 50 " " " " Surrogate: o-Terphen.vl 106 4 , (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: (805) 925-3376 Page 8 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by : Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 BIC0815 03/26/21 12:17 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzene ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzenc ND 1.2 1,3-Dichlorobenzenc ND 1.2 I A-Dichlorobenzenc ND 1.2 Dichlorodifluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 LI-Dichloroethene ND L2 cis- 1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 22-Dichloropropane ND 1.2 1. 1 -Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 " Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 9 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples = Sample ID : Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-0 7 Ilexachlorobutadiene ND 1.2 mg/kg 1000 B1('0815 03/20/21 12:17 EPA8260B 4-Isopropyl Toluene ND 1.2 " " Isopropylbenzene ND 1.2 " " Methylene chloride ND 1.2 " Naphthalene NI) 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachlorocthane ND 1.2 1,1,2,2-1'etrachlorocthane ND 1.2 Tetrachlorocthane (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene NI) 1.2 1,2,4-Trichlorobenzene NI) 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethanc ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene NI) 1.2 13.5-Trimethylbenzene ND 1.2 Vinvl chloride ND 1.2 Xylenes (total) ND 1.2 " Surrogate: Uibromofhuoroinethanr 92 "/n ( 7-5- 122) 11" Surrogate: Toluene-l8 S4 % (66 - 1 2S) Surrogate: 4-Bromoflao» oben_ene 92 ifi (76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 10 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury NJ) 0.092 mg/kg I BIC0807 03/26/21 14:41 EPA 7471A Total Metals by ICP Antimony ND 2.4 mglkg I BIC0810 03/26/21 13:36 EPA 601OB Arsenic 4.2 1.9 Barium 140 0.95 Bervllium 0.51 0.47 Cadmium NI) 0.24 Chromium 52 0.47 Cobalt 16 0.47 Copper 23 0.95 Lead 7.0 0.47 Molybdenum ND 0.47 Nickel 72 0.47 Selenium ND 1.9 " Silver ND 0.47 Thallium ND 0.95 Vanadium 33 1.9 " Zinc 20 1.9 STLC Metals by ICP Chromium ND 0.10 ms/L 2 B I D0007 04/01 /21 14:48 STLC/EPA 601 OB Volatile Organic TPH by GC/FID N-02 TPII Gasoline (('5-C12) ND 4.6 mg/kg 1 BIC0802 03/26'21 11:39 EPA 8015M R-07 Surrogate: 4-Bromo/luoroben_ene 104 % (31 - 168) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 11 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TPII Diesel (03-('22) ND 9.9 TPlI Motor Oil (('23-C40) ND 50 Surrogate: o-Tetphen.vl 10S V. mg/kg I B1('0798 03/26/2108:02 EPA8015M (65-133) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 12 of 79 WAKM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by : Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mglkg 1000 B1('0815 03/26/21 12:43 EPA8260B Bromobenzene ND 1.2 " Broniochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene NI) 1.2 tent-Butylbenzene NI) 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc NI) 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-C'hlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromnochloromethane ND 1.2 1.2-Dibromo-3-chloropropanc ND 1.2 I.2-Dibromoelhane(EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND L2 1,3-Dichlorobenzene ND 1.2 14-Dichlorobenzene ND 1.2 Dichlorodi'fluoromethane ND 1.2 " 1,1-Dichloroethane NI) 1.2 1,2-Dieliloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1,2-Dichlorocthene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 13 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 IIexachlorobutadiene ND 1.2 mg/kg 1000 B I ('0815 03/26/21 12:43 EPA 9260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 L1,2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzcnc ND 1.2 1,2,4-Trichloroben7ene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorotluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1,2.4-Trimethylbenzene ND 1.2 1,3,5-Triniethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibronrolluoronuthiurr 9 75 - 122) Surrogate: Tolucnc-dR 95 % ( 66 - 128 ) Surrogate: 4-BromoJhroroben-cnc 90 45 1 76 - 122 I The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 14 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportI Analytical i Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg 1 BIC0807 03/26/2114:44 EPA 7471A Total Metals by ICP Antimony ND 2.3 mg,'kg 1 B1('0810 03/26/21 13:38 EPA 601OB Arsenic 2.6 1.8 " Barium 5.8 0.92 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 6.9 0.46 Cobalt 0.92 0.46 Copper 1.9 0.92 Lead 3.7 0.46 Molybdenum 2.6 0.46 Nickel 4.1 0.46 Selenium ND 1.8 " Silver ND 0.46 " Thallium ND 0.92 Vanadium 4.6 1.8 Zinc 6.8 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C 12) 35 5.1 nigIg I B 1('0802 03/26/21 12:05 EPA 8015M Surrogate: 4-Bronwffit rohenzene 148 ";, (31 - 168) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Terphettrl 17 9.9 mglkg 1 72 50 " " 107 'b (65 - 733 ) BIC0798 03/26 21 11:03 EPA 8015M D-04 " D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 15 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID : Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg/kg 1000 B1('0815 03/26/21 13:08 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoform ND 1.2 Brotnomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 12 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronho-3-chloropropane ND 1.2 " 12-Dibromoethane (1:)B) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenz_ene ND 1.2 1,3-Dichlorobcnzenc ND 1.2 IA-Dichlorobcnzenc ND 1.2 Dichloroditluoromethane ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND 1.2 " cis- 1,2-Dich loroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2.2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-l3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Iiexachlorobutadiene ND 1.2 mgtkg 1000 BIC0815 03/26/21 13:08 ITA8260B 4-Isopropyl Toluene ND 1.2 " Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 I . 1, 1,2-1'etrachloroethane ND 1.2 1,L2.2-Tetrachloroethane ND 1.2 Tetrachlorocthene (PCk) ND 1.2 Tolucnc ND 1.2 1,2.3-Trichlorobenzenc ND 1.2 " 1,14-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 " Trichloroethane (TC'E) ND 1.2 Trichlorotluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2A-Trimethylbenzene ND 1.2 13.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylcncs (total) ND 1.2 " Surrogate: Uihronudlrwnmtet}tmtc 95 Y„ ( 75 - 122 ) Surrogate: Toluene-dh 95 c'.' ( 66 - 12S ) Surrogate: 4-Br(»no/lnorohen_ene 92 1'n ( 76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 17 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportI Analytical t Sample ID : Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mg'kg I B1('0807 03/26/21 14:46 EPA 7471A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B 1 C0910 03/20/21 13:41 EPA 601(1B Arsenic 5.4 1.9 Barium 32 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 15 0.47 " Cobalt 4.3 0.47 Copper 11 0.93 Lead 8.3 0.47 Molybdenum 2.9 0.47 Nickel 19 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 13 1.9 Zinc 19 L9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 35 4.9 mg/kg 1 BIC0802 03/26/21 12:31 EPA 8015M Surrogate: 4-Bromo/laoroben_ene 145'% (31 - 16S) 11" 11 Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Tcrphen 1 11 10 in/kg I 110 50 " " 106`10 (65-133) BIC0798 03/26'2111:31 EPA 8015M D-04 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 18 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report t Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by: Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mg�kg 1000 B1('0815 03/26/21 13:34 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 l3romofortn ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzenc ND 1.2 Chlorocthanc ND 1.2 Chlorolonn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 " 1.2-Dibromoethane (ED13) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichloroditluoromcthanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethenc ND 1.2 cis-1.2-Dichlorocthane ND 1.2 trans-1,2-Dichloroethane ND 1.2 1,2-Dichloropropane ND 1.2 1,3-1)ichloropropane ND 1.2 22-Dichloropropane ND 1.2 " 1,1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Iithylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.cornWeports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 19 of 79 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 I i exa ch I orobutadi en c ND 1.2 mg/kg 1000 B1('0815 03/26/2113:34 EPA8200B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 " 1.1,2,2-Tetrachloroethane ND 1.2 Tetrachloroethane WCE) ND 1.2 Toluene ND 1.2 1,23-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trieliloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1 2.3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dibrrnnolhmromethane 95 `N, ( 75 - 122 ) Surrogate: Toluene-c18 86 'Ni, (66 - 12b') " Surrogate: 4-Broniglluoroben-ene 94 4 (76 - 122) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl1ent.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 20 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank Bottom W. End Sampled: 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 B 1('0807 03/26/21 14:48 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B 1('0810 03/26/21 13:44 EPA 6010B Arsenic ND 2.0 Barium 9.9 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 8.0 0.49 Cobalt 1.2 0.49 Copper 1.6 0.98 " Lead 3.4 0.49 Molybdenum 1.1 0.49 Nickel 4.7 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 5.9 2.0 Zinc 7.9 2.0 Volatile Organic TPH by GC/FID TP11 Gasoline (('5-C12) 6.1 4.5 mgtkg 1 B1('0804 03/26/21 10:55 EPA 9015M Surrogate: a-Brontufluoroben_cne 108 "o (31 - 168) 11" 11 Semi -Volatile Organic TPH by GC/FID TPH Diesel (('13-C22) ND 9.9 mg�kg I B1C0798 03/26/21 10:21 EPA 8015M TPH Motor Oil (('23-('40) ND 50 " " " " " Surrogate: o-Tetrhenrl 106 'Sb (65 - 1.33) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 79 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B I C0815 03/26/21 13:59 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tent -Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 C'hlorobenzene ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 " 4-Chlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (ED13) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 " 1,4-Dichlorobenzene ND 1.2 " Dichloroditluoroniethane ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 " trans-1,2-Dichloroethene ND 1.2 I.2-Dichloropropane ND 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Dichloropropene ND 1.2 cis- 1.3-I)ichloropropenc ND 1.2 trans-1,3-Dichloropropene ND 1.2 Fthylbcnzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hex achl OTobuladlene ND 1.2 mglkg 1000 BIC0815 03/26/21 13:59 EPA8260B 4-1sopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1,1.2,2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCPs) ND 1.2 Toluene ND 1.2 1.2,3-Trichlorobenzcne ND 1.2 1,2.4-Trichloroben7ene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 1,3,54'rimethylbeuzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibrumo)lttoro ncthtntc 93 % ( 75 - 122) Surrogate Toluene-d8 SS' I! "I ( 66 - 128 ) " Surrogate. 4-Bromn/luoroben_enn 94'/ ( 76- 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 23 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mglkg 1 B 1 C0807 03/26/21 14:54 TPA 7471 A Total Metals by ICP Antimonv 8.2 2.4 mg/kg I B1('0810 03/26/21 13:47 EPA 601OB Arsenic 8.9 1.9 "11" Barium 260 0.96 "11" " Beryllium ND 0.48 " " Cadmium ND 0.24 " " Chromium 55 0.48 " N-02 Cobalt 12 0.48 " " Copper 120 0.96 Lead 550 0.48 " " " " N-02, N-03 Molybdenum 1.1 0.48 Nickel 150 0.49 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 33 1.9 Zinc 720 1.9 STLC Metals by ICP Chromium 0.34 0.10 mg/L 2 B 1 D0007 04/01 /21 14:40 STLC/F.PA 6010B Lead 56 0.10 N-07 TCLP Metals by ICP Lead 0.25 0.050 mg/L I B 1 D0112 04/06/21 12:18 EPA 1311 /FPA 6010B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria. CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 24 of 79 6 �NM 16 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/FID TPH Gasoline (("'5-02) ND 4.9 mg/kg 1 B1('0904 03/2621 11:52 EPA 8015M R-07 Surrogate: 4-Bromo/luorohenzene lull % (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 71 40 mg/kg 4 BIC0798 03/26'21 11:59 EPA 8015M D-04 TPH Motor Oil (C23-C40) 520 200 1. 11 11 .1 11D-04 Surrogate: o-k1phenYl 108 % (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 25 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg,kg 1000 BIC0815 03/26/21 14:25 EPA9260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Bromoform ND 1.2 Bromotnethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 " Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-0hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibrotno-3-chloropropane ND 1.2 I.2-Dibromoethane (ED13) ND 1.2 Dibromomethane ND 1.2 " 1.2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 ]A-Dichlorobenzene ND 1.2 Dichlorodilluoromethanc ND 1.2 I.1-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane NI) 1.2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis- 1,3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 26 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mgIg 1000 B1('0815 03/26/21 14:25 EPA 8260B 4-1sopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1. 1.2-Tetrachloroethane ND 1.2 I.1.2.2-Tetrachloroethane ND 1.2 " Tctrachlorocthcne IPCE) ND 1.2 " Toluene ND 1.2 1,2,3-Trichlorobcnzene ND 1.2 1,2A-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorolluoromethane ND 1.2 " 1.2.3-Trichloropropane ND 1.2 1.2,4=1'rimethylbenzene Nl) 1.2 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Uihrunui/hun'oanethunc 97 ". ( 75 - 122) " Surrogate: Toluene-dS 90 if, ( 66 - 128) " Surrogate: 4-Brom0/Iuorobetr_-rene NR 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mg'kg I B 1 C0807 03/20/21 14:56 EPA 7471 A Total Metals by ICP Antimony ND 2.4 ing;kg 1 BIC0810 03/26/21 13:50 EPA6010B Arsenic 4.1 1.9 Barium 180 0.96 Beryllium 0.53 0.49 Cadmium ND 0.24 Chromium 78 0.48 Cobalt 16 0.48 Copper 31 0.96 Lead 37 0.48 Molybdenum ND 0.48 Nickel 100 0.48 Selenium I N D 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 47 1.9 Zinc 69 1.9 STLC Metals by ICP Chromium 0.25 0.10 mg/L 2 BID0007 04/01/21 14:51 STLC/EPA6010B Volatile Organic TPH by GC/FID N-02 TPH Gasoline (C5-('12) ND 4.7 mg/kg I B1('0804 03/26/21 12:20 EPA 8015M R-07 Sm•rogate: d-BromoJTnorobenzene 107 " (31 - 168 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by : Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi -Volatile Organic TPH by GC/FID TP11 Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-TerphenVl 27 9.9 tng'kg 1 B 1 C0798 03/26/21 13:02 EPA 8015M D-06 610 50 107"/„ (65-133) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 29 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg%kg 1 B1C0817 03/26/21 13:46 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodiehloromethane ND 0,0050 Bromofonn ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobcnzene ND 0.0050 Chlorocthanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 " 1.2-Dibromo-3-chloropropane ND 0.0050 " 1.2-Dibromoethane (ED13) ND 0.0050 Dibronxnnethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 " I A-Dichlorobenzene ND 0.0050 Dichloroditluoromethanc ND 0.0050 " 1, 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 " trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 12-Dichloropropane ND 0.0050 1,1-Dichloropropene ND 0.0050 cis-I.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 Elhvlbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 30 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID: 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Ilexachlorobutadiene ND 0.0050 mg/kg 1 B1('0817 03/26/21 13:46 EPA 8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbeuzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1, 1, 1,2-Tetrachloroethane ND 0.0050 1,1.2.2-1'etrachloroethane ND 0.0050 " Tetrachloroethene tPCE) ND 0.0050 " Toluene ND 0.0050 1,2,3-Trichlorobenzene ND 0.0050 1.2,4-Trichlorobenzene ND 0.0050 1. 1, 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethane (TCE) ND 0.0050 " Trichlorotluoromethane ND 0.0050 12.3-Trichloropropane ND 0.0050 1.2.4-Trimethylbenzene ND 0.0050 13,5=Riniethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylcncs (total) ND 0.0050 Surrogate: Uibronwlluorornethane 94 `% ( 75 - 122 I " Surrogate. Toluenc,48 89 9i, (66 - 12S) " Surrogate 4-13ronu,/luarubc p_cpe 89 4' ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 805 925-3376 Page 31 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury 0.14 0.095 mglkg 1 B1C0807 03/26/21 14:58 EPA7471A Total Metals by ICP Antimony ND 2.4 mg/kg 1 BIC0810 03/20/21 13:52 EPA6010B Arsenic 5.9 1.9 Barium 170 0.97 Bervllium 0.50 0.49 Cadmium ND 0.24 Chromium 41 0.49 Cobalt 16 0.49 Copper 27 0.97 Lead 10 0.49 Molybdenum ND 0.49 Nickel 38 0.49 Selenium ND L9 Silver ND 0.49 "Thallium ND 0.97 Vanadium 33 1.9 Zinc 27 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) N'D 4.7 nualkg I BIC0804 03/26/21 12:49 EPA 8015M R-07 Surrogate: 4-Bromo/hmrnhenzene 96 %o (31 - 168) " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C 13-C22) ND 10 mg/kg I B I C0798 03/26/21 10:49 EPA 8015M TPH Motor Oil (C23-C40) 85 50 " " " " 11 Surrogate: o-Terphern'l 105 �b (65 - 133) 11 " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 32 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID: Control Sampled : 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID : 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg/kg 1 B 1 C0R 17 03/26/21 14:44 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromofonn ND 0.0050 Bromomethanc ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 " Chlorobenzenc ND 0.0050 " Chloroethanc ND 0.0050 Chloroform ND 0.0050 C hloromethane ND 0.0050 2-Chlorotoluenc ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 1.2-Dibromoethane (EDB) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1,3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 Dichloroditluoromethanc ND 0.0050 1J-Dichloroethene ND 0.0050 " 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0,0050 trans-1,2-Dichloroethene ND 0.0050 1.2-Dichloropropane ND 0.0050 1.3-Dichloropropane ND 0.0050 2.2-Dichloropropane ND 0.0050 " 1,1-Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene N'D 0.0050 F.thylbenzenc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 33 of 79 C A &M. Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by : Lab ID : 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) 11exachi orobutadiene ND 0.0050 mglkg 1 B1('0817 03/26/21 14:44 EPA8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methvlene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1.1,2-Tetrachloroethane ND 0.00.50 1,1,2.2-Tetrachloroethane ND 0.0050 Tctrachlorocthcne (PCE) ND 0.0050 " Toluene ND 0.0050 1,2.3-Trichlorobenzcnc ND 0.0050 1,2,4-Trichlorobenrene ND 0.0050 1, 1, 1 -Trichloroethane ND 0.11115() 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1.2.3-Trichloropropane ND 0.0050 1,2.4-Trimethylbenzene ND 0.0050 1,3,5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 X_vlcncs (total) ND 0.0050 Surrogate: Dihronuillaoronuechaite° 93 N, ( 75 - 122 ) Surrogate. Toluene-d8 95 `%b ( 66 - 128) Surrogate: 4-BromnJluurube'n_ene 98 4„ ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 34 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical t Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by : Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mg/kg I BIC'0807 03/26/21 15:00 EPA 7471A Total Metals by ICP Antimony ND 2.5 mg/kg I BI C0810 03/26/21 13:55 EPA 601 OB Arsenic 3.6 2.0 " Barium 13 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 11 0.50 Cobalt 1.9 0.50 " Copper 5.3 1.0 Lead 4.3 0.50 Molybdenum 2.5 0.50 Nickel 9.0 0.50 " Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 8.4 2.0 Zinc 8.8 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-Cl2) 42 4.9 mg/kg 1 BIC0804 03/26/21 13:17 EPA 8015M Surrogate: 4-BromoJluorohen_ene 196 °ter, (31 - 168) S-02 Semi -Volatile Organic TPH by GC/FID TPH Diesel (CI 3-C221 ND 9.9 mg/kg I BIC0798 03/26,'21 10:35 EPA8015M TPH Motor Oil (C23-C40) 52 50 " " " " " Surrogate: u-Teiphenrl 106';;> (65 - 133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 35 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report i Sample ID: Soil Pile N Sampled : 03/25/21 11:40 Matrix: Solid Sampled by : Lab ID : 2101841-10 Field Data: NA I Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mg kg 1 B1('0817 03/26/21 12:49 EPA 8260B Bromobenzene ND 0.045 Bromochloromethane ND 0.045 Bromodichloromethanc ND 0.045 Bromoform ND 0.045 Bromomethane ND 0.045 n-Butvlbenzene 0.22 0.045 sec-Butvlbenzene 0.11 0.045 tert-Butylbenzene ND 0.045 " Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 Chloroethane ND 0.045 Chloroform ND 0.045 Chloromethane ND 0.045 2-Chlorotoluene ND 0.045 4-Chlorotoluene ND 0.045 " Dibromochloromethane ND 0.045 " 1.2-Dibromo-3-chloropropanc ND 0.045 1.2-Dibromoethane (EDB) ND 0.045 Dibronwmethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichloroben7ene ND 0.045 1.4-Dichlorobenzene ND 0.045 Dichloroditluoromethanc ND 0.045 1, 1 -Dichlorocthane ND 0.045 1,2-Dichloroctlhane ND 0.045 1,1-Dichloroethene ND 0.045 " cis-1,2-Dichloroethene ND 0.045 " trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 13-Dichloropropane ND 0.045 2.2-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis-L3-Dichloropropene ND 0.045 trans-1,3-Dichloropropene ND 0.045 Ethylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID : Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by : Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlombutadiene ND 0.045 mg/kg 1 B1('0817 03/26/21 12:49 EPA8260B 4-Isopropyl Toluene ND 0.045 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene 0.15 0.045 " Styrene ND 0.045 1,1,1.2-Tetrachlomethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0.045 Tetrachloroethene (PCE) ND 0_045 Toluene ND 0.045 1,23-Trichlorobenzene ND 0.045 " 1.2,4-Trichlorobenzene ND 0.045 1, 1 _ I -Trichloroethane ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethane (TCE) ND 0.045 Trichlorotluoromethane ND 0.045 1,2.3-Trichloropropane ND 0.045 1,2.4-Trimcthylbenzenc ND 0.045 I.3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: Dibromalluoromethane 92 `! ( 75. 1 22 ) Surrogate: Te)luene48 97 ` , ( 66 t.128) " Surrogate: d-Bromq luorobenzene 99 ""I ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by : Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mg/kg 1 B 1 ('0807 03/26/21 15:02 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mgtkg 1 B I C0810 03/26/2) 14:06 EPA 6010B Arsenic 4.5 2.0 Barium 47 1.0 Beryllium ND 0.50 Cadmium ND 0.25 Chromium 18 0.50 Cobalt 3.6 0.50 Copper 9.8 1.0 Lead 16 0.50 Molybdenum 2.1 0.50 Nickel 36 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 15 2.0 Zinc 29 2.0 Volatile Organic TPH by GC/FID TPII Gasoline (C5-C12') ND 4.4 mg/kg 1 BIC0804 03/26/21 13:46 EPA 8015M R-07 Sarrogute: 4-Bromo/Ittoroben_ene 100 % (31 - 108 ) 11 Semi -Volatile Organic TPH by GC/FID Tell Diesel (('13-('22) ND 10 mg/kg 1 B1C0798 03/26/21 12:27 EPA 8015M TPH Motor Oil (C23-C40) 260 50 " " " Surrogate: o-Tetphemd ION 1So (65 - 133) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 38 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical i Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0049 mgtkg I B 1 C0817 03/20/21 15:13 EPA 826013 Bromobenzene ND 0.0049 Bromochloromethane ND 0.0049 Bromodichloromethane ND 0.0049 Bromoform ND 0.0049 Bromomethane ND 0,0049 n-Butvlbenzene ND 0.0049 " sec-Butylbenzene ND 0.0049 tert-Butylbenzenc ND 0.0049 Carbon tetrachloride ND 0.0049 Chlorobenzene ND 0.0049 Chloroethane ND 0.0049 Chloroform ND 0.0049 Chloromethane ND 0.0049 2-Chlorotoluene ND 0.0049 4-Chlorotoluene ND 0,0049 Dibromochloromethane ND 0.0049 1.2-Dibromo-3-chloropropane ND 0.0049 1,2-Dibromoethane tEDB1 ND 0.0049 Dibromomethane ND 0.0049 1,2-Dichloroben7enc ND 0.0049 1.3-Dichlorobenzene ND 0.0049 1,4-Dichlorobenzenc ND 0.0049 Dichloroditluoromcthane ND 0.0049 1, 1 -Dichloroethane ND 0.0049 1,2-Dichloroethane ND 0.0049 " 1, 1 -Dichloroethene ND 0.0049 cis-1.2-Dichloroethene ND 0.0049 trans-1,2-Dichloroethene ND 0.0049 1,2-Dichloropropane ND 0.0049 13-Dichloropropane ND 0.0049 2.2-Dichloropropane ND 0.0049 1, 1 -Dichloropropene ND 0.0049 cis-1.3-Dichloropropene ND 0.0049 trans-1,3-Dichloropropene ND 0.0049 Ethylbcnzene ND 0.0049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by : Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Iiexachlorobutadiene ND 0.0049 mg'kg 1 B1C0817 03/26/21 15:13 EPA8260B 4-Isopropyl Toluene ND 0.0049 Isopropylbenzene ND 0.0049 Methylene chloride ND 11 0049 Naphthalene ND 0.0049 n-Propylbenzene ND 0.0049 Styrene ND 0.0049 1, 1, 1,2-Tetrachloroethane ND 0.0049 1,1.2.2-Tetrachloroethane ND 0.0049 Tetrachloroethene (PCE) ND 0.0049 ToILIc11C ND 0.0049 1,2,3-Trichlorobenzene ND 0.0049 1.2.4-Trichloroben7ene ND 0.0049 I,1,1-Trichloroethane ND 0.0049 1.1.2-Tricliloroethane ND 0.0049 Trichloroethene (TCE) ND 0.0049 " Trichloroiluoromethane ND 0.0049 1,2,3-Trichloropropane ND 0,0049 12,4-Trimethylbenzene ND 0.0049 1,3,5=Gimethylbenzene ND 0.0049 Vinyl chloride ND 0.0049 Xylenes (total) ND 0.0049 Sunngate: Uibramolluoromethanc 91 /, ( 75 - 122 ) Surrogate: Toluene-dN 95 '<i, ( 66 - 128) Surrogate: 4-Bromo/luoroben_cne 97 % (76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) Surrogate: 4-Bromolluoroberr-ene Semi -Volatile Organic TPH by GC/FID ND 0.097 mgtkg 1 Bl('0807 03/20121 15:04 EPA 7471A ND 2.3 mg/kg 1 BIC0810 03/26/21 14:09 EPA601013 5.6 1.9 23 0.93 ND 0.47 ND 0.23 14 0.47 2.5 0.47 6.8 0.93 7.3 0.47 3.7 0.47 11 0.47 ND 1.9 ND 0.47 ND 0.93 15 1.9 15 1.9 ND 4.7 mglkg 1 BIC0804 03/26/21 14:14 EPA8015M R-07 103% (31-168) TPII Diesel (C 13-('22) ND 9.9 mgIg 1 TPH Motor Oil (C23-C40) 75 50 1." Surrogate: o-T67)henYl 107'%h (65 - 133 ) B 1 C0798 03126'21 1 1:17 EPA 8015M D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 41 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report Sample ID : Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by : Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mgtkg 1 BIC1817 03/26/2115:43 EPA8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 " Bromodichloromethane ND 0.0050 Bromoform ND 0,0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzenc ND 0.0050 " Carbon tctracliloridc ND 0.0050 " Chlorobenzene ND 0.0050 Chloroethanc ND 0.0050 Chloroform ND 0.0050 Chlommethane ND 0.0050 2-Chlorotoluenc ND 0.0050 4-Chloroioluene ND 0.0050 " Dibromochloromethane ND 0.0050 11-Dibromo-3-chloropropane ND 0.0050 12-Dibromoethane (EDB) ND 0.0050 Dibromontethane ND 0.0050 1,2-Dichlorobcnzenc ND 0.0050 1.3-Dichlorobcnzenc ND 0.0050 IA-Dichlorobcnzenc ND 0.0050 Dichloroditluoromethanc ND 0.0050 1, 1 -Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethane AND 0.0050 cis-1,2-Dichloroethenc ND 0.0050 trans-1,2-Dichloroethane ND 0.0050 " 1,2-Dichloropropane ND 0.0050 13-Dichloropropane ND 0.0050 2.2-Dichloropropane ND 0.0050 1,1-Di chloropropene ND 0.0050 cis-13-Dichloropropene ND 0.0050 trans-1,3-Di chloropropene ND 0.0050 Ethylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 5 925-3376 Page 42 of 79 1611400 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by : Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Tlexachlorobutadiene ND 0.0050 mg/kg 1 BIC0817 03/26/21 15:43 ITA 8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.0050 1,1.2,2-Tetrachloroethane ND 0.0050 Tctrachlorocthcnc (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobcn7enc ND 0.0050 1,2.4-Trichlorobenzene ND 0.0050 " 1, 1, 1 -Trichloroethanc ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethenc (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2,3-Trichloropropane ND 0.0050 " 1,2,4-Trimethylbenzene ND 0.0050 1,3.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylcncs (total) ND 0.0050 Surrogate: Dibrcnnolluoromethmte 91 `.'-„ ( 75 - 122 ) Surrogate: Toluene -de 94 9i, ( 66 - 128 ) Surrogate: 4-Bromo/hroroben_ene 97'N, ( 76 - 12 2 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 43 of 79 WA Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ReportAnalytical t Sample ID : Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mg/kg 1 B 1('0807 03/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I C 0810 03 /26:21 14:1 1 EPA 601 OB Arsenic 2.0 19 Barium 5.5 0.96 Beryllium ND 0.48 Cadmium ND 0.24 Chromium 6.4 0.49 Cobalt 0.76 0.48 Copper 1.8 0.96 Lead 3.7 0.49 Molybdenum 1.6 0.48 Nickel 3.9 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 " Vanadium 5.2 1.9 " Zinc 5.2 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.9 mg/kg 1 BIC0804 03/26/21 14:42 EPA 8015M R-07 Surrogutc: 102 % (31 - 16S ) Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-('22) ND 10 mg'kg 1 B1C0798 03126 21 11:45 EPA 8015M TPH Motor Oil (C23-C40) 120 50 " " " " Surrogate: o-Tcc1/hc n.1,1 107'l0 (65 - 133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples El Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by : Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mgticg 1 B I C0817 03/26/21 16:12 EPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Brotnodichloromethane ND 0.0050 Bromoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 " sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 Chloroethane ND 0.0050 Chloroform ND 0.0050 " Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-C'hlorotoluene ND 0.0050 " Dibromochloromethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 " 1.2-Dibromoethane (EDB) ND 0.0050 Dibromomethane ND 0.0050 1,2-Dichlorobenzcne ND 0.0050 " 1.3-Dichlorobenzcne NI) 0.0050 IA-Dichlorobenzcne ND 0.0050 Dichloroditluoromcthane ND 0.0050 l,l-Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 1,1-Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 trans-1.2-Dichloroethene NI) 0.0050 1,2-Dichloropropane ND 0.0050 " 13-Dichloropropane ND 0.0050 2,2-Dichloropropane NJ) 0.0050 1.1-Dichloropropene NI) 0.0050 cis-1.3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene NI) 0.0050 Fthylbenzene ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 45 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Analytical Report for Samples Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) Hexachlorobutadiene ND 0.0050 mgtkg I B1('0817 03/26/21 16:12 EPA 8260B 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1_12-Tetrachloroethane ND 0.0050 1,12,2-Ictrachloroethane ND 0.0050 Tetrachlorocthcne dICE) ND 0.0050 Toluene ND 0.0050 1.2,3-Trichlorobcnzcne ND 0.0050 1,2,4-Triehlorobenzene ND 0.0050 1, 1. 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 Trichloroethane (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2.3-Trichloropropane ND 0.0050 1,24-Trimethylbenzene ND 0.0050 " 1,3,5-Trimethyl benzene ND 0.0050 Vinyl chloride ND 0.0050 Xylcnes (total) ND 0.0050 Surrogate: Dibro»tglluorrmrethrr»(, 91 % ( 75 - 122) Surrogate: Toluene-(18 95 % ! 66- 128 ) Surrogate: 4-Bur» nn/humvhcttcette 97 % ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 46 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0807 - EPA 7471A Preparation: EPA 7471A Prep 03/26/21 07:43 Blank (B1C0807-BLK1) Analyzed: 03/26/21 13:21 Mercury ND 0.10 mgkg LCS (BlC0807-BS1) Analyzed: 03/26/21 13:17 Mercury 0.792 0.10 mg/kg 0.833 95 85-115 LCS Dup (B1C0807-BSD1) Analyzed: 03/26/21 13:19 Mercury 0.793 0.10 mg/kg 0.833 94 85-115 1 20 Duplicate (BIC0807-DUPl) Source: 2101842-02 Analyzed: 03/26/21 13:25 Mercury 0.0556 0.096 mg/kg 0.0554 0.3 20 Matrix Spike (BlC0807-MS1) Source: 2101842-02 Analyzed: 03/26/21 13:27 Mercury 0.855 0.096 mg/kg 0.796 0.0554 100 75-125 Matrix Spike Dup (B1C0807-MSDl) Source: 2101842-02 Analyzed: 03/26/21 13:29 Mercury 0.750 0.087 mg -'kg 0.727 0.0554 96 75-125 13 20 Post Spike (BlC0807-PS1) Source: 2101842-02 Analyzed: 03/26/21 13:31 Mercury 5.17 ug/L 5.00 0.347 97 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 47 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total' - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Blank (B1C0810-BLK1) Analyzed: 03/26/21 12:16 Antimony ND 2.5 mgIg Arsenic ND 2.0 Barium ND 1.0 Beryllium ND 0.50 Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " Nickel ND 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 LCS (B1C0810-BSI) Analyzed: 03/26/21 12:40 Antimony 100 2.5 mg/kg 100 100 80-120 Arsenic 101 2.0 100 101 80-120 Barium 102 1.0 100 102 80-120 Beryllium 103 0.50 100 103 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 103 0.50 100 103 80-120 Cobalt 103 0.50 100 103 80-120 Copper 103 1.0 100 103 80-120 Lead 103 0.50 100 103 80-120 Molybdenum 100 0.50 100 100 80-120 Nickel 103 0.50 100 103 80-120 Selenium 100 2.0 100 100 80-120 Silver 5.Oo 0.50 5.00 101 80-120 Thallium 104 LO 100 104 80-120 Vanadium 100 2.0 100 100 80-120 Zinc 103 2.0 100 103 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 48 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 ControlTotal Metals by 1CP - Quality Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 LCS Dup (B1C0810-BSDI) Analyzed: 03/26/21 12:43 Antimony 101 2.5 mgtkg 100 101 80-120 0.7 20 Arsenic 102 2.0 100 102 80-120 0.9 20 Barium 102 1.0 100 102 80-120 0.3 20 Beryllium 104 0.50 100 104 80-120 0.9 20 Cadmium 103 0.25 100 103 80-120 0.5 20 Chromium 104 0.50 100 104 80-120 1 20 Cobalt 104 0.50 100 104 80-120 0.5 20 Copper 104 LO 100 104 80-120 0.9 20 Lead 104 0.50 100 104 80-120 0.8 20 Molybdenum 101 0.50 100 101 80-120 0.9 20 Nickel 104 0.50 100 104 80-120 0.5 20 Selenium 101 2.0 100 101 80-120 0.7 20 Silver 5.16 0.50 5.00 103 80-120 2 20 Thallium 104 H) 100 104 80-120 0.3 20 Vanadium 102 2.0 100 102 80-120 1 20 Zinc 103 2.0 100 103 80-120 0.5 20 Duplicate (BlC0810-DUPl) Source: 2101840-03 Analyzed: 03/26/21 13:06 Antimony ND 2.4 mg/kg 0.966 20 Arsenic 2.64 1.9 3.12 17 20 Barium 118 0.95 116 2 20 Beryllium ND 0.47 ND 20 Cadmium ND 0.24 ND 20 Chromium 16.3 0.47 17.6 8 20 Cobalt 3.67 0.47 4.26 15 20 Copper 9.50 0.95 8.79 8 20 Lead 6.24 0.47 5.56 12 20 Molybdenum 1.46 0.47 1.27 14 20 Nickel 20.8 0.47 23.4 12 20 Selenium ND 1.9 ND 20 Silver ND 0.47 ND 20 Thallium ND 0.95 ND 20 Vanadium 15.0 1.9 15.4 3 20 Zinc 34.0 1.9 29.6 14 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Metals by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Matrix Spike (BlC0810-MS1) Source: 2101840-03 Analyzed: 03/26/21 12:45 Antimony 49.8 2.4 mg'kg 97.6 ND 51 10-116 Arsenic 100 2.0 97.6 3.12 100 77-121 Barium 196 0.98 97.6 116 82 30-169 Beryllium 98.3 0.49 97.6 ND 101 86-111 Cadmium 93.4 0.24 97.6 ND 96 81-112 Chromium 113 0.49 97.6 17.6 97 75-129 Cobalt 96.4 0.49 97.6 4.26 94 71-121 Copper 106 0.98 97.0 8.79 100 68-135 Lead 98.5 0.49 97.6 5.56 95 72-121 Molybdenum 89.8 0.49 9T6 1.27 91 70-112 Nickel Ill 0.49 97.6 23.4 90 73-121 Selenium 94.7 2.0 97.6 ND 97 76-110 Silver 4.74 0.49 4.88 ND 97 54-132 Thallium 91.2 0.98 97.6 ND 93 64-120 Vanadium 112 2.0 97.6 15.4 99 78-124 Zinc 122 2.0 97.0 29.6 95 50-143 Matrix Spike Dup (B1C0810-MSD1) Source: 2101840-03 Analyzed: 03/26/21 12:55 Antimony 48.3 2.5 mg/kg 98.0 ND 49 10-116 3 20 Arsenic 102 2.0 98.0 3.12 101 77-121 1 20 Barium 203 0.98 98.0 116 89 30-169 4 20 Beryllium 99.4 0.49 98.0 ND 101 86-111 1 20 Cadmium 95.0 0.25 98.0 ND 97 81-112 2 20 Chromium 117 0.49 98.0 17.6 101 75-129 4 20 Cobalt 98.2 0.49 98.0 4.26 96 71-121 2 20 Copper 110 0.98 98.0 8.79 103 68-135 3 20 Lead 100 0.49 98.0 5.56 97 72-121 2 20 Nlolvbdenum 91.3 0.49 98.0 1.27 92 70-112 2 20 Nickel 113 0.49 98.0 23.4 92 73-121 2 20 Selenium 96.4 2.0 98.0 ND 98 76-116 2 20 Silver 4.89 0.49 4.90 ND 100 54-132 3 20 Thallium 93.1 0.99 98.0 ND 95 64-120 2 20 Vanadium 115 2.0 98.0 15.4 102 78-124 3 20 Zinc 124 2.0 98.0 29.6 96 50-143 1 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: 805 925-337ti Page 50 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Total Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Post Spike (B1C0810-PS1) Source: 2101840-03 Analyzed: 03/26/21 12:58 Antimony 1.97 mg/L 2.00 0.0203 98 75-125 Arsenic 2.08 2.00 0.0657 101 75-125 Barium 4.39 2.00 2.43 97 75-125 Beryllium 1.99 2.00 0.00456 99 75-125 Cadmium 1.89 2.00 -0.00476 94 75-125 Chromium 2.37 2.00 0.370 100 75-125 Cobalt 1.97 2.00 0.0898 94 75-125 Copper 2.25 2.00 0.185 103 75-125 Lead 2.02 2.00 0.117 95 75-125 Molybdenum 1.98 2.00 0.0269 98 75-125 Nickel 2.37 2.00 0.492 94 75-125 Selenium 1.97 2.00 0.000298 98 75-125 Silver 0.0974 0.100 -0.00288 97 75-125 Thallium 1.88 2.00 -0.0363 94 75-125 Vanadium 2.30 2.00 0.324 99 75-125 Zinc 2.50 2.00 0.623 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 STLC Metals by 'Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlDO007 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/01/21 09:01 Blank (B1D0007-BLKI) Analyzed: 04/01/21 14:11 Chromium ND 0.050 mg/L Lead ND 0.050 " LCS (B1D0007-BS1) Analyzed: 04/01/21 14:24 Chromium 9.98 0.050 mg/L 10.0 Lead 10.0 0.050 1110.0 LCS Dup (B1D0007-BSD1) Analyzed: 04/01/21 14:27 Chromium 9.89 0.050 mg/l. 10.0 Lead 9.90 0.050 1110.0 Duplicate (B1D0007-DUPI) Source: 2101841-07 Analyzed: 04/01/21 14:42 Chromium 0341 0.10 mg/L 0.342 Lead 59.7 0.10 1156.1 Leach Fluid Blank (B1D0007-LBK1) Analyzed: 04/01/21 14:13 Chromium ND 0.10 mg/L Lead ND 0.10 11 100 80-120 100 80-120 99 80-120 0.9 20 99 80-120 2 20 0.3 20 4 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 52 of 79 WAL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 TCLP Metals by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlD0112 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/06/21 10:26 Blank (B1D0112-BLKI) Analyzed: 04/06/21 12:08 Lead ND 0.050 mg/L LCS (B1D0112-BSI) Analyzed: 04/06/21 12:13 Lcad 9.64 0.050 mg/L 10.0 96 80-120 LCS Dup (B1D0112-BSDI) Analyzed: 04/06/21 12:16 Lcad 9.79 0.050 mg/1- 10.0 98 80-120 1 20 Duplicate (B1D0112-DUPl) Source: 2101841-07 Analyzed: 04/06/21 12:21 Lcad 0.242 0.050 mg/L 0.246 2 20 Leach Fluid Blank (B1D0112-LBK1) Analyzed: 04/06/21 12:11 Lcad ND 0.050 mg/L The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 53 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0802 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:22 Blank (BlC0802-BLKI) Analyzed: 03/26/21 08:30 TPH Gasoline (C5-(" 12) ND 0.50 mgkg Surrogate:4-Bromolluorobenzene• 0.127 " 0.125 101 31-168 LCS (BlC0802-BSI) Analyzed: 03/26/21 06:59 TPHGasoline (C5-C12) 1.01 0.50 mgrkg 1.00 101 62-151 Sur-rogate:4-Bromo/luorohenzeni, 0.152 0.125 121 31-168 LCS Dup (B1C0802-BSD1) Analyzed: 03/26/21 07:25 TPH Gasoline (C5-C12) 0.958 0.50 mg/kg 0.996 96 62-151 5 20 Surrogale:4-Bromo/luorobenzene 0.142 " 0.125 114 31-168 Duplicate (B1C0802-DUP1) Source: 2101840-01 Analyzed: 03/26/21 09:29 TPH Gasoline (C5-('12) ND 0.50 mg/kg ND 20 Surogate.4-Bromolluorobenzcnc 0.131 0.124 105 31-168 Matrix Spike (B1C0802-MS1) Source: 2101836-04 Analyzed: 03/26/21 16:07 TPH Gasoline (C 5-('12) 0.989 0.50 mgkg 1.00 ND 99 10-166 Surrogette:4-Bromolluorobcnzc-ne 0.146 " 0.126 116 31-168 Matrix Spike Dup (BlC0802-MSDI) Source: 2101836-04 Analyzed: 03/26/21 16:33 TPH Gasoline (('5-('12) 0.971 0.50 mg/kg 0.992 ND 98 10-166 2 20 Surrogate:4-Brorn(illuore)henzene 0.149 110.124 120 31-168 Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Blank (BlC0804-BLK1) Analyzed: 03/26/21 10:27 T11H Gasoline (('5-('12) ND 0.50 mg/kg Surogate:4-Bromolluorobenzene 0.133 110.125 107 31-168 LCS (BlC0804-BS1) Analyzed: 03/26/21 09:30 TPH Gasoline (C5-('12) 1.24 0.50 mgkg 0.999 124 62-151 Surrogate:4-Bronurllrmruhcnzerrc 0.147 " 0.125 118 31-168 LCS Dup (B1C0804-BSD1) Analyzed: 03/26/21 09:59 TP1I Gasoline (C5-C12) 1.32 0.50 mg/kg 0.999 132 62-151 7 20 Surrogate. 4-Brcmtolluorohen_ene 0.104 0.125 131 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 - Page 54 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic TPH by 1 - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Duplicate (B1C0804-DUPl) Source: 2101841-06 Analyzed: 03/26/21 11:24 TPII Gasoline (('5-C12) 10.0 4.3 mg/kg 6.12 48 20 QR-03 Surrogate:4-8ronmlluorobenzene 1.3S 111.08 128 31-168 Matrix Spike (B1C0804-MS1) TPH Gasoline (C5-C12) Surrogate: 4-Bromulluorohenzene Matrix Spike Dup (BlC0804-MSD1) TPII Gasoline (C5-C12) Surrogate:4-BromoJluorohenzene Source:2101838-06 Analyzed: 03/26/2120:00 1.13 0.49 mg/kg 0.979 ND 0.159 110.122 Source:2101838-06 Analyzed: 03/26/21 20:29 1.21 0.50 ing/kg 1.00 ND 0.155 110.125 116 10-166 130 31-168 120 10-166 6 20 123 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805j 925-3376 Page 55 of 79 G A m- Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Semi -Volatile Organic TPH by GC/FID - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0798 - EPA 8015M Preparation: EPA 3550C 03/25/21 17:29 Blank (B1C0798-BLK1) Analyzed: 03/26/21 07:35 TPH Diesel (C13-('22) ND 10 mg/kg TPH Motor Oil (C'23-C40) ND 50 " Surrogate: o-Tecphecml 53.7 " 49.8 108 65-133 LCS (B1C0798-BS1) Analyzed: 03/26/21 07:07 TPH Diesel (C13-C22) 508 9.9 mg1g, 496 102 77-114 TPH Motor Oil (C23-('40) 549 50 496 111 76-128 Surrogate: o-Tecphenvl 50.7 49.6 102 65-133 LCS Dup (BlC0798-BSD1) Analyzed: 03/26/21 07:21 TPH Diesel (C13-C22) 501 9.9 mg/kg 497 101 77-114 1 20 TPH Motor Oil (C23-C40) 557 50 497 112 76-128 2 20 Surrogate: o-Tecphen-Vl 53.5 49.7 108 65-133 Duplicate (B1C0798-DUPI) Source: 2101840-01 Analyzed: 03/26/21 08:44 TPII Diesel (C13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) 43.1 50 44.8 4 20 Surrogate: o-Tciphenrl 53.4 49.8 107 65-133 Matrix Spike (BlC0798-MS1) Source: 2101840-01 Analyzed: 03/26/21 13:48 TPH Diesel (C13-('22) 507 9.9 mg/kg 497 ND 102 45-149 TPII Motor Oil (('23-C40) 556 50 497 44.8 103 34-175 Surrogate: o-Tecphen.0 55.9 49.7 113 65-133 Matrix Spike Dup (B1C0798-MSDI) Source: 2101840-01 Analyzed: 03/26/21 14:02 TPH Diesel (('13-C22) 488 10 mglkg 499 ND 98 45-149 4 20 TPH Motor Oil (('23-C40) 548 50 499 44.8 WI 34-175 1 20 Surrogate: o-Tecphecgl 55.2 " 49.9 111 65-133 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 56 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet poControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (BI C0815-BLKI) Analyzed: 03/26/21 11:26 Benzene ND 0.25 mg!kg Bromobenzene ND 0.25 Bromochloromcthane ND 0.25 " Bromodichloromethane ND 0.25 Bromotorm ND 0.25 Bromomethane ND 0.25 " n-Butylbenzene ND 0.25 " sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 Chlorobenzene ND 0.25 Chloroethane ND 0.25 Chloroform ND 0.25 " Chloromethane ND 0.25 2-Chlorutoluene ND 0.25 4-C:hlorotoluene ND 0.25 Dibromochloromethanc ND 0.25 " 1,2-Dibromo-3-chloropropane ND 0.25 " 1,2-Dibromoethan e (EDB) ND 0.25 " Dibromomethane ND 0.25 1,2-Dichlorobenzene ND 0.25 " 1.3-Dichlorobenzene ND 0.25 " 1,4-Dichlorobenzene ND 0.25 Dichloroditluoromcthanc ND 0.25 I,1-Dichloroethane ND 0.25 1.2-Dichloroethane ND 0.25 " l,l-Dichloroethene ND 0.25 " cis - I ?-Dichloroethene ND 0.25 trans-1,2-Dichloroethene ND 0.25 12-Dichloropropane ND 0.25 " 1,3-Dichloropropane ND 0.25 " 2.2-Dichloropropane ND 0.25 " 1,1-Diehloropropene ND 0.25 " cis-1.3-Diehloropropene ND 0.25 trans-1,3-Diehloropropene ND 0.25 Fthvlbenzene ND 0.25 Ilexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 " Niethylene chloride ND 0.25 Naphthalene ND 0.25 " n-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX 805 925-3376 Page 57 of 79 161*y; Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (BlC0815-BLKI) Analyzed: 03/26/21 11:26 Styrene ND 0.25 mgIg 1, 1, 1.2-Tetrachloroethane ND 0.25 " 1,1.2,2-Tetrachlorocthane ND 0.25 Tetrachloroetliene (PCE) ND 0.25 " Toluene ND 0.25 1,2,3-Trichlorobenzene ND 0.25 1,2.4-Trichlorobenzene ND 0.25 1,1,1-Trichloroethane ND 0.25 1,1,2-Trichloroethane ND 0.25 Trichloroethene (TCE) ND 0.25 " Trichlorofluoromethane ND 0.25 1,2,3-Trichloropropane ND 0.25 12,4-Triniethylbenzene ND 0.25 " 1,3,5-Trimethyl benzene ND 0.25 Vinyl chloride ND 0.25 Xylenes (total) ND 0.25 Surrogate: Dibromu/luoromethanc 0.0445 0.0498 89 75-122 Surrogate: Toluene-d8 0.0455 0.0498 91 66-128 Surrogate:4-Bromollaoroben:ene 0.0479 0.0498 96 76-122 LCS (BlC0815-BS1) Analyzed: 03/26/21 09:44 Benzene 1.80 0.25 mgtkg 1.99 91 75-131 Bromobenzene 1.97 0.25 1.99 99 75-136 Bromochloromcthane 1.67 0.25 1.99 84 70-135 Bromodichloromethane 1.84 0.25 1.99 93 76-137 Bromoturm 1.68 0.25 1.99 85 55-139 Bromomethane 1.49 0.25 1.99 75 10-157 u-Butylbenzene 2.38 0.25 1.99 120 62-166 sec-Butylbeuzene 2.50 0.25 1.99 126 72-167 tort-Butylbenzene 2.33 0.25 1.99 117 69-158 Carbon tetrachloride 1.77 0.25 1.99 89 70-140 C'hlorobeuzene 1.94 0.25 1.99 98 76-137 Chloroethane 2.09 0.25 1.99 105 10-104 Chloroform 1.80 0.25 1.99 91 75-123 Chloromethane 1.73 0.2.5 1.99 87 26-140 2-Chlorotoluene 2.11 0.25 1.99 106 73-145 4-Chlorotoluene 2.13 0.25 1.99 107 67-151 Dibromochloromethane 1.80 0.25 1.99 90 68-144 1,2-Dibromo-3-cliloropropane 1.63 0.25 1.99 82 45-148 1,2-Dibromoethane (EDB) 1.80 0.25 1.99 91 73-134 Dibromomcthane 1.66 0.25 1.99 84 70-140 1.2-Dichlorobenzenc 2.15 0.25 1.99 108 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 58 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatilepoControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS (B1C0815-BSI) Analyzed: 03/26/21 09:44 1,3-Dichlorobenzcnc 2,19 0.25 rngtkg 1.99 110 76-146 1,4-Dichlorobenzcnc 2.10 0,25 1.99 106 72-140 Dichloroditluoromcthanc 1.73 0.25 1.99 87 10-166 l,l-Dichloroethane 1.82 0.25 1.99 92 65-139 1,2-Dichlorocthanc 1.90 0.25 1.99 90 67-125 1,1-Dichloroethene 2.05 0.25 1.99 103 54-168 cis-1 2-Dichloroethene 1.80 0.25 1,99 91 74-135 trans-1,2-Dichloroethene 1.98 0.25 1.99 100 68-149 1,2-Dichloropropane 1.77 0.25 1.99 89 74-130 13-Dichloropropane 1.83 0.25 1.99 92 68-130 2,2-Dichloropropane 1.95 0.25 1.99 98 33-187 1,1-Dichloropropene 1.95 0.25 1.99 98 71-140 cis- 1.3-Dichloropropene 1.79 0.25 1.99 90 78-135 trans- l,3-Di chloropropene 1.90 0.25 1.99 96 70-137 Ethvlbenzene 1.93 0.25 1.99 97 69-143 Hexachlorobutadiene 3.12 0.25 1.99 157 69-203 4-Isopropyl Toluene 2.38 0.25 1.99 120 74-154 Isopropylbenzene 2.11 0.25 1.99 106 72-157 Methylene chloride 1.75 0.25 " 1.99 88 49-129 Naphthalene 1.84 0.25 1.99 93 61-158 ❑-Propylbenzene 2.17 0.25 1.99 109 69-147 Styrene 1.92 0.25 1.99 97 71-144 1,1,1,2-Tetrachloroethane 1.92 0.25 1.99 97 78-132 1,1,2,2=I'ctrachloroethane 1.90 0.25 L99 96 64-138 Tetrachloroethene IKE) 2.09 0.25 1.99 105 74-148 Toluene 1.82 0.25 1.99 92 76-131 1,2,3-Trichlorobenzene 2.11 0.25 1.99 106 63-170 1,2.4-Trichlorobenzene 2.20 0.25 1.99 110 71-165 1,1,1-Trichloroethane 1.97 0.25 1.99 99 74-137 1.1,2 Trichloroethane 1.82 0.25 1.99 91 68-134 Trichloroethene (TCE) 1.94 0.25 1.99 98 79-139 Trichlorofluoromethane 2.20 0.25 1.99 111 32-154 1.2,3-Trichloropropane 1.77 0.25 1.99 89 69-125 12.4-Trintethylbenzene 2.14 0.25 1.99 108 67-144 1,3.5-Trimethyl benzene 2.17 0.25 1.99 109 66-154 Vinyl chloride 2.27 0.25 1.99 114 39-150 Xylenes (total) 5.95 0.25 5.96 100 71-147 Surrogate: Dibrotnollitoronrethauc (01496 0.0497 100 75-123 Surrogate: Tduene-JY 0.0462 0.0497 93 66-128 Surrogate:4-Bromq/luoraheii_eirt 0.0451 0.0497 91 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 59 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Oreutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Linrit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (B1C0815-BSDI) Analyzed: 03/26/21 10:09 Benzene 1.97 0.25 mg'kg 2.00 94 75-131 4 20 Bromobenzene 2.02 0.25 2.00 101 75-136 2 20 Bromochloromethanc 1.69 0.25 2.00 85 70-135 2 20 Bromodichloromethane 1.93 0.25 2.00 97 76-137 5 20 Bromoform 1.80 0.25 2.00 90 55-139 7 20 Bromomethane 1.21 0.25 2.00 61 10-157 20 20 n-Butylbenzene 2.45 0.25 2.00 123 62-166 3 20 sec-Butylbenzene 2.48 0.25 2.00 124 72-167 09 20 tort-Butylbenzene 2.38 0.25 2.00 119 69-158 2 20 Carbon tetrachloride 1.87 0.25 2.00 94 70-140 6 20 Chlorobenzene 2.07 0.25 2.00 104 76-137 7 20 Chloroethane 2.21 0.25 2.00 111 10-164 6 20 Chloroform 1.81 0.25 2.00 90 75-123 0.4 20 Chloromethane 1.82 0.25 2.00 91 26-146 5 20 2-Chlorololuene 2.26 0.25 2.00 113 73-145 7 20 4-Chlorotoluene 2.25 0.25 2.00 112 67-151 5 20 Dibromochloromethane 1.97 0.25 2,00 98 68-144 9 20 1.2-Dibromo-3-chloropropane 1.84 0.25 2.00 92 45-148 12 20 1.2-Dibrotnoethane (EDB) 1.98 0.25 2.00 99 73-134 9 20 Dibromomcthane 1.75 0.25 2.00 87 70-140 5 20 1,2-Dichlorobenzene 2.18 0.25 2.00 109 78-142 1 20 1.3-Dichlorobenzene 2.30 0.25 2.00 115 76-146 5 20 1.4-Dichlorobenzene 2.06 0.25 2.00 103 72-140 2 20 Dichlorodifluormmcthane 1.73 0.25 2.00 86 10-166 0.1 20 I,1-Dichloroethane 1.95 0.25 2.00 98 65-119 7 20 1.2-Dichlorocthanc 1.93 0.25 2.00 96 67-125 7 20 1,1-Dichloroethene 2.07 0.25 2.00 103 54-168 0.6 20 cis-1.2-Dichloroethene 1.86 0.25 2.00 93 74-135 4 20 trans-1,2-Dichloroethene 2.11 0.25 2.00 105 68-149 6 20 12-Dichloropropane 1.82 0.25 2.00 91 74-130 3 20 1,3-Dichloropropane 1.84 0.25 2.00 92 68-130 0.6 20 2,2-Dichloropropane 1.94 0.25 2.00 97 33-187 0.4 20 1 .1 -Dichloropropene 2.04 0.25 2.00 102 71-140 5 20 cis-L3-Dichloropropene 1.80 0.25 2.00 90 78-135 0.5 20 trans-1,3-Dichloropropene L94 0.25 2.00 97 70-137 2 20 Ethvlbenzene 2.06 0.25 2.00 103 69-143 6 20 1lexachlorobutadiene 3.30 0.25 2.00 165 69-203 6 20 4-Isopropyl Toluene 2.42 0.25 2.00 121 74-154 2 20 Isopropylbenzene 2.19 0.25 2.00 109 72-157 3 20 methylene chloride 1.87 0.25 2.00 94 49-129 7 20 Naphthalene 2.04 0.25 2.00 102 61-158 1() 20 n-Propylbenzene 2.30 0.25 2.00 115 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Coinpounds by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (B1C0815-BSDI) Analyzed: 03/26/21 10:09 Styrene 2.06 0.25 mg/kg 2.00 103 71-144 7 20 1, 1, 1,2-Tetrachloroethane 2.04 0.25 2.00 102 78-132 6 20 1,1,2.2-Tetrachloroethane 2.02 0.25 2.00 101 64-138 6 20 Tetrachloroethane (PCE) 2.18 0.25 2.00 109 74-148 4 20 Toluene 1.91 0.25 2.00 96 76-131 5 20 1,2,3-Trichlorobenzene 2.36 0.25 2.00 IIS 63-170 12 20 1,2,4-Trichlorobenzene 2.37 0.25 2.00 118 71-165 7 20 1,1,1-Trichloroethane 1.98 0.25 2.00 99 74-137 0.8 20 1,1,2-Trichloroethane 1.92 0.25 2.00 96 68-134 6 20 Trichloroethene (TCE) 1.92 0.25 2.00 96 79-139 0.9 20 Trichlorotluoromethane 2.15 0.25 2.00 107 32-154 3 20 1,2,3-Trichloropropane 1.78 0.25 2.00 89 69-125 0.3 20 1.2.4-Trintethylbenzene 2.19 0.25 2.00 110 67-144 2 20 1,3,5-Trimethylbenzene 2.24 0.25 2.00 112 66-154 3 20 Vinyl chloride 2.22 0.25 2.00 111 39-150 2 20 Xylenes (total) 6.14 0.25 6.00 102 71-147 3 20 Surrogate: DibromoJhioromcthanc 0.0492 0.0500 98 75-122 Surrogate: Toluene-dR 0.0452 0.0500 90 66-128 Surrogate:4-Bromo/luomhenrene 0.0464 0.0500 93 76-122 Duplicate (B1C0815-DUPI) Source: 2101841-07 Analyzed: 03/26/21 14:51 Benzene ND 1.2 mg/kg ND 20 Broniobenzene ND 1.2 ND 20 Bromochlorontcthanc ND 1.2 " ND 20 Bromodichlorome(hane ND 1.2 ND 20 Bromofornt ND 1.2 ND 20 Bromontethane ND 1.2 " ND 20 n-Butylbenzene ND 1.2 ND 20 sec-Butylbenzene ND 1.2 ND 20 tort-Butylbenzene ND 1.2 NI> 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzeue ND 1.2 ND 20 Chloroethatte ND 1.2 ND 20 Chloroform ND 1.2 ND 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 4-Chlorotoluene ND 1.2 ND 20 Dibromochloromethane ND 1.2 ND 20 1,2-1)ibronto-3-clhloropropaitc ND 1.2 ND 20 1,2-Dibromocthane (EDB) ND 1.2 ND 20 Dibromomethane ND 1.2 ND 20 1.2-Dic•hlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 61 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Duplicate (WC0815-DUPI) Source: 2101841-07 Analyzed: 03/26/21 14:51 1,3-Dich1orobcnzcnc ND 1.2 mg!kg ND 20 1,4-Dichlorobenzene ND 1.2 ND 20 Dichloroditluoromethanc ND 1.2 ND 20 I,1-Dichloroethane ND 1.2 ND 20 1,2-Dichloroethane ND 12 ND 20 1,1-Dichloroethene ND 1.2 ND 20 cis-1.2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropane ND 1.2 ND 20 1.3-Dichloropropane ND 1.2 ND 20 2,2-Dichloropropane ND 1.2 ND 20 1, 1 -Dichloropropene ND 1.2 ND 20 cis-1.3-Dichloropropene ND 1.2 ND 20 trans-1,3-Dichloropropene ND 1.2 ND 20 Ethylbenzene ND 1.2 " ND 20 1lexachlorobutadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 Isopropylbcnzene ND 1.2 ND 20 Methylene chloride ND 1.2 " ND 20 Naphthalene ND 1.2 ND 20 n-Prupylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1,1,1,2-Tetrachlorocthane ND 1.2 ND 20 1,1.2,2-Tctrachlorocthanc ND 1.2 ND 20 Tetrachloroethene 1PCE) ND 1.2 ND 20 TOIUCIIC ND 1.2 " ND 20 1,2,3-Trichlorobenzene ND 1.2 ND 20 1,2,4-Trichlorobenzene ND 1.2 ND 20 1, 1, 1 -Trichloroethane ND 1.2 ND 20 1,1,2-1'richloroethanc ND 1.2 ND 20 Trichloroethene (TCE) ND 1.2 ND 20 Trichlorofluoromethane ND 1.2 ND 20 1,2,3-Trichlompropane ND 1.2 ND 20 1,2,4-Trimethylbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 " ND 20 Vinyl chloride ND 1.2 ND 20 Xylenes (total) ND 12 ND 20 Surrogate: Dihrunm/huirurncthuur 0.0468 0.0494 95 75-122 Surrogate:7bluene-d8 0.0455 0.0494 92 66-128 Surrogate:4-Bronmlluorohenzene 0.0466 0.0494 94 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 62 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (B1C0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Benzene 8,51 1.2 mg/kg 9.92 ND 86 36-146 Bromobenzene 8.76 1.2 9.92 ND 88 28-152 Bromochloromcthane 9.53 1.2 9.92 ND 86 43-146 Bromodichlorotnethane 8.97 1.2 9.92 ND 90 43-153 Bromoform 9.44 1.2 9.92 ND 85 26-151 Bromomethane 4.77 1.2 9.92 ND 48 10-158 n-Butylbenzene 8.02 1.2 9.92 0.499 76 10-171 sec-Butylbenzene 9.66 1.2 9.92 ND 97 10-176 tert-1utylbenzene 9.42 1.2 992 ND 95 19-168 Carbon tetrachloride 8.16 1.2 9.92 ND 82 29-151 Chlorobenzene 8.93 1.2 9.92 ND 90 31-151 Chloroethane 10.4 1.2 9.92 ND 105 13-160 Chloroform 9.01 1.2 9.92 ND 91 44-137 Chloromethane 7.13 1.2 9.92 ND 72 10-144 2-Chlorotoluene 8.99 1.2 9.92 ND 91 24-158 4-Chlorotoluene 8.51 1.2 9.92 ND 86 19-160 Dibromochloromethane 9.48 1.2 9.92 ND 96 40-153 1,2-Dibronio-3-chloropropane 9.07 1.2 9.92 ND 91 21-164 1,2-Dibrontoethane(ED13) 9.81 1.2 9.92 ND 99 41-148 Dibromomcthane 9.47 1.2 9.92 ND 85 45-158 1,2-Dichlorobenzenc 9.26 1.2 9.92 ND 93 24-158 1,3-Dichlorobenzenc 8.93 1.2 9.92 ND 90 19-160 1,4-Dichlorobenzene 8.53 1.2 9.92 ND 86 20-152 Dichlorodifluoromcthane 6.47 1.2 9.92 ND 65 10-153 1,1-Dichloroethane 8.67 1.2 9.92 ND 87 35-149 1,2-Dichlorocthene 9.37 1.2 9.92 ND 94 42-132 1,1-Dichloroethene 8.72 1.2 9.92 ND 88 18-174 cis-1.2-Dichloroethene 8.62 1.2 9.92 ND 87 41-146 trans-1,2-Dichloroethene 9.52 1.2 9.92 ND 96 27-161 1.2-Dichloropropane 8.67 1.2 9.92 ND 87 42-145 1,3-Dichloropropane 9.17 1.2 9.92 ND 92 42-141 2.2-Dichloropropane 8.42 1.2 9.92 ND 85 10-166 1,1-Dichloropropene 8.71 1.2 9.92 ND 88 28-151 cis-1,3-Dichloropropene 8.40 1.2 9.92 ND 85 38-148 trans-1,3-Dichloropropene 9.73 1.2 9.92 ND 98 36-144 Ethylbenzene 8.85 1.2 9.92 ND 89 16-162 Hexachlorobutadiene 8.06 1.2 9.92 ND 87 10-193 4-Isopropyl Toluene 8.50 1.2 9.92 ND 86 11-167 Isopropylbenzene 9.00 1.2 9.92 ND 91 13-174 Nlethvlene chloride 8.75 1.2 9.92 ND 88 30-131 Naphthalene 9.21 1.2 9.92 ND 93 10-178 n-Propylbenzene 8.74 1.2 9.92 ND 88 12-160 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 63 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet t by Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Matrix Spike (B1C0815-MS1) Source: 2101841-04 Analyzed: 03/26/21 18:41 Styrene 8.81 1.2 mg/kg 9.92 ND 89 23-160 1, 1, 1,2-Tetrachloroethane 9.93 1.2 9.92 ND 100 36-152 1,1,2,2-Tetrachlorocthanc 9.13 1.2 9.92 ND 92 19-17.5 Tetrachloroethene(PCE) 8.53 1.2 9.92 ND 86 23-162 Toluene 8.41 1.2 9.92 ND 85 26-152 1,2,3-Trichlorobenzene 8.62 1.2 9.92 ND 87 10-168 1.2,4-1'richlorobenzene 8.22 1.2 9.92 ND 83 10-170 1,1,1-Trichloroethane 9.36 1.2 9.92 ND 94 36-150 1,1,2-Trichloroethane 9.70 L2 9.92 ND 98 25-179 Trichloroethene (TCE) 8.55 1.2 9.92 ND 86 29-167 Trichlorotluoromethane 8.61 1.2 9.92 ND 87 15-156 1,2,3-Trichloropropane 8.96 1.2 9.92 ND 90 26-177 1,2.4-Trimethylbenzene 8.51 1.2 9.92 ND 86 14-157 1.3,5-Trimethylbenzene 8.70 1.2 9.92 ND 88 10-167 Vinyl chloride 9.41 1.2 9.92 ND 95 14-154 Xylenes (total) 26.2 1.2 29.8 ND 88 21-162 Surrogate: Dibroniolluoromc-thane 0.0487 0.0496 98 75-122 Surrogate. Toluene-dS 0.0457 0.0490 92 66-128 Surrogate:4-Bromo/luorohenrenc 0.0455 0.0496 92 76-122 Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (BlC0817-BLKI) Analyzed: 03/26/21 12:18 Benzene ND 0.0050 mg/kg Bromobenzene ND 0.0050 " Bromochloromethane ND 0.0050 " Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 " Bromomethane ND 0.0050 n-Butylbcnzcne ND 0.0050 sec-Butylbenzene ND 0.0050 " tort-Butylbenzenc ND 0.0050 " Carbon tetrachloride ND 0.0050 " Chlorobenzene ND 0.0050 C hloroethane ND 0.0050 " Chloroform ND 0.0050 " Chloromethane ND 0.0050 2-Chlorotoluene ND 0,0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 1,2-Dibronx>-3-chloropropane ND 0.0050 1.2-Dibromoethane (E.DB) ND 0.0050 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 64 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlCO817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (B1C0817-BLK1) Analyzed: 03/26/21 12:18 Dibromomethane ND 0.0050 mg/kg 1,2-Dichlorobenzene ND 0.0050 " 1.3-Dichlorobenzene ND 0.0050 " 1,4-Dichlorobenzene NI) 0.0050 Dichlorodilluoromcthanc ND 0.0050 " LI-Dichloroethane ND 0.0050 " 1,2-Dichloroethane ND 0.0050 " 1, 1 -Dichloroethene ND 0.0050 " cis-1.2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene NI) 0.0050 " 1,2-Dichloropropaue ND 0.0050 " 1,3-Dichloropropane ND 0.0050 " 2,2-Dichloropropane ND 0.0050 " 1,1-Dichloropmpcne ND 0.0050 " cis-1,3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethylbenzene ND 0.0050 " Ilexachlorobutadiene ND 0.0050 " 4-Isopropyl Toluene ND 0.0050 Isopropylbcnzcne ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 " Styrcnc ND 0,0050 " 1,1,1,2-Tetraehloroethane ND 0.0050 1,1,2.2-Tetrachloroethane ND 0.0050 Tetrachloroethene (PCE) ND 0.0050 " Toluene ND 0.0050 " 1,2,3-Trichlorobenzene NI) 0.0050 1,2.4-Trichlorobenzene ND 0.0050 " 1,1,1-Trichloroethane ND 0.0050 " 1,1,2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 " Trichlorotluoromethane ND 0.0050 " 1,2.3-Trichloropropane ND 0.0050 1,2.4-1'rimethylbenzene ND 0.0050 " 13.5-Trimethylbenzene NI) 0.0050 " Vinyl chloride NI) 0.0050 " Xylenes (total) ND 0.0050 Surrogate: Uihroiaollttorometltanc, 0.0459 0.0495 93 75-122 Surrogate: 'Toluene--dR 0.0472 0.0495 95 66-128 Surrogate:4-BronmJluorohen_ene 0.0483 0.0495 98 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 65 of 79 WIL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 CoI Volatile Organic mpounds by Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (B1C0817-BSI) Analyzed: 03/26/21 10:22 Benzene 0.0342 0.0050 mg/kg 0.0398 86 75-131 Bromobenzene 0.0367 0.0050 0.0398 92 75-136 Bromochloromethane 0.0329 0.0050 0.0398 82 70-135 Bromodichloromethane 0.0334 0.0050 0.0398 84 76-137 Bromoform 0.0369 0.0050 0.0398 93 55-139 Bromomethane 0.0230 0.0050 0.0399 58 10-157 u-Butylbenzene 0A396 0.0050 0.0398 99 62-166 sec-Butylbenzene 0.0452 0.0050 0.0398 114 72-167 tert-Butylbenzene 0.0427 0.0050 0.0398 108 69-158 Carbon tetrachloride 0.0348 0.0050 0.0398 87 70-140 Chlorobenzene 0.0374 0.0050 0.0398 94 76-137 Chloroethane 0.0413 0.0050 0.0398 104 10-164 Chloroform 0.0323 0.0050 0.0398 81 75-123 Chloromethane 0.0324 0.0050 0.0398 82 26-146 2-Chlorotoluene 0.0390 0.0050 0.0398 100 73-145 4-Chlorotoluene 0.0405 0.0050 0.0398 102 67-151 Dibrotvochlorontethane 0.0371 0.0050 0.0398 93 68-144 1,2-Dibromo-3-chloropropane 0.0355 0.0050 0.0398 89 45-148 1,2-Dibromoethane (EDB) 0.0369 0.0050 0.0398 93 73-134 Dibromomcthanc 0.0328 0.0050 0.0398 82 70-140 1,2-Dichlorobenzene 0.0402 0.0050 0.0398 101 78-142 1,3-Dichlorobenzene 0.0406 0.0050 0.0398 102 76-146 1,4-Dichlorobenzene 0.0388 0.0050 0.0398 97 72-140 Dichlorodifluoromcthane 0.0375 0.0050 0.0398 94 10-166 1, 1 -Dichloroethane 0.0342 0.0050 0.0398 86 65-139 1,2-Dichlorocthene 0.0336 0.0050 0.0398 84 67-125 1.1-Dichloroethene 0.0360 0.0050 0,0398 90 54-168 cis-1,2-Dichloroethene 0.0346 0.0050 0.0398 87 74-135 trans-1,2-Dichloroethene 0.0375 0.0050 0.0398 94 68-149 1,2-Dichloropropane 0.0336 0.0050 0.0398 84 74-130 1,3-Dichloropropane 0.0356 0.0050 0.0398 90 68-130 22-Dichloropropane 0.0394 0.0050 0.0398 99 33-187 1. 1 -Dichloropropene 0.0350 0.0050 0.0398 88 71-140 cis-1.3-Dichloropropene 0.0349 0.0050 0.0398 88 78-135 trans-1,3-Dichloropropene 0.0393 0.0050 0.0398 99 70-137 Ethylbenzene 0.0379 0.0050 0.0398 95 69-143 Hexachlorobutadiene 0.0480 0.0050 0.0398 121 69-203 4-Isopropyl Toluene 0.0438 0.0050 0.0398 110 74-154 Isopropylbenzene 0.0408 0.0050 0.0398 102 72-157 methylene chloride 0.0320 0.0050 0.0398 80 49-129 Naphthalene 0.0429 0.0050 0.0398 108 61-158 u-Propylbenzene 0.0417 0.0050 0.0398 105 69-147 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 66 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GUMS - Quality Control IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (BlC0817-BSI) Analyzed: 03/26/21 10:22 Styrene 0.0384 0.0050 mg!kg 0.0398 97 71-144 1, 1, 1,2-Tetrachloroethane 0.0379 0.0050 0.0398 95 78-132 1,1.2,2-Tetrachloroethane 0.0390 0.0050 0.0398 98 64-138 Tetrachloroethene WCE) 0.0386 0.0050 0.0398 97 74-148 Toluene 0.0330 0.0050 0.0398 83 76-131 1,2,3-Trichlorobenzene 0.0434 0.0050 0.0398 109 63-170 1,2,4-Trichloroben7ene 0.0433 0.0050 0.0398 109 71-165 1,1,1-Trichloroethane 0.0349 0.0050 0.0399 88 74-137 1,1,2-Trichloroethane 0.0364 0.0050 0.0398 92 68-134 Triehloroethene (TCE) 0.0344 0.0050 0.0398 86 79-139 Trichlorofluoromethane 0.0382 0.0050 0.0398 96 32-154 1,2,3-Trichloropropane 0.0367 0.0050 0.0398 92 69-125 1,2,4-Trimethylbeuzene 0.0390 0.0050 0.0398 98 67-144 1,3,5-Trimethylbenzene 0.0409 0.0050 0.0398 103 66-154 Vinyl chloride 0.0373 0.0050 0.0398 94 39-150 Xylenes (total) 0,115 0.0050 0.119 97 71-147 Surrogate: DihromoJluoromethane 0.0474 0.0497 95 75-122 Surrogate: Toluene d8 0.0478 0.0497 96 66-128 Surrogate:4-Bromofluorobenzene 0.0490 0.0497 99 76-122 LCS Dup (B1C0817-BSD1) Analyzed: 03/26/21 10:51 Benzene 0,0353 0.0050 mg/kg 0.0398 89 75-131 3 20 Bromobenzene 0.0390 0,0050 0.0399 98 75-136 6 20 Bromochloromethane 0.0339 0.0050 0.0398 85 70-135 3 20 Bromodichloromethane 0.0349 0.0050 0.0398 88 76-137 4 20 Bromoform 0.0390 0.0050 0,0398 98 55-139 6 20 Bromomethane 0.0259 0.0050 0.0398 65 10-157 12 20 u-Butylbenzene 0.0425 0.0050 0.0398 107 62-I66 7 20 sec-Butylbenzene 0.0487 0.0050 0.0398 122 72-167 7 20 tert-Butylbenzene 0.0459 0.0050 0.0398 115 69-I58 7 20 Carbon tetrachloride 0.0363 0.0050 0.0398 91 70-140 4 20 Chlorobenzene 0.0396 0.0050 0.0398 99 76-137 6 20 Chloroethane 0.0404 0.0050 0.0398 1M 10-164 2 20 Chloroform 0.0339 0.0050 0.0398 85 75-123 5 20 Chloromethane 0.0344 0.0050 0.0398 86 26-140 6 20 2-Chlorotoluene 0,0425 0.0050 0.0398 107 73-145 7 20 4-Chlorotoluene 0.0431 0.0050 0.0399 108 67-151 6 20 Dibromochloromethane 0.0391 0.0050 0.0398 98 68-144 5 20 1,2-Dibronto-3-chloropropanc 0.0367 0.0050 0.0398 92 45-148 3 20 1,2-Dibromoethane (EDB) 0.0387 0.0050 0.0398 97 73-134 5 20 Dibromonuthane 0.0337 0.0050 0.0398 85 70-140 3 20 1,2-Diehlorobenzene 0.0426 0.0050 0.0398 107 78-142 6 20 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 IWAIWAMna Page 67 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds by GC/MS - Quality Control IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlCO817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS Dup (B1C0817-BSDl) Analyzed: 03/26/21 10:51 1,3-Dichlorobenzene 0.0435 0.0050 mg/kg 0.0398 109 76-146 7 20 1,4-Dichlorobenzene 0.0413 0.0050 0.0398 104 72-140 6 20 Dichlorodifluoromethanc 0.0383 0.0050 0.0398 96 10-166 2 20 1,1-Dichloroethane 0.0354 0.0050 0.0399 89 65-139 4 20 1,2-Dichlorocthanc 0.0346 0.0050 0.0398 87 67-125 3 20 1, 1 -Dichloroethene 0.0372 0.0050 0.0398 93 54-169 3 20 cis-12-Dichloroethene W0359 0.0050 0.0398 90 74-135 4 20 trans-1,2-Dichloroethene 0.0389 0.0050 0.0398 98 68-149 4 20 1,2-Dichloropropane 0.0350 0.0050 0.0398 88 74-130 4 20 1,3-Dichloropropane 0.0372 0.0050 0.0398 93 68-130 4 20 2,2-Dichloropropane 0.0403 0.0050 0.0398 WI 33-187 2 20 1, 1 -Dichloropropene 0.0365 0.0050 0.0398 91 71-140 4 20 cis-1,3-Dichloropropene 0.0362 0.0050 0.0398 91 78-135 4 20 trans-1,3-Dichloropropene 0.0415 0.0050 0.0399 104 70-137 5 20 Ethylbenzene 0.0402 0.0050 0.0398 101 69-143 6 20 1fexachlorobutadiene 0,0509 0.0050 0.0398 128 69-203 6 20 4-Isopropyl Toluene 0.0471 0.0050 0.0398 118 74-154 7 20 Isopropylbenzene 0.0437 0.0050 0.0398 110 72-157 7 20 Methylene chloride 0.0333 0.0050 0.0398 84 49-129 4 20 Naphthalene 0.0453 0.0050 0.0398 114 61-158 6 20 u-Propylbenzene 0.0443 0.0050 0.0398 111 69-147 6 20 Styrene 0.0410 0.0050 0.0398 103 71-144 6 20 1, 1, 1,2-Tetrachloroethane 0.0402 0.0050 0.0398 101 78-132 6 20 1,1,2,2-1'etrachlorocthane 0.0407 0.0050 0.0398 102 64-138 4 20 Tetrachloroethene(PCE) 0.0412 0.0050 0.0398 103 74-148 6 20 Toluene 0.0349 0.0050 0.0398 88 76-131 6 20 1,2,3-Trichlorobenzene 0.0459 0.0050 0.0398 115 63-170 6 20 1,2.4-Trichlorobenzene 0.0448 0.0050 0.0398 112 71-165 4 20 1, 1, 1 -Trichloroethane 0.0365 0.0050 0.0398 92 74-137 5 20 1,1,2-Trichloroethane 0.0386 0.0050 0.0398 97 68-134 6 20 Tichloroethene (TCE) 0.0365 0.0050 0.0399 92 79-139 6 20 Trichlorofluoromethane 0.0398 0.0050 0.0398 100 32-154 4 20 1,2,3-Trichloropropane 0.0384 0.0050 0.0398 96 69-125 5 20 1,24-Trimethylbenzene 0.0422 0.0050 0.0398 106 67-144 8 20 1,3.5-Trimethylbenzene 0.0437 0.0050 0.0398 110 66-154 7 20 Vinyl chloride 0.0382 0.0050 0.0398 96 39-150 2 20 Xylenes (total) 0.123 0.0050 0.120 103 71-147 7 20 Surrogate: Dibronwlhwronrethane 0.0467 0.0498 94 75-122 Surrogate: Toluene-d# 0.0473 0.0498 95 40-128 Surrogate:4-BronurJluorirhenzeae 0.0495 0.0498 99 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 68 of 79 r A .; rrara NZW=�LM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (BlC0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromethanc ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromotbmt ND 0.0050 NI) 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene NI) 0.0050 NI) 20 Chloroethane ND 0.0050 ND 20 Chloroform NI) 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorotoluene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1.2-Dibromo-3-chloropropane ND 0.0050 NI) 20 1,2-Dibromoethane (F.DB) ND 0.0050 NI) 20 Dibromomethane ND 0.0050 ND 20 1,2-Diehlorobenzene ND 0.0050 NI) 20 1,3-Dichlorobenzenc ND 0.0050 ND 20 IA-Dichlorobenzene ND 0.0050 ND 20 Dichlorodifluoromcthanc ND 0.0050 NI) 20 1,1-Dichloroethane NI) 0.0050 ND 20 1,2-Diehloroethanc ND 0.0050 ND 20 LI-Dichloroethene ND 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane ND 0.0050 ND 20 2,2-Dichloropropane NI) 0.0050 ND 20 1.1-Dichloropropene ND 0.0050 ND 20 cis- 1,3-Dichloropropene NI) 0.0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 ND 20 1-thylbenzene NI) 0.0050 ND 20 Ilexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 Isopropylbenzene ND 0.0050 ND 20 Methylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 69 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Volatilet pt Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPl) Source: 2101841-08 Analyzed: 03/26/21 14:15 Styrene ND 0.0050 mglkg NI) 20 1, 1, 1,2-Tetrachloroethane NI) 0.0050 ND 20 1,1,2,2-Tetrachlorocthanc ND 0.0050 NI) 20 Tetrachloroethene (PCE) NY) 0.0050 ND 20 Toluene ND 0.0050 ND 20 1,2,3-Trichlorobenzene ND 0.0050 ND 20 1,2,4=rrichloroben7ene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1.1,2-Trichloroethane ND 0.0050 NI) 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethane ND 0.0050 NI) 20 1,2,3-Trichloropropane NI) 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1.3,5-Trimethylben7ene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 ND 20 Surrogate: l)lhronui/luaromethmrc 0.0460 0.0496 93 75-122 Surrogate Tohiene-d8 0.0472 0.0496 95 66-128 Surrogate:4-BromoJluorohenzene 0.0480 0.0496 97 76-122 Matrix Spike (BIC0817-MSI) Source: 2101941-12 Analyzed: 03/26/21 20:05 Benzene 0.0322 0.0050 mg/kg 0.0399 ND 81 36-146 Bromobenzene 0.0319 0.0050 0.0399 ND 80 28-152 Bromochloromethane 0.0323 0.0050 0.0399 NI) 81 43-146 Bromodichloromethane 0.0322 0.0050 0.0399 ND 81 43-153 Bromoform 0.0376 0.0050 0.0399 ND 94 26-151 Bromomethane 0.0290 0.0050 0.0399 ND 73 10-158 n-Butylbenzene 0.0242 0.0050 0.0399 ND 61 10-171 sec-Butylbenzene 0.0324 0.0050 0.0399 ND 81 10-176 tert-Butylbenzene 0.0335 0.0050 0.0399 NI) 84 19-168 Carbon tetrachloride 0.0322 0.0050 0.0399 ND 81 29-151 C'hlorobenzene 0.0337 0.0050 0.0399 NI) 84 31-151 Chloroethane 0.0346 0.0050 0.0399 ND 87 13-160 Chloroform 0.0316 0.0050 0.0399 NU 79 44-137 Chloromethane 0.0329 0.0050 0.0399 ND 82 10-144 2-Chlorotoluene 0.0335 0.0050 0.0399 ND 84 24-158 4-Chlorotoluene 0.0330 0.0050 0.0399 ND 83 19-160 Dibromochloromethane 0.0370 0.0050 0.0399 ND 93 40-153 1,2-Dibromo-3-chloropropane 0.0333 0.0050 0.0399 ND 84 21-164 1,2-Dibromoethane (EDB) 0.0366 0.0050 0.0399 ND 92 41-148 Dibromomethanc 0.0315 0.0050 0.0399 ND 79 45-158 1,2-Dichlorobenzene 0.0325 0.0050 0.0399 NI) 82 24-158 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIlent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 70 of 79 at A MML Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Matrix Spike (BlC0817-MSI) Source: 2101841-12 Analyzed: 03/26/21 20:05 13-Dichlorobenzene 0.0321 0.0050 mg/kg 0.0399 ND 80 19-160 14-Dichlorobenzene 0.0305 0.0050 0.0399 ND 76 20-152 Dichlorodilluoromcthane 0.0373 0.0050 0.0399 ND 93 10-153 I,I-Dichloroethene 0.0332 0.0050 0.0399 ND 83 35-148 1,2-Dichlorocthanc 0.0321 0.0050 0.0399 ND 80 42-132 1, 1 -Dichloroethene 0.0345 0.0050 0.0399 ND 86 18-174 cis-1,2-Dichloroethene 0.0335 0.0050 0.0399 ND 84 41-146 trans-1,2-Dichloroethene 0.0354 0.0050 0.0399 ND 89 27-161 1 .2-Dichloropropane 0.0321 0.0050 0.0399 ND 80 42-145 1,3-Dichloropropane 0.0358 0.0050 0.0399 ND 90 42-141 2,2-Dichloropropane 0.0344 0.0050 0.0399 ND 86 10-166 1,1-Dichloropropene 0.0321 0.0050 0.0399 ND 80 28-151 cis-1,3-Dichloropropene 0.0320 0.0050 0.0399 ND 80 38-148 trans-1,3-Dichloropropene 0.0376 0.0050 0.0399 ND 94 36-144 Ethylbenzene 0.0324 0.0050 0.0399 ND 81 16-162 1lexachlorobutadiene 0.0223 0.0050 0.0399 ND 56 10-193 4-Isopropyl Toluene 0.0300 0.0050 0.0399 ND 75 11-167 Isopropylbenzene 0.0328 0.0050 0.0399 ND 82 13-174 Nlethylene chloride 0.0310 0.0050 0.0399 ND 78 30-131 Naphthalene 0.0314 0.0050 0.0399 ND 79 10-178 n-Propylbenzene 0.0325 0.0050 0.0399 ND 81 12-160 Styrene 0.0336 0.0050 0.0399 ND 84 23-160 1,1,1,2-Tetrachloroethane 0.0368 0.0050 0.0399 ND 92 36-152 1,1,2,2-1'etrachloroethane 0.0365 0.0050 0.0399 ND 91 19-175 Tetrachloroethane (PCE) 0.0339 0.0050 0.0399 ND 85 23-162 Toluene 0.0291 0.0050 0.0399 ND 73 26-152 1,2,3-Triclilorobenzene 0.0262 0.0050 0.0399 ND 66 10-168 1,2,4=lichlorobenzene 0.0257 0.0050 0.0399 ND 64 10-170 I,1,1-Trichloroethane 0.0334 0.0050 0.0399 ND 84 36-150 1,1,2-Trichloroethane 0.0364 0.0050 0.0399 ND 91 25-179 Trichloroethane (TCE) 0.0339 0.0050 0.0399 ND 85 29-167 Trichlorofluoromethane 0.0379 0.0050 0.0399 ND 95 15-156 1,2,3-Trichloropropane 0.0376 0.0050 0.0399 ND 94 26-177 L2.4-Trimethylbenzene 0.0308 0.0050 0.0399 ND 77 14-157 1,3,5-Trimethylbenzene 0.0323 0.0050 0.0399 ND 81 10-167 Vinyl chloride 0.0368 0.0050 0.0399 ND 92 14-154 Xylenes (total) 0.0983 0.0050 0.120 ND 82 21-162 Surrogate: Dibromo/luoromethanc 0.0459 0.0499 92 75-122 Surrogate: Toluene-dN 0.0473 0.0499 95 66-128 Surrogate:4-Bromoguorobenzene 0.0486 0.0499 97 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 71 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-E.LAP 8015 Diesel & Motor Oil List EPA 9015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal STLC Metals by ICP 601013 STLC Chromium STLC/EPA 601013 Water OEC, CA -FLAP 601013 STLC Lead STLC/EPA 6010E Water OEC. CA-ELAP STLC Metals Extraction STLC Metals Extraction STLC Solid OEC. Internal TCLP Metals by ICP 6010B WIT Lead EPA 1311/EPA 6010B Water OEC, CA -FLAP TCLP Metals Extraction TCLP Metals Extraction EPA 1311 Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 r i Page 72 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) lnalysis Method Matrix Laboratory & Certification Total Metals by ICP 601 OB Total Antimony EPA 6010E Solid OEC. CA -FLAP 601013Total Arsenic EPA 601013 Solid OEC, CA-ELAP 001013 Total Barium EPA 6010B Solid OEC, CA-ELAP 6010B Total Beryllium EPA 601013 Solid OEC, CA-ELAP 6010E Total Cadmium EPA 6010B Solid OEC, CA-ELAP 6010E Total Chromium EPA 6010B Solid OEC, CA -FLAP 601013 Total Cobalt EPA 601013 Solid OEC, CA-ELAP 6010E Total Copper EPA 6010B Solid OEC, CA-ELAP 6010E Total Lcad EPA 6010E Solid OEC, CA-ELAP 6010B Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 6010E Total Nickel EPA 6010E Solid OEC, CA-ELAP 6010E Total Selenium EPA 6010E Solid OEC, CA-ELAP 601013 Total Silver EPA 6010E Solid OEC, CA-ELAP 601013 Total Thallium EPA 6010E Solid OEC, CA-ELAP 6010B Total Vanadium EPA 6010E Solid OEC. CA-ELAP 6010E Total Zinc EPA 6010E Solid OEC, CA-ELAP Volatile Organic Compounds by GUMS 8260B Full List EPA 8260B Solid OEC. CA-ELAP The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 73 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Sample Method Summary (Continued) nalysis Method Matrix Laboratory & Certification Volatile Organic TPH by GC/FID 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPII-Gasolinc EPA 8015M Solid OEC, CA -FLAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC_ CA -FLAP 8015 TPH-Gasolinc EPA 8015M Solid OEC, Internal 8015 TPII-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasolinc EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 74 of 79 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. slntRat Orcutt CA, 93457 Project Manager: Clarence Reynolds 04/06/2021 16:03 Notes and Definitions Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantization. D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyze concentration exceeds STLC limit. QR-03 The RPD value for the sample duplicate or MS!MSD was outside of QC acceptance limits due to matrix interference. QC batch accepted based on LCS and or LCSD recovery and/or RPD values. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. S-02 The surrogate recovery for this sample cannot be accurately quantified due to interference from coeluting organic compounds present in the sample extract. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 75 of 79 zs 0 u7 fV T U7 O 90 cu tl �sL N _ C 0. IL a 21 0 U = td LLCM cu a�u � R ILO S m ro Z W ,a. C N .°i a v E E m m E m o 0; t 0 m U P C J N N U . SPIIOS PGAlosta Iglol /4[AISO.UOOto m i agog tl1,908 a w 8Od / Lsed v d � p ao +GIII4tnlu6l C Q !fj U x C OOLZ9-s3OAS Qi w WSLOB OWaJ- dHlcx , z r7 a is BPUInS 1 eplueAD AAILSBou }Em- dgo C Q d Lsl-I Ilnj 809i8 o Z u N m A Z � ❑ sInew - LZ still y cL iA ci a m J a (1 4 m GI m y r+ N 124 IX CL a 0 a tmm C N Q C m. C OHO t� ❑� N # r m 91 la f I r t J 3 fi ,E0 U 0000 301 Z❑ 7 O` � � C m m m � •h�ry U Q C r.C.i (j LL 3 O Z U G O O❑ N n a m s�v x ❑ ❑ i .c 3 R r m UU' ...0 cc it C w E d _ s rw y o `m m o c m m w i� 0 to a c, O 00 U e s90 e.99 o ❑ w m •p '0 'O N m � 'LO y C. © C t t a `a Cc M n E m m E c c c vv�E,awv►-I- E m m m m p O n a o N LC) 0 co Co zs III 5 • ®_ IL . =a -tea E d U 7 r r r �❑ 2 t 0 ti yx 4 sPlloS N paAlosia Idol CIO ai w ci AIIAIsoLoO G O Z9091 H1,808 i a� 90d l lsad U �GlIlgGllu61 C N a: c Oozzo GOOAS at � O WOOD OWCIS - dHlCL X i o opuinS hEE o w r!1 a, W / oplueAC) anpoeea E m Zo N y ;sll Ilnd 809ZB 11 O z �o N ,a sinew zz Gull �. L u d w c ❑ m tv J m m m m `` g o > > p -m 5. L a m AJ ='o o_ co W a £ x _ co _ 00 00 CYJ El V — g � e � E of E ai E ❑ b:❑ 0% � �- c ~ ?:: 4 U O0 z C t,C ❑ O m d m m Qj es �' E C Oco W G co ❑ m❑ ❑ L o app V) D6 N z V N „ X . ❑ ❑ Te w W� S • V vO a W � 0. m y E ' rn� Fi k p N ca i o ❑ � • c `" CC O = L va C l4 6t � O o �5 �i � • � y _> ❑ � �❑ m m m m d m m m L 'O ei O O F O MO C Q Q inN N a m g og a d t F L 7 c 7 c= 7 N E 9t s m ' o r m d VCOO F _G cc d N 2 b E d N z 0 F v D r N U W 0. (n § 6. \ 00 0 & d \ « R z E z G 2 2 Ei ■ 2 � � 2 Bannon \ I 5 E 7 / § / § m - -0 (0) o o 7 0) _ £ ) ` z z « 'an)B CD = _ U 2 E \ ] @ c -0 a'a§ _ § \ , k / § 2 ) k Ef \ { k \ k § \ \ � D / Z) K) 3 / d 3 \ \ \ 2 § & & R / ƒ { ` ƒ ` )� � ® \ k _ 7 A k f 2 § :0: ¥ $ ) a k } - } _ ) . E $ 2 u ■ / a) CD § 7) « ` )ƒ§k2$0§ § z a \$ 2\ k w T 2 k 8\ %° \ s 7ƒ E E 2 S o < E 2 - 2 \ E) t f o // K) a{ 0 0\ 0 7 \ § « IL ) \ k) ƒ o D ® ' « 2 ) § o < 3 § / d \ b E£ G b A - .2) J J w \ R- /» w f/ 0 f 5co E 0 00 k E k o\ )«§ &\ b ■ o J o$ U CL \ E S § E 2 d O N N C I N E E O U d c `o U� 0 4) Z d N N d c a a a a a a a a UO2 aa a a a 7o a a a a a a a a a H,20- a dw a a a a0000000 0 0 0 0 0 0 0 00000000000 000000000 0 0 2� m m� m m U� m m� m m m m N m m(D U) m m U) U) U 0) fn m m W N co CD(n U) C C C C C C C C C C E s C C E C C C C G C C C E E E Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y l0 f0 Q N f0 Q (6 (0 Q N (0 Q N f0 Q f0 f0 Q W f6 Q f6 f0 Q N W Q f6 [0 Q W f0 Q f0 f0 ¢ N (6 Q > > , > , , , > eD 00 N 00 a0 N 00 OD N 00 00 N 00 00 N a0 a0 N 00 00 N 00 00 N c0 OD 00 00 N 00 00 N a0 00 N 00 00 N N N O N O N O) N O 01 O m N m al N rn rn N 0/ O O N d) O O) N O O O O O O O m N O O) O 0/ N O m O N O 0)Ov O NE O 61 v N v OJ a N o y y y y O y m ;g :o H(14 v o y y v o m a N LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL O .Q U N ¢ ¢ ¢ ¢ ¢ ¢ ¢ ¢ ¢ ¢ ¢ ¢ ¢ N N N N N O N fn N N O N N N N O N N N N O N N N N O N N N N O N N N N O N N N N O N N N N O N N N N O N N N N O N N N N N N N N O C l0 f0 > N f6 > f0 W > 2 f0 > 2 2 > f6 (0 > N f0 > (C f6 > f6 (6 > 9 T > N f6 > T (0 T f0 > (a () (7 J U (� J C7 U J O C7 J U C) J () (7 J(D () J (D O J (7 O J 0 U J C) O J 0 U ME CD (D J E N N E N N E N N E N N E N N E N N E N N E N N E N N E N N E N N E N N N N E 0 00 a0a0aDNa0a0 0 00 0 00N0NN0No Na0NeDa0 N a0 a0 Na0N No 00 0 a0apN 00 0 a0a0 0 0 a0 0 a0 N 0aD oU -O HT. °0 ¢ m U¢ m U¢ m U¢ m U¢ m U¢ O N N N M M M V I V<- U (O -.0U 00 000 0 0 0 0 0 0 0 0 0 f a I t a X CD mN C Elo E O N U J N U pCD CO O U N N y > a E w 00 O N t6 m ♦� N O> ♦�QiL o 4— 0 4. ♦v ++ o CL CL U V N c m to 0 m a 4 ' c A o 9 m e 1� ".! 0 a E E m o v _E F- H F- ❑ O 0 -1 E c SPIIOS =.1 PSAIOS10Idol 14lAlSOLOO G O p zoos Moe L � a� 93d ! 18edklimmusl v Qi � y a C Q V p" DOM-SOOAS LQ y w960eOwao-dHl iC }` !�x x; L d O zo ct GPUlnS F Z a y 39[ i Nnd f309Z8 o er N Zn tlJ 'L y Z ` +�+ i U m ❑ i C' d a 911"aw ZZ anli v a iv ro > m >, m h m M p 1 > O o N v > > c 0 N # m d m m N w 1 N U D: E To pJa ca II . 00 J ❑ _ .� o U � tL g th - f 5i E j-� 3 J S F- F- o,' d tn N `� f } 2�:•� Qr L' O r > � Z n 7 � ,0 LO C N 0 � Qm e4Y1 m m p E c Z V m p A O a❑ p N y E N •w l0 ui sr, h w OM . Q r eC3 O CL r O S N O o ce > c s o p N ^L ^( t K m > i a a O 00 U Ln r+1 n ❑ m m m y m CD m i. 'CS C O C t1 t`� w N N CL E o � U Q Z) G C C C N @ 4 U vi O F w U R o oz N a 0 ^0a � N � U � �y •>� � F l-' s7 0 m tz sPUOS tV Penlos101e1ol m ci m AllelsouoC) A i0 m G Q Q a e3d I lsed g U Ailli4eNuBl I C Q N U x oocze SODAS CL ws lae owao - dHl xx L yd0 ;p z ,a a, ePUlnS 1 ePluvAo enp0ee}t °' � isll Ilnd B09Ze z d eo N a d z y elew ZZ apil V 7�. `� 61 � Ci Z ❑ ayi a0 to o..N > > m a n N y Ot y m - o d A W m m c _ ¢ m W'. 00 ��X{' �x U 0,4 r C • E • d E F F E04 �. U 00 3 o b Z ❑ :r: w L 0 o (D 3 o n a o m' :�. m 33 m m,.•.L s ❑❑ xoll :. 00 c O U y u .r. �'�� o E d �i. � CS» y a o::: N CJ t N CM ....�j. i! Cl 7 a, 0 w 10 Q • �� 1.y V C E a O a. i O o 00 0S U z co • M +�. "� 2 Q ❑ m m m C p O a 7 P CL Ey t r el s yam.:. a o a l0 m C C C ct r� U ►- 1— J Ir Q' Q' 3: 6 Z O U a W IL U) is 00 4 u7 N O> C> 0 U- 8= a` F i a� aau m E E m E m o U 0 H H F 0 6 0 E m JuE m r Sp11oS peAIOSIO linol f�cra m ai 611AISOMOD w is io O O O k Zoos I woos � a> aOd I Wed U �tllgg11u81 rn c co m U J o OOLZB'SOOAS WSt080W0'J dHl } x v O 0 O Z L N cn , ar. co y E m h 03 epUluS epluvAO 8Altaeaa F— u m > C!? co d "� lSll llnd t309Z8 O 4 -` z SIeIeW - epll >< X cod CY, ZZ ayi r .o ❑ T J � Co m M p aES a _ 3 fl v c> a> 3 c =a < at O oo .+ OD S9. ❑ _m 0 3 a❑ cON £ EE E. ID U 00 3 zOQ O ( C c• . ' ' oo O„ E - QI Ql Gf Ix3 - 0 n❑s 8 L4C fr. N Y V d L G i �., 6t .O F .� w [Ys ,,,,,. .a 4 m i d• Q, d C d �. L p m a c a 0 O m K ,{ c% fl � ❑ m to n L m N a m a mCL y m O 7 F Vl N N E n nni d C E? d a 'w e c c A U vi U '-I CR I w U l F- a N C �D u V d m z 0 H U D z Q U W a rn 0 a K 9 co L6 N 6S cc U- 13 Xt a U Q• E E E c u .}. f= - 1= ❑ ❑ E m tti p� rJ•• m SPIIOS N Pen10810 IMOl ~ c� ci ui IGInISOMOO A Q 0 ZBoBI VLB0B ,n a 80d I ISed � � �illigellO81 x c Oo1ZS'SOOAS QS N WROBOMD-dHl X L d O z = a rn = d E es epUIOS I ePluedO en OBStj I w t0 d Z y is1111nj 8oBZ8 * Z N SIS1eW ` Zr 81111 d 8 Z 7 ❑ Cr V O� d etei .G ❑ m J v � G o � 0i V 1" c m a to d' -g N Q C N , CA ❑ m 4' v g _o E - Ll:. tn m ❑ U 000 z r.: a vi Ls. V to 3 N s ❑❑ x R u� c v� u i r G o _ i O p = G L N C O CL rn � y M at a O a L O o 00 6 U t� = y � • n'► • `-- ''� 2 � D ^, cu . E ::l: LS. 0. O l0 C C c Analytical Report Oilfield Environmental & Compliance, Inc. Clarence Reynolds OEC Work Order: 2101841 Pacific Petroleum California P. O. Box 2646 Report Date: March 26, 2021 17:07 Orcutt, CA 93457 Project: Pacific Petroleum Number: Natural Healing Centers, 2600 Broad St. Enclosed is an analytical report for the above referenced project. The samples included in this report were received on March 25, 2021 15:00 and analyzed in accordance with the attached chain -of -custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: Meredith Sprister, Business Director msprister@oecusa.com California ELAP Certification # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample Sample ID Laboratory ID Client Matrix Lab Matrix Date Sampled Date Received Tank N Wall Tank S Wall Tank E Wall Tank W Wall 2101841-01 2101841-02 2101841-03 2101841-04 Solid Solid Solid Solid Solid Solid Solid Solid 03/25/2021 11:15 03/25/2021 11:20 03/25/2021 11:25 03/25/2021 11:30 03/25/2021 15:00 03/25/2021 15:00 03/25/2021 15:00 03/25/2021 15:00 Tank Bottom E. End 2101841-05 Solid Solid 03/25/2021 11:05 03/25/2021 15:00 Tank Bottom W. End 2101841-06 Solid Solid 03/25/2021 11:10 03/25/2021 15:00 Sump Trench W 2101841-07 Solid Solid 03/25/2021 11:35 03/25/2021 15:00 Sump Trench S 2101841-08 Solid Solid 03/25/2021 11:38 03/25/2021 15:00 Control 2101841-09 Solid Solid 03/25/202111:00 03/25/2021 15:00 Soil Pile N 2101841-10 Solid Solid 03/25/2021 11:40 03/25/2021 15:00 Soil Pile S 2101841-11 Solid Solid 03/25/2021 11:45 03/25/2021 15:00 Soil Pile W 2101841-12 Solid Solid 03/25/2021 11:50 03/25/2021 15:00 Soil Pile E 2101841-13 Solid Solid 03/25/2021 12:10 03/25/2021 15:00 Sample Batch Preparation Analysis Batch ID Preparation Date/Time Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List BIC0798 03/25/2021 17:29 Total Metals by CVAA Mercury Total EPA 7471A B1('0807 03/26/2021 07:43 Total Metals by ICP 601013"Cotal B I C0810 03/26/2021 08:36 Volatile Organic Compounds by GC/MS 8260B Full List B 1 C0815 03/262021 09:17 8260B Full List B 1 C0817 03/26/2021 1 1:40 Volatile Organic TPH by GC/FID 9015 TPI I -Gasoline B 1 C0802 03/26;2021 05:22 8015 TPH-Gasoline B1C0804 03/2612021 05:26 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 2 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report foi- Samples Sample ID : Tank N Wall Sampled : 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID : 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mgtkg 1 B 1 C0807 03/26/21 14:37 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg -kg 1 B 1 C0910 03/26/21 13:30 EPA 6010B Arsenic 8.9 2.0 Barium 150 0.98 Bervllium 0.61 0.49 Cadmium ND 0.24 Chromium 51 0.49 Cobalt 17 0.49 Copper 28 0.98 Lead 9.1 0.49 Nlolvbdenum 2.6 0.49 " Nickel 76 0.49 Selenium ND 2.0 Silver ND 0.49 " Thallium ND 0.98 Vanadium 39 2.0 Zinc 32 2.0 Volatile Organic TPH by GC/FID TPI1 Gasoline (C5-C12) ND 4.9 mg/kg 1 BIC0802 03/26/21 10:47 EPA 8015M Surrogate: 4-Bromn/Zuoroben_ene 103 (31 - 168) 11 " 11 Semi -Volatile Organic TPH by GOOD TPH Diesel (03-C22) TPH Motor Oil (('23-C40) Surrogate: o-Telphenrl ND 10 mg/kg I BIC0798 03/26t21 07:48 EPA 8015M ND 50 " " " " " 107% (65-133) N-02 R-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report mnst be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 3 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 tng!kg 1000 BIC0815 03126`21 11:52 EPA 8260B Bromobenzene ND 1.2 Bromochlorotnethane ND 1.2 Bromodichloromethane ND 1.2 " Bromoform ND 1.2 Bromomethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 " tert-Butyl benzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzcne ND 1.2 Chloroethane ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Clilorotoluene ND 1.2 Dibromochloromethane ND 1.2 " 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethanc ND 1.2 1.2-Dichlorobenzene ND 1.2 1,3-I)ichlorobenzenc ND 1.2 1,4-Dichlorobenzcnc ND 1.2 " Dichloroditluoromethanc ND 1.2 I,I-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1,1-Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropatie ND 1.2 " 1,3-Dichloropropane ND 1.2 " 2,2-Dichloropropane ND 1.2 I,1-Dichloropropene ND 1.2 cis- 1.3 -Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 Ethylbenzenc ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 4 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Tank N Wall Sampled: 03/25/21 11:15 Matrix: Solid Sampled by: Lab ID: 2101841-01 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg'kg 1000 BIC0815 03126'21 11:52 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1. 1,2-Tetrachloroethane ND 1.2 1,1,22-Tetrachloroethane ND 1.2 Tetrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzcnc ND 1.2 " I,24-Trichlorobenzene ND 1.2 " 1,1,1-Trichloroethanc ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TC'E) ND 1.2 Trichlorolluoromethane ND 1.2 I.2.3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 " 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate. Dibromo/luoromethane 97 75 - 122) " Surrogate. Toluene-dh' 92 "/„ ( 66- 128 ) Surrogate: 4-B omnJluoroben_ene 92 go (76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way. Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 5 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.096 mg/kg 1 B I C0807 03/26/21 14:39 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg1kg 1 B 1 C0810 03/26/21 13:33 EPA 601(1B Arsenic 4.1 2.0 Barium 11 0.98 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 9.0 0.49 " Cobalt 1.4 0.49 Copper 3.5 0.98 Lead 2.5 0.49 Molybdenum 3.3 0.49 Nickel 6.8 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 6.3 2.0 Zinc 9.7 2.0 Volatile Organic TPH by GOOD TPII Gasoline (C5-C12) Sarrogate:4-Bromo/laoroben_ene Semi -Volatile Organic TPH by GOOD TPH Diesel (C13-C22) TP11 Motor Oil (C23-('40) Surrogate: o-Teiphernd ND 4.5 nig/kg I B I C0802 0312621 11:13 EPA 8015M 103 ";, (31-168) ND 10 mg!kg 1 BIC0798 03/26/21 10:07 EPA8015M ND 50 11"11 11 " IOh°;', (65-133) 11" R-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805; 925-3376 Page 6 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID : 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mglkg 1000 BIC0815 03/26/21 12:17 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 " Bromofortn ND 1.2 Bromotnethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butvlbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobcnzenc ND 1.2 Chlorocthanc ND 1.2 Chloroform ND 1.2 Chloromethane ND 1.2 2-Chlorotohene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromocthane (EDB) ND 1.2 Dibrtnnomethaue ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 " Dichloroditluoromcthane ND 1.2 " l,l-Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 " 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I,I-Dichloropropene ND 1.2 cis- 1.3 -Dichloropropene ND 1.2 mans-1,3-Dichloropropene ND 1.2 Ethylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 7 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Tank S Wall Sampled: 03/25/21 11:20 Matrix: Solid Sampled by: Lab ID: 2101841-02 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 I I exachlorobutadiene ND 1.2 mg%kg 1000 BIC0815 03/26/21 12:17 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 L1,1,2-Tetrachloroethane ND 1.2 1,1,22-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichlorocthane ND 1.2 1,1,2-Trichloroethane ND 1.2 Triehloroethene (TCE) ND 1.2 " Trichlorotluoromethane ND 1.2 1,2.3-Trichloropropane ND 1.2 1,2,4-Trimethylbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dibromq/kmromethanc 92 % (75 - 122 ) Surrogate: Toluene-d8 84 `:,, ( 66 - 128 ) Surrogate: 4-Bromo luorohen-ene 92 % (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 8 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical t Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.092 mg/kg 1 BIC0807 03/26/21 14:41 EPA 7471A Total Metals by ICP Antimony ND 2.4 mglkg 1 B 1 C'0810 03/26/21 13:36 EPA 6010B Arsenic 4.2 1.9 Barium 140 0.95 " Bervllium 0.51 0.47 Cadmium ND 0.24 Chromium 52 0.47 N-02 Cobalt 16 0.47 Copper 23 0.95 " Lead 7.0 0.47 Molybdenum ND 0.47 Nickel 72 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.95 Vanadium 33 1.9 Zinc 20 1.9 " Volatile Organic TPH by GC/FID TPNGasoline (C5-C12) ND 4.6 mg/kg 1 BIC0802 03/26'21 11:39 EPA8015M R-07 Surrogate: 4-Bromo/7uoroben_ene 104 % (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) ND 9.9 mg/kg 1 B1('0798 03/26/21 09:02 EPA 8015M TPH Motor Oil (('23-C40) ND 50 " " " " Surrogate: o-Tecrhem•1 108 ,11 11 (65 - 133) " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 11805 925-3376 Page 9 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID : Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GOMS R-07 Benzene ND 1.2 mg!kg 1000 B1C'0815 03/26/2112:43 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 " Bromodichloromethane ND 1.2 Broniofonn ND 1.2 Bromomethane ND 1.2 " n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 " Chlorobenzenc ND 1.2 Chlorocthane ND 1.2 C'hlorofbnn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibronio-3-chloropropane ND 1.2 12-Dibromocthane (FDB) ND 1.2 Dibromomethane ND 1.2 " 12-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodifluoromelhanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 I,1-Dichloroethene ND 1.2 cis-1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1,1-Diehloropropene ND L2 cis- 1.3-Diehloropropene ND 1.2 trans-1,3-Diehloropropene ND 1.2 Fthylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 10 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Tank E Wall Sampled: 03/25/21 11:25 Matrix: Solid Sampled by: Lab ID : 2101841-03 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) R-07 Hexachlorobutadiene ND 1.2 mg/kg 1000 B1 C0815 03/26/21 12:43 EPA 8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 " Methylene chloride ND 1.2 " Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Stvrene ND 1.2 " 1,1.1,2-Tetrachloroethane ND 1.2 1,1,2,2-Tetrachlorocthane ND 1.2 Tetrachlorocthene ( PCEI ND 1.2 " TOInenC ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroelhane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorothwromethane ND 1.2 1.23-Trichloropropane ND 1.2 " 1,2,4-1'rimethylbenzene ND 1.2 1.3,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dihrunu,lhunrnyr glrauri• 92 N, ( 75- 122) Surrogate: Toluene-dR 95 "„ ( 66 - 128) Surrogate: 4-Broniglluoroben_ene 90 4,, (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 11 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.094 mg/kg 1 BIC0807 03/26/21 14:44 EPA 7471A Total Metals by ICP Antimony ND 2.3 mglkg I BlC08I0 03/26/2113:38 EPA 6010B Arsenic 2.6 1.8 Barium 5.8 0.92 Beryllium ND 0.46 Cadmium ND 0.23 Chromium 6.9 0.46 Cobalt 0.92 0.46 Copper 1.9 0.92 Lead 3.7 0.46 Molybdenum 2.6 0.46 " Nickel 4.1 0.46 Selenium ND 1.8 " Silver ND 0.46 Thallium ND 0.92 Vanadium 4.6 1.8 Zinc 6.8 1.8 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 35 5.1 mg.1kg 1 BIC0802 03/26/21 12:05 EPA 8015M Surrogate: 4-Bronm/luorohenzene 14S 9, (31 - 168) 11" 11 Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate: o-Teiphen.Vl 17 9.9 mg/kg 1 72 50 " " 107'/, (65 - 133 ) BIC0798 03J26'21 11:03 EPA 8015M D-04 D-04 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 e 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 12 of 65 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID : Tank W Wall Sampled : 03/25/21 11:30 Matrix: Solid Sampled by : Lab ID : 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mg/kg 1000 B 1 C'0815 03/26/21 13:08 EPA 8200B Bmmobenzene ND 1.2 Bromochloromethane ND 1.2 " Brontodichloromethane ND 1.2 Bromoform ND 1.2 Bromomethane ND 1.2 " n-BuMbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 " " Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethanc ND 1.2 Chloroform ND 1.2 " Chloromethane ND 1.2 2-Chlorotohiene ND 1.2 4-Chlorotoluene ND 1.2 " " Dibromochloromethanc ND 1.2 1,2-Dibronto-3-chloropropane ND 1.2 1,2-Dibrotnoethane (EDB) ND 1.2 Dibromontethane ND 1.2 1.2-Dichlorobenzene ND 1.2 13-Dichlorobcnzenc ND 1.2 1,4-Dichlorobenzcnc ND 1.2 Dichlorodilluoromethane ND 1.2 1, 1 -Diehl oroet h ane ND 1.2 1,2-Dichloroethaue ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1,2-Dichloropropane ND L2 1,3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-1,3-Dichloropropene ND 1.2 trans- l,3-Dichloropropene ND 1.2 Ethylbenzenc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 13 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank W Wall Sampled: 03/25/21 11:30 Matrix: Solid Sampled by: Lab ID: 2101841-04 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GGMS (Continued) R-07 Ilexachlorobutadiene ND 1.2 mg'kg 1000 B1('0815 03/262113:08 FPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 1, 1, 1,2-Tetrachloroethane ND 1.2 1,1,2,2=Tetrachlorocthane ND 1.2 Tctrachlorocthene (PCE) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,24-Trichlorobenzene ND 1.2 1, 1, 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Triehloroethene (TCF) ND 1.2 " Trichlorofluoromethane ND 1.2 1,2,3-Trichloropropane ND 1.2 " 1.2.4-Trimethylbenzene ND 1.2 1,3.5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Uibromo luoromethanr 95 '% (75 - 122 ) Surrogate: Tolucne48 95 % ( 66 - 12S ) Surrogate: 4-BromuJTtturuheu=enc 92 `,, (76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805) 925-3376 Page 14 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by : Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.095 mgrkg I B 1 C0807 03/26/21 14:46 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mgrkg 1 B1C0810 03/26/21 13:41 EPA 0010B Arsenic 5.4 1.9 Barium 32 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 15 0.47 Cobalt 4.3 0.47 Copper 11 0.93 " Lead 8.3 0.47 Molybdenum 2.9 0.47 " Nickel 19 0.47 Selenium ND 1.9 Silver ND 0.47 " Thallium ND 0.93 Vanadium 13 1.9 Zinc 19 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-('12) 35 4.9 nig/kg 1 BIC0802 03/26/21 12:31 EPA 8015M Surrogate 4-Bromu/luorobenzene 145 e/., (31 - 168) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 11 10 mg/kg 1 BIC0798 03/2621 11:31 EPA 8015M D-04 TPH Motor Oil (C23-('40) 110 50 " " " D-04 Surrogate: o-Terphenr( 106 `S6 (65 - 133 ) 11 11 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report mast be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oacusa.com FAX: (805) 925-3376 Page 15 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 I Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by: Lab ID: 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 1.2 mgtkg 1000 B1C0815 03/26/2113:34 EPA8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bromoforin ND 1.2 Bromomcthane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 " tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethanc ND 1.2 Chlorotbmm ND 1.2 Chloromethane ND 1.2 " 2-Chlorotoluene ND 1.2 4-C'hlorotoluene ND 1.2 " Dibromochloromethane ND 1.2 1,2-Dibrouio-3-chloropropane ND 1.2 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 1,2-Dichlorobenzene ND 1.2 1,3-Dichlorobenzene ND 1.2 1,4-Dichlorobenzene ND 1.2 Dichlorodilluoromethanc ND 1.2 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 1, 1 -Dichloroethene ND 1.2 cis-1,2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 1.3-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 I.1-Dichloropropene ND 1.2 cis- 1.3-Dichloropropene ND 1.2 trans- l,3-Dichloropropene ND 1.2 Etylbenzene ND 1.2 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 16 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank Bottom E. End Sampled: 03/25/21 11:05 Matrix: Solid Sampled by: Lab ID : 2101841-05 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 1.2 nl_L' kg I1111!) B I COX 1 S 03 '_h : 1 11 id EPA 8260B 4-Isopropyl Toluene ND 1 2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 Naphthalene ND 1.2 n-Propylbenzene ND 1.2 " Styrene ND 1.2 1,1,1.2-Tetrachloroethane ND 1.2 1,1,22-Tetrachloroethane ND 1.2 Tetrachlorocthene IPCE) ND 1.2 Toluene ND 1.2 1,23-Trichlorobenzene ND 1.2 1,14-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichlorofluoromethanc ND 1.2 1,2,3-Trichloropropane ND 1.2 1,2,4-Trimethvlbenzene ND 1.2 13,5-Trimethylbenzene ND 1.2 Vinyl chloride ND 1.2 Xylenes (total) ND 1.2 Surrogate: Dihranofthumomethane 95 ; ( 75 - 122) " Surrogate: Toluene-d8 86Ni, ( 66 - 12S ) " Surrogate: 4-Bromco/lum•ohen:ene 94 % (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 WWW.oecusa.Com FAX: (805) 925-3376 Page 17 of 65 DIC-IN Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank Bottom W. End Sampled: 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID: 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.091 mg/kg 1 BI('0807 03/26/21 14:48 EPA 7471A Total Metals by ICP Antimony ND 2.4 mgrkg 1 Bl C0810 03/26/21 13:44 EPA 601 OB Arsenic ND 2.0 Barium 9.9 0.98 " Beryllium ND 0.49 " Cadmium ND 0.24 Chromium 8.0 0.49 Cobalt 1.2 0.49 Copper 1.6 0.98 Lead 3.4 0.49 Alolvbdenum 1.1 0.49 ]Nickel 4.7 0.49 Selenium ND 2.0 Silver ND 0.49 Thallium ND 0.98 Vanadium 5.9 2.0 Zinc 7.9 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 6.1 4.5 mg/kg 1 B1('0804 03/26/21 10:55 EPA 8015M Surrogate: 4-Brum0llaorobe11:7ene 108 % (31 - 168) " Semi -Volatile Organic TPH by GC/FIB TPH Diesel (('13-('22) ND 9.9 mgikg 1 B1('0798 03/26/21 10:21 EPA 8015M TPH Motor nil (C23-('40) ND 50 "11" " " Surrogate: o-Terrherrrl 106 9f, (65 - 133) 11 11 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 18 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Tank Bottom W. End Sampled: 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 ingIg 1000 BIC0815 03/26/21 13:59 F.PA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Broniodichloromethane ND 1.2 Bromofornn ND L2 Bromanethane ND 1.2 n-Butylbenzene ND 1.2 sec-Butylbenzene ND 1.2 tert-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzcne ND 1.2 Chloroethanc ND 1.2 Chlorotbnn ND 1.2 Chloromethane ND 1.2 2-Chlorotoluene ND 1.2 4-Chlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1.2-Dibromo-3-chloropropane ND 1.2 1,2-Dibromoethane (FDB) ND 1.2 Dibromomethane ND 1.2 1.2-Dichlorobenzene ND 1.2 1,3-Dichlorobcnzene ND 1.2 I A-Dichlorobcnzene ND 1.2 Dichlorodilluorinnethane ND 1.2 " 1, 1 -Dichloroethane ND 1.2 1,2-Dichloroethane ND 1.2 " I,I-Dichloroethene ND 1.2 cis- 1.2-Dichloroethene ND 1.2 trans-1,2-Dichloroethene ND 1.2 1.2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1, 1 -Dichloropropene ND 1.2 cis-l3-Dichloropropanc ND 1.2 trans-1,3-Dichloropropanc ND 1.2 F.thylbenzcnc ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 19 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sample ID: Tank Bottom W. End Sampled : 03/25/21 11:10 Matrix: Solid Sampled by: Lab ID : 2101841-06 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 14exachIorobutadiene ND 1.2 mg/kg 1000 BIC0815 03/26/21 13:59 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND 1.2 Methylene chloride ND 1.2 " Naphthalene ND 1.2 n-Propylbenzene ND 1.2 Styrene ND 1.2 1,1,1,2-Tetrachloroethane ND 1.2 1.1,2.2-Tetrachloroethane ND 1.2 Tctrachlorocthcne (PCE) ND 1.2 Toluene ND 1.2 1.2,3-Trichlorobcnzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1,1,1-Trichloroethane ND 1.2 " 1,1,2-Trichloroethane ND 1.2 Trichloroethane (TCE) ND 1.2 Trichlorofluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 1.2,4-Triniethylbenzene ND 1.2 " 13,5-Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 Xylencs (total) ND 1.2 Surrogate: Dibronuglluoromethane 93 . (75 - 122) Surrogate: Tohiene-dh h'S IN (66 - 12S ) Surrogate: 4-Brornoffito oben_ene 94 % (76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX (805) 925-3376 Page 20 of 65 &T*�, Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.089 mg'kg 1 B 1 C0807 03/26/21 14:54 EPA 7471 A Total Metals by ICP Antimony 8.2 2.4 mg/kg 1 B1('0810 03/26/21 13:47 EPA 601(IB Arsenic 8.9 1.9 Barium 260 0.96 Beryllium NI) 0.48 Cadmium ND 0.24 Chromium 55 0.48 " Cobalt 12 0A8 Copper 120 0.96 " Lead 550 0.48 Molybdenum 1.1 0.48 Nickel 150 0.48 Selenium ND 1.9 Silver ND 0.48 " Thallium ND 0.96 " Vanadium 33 1.9 Zinc 720 1.9 Volatile Organic TPH by GC/FID N-02 N-02, N-03 TPH Gasoline (('5-C12) ND 4.9 mgtkg 1 B1('0804 03/26`21 11:52 EPA 8015M R-07 Surrogate: 4-Bromolluorohenrene 100 4b (31 - 168) 11 " Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 71 40 mg/kg 4 BIC0798 03/26'2111:59 EPA8015M D-04 TPH Motor Oil (C23-C40) 520 200 " " " " " D-04 Surrogate: o-Tciphern l 1081,111) (05 - 133) 11 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 21 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID: 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS R-07 Benzene ND 1.2 mglkg 1000 B 1 C0815 03/26/21 14:25 EPA 8260B Bromobenzene ND 1.2 Bromochloromethane ND 1.2 Bromodichloromethane ND 1.2 Bronioform ND 1.2 Bromomethane ND 1.2 n-Butvlbenzene ND 1.2 " sec-Butylbenzene ND 1.2 tort-Butylbenzene ND 1.2 Carbon tetrachloride ND 1.2 Chlorobenzene ND 1.2 Chloroethane ND 1.2 C'hlorolbrm ND 1.2 Chloroniethane ND 1.2 2-Chlorotolaenc ND 1.2 4-C'hlorotoluene ND 1.2 Dibromochloromethane ND 1.2 1,2-Dibronxi-3-chloropropane ND 1.2 " 1,2-Dibromoethane (EDB) ND 1.2 Dibromomethane ND 1.2 12-Dichlorobenzene ND 1.2 1.3-Dichlorobenzene ND 1.2 1,4-Dichlorobeivenc ND 1.2 Dichloroditluoromcthane ND 1.2 1, 1 -Dichloroethane ND 1.2 " 1,2-Dichloroethane ND 1.2 1,1-Dichloroethane ND 1.2 cis-L2-Dichloroethene ND 1.2 trans-1,2-Dicliloroethene ND 1.2 1,2-Dichloropropane ND 1.2 13-Dichloropropane ND 1.2 2,2-Dichloropropane ND 1.2 1.1-Dichloropropene ND 1.2 cis-1.3-Dichloropropene ND 1.2 trans-1,3-Dichloropropene ND 1.2 F.thylbenzene ND 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 22 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample ID: Sump Trench W Sampled: 03/25/21 11:35 Matrix: Solid Sampled by: Lab ID : 2101841-07 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Hexachlorobutadiene ND 1.2 mgncg 1000 BIC0815 03/26/2114:25 EPA8260B 4-Isopropyl Toluene ND 1.2 Isopropylbenzene ND L2 Methylene chloride ND 1.2 Naphthalene ND 1.2 " n-Propylbenzene ND 1.2 Styrene ND 1.2 " 1. 1, 1,2-Tetrachloroethane ND 1.2 " 1.1,2,2-Tetrachloroethane ND 1.2 " Tetrachloroethenc (PCIi) ND 1.2 Toluene ND 1.2 1,2,3-Trichlorobenzene ND 1.2 1,2,4-Trichlorobenzene ND 1.2 1, 1. 1 -Trichloroethane ND 1.2 1,1,2-Trichloroethane ND 1.2 Trichloroethene (TCE) ND 1.2 Trichloroiluoromethane ND 1.2 1,23-Trichloropropane ND 1.2 " 1,2,4-Trimethylbenzene ND 1.2 " 1,3,5-Trimethylbenzene ND 1.2 " Vinyl chloride ND 1.2 " Xylenes (total) ND 1.2 " Surrogate: Dihrontolhmronicthane 97 3b ( 75 - 122 ) Surrogate: Toluene-dR 90'N< (66 - 128 ) Surrogate: 4-Bronio)luoroheircne RS /, ( 76 - 122) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 23 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.098 mgtkg 1 B 1 C0907 03/26/21 14:56 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgtkg I BIC0810 03/26/21 13:50 EPA 601OB Arsenic 4.1 1.9 Barium 180 0.96 Bervllium 0.53 0.48 Cadmium ND 0.24 Chromium 78 0.48 Cobalt 16 0.48 Copper 31 0.96 Lead 37 0.49 Molybdenum ND 0.48 Nickel 100 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 47 19 Zinc 69 1.9 Volatile Organic TPH by GC/FID N-02 TP1) Gasoline 105-C121 ND 4.7 mg/kg I BIC0804 03/26./21 12:20 EPA 8015M R-07 Surrogate: 4-Bromo/luoroben_ene 107':0 (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) 27 9.9 mgtkg 1 B1('0798 03/26/21 13:02 EPA 8015M D-06 TPH Motor Oil (C23-C40) 610 50 " " " " 11 Surrogate: o-Teiphem l 107 (65 - 133) " 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 24 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples I Sample ID: Sump Trench S Sampled : 03/25/21 11:38 Matrix: Solid Sampled by: Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mglkg 1 BIC0817 03/26/21 13:46 FPA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Brornoform ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butyl benzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzcne ND 0.0050 " Chhtrocthanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromuchloromethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (EDB) ND 0A050 Dibromoutethane ND 0.0050 1,2-Dichlorobenzenc ND 0.0050 1.3-Dichlorobenzenc ND 0.0050 1,4-Dichlorobenzenc ND 0.0050 Dichlorodiiluoromcthane ND 0.0050 1. 1 -Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 I,I-Dichloroethene ND 0.0050 cis-1.2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 " 12-Dichloropropane ND 0.0050 1.3-Dichloropropane ND 0.0050 2.2-Dichloropropane ND 0,0050 1. 1 -Dichloropropene ND 0.0050 cis- I3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 1=thylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 25 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: R O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Sample ID: Sump Trench S Sampled: 03/25/21 11:38 Matrix: Solid Sampled by : Lab ID : 2101841-08 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) llexachlorobutadiene ND 0.0050 mg/kg I B 1('0817 03/26/21 13:46 EPA 8260B 4-Isopropyl Toluene ND 0.0050 lsopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1, 1, 1,2-Tetrachloroethane ND 0.0050 1,1,2,2-1'etrachloroethane ND 0.0050 7ctrachlorocthcnc (PCE) ND 0.0050 Toluene ND 0.0050 1,2.3-Trichlorobenzene ND 0.0050 1,2,4-Trichlorobenzene ND 0.0050 I,I,I-Trichloroethane ND 0.0050 1,1,2-Tricliloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 Trichlorofluoromethane ND 0.0050 1,2.3-Trichloropropane ND 0.0050 1,2,4-Trimethylbenzene ND 0.0050 1,3,5-Triniethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylcncs (total) ND 0.0050 Surrogate: Dihromolluoromethane 94 %, ( 75 - 122 ) Surrogate: Toluene-dS 89111„ (66 - 128) Sw•rogate: 4-Brontnfluorohen_ene• 89 `:,, ( 76 - 122) " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 26 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID: 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method 7 Notes Total Metals by CVAA Mercury 0.14 0.095 mgikg 1 B I C0807 03/26/21 14:58 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mg/kg 1 B I C0810 03/26/21 13:52 EPA 601013 Arsenic 5.9 1.9 Barium 170 0.97 Bervllium 0.50 0.49 Cadmium ND 0.24 Chromium 41 0.49 Cobalt 16 0.49 Copper 27 0.97 Lead 10 0.49 Molybdenum ND 0.49 Nickel 38 0.49 Selenium ND 1.9 Silver ND 0.49 Thallium ND 0.97 Vanadium 33 1.9 Zinc 27 1.9 Volatile Organic TPH by GC/FID TPH UasoIme (C5-C12) ND Surrogate: 4-Bronm/hnirohen_ene Semi -Volatile Organic TPH by GC/FID 4.7 mgIkg I BIC0804 03/26/21 12:49 EPA8015M R-07 96% (31-168) " 11" TPH Diesel (CI3-C22) ND 10 TPH Motor Oil (C23-C40) 85 50 Surrogate: o-Terphenrl 105'%0 mg/kg I BIC0798 03/26/21 10:49 EPA8015M (65-133) 11" 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 27 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Control Sampled: 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID : 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mgtkg 1 BIC0817 03/26/21 14:44 FPA8260B Bromobenzene ND 0.0050 Bronuichloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromofonn ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tort-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobcnzenc ND 0.0050 " Chlorociliane ND 0.0050 " Chloroform ND 0.0050 C'hloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 Dibromochloronrethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (EDB) ND 0.0050 " Dibromomethane ND 0.0050 " 1.2-Dichlorobenzene ND 0.0050 1,3-Dichlorobenzene ND 0.0050 1,4-Dichlorobenzene ND 0.0050 Dichlorodifluoromethane ND 0.0050 " 1,1-Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 LI-Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 13-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.00(1 1.1-Dichloropropene ND 0.0050 cis-13-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 " Fthylbenzcne ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 28 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Control Sampled : 03/25/21 11:00 Matrix: Solid Sampled by: Lab ID : 2101841-09 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) llexachlorobutadiene ND 0.0050 mglkg 1 B1C0817 03/26/2) 14:44 EPA8260E 4-1sopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethane ND 0.0050 1.1,2.2-1'etrachloroethane ND 0.0050 Tetrachlorocthcne (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Tricliloroben7cne ND 0.0050 1,2,4-Trichlorobenzene ND 0.0050 1,1.1-Trichloroethane ND 0.0050 1,1,2-Tricliloroethane ND 0.0050 Tricbloroethene (TCE) ND 0.0050 " Trichlorofluoromethane ND 0.0050 " 1,2,3-Trichloropropane ND 0.0050 L2,4-Trimethylbenzene ND 0.0050 1,3.5-Trimethylbenzene ND 0.0050 " Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: Dihronwlluorome thane 93 % ( 75 - 122 ) Surrogate: Toluene-d8 95 '.' ; (66 - 128) Surrogate: 98111, f 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 29 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by : Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.099 mg/kg 1 B 1('0807 03/26/21 15:00 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg 1 B I C0810 03/26/21 13:55 EPA 601 OB Arsenic 3.6 2.0 Barium 13 LO Beryllium ND 0.50 Cadmium ND 0.25 Chromium 11 0.50 Cobalt 1.9 0.50 " Copper 5.3 LO Lead 4.3 0.50 Molybdenum 2.5 0.50 Nickel 9.0 0.50 Selenium I 2.0 Silver ND 0.50 Thallium ND 1.0 Vanadium 8.4 2.0 Zinc 8.8 2.0 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) 42 4.9 mg/kg 1 BIC0804 03/26/2113:17 EPA8015M Surrogate: 4-Broniglluorobenzene 196 1% (31 - 168) S-02 Semi -Volatile Organic TPH by GC/FID TPII Diesel (C13-C22) ND 9.9 mg.!kg I BIC0798 03/26/21 10:35 EPA 8015M TPH Motor Oil (C23-C40) 52 50 " " " " " Surrogate: o-Terphenl,l 106 7b 11 (65 - 133) " " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 30 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene ND 0.045 mg/kg 1 B I C0817 03/26/21 12:49 EPA 8260B Bromobenzene ND 0.045 Bromochlorometliane ND 0.045 Bromodichloromethane ND 0.045 Bromofonn ND 0.045 Bromoinethane ND 0.045 n-Butvlbenzene 0.22 0.045 sec-Butvlbenzene 0.11 0.04.5 tert-Butylbenzene ND 0.045 Carbon tetrachloride ND 0.045 Chlorobenzene ND 0.045 Chloroethane ND 0.045 Chloroform ND 0.045 Chloromethanc ND 0.045 2-Chlorotoluenc ND 0.045 " 4-Chlorotoluene ND 0.045 " Dibromochloromethane ND 0.045 1,2-Dibromo-3-chloropropane ND 0.045 " 1,2-Dibromoethane (EDB) ND 0.045 Dibromomethane ND 0.045 1,2-Dichlorobenzene ND 0.045 1,3-Dichlorobenzene ND 0.045 " 1,4-Dichlorobenzene ND 0.045 Dichlorodifluoromethane ND 0.045 1,1-Dichlorocthanc ND 0.045 1,2-Dichlorocthanc ND 0.045 1,1-Dichloroethene ND 0.045 cis-1,2-Dichloroethene ND 0.045 trans-1,2-Dichloroethene ND 0.045 1,2-Dichloropropane ND 0.045 " 13-Dichloropropane ND 0.045 12-Dichloropropane ND 0.045 1, 1 -Dichloropropene ND 0.045 cis- 1.3 -Dichloropropene ND 0.045 " trans-1,3-Dichloropropene ND 0.045 Euylbenzene ND 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 31 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile N Sampled: 03/25/21 11:40 Matrix: Solid Sampled by: Lab ID : 2101841-10 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) R-07 Ilexachlorobutadiene ND 0.045 mg/kg 1 B1(`0817 03/26/2112:49 EPA8260B 4-Isopropyl Toluene ND 0A45 Isopropylbenzene ND 0.045 Methylene chloride ND 0.045 Naphthalene ND 0.045 n-Propylbenzene 0.15 0.045 Styrene ND 0.045 1,1,1,2-Tetrachloroethane ND 0.045 1,1,2,2-Tetrachloroethane ND 0,045 " Tetrachloroethene WCE) ND 0.045 Toluene ND 0.045 1,23-Trichlorobenzene ND 0.045 1,2,4-Trichlorobenzene ND 0.045 1,1,1-Triehloroethanc ND 0.045 1,1,2-Trichloroethane ND 0.045 Trichloroethene (TCF.) ND 0.045 'Frichlorotluoromethane ND 0.045 1,2,3-Trichloropropanc ND 0.045 1,2,4-Trimcthylbcnzenc ND 0.045 1,3,5-Trimethylbenzene ND 0.045 Vinyl chloride ND 0.045 Xylenes (total) ND 0.045 Surrogate: 92 :'o (75 - Ill) " Surrogate: Toluene-da 97 % (66 - 128 ) Surrogate: 4-Bromo/luorohencene 99 "'„ ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 32 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical t Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID: 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mg/kg 1 B I C0807 03/26/21 15:02 EPA 7471 A Total Metals by ICP Antimony ND 2.5 mg/kg I B1('0810 03/26/21 14:06 EPA 601OB Arsenic 4.5 2.0 Barium 47 LO Beryllium ND 0.50 Cadmium ND 0.25 " Chromium 18 0.50 Cobalt 3.6 0.50 Copper 9.8 1.0 Lead 16 0.50 Molybdenum 2.1 0.50 Nickel 36 0.50 Selenium ND 2.0 Silver ND 0.50 Thallium ND LO Vanadium 15 2.0 Zinc 29 2.0 Volatile Organic TPH by GC/FID TPI I Gasoline (C5-C 12) ND 4.4 mg/kg 1 B I C0804 03/26/21 13:46 EPA 8015M R-07 Surrogate: 4-Bromolluoroben_ene 100 "/„ (31 - 168) 11" 11 Semi -Volatile Organic TPH by GC/FID TPH Diesel (C13-('22) ND 10 mgIg 1 B1('0798 03/26/21 12:27 EPA 8015M TPII Motor Oil (C23-C40) 260 50 " " " " " Surrogate. o-Tetphenrl 10S 1.� (65 - 133 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oee.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 33 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GCIMS Benzene ND 0.0049 mg/kg 1 B I ('0817 03/26/21 15:13 EPA 8260B Brontobenzene ND 0.0049 Bromochloromethane ND 0.0049 Bromodichlorancthane ND 0.0049 " Bromofonn ND 0.0049 Bromomethane ND 0.0049 n-Butylbenzene ND 00049 sec-Butylbenzene ND 0.0049 tert-Butylbenzene ND 0.0049 Carbon tetrachloride ND 0.0049 Chlorobenzcnc ND 0.0049 Chloroethane ND 0.0049 Chloroform ND 0.0049 Chloromethane ND 0.0049 " 2-Chlorotoluene ND 0.0049 4-C'hlorotoluene ND 0.0049 Dibromochloromethane ND 0.0049 1,2-Dibromo-3-chloropropane ND 0.0049 1.2-Dibrontoethane (EDB) ND 0.0049 Dibromomethane ND 0.0049 1,2-Dichlorobenzene ND 0.0049 1,3-Dich1orobcnzcnc ND 0.0049 1,4-Dichlorobcnzcnc ND 0.0049 Dichloroditluoromcthanc ND 0.0049 1J-Dichloroethane ND 0.0049 1,2-Dicliloroethane ND 0.0049 I J-Dichloroethene ND 0.0049 cis-1,2-Dichloroethene ND 0.0049 trans-1,2-Dichloroethene ND 0,0049 1,2-Dichloropropane ND 0.0049 I.3-Dichloropropane ND 0.0049 2,2-Dichloropropane ND 0.0049 1, 1 -Dichloropropene ND 0.0049 cis- I3-Dichloropropene ND 0.0049 trans-1,3-Dichloropropene ND 0.0049 Ethylbenzene ND 0.0049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Wa,, . Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 34 of 65 O-qM f 1W 1&111� Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile S Sampled: 03/25/21 11:45 Matrix: Solid Sampled by: Lab ID : 2101841-11 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) IIexachi orobutadiene ND 0.0049 mg -'kg 1 BIC0817 03/20/21 15:13 EPA 8260B 4-Isopropyl Toluene ND 0.0049 lsopropylbenzene ND 0.0049 Methylene chloride ND 0.0049 Naphthalene ND 0.0049 " n-Propylbenzene ND 0.0049 Styrene ND 0.0049 1,1,1,2-Tetrachloroethane ND 0.0049 1,1.2.2-Tetrachloroethane ND 0.0049 Tetrachlorocthcne (PCE) ND 0,0049 Toluene ND 0.0049 1.2,3-Trich1orobcnzcnc ND 0.0049 1,2,4-Trichlorobenrene ND 0.0049 1, 1, 1 -Trichloroethane ND 0.0049 1,1,2-Trichloroethane ND 0.0049 Trichloroethene (TCE) ND 0.0049 Trichlorolluorotnethane ND 0.0049 12.3-Trichloropropane ND 0.0049 1,14-Trimethylbenzene ND 0.0049 13.5-Triiuethylbenzene ND 0.0049 Vinyl chloride ND 0.0049 Xylencs (total) ND 0.0049 Surrogate: Dibrontglhmrornethmu• 91 ;a ( 75 - 122) Surrogate: Toluenc-e18 95 ,,, (66 - 128 ) Surrogate: 4-BromnJ7noruhen_c'ne 97 9b ( 76 - 122 ) The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIle nt.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 35 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.097 mg/kg 1 B I C0807 03/26/21 15:04 EPA 7471 A Total Metals by ICP Antimony ND 2.3 mg/kg 1 B I C0810 03/26/21 14:09 EPA 601(1B Arsenic 5.6 1.9 Barium 23 0.93 Beryllium ND 0.47 Cadmium ND 0.23 Chromium 14 0.47 Cobalt 2.5 0.47 Copper 6.8 0.93 Lead 7.3 0.47 Molybdenum 3.7 0.47 Nickel 11 0.47 Selenium ND 1.9 Silver ND 0.47 Thallium ND 0.93 Vanadium 15 1.9 Zinc 15 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.7 mg 'kg 1 BIC0804 03/26/21 14:14 EPA 8015M R-07 Surrogate: 4-Brotno/luoroben_ene 103 "5i (31 - 168) " Semi -Volatile Organic TPH by GC/FID TP11 Diesel (('13-C22) ND 9.9 mg/kg 1 BIC0798 03/26'21 11:17 EPA 8015M TPH Motor Oil (('23-C40) 75 50 " " " " " D-04 Surrogate. o-Kvphctpd 107 (65 - 133) 11" The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cllent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 36 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report for Samples Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID : 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS Benzene ND 0.0050 mgtkg 1 B I C0817 03/26/21 15:43 P.PA 8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 Bromofonn ND 0.0050 Bromomethane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene ND 0.0050 Carbon tetrachloride ND 0.0050 Chlorobcnzene ND 0.0050 Chloroethanc ND 0.0050 Chloroform ND 0.0050 Chloromethane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 " Dibromochloromethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 1,2-Dibromoethane (F.DB) ND 0.0050 " Dibromoniethane ND 0.0050 1,2-Dichlorobenzene ND 0.0050 1.3-Dichlorobenzene ND 0.0050 " 1,4-Dichlorobe117e11e ND 0.0050 Dichlorodilluoromethane ND 0.0050 1,1-Dichloroethane ND 0.0050 1,2-Dichloroethane ND 0.0050 l,l-Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 1,1-Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 trans-1,3-Dichloropropene ND 0.0050 lithylbenzene ND 0.00150 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 37 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Analytical Report Sample ID: Soil Pile W Sampled: 03/25/21 11:50 Matrix: Solid Sampled by: Lab ID: 2101841-12 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS (Continued) Hexachlorobutadiene ND 0.0050 mg/kg I B1C"0817 03/26/21 15:43 EPA826013 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 Naphthalene ND 0.0050 n-Propylbenzene ND 0.0050 Styrene ND 0.0050 1,1,1,2-Tetrachloroethanc ND 0.0050 " 1.1,22-Tetrachloroethanc ND 0.0050 Tetrachlorocthcne (PCE) ND 0.0050 Toluene ND 0.0050 1,2,3-Trichlorobenzcnc ND 0.0050 1,2,4-Trichlorobenrene ND 0.000 1, 1, 1 -Trichloroethane ND 0.0050 1,1,2-Trichloroetliane ND 0.0050 Trichloroethene (WE) ND 0.0050 Trichlorolluoromethanc ND 0.0050 1,2,3-Trichloropropane ND 0.0050 " 1,24-Triniethylbenzene ND 0.0050 13.5-Trimethylbenzene ND 0.0050 Vinyl chloride ND 0.0050 Xylencs (total) ND 0.0050 Surrogate: Dibrnmolluorometlrane 91 l& (75 - 122) Surrogate: Toluene-elS 94 ''1,, (66 - 128 ) Surrogate: 4-Brumolluoruhc it-ene 97 % (76 - 122) The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 38 of 65 rA AM Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical i Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury ND 0.090 mg/kg 1 B I C0807 03/26/21 15:06 EPA 7471 A Total Metals by ICP Antimony ND 2.4 mgtkg 1 BIC'0810 03/262114:11 EPA 601(1B Arsenic 2.0 1.9 Barium 5.5 0.96 Beryllium ND 0.49 Cadmium ND 0.24 Chromium 6.4 0.48 Cobalt 0.76 0.48 Copper 1.8 0.96 Lead 3.7 0.48 Molvbdenum 1.6 0.48 Nickel 3.9 0.48 Selenium ND 1.9 Silver ND 0.48 Thallium ND 0.96 Vanadium 5.2 1.9 Zinc 5.2 1.9 Volatile Organic TPH by GC/FID TPH Gasoline (C5-C12) ND 4.9 mg/kg 1 BIC0804 03/26/21 14:42 EPA 8015M R-07 Surrogate: 4-B1-onm/htoroben:cne 102 No (31 - 168 ) Semi -Volatile Organic TPH by GC/FID TPH Diesel (CI 3-C22) ND 10 mglkg I B1 C0798 03t26=21 11:45 EPA 8015M TP11 Motor Oil (C23-C40) 120 50 " " " " " Surrogate: o-Teryhenyl 107 96 (65 - 133) 11° 11 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cl1ent.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 39 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample ID: Soil Pile E Sampled: 03/25/21 12:10 Matrix: Solid Sampled by: Lab ID: 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GUMS Benzene ND 0.0050 mg,kg 1 BIC0817 03/26/21 16:12 EPA8260B Bromobenzene ND 0.0050 Bromochloromethane ND 0.0050 Bromodichloromethane ND 0.0050 " Bromoform ND 0.0050 Bromotnelhane ND 0.0050 n-Butylbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 tert-Butylbenzene N{) 0.0050 Carbon tetrachloride ND 0.0050 Chlorobenzenc ND 0.0050 Chlorocthane ND 0,0050 " Chloroform ND 0.0050 Chloromelhane ND 0.0050 2-Chlorotoluene ND 0.0050 4-Chlorotoluene ND 0.0050 " Dibromochloromethane ND 0.0050 1.2-Dibromo-3-chloropropane ND 0.0050 1,24Dibromoelhane (EDB) ND 0.0050 Dibromomethaue ND 0.0050 I.2-Dichlorobenzene ND 0.0050 1,3-Dichlorobenzene ND 0.0050 I A-Dichlorobenzene ND 0.0050 Dichloroditluoromcthane ND 0.0050 1, 1 -Dichloroethanc ND 0.0050 1,2-Dichloroethane ND 0.0050 1, 1 -Dichloroethene ND 0.0050 cis-1,2-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 1,2-Dichloropropane ND 0.0050 13-Dichloropropane ND 0.0050 " 2,2-Dichloropropane ND 0.0050 1.1-Dichloropropane ND 0.0050 cis-1.3-Dichloropropenc ND 0.0050 trans-1,3-Dichloropropane ND 0.0050 " Fthylbenzcnc ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 40 of 65 [61*y Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 ReportAnalytical Sam Sample ID: Soil Pile E Sampled: 03/25/21 12:10 P Matrix: Solid Sampled by: Lab ID : 2101841-13 Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS (Continued) Hexachlorobuladiene ND 0.0050 mgtkg 4-Isopropyl Toluene ND 0.0050 Isopropylbenzene ND 0.0050 Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 Styrene ND 0.0050 " 1,1,1.2-Tetrachloroethane ND 0.0050 " I.1,2,2-Tetrachloroethane ND 0.0050 " Torachlorocthcne WCE) ND 0.0050 " Toluene ND 0.0050 1,2,3-Trichlorobenzenc ND 0.0050 " L2.4-Trichlorobenzene ND 0.0050 " 1,1,I-Trichloroethane ND 0.0050 1,1,2-Trichloroethane ND 0.0050 " Trichloroethene (TCE) ND 0.0050 " Trichlorofluorontethane ND 0.0050 " 1.2.3-Trichloropropane ND 0.0050 " 1.2.4-Trimethylbenzene ND 0.0050 I.3,5-Trimethylbenzene ND 0.0050 " Vinyl chloride ND 0.0050 Xylcnes (total) ND 0.0050 Surrogate: Dihromofluoromethane 91 % (75 - 122 ) Surrogate: Toluene•-ds 95 (66- 12S ) Surrogate: 4-Brwno1luorohen_ene 97 °o (76 - 122 ) 1 B I C0817 03/26/21 16:12 EPA 8260B The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comkreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 41 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Total Metals by CX2'AA - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0807 -EPA 7471A Preparation: EPA 7471A Pre Blank (B1C0807-BLK1) Mercury ND LCS (BIC0807-BSI) Mercury 0.792 LCS Dup (BlC0807-BSDI) Mercury 0.783 Duplicate (BlC0807-DUPl) Source: 2101842-02 Mercury 0.0556 Matrix Spike (B1C0807-MS1) Source: 2101842-02 Mercury 0.855 Matrix Spike Dup (B1C0807-MSD1) Source: 2101842-02 Mercury 0.750 Post Spike (BIC0807-PSI) Source: 2101842-02 Mercury 5.17 03/26/21 07:43 Analyzed: 03/26/21 13:21 0.10 mg/kg Analyzed: 03/26/21 13:17 0.10 mg/kg 0.833 95 85-115 Analyzed: 03/26/21 13:19 0.10 mg/kg 0.833 94 85-115 1 20 Analyzed: 03/26/21 13 :25 0.096 mg/kg 0.0554 0.3 20 Analyzed: 03/26/21 13:27 0.096 mgtkg 0.796 0.0554 100 75-125 Analyzed: 03/26/21 13:29 0.087 mg/kg 0.727 0.0554 96 75-125 13 20 Analyzed: 03/26/21 13:31 ug/l' .5.00 0.347 97 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 42 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Blank (B1C0810-BLK1) Analyzed: 03/26/21 12:16 Antimony ND 2.5 mg/kg Arsenic ND 2.0 " Barium ND 1.0 Beryllium ND 0.50 " Cadmium ND 0.25 " Chromium ND 0.50 " Cobalt ND 0.50 " Copper ND 1.0 " Lead ND 0.50 " Molybdenum ND 0.50 " Nickel ND 0.50 " Selenium ND 2.0 " Silver ND 0.50 " Thallium ND 1.0 Vanadium ND 2.0 " Zinc ND 2.0 " LCS (B1C0810-BS1) Analyzed: 03/26/21 12:40 Antimony 100 2.5 mg/kg 100 100 80-120 Arsenic 101 2.0 100 101 80-120 Barium 102 1.0 100 102 80-120 Beryllium 103 0.50 100 103 80-120 Cadmium 102 0.25 100 102 80-120 Chromium 103 0.50 100 103 80-120 Cobalt 103 0.50 100 103 80-120 Copper 103 1.0 100 103 80-120 1-cad 103 0.50 100 103 80-120 Molvbdenum 100 0.50 100 100 80-120 Nickel 103 0.50 100 103 80-120 Selenium 100 2.0 100 100 80-120 Silver 5.06 0.50 5.00 101 80-120 Thallium 104 1.0 100 104 80-120 Vanadium 100 2.0 100 100 80-120 Zinc 103 2.0 100 103 80-120 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 43 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 TotalControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 LCS Dup (B1C0810-BSD1) Analyzed: 03/26/21 12:43 Antimony 101 2.5 mg/kg 100 101 80-120 0.7 20 Arsenic 102 2.0 100 102 80-120 0.9 20 Barium 102 1.0 100 102 80-120 0.3 20 Beryllium 104 0.50 100 104 80-120 0.9 20 Cadmium 103 0.25 100 103 80-120 0.5 20 Chromium 104 0.50 100 104 80-120 1 20 Cobalt 104 0.50 100 104 80-120 0.5 20 Copper 104 1.0 100 104 80-120 0.9 20 Lead 104 0.50 100 104 80-120 0.8 20 Molybdenum 101 0.50 100 101 80-120 0.9 20 Nickel 104 0.50 100 104 80-120 0.5 20 Selenium 101 2.0 100 101 80-120 0.7 20 Silver 5.16 0.50 5.00 103 80-120 2 20 Thallium 104 1.0 100 104 80-120 0.3 20 Vanadium 102 2.0 100 102 80-120 1 20 Zinc 103 2.0 100 103 80-120 0.5 20 Duplicate (B1C0810-DUPI) Source: 2101840-03 Analyzed: 03/26/21 13:06 Antimony ND 2.4 mg!kg 0.966 20 Arsenic 2.64 1.9 3.12 17 20 Barium 118 0.95 116 2 20 Beryllium ND 0.47 ND 20 Cadmium ND 0.24 ND 20 Chromium 16.3 0.47 17.6 8 20 Cobalt 3.67 0.47 4.26 15 20 Copper 9.50 0.95 9.79 8 20 Lead 6.24 0.47 5.56 12 20 Molvbdenum 1.46 0.47 1.27 14 20 Nickel 20.8 0.47 23.4 12 20 Selenium ND 1.9 ND 20 Silver ND 0.47 ND 20 Thallium ND 0.95 ND 20 Vanadium 15.0 1.9 15.4 3 20 Zinc 34.0 1.9 29.6 14 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 44 of 65 AL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BIC0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Matrix Spike (B1C0810-MS1) Source: 2101840-03 Analyzed: 03/26/21 12:45 Antimony 49.8 2.4 mg1kg 97.6 ND 51 10-116 Arsenic 100 2.0 97.6 3.12 100 77-121 Barium 196 0.98 97.6 116 82 30-169 Beryllium 98.3 0.49 97.6 ND 101 96-111 Cadmium 93.4 0.24 97.6 ND 96 81-112 Chromium 113 0.49 97.6 17.6 97 75-129 Cobalt 96.4 0.49 97.6 4.26 94 71-121 Copper 106 0.98 97.6 9.79 100 68-135 Lead 98.5 0.49 97.6 5.56 95 72-121 Molybdenum 89.8 0.49 97.6 1.27 91 70-112 Nickel 111 0.49 97.6 23.4 90 73-121 Selenium 94.7 2.0 97.6 ND 97 76-116 Silver 4.74 0.49 4.98 ND 97 54-132 Thallium 91.2 0.98 97.6 ND 93 64-120 Vanadium 112 2.0 97.6 15.4 99 78-124 Zinc 122 2.0 97.6 29.6 95 50-143 Matrix Spike Dup (B1C0810-MSD1) Source: 2101840-03 Analyzed: 03/26/21 12:55 Antimony 48.3 2.5 mg/kg 98.0 ND 49 10-116 3 20 Arsenic 102 2.0 98.0 3.12 101 77-121 1 20 Barium 203 0.98 98.0 116 89 30-169 4 20 Beryllium 99.4 0.49 98.0 ND 101 86-I11 1 20 Cadmium 95.0 0.25 98.0 ND 97 81-112 2 20 Chromium 117 0.49 98.0 17.6 WI 75-129 4 20 Cobalt 98,2 0.49 98.0 4.26 96 71-121 2 20 Copper 110 0.98 98.0 8.79 103 68-135 3 20 Lead 100 0.49 98.0 5.56 97 72-121 2 20 Molybdenum 91.3 0.49 98.0 1.27 92 70-112 2 20 Nickel 113 0.49 98.0 23.4 92 73-121 2 20 Selenium 96.4 2.0 98.0 ND 98 76-116 2 20 Silver 4.89 0.49 4.90 ND 100 54-132 3 20 Thallium 93.1 0.98 98.0 ND 95 64-120 2 20 Vanadium 115 2.0 98.0 15.4 102 78-124 3 20 Zinc 124 2.0 98.0 29.6 96 50-143 1 20 The results in this report apply to the samples analyzed in accordance with the chain ofcustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 45 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0810 - EPA 6010B Preparation: EPA 3050B 03/26/21 08:36 Post Spike (B1C0810-PS1) Source: 2101840-03 Analyzed: 03/26/21 12:58 Antimony 1.97 mg/L 2.00 0.0203 98 75-125 Arsenic 2.08 2.00 0.0657 101 75-125 Barium 4.39 2.00 2.43 97 75-125 Beryllium 1.99 2.00 0.00456 99 75-125 Cadmium 1.89 2.00 -0.00476 94 75-125 Chromium 2.37 2.00 0.370 100 75-125 Cobalt 1.97 2.00 0.0898 94 75-125 Copper 2.25 2.00 0.185 103 75-125 Lead 2.02 2.00 0.117 95 75-125 Molybdenum 1.98 2.00 0.0268 98 75-125 Nickel 2.37 2.00 0.492 94 75-125 Selenium 1.97 2.00 0.000298 98 75-125 Silver 0.0974 0.100 -0.00299 97 75-125 Thallium 1.88 2.00 -0.0363 94 75-125 Vanadium 2.30 2.00 0.324 99 75-125 Zinc 2.50 2.00 0.623 94 75-125 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 46 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0802 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:22 Blank (BIC0802-BLK1) Analyzed: 03/26/21 08:30 TPH Gasoline (C5-C`12) ND 0.50 mg/kg Surrogate:4-Bromg1luurobcn_ene 0.127 110.125 101 31-168 LCS (BlC0802-BS1) Analyzed: 03/26/21 06:59 TPH Gasoline (C5-C12) 1.01 0.50 mg/kg 1.00 WI 62-151 Surrogate:4-Bronuilluorobensenr 0.152 " 0.125 121 31-168 LCS Dup (B1C0802-BSD1) Analyzed: 03/26/21 07:25 TPH Gasoline (C5-C12) 0.958 0.50 mg/kg 0.996 96 62-151 5 20 Surrogate: 4-Bromgfluorohen:ene 0.142 0.125 114 31-168 Duplicate (B1C0802-DUPl) Source: 2101840-01 Analyzed: 03/26/21 09:29 TPH Gasoline (C 5-C12) ND 0.50 mg/kg ND 20 Surrogate:4-Bromolluorobenzene 0.131 " 0.124 105 31-168 Batch BlC0804 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 03/26/21 05:26 Blank (BlC0804-BLK1) Analyzed: 03/26/21 10:27 TPI1Gasoline (C5-('12) ND 0.50 mg/kg Surrogate:4-Bromolluorohenzene 0.133 " 0.125 107 31-168 LCS (BlC0804-BSI) Analyzed: 03/26/21 09:30 TPH Gasoline (('5-C12) 1.24 0.50 mg/kg 0.998 124 62-151 Surrogate:4-Bromolhurohenzene 0.147 110.125 /is 31-168 LCS Dup (B1C0804-BSDI) Analyzed: 03/26/21 09:59 TPH Gasoline (C5-C12) 1.32 0.50 mg/kg 0.998 132 62-151 7 20 Surrogate:4-Bromolluorobeuzene 0.164 0.125 131 31-168 Duplicate (B1C0804-DUPl) Source: 2101841-06 Analyzed: 03/26/21 11:24 TPH Gasoline (C5-('l2) 10.0 4.3 mg/kg 6.12 48 20 QR-03 Surrogate:4-Bromolluorohen_enc• 1.38 " 1.08 128 31-168 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 47 of 65 tm'&�Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Semi -Volatile Organic TPH by 1Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0798 - EPA 8015M Preparation: EPA 3550C 03/25/21 17:29 Blank (Bl C0798-BLK1) Analyzed: 03/26/21 07:35 TPII Diesel Wl3-C22) ND 10 mg/kg TPH Motor Oil (C23-C40) ND 50 " Surrogate: o-Teiphen.vl 53.7 " 49.8 10N 65-133 LCS (BlC0798-BS1) Analyzed: 03/26/21 07:07 TPH Diesel (C13-C22) 508 9.9 mg/kg 496 102 77-114 TPH Motor Oil (C23-('40) 549 50 496 111 76-128 Surrogate: o-Terphenyl 50.7 49.6 102 65-133 LCS Dup (BlC0798-BSD1) Analyzed: 03/26/21 07:21 TPII Diesel (C13-C22) 501 9.9 mg/kg 497 101 77-1 I4 1 20 TPH Motor Oil (C23-C40) 557 50 497 112 76-129 2 20 Surrogate: o-TetphcgY1 53.5 49.7 108 65-133 Duplicate (B1C0798-DUPI) Source: 2101840-01 Analyzed: 03/26/21 08:44 TPH Diesel (('13-C22) ND 10 mg/kg ND 20 TPH Motor Oil (('23-C40) 43.1 50 44.8 4 20 Surrogate: o-7cipheml 53.4 49.8 107 65-133 Matrix Spike (BlC0798-MSI) Source: 2101840-01 Analyzed: 03/26/21 13:48 TPII Diesel (C13-('22) 507 9.9 mg/kg 497 ND 102 45-149 TPII Motor Oil (C'23-C'40) 556 50 497 44.8 103 34-175 Surrogate: o-Teiphem'l 55.9 49.7 113 65-133 Matrix Spike Dup (BlC0798-MSDI) Source: 2101840-01 Analyzed: 03/26/21 14:02 TPH Diesel (C13-C22) 488 10 mg/kg 499 ND 98 45-149 4 20 TPH Motor Oil (C'23-('40) 548 50 499 44.8 101 34-175 1 20 Surrogate: o-Tiapheiml 55.2 49.9 111 65-133 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 48 of 65 (im Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (Bl C0815-BLKI) Analyzed: 03/26/21 11:26 Benzene ND 0.25 mg/kg Bromobenzene ND 0.25 Bromochloromethanc ND 0.25 Bromodichloromethane ND 0.25 " Bromotorm ND 0.25 " Bromomethane ND 0.25 n-Butylbenzene ND 0.25 " sec-Butylbenzene ND 0.25 tert-Butylbenzene ND 0.25 Carbon tetrachloride ND 0.25 Chlorobenzene ND 0.25 " Chloroethane ND 0.25 Chloroform ND 0.25 " Chloromethane ND 0.25 2-Chlorotoluene ND 0.25 " 4-Chlorotoluene ND 0.215 " Dibromochloromethane ND 0.25 " 1,2-Dibronio-3-chloropropane ND 0.25 1,2-Dibronioethane (EDB) ND 0.25 Dibronxrtnethanc ND 0.25 " 1,2-I)ichlorobenzene ND 0.25 " 1,3-Dichloroben7cnc ND 0.25 1,4-Dichlorobenzene ND 0.25 " Dichloroditluoronicthanc ND 0.25 " 13-Dichloroethene ND 0.25 " 1,2-Dichlorocthanc ND 0.25 1, 1 -Dichloroethene ND 0.25 cis-1,2-Dichloroethene ND 0.25 " trans-1,2-Dichlotoethene ND 0.25 " 1,2-Dichloropropane ND 0.25 " 1,3-Dichloropropane ND 0.25 2,2-Dichloropropane ND 0.25 " 1, 1 -Dichloropropene ND 0.25 " cis-1.3-Dichloropropene ND 0.25 trans-1,3-Dichloropropene ND 0.25 Ethylbenzene ND 0.25 " Hexachlorobutadiene ND 0.25 4-Isopropyl Toluene ND 0.25 " Isopropylbenzene ND 0.25 " Methylene chloride ND 0.25 Naphthalene ND 0.25 u-Propylbenzene ND 0.25 " The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 49 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch B1C0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Blank (BlC0815-BLK1) Analyzed: 03/26/21 11:26 Styrene ND 0.25 nrg/kg 1, 1, 1,2-Tetracliloroethane ND 0.25 I,I.2,2-Tetrachloroethane ND 0.25 Tetrachloroethene (PCE) ND 0.25 " Toluene ND 0.25 " 1,2,3-Trichlorobenzene ND 0.25 " 1.2,4-Trichlorobenzene ND 0.25 1,1,1-Trichloroethane ND 0.25 1.1,2- Trichloroethane ND 0.25 Trichloroethene (TCE) ND 0.25 Trichlorotluoromethane ND 0.25 " 1,2,3-Trichloropropane ND 0.25 " 1,2.4-Trimethylbenzene ND 0.25 " 1,3,5-Trimethylben7ene ND 0.25 " Vinyl chloride ND 0.25 " Xylenes (total) ND 0.25 " Surrogate: Dibromq/luoromcthmre 0.0445 0.0498 89 75-122 Surrogate: Toluene-d8 0.0455 0.0498 91 66-128 Surrogate: 4-Bromolluorohenzene 0.0479 0.0498 96 76-122 LCS (BlC0815-BS1) Analyzed: 03/26/21 09:44 Benzene 1.80 0.25 mg/kg 1.99 91 75-131 Bromobenzene 1.97 0.25 1.99 99 75-136 Bromochloromethane 1.67 0.25 1.99 84 70-135 Bromodichloromethane 1.84 0.25 1.99 93 76-137 Bromoform 1.68 0.25 1.99 85 55-139 Bromomethane 1.49 0.25 1.99 75 10-157 n-Butylbenzene 2.38 0.25 1.99 120 62-166 sec-Butylbenzene 2.50 0.25 1.99 126 72-167 tert-Butylbenzene 2.33 0.25 1.99 117 69-158 Carbon tetrachloride 1.77 0.25 1.99 89 70-140 Chlorobenzene 1.94 0.25 1.99 98 76-137 Chloroethane 2.09 0.25 1.99 105 10-104 Chlorofonn 1.80 0.25 1.99 91 75-123 Chloromethane 1.73 0.25 1.99 87 26-146 2-Chlavtoluene 2.11 0.25 1.99 106 73-145 4-Chlorotoluene 2.13 0.25 1.99 107 67-151 Dibromochloromethane 1.80 0.25 1.99 90 68-144 1,2-Dibromo-3-chloropropanc 1.63 0.25 1.99 82 45-148 1,2-Dibromoethane (EDB) 1.80 0.25 1.99 91 73-134 Dibromomcthanc 1.66 0.25 1.99 84 70-140 1,2-Dichlorobenzene 2.15 0.25 1.99 108 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 50 of 65 WIL Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS (B1C0815-BSI) Analyzed: 03/26/21 09:44 13-Dichlorobenzenc 2.19 0.25 mg/kg 1.99 110 76-146 14-Dichlorobenzene 2.10 0.25 1.99 106 72-140 Dichlorodifluoromethane 1.73 0.25 1.99 87 10-166 I,1-Dichloroethane 1.82 0.25 1.99 92 65-139 1,2-Dichlorocthanc 1.80 0.25 1.99 90 67-125 1,1-Dichloroethene 2.05 0.25 1.99 103 54-168 cis-L2-Dichloroethene 1.80 0.25 1.99 91 74-135 trans-1,2-Dichloroethene 1.98 0.25 1.99 100 68-149 1,2-Dichloropropane 1.77 0.25 1.99 89 74-130 1,3-Dichloropropane 1.83 0.25 1.99 92 68-130 2,2-Dichloropropane 1.95 0.25 1.99 98 33-187 1, 1 -Dichloropropene 1.95 0.25 1.99 98 71-140 cis- 1,3-Dichloropropene 1.79 0.25 1.99 90 78-135 trans-1,3-Dichloropropene 1.90 0.25 1.99 96 70-137 Ethylbenzene 1.93 0.25 1.99 97 69-143 Hexachlorobutadiene 3.12 0.25 1.99 157 69-203 4-Isopropyl Toluene 2.38 0.25 1.99 120 74-154 Isopropylbenzene 2.11 0.25 1.99 106 72-157 Methylene chloride 1.75 0.25 1.99 88 49-129 Naphthalene 1.84 0.25 1.99 93 61-158 n-Propylbenzene 2.17 0.25 1.99 109 69-147 Styrene 1.92 0.25 1.99 97 71-144 1, 1. 1,2-Tetrachloroethane 1.92 0.25 1.99 97 78-132 1,1.2,2-Tctrachlorocthanc 1.90 0.25 1.99 96 64-138 Tetrachloroethene (PCE) 2.09 0.25 1.99 105 74-148 Toluene 1.82 0.25 1.99 92 76-131 1,2,3-Trichlorobenzene 2.11 0.25 1.99 106 63-170 12,4-Trichlorobenzene 2.20 0.25 1.99 110 71-165 1, 1, 1 -Trichloroethane 1.97 0.25 1.99 99 74-137 1.1,2-Trichloroethane 1.82 0.25 1.99 91 68-134 Trichloroethene(TCE) 1.94 0.25 1.99 98 79-139 Trichlorofluoromethane 2.20 0.25 1.99 111 32-154 1,2.3-Trichloropropane 1.77 0.25 1.99 89 69-125 1,2.4-Trimethvlbenzene 2.14 0.25 1.99 108 67-144 1,3,5-Trimethylbenzene 2.17 0.25 1.99 109 66-154 Vinyl chloride 2.27 0.25 1.99 114 39-150 Xylenes (total) 5.95 0.25 5.96 100 71-147 Surrogutc: Dibrumo/luarnmcthanc 0.0496 0.0497 100 75-122 Surrogate: 7oluene-d8 0.0462 0.0497 93 66-128 Smragute:4-Bromolluorobenze•n" 0.0451 0.0497 91 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 51 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 I Volatile Organic Compounds Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (B1CO815-BSDI) Analyzed: 03/26/21 10:09 Benzene 1.87 0.25 mg,kg 2.00 94 75-131 4 20 Bromobenzene 2.02 0.25 2.00 101 75-136 2 20 Bromochlor•anethanc 1.69 0.25 2.00 85 70-135 2 20 Bromodichloromethane 1.93 0.25 2.00 97 76-137 5 20 Brontofonn 1.80 0.25 2.00 90 55-139 7 20 Bromomethane 1.21 0.25 2.00 ()l 10-157 20 20 n-Butvlbenzene 2.45 0.25 2.00 123 62-166 3 20 sec-Butylbenzene 2.48 0.25 2.00 124 72-167 0.9 20 tert-Butylbenzene 2.39 0.25 2.00 119 69-158 2 20 Carbon tetrachloride 1.87 0.25 2.00 94 70-140 6 20 Chlorobenzene 2.07 0.25 2.00 104 76-137 7 20 Chloroethane 2.21 0.25 2.00 111 10-164 6 20 Chloroform 1.81 0.25 2.00 90 75-123 0.4 20 Chloromethane 1.82 0.25 2.00 91 26-146 5 20 2-Chlorotoluene 2.26 0.25 2.00 113 73-145 7 20 4-Chlorotoluene 2.25 0.25 2.00 112 67-151 5 20 Dibromochloromethane 1.97 0.25 2.00 98 68-144 9 20 1.2-Dibmmo-3-chloropropane 1.84 0.25 2.00 92 45-148 12 20 1,2-Dibromoethane (EDB) 1.98 0.25 2.00 99 73-134 9 20 Dibromomcthanc 1.75 0.25 2.00 87 70-140 5 20 1,2-Dichlorobenzene 2.18 0.25 2.00 109 78-142 1 20 1,3-Dichlorobenzene 2.30 0.25 2.00 115 76-146 5 20 1,4-Dichlorobenzene 2.06 0.25 2.00 103 72-140 2 20 Dichloroditluoromcthanc 1.73 0.25 2.00 86 10-166 0.1 20 1,1-Dichloroethene 1.95 0.25 2.00 98 65-139 7 20 1,2-Dichlorocthanc 1.93 0.25 2.00 96 67-125 7 20 LI-Dichloroethene 2.07 0.25 2.00 103 54-168 0.6 20 cis-1.2-Dichloroethene 1.86 0.25 2.00 93 74-135 4 20 trans-1,2-Dichloroethene 2.11 0.25 2.00 105 68-149 6 20 1.2-Dichloropropane 1.82 0.25 2.00 91 74-130 3 20 13-Dichloropropane 1.84 0.25 2.00 92 68-130 0.6 20 2.2-Dichloropropane 1.94 0.25 2.00 97 33-187 0.4 20 1,1-Dichloropropene 2.04 0.25 2.00 102 71-140 5 20 cis-1.3-Dichloropropene 1.80 0.25 2.00 90 78-135 0.5 20 trans-1,3-Dichloropropene 1.94 0.25 2,00 97 70-137 2 20 Etylbenzene 2.06 0.25 2.00 103 69-143 6 20 Hexachlorobutadiene 3.30 0.25 2.00 165 69-203 6 20 4-Isopropyl Toluene 2.42 0.25 2.00 121 74-154 2 20 Isopropylbenzene 2.19 0.25 2.00 109 72-157 3 20 Methylene chloride 1.87 0.25 2.00 94 49-129 7 20 Naphthalene 2.04 0.25 2.00 102 61-158 IO 20 n-Propylbenzene 2.30 0.25 2.00 115 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain ofeustody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 52 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Coinpounds by GC/NlS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 LCS Dup (BlC0815-BSDI) Analyzed: 03/26/21 10:09 Styrene 2.06 0.25 mg,kg 2.00 103 71-144 7 20 1, 1, 1,2-Tetrachloroethane 2.04 0.25 2.00 102 78-132 6 20 1,L2,2-Tetrachlorocthanc 2.02 0.25 2.00 101 64-138 6 20 Tetrachloroethene (PCE) 2.18 0.25 2.00 109 74-148 4 20 Toluene 1.91 0.25 2.00 96 76-131 5 20 1,23-Trichlorobenzenc 2.36 0.25 2.00 its 63-170 12 20 1,24-Trichlorobenzene 2.37 0.25 2.00 118 71-165 7 20 1, 1, 1 -Trichloroethane 1.98 0.25 2.00 99 74-137 0.8 20 1.12-Trichloroethane 1.92 0.25 2.00 96 68-134 6 20 Trichloroethene (TCE) 1.92 0.25 2.00 96 79-139 0.9 20 Trichlorotluoromethane 2.15 0.25 2.00 107 32-154 3 20 1,2,3-Tricbloropropane 1.78 0.25 2.00 89 69-125 0.3 20 12,4-Trimethylbenzene 2.19 0.25 2.00 110 67-144 2 20 1,3,5-Trimethylbenzene 2.24 0.25 2.00 112 66-154 3 20 Vinyl chloride 2.22 0.25 2.00 1 I I 39-150 2 20 Xylenes (total) 6.14 0.25 6.00 102 71-147 3 20 Surrogate: Dibronwlluorumethant, 0.0492 " 0.0500 98 75-122 Surrogate: Toluene-d8 0.0452 0.0500 90 66-128 Surrogui :4-Bromo/luorobenzene 0.0464 0.05110 93 76-122 Duplicate (B1C0815-DUPl) Source: 2101841-07 Analyzed: 03/26/21 14:51 Benzene ND 1.2 mg/kg ND 20 Bromobenzene ND 1.2 ND 20 Bromochlon»ncthanc ND 1.2 ND 20 Bromodichloromethane ND 1.2 ND 20 Bromoturm ND 1.2 ND 20 Bromomethane ND 1.2 ND 20 n-Butylbenzene ND 1.2 ND 20 sec-Butylbenzene ND 1.2 ND 20 tert-Butylbenzene ND 1.2 ND 20 Carbon tetrachloride ND 1.2 ND 20 Chlorobenzene ND 1.2 ND 20 Chloroethane ND 1.2 ND 20 Chloroform ND 1.2 ND 20 Chloromethane ND 1.2 ND 20 2-Chlorotoluene ND 1.2 ND 20 4-C hlorotoluene ND 1.2 ND 20 Dibromochloromethane ND 1.2 ND 20 1,2-Dibronui-3-chloropropane ND 1.2 ND 20 1,2-Dibromoethane (EDB) ND 1.2 ND 20 Dibronxnncthanc ND 1.2 ND 20 1,2-Diehlorobenzene ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 53 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic pi Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0815 - EPA 8260B Preparation: EPA 5035/5030B MEOH 03/26/21 09:17 Duplicate (B1C0815-DUPl) Source: 2101841-07 Analyzed: 03/26/21 14:51 1,3-Dichlorobenzenc ND 1.2 mg/kg ND 20 I A-Dichlorobenzene ND 1.2 ND 20 Dichlorodifluorotncthanc ND 1.2 ND 20 l,l-Dichloroethane ND 1.2 ND 20 1,2-Dichlorocthanc ND 1.2 ND 20 1.1-Dichloroethene ND 1.2 ND 20 cis-1 2-Dichloroethene ND 1.2 ND 20 trans-1,2-Dichloroethene ND 1.2 ND 20 1,2-Dichloropropaue ND 1.2 ND 20 1,3-Dichloropropane ND 1.2 ND 20 2,2-Dichloropropane ND 1.2 ND 20 1,1-Dichloropropene ND 1.2 ND 20 cis-1,3-Dichloropropeue ND 1.2 ND 20 trans-1,3-Dichloropropene ND 1.2 ND 20 Ethylbenzene ND 1.2 ND 20 Hexachlorobutadiene ND 1.2 ND 20 4-Isopropyl Toluene ND 1.2 ND 20 isopropylbenzene ND 1.2 ND 20 Methylene chloride ND 1.2 ND 20 Naphthalene ND 1.2 ND 20 n-Propylbenzene ND 1.2 ND 20 Styrene ND 1.2 ND 20 1, 1, 1,2-Tetrachloroethane ND 1.2 ND 20 1,1,2,2-1'etrachloroethane ND 1.2 ND 20 Tetraehloroethene (PCE) ND 1.2 ND 20 Toluene ND 1.2 ND 20 1,2,3-Trichlorobenzene ND 1.2 ND 20 1,2,4-Trichlorobenzene ND 1.2 ND 20 Ll,I-Trichloroethane ND 1.2 ND 20 1,1,2-Trichloroethane ND 1.2 ND 20 Trichloroethene (TCE) ND 1.2 ND 20 Trichlorofluoromethane ND 1.2 ND 20 1,2,3-Trichloropropane ND 1.2 ND 20 1,2,4-Trimethvlbenzene ND 1.2 ND 20 1,3,5-Trimethylbenzene ND 1.2 " ND 20 `.'iny] chloride ND 1.2 ND 20 Xylenes (total) ND 1.2 ND 20 Surrogate: UihrontuJhruromethunc 0.0468 0.0494 95 75-137 Surrogate: Toluene-d8 0.0455 0.0494 92 66-128 Surrogate: 4-Bromolluorobenaene 0.0466 0.0494 94 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 54 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatilepi Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (Bl C0817-BLK1) Analyzed: 03/26/21 12:18 Benzene ND 0.0050 mgrkg Bromobenzene ND 0.0050 " Bromochloromcthanc ND 0.0050 Bromodichloromethane ND 0.0050 Bromotbrm ND 0.0050 " Bromomethane ND 0.0050 " u-Butvlbenzene ND 0.0050 sec-Butylbenzene ND 0.0050 " tert-Butylbenzene ND 0.0050 " Carbon tetrachloride ND 0.0050 Chlorobenzene ND 0.0050 " Chloroethanc ND 0.0050 Chloroform ND 0.0050 " Chloromethane ND 0.0050 " 2-Chlorotoluene ND 0.0050 " 4-Chlorotoluene ND 0.0050 Dibromochloromethane ND 0.0050 1,2-IDibromo-3-chloropropane ND 0.0050 1,2-Dibronioethane (EDB) ND 0.0050 " Dibromomcthanc ND 0.0050 " 1,2-Dichlorobenzene ND 0.0050 " 1.3-Dichlorobenzene ND 0.0050 " 1,4-Dichlorobenzene ND 0.0050 " Dichlorodilluoromcthanc ND 0.0050 " 1,1-Dichloroethene ND 0.0050 " 1,2-Dichlorocthanc ND 0.0050 " LI-Dichloroethene ND 0.0050 " cis-12-Dichloroethene ND 0.0050 trans-1,2-Dichloroethene ND 0.0050 " 1,2-Dichloropropane ND 0.0050 " 1,3-Dichloropropane ND 0.0050 2,2-Dichloropropane ND 0.0050 " 1, 1 -Dichloropropene ND 0.0050 cis-1.3-Dichloropropene ND 0.0050 " trans-1,3-Dichloropropene ND 0.0050 Ethylbenzene ND 0.0050 " Ilexachlorobutadiene ND 0.0050 4-Isopropyl Toluene ND 0.0050 " Isopropylbenzene ND 0.0050 " Methylene chloride ND 0.0050 " Naphthalene ND 0.0050 " n-Propylbenzene ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 55 of 65 �i M�� � Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 VolatileControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 11:40 Blank (BlC0817-BLK1) Analyzed: 03/26/21 12:18 Styrene ND 0.0050 mg -kg 1, 1, 1,2-Tetrachloroethane ND 0.0050 1,1,2,2-Tctrachloroethane ND 0.0050 " Tetraehloroethene (PCE) ND 0.0050 Toluene ND 0.0050 " 1,2,3-Trichlorobenzene ND 0.0050 " 1,2,4-Trichlorobenzene ND 0.0050 " 1,1,1-Trichhiroethane ND 0.0050 " 1,1.2-Trichloroethane ND 0.0050 Trichloroethene (TCE) ND 0.0050 " Trichlorofluoromethanc ND 0.0050 " 1,2,3-Trichloropropane ND 0.0050 1,2,4-Triniethylbenzene ND 0.0050 " 1,3,5-Triniethylbenzene ND 0.0050 Vinvl chloride ND 0,0050 " Xylenes (total) ND 0.0050 " Surrogate: Dibrotnolluorontethtute 0.0459 0.0495 93 75-122 Surrogate: Toluene-d8 0.0472 0.0495 95 66-128 Surrogate:4-Bromohuorobenreue 0.0483 0.0495 98 76-122 LCS (B1C0817-BS1) Analyzed: 03/26/21 10:22 Benzene 0.0342 0.0050 nig/kg 0.0398 86 75-131 Bromobenzene 0.0367 0.0050 0.0399 92 75-136 Bromochlorouicthane 0.0328 0.0050 0.0398 82 70-135 Bromodichloromethane 0.0334 0.0050 0,0399 84 76-137 Bromoform 0.0369 0.0050 0.0398 93 55-139 Bromomethane 0.0230 0.0050 0.0398 58 10-157 n-Butylbenzene 0.0396 0.0050 0.0398 99 62-166 sec-Butylbenzene 0.0452 0.0050 0.0398 114 72-167 tort-Butylbenzene 0.0427 0.0050 0.0398 108 69-158 Carbon tetrachloride 0.0348 0.0050 0.0398 87 70-140 Chlorobenzene 0.0374 0.0050 0.0398 94 76-137 Chloroethane 0.0413 0.0050 0.0398 104 10-164 Chloroform 0.0323 0.0050 0,0398 81 75-123 Chloromethane 0.0324 0.0050 0.0398 82 26-140 2-Chlorotoluene 0.0396 0.0050 0.0398 100 73-145 4-Chlorotoluene 0.0405 0.0050 0.0398 102 67-151 Dibromochloromethane 0.0371 0.0050 0.0398 93 68-144 1,2-Dibronio-3-chloropropanc 0.0355 0.0050 0.0398 89 45-148 1,2-Dibronioethane (EDB) 0.0369 0,0050 0.0398 93 73-134 Dibromonicthane 0.0328 0.0050 0.0398 82 70-140 1,2-Dichlorobenzene 0.0402 0.0050 0.0398 WI 78-142 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 56 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Coinpounds by GC/MS - Quality Control J Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS (B1C0817-BS1) Analyzed: 03/26/21 10:22 1,3-Dicltlorobenzenc 0.0406 0.0050 mg:Ig 0.0398 102 76-146 1,4-Dichlorobenzene 0.0388 0.0050 0.0398 97 72-140 Dichlorodifluoromethanc 0.0375 0.0050 0.0398 94 10-166 I,I-Dichloroethane 0.0342 0.0050 0.0398 86 65-139 1.2-Dichloroethane 0.0336 0.0050 0.0398 84 67-125 I,1-Dichloroethene 0.0360 0.0050 0.0398 90 54-168 cis-1.2-Dichloroethene 0.0346 0.0050 0.0398 87 74-135 trans-1,2-Dichloroethene 0.0375 0.0050 0.0398 94 68-149 1,2-Dichloropropane 0.0336 0.0050 0.0398 84 74-130 1,3-Dichloropropane 0.0356 0.0050 0.0398 90 68-130 2,2-Dichloropropane 0.0394 0.0050 0.0398 99 33-187 1,1-Dichloropropene 0.0350 0.0050 0.0398 88 71-140 cis- I .3-Dichloropropene 0.0349 0.0050 0.0398 88 78-135 trans-1,3-Dichloropropene 0.0393 0.0050 0.0398 99 70-137 Ethylbenzene 0.0379 0.0050 0.0398 95 69-143 11exachlorobutadiene 0.0480 0.0050 0.0398 121 69-203 4-Isopropyl Toluene 0.0438 0.0050 0.0398 110 74-154 Isopropylbenzene 0.0408 0.0050 0.0398 102 72-157 Methylene chloride 0.0320 0.0050 0.0398 80 49-129 Naphthalene 0.0429 0.0050 0.0398 108 61-158 n-Propylbenzene 0.0417 0.0050 0.0398 105 69-147 Styrene 0.0394 0.0050 0.0398 97 71-144 1,1,1,2-Tetrachloroethane 0.0379 0.0050 0.0398 95 78-132 1,1,22-Tetrachloroethane 0.0390 0.0050 0.0398 98 64-138 Tetrachloroethene (PCE) 0.0386 0.0050 0.0398 97 74-148 Toluene 0.0330 0.0050 0.0398 83 76-131 1,2,3-Trichlorobenzene 0.0434 0.0050 0.0398 109 63-170 1,2.4-Trichlorobenzene 0.0433 0.0050 0.0398 109 71-165 1, 1, 1 -Trichloroethane 0.0349 0.0050 0.0398 88 74-137 1,12-Trichloroethanc 0.0364 0.0050 0.0398 92 68-134 Trichloroethene(TCE) 0.0344 0.0050 0.0398 86 79-139 Trichlorotluoromethanc 0.0382 0.0050 0.0398 96 32-154 1,2,3-Trichloropropane 0.0367 0.0050 0.0398 92 69-125 1.2,4-Trimethylbenzene 0.0390 0.0050 0.0398 98 67-144 1,3,5-Trimethyl benzene 0.0409 0.0050 0.0398 103 66-154 Vinyl chloride 0.0373 0.0050 0.0398 94 39-150 Xylenes (total) 0.115 0.0050 0.119 97 71-147 Surrogate: Dihrontoflttorontcghttiii, 0.0474 0.0497 95 75-122 Surrogate: Toluene-dS 0.0478 0.0497 96 66-128 Sarrogate:4-Bromglluoroben_eml 0.0490 0.0497 99 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 57 of 65 C&T*Y Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic Compounds by GUMS - Quality Control Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS Dup (BlC0817-BSD1) Analyzed: 03/26/21 10:51 Benzene 0.0353 0.0050 mg%kg 0.0398 89 75-131 3 20 Bromobenzene 0.0390 0.0050 0.0398 98 75-136 6 20 Bromochloromethanc 0.0339 0.0050 0.0398 85 70-135 3 20 Bromodichloromethane 0.0349 0.0050 0.0398 88 76-137 4 20 Bromotiinn 0.0390 0.0050 0.0399 98 55-139 6 20 Bromomethane 0.0259 0.0050 0.0398 65 10-157 12 20 n-Butylbenzene 0.0425 0.0050 0.0398 107 62-166 7 20 sec-Butylbenzene 0.0487 0.0050 0.0398 122 72-167 7 20 tert-Butylbenzene 0.0459 0.0050 0.0398 115 69-158 7 20 Carbon tetrachloride 0.0363 0.0050 0.0398 91 70-140 4 20 Chlorobenzene 0.0396 0.0050 0.0398 99 76-137 6 20 Chloroethane 0.0404 0.0050 0.0398 101 10-164 2 20 Chloroform 0.0339 0.0050 0.0398 85 75-123 5 20 Chloromethane 0.0344 0.0050 0.0398 86 26-146 6 20 2-Chlorotoluene 0.0425 0.0050 0.0398 107 73-145 7 20 4-Chlorotoluene 0.0431 0.0050 0.0398 108 67-151 6 20 Dibromochloromethone 0.0391 0.0050 0.0398 98 68-144 5 20 1,2-Dibromo-3-chloropropane 0.0367 0.0050 0.0398 92 45-148 3 20 1,2-Dibromoethane (EDB) 0.0387 0.0050 0.0398 97 73-134 5 20 Dibnunomethane 0.0337 0.0050 0.0398 85 70-140 3 20 1,2-Dichlorobenzene 0.0426 0.0050 0.0398 107 78-142 6 20 1,3-Dichlorobenzene 0.0435 0.0050 0.0398 109 76-146 7 20 I A-Dichlorobenzene 0.0413 0.0050 0.0398 104 72-140 6 20 Dichloroditluoromethanc 0.0383 0.0050 0.0398 96 10-166 2 20 1,1-Dichloroethanc 0.0354 0.0050 0.0398 89 65-139 4 20 12-Dichloroethanc 0.0346 0.0050 0.0398 87 67-125 3 20 1,1-Dichloroethene 0.0372 0.0050 0.0399 93 54-168 3 20 cis-1,2-Dichloroethene 0.0359 0.0050 0.0398 90 74-135 4 20 trans-1,2-Dichloroethene 0.0389 0.0050 0,0398 98 68-149 4 20 1,2-Dichloropropane 0.0350 0.0050 0.0398 88 74-130 4 20 1,3-Dichloropropaue 0.0372 0.0050 0.0398 93 68-130 4 20 12-Dichloropropane 0.0403 0.0050 0.0398 101 33-187 2 20 1, 1 -Dichloropropene 0.0305 0.0050 0.0398 91 71-140 4 20 cis-1.3-Dichloropropene 0.0362 0.0050 0.0399 91 78-135 4 20 trans-1,3-Dichloropropene 0.0415 0.0050 0.0398 104 70-137 5 20 Ethylbenzene 0.0402 0.0050 0.0398 101 69-143 6 20 1lexachlorobutadiene 0.0509 0.0050 0.0398 128 69-203 6 20 4-Isopropyl Toluene 0.0471 0.0050 0.0398 118 74-154 7 20 Isopropylbenzene 0.0437 0.0050 0.0398 I10 72-157 7 20 methylene chloride 0.0333 0.0050 0.0398 84 49-129 4 20 Naphthalene 0.0453 0.0050 0.0398 114 61-158 6 20 n-Propylbenzene 0,0443 0.0050 0.0398 111 69-147 6 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 58 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 VolatilepiControl Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 LCS Dup (B1C0817-BSDI) Analyzed: 03/26/21 10:51 Styrene 0.0410 0.0050 mg/kg 0.0398 103 71-144 6 20 1,1,1,2-Tetrachloroethane 0.0402 0.0050 0.0398 101 78-132 6 20 1,1,2,221'etrachloroethane 0.0407 0.0050 0.0398 102 64-139 4 20 Tetrachloroethene (PCE) 0.0412 0.0050 0.0398 103 74-148 6 20 Toluene 0,0349 0.0050 0,0398 88 76-131 6 20 1,2,3-Trichlorobenzene 0.0459 0.0050 0.0398 115 63-170 6 20 12.4-Trichloroben7ene 0.0448 0.0050 0.0398 112 71-165 4 20 1, 1, 1 -Trichloroethane 0.0365 0.0050 0.0398 92 74-137 5 20 1.1,2-Trichloroethane 0.0396 0.0050 0.0398 97 68-134 6 20 Trichloroethene (TCE) 0.0365 0.0050 0.0398 92 79-139 6 20 Trichlorotluoromethane 0.0398 0.0050 0.0398 100 32-154 4 20 1,2,3-Trichloropropane 0.0384 0.0050 0.0398 96 69-125 5 20 1,2,4-Trimethylbenzene 0.0422 0.0050 0.0398 106 67-144 8 20 1,3,5-Trim ethylbenzene 0.0437 0.0050 0.0398 110 66-154 7 20 Vinyl chloride 0.0382 0.0050 0.0398 96 39-150 2 20 Xylenes (total) 0.123 0.0050 0.120 103 71-147 7 20 Surrogate: Uibromolhnrromethane 0.0467 0.0498 94 75-122 Surrogate: Toluene-d8 0.0473 11.1149E 95 66-128 Surrogate:4-Bromo/luorohenzenc 0.0495 0.0498 99 76-122 Duplicate (B1C0817-DUPI) Source: 2101841-08 Analyzed: 03/26/21 14:15 Benzene ND 0.0050 mg/kg ND 20 Bromobenzene ND 0.0050 ND 20 Bromochloromcthane ND 0.0050 ND 20 Bromodichloromethane ND 0.0050 ND 20 Bromotonn ND 0.0050 ND 20 Bromomethane ND 0.0050 ND 20 n-Butylbenzene ND 0.0050 ND 20 sec-Butylbenzene ND 0.0050 ND 20 tert-Butylbenzene ND 0.0050 ND 20 Carbon tetrachloride ND 0.0050 ND 20 Chlorobenzene ND 0.0050 ND 20 Chloroethane ND 0.0050 ND 20 Chloroform ND 0.0050 ND 20 Chloromethane ND 0.0050 ND 20 2-Chlorotoluene ND 0.0050 ND 20 4-Chlorot0luene ND 0.0050 ND 20 Dibromochloromethane ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane ND 0.0050 ND 20 1,2-Dibromoethane (EDB) ND 0.0050 ND 20 Dibrotnomethanc ND 0.0050 ND 20 1,2-Dichlorobenzene ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 59 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Volatile Organic C,oinpounds by GUMS - Quality Control IAnalyte Result RL Units Spike Source %REC %REC RPD RPD Notes Level Result Limits Limit Batch BlC0817 - EPA 8260B Preparation: EPA 5035/5030B Solid 03/26/21 08:40 Duplicate (B1C0817-DUPI) Source: 2101941-08 Analyzed: 03/26/21 14:15 1,3-Dichlorobenzenc ND 0.0050 mg/kg ND 20 1,4-Dichlorobenzene ND 0.0050 ND 20 Dichloroditluoromcthanc ND 0.0050 ND 20 I,1-Dichloroethane ND 0.0050 ND 20 1.2-Dichloroethane ND 0.0050 NI) 20 1, 1 -Dichloroethene NI) 0.0050 ND 20 cis-1,2-Dichloroethene ND 0.0050 ND 20 trans-1,2-Dichloroethene ND 0.0050 ND 20 1,2-Dichloropropane ND 0.0050 ND 20 1,3-Dichloropropane NI) 0.0050 ND 20 2.2-Dichloropropane ND 0.0050 NI) 20 1, 1 -Dichloropropene ND 0.0050 ND 20 cis-1,3-Dichloropropene NI) 0,0050 ND 20 trans-1,3-Dichloropropene ND 0.0050 NJ) 20 Ethylbenzene ND 0.0050 ND 20 Hexachlorobutadiene ND 0.0050 ND 20 4-Isopropyl Toluene ND 0.0050 ND 20 ]sopropylbenzene ND 0.0050 ND 20 Nlethylene chloride ND 0.0050 ND 20 Naphthalene ND 0.0050 ND 20 n-Propylbenzene ND 0.0050 ND 20 Styrene ND 0.0050 ND 20 1, 1, 1,2-Tetrachloroetliane ND 0.0050 ND 20 1.1,2,2-Tetrachlorocthane ND 0.0050 ND 20 Tetrachloroethene (PCE) ND 0.0050 " ND 20 Toluene ND 0.0050 ND 20 L2,3-Trichlorobenzene ND 0.0050 ND 20 1,14-Trichlorobenzene ND 0.0050 ND 20 1, 1, 1 -Trichloroethane ND 0.0050 ND 20 1,1,2-Trichloroethane NI) 0.0050 ND 20 Trichloroethene (TCE) ND 0.0050 ND 20 Trichlorotluoromethane ND 0.0050 ND 20 1,2,3-Trichloropropane ND 0.0050 ND 20 1,2,4-Trimethylbenzene ND 0.0050 ND 20 1,3.5-Trimethylbenzene ND 0.0050 ND 20 Vinyl chloride ND 0.0050 ND 20 Xylenes (total) ND 0.0050 NI) 20 Surrogate. Dibronwlluoront(,thmic, 0.0460 0.0496 93 75-122 Surrogate. T)hiene-dS 0.047' 0.0496 95 66-128 Surrogate:4-BromoJluorohen:ene 0.0480 0.0496 97 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client. oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: 805 925-3376 Page 60 of 65 r A 1.16�R Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 Sample Method Summary /nalysis Method Matrix Laboratory & Certification Semi -Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAY 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OFC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC_ CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA -FLAP 8015 Diesel & Motor Oil List EPA 8015M Solid OEC. Internal 8015 Diesel & Motor Oil List EPA 8015M Solid OEC, CA-ELAP Total Metals by CVAA Mercury Total EPA 7471 A EPA 7471 A Solid OEC, CA -FLAP Total Metals by ICP 601013 Total Antiutony EPA 6010E Solid OEC, CA-ELAP 6010E Total Arsenic EPA 601013 Solid OEC, CA-ELAP 6010E Total Barium EPA 601013 Solid OF.C, CA -FLAP 601013 Total Beryllium EPA 601013 Solid OEC, CA-ELAP 6010E Total Cadmium EPA 6010E Solid OEC, CA -FLAP 6010E Total Chromium EPA 601013 Solid Of,(', CA-ELAP 601013 Total Cobalt EPA 6010B Solid OEC, CA-ELAP 6010B Total Copper EPA 601013 Solid OEC_ CA-ELAP 601013 Total Lead EPA 601013 Solid OEC. CA-ELAP 601013 Total Molybdenum EPA 6010B Solid OEC, CA-ELAP 6010B Total Nickel EPA 601013 Solid OF.C, CA -FLAP 601013 Total Selenium EPA 6010B Solid OEC, CA-ELAP 6010E Total Silver EPA 6010E Solid OEC. CA -FLAP 6010E Total Thallium EPA 6010E Solid OEC, CA-ELAP 601013 Total Vanadium EPA 601013 Solid OEC, CA-E.LAP 601013 Total Zinc EPA 6010E Solid OEC, CA -FLAP The results in this report apply to the samples analyzed in accordance with the chain of eustodv document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: cIient.oec.comlreports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 61 of 65 Oilfield Environmental &Compliance, Inc. Pacific Petroleum California Project: Pacific Petroleum WO & Reported: P. O. Box 2646 Project Number: Natural Healing Centers, 2600 Broad St. 2101841 Orcutt CA, 93457 Project Manager: Clarence Reynolds 03/26/2021 17:07 MethodSample nalysis Method Matrix Laboratory & Certification Volatile Organic Compounds by GC/MS 8260B Full List EPA 8260B Solid OEC, CA -FLAP Volatile Organic TPH by GC/FID 8015 TPII-Gasoline EPA 8015M Solid OF,C', Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPII-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OFC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC. Internal 8015 TPH-Gasoline EPA 8015M Solid OEC. CA-ELAP 8015 TPH-Gasoline EPA 8015M Solid OEC, Internal 8015 TPH-Gasoline EPA 8015M Solid OEC, ('A-ELAP DefinitionsNotes and Qualifier Definition MDL Method Detection Limit RL Reporting Limit (Quantitation Limit) ND Analyte NOT DETECTED at or above the method limit (MDL) RPD Relative Percent Difference D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-02 Analyte concentration below TTLC but above I Ox STLC. N-03 Analytc concentration above 20x WIT. OR-03 The RPD value for the sample duplicate or MS%MSD was outside of QC acceptance limits due to matrix interference. QC batch accepted based on LCS and or LCSI) recovery and/or RPD values. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state'tcderal ha7ard0US waste criteria limits. 5-02 The surrogate recovery for this sample cannot be accurately quantified due to interference from cocluting organic compounds present in the sample extract. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 922-4772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 62 of 65 9 0 c.i 0 cc LA - Q a. a � F C »mow E E Em m o V � � H O❑ c m � H WOOS peAIOSIG 1"01 � AIAIS"00 y °! G O 0 ZBOB I v woo ` i 80d 132ed y d folQeilual U c � p rn Q v U x ooca8-SODAS c MIS1,OB Owas dHt x C m y z L : S o y �a a, a, !n is epulnScc I epluvAO oAnaeetl03 S 1 i v� o +% `� N y 3sl I and 808Z8 0 L N y qQ �� ►. vi z ❑ ate+ Sleiew ZZ anti X w v� U a d o4 m r .c D T � v m m C, c Q r R wxx m CL V > > p 5 a OOa N Q m LL G Q ❑ U _ J 3 fi E E❑ q:Ct z 0e ti m C r ~ O ❑ .O 6 01 m QI � �- :3 K oo E El r%W ❑D r x 10 r� �. Oq r o 4 4 u Vr a, m 0 w 1� O o ❑ m m m U m O. m a F © ®� �` v Or N N y p Oil m E y to C C C L1 lu y U c%1 U Er OG W U ~ H -J d' tY ?y O �a 9 st a. oa0 E E E m � U � 1-• F= 1— ;7 4 3 t o w V N .PIIOS C� paA10910 IM01 Cn m m m AIIAIBOLop O G G Me I Moo � a� sod / load ti Illllgallusl N n� e ¢ � U OOLZO - SOOAS H WOOR OW00' dHl h L a « Q O Z = a' spUIOS Fm laPlu9Ap anpaeea rA �• ..+� Z s> o MI Ilnd Booze X N � A Z ❑ ololaW • ZZ ogll ate+ •y :: Z; U s° � a N a. in t� C, d a } .a ❑ o J n m m m `` m 0 > m v > a a — aCL �. C w d' 00 GE N � / • � � C 00� aU Eli �h m • IE E —. °+ 0 Q O U °�° 3 o Z❑r wL c Do m G r c w � 3 3 0 G f3 G El Z V x •L ❑❑ w a n o V _^ � ° t) oCL o m is in o 0❑ mmm mr y m m m m (D G �' `o a Q. N M bl E n c L to Or a 7 a M N E g CL Uv�UFawv►- JI IL a > E § \ I 0 04 E - e ) < E ) k j L n r- CL k E 2 k75 � ) e � - \ 7 n )o ) } �0 ECc / f f 0 I o U) § ƒ « 7 f 0 A t o E O ■ 4 3 3 z z ƒ & k k k 0 0 o 0:-: ■ O memo ■ Um ° C ki �°# CD x 0 $ ° § � = 7 \ / K ) ƒ § £ _ < o ] JEELL w L $ � / E [ $ D E f < E § = e 0 0 $ , 0 ® 0 /LL LD > » © ] 7« S a a/ n � \ k < w \) k ) ) ) w w V pl C N E E O U m C O d m N N a` a a a a a aa c L2� L72 a a a L 0a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N U U N U N N U c c c c c c c c c c c c c c c c c c c c c c c c c c Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y 3 3 3 3 m¢ 9 0 m 3 m Q o m 9 m 9 a 0 m 3 m 9 a 0 m 9 m 3 Q 0 �o 9 m 9 Q 0 o o 0 0 0 0 0 a0 e0 a0 a0 N aD a0 N ao ao N a0 ao N ao a0 N a0 ao IN a0 c0 N 00 a0 N c0 ao N 00 a0 d ao CD N 9p co N N N O O N rn O O N O m O O N N O) O 0 N d O) N O N N O O m N N rn O rn N N rn O rn N O O) N m N N O O) N m N O O) O N O m N0) Ov_v cn cIL y m m v O ,v_ N m g N y o g O m ,v_ v 0 m v a y m o v 0 y v g y m o y y 0 o oo y N UON LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LL LLLL LL LL C O .a o QJ Q Q Q Q QO Q ONU V1 O NNOMnOVWOUNNVOWn W 0 O o to t�o 0Q ffnn wN OQ Vfn tfn Oa Nn Un No' cop > m> m > >OJ J7co (� � (N (� C� C0N� �-o NNENN N_ O0 Nm CD O 0 Om O 00 O 04 cU O f°U Q m U Q m I. U Q m U Q m U Q m U Q m U Q m U Q m U Q m U Q m U Q m U Q m U Q m U O N N 1) M O O O -Cl) O O O O O O O O O O O O O O O O O O O. t 4 a cI0 O �•N U J N U Z N m> a I E 10 0 oO 4 LO N Q1 co 0 9 to m A by w=n q aa� E E E a E c J SPIIOS PBAIOSIO 10401 C-) Y ,UlMSauoO C C G i ZBOB I vl 608 w 8Od I ig®d �f 9 @ 61 Ulllgvllu81 ¢ G U 00caB'900AS WS LOB OWO'J' dHl L � cp Z L G a L d y, r as BPulnS I BPIURAO BAaoeaarz m d to m Z 38Ii Ilnd 808Z8 N a Z BleleW - ZZ Ball J\. d .c ❑ LL a OI m a r�- n ¢ r f m V O v :n E a m m Q:� E s� c Toa m �0 cmQ Y m � O ❑ U w � qq ❑ ih Eon ❑:.. z❑ ? O m i Y C d � G ID L M E E y y «❑ o 0 0 c ❑ ❑ } x C L w W E m g a c o a o m C .c cai CD _ ti L V p c a p !T C C d m m ,C rc K o e{ t r► V d 96 a. O 00 U - H o ❑ m m m m m c d f c p o E m C�i `_ p� t H H av o L C E°. ff ..,. N _ © C-� -� Y' C_, .7 .�... C o C C m ;E . y d r m m N ;u c U° vi U F a W U I'- iE'- j >X E T' O K U LL O Z OD 4 a Z& co 0 Lh 0 LLLL A g 0tS e- m u u Ci c o a a B a s ci q ss. E E E d our i= ❑o E o O m J W sPHOS N POA104IG 1B1o1 �- c/� 1111AlsauoO m G G O zoos V208 a 89d I Is v 'a aCi �lillgpllu8l c ,Q co x OOLZB SOOAS w � wsWs owao• aHi xx� L Ldo z .�`. = a 1 •a 00 Vj y �, epUlnS / ePlus�t� enaasea ow Q z o .049 °� d isi111nd 808Z8 `> > o a+ r4 'L s N � Z ❑ OQ a slwew - zz earl j1 .c ❑ a > ob >n £ m m ro m m ca m n 3: E C N N� V, 000p cmQ 2 r ♦ � c r ❑ U Cal a_ ° • F E E 1- ❑ Q 147' o zp� 0 ' `m 00 CD o o E c o W A❑ e r a 33 z0 a a a N e X ci ❑❑ } C G ( ca 0g n C O U �< a d � m Ed 1• � �$.m� t, - o N 0�3 o c oev+ a c° a mm a p 0.0 °D U L) 0 -, 3 ! Ln M ... a ■❑ m m m �' g h m a a v U c P E' E N Le y CL E n� d s F F o ff (� 9 m E w E c m P I {b m N z _o U N z J Q W IL W APPENDIX! E Statement of Qualifications STATEMENT OF QUALIFICATIONS Buena Resources, Inc. is a locally owned and operated full -service environmental company providing environmental consulting, field services and analytical services. Our environmental professionals are experienced in Phase I assessment, Phase II subsurface investigations and Phase III remediation. Our staff consists of professional engineers and environmental technicians. Personnel are OSHA 40 hour trained to perform environmental work when hazardous chemicals are involved. Clients for whom we've performed our services include major oil company, large utilities, industrial facilities, lending institutions, real estate developers and property owners and sellers. The following professionals performed work related to this project: Mr. Daniel Ringstmeyer is a Registered Professional Engineer, Colorado and California, Registered Environmental Assessor, Certified OSHA 40-Hour Trained worker, 8-Hour Trained Haz-mat Supervisor and a licensed California General Engineering Contractor. Mr. Ringstmeyer holds a Bachelors of Science in civil engineering from the South Dakota State University. He is the Founder/Owner and Principal Engineer of Buena Resources, Inc. and CIRRUS Environmental, Inc. He is the Principle Engineer responsible for all work performed by the environmental consulting/contracting firm. Mr. Ringstmeyer has conducted Phase I ESA assessments, Phase II subsurface investigations and Phase III remediation projects for sites throughout California and Mexico. He has designed and managed many successful remediation projects utilizing soil vapor extraction/thermal oxidation, bioremediation, groundwater pump and treat, and carbon adsorption throughout California and Mexico including the closure of a large Class I TSD Landfill facility. He has also directly been responsible for the closure of several idled oil fields and illegal agriculture landfills.