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HomeMy WebLinkAboutPRR24130 Evans[TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2102508 Report Date: May 03, 2021 16:36 Natural Healing CenterNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on April 23, 2021 13:40 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com California ELAP Certification # 2438 client.oec.com\reportsClient Connect: Page 1 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix Bin 2094-A 2102508-01 04/23/2021 11:00 04/23/2021 13:40Solid Solid Bin 2094-B 2102508-02 04/23/2021 11:05 04/23/2021 13:40Solid Solid Bin 2094-C 2102508-03 04/23/2021 11:10 04/23/2021 13:40Solid Solid Bin 20340-A 2102508-04 04/23/2021 11:15 04/23/2021 13:40Solid Solid Bin 20340-B 2102508-05 04/23/2021 11:20 04/23/2021 13:40Solid Solid Bin 20340-C 2102508-06 04/23/2021 11:25 04/23/2021 13:40Solid Solid Bin 20158-A 2102508-07 04/23/2021 11:30 04/23/2021 13:40Solid Solid Bin 20158-B 2102508-08 04/23/2021 11:35 04/23/2021 13:40Solid Solid Bin 20158-C 2102508-09 04/23/2021 11:40 04/23/2021 13:40Solid Solid Bin 2088-A 2102508-10 04/23/2021 11:45 04/23/2021 13:40Solid Solid Bin 2088-B 2102508-11 04/23/2021 11:50 04/23/2021 13:40Solid Solid Bin 2088-C 2102508-12 04/23/2021 11:55 04/23/2021 13:40Solid Solid Bin 20376-A 2102508-13 04/23/2021 12:00 04/23/2021 13:40Solid Solid Bin 20376-B 2102508-14 04/23/2021 12:05 04/23/2021 13:40Solid Solid Bin 20376-C 2102508-15 04/23/2021 12:10 04/23/2021 13:40Solid Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 2 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID *** DEFAULT GENERAL METHOD *** Asbestos Bulk PLM-(non-soil& Asphalt)(sub) OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 04/27/2021 07:10B1D0766 STLC Metals by ICP 6010B STLC 04/30/2021 10:33B1D0916 STLC Metals Extraction STLC Metals Extraction 04/28/2021 12:44B1D0838 TCLP Metals by ICP 6010B TCLP 04/30/2021 10:49B1D0919 TCLP Metals Extraction TCLP Metals Extraction 04/28/2021 12:48B1D0839 Total Metals by CVAA Mercury Total EPA 7471A 04/26/2021 09:00B1D0711 Total Metals by ICP 6010B Total 04/26/2021 07:37B1D0734 Volatile Organic Compounds by GC/MS 8260B Full List 04/23/2021 12:11B1D0650 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 04/23/2021 14:16B1D0692 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 3 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.095 B1D0711 04/26/21 14:53mg/kg 1Mercury0.094 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 13:51mg/kg B1D07341Antimony2.4 "7.4 """"Arsenic 1.9 "690 """"Barium 0.97 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "64 """"Chromium 0.48 N-02 "14 """"Cobalt 0.48 "260 """"Copper 0.97 N-02 "2400 """"Lead 0.48 N-01, N-03 "2.0 """"Molybdenum 0.48 "94 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.97 "31 """"Vanadium 1.9 "1300 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.28 B1D0916 05/03/21 12:58mg/L 2Chromium0.10 "1.6 """"Copper 0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B2.0 B1D0919 05/03/21 14:09mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 4 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 14:32mg/kg B1D06921TPH Gasoline (C5-C12)4.9 R-07 """( 39 - 157 )94 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/27/21 15:24mg/kg B1D07661TPH Diesel (C13-C22)10 "97 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )84 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 5 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 17:17mg/kg B1D06501Benzene0.051 ND """ ""Bromobenzene 0.051 ND """ ""Bromochloromethane 0.051 ND """ ""Bromodichloromethane 0.051 ND """ ""Bromoform 0.051 ND """ ""Bromomethane 0.051 ND """ ""n-Butylbenzene 0.051 ND """ ""sec-Butylbenzene 0.051 ND """ ""tert-Butylbenzene 0.051 ND """ ""Carbon tetrachloride 0.051 ND """ ""Chlorobenzene 0.051 ND """ ""Chloroethane 0.051 ND """ ""Chloroform 0.051 ND """ ""Chloromethane 0.051 ND """ ""2-Chlorotoluene 0.051 ND """ ""4-Chlorotoluene 0.051 ND """ ""Dibromochloromethane 0.051 ND """ ""1,2-Dibromo-3-chloropropane 0.051 ND """ ""1,2-Dibromoethane (EDB)0.051 ND """ ""Dibromomethane 0.051 ND """ ""1,2-Dichlorobenzene 0.051 ND """ ""1,3-Dichlorobenzene 0.051 ND """ ""1,4-Dichlorobenzene 0.051 ND """ ""Dichlorodifluoromethane 0.051 ND """ ""1,1-Dichloroethane 0.051 ND """ ""1,2-Dichloroethane 0.051 ND """ ""1,1-Dichloroethene 0.051 ND """ ""cis-1,2-Dichloroethene 0.051 ND """ ""trans-1,2-Dichloroethene 0.051 ND """ ""1,2-Dichloropropane 0.051 ND """ ""1,3-Dichloropropane 0.051 ND """ ""2,2-Dichloropropane 0.051 ND """ ""1,1-Dichloropropene 0.051 ND """ ""cis-1,3-Dichloropropene 0.051 ND """ ""trans-1,3-Dichloropropene 0.051 ND """ ""Ethylbenzene 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 6 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-A Sampled : 04/23/21 11:00 Lab ID : 2102508-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 17:17mg/kg B1D06501Hexachlorobutadiene0.051 ND """ ""4-Isopropyl Toluene 0.051 ND """ ""Isopropylbenzene 0.051 ND """ ""Methylene chloride 0.051 ND """ ""Naphthalene 0.051 ND """ ""n-Propylbenzene 0.051 ND """ ""Styrene 0.051 ND """ ""1,1,1,2-Tetrachloroethane 0.051 ND """ ""1,1,2,2-Tetrachloroethane 0.051 ND """ ""Tetrachloroethene (PCE)0.051 ND """ ""Toluene 0.051 ND """ ""1,2,3-Trichlorobenzene 0.051 ND """ ""1,2,4-Trichlorobenzene 0.051 ND """ ""1,1,1-Trichloroethane 0.051 ND """ ""1,1,2-Trichloroethane 0.051 ND """ ""Trichloroethene (TCE)0.051 ND """ ""Trichlorofluoromethane 0.051 ND """ ""1,2,3-Trichloropropane 0.051 ND """ ""1,2,4-Trimethylbenzene 0.051 ND """ ""1,3,5-Trimethylbenzene 0.051 ND """ ""Vinyl chloride 0.051 ND """ ""Xylenes (total)0.051 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )89 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 7 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:02mg/kg B1D07111Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 13:54mg/kg B1D07341Antimony2.4 "7.6 """"Arsenic 1.9 "220 """"Barium 0.97 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "100 """"Chromium 0.48 N-02, N-03 "15 """"Cobalt 0.48 "61 """"Copper 0.97 "320 """"Lead 0.48 N-02, N-03 "1.6 """"Molybdenum 0.48 "130 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.97 "38 """"Vanadium 1.9 "410 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.29 B1D0916 05/03/21 13:00mg/L 2Chromium0.10 "20 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/03/21 14:26mg/L B1D09191Chromium0.050 "0.31 """"Lead 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 8 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 14:58mg/kg B1D06921TPH Gasoline (C5-C12)4.8 R-07 """( 39 - 157 )99 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M16B1D076604/27/21 15:24mg/kg 1TPH Diesel (C13-C22)10 D-06 "150 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )80 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 9 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 17:45mg/kg B1D06501Benzene0.049 ND """ ""Bromobenzene 0.049 ND """ ""Bromochloromethane 0.049 ND """ ""Bromodichloromethane 0.049 ND """ ""Bromoform 0.049 ND """ ""Bromomethane 0.049 ND """ ""n-Butylbenzene 0.049 ND """ ""sec-Butylbenzene 0.049 ND """ ""tert-Butylbenzene 0.049 ND """ ""Carbon tetrachloride 0.049 ND """ ""Chlorobenzene 0.049 ND """ ""Chloroethane 0.049 ND """ ""Chloroform 0.049 ND """ ""Chloromethane 0.049 ND """ ""2-Chlorotoluene 0.049 ND """ ""4-Chlorotoluene 0.049 ND """ ""Dibromochloromethane 0.049 ND """ ""1,2-Dibromo-3-chloropropane 0.049 ND """ ""1,2-Dibromoethane (EDB)0.049 ND """ ""Dibromomethane 0.049 ND """ ""1,2-Dichlorobenzene 0.049 ND """ ""1,3-Dichlorobenzene 0.049 ND """ ""1,4-Dichlorobenzene 0.049 ND """ ""Dichlorodifluoromethane 0.049 ND """ ""1,1-Dichloroethane 0.049 ND """ ""1,2-Dichloroethane 0.049 ND """ ""1,1-Dichloroethene 0.049 ND """ ""cis-1,2-Dichloroethene 0.049 ND """ ""trans-1,2-Dichloroethene 0.049 ND """ ""1,2-Dichloropropane 0.049 ND """ ""1,3-Dichloropropane 0.049 ND """ ""2,2-Dichloropropane 0.049 ND """ ""1,1-Dichloropropene 0.049 ND """ ""cis-1,3-Dichloropropene 0.049 ND """ ""trans-1,3-Dichloropropene 0.049 ND """ ""Ethylbenzene 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 10 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-B Sampled : 04/23/21 11:05 Lab ID : 2102508-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 17:45mg/kg B1D06501Hexachlorobutadiene0.049 ND """ ""4-Isopropyl Toluene 0.049 ND """ ""Isopropylbenzene 0.049 ND """ ""Methylene chloride 0.049 ND """ ""Naphthalene 0.049 ND """ ""n-Propylbenzene 0.049 ND """ ""Styrene 0.049 ND """ ""1,1,1,2-Tetrachloroethane 0.049 ND """ ""1,1,2,2-Tetrachloroethane 0.049 ND """ ""Tetrachloroethene (PCE)0.049 ND """ ""Toluene 0.049 ND """ ""1,2,3-Trichlorobenzene 0.049 ND """ ""1,2,4-Trichlorobenzene 0.049 ND """ ""1,1,1-Trichloroethane 0.049 ND """ ""1,1,2-Trichloroethane 0.049 ND """ ""Trichloroethene (TCE)0.049 ND """ ""Trichlorofluoromethane 0.049 ND """ ""1,2,3-Trichloropropane 0.049 ND """ ""1,2,4-Trimethylbenzene 0.049 ND """ ""1,3,5-Trimethylbenzene 0.049 ND """ ""Vinyl chloride 0.049 ND """ ""Xylenes (total)0.049 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 11 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-03 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.17 B1D0711 04/26/21 15:04mg/kg 1Mercury0.098 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:05mg/kg B1D07341Antimony2.5 "7.7 """"Arsenic 2.0 "280 """"Barium 1.0 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "52 """"Chromium 0.50 N-02 "10 """"Cobalt 0.50 "79 """"Copper 1.0 "270 """"Lead 0.50 N-02, N-03 "1.1 """"Molybdenum 0.50 "69 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "34 """"Vanadium 2.0 "370 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.24 B1D0916 05/03/21 13:03mg/L 2Chromium0.10 "22 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.11 B1D0919 05/03/21 14:29mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 12 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 15:24mg/kg B1D06921TPH Gasoline (C5-C12)4.8 R-07 """( 39 - 157 )93 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/27/21 15:47mg/kg B1D07661TPH Diesel (C13-C22)10 "220 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )79 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 13 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 18:12mg/kg B1D06501Benzene0.049 ND """ ""Bromobenzene 0.049 ND """ ""Bromochloromethane 0.049 ND """ ""Bromodichloromethane 0.049 ND """ ""Bromoform 0.049 ND """ ""Bromomethane 0.049 ND """ ""n-Butylbenzene 0.049 ND """ ""sec-Butylbenzene 0.049 ND """ ""tert-Butylbenzene 0.049 ND """ ""Carbon tetrachloride 0.049 ND """ ""Chlorobenzene 0.049 ND """ ""Chloroethane 0.049 ND """ ""Chloroform 0.049 ND """ ""Chloromethane 0.049 ND """ ""2-Chlorotoluene 0.049 ND """ ""4-Chlorotoluene 0.049 ND """ ""Dibromochloromethane 0.049 ND """ ""1,2-Dibromo-3-chloropropane 0.049 ND """ ""1,2-Dibromoethane (EDB)0.049 ND """ ""Dibromomethane 0.049 ND """ ""1,2-Dichlorobenzene 0.049 ND """ ""1,3-Dichlorobenzene 0.049 ND """ ""1,4-Dichlorobenzene 0.049 ND """ ""Dichlorodifluoromethane 0.049 ND """ ""1,1-Dichloroethane 0.049 ND """ ""1,2-Dichloroethane 0.049 ND """ ""1,1-Dichloroethene 0.049 ND """ ""cis-1,2-Dichloroethene 0.049 ND """ ""trans-1,2-Dichloroethene 0.049 ND """ ""1,2-Dichloropropane 0.049 ND """ ""1,3-Dichloropropane 0.049 ND """ ""2,2-Dichloropropane 0.049 ND """ ""1,1-Dichloropropene 0.049 ND """ ""cis-1,3-Dichloropropene 0.049 ND """ ""trans-1,3-Dichloropropene 0.049 ND """ ""Ethylbenzene 0.049 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 14 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2094-C Sampled : 04/23/21 11:10 Lab ID : 2102508-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 18:12mg/kg B1D06501Hexachlorobutadiene0.049 ND """ ""4-Isopropyl Toluene 0.049 ND """ ""Isopropylbenzene 0.049 ND """ ""Methylene chloride 0.049 ND """ ""Naphthalene 0.049 ND """ ""n-Propylbenzene 0.049 ND """ ""Styrene 0.049 ND """ ""1,1,1,2-Tetrachloroethane 0.049 ND """ ""1,1,2,2-Tetrachloroethane 0.049 ND """ ""Tetrachloroethene (PCE)0.049 ND """ ""Toluene 0.049 ND """ ""1,2,3-Trichlorobenzene 0.049 ND """ ""1,2,4-Trichlorobenzene 0.049 ND """ ""1,1,1-Trichloroethane 0.049 ND """ ""1,1,2-Trichloroethane 0.049 ND """ ""Trichloroethene (TCE)0.049 ND """ ""Trichlorofluoromethane 0.049 ND """ ""1,2,3-Trichloropropane 0.049 ND """ ""1,2,4-Trimethylbenzene 0.049 ND """ ""1,3,5-Trimethylbenzene 0.049 ND """ ""Vinyl chloride 0.049 ND """ ""Xylenes (total)0.049 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 15 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-04 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.13 B1D0711 04/26/21 15:06mg/kg 1Mercury0.087 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:07mg/kg B1D07341Antimony2.5 "7.3 """"Arsenic 2.0 "230 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "58 """"Chromium 0.49 N-02 "12 """"Cobalt 0.49 "63 """"Copper 0.98 "390 """"Lead 0.49 N-02, N-03 "2.1 """"Molybdenum 0.49 "69 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "35 """"Vanadium 2.0 "530 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.24 B1D0916 05/03/21 13:05mg/L 2Chromium0.10 "14 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.20 B1D0919 05/03/21 14:31mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 16 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 15:50mg/kg B1D06921TPH Gasoline (C5-C12)5.2 R-07 """( 39 - 157 )99 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/27/21 15:47mg/kg B1D07661TPH Diesel (C13-C22)10 "170 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 17 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 18:40mg/kg B1D06501Benzene0.051 ND """ ""Bromobenzene 0.051 ND """ ""Bromochloromethane 0.051 ND """ ""Bromodichloromethane 0.051 ND """ ""Bromoform 0.051 ND """ ""Bromomethane 0.051 ND """ ""n-Butylbenzene 0.051 ND """ ""sec-Butylbenzene 0.051 ND """ ""tert-Butylbenzene 0.051 ND """ ""Carbon tetrachloride 0.051 ND """ ""Chlorobenzene 0.051 ND """ ""Chloroethane 0.051 ND """ ""Chloroform 0.051 ND """ ""Chloromethane 0.051 ND """ ""2-Chlorotoluene 0.051 ND """ ""4-Chlorotoluene 0.051 ND """ ""Dibromochloromethane 0.051 ND """ ""1,2-Dibromo-3-chloropropane 0.051 ND """ ""1,2-Dibromoethane (EDB)0.051 ND """ ""Dibromomethane 0.051 ND """ ""1,2-Dichlorobenzene 0.051 ND """ ""1,3-Dichlorobenzene 0.051 ND """ ""1,4-Dichlorobenzene 0.051 ND """ ""Dichlorodifluoromethane 0.051 ND """ ""1,1-Dichloroethane 0.051 ND """ ""1,2-Dichloroethane 0.051 ND """ ""1,1-Dichloroethene 0.051 ND """ ""cis-1,2-Dichloroethene 0.051 ND """ ""trans-1,2-Dichloroethene 0.051 ND """ ""1,2-Dichloropropane 0.051 ND """ ""1,3-Dichloropropane 0.051 ND """ ""2,2-Dichloropropane 0.051 ND """ ""1,1-Dichloropropene 0.051 ND """ ""cis-1,3-Dichloropropene 0.051 ND """ ""trans-1,3-Dichloropropene 0.051 ND """ ""Ethylbenzene 0.051 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 18 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-A Sampled : 04/23/21 11:15 Lab ID : 2102508-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 18:40mg/kg B1D06501Hexachlorobutadiene0.051 ND """ ""4-Isopropyl Toluene 0.051 ND """ ""Isopropylbenzene 0.051 ND """ ""Methylene chloride 0.051 ND """ ""Naphthalene 0.051 ND """ ""n-Propylbenzene 0.051 ND """ ""Styrene 0.051 ND """ ""1,1,1,2-Tetrachloroethane 0.051 ND """ ""1,1,2,2-Tetrachloroethane 0.051 ND """ ""Tetrachloroethene (PCE)0.051 ND """ ""Toluene 0.051 ND """ ""1,2,3-Trichlorobenzene 0.051 ND """ ""1,2,4-Trichlorobenzene 0.051 ND """ ""1,1,1-Trichloroethane 0.051 ND """ ""1,1,2-Trichloroethane 0.051 ND """ ""Trichloroethene (TCE)0.051 ND """ ""Trichlorofluoromethane 0.051 ND """ ""1,2,3-Trichloropropane 0.051 ND """ ""1,2,4-Trimethylbenzene 0.051 ND """ ""1,3,5-Trimethylbenzene 0.051 ND """ ""Vinyl chloride 0.051 ND """ ""Xylenes (total)0.051 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 19 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-05 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.095 B1D0711 04/26/21 15:08mg/kg 1Mercury0.091 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:10mg/kg B1D07341Antimony2.5 "10 """"Arsenic 2.0 "240 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "50 """"Chromium 0.49 N-02 "11 """"Cobalt 0.49 "54 """"Copper 0.98 "800 """"Lead 0.49 N-02, N-03 "0.77 """"Molybdenum 0.49 "79 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "37 """"Vanadium 2.0 "350 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.29 B1D0916 05/03/21 13:08mg/L 2Chromium0.10 "120 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.23 B1D0919 05/03/21 14:34mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 20 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 16:16mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )99 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M37B1D076604/27/21 16:09mg/kg 1TPH Diesel (C13-C22)10 D-06 "280 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 21 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 19:07mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 22 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-B Sampled : 04/23/21 11:20 Lab ID : 2102508-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 19:07mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )91 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 23 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-06 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:10mg/kg B1D07111Mercury0.091 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:13mg/kg B1D07341Antimony2.4 "11 """"Arsenic 2.0 "340 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.24 "50 """"Chromium 0.49 N-02 "14 """"Cobalt 0.49 "230 """"Copper 0.98 "1200 """"Lead 0.49 N-01, N-03 "1.7 """"Molybdenum 0.49 "73 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "32 """"Vanadium 2.0 "1000 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.32 B1D0916 05/03/21 13:11mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.84 B1D0919 05/03/21 14:36mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 24 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 16:42mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )96 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M29B1D076604/27/21 16:09mg/kg 1TPH Diesel (C13-C22)10 D-06 "150 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )83 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 25 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 19:35mg/kg B1D06501Benzene0.050 ND """ ""Bromobenzene 0.050 ND """ ""Bromochloromethane 0.050 ND """ ""Bromodichloromethane 0.050 ND """ ""Bromoform 0.050 ND """ ""Bromomethane 0.050 ND """ ""n-Butylbenzene 0.050 ND """ ""sec-Butylbenzene 0.050 ND """ ""tert-Butylbenzene 0.050 ND """ ""Carbon tetrachloride 0.050 ND """ ""Chlorobenzene 0.050 ND """ ""Chloroethane 0.050 ND """ ""Chloroform 0.050 ND """ ""Chloromethane 0.050 ND """ ""2-Chlorotoluene 0.050 ND """ ""4-Chlorotoluene 0.050 ND """ ""Dibromochloromethane 0.050 ND """ ""1,2-Dibromo-3-chloropropane 0.050 ND """ ""1,2-Dibromoethane (EDB)0.050 ND """ ""Dibromomethane 0.050 ND """ ""1,2-Dichlorobenzene 0.050 ND """ ""1,3-Dichlorobenzene 0.050 ND """ ""1,4-Dichlorobenzene 0.050 ND """ ""Dichlorodifluoromethane 0.050 ND """ ""1,1-Dichloroethane 0.050 ND """ ""1,2-Dichloroethane 0.050 ND """ ""1,1-Dichloroethene 0.050 ND """ ""cis-1,2-Dichloroethene 0.050 ND """ ""trans-1,2-Dichloroethene 0.050 ND """ ""1,2-Dichloropropane 0.050 ND """ ""1,3-Dichloropropane 0.050 ND """ ""2,2-Dichloropropane 0.050 ND """ ""1,1-Dichloropropene 0.050 ND """ ""cis-1,3-Dichloropropene 0.050 ND """ ""trans-1,3-Dichloropropene 0.050 ND """ ""Ethylbenzene 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 26 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20340-C Sampled : 04/23/21 11:25 Lab ID : 2102508-06 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 19:35mg/kg B1D06501Hexachlorobutadiene0.050 ND """ ""4-Isopropyl Toluene 0.050 ND """ ""Isopropylbenzene 0.050 ND """ ""Methylene chloride 0.050 ND """ ""Naphthalene 0.050 ND """ ""n-Propylbenzene 0.050 ND """ ""Styrene 0.050 ND """ ""1,1,1,2-Tetrachloroethane 0.050 ND """ ""1,1,2,2-Tetrachloroethane 0.050 ND """ ""Tetrachloroethene (PCE)0.050 ND """ ""Toluene 0.050 ND """ ""1,2,3-Trichlorobenzene 0.050 ND """ ""1,2,4-Trichlorobenzene 0.050 ND """ ""1,1,1-Trichloroethane 0.050 ND """ ""1,1,2-Trichloroethane 0.050 ND """ ""Trichloroethene (TCE)0.050 ND """ ""Trichlorofluoromethane 0.050 ND """ ""1,2,3-Trichloropropane 0.050 ND """ ""1,2,4-Trimethylbenzene 0.050 ND """ ""1,3,5-Trimethylbenzene 0.050 ND """ ""Vinyl chloride 0.050 ND """ ""Xylenes (total)0.050 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 27 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-07 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.11 B1D0711 04/26/21 15:12mg/kg 1Mercury0.092 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP EPA 6010B5.9 B1D0734 04/26/21 14:16mg/kg 1Antimony2.5 "8.5 """"Arsenic 2.0 "260 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "65 """"Chromium 0.49 N-02 "11 """"Cobalt 0.49 "77 """"Copper 0.98 "530 """"Lead 0.49 N-02, N-03 "1.2 """"Molybdenum 0.49 "91 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "34 """"Vanadium 2.0 "780 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.59 B1D0916 05/03/21 13:21mg/L 2Chromium0.10 "17 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.12 B1D0919 05/03/21 14:39mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 28 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 28 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 17:08mg/kg B1D06921TPH Gasoline (C5-C12)5.1 R-07 """( 39 - 157 )98 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M38B1D076604/27/21 16:32mg/kg 1TPH Diesel (C13-C22)10 "150 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 29 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 29 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 20:02mg/kg B1D06501Benzene0.045 ND """ ""Bromobenzene 0.045 ND """ ""Bromochloromethane 0.045 ND """ ""Bromodichloromethane 0.045 ND """ ""Bromoform 0.045 ND """ ""Bromomethane 0.045 ND """ ""n-Butylbenzene 0.045 ND """ ""sec-Butylbenzene 0.045 ND """ ""tert-Butylbenzene 0.045 ND """ ""Carbon tetrachloride 0.045 ND """ ""Chlorobenzene 0.045 ND """ ""Chloroethane 0.045 ND """ ""Chloroform 0.045 ND """ ""Chloromethane 0.045 ND """ ""2-Chlorotoluene 0.045 ND """ ""4-Chlorotoluene 0.045 ND """ ""Dibromochloromethane 0.045 ND """ ""1,2-Dibromo-3-chloropropane 0.045 ND """ ""1,2-Dibromoethane (EDB)0.045 ND """ ""Dibromomethane 0.045 ND """ ""1,2-Dichlorobenzene 0.045 ND """ ""1,3-Dichlorobenzene 0.045 ND """ ""1,4-Dichlorobenzene 0.045 ND """ ""Dichlorodifluoromethane 0.045 ND """ ""1,1-Dichloroethane 0.045 ND """ ""1,2-Dichloroethane 0.045 ND """ ""1,1-Dichloroethene 0.045 ND """ ""cis-1,2-Dichloroethene 0.045 ND """ ""trans-1,2-Dichloroethene 0.045 ND """ ""1,2-Dichloropropane 0.045 ND """ ""1,3-Dichloropropane 0.045 ND """ ""2,2-Dichloropropane 0.045 ND """ ""1,1-Dichloropropene 0.045 ND """ ""cis-1,3-Dichloropropene 0.045 ND """ ""trans-1,3-Dichloropropene 0.045 ND """ ""Ethylbenzene 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 30 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-A Sampled : 04/23/21 11:30 Lab ID : 2102508-07 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 20:02mg/kg B1D06501Hexachlorobutadiene0.045 ND """ ""4-Isopropyl Toluene 0.045 ND """ ""Isopropylbenzene 0.045 ND """ ""Methylene chloride 0.045 ND """ ""Naphthalene 0.045 ND """ ""n-Propylbenzene 0.045 ND """ ""Styrene 0.045 ND """ ""1,1,1,2-Tetrachloroethane 0.045 ND """ ""1,1,2,2-Tetrachloroethane 0.045 ND """ ""Tetrachloroethene (PCE)0.045 ND """ ""Toluene 0.045 ND """ ""1,2,3-Trichlorobenzene 0.045 ND """ ""1,2,4-Trichlorobenzene 0.045 ND """ ""1,1,1-Trichloroethane 0.045 ND """ ""1,1,2-Trichloroethane 0.045 ND """ ""Trichloroethene (TCE)0.045 ND """ ""Trichlorofluoromethane 0.045 ND """ ""1,2,3-Trichloropropane 0.045 ND """ ""1,2,4-Trimethylbenzene 0.045 ND """ ""1,3,5-Trimethylbenzene 0.045 ND """ ""Vinyl chloride 0.045 ND """ ""Xylenes (total)0.045 """( 74 - 122 )96 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )93 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 31 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-08 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.12 B1D0711 04/26/21 15:14mg/kg 1Mercury0.090 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:19mg/kg B1D07341Antimony2.5 "6.5 """"Arsenic 2.0 "270 """"Barium 0.99 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "86 """"Chromium 0.49 N-02 "25 """"Cobalt 0.49 "60 """"Copper 0.99 "190 """"Lead 0.49 N-02, N-03 "1.0 """"Molybdenum 0.49 "170 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "35 """"Vanadium 2.0 "380 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.34 B1D0916 05/03/21 13:23mg/L 2Chromium0.10 "13 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.29 B1D0919 05/03/21 14:41mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 32 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 17:34mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )89 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M93B1D076604/28/21 15:31mg/kg 4TPH Diesel (C13-C22)40 D-06 "320 """"TPH Motor Oil (C23-C40)200 """( 65 - 136 )84 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 33 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 33 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 20:30mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 34 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 34 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-B Sampled : 04/23/21 11:35 Lab ID : 2102508-08 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 20:30mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )87 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 35 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 35 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-09 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:16mg/kg B1D07111Mercury0.087 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP EPA 6010B38B1D073404/26/21 14:22mg/kg 1Antimony2.5 "13 """"Arsenic 2.0 "610 """"Barium 0.99 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "63 """"Chromium 0.49 N-02 "19 """"Cobalt 0.49 "78 """"Copper 0.99 "8000 "04/26/21 14:50"100Lead49 N-01, N-03 "1.8 "04/26/21 14:22"1Molybdenum0.49 "110 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "39 """"Vanadium 2.0 "2100 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.27 B1D0916 05/03/21 13:26mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.054 B1D0919 05/03/21 14:44mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 36 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 36 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 18:00mg/kg B1D06921TPH Gasoline (C5-C12)5.0 R-07 """( 39 - 157 )97 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M39B1D076604/27/21 16:32mg/kg 1TPH Diesel (C13-C22)10 D-06 "110 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )75 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 37 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 37 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/23/21 23:41mg/kg B1D06501Benzene0.052 ND """ ""Bromobenzene 0.052 ND """ ""Bromochloromethane 0.052 ND """ ""Bromodichloromethane 0.052 ND """ ""Bromoform 0.052 ND """ ""Bromomethane 0.052 ND """ ""n-Butylbenzene 0.052 ND """ ""sec-Butylbenzene 0.052 ND """ ""tert-Butylbenzene 0.052 ND """ ""Carbon tetrachloride 0.052 ND """ ""Chlorobenzene 0.052 ND """ ""Chloroethane 0.052 ND """ ""Chloroform 0.052 ND """ ""Chloromethane 0.052 ND """ ""2-Chlorotoluene 0.052 ND """ ""4-Chlorotoluene 0.052 ND """ ""Dibromochloromethane 0.052 ND """ ""1,2-Dibromo-3-chloropropane 0.052 ND """ ""1,2-Dibromoethane (EDB)0.052 ND """ ""Dibromomethane 0.052 ND """ ""1,2-Dichlorobenzene 0.052 ND """ ""1,3-Dichlorobenzene 0.052 ND """ ""1,4-Dichlorobenzene 0.052 ND """ ""Dichlorodifluoromethane 0.052 ND """ ""1,1-Dichloroethane 0.052 ND """ ""1,2-Dichloroethane 0.052 ND """ ""1,1-Dichloroethene 0.052 ND """ ""cis-1,2-Dichloroethene 0.052 ND """ ""trans-1,2-Dichloroethene 0.052 ND """ ""1,2-Dichloropropane 0.052 ND """ ""1,3-Dichloropropane 0.052 ND """ ""2,2-Dichloropropane 0.052 ND """ ""1,1-Dichloropropene 0.052 ND """ ""cis-1,3-Dichloropropene 0.052 ND """ ""trans-1,3-Dichloropropene 0.052 ND """ ""Ethylbenzene 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 38 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 38 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20158-C Sampled : 04/23/21 11:40 Lab ID : 2102508-09 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/23/21 23:41mg/kg B1D06501Hexachlorobutadiene0.052 ND """ ""4-Isopropyl Toluene 0.052 ND """ ""Isopropylbenzene 0.052 ND """ ""Methylene chloride 0.052 ND """ ""Naphthalene 0.052 ND """ ""n-Propylbenzene 0.052 ND """ ""Styrene 0.052 ND """ ""1,1,1,2-Tetrachloroethane 0.052 ND """ ""1,1,2,2-Tetrachloroethane 0.052 ND """ ""Tetrachloroethene (PCE)0.052 ND """ ""Toluene 0.052 ND """ ""1,2,3-Trichlorobenzene 0.052 ND """ ""1,2,4-Trichlorobenzene 0.052 ND """ ""1,1,1-Trichloroethane 0.052 ND """ ""1,1,2-Trichloroethane 0.052 ND """ ""Trichloroethene (TCE)0.052 ND """ ""Trichlorofluoromethane 0.052 ND """ ""1,2,3-Trichloropropane 0.052 ND """ ""1,2,4-Trimethylbenzene 0.052 ND """ ""1,3,5-Trimethylbenzene 0.052 ND """ ""Vinyl chloride 0.052 ND """ ""Xylenes (total)0.052 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )91 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 39 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 39 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-10 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.19 B1D0711 04/26/21 15:18mg/kg 1Mercury0.088 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:25mg/kg B1D07341Antimony2.5 "9.0 """"Arsenic 2.0 "380 """"Barium 1.0 ND """ ""Beryllium 0.50 "1.3 """"Cadmium 0.25 "44 """"Chromium 0.50 "13 """"Cobalt 0.50 "36 """"Copper 1.0 "360 """"Lead 0.50 N-02, N-03 "0.73 """"Molybdenum 0.50 "71 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "35 """"Vanadium 2.0 "780 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B12B1D091605/03/21 13:28mg/L 2Lead0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.092 B1D0919 05/03/21 14:46mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 40 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 40 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 18:26mg/kg B1D06921TPH Gasoline (C5-C12)4.6 R-07 """( 39 - 157 )98 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M21B1D076604/27/21 16:54mg/kg 1TPH Diesel (C13-C22)10 D-06 "140 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )80 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 41 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 41 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 00:08mg/kg B1D06501Benzene0.052 ND """ ""Bromobenzene 0.052 ND """ ""Bromochloromethane 0.052 ND """ ""Bromodichloromethane 0.052 ND """ ""Bromoform 0.052 ND """ ""Bromomethane 0.052 ND """ ""n-Butylbenzene 0.052 ND """ ""sec-Butylbenzene 0.052 ND """ ""tert-Butylbenzene 0.052 ND """ ""Carbon tetrachloride 0.052 ND """ ""Chlorobenzene 0.052 ND """ ""Chloroethane 0.052 ND """ ""Chloroform 0.052 ND """ ""Chloromethane 0.052 ND """ ""2-Chlorotoluene 0.052 ND """ ""4-Chlorotoluene 0.052 ND """ ""Dibromochloromethane 0.052 ND """ ""1,2-Dibromo-3-chloropropane 0.052 ND """ ""1,2-Dibromoethane (EDB)0.052 ND """ ""Dibromomethane 0.052 ND """ ""1,2-Dichlorobenzene 0.052 ND """ ""1,3-Dichlorobenzene 0.052 ND """ ""1,4-Dichlorobenzene 0.052 ND """ ""Dichlorodifluoromethane 0.052 ND """ ""1,1-Dichloroethane 0.052 ND """ ""1,2-Dichloroethane 0.052 ND """ ""1,1-Dichloroethene 0.052 ND """ ""cis-1,2-Dichloroethene 0.052 ND """ ""trans-1,2-Dichloroethene 0.052 ND """ ""1,2-Dichloropropane 0.052 ND """ ""1,3-Dichloropropane 0.052 ND """ ""2,2-Dichloropropane 0.052 ND """ ""1,1-Dichloropropene 0.052 ND """ ""cis-1,3-Dichloropropene 0.052 ND """ ""trans-1,3-Dichloropropene 0.052 ND """ ""Ethylbenzene 0.052 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 42 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 42 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-A Sampled : 04/23/21 11:45 Lab ID : 2102508-10 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 00:08mg/kg B1D06501Hexachlorobutadiene0.052 ND """ ""4-Isopropyl Toluene 0.052 ND """ ""Isopropylbenzene 0.052 ND """ ""Methylene chloride 0.052 ND """ ""Naphthalene 0.052 ND """ ""n-Propylbenzene 0.052 ND """ ""Styrene 0.052 ND """ ""1,1,1,2-Tetrachloroethane 0.052 ND """ ""1,1,2,2-Tetrachloroethane 0.052 ND """ ""Tetrachloroethene (PCE)0.052 ND """ ""Toluene 0.052 ND """ ""1,2,3-Trichlorobenzene 0.052 ND """ ""1,2,4-Trichlorobenzene 0.052 ND """ ""1,1,1-Trichloroethane 0.052 ND """ ""1,1,2-Trichloroethane 0.052 ND """ ""Trichloroethene (TCE)0.052 ND """ ""Trichlorofluoromethane 0.052 ND """ ""1,2,3-Trichloropropane 0.052 ND """ ""1,2,4-Trimethylbenzene 0.052 ND """ ""1,3,5-Trimethylbenzene 0.052 ND """ ""Vinyl chloride 0.052 ND """ ""Xylenes (total)0.052 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 43 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 43 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508- Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.11 B1D0711 04/26/21 15:20mg/kg 1Mercury0.099 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:28mg/kg B1D07341Antimony2.5 "15 """"Arsenic 2.0 "270 """"Barium 0.98 ND """ ""Beryllium 0.49 "1.4 """"Cadmium 0.25 "130 """"Chromium 0.49 N-02, N-03 "16 """"Cobalt 0.49 "68 """"Copper 0.98 "440 """"Lead 0.49 N-02, N-03 "1.2 """"Molybdenum 0.49 "120 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "38 """"Vanadium 2.0 "1400 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.23 B1D0916 05/03/21 13:31mg/L 2Chromium0.10 "14 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/03/21 14:49mg/L B1D09191Chromium0.050 "0.27 """"Lead 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 44 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 44 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 20:35mg/kg B1D06921TPH Gasoline (C5-C12)4.6 R-07 """( 39 - 157 )97 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M17B1D076604/27/21 16:54mg/kg 1TPH Diesel (C13-C22)10 D-06 "87 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )74 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 45 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 45 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 00:35mg/kg B1D06501Benzene0.045 ND """ ""Bromobenzene 0.045 ND """ ""Bromochloromethane 0.045 ND """ ""Bromodichloromethane 0.045 ND """ ""Bromoform 0.045 ND """ ""Bromomethane 0.045 ND """ ""n-Butylbenzene 0.045 ND """ ""sec-Butylbenzene 0.045 ND """ ""tert-Butylbenzene 0.045 ND """ ""Carbon tetrachloride 0.045 ND """ ""Chlorobenzene 0.045 ND """ ""Chloroethane 0.045 ND """ ""Chloroform 0.045 ND """ ""Chloromethane 0.045 ND """ ""2-Chlorotoluene 0.045 ND """ ""4-Chlorotoluene 0.045 ND """ ""Dibromochloromethane 0.045 ND """ ""1,2-Dibromo-3-chloropropane 0.045 ND """ ""1,2-Dibromoethane (EDB)0.045 ND """ ""Dibromomethane 0.045 ND """ ""1,2-Dichlorobenzene 0.045 ND """ ""1,3-Dichlorobenzene 0.045 ND """ ""1,4-Dichlorobenzene 0.045 ND """ ""Dichlorodifluoromethane 0.045 ND """ ""1,1-Dichloroethane 0.045 ND """ ""1,2-Dichloroethane 0.045 ND """ ""1,1-Dichloroethene 0.045 ND """ ""cis-1,2-Dichloroethene 0.045 ND """ ""trans-1,2-Dichloroethene 0.045 ND """ ""1,2-Dichloropropane 0.045 ND """ ""1,3-Dichloropropane 0.045 ND """ ""2,2-Dichloropropane 0.045 ND """ ""1,1-Dichloropropene 0.045 ND """ ""cis-1,3-Dichloropropene 0.045 ND """ ""trans-1,3-Dichloropropene 0.045 ND """ ""Ethylbenzene 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 46 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 46 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-B Sampled : 04/23/21 11:50 Lab ID : 2102508-11 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 00:35mg/kg B1D06501Hexachlorobutadiene0.045 ND """ ""4-Isopropyl Toluene 0.045 ND """ ""Isopropylbenzene 0.045 ND """ ""Methylene chloride 0.045 ND """ ""Naphthalene 0.045 ND """ ""n-Propylbenzene 0.045 ND """ ""Styrene 0.045 ND """ ""1,1,1,2-Tetrachloroethane 0.045 ND """ ""1,1,2,2-Tetrachloroethane 0.045 ND """ ""Tetrachloroethene (PCE)0.045 ND """ ""Toluene 0.045 ND """ ""1,2,3-Trichlorobenzene 0.045 ND """ ""1,2,4-Trichlorobenzene 0.045 ND """ ""1,1,1-Trichloroethane 0.045 ND """ ""1,1,2-Trichloroethane 0.045 ND """ ""Trichloroethene (TCE)0.045 ND """ ""Trichlorofluoromethane 0.045 ND """ ""1,2,3-Trichloropropane 0.045 ND """ ""1,2,4-Trimethylbenzene 0.045 ND """ ""1,3,5-Trimethylbenzene 0.045 ND """ ""Vinyl chloride 0.045 ND """ ""Xylenes (total)0.045 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 47 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 47 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-12 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:30mg/kg B1D07111Mercury0.096 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:31mg/kg B1D07341Antimony2.5 "13 """"Arsenic 2.0 "300 """"Barium 0.99 ND """ ""Beryllium 0.49 "19 """"Cadmium 0.25 N-02 "56 """"Chromium 0.49 N-02 "17 """"Cobalt 0.49 "1100 """"Copper 0.99 N-02 "390 """"Lead 0.49 N-02, N-03 "1.1 """"Molybdenum 0.49 "100 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "34 """"Vanadium 2.0 "660 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.088 B1D0916 05/03/21 13:34mg/L 2Cadmium0.050 "0.24 """"Chromium 0.10 "0.69 """"Copper 0.10 "10 """"Lead 0.10 N-07 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 48 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 48 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.085 B1D0919 05/03/21 14:59mg/L 1Lead0.050 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 21:01mg/kg B1D06921TPH Gasoline (C5-C12)4.8 R-07 """( 39 - 157 )96 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M20B1D076604/27/21 17:17mg/kg 1TPH Diesel (C13-C22)10 D-06 "130 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )78 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 49 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 49 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 01:02mg/kg B1D06501Benzene0.045 ND """ ""Bromobenzene 0.045 ND """ ""Bromochloromethane 0.045 ND """ ""Bromodichloromethane 0.045 ND """ ""Bromoform 0.045 ND """ ""Bromomethane 0.045 ND """ ""n-Butylbenzene 0.045 ND """ ""sec-Butylbenzene 0.045 ND """ ""tert-Butylbenzene 0.045 ND """ ""Carbon tetrachloride 0.045 ND """ ""Chlorobenzene 0.045 ND """ ""Chloroethane 0.045 ND """ ""Chloroform 0.045 ND """ ""Chloromethane 0.045 ND """ ""2-Chlorotoluene 0.045 ND """ ""4-Chlorotoluene 0.045 ND """ ""Dibromochloromethane 0.045 ND """ ""1,2-Dibromo-3-chloropropane 0.045 ND """ ""1,2-Dibromoethane (EDB)0.045 ND """ ""Dibromomethane 0.045 ND """ ""1,2-Dichlorobenzene 0.045 ND """ ""1,3-Dichlorobenzene 0.045 ND """ ""1,4-Dichlorobenzene 0.045 ND """ ""Dichlorodifluoromethane 0.045 ND """ ""1,1-Dichloroethane 0.045 ND """ ""1,2-Dichloroethane 0.045 ND """ ""1,1-Dichloroethene 0.045 ND """ ""cis-1,2-Dichloroethene 0.045 ND """ ""trans-1,2-Dichloroethene 0.045 ND """ ""1,2-Dichloropropane 0.045 ND """ ""1,3-Dichloropropane 0.045 ND """ ""2,2-Dichloropropane 0.045 ND """ ""1,1-Dichloropropene 0.045 ND """ ""cis-1,3-Dichloropropene 0.045 ND """ ""trans-1,3-Dichloropropene 0.045 ND """ ""Ethylbenzene 0.045 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 50 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 50 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 2088-C Sampled : 04/23/21 11:55 Lab ID : 2102508-12 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 01:02mg/kg B1D06501Hexachlorobutadiene0.045 ND """ ""4-Isopropyl Toluene 0.045 ND """ ""Isopropylbenzene 0.045 ND """ ""Methylene chloride 0.045 ND """ ""Naphthalene 0.045 ND """ ""n-Propylbenzene 0.045 ND """ ""Styrene 0.045 ND """ ""1,1,1,2-Tetrachloroethane 0.045 ND """ ""1,1,2,2-Tetrachloroethane 0.045 ND """ ""Tetrachloroethene (PCE)0.045 ND """ ""Toluene 0.045 ND """ ""1,2,3-Trichlorobenzene 0.045 ND """ ""1,2,4-Trichlorobenzene 0.045 ND """ ""1,1,1-Trichloroethane 0.045 ND """ ""1,1,2-Trichloroethane 0.045 ND """ ""Trichloroethene (TCE)0.045 ND """ ""Trichlorofluoromethane 0.045 ND """ ""1,2,3-Trichloropropane 0.045 ND """ ""1,2,4-Trimethylbenzene 0.045 ND """ ""1,3,5-Trimethylbenzene 0.045 ND """ ""Vinyl chloride 0.045 ND """ ""Xylenes (total)0.045 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )98 %Surrogate: Toluene-d8 """( 75 - 121 )88 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 51 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 51 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-13 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:32mg/kg B1D07111Mercury0.091 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:41mg/kg B1D07341Antimony2.5 "7.0 """"Arsenic 2.0 "360 """"Barium 1.0 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "48 """"Chromium 0.50 "10 """"Cobalt 0.50 "620 """"Copper 1.0 N-02 "940 """"Lead 0.50 N-02, N-03 "1.4 """"Molybdenum 0.50 "66 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "34 """"Vanadium 2.0 "610 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B2.4 B1D0916 05/03/21 13:36mg/L 2Copper0.10 "51 """"Lead 0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B4.7 B1D0919 05/03/21 15:01mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 52 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 52 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 21:27mg/kg B1D06921TPH Gasoline (C5-C12)5.2 R-07 """( 39 - 157 )92 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M12B1D076604/27/21 17:17mg/kg 1TPH Diesel (C13-C22)10 D-06 "67 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )73 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 53 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 53 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 01:29mg/kg B1D06501Benzene0.050 ND """ ""Bromobenzene 0.050 ND """ ""Bromochloromethane 0.050 ND """ ""Bromodichloromethane 0.050 ND """ ""Bromoform 0.050 ND """ ""Bromomethane 0.050 ND """ ""n-Butylbenzene 0.050 ND """ ""sec-Butylbenzene 0.050 ND """ ""tert-Butylbenzene 0.050 ND """ ""Carbon tetrachloride 0.050 ND """ ""Chlorobenzene 0.050 ND """ ""Chloroethane 0.050 ND """ ""Chloroform 0.050 ND """ ""Chloromethane 0.050 ND """ ""2-Chlorotoluene 0.050 ND """ ""4-Chlorotoluene 0.050 ND """ ""Dibromochloromethane 0.050 ND """ ""1,2-Dibromo-3-chloropropane 0.050 ND """ ""1,2-Dibromoethane (EDB)0.050 ND """ ""Dibromomethane 0.050 ND """ ""1,2-Dichlorobenzene 0.050 ND """ ""1,3-Dichlorobenzene 0.050 ND """ ""1,4-Dichlorobenzene 0.050 ND """ ""Dichlorodifluoromethane 0.050 ND """ ""1,1-Dichloroethane 0.050 ND """ ""1,2-Dichloroethane 0.050 ND """ ""1,1-Dichloroethene 0.050 ND """ ""cis-1,2-Dichloroethene 0.050 ND """ ""trans-1,2-Dichloroethene 0.050 ND """ ""1,2-Dichloropropane 0.050 ND """ ""1,3-Dichloropropane 0.050 ND """ ""2,2-Dichloropropane 0.050 ND """ ""1,1-Dichloropropene 0.050 ND """ ""cis-1,3-Dichloropropene 0.050 ND """ ""trans-1,3-Dichloropropene 0.050 ND """ ""Ethylbenzene 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 54 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 54 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-A Sampled : 04/23/21 12:00 Lab ID : 2102508-13 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 01:29mg/kg B1D06501Hexachlorobutadiene0.050 ND """ ""4-Isopropyl Toluene 0.050 ND """ ""Isopropylbenzene 0.050 ND """ ""Methylene chloride 0.050 ND """ ""Naphthalene 0.050 ND """ ""n-Propylbenzene 0.050 ND """ ""Styrene 0.050 ND """ ""1,1,1,2-Tetrachloroethane 0.050 ND """ ""1,1,2,2-Tetrachloroethane 0.050 ND """ ""Tetrachloroethene (PCE)0.050 ND """ ""Toluene 0.050 ND """ ""1,2,3-Trichlorobenzene 0.050 ND """ ""1,2,4-Trichlorobenzene 0.050 ND """ ""1,1,1-Trichloroethane 0.050 ND """ ""1,1,2-Trichloroethane 0.050 ND """ ""Trichloroethene (TCE)0.050 ND """ ""Trichlorofluoromethane 0.050 ND """ ""1,2,3-Trichloropropane 0.050 ND """ ""1,2,4-Trimethylbenzene 0.050 ND """ ""1,3,5-Trimethylbenzene 0.050 ND """ ""Vinyl chloride 0.050 ND """ ""Xylenes (total)0.050 """( 74 - 122 )96 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )89 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 55 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 55 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-14 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.20 B1D0711 04/26/21 15:34mg/kg 1Mercury0.097 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:44mg/kg B1D07341Antimony2.5 "6.7 """"Arsenic 2.0 "440 """"Barium 0.99 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "73 """"Chromium 0.50 N-02 "9.4 """"Cobalt 0.50 "57 """"Copper 0.99 "2000 """"Lead 0.50 N-01, N-03 "2.5 """"Molybdenum 0.50 "68 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 0.99 "30 """"Vanadium 2.0 "770 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.23 B1D0916 05/03/21 13:39mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.99 B1D0919 05/03/21 15:04mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 56 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 56 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 21:53mg/kg B1D06921TPH Gasoline (C5-C12)5.1 R-07 """( 39 - 157 )96 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M04/28/21 15:08mg/kg B1D07661TPH Diesel (C13-C22)10 "64 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )79 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 57 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 57 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 01:57mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 58 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 58 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-B Sampled : 04/23/21 12:05 Lab ID : 2102508-14 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 01:57mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )97 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )91 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 59 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 59 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102508-15 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A04/26/21 15:36mg/kg B1D07111Mercury0.094 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B04/26/21 14:47mg/kg B1D07341Antimony2.4 "5.6 """"Arsenic 1.9 "320 """"Barium 0.97 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "49 """"Chromium 0.48 "10 """"Cobalt 0.48 "41 """"Copper 0.97 "440 """"Lead 0.48 N-02, N-03 "0.80 """"Molybdenum 0.48 "68 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.97 "38 """"Vanadium 1.9 "580 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B40B1D091605/03/21 13:41mg/L 2Lead0.10 N-07 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP EPA 1311/EPA 6010B0.20 B1D0919 05/03/21 15:06mg/L 1Lead0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 60 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 60 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M04/23/21 22:18mg/kg B1D06921TPH Gasoline (C5-C12)4.6 R-07 """( 39 - 157 )94 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M140B1D076604/28/21 16:38mg/kg 2TPH Diesel (C13-C22)20 D-06 "360 """"TPH Motor Oil (C23-C40)100 """( 65 - 136 )120 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 61 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 61 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B04/24/21 02:24mg/kg B1D06501Benzene0.047 ND """ ""Bromobenzene 0.047 ND """ ""Bromochloromethane 0.047 ND """ ""Bromodichloromethane 0.047 ND """ ""Bromoform 0.047 ND """ ""Bromomethane 0.047 ND """ ""n-Butylbenzene 0.047 ND """ ""sec-Butylbenzene 0.047 ND """ ""tert-Butylbenzene 0.047 ND """ ""Carbon tetrachloride 0.047 ND """ ""Chlorobenzene 0.047 ND """ ""Chloroethane 0.047 ND """ ""Chloroform 0.047 ND """ ""Chloromethane 0.047 ND """ ""2-Chlorotoluene 0.047 ND """ ""4-Chlorotoluene 0.047 ND """ ""Dibromochloromethane 0.047 ND """ ""1,2-Dibromo-3-chloropropane 0.047 ND """ ""1,2-Dibromoethane (EDB)0.047 ND """ ""Dibromomethane 0.047 ND """ ""1,2-Dichlorobenzene 0.047 ND """ ""1,3-Dichlorobenzene 0.047 ND """ ""1,4-Dichlorobenzene 0.047 ND """ ""Dichlorodifluoromethane 0.047 ND """ ""1,1-Dichloroethane 0.047 ND """ ""1,2-Dichloroethane 0.047 ND """ ""1,1-Dichloroethene 0.047 ND """ ""cis-1,2-Dichloroethene 0.047 ND """ ""trans-1,2-Dichloroethene 0.047 ND """ ""1,2-Dichloropropane 0.047 ND """ ""1,3-Dichloropropane 0.047 ND """ ""2,2-Dichloropropane 0.047 ND """ ""1,1-Dichloropropene 0.047 ND """ ""cis-1,3-Dichloropropene 0.047 ND """ ""trans-1,3-Dichloropropene 0.047 ND """ ""Ethylbenzene 0.047 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 62 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 62 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Analytical Report for Samples Bin 20376-C Sampled : 04/23/21 12:10 Lab ID : 2102508-15 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B04/24/21 02:24mg/kg B1D06501Hexachlorobutadiene0.047 ND """ ""4-Isopropyl Toluene 0.047 ND """ ""Isopropylbenzene 0.047 ND """ ""Methylene chloride 0.047 ND """ ""Naphthalene 0.047 ND """ ""n-Propylbenzene 0.047 ND """ ""Styrene 0.047 ND """ ""1,1,1,2-Tetrachloroethane 0.047 ND """ ""1,1,2,2-Tetrachloroethane 0.047 ND """ ""Tetrachloroethene (PCE)0.047 ND """ ""Toluene 0.047 ND """ ""1,2,3-Trichlorobenzene 0.047 ND """ ""1,2,4-Trichlorobenzene 0.047 ND """ ""1,1,1-Trichloroethane 0.047 ND """ ""1,1,2-Trichloroethane 0.047 ND """ ""Trichloroethene (TCE)0.047 ND """ ""Trichlorofluoromethane 0.047 ND """ ""1,2,3-Trichloropropane 0.047 ND """ ""1,2,4-Trimethylbenzene 0.047 ND """ ""1,3,5-Trimethylbenzene 0.047 ND """ ""Vinyl chloride 0.047 ND """ ""Xylenes (total)0.047 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )97 %Surrogate: Toluene-d8 """( 75 - 121 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 63 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 63 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0711 - EPA 7471A Prep[TOC] Batch B1D0711 - EPA 7471A Preparation: EPA 7471A Prep 04/26/21 09:00 Blank (B1D0711-BLK1) [TOC_3]Blank (B1D0711-BLK1)[TOC] Analyzed: 04/26/21 14:37 Mercury mg/kgND0.10 LCS (B1D0711-BS1) [TOC_3]LCS (B1D0711-BS1)[TOC] Analyzed: 04/26/21 14:31 Mercury mg/kg0.803 0.10 0.833 85-11596 LCS Dup (B1D0711-BSD1) [TOC_3]LCS Dup (B1D0711-BSD1)[TOC] Analyzed: 04/26/21 14:33 Mercury mg/kg0.765 0.10 0.833 2085-11592 5 Duplicate (B1D0711-DUP1)Source: 2102489-02 [TOC_3]Duplicate (B1D0711-DUP1)[TOC] Analyzed: 04/26/21 14:45 Mercury mg/kg0.0432 0.099 0.0418 203 Matrix Spike (B1D0711-MS1)Source: 2102489-02 [TOC_3]Matrix Spike (B1D0711-MS1)[TOC] Analyzed: 04/26/21 14:47 Mercury mg/kg0.843 0.090 0.746 0.0418 75-125107 Matrix Spike Dup (B1D0711-MSD1)Source: 2102489-02 [TOC_3]Matrix Spike Dup (B1D0711-MSD1)[TOC] Analyzed: 04/26/21 14:49 Mercury mg/kg0.673 0.087 0.723 0.0418 20 QR-0275-12587 22 Post Spike (B1D0711-PS1)Source: 2102489-02 [TOC_3]Post Spike (B1D0711-PS1)[TOC] Analyzed: 04/26/21 14:51 Mercury ug/L5.23 5.00 0.273 85-11599 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 64 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 64 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0734 - EPA 3050B[TOC] Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Blank (B1D0734-BLK1) [TOC_3]Blank (B1D0734-BLK1)[TOC] Analyzed: 04/26/21 13:29 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1D0734-BS1) [TOC_3]LCS (B1D0734-BS1)[TOC] Analyzed: 04/26/21 13:04 Antimony mg/kg97.0 2.5 100 80-12097 Arsenic "100 2.0 100 80-120100 Barium "93.5 1.0 100 80-12094 Beryllium "99.0 0.50 100 80-12099 Cadmium "99.2 0.25 100 80-12099 Chromium "102 0.50 100 80-120102 Cobalt "100 0.50 100 80-120100 Copper "104 1.0 100 80-120104 Lead "99.4 0.50 100 80-12099 Molybdenum "98.4 0.50 100 80-12098 Nickel "102 0.50 100 80-120102 Selenium "101 2.0 100 80-120101 Silver "5.04 0.50 5.00 80-120101 Thallium "108 1.0 100 80-120108 Vanadium "99.8 2.0 100 80-120100 Zinc "97.0 2.0 100 80-12097 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 65 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 65 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 LCS Dup (B1D0734-BSD1) [TOC_3]LCS Dup (B1D0734-BSD1)[TOC] Analyzed: 04/26/21 13:06 Antimony mg/kg97.8 2.5 100 2080-12098 0.8 Arsenic "101 2.0 100 2080-120101 0.7 Barium "93.6 1.0 100 2080-12094 0.2 Beryllium "98.6 0.50 100 2080-12099 0.4 Cadmium "99.5 0.25 100 2080-120100 0.3 Chromium "103 0.50 100 2080-120103 0.8 Cobalt "101 0.50 100 2080-120101 0.3 Copper "104 1.0 100 2080-120104 0.8 Lead "99.8 0.50 100 2080-120100 0.3 Molybdenum "99.4 0.50 100 2080-12099 0.9 Nickel "102 0.50 100 2080-120102 0.4 Selenium "101 2.0 100 2080-120101 0.1 Silver "5.04 0.50 5.00 2080-120101 0.1 Thallium "108 1.0 100 2080-120108 0.5 Vanadium "100 2.0 100 2080-120100 0.4 Zinc "97.4 2.0 100 2080-12097 0.4 Duplicate (B1D0734-DUP1)Source: 2102489-01 [TOC_3]Duplicate (B1D0734-DUP1)[TOC] Analyzed: 04/26/21 13:35 Antimony mg/kgND2.5 ND 20 Arsenic "5.86 2.0 6.40 209 Barium "87.5 0.99 72.5 2019 Beryllium "0.369 0.49 0.419 2012 Cadmium "ND 0.25 ND 20 Chromium "20.3 0.49 22.2 209 Cobalt "6.53 0.49 6.95 206 Copper "18.4 0.99 21.5 2016 Lead "5.52 0.49 6.10 2010 Molybdenum "1.50 0.49 2.18 20 QR-0437 Nickel "25.9 0.49 30.4 2016 Selenium "ND 2.0 ND 20 Silver "ND 0.49 ND 20 Thallium "ND 0.99 ND 20 Vanadium "18.9 2.0 20.6 209 Zinc "49.7 2.0 53.8 208 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 66 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 66 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Matrix Spike (B1D0734-MS1)Source: 2102489-01 [TOC_3]Matrix Spike (B1D0734-MS1)[TOC] Analyzed: 04/26/21 13:08 Antimony mg/kg30.5 2.5 98.3 ND 10-11631 Arsenic "102 2.0 98.3 6.40 77-12197 Barium "159 0.98 98.3 72.5 30-16988 Beryllium "93.2 0.49 98.3 0.419 86-11194 Cadmium "90.1 0.25 98.3 ND 81-11292 Chromium "124 0.49 98.3 22.2 75-129103 Cobalt "98.3 0.49 98.3 6.95 71-12193 Copper "123 0.98 98.3 21.5 68-135103 Lead "95.5 0.49 98.3 6.10 72-12191 Molybdenum "87.8 0.49 98.3 2.18 70-11287 Nickel "122 0.49 98.3 30.4 73-12193 Selenium "91.6 2.0 98.3 ND 76-11693 Silver "4.59 0.49 4.92 ND 54-13293 Thallium "94.7 0.98 98.3 ND 64-12096 Vanadium "117 2.0 98.3 20.6 78-12498 Zinc "142 2.0 98.3 53.8 50-14389 Matrix Spike Dup (B1D0734-MSD1)Source: 2102489-01 [TOC_3]Matrix Spike Dup (B1D0734-MSD1)[TOC] Analyzed: 04/26/21 13:11 Antimony mg/kg28.7 2.4 97.7 ND 2010-11629 6 Arsenic "99.5 2.0 97.7 6.40 2077-12195 2 Barium "173 0.98 97.7 72.5 2030-169103 9 Beryllium "90.5 0.49 97.7 0.419 2086-11192 3 Cadmium "86.7 0.24 97.7 ND 2081-11289 4 Chromium "120 0.49 97.7 22.2 2075-129100 3 Cobalt "95.5 0.49 97.7 6.95 2071-12191 3 Copper "120 0.98 97.7 21.5 2068-135101 3 Lead "92.4 0.49 97.7 6.10 2072-12188 3 Molybdenum "85.4 0.49 97.7 2.18 2070-11285 3 Nickel "121 0.49 97.7 30.4 2073-12192 1 Selenium "87.5 2.0 97.7 ND 2076-11690 5 Silver "4.44 0.49 4.88 ND 2054-13291 3 Thallium "90.3 0.98 97.7 ND 2064-12092 5 Vanadium "115 2.0 97.7 20.6 2078-12496 2 Zinc "141 2.0 97.7 53.8 2050-14389 0.6 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 67 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 67 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0734 - EPA 6010B Preparation: EPA 3050B 04/26/21 07:37 Post Spike (B1D0734-PS1)Source: 2102489-01 [TOC_3]Post Spike (B1D0734-PS1)[TOC] Analyzed: 04/26/21 13:14 Antimony mg/L1.85 2.00 -0.00714 75-12593 Arsenic "2.15 2.00 0.129 75-125101 Barium "3.34 2.00 1.46 75-12594 Beryllium "1.96 2.00 0.00843 75-12597 Cadmium "1.88 2.00 -0.0200 75-12594 Chromium "2.46 2.00 0.448 75-125100 Cobalt "2.05 2.00 0.140 75-12596 Copper "2.56 2.00 0.433 75-125106 Lead "2.01 2.00 0.123 75-12594 Molybdenum "1.97 2.00 0.0438 75-12596 Nickel "2.55 2.00 0.613 75-12597 Selenium "1.96 2.00 -0.0375 75-12598 Silver "0.0965 0.100 -0.00476 75-12596 Thallium "1.98 2.00 -0.0435 75-12599 Vanadium "2.41 2.00 0.416 75-125100 Zinc "2.96 2.00 1.08 75-12594 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 68 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 68 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: STLC Metals by ICP - Quality Control[TOC_1]STLC Metals by IC Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0916 - EPA 3010A Leachate[TOC] Batch B1D0916 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:33 Blank (B1D0916-BLK1) [TOC_3]Blank (B1D0916-BLK1)[TOC] Analyzed: 05/03/21 12:22 Cadmium mg/LND0.025 Chromium "ND 0.050 Copper "ND 0.050 Lead "ND 0.050 LCS (B1D0916-BS1) [TOC_3]LCS (B1D0916-BS1)[TOC] Analyzed: 05/03/21 12:35 Cadmium mg/L9.62 0.025 10.0 80-12096 Chromium "9.56 0.050 10.0 80-12096 Copper "9.66 0.050 10.0 80-12097 Lead "9.70 0.050 10.0 80-12097 LCS Dup (B1D0916-BSD1) [TOC_3]LCS Dup (B1D0916-BSD1)[TOC] Analyzed: 05/03/21 12:37 Cadmium mg/L9.68 0.025 10.0 2080-12097 0.6 Chromium "9.59 0.050 10.0 2080-12096 0.3 Copper "9.70 0.050 10.0 2080-12097 0.4 Lead "9.78 0.050 10.0 2080-12098 0.9 Duplicate (B1D0916-DUP1)Source: 2102467-01 [TOC_3]Duplicate (B1D0916-DUP1)[TOC] Analyzed: 05/03/21 12:53 Cadmium mg/LND0.050 ND 20 Chromium "0.0860 0.10 0.111 20 QR-0425 Copper "1.53 0.10 1.76 2014 Lead "0.773 0.10 0.930 2018 Leach Fluid Blank (B1D0916-LBK1) [TOC_3]Leach Fluid Blank (B1D0916-LBK1)[TOC] Analyzed: 05/03/21 12:25 Cadmium mg/LND0.050 Chromium "ND 0.10 Copper "ND 0.10 Lead "ND 0.10 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 69 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 69 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: TCLP Metals by ICP - Quality Control[TOC_1]TCL Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0919 - EPA 3010A Leachate[TOC] Batch B1D0919 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 04/30/21 10:49 Blank (B1D0919-BLK1) [TOC_3]Blank (B1D0919-BLK1)[TOC] Analyzed: 05/03/21 13:54 Chromium mg/LND0.050 Lead "ND 0.050 LCS (B1D0919-BS1) [TOC_3]LCS (B1D0919-BS1)[TOC] Analyzed: 05/03/21 14:02 Chromium mg/L9.42 0.050 10.0 80-12094 Lead "9.97 0.050 10.0 80-120100 LCS Dup (B1D0919-BSD1) [TOC_3]LCS Dup (B1D0919-BSD1)[TOC] Analyzed: 05/03/21 14:04 Chromium mg/L9.35 0.050 10.0 2080-12094 0.7 Lead "9.82 0.050 10.0 2080-12098 2 Duplicate (B1D0919-DUP1)Source: 2102508-01 [TOC_3]Duplicate (B1D0919-DUP1)[TOC] Analyzed: 05/03/21 14:11 Chromium mg/LND0.050 ND 20 Lead "1.60 0.050 2.02 20 QR-0424 Leach Fluid Blank (B1D0919-LBK1) [TOC_3]Leach Fluid Blank (B1D0919-LBK1)[TOC] Analyzed: 05/03/21 13:57 Chromium mg/LND0.050 Lead "ND 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 70 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 70 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0692 - EPA 5035/5030B Solid GC[TOC] Batch B1D0692 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 04/23/21 08:32 Blank (B1D0692-BLK1) [TOC_3]Blank (B1D0692-BLK1)[TOC] Analyzed: 04/23/21 10:26 TPH Gasoline (C5-C12)mg/kgND0.50 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1030.128 LCS (B1D0692-BS1) [TOC_3]LCS (B1D0692-BS1)[TOC] Analyzed: 04/23/21 09:34 TPH Gasoline (C5-C12)mg/kg1.07 0.50 1.00 68-139107 "0.126 39-157Surrogate: 4-Bromofluorobenzene 1160.146 LCS Dup (B1D0692-BSD1) [TOC_3]LCS Dup (B1D0692-BSD1)[TOC] Analyzed: 04/23/21 10:00 TPH Gasoline (C5-C12)mg/kg1.05 0.49 0.988 2068-139106 2 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1210.150 Duplicate (B1D0692-DUP1)Source: 2102433-01RE1 [TOC_3]Duplicate (B1D0692-DUP1)[TOC] Analyzed: 04/23/21 22:44 TPH Gasoline (C5-C12)mg/kgND4.8 ND 20 "1.20 39-157Surrogate: 4-Bromofluorobenzene 981.18 Matrix Spike (B1D0692-MS1)Source: 2102433-01RE1 [TOC_3]Matrix Spike (B1D0692-MS1)[TOC] Analyzed: 04/23/21 23:10 TPH Gasoline (C5-C12)mg/kg8.79 4.9 9.80 ND 10-17190 "1.23 39-157Surrogate: 4-Bromofluorobenzene 1091.34 Matrix Spike Dup (B1D0692-MSD1)Source: 2102433-01RE1 [TOC_3]Matrix Spike Dup (B1D0692-MSD1)[TOC] Analyzed: 04/23/21 23:36 TPH Gasoline (C5-C12)mg/kg8.26 4.4 8.77 ND 2010-17194 6 "1.10 39-157Surrogate: 4-Bromofluorobenzene 1181.29 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 71 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 71 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0766 - EPA 3550C[TOC] Batch B1D0766 - EPA 8015M Preparation: EPA 3550C 04/27/21 07:10 Blank (B1D0766-BLK1) [TOC_3]Blank (B1D0766-BLK1)[TOC] Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "49.8 65-136Surrogate: o-Terphenyl 8441.9 LCS (B1D0766-BS1) [TOC_3]LCS (B1D0766-BS1)[TOC] Analyzed: 04/27/21 13:53 TPH Diesel (C13-C22)mg/kg42010 499 72-11584 TPH Motor Oil (C23-C40)"404 50 499 74-12681 "49.9 65-136Surrogate: o-Terphenyl 8643.0 LCS Dup (B1D0766-BSD1) [TOC_3]LCS Dup (B1D0766-BSD1)[TOC] Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22)mg/kg42010 500 2072-11584 0.2 TPH Motor Oil (C23-C40)"402 50 500 2074-12680 0.5 "50.0 65-136Surrogate: o-Terphenyl 8542.3 Duplicate (B1D0766-DUP1)Source: 2102489-01 [TOC_3]Duplicate (B1D0766-DUP1)[TOC] Analyzed: 04/27/21 15:02 TPH Diesel (C13-C22)mg/kgND9.9 ND 20 TPH Motor Oil (C23-C40)"ND 50 ND 20 "49.6 65-136Surrogate: o-Terphenyl 7838.9 Matrix Spike (B1D0766-MS1)Source: 2102489-01 [TOC_3]Matrix Spike (B1D0766-MS1)[TOC] Analyzed: 04/27/21 14:17 TPH Diesel (C13-C22)mg/kg4309.9 497 ND 46-14786 TPH Motor Oil (C23-C40)"418 50 497 ND 35-17184 "49.7 65-136Surrogate: o-Terphenyl 8140.2 Matrix Spike Dup (B1D0766-MSD1)Source: 2102489-01 [TOC_3]Matrix Spike Dup (B1D0766-MSD1)[TOC] Analyzed: 04/27/21 14:40 TPH Diesel (C13-C22)mg/kg48010 499 ND 2046-14796 11 TPH Motor Oil (C23-C40)"429 50 499 ND 2035-17186 3 "49.9 65-136Surrogate: o-Terphenyl 8944.5 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 72 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 72 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1D0650 - EPA 5035/5030B MEOH[TOC] Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (B1D0650-BLK1) [TOC_3]Blank (B1D0650-BLK1)[TOC] Analyzed: 04/23/21 16:50 Benzene mg/kgND0.0050 Bromobenzene "ND 0.0050 Bromochloromethane "ND 0.0050 Bromodichloromethane "ND 0.0050 Bromoform "ND 0.0050 Bromomethane "ND 0.0050 n-Butylbenzene "ND 0.0050 sec-Butylbenzene "ND 0.0050 tert-Butylbenzene "ND 0.0050 Carbon tetrachloride "ND 0.0050 Chlorobenzene "ND 0.0050 Chloroethane "ND 0.0050 Chloroform "ND 0.0050 Chloromethane "ND 0.0050 2-Chlorotoluene "ND 0.0050 4-Chlorotoluene "ND 0.0050 Dibromochloromethane "ND 0.0050 1,2-Dibromo-3-chloropropane "ND 0.0050 1,2-Dibromoethane (EDB)"ND 0.0050 Dibromomethane "ND 0.0050 1,2-Dichlorobenzene "ND 0.0050 1,3-Dichlorobenzene "ND 0.0050 1,4-Dichlorobenzene "ND 0.0050 Dichlorodifluoromethane "ND 0.0050 1,1-Dichloroethane "ND 0.0050 1,2-Dichloroethane "ND 0.0050 1,1-Dichloroethene "ND 0.0050 cis-1,2-Dichloroethene "ND 0.0050 trans-1,2-Dichloroethene "ND 0.0050 1,2-Dichloropropane "ND 0.0050 1,3-Dichloropropane "ND 0.0050 2,2-Dichloropropane "ND 0.0050 1,1-Dichloropropene "ND 0.0050 cis-1,3-Dichloropropene "ND 0.0050 trans-1,3-Dichloropropene "ND 0.0050 Ethylbenzene "ND 0.0050 Hexachlorobutadiene "ND 0.0050 4-Isopropyl Toluene "ND 0.0050 Isopropylbenzene "ND 0.0050 Methylene chloride "ND 0.0050 Naphthalene "ND 0.0050 n-Propylbenzene "ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 73 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 73 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Blank (B1D0650-BLK1)Analyzed: 04/23/21 16:50 Styrene mg/kgND0.0050 1,1,1,2-Tetrachloroethane "ND 0.0050 1,1,2,2-Tetrachloroethane "ND 0.0050 Tetrachloroethene (PCE)"ND 0.0050 Toluene "ND 0.0050 1,2,3-Trichlorobenzene "ND 0.0050 1,2,4-Trichlorobenzene "ND 0.0050 1,1,1-Trichloroethane "ND 0.0050 1,1,2-Trichloroethane "ND 0.0050 Trichloroethene (TCE)"ND 0.0050 Trichlorofluoromethane "ND 0.0050 1,2,3-Trichloropropane "ND 0.0050 1,2,4-Trimethylbenzene "ND 0.0050 1,3,5-Trimethylbenzene "ND 0.0050 Vinyl chloride "ND 0.0050 Xylenes (total)"ND 0.0050 "0.0498 74-122Surrogate: Dibromofluoromethane 970.0484 "0.0498 65-128Surrogate: Toluene-d8 960.0479 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 910.0453 LCS (B1D0650-BS1) [TOC_3]LCS (B1D0650-BS1)[TOC] Analyzed: 04/23/21 14:31 Benzene mg/kg0.0389 0.0050 0.0396 70-13198 Bromobenzene "0.0369 0.0050 0.0396 74-13093 Bromochloromethane "0.0351 0.0050 0.0396 64-13389 Bromodichloromethane "0.0368 0.0050 0.0396 69-13793 Bromoform "0.0337 0.0050 0.0396 55-13285 Bromomethane "0.0397 0.0050 0.0396 10-142100 n-Butylbenzene "0.0440 0.0050 0.0396 64-156111 sec-Butylbenzene "0.0465 0.0050 0.0396 75-155117 tert-Butylbenzene "0.0438 0.0050 0.0396 74-144110 Carbon tetrachloride "0.0396 0.0050 0.0396 67-135100 Chlorobenzene "0.0399 0.0050 0.0396 73-134101 Chloroethane "0.0366 0.0050 0.0396 10-16792 Chloroform "0.0371 0.0050 0.0396 69-12494 Chloromethane "0.0286 0.0050 0.0396 34-13672 2-Chlorotoluene "0.0421 0.0050 0.0396 75-135106 4-Chlorotoluene "0.0420 0.0050 0.0396 70-138106 Dibromochloromethane "0.0370 0.0050 0.0396 67-13593 1,2-Dibromo-3-chloropropane "0.0368 0.0050 0.0396 41-14993 1,2-Dibromoethane (EDB)"0.0365 0.0050 0.0396 68-13192 Dibromomethane "0.0322 0.0050 0.0396 61-14081 1,2-Dichlorobenzene "0.0409 0.0050 0.0396 76-136103 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 74 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 74 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS (B1D0650-BS1)Analyzed: 04/23/21 14:31 1,3-Dichlorobenzene mg/kg0.0427 0.0050 0.0396 76-138108 1,4-Dichlorobenzene "0.0410 0.0050 0.0396 72-132104 Dichlorodifluoromethane "0.0196 0.0050 0.0396 10-15550 1,1-Dichloroethane "0.0399 0.0050 0.0396 63-139101 1,2-Dichloroethane "0.0359 0.0050 0.0396 64-12691 1,1-Dichloroethene "0.0435 0.0050 0.0396 52-167110 cis-1,2-Dichloroethene "0.0380 0.0050 0.0396 70-13596 trans-1,2-Dichloroethene "0.0421 0.0050 0.0396 67-147106 1,2-Dichloropropane "0.0368 0.0050 0.0396 68-13193 1,3-Dichloropropane "0.0359 0.0050 0.0396 64-12891 2,2-Dichloropropane "0.0404 0.0050 0.0396 63-154102 1,1-Dichloropropene "0.0386 0.0050 0.0396 68-13897 cis-1,3-Dichloropropene "0.0376 0.0050 0.0396 72-13495 trans-1,3-Dichloropropene "0.0385 0.0050 0.0396 69-13297 Ethylbenzene "0.0404 0.0050 0.0396 68-136102 Hexachlorobutadiene "0.0446 0.0050 0.0396 72-198113 4-Isopropyl Toluene "0.0439 0.0050 0.0396 74-150111 Isopropylbenzene "0.0429 0.0050 0.0396 71-149108 Methylene chloride "0.0402 0.0050 0.0396 51-127102 Naphthalene "0.0436 0.0050 0.0396 57-158110 n-Propylbenzene "0.0435 0.0050 0.0396 70-143110 Styrene "0.0412 0.0050 0.0396 68-138104 1,1,1,2-Tetrachloroethane "0.0373 0.0050 0.0396 76-13094 1,1,2,2-Tetrachloroethane "0.0407 0.0050 0.0396 60-136103 Tetrachloroethene (PCE)"0.0381 0.0050 0.0396 73-13896 Toluene "0.0371 0.0050 0.0396 72-12894 1,2,3-Trichlorobenzene "0.0390 0.0050 0.0396 61-16698 1,2,4-Trichlorobenzene "0.0406 0.0050 0.0396 71-158103 1,1,1-Trichloroethane "0.0389 0.0050 0.0396 71-13598 1,1,2-Trichloroethane "0.0341 0.0050 0.0396 64-13286 Trichloroethene (TCE)"0.0374 0.0050 0.0396 74-13994 Trichlorofluoromethane "0.0379 0.0050 0.0396 30-15696 1,2,3-Trichloropropane "0.0383 0.0050 0.0396 67-12397 1,2,4-Trimethylbenzene "0.0419 0.0050 0.0396 68-134106 1,3,5-Trimethylbenzene "0.0440 0.0050 0.0396 71-140111 Vinyl chloride "0.0352 0.0050 0.0396 43-14489 Xylenes (total)"0.122 0.0050 0.119 69-138102 "0.0495 74-122Surrogate: Dibromofluoromethane 990.0490 "0.0495 65-128Surrogate: Toluene-d8 960.0475 "0.0495 75-121Surrogate: 4-Bromofluorobenzene 960.0476 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 75 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 75 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (B1D0650-BSD1) [TOC_3]LCS Dup (B1D0650-BSD1)[TOC] Analyzed: 04/23/21 14:59 Benzene mg/kg0.0417 0.0050 0.0398 2070-131105 7 Bromobenzene "0.0394 0.0050 0.0398 2074-13099 6 Bromochloromethane "0.0377 0.0050 0.0398 2064-13395 7 Bromodichloromethane "0.0392 0.0050 0.0398 2069-13798 6 Bromoform "0.0363 0.0050 0.0398 2055-13291 8 Bromomethane "0.0416 0.0050 0.0398 2010-142105 5 n-Butylbenzene "0.0475 0.0050 0.0398 2064-156120 8 sec-Butylbenzene "0.0493 0.0050 0.0398 2075-155124 6 tert-Butylbenzene "0.0464 0.0050 0.0398 2074-144117 6 Carbon tetrachloride "0.0418 0.0050 0.0398 2067-135105 5 Chlorobenzene "0.0420 0.0050 0.0398 2073-134106 5 Chloroethane "0.0394 0.0050 0.0398 2010-16799 7 Chloroform "0.0392 0.0050 0.0398 2069-12499 5 Chloromethane "0.0302 0.0050 0.0398 2034-13676 5 2-Chlorotoluene "0.0435 0.0050 0.0398 2075-135109 3 4-Chlorotoluene "0.0431 0.0050 0.0398 2070-138108 3 Dibromochloromethane "0.0397 0.0050 0.0398 2067-135100 7 1,2-Dibromo-3-chloropropane "0.0410 0.0050 0.0398 2041-149103 11 1,2-Dibromoethane (EDB)"0.0388 0.0050 0.0398 2068-13198 6 Dibromomethane "0.0334 0.0050 0.0398 2061-14084 4 1,2-Dichlorobenzene "0.0429 0.0050 0.0398 2076-136108 5 1,3-Dichlorobenzene "0.0444 0.0050 0.0398 2076-138112 4 1,4-Dichlorobenzene "0.0436 0.0050 0.0398 2072-132110 6 Dichlorodifluoromethane "0.0206 0.0050 0.0398 2010-15552 5 1,1-Dichloroethane "0.0424 0.0050 0.0398 2063-139107 6 1,2-Dichloroethane "0.0395 0.0050 0.0398 2064-12699 10 1,1-Dichloroethene "0.0446 0.0050 0.0398 2052-167112 2 cis-1,2-Dichloroethene "0.0413 0.0050 0.0398 2070-135104 8 trans-1,2-Dichloroethene "0.0447 0.0050 0.0398 2067-147112 6 1,2-Dichloropropane "0.0401 0.0050 0.0398 2068-131101 9 1,3-Dichloropropane "0.0383 0.0050 0.0398 2064-12896 6 2,2-Dichloropropane "0.0436 0.0050 0.0398 2063-154110 8 1,1-Dichloropropene "0.0416 0.0050 0.0398 2068-138105 8 cis-1,3-Dichloropropene "0.0407 0.0050 0.0398 2072-134102 8 trans-1,3-Dichloropropene "0.0414 0.0050 0.0398 2069-132104 7 Ethylbenzene "0.0422 0.0050 0.0398 2068-136106 4 Hexachlorobutadiene "0.0478 0.0050 0.0398 2072-198120 7 4-Isopropyl Toluene "0.0465 0.0050 0.0398 2074-150117 6 Isopropylbenzene "0.0461 0.0050 0.0398 2071-149116 7 Methylene chloride "0.0427 0.0050 0.0398 2051-127108 6 Naphthalene "0.0454 0.0050 0.0398 2057-158114 4 n-Propylbenzene "0.0460 0.0050 0.0398 2070-143116 6 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 76 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 76 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 LCS Dup (B1D0650-BSD1)Analyzed: 04/23/21 14:59 Styrene mg/kg0.0437 0.0050 0.0398 2068-138110 6 1,1,1,2-Tetrachloroethane "0.0395 0.0050 0.0398 2076-13099 6 1,1,2,2-Tetrachloroethane "0.0415 0.0050 0.0398 2060-136104 2 Tetrachloroethene (PCE)"0.0400 0.0050 0.0398 2073-138100 5 Toluene "0.0399 0.0050 0.0398 2072-128100 7 1,2,3-Trichlorobenzene "0.0432 0.0050 0.0398 2061-166109 10 1,2,4-Trichlorobenzene "0.0439 0.0050 0.0398 2071-158110 8 1,1,1-Trichloroethane "0.0415 0.0050 0.0398 2071-135104 6 1,1,2-Trichloroethane "0.0377 0.0050 0.0398 2064-13295 10 Trichloroethene (TCE)"0.0396 0.0050 0.0398 2074-13999 6 Trichlorofluoromethane "0.0412 0.0050 0.0398 2030-156104 9 1,2,3-Trichloropropane "0.0381 0.0050 0.0398 2067-12396 0.6 1,2,4-Trimethylbenzene "0.0448 0.0050 0.0398 2068-134113 7 1,3,5-Trimethylbenzene "0.0461 0.0050 0.0398 2071-140116 5 Vinyl chloride "0.0371 0.0050 0.0398 2043-14493 5 Xylenes (total)"0.128 0.0050 0.119 2069-138108 5 "0.0497 74-122Surrogate: Dibromofluoromethane 1010.0504 "0.0497 65-128Surrogate: Toluene-d8 960.0476 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 960.0475 Duplicate (B1D0650-DUP1)Source: 2102489-01 [TOC_3]Duplicate (B1D0650-DUP1)[TOC] Analyzed: 04/24/21 03:18 Benzene mg/kgND0.0050 ND 20 Bromobenzene "ND 0.0050 ND 20 Bromochloromethane "ND 0.0050 ND 20 Bromodichloromethane "ND 0.0050 ND 20 Bromoform "ND 0.0050 ND 20 Bromomethane "ND 0.0050 ND 20 n-Butylbenzene "ND 0.0050 ND 20 sec-Butylbenzene "ND 0.0050 ND 20 tert-Butylbenzene "ND 0.0050 ND 20 Carbon tetrachloride "ND 0.0050 ND 20 Chlorobenzene "ND 0.0050 ND 20 Chloroethane "ND 0.0050 ND 20 Chloroform "ND 0.0050 ND 20 Chloromethane "ND 0.0050 ND 20 2-Chlorotoluene "ND 0.0050 ND 20 4-Chlorotoluene "ND 0.0050 ND 20 Dibromochloromethane "ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane "ND 0.0050 ND 20 1,2-Dibromoethane (EDB)"ND 0.0050 ND 20 Dibromomethane "ND 0.0050 ND 20 1,2-Dichlorobenzene "ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 77 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 77 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Duplicate (B1D0650-DUP1)Source: 2102489-01 Analyzed: 04/24/21 03:18 1,3-Dichlorobenzene mg/kgND0.0050 ND 20 1,4-Dichlorobenzene "ND 0.0050 ND 20 Dichlorodifluoromethane "ND 0.0050 ND 20 1,1-Dichloroethane "ND 0.0050 ND 20 1,2-Dichloroethane "ND 0.0050 ND 20 1,1-Dichloroethene "ND 0.0050 ND 20 cis-1,2-Dichloroethene "ND 0.0050 ND 20 trans-1,2-Dichloroethene "ND 0.0050 ND 20 1,2-Dichloropropane "ND 0.0050 ND 20 1,3-Dichloropropane "ND 0.0050 ND 20 2,2-Dichloropropane "ND 0.0050 ND 20 1,1-Dichloropropene "ND 0.0050 ND 20 cis-1,3-Dichloropropene "ND 0.0050 ND 20 trans-1,3-Dichloropropene "ND 0.0050 ND 20 Ethylbenzene "ND 0.0050 ND 20 Hexachlorobutadiene "ND 0.0050 ND 20 4-Isopropyl Toluene "ND 0.0050 ND 20 Isopropylbenzene "ND 0.0050 ND 20 Methylene chloride "ND 0.0050 ND 20 Naphthalene "ND 0.0050 ND 20 n-Propylbenzene "ND 0.0050 ND 20 Styrene "ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane "ND 0.0050 ND 20 1,1,2,2-Tetrachloroethane "ND 0.0050 ND 20 Tetrachloroethene (PCE)"ND 0.0050 ND 20 Toluene "ND 0.0050 ND 20 1,2,3-Trichlorobenzene "ND 0.0050 ND 20 1,2,4-Trichlorobenzene "ND 0.0050 ND 20 1,1,1-Trichloroethane "ND 0.0050 ND 20 1,1,2-Trichloroethane "ND 0.0050 ND 20 Trichloroethene (TCE)"ND 0.0050 ND 20 Trichlorofluoromethane "ND 0.0050 ND 20 1,2,3-Trichloropropane "ND 0.0050 ND 20 1,2,4-Trimethylbenzene "ND 0.0050 ND 20 1,3,5-Trimethylbenzene "ND 0.0050 ND 20 Vinyl chloride "ND 0.0050 ND 20 Xylenes (total)"ND 0.0050 ND 20 "0.0496 74-122Surrogate: Dibromofluoromethane 970.0479 "0.0496 65-128Surrogate: Toluene-d8 980.0485 "0.0496 75-121Surrogate: 4-Bromofluorobenzene 910.0452 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 78 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 78 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (B1D0650-MS1)Source: 2102489-02 [TOC_3]Matrix Spike (B1D0650-MS1)[TOC] Analyzed: 04/24/21 04:12 Benzene mg/kg0.0404 0.0050 0.0402 ND 37-145101 Bromobenzene "0.0359 0.0050 0.0402 ND 29-14789 Bromochloromethane "0.0367 0.0050 0.0402 ND 40-14591 Bromodichloromethane "0.0384 0.0050 0.0402 ND 39-15396 Bromoform "0.0332 0.0050 0.0402 ND 32-14383 Bromomethane "0.0467 0.0050 0.0402 ND 10-141116 n-Butylbenzene "0.0324 0.0050 0.0402 ND 10-16281 sec-Butylbenzene "0.0408 0.0050 0.0402 ND 14-168102 tert-Butylbenzene "0.0388 0.0050 0.0402 ND 21-15997 Carbon tetrachloride "0.0380 0.0050 0.0402 ND 28-14895 Chlorobenzene "0.0384 0.0050 0.0402 ND 32-14896 Chloroethane "0.0502 0.0050 0.0402 ND 11-166125 Chloroform "0.0400 0.0050 0.0402 ND 40-139100 Chloromethane "0.0350 0.0050 0.0402 ND 18-13587 2-Chlorotoluene "0.0362 0.0050 0.0402 ND 25-15190 4-Chlorotoluene "0.0363 0.0050 0.0402 ND 22-15090 Dibromochloromethane "0.0359 0.0050 0.0402 ND 40-14789 1,2-Dibromo-3-chloropropane "0.0390 0.0050 0.0402 ND 25-15897 1,2-Dibromoethane (EDB)"0.0369 0.0050 0.0402 ND 38-14792 Dibromomethane "0.0319 0.0050 0.0402 ND 39-15079 1,2-Dichlorobenzene "0.0362 0.0050 0.0402 ND 24-15490 1,3-Dichlorobenzene "0.0369 0.0050 0.0402 ND 21-15392 1,4-Dichlorobenzene "0.0362 0.0050 0.0402 ND 21-14690 Dichlorodifluoromethane "0.0188 0.0050 0.0402 ND 10-14947 1,1-Dichloroethane "0.0420 0.0050 0.0402 ND 34-151105 1,2-Dichloroethane "0.0400 0.0050 0.0402 ND 40-137100 1,1-Dichloroethene "0.0449 0.0050 0.0402 ND 21-172112 cis-1,2-Dichloroethene "0.0385 0.0050 0.0402 ND 38-14796 trans-1,2-Dichloroethene "0.0409 0.0050 0.0402 ND 30-160102 1,2-Dichloropropane "0.0397 0.0050 0.0402 ND 39-14699 1,3-Dichloropropane "0.0396 0.0050 0.0402 ND 39-14199 2,2-Dichloropropane "0.0280 0.0050 0.0402 ND 26-14970 1,1-Dichloropropene "0.0385 0.0050 0.0402 ND 28-15096 cis-1,3-Dichloropropene "0.0371 0.0050 0.0402 ND 34-14992 trans-1,3-Dichloropropene "0.0384 0.0050 0.0402 ND 36-14396 Ethylbenzene "0.0397 0.0050 0.0402 0.00290 23-15092 Hexachlorobutadiene "0.0313 0.0050 0.0402 ND 10-19278 4-Isopropyl Toluene "0.0385 0.0050 0.0402 0.00290 11-16589 Isopropylbenzene "0.0406 0.0050 0.0402 0.00202 17-16696 Methylene chloride "0.0456 0.0050 0.0402 ND 28-135114 Naphthalene "0.0441 0.0050 0.0402 0.00948 10-17486 n-Propylbenzene "0.0393 0.0050 0.0402 0.00310 16-15690 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 79 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 79 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1D0650 - EPA 8260B Preparation: EPA 5035/5030B MEOH 04/23/21 12:11 Matrix Spike (B1D0650-MS1)Source: 2102489-02 Analyzed: 04/24/21 04:12 Styrene mg/kg0.0387 0.0050 0.0402 ND 24-15496 1,1,1,2-Tetrachloroethane "0.0367 0.0050 0.0402 ND 38-14991 1,1,2,2-Tetrachloroethane "0.0387 0.0050 0.0402 ND 22-16496 Tetrachloroethene (PCE)"0.0349 0.0050 0.0402 ND 25-15387 Toluene "0.0376 0.0050 0.0402 ND 26-14994 1,2,3-Trichlorobenzene "0.0323 0.0050 0.0402 ND 10-16380 1,2,4-Trichlorobenzene "0.0323 0.0050 0.0402 ND 10-16281 1,1,1-Trichloroethane "0.0387 0.0050 0.0402 ND 34-14996 1,1,2-Trichloroethane "0.0397 0.0050 0.0402 ND 25-17599 Trichloroethene (TCE)"0.0386 0.0050 0.0402 ND 25-17096 Trichlorofluoromethane "0.0487 0.0050 0.0402 ND 19-155121 1,2,3-Trichloropropane "0.0403 0.0050 0.0402 ND 32-165100 1,2,4-Trimethylbenzene "0.0466 0.0050 0.0402 0.0183 15-15070 1,3,5-Trimethylbenzene "0.0413 0.0050 0.0402 0.00496 10-15890 Vinyl chloride "0.0446 0.0050 0.0402 ND 22-148111 Xylenes (total)"0.130 0.0050 0.120 0.0173 22-15393 "0.0502 74-122Surrogate: Dibromofluoromethane 970.0487 "0.0502 65-128Surrogate: Toluene-d8 960.0484 "0.0502 75-121Surrogate: 4-Bromofluorobenzene 940.0474 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 80 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 80 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid STLC Metals by ICP STLC/EPA 6010B OEC, CA-ELAP6010B STLC Cadmium Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Chromium Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Copper Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Lead Water STLC Metals Extraction STLC OEC, InternalSTLC Metals Extraction Solid TCLP Metals by ICP EPA 1311/EPA 6010B OEC, CA-ELAP6010B TCLP Chromium Water EPA 1311/EPA 6010B OEC, CA-ELAP6010B TCLP Lead Water TCLP Metals Extraction EPA 1311 OEC, CA-ELAPTCLP Metals Extraction Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 81 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 81 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample Method Summary (Continued) Laboratory & CertificationMethodAnalysisMatrix Total Metals by CVAA EPA 7471A OEC, CA-ELAPMercury Total EPA 7471A Solid Total Metals by ICP EPA 6010B OEC, CA-ELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP8260B Full List Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 82 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 82 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Sample Method Summary (Continued) Laboratory & CertificationMethodAnalysisMatrix Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 83 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 83 of 94 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/03/2021 16:36Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102508 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL D-06 Results in the diesel organics range are primarily due to overlap from a heavy oil range product. N-01 Analyte concentration exceeds TTLC. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. N-07 STLC analyte concentration exceeds STLC limit. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 84 of 88 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 84 of 94 EMSL Analytical, Inc. 464 McCormick Street San Leandro, CA 94577 Tel/Fax: (510) 895-3675 / (510) 895-3680 http://www.EMSL.com / sanleandrolab@emsl.com 092105912EMSL Order: Customer ID:OILF50 Customer PO:2102508 Project ID: Attention:Phone:Shahanaz Parvin (805) 922-4772 Fax:Oilfield Environmental and Compliance (805) 925-3376 Received Date:307 Roemer Way 04/26/2021 8:45 AM Analysis Date:Suite 300 04/26/2021 Collected Date:Santa Maria, CA 93454-1105 04/23/2021 Project:2102508 Test Report: Asbestos Analysis of Bulk Materials via EPA 600/R-93/116 Method using Polarized Light Microscopy Sample Description Appearance % Fibrous % Non-Fibrous Non-Asbestos Asbestos % Type 2102508-16 092105912-0001 None DetectedQuartz Non-fibrous (Other) 50% 50% Tan Non-Fibrous Homogeneous 2102508-17 092105912-0002 None DetectedQuartz Ca Carbonate Non-fibrous (Other) 50% 40% 10% Gray Non-Fibrous Homogeneous Analyst(s) Gavin Lee (2)Cecilia Yu, Laboratory Manager or Other Approved Signatory EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 “Interim Method”) but augmented with procedures outlined in the 1993 (”final”) version of the method. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. Non-friable organically bound materials present a problem matrix and therefore EMSL recommends gravimetric reduction prior to analysis. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample. Estimation of uncertainty is available on request. Samples analyzed by EMSL Analytical, Inc San Leandro, CA NVLAP Lab Code 101048-3, WA C884 Initial report from: 04/26/2021 13:36:56 Page 1 of 1ASB_PLM_0008_0001 - 1.78 Printed: 4/26/2021 1:36 PM File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2314.D Operator : EW Acquired : 23 Apr 2021 2:32 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-01@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 14 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2314.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2315.D Operator : EW Acquired : 23 Apr 2021 2:58 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-02@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 15 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOMD2315.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2316.D Operator : EW Acquired : 23 Apr 2021 3:24 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-03@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 16 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2316.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2317.D Operator : EW Acquired : 23 Apr 2021 3:50 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-04@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 17 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2317.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2318.D Operator : EW Acquired : 23 Apr 2021 4:16 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-05@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 18 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2318.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2319.D Operator : EW Acquired : 23 Apr 2021 4:42 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-06@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 19 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2319.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2320.D Operator : EW Acquired : 23 Apr 2021 5:08 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-07@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 20 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2320.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2321.D Operator : EW Acquired : 23 Apr 2021 5:34 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-08@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 21 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOMD2321.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2322.D Operator : EW Acquired : 23 Apr 2021 6:00 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-09@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 22 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2322.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2323.D Operator : EW Acquired : 23 Apr 2021 6:26 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-10@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 23 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2323.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2328.D Operator : EW Acquired : 23 Apr 2021 8:35 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-11@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 28 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2328.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2329.D Operator : EW Acquired : 23 Apr 2021 9:01 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-12@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 29 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOMD2329.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2330.D Operator : EW Acquired : 23 Apr 2021 9:27 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-13@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 30 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOMD2330.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2331.D Operator : EW Acquired : 23 Apr 2021 9:53 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-14@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 31 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2331.D\FID1A File : C:\HPCHEM\1\DATA\2021\APR21\042321\GOMD2332.D Operator : EW Acquired : 23 Apr 2021 10:18 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102508-15@1:10 PREP Misc Info : 1@B1D0692 GRO Solid Vial Number: 32 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOMD2332.D\FID1A Page 85 of 94 Page 86 of 94 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLDYRD(60/ekuijuieihekuijuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 87 of 94 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$3ODVWLF%DJ(06/$QDO\WLFDO,QF6ROLG$R]*ODVV(06/$QDO\WLFDO,QF6ROLG5HFHLSW/RJLQ%\’$5HFHLSW5HYLHZHG%\$00Page 88 of 94 Page 89 of 94 Page 90 of 94 OrderID: 092105912Page 1 Of 1Page 91 of 94 STLC Cr, Cu; TCLP PbSTLC Cr, Pb; TCLP Cr,PbSTLC Cr, Pb; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr, Pb; TCLP PbSTLC Cr; TCLP PbSTLC Pb; TCLP PbPage 92 of 94 STLC Cr, Pb; TCLP Cr,PbSTLC Cr,Cd,Cu,Pb; TCLP PbSTLC Cu, Pb; TCLP PbSTLC Cr; TCLP PbSTLC Pb; TCLP Pbadded all above 6010B STLC & TCLP SP 4/28/2021Page 93 of 94 OrderID: 092105912Page 1 Of 1Page 94 of 94 [TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2102742 Report Date: May 06, 2021 17:25 Natural Healing CenterNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 05, 2021 08:00 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com California ELAP Certification # 2438 client.oec.com\reportsClient Connect: Page 1 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix NW Corner 2102742-01 05/04/2021 14:30 05/05/2021 08:00Solid Solid NE Corner 2102742-02 05/04/2021 14:35 05/05/2021 08:00Solid Solid SW Corner 2102742-03 05/04/2021 14:40 05/05/2021 08:00Solid Solid SE Corner 2102742-04 05/04/2021 14:45 05/05/2021 08:00Solid Solid Center 2102742-05 05/04/2021 14:50 05/05/2021 08:00Solid Solid [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 05/05/2021 10:31B1E0062 Total Metals by CVAA Mercury Total EPA 7471A 05/05/2021 08:00B1E0098 Total Metals by ICP 6010B Total 05/05/2021 09:08B1E0102 Volatile Organic Compounds by GC/MS 8260B Full List 05/05/2021 09:05B1E0101 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 05/05/2021 06:24B1E0095 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 2 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NW Corner Sampled : 05/04/21 14:30 Lab ID : 2102742-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:11mg/kg B1E00981Mercury0.096 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:33mg/kg B1E01021Antimony2.5 "7.8 """"Arsenic 2.0 "120 """"Barium 0.99 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "44 """"Chromium 0.50 "18 """"Cobalt 0.50 "36 """"Copper 0.99 "16 """"Lead 0.50 ND """ ""Molybdenum 0.50 "71 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 0.99 "43 """"Vanadium 2.0 "68 """"Zinc 2.0 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M19B1E009505/05/21 12:06mg/kg 1TPH Gasoline (C5-C12)4.4 D-04 """( 39 - 157 )109 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M490B1E006205/05/21 19:52mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )89 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 3 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NW Corner Sampled : 05/04/21 14:30 Lab ID : 2102742-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 16:56mg/kg B1E01011000Benzene1.3 ND """ ""Bromobenzene 1.3 ND """ ""Bromochloromethane 1.3 ND """ ""Bromodichloromethane 1.3 ND """ ""Bromoform 1.3 ND """ ""Bromomethane 1.3 ND """ ""n-Butylbenzene 1.3 ND """ ""sec-Butylbenzene 1.3 ND """ ""tert-Butylbenzene 1.3 ND """ ""Carbon tetrachloride 1.3 ND """ ""Chlorobenzene 1.3 ND """ ""Chloroethane 1.3 ND """ ""Chloroform 1.3 ND """ ""Chloromethane 1.3 ND """ ""2-Chlorotoluene 1.3 ND """ ""4-Chlorotoluene 1.3 ND """ ""Dibromochloromethane 1.3 ND """ ""1,2-Dibromo-3-chloropropane 1.3 ND """ ""1,2-Dibromoethane (EDB)1.3 ND """ ""Dibromomethane 1.3 ND """ ""1,2-Dichlorobenzene 1.3 ND """ ""1,3-Dichlorobenzene 1.3 ND """ ""1,4-Dichlorobenzene 1.3 ND """ ""Dichlorodifluoromethane 1.3 ND """ ""1,1-Dichloroethane 1.3 ND """ ""1,2-Dichloroethane 1.3 ND """ ""1,1-Dichloroethene 1.3 ND """ ""cis-1,2-Dichloroethene 1.3 ND """ ""trans-1,2-Dichloroethene 1.3 ND """ ""1,2-Dichloropropane 1.3 ND """ ""1,3-Dichloropropane 1.3 ND """ ""2,2-Dichloropropane 1.3 ND """ ""1,1-Dichloropropene 1.3 ND """ ""cis-1,3-Dichloropropene 1.3 ND """ ""trans-1,3-Dichloropropene 1.3 ND """ ""Ethylbenzene 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 4 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NW Corner Sampled : 05/04/21 14:30 Lab ID : 2102742-01 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 16:56mg/kg B1E01011000Hexachlorobutadiene1.3 ND """ ""4-Isopropyl Toluene 1.3 ND """ ""Isopropylbenzene 1.3 ND """ ""Methylene chloride 1.3 ND """ ""Naphthalene 1.3 ND """ ""n-Propylbenzene 1.3 ND """ ""Styrene 1.3 ND """ ""1,1,1,2-Tetrachloroethane 1.3 ND """ ""1,1,2,2-Tetrachloroethane 1.3 ND """ ""Tetrachloroethene (PCE)1.3 ND """ ""Toluene 1.3 ND """ ""1,2,3-Trichlorobenzene 1.3 ND """ ""1,2,4-Trichlorobenzene 1.3 ND """ ""1,1,1-Trichloroethane 1.3 ND """ ""1,1,2-Trichloroethane 1.3 ND """ ""Trichloroethene (TCE)1.3 ND """ ""Trichlorofluoromethane 1.3 ND """ ""1,2,3-Trichloropropane 1.3 ND """ ""1,2,4-Trimethylbenzene 1.3 ND """ ""1,3,5-Trimethylbenzene 1.3 ND """ ""Vinyl chloride 1.3 ND """ ""Xylenes (total)1.3 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 5 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NE Corner Sampled : 05/04/21 14:35 Lab ID : 2102742-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:13mg/kg B1E00981Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:36mg/kg B1E01021Antimony2.4 "5.0 """"Arsenic 1.9 "140 """"Barium 0.94 ND """ ""Beryllium 0.47 ND """ ""Cadmium 0.24 "160 """"Chromium 0.47 N-02, N-03 "22 """"Cobalt 0.47 "37 """"Copper 0.94 "6.8 """"Lead 0.47 "0.51 """"Molybdenum 0.47 "270 """"Nickel 0.47 N-02 ND """ ""Selenium 1.9 ND """ ""Silver 0.47 "1.7 """"Thallium 0.94 "61 """"Vanadium 1.9 "59 """"Zinc 1.9 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M5.6 B1E0095 05/05/21 12:32mg/kg 1TPH Gasoline (C5-C12)4.3 D-04 """( 39 - 157 )108 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M310B1E006205/05/21 21:27mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )85 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 6 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NE Corner Sampled : 05/04/21 14:35 Lab ID : 2102742-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 17:24mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 7 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples NE Corner Sampled : 05/04/21 14:35 Lab ID : 2102742-02 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 17:24mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )95 %Surrogate: Dibromofluoromethane """( 65 - 128 )94 %Surrogate: Toluene-d8 """( 75 - 121 )86 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 8 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SW Corner Sampled : 05/04/21 14:40 Lab ID : 2102742-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-03 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:15mg/kg B1E00981Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:46mg/kg B1E01021Antimony2.3 "4.5 """"Arsenic 1.9 "200 """"Barium 0.93 ND """ ""Beryllium 0.47 ND """ ""Cadmium 0.23 "310 """"Chromium 0.47 N-02, N-03 "55 """"Cobalt 0.47 "45 """"Copper 0.93 "9.5 """"Lead 0.47 "0.68 """"Molybdenum 0.47 "430 """"Nickel 0.47 N-02 ND """ ""Selenium 1.9 ND """ ""Silver 0.47 ND """ ""Thallium 0.93 "70 """"Vanadium 1.9 "69 """"Zinc 1.9 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M7.8 B1E0095 05/05/21 12:58mg/kg 1TPH Gasoline (C5-C12)5.0 D-04 """( 39 - 157 )101 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M220B1E006205/05/21 21:51mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )84 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 9 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SW Corner Sampled : 05/04/21 14:40 Lab ID : 2102742-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 17:51mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 10 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SW Corner Sampled : 05/04/21 14:40 Lab ID : 2102742-03 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 17:51mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )93 %Surrogate: Dibromofluoromethane """( 65 - 128 )94 %Surrogate: Toluene-d8 """( 75 - 121 )88 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 11 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SE Corner Sampled : 05/04/21 14:45 Lab ID : 2102742-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-04 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:17mg/kg B1E00981Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:49mg/kg B1E01021Antimony2.3 "5.0 """"Arsenic 1.8 "180 """"Barium 0.92 ND """ ""Beryllium 0.46 ND """ ""Cadmium 0.23 "46 """"Chromium 0.46 "14 """"Cobalt 0.46 "41 """"Copper 0.92 "13 """"Lead 0.46 ND """ ""Molybdenum 0.46 "85 """"Nickel 0.46 ND """ ""Selenium 1.8 ND """ ""Silver 0.46 "1.9 """"Thallium 0.92 "39 """"Vanadium 1.8 "57 """"Zinc 1.8 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M5.6 B1E0095 05/05/21 13:24mg/kg 1TPH Gasoline (C5-C12)4.4 D-04 """( 39 - 157 )108 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M190B1E006205/05/21 22:15mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )85 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 12 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SE Corner Sampled : 05/04/21 14:45 Lab ID : 2102742-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 18:18mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 13 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples SE Corner Sampled : 05/04/21 14:45 Lab ID : 2102742-04 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 18:18mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )98 %Surrogate: Dibromofluoromethane """( 65 - 128 )96 %Surrogate: Toluene-d8 """( 75 - 121 )90 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 14 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples Center Sampled : 05/04/21 14:50 Lab ID : 2102742-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA [TOC_1]2102742-05 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/05/21 12:19mg/kg B1E00981Mercury0.086 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/06/21 13:52mg/kg B1E01021Antimony2.4 "7.0 """"Arsenic 1.9 "140 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "72 """"Chromium 0.48 N-02 "22 """"Cobalt 0.48 "78 """"Copper 0.96 "15 """"Lead 0.48 "0.99 """"Molybdenum 0.48 "160 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 "1.3 """"Thallium 0.96 "62 """"Vanadium 1.9 "80 """"Zinc 1.9 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M7.7 B1E0095 05/05/21 13:49mg/kg 1TPH Gasoline (C5-C12)4.8 D-04 """( 39 - 157 )106 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M350B1E006205/05/21 22:38mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )86 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 15 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples Center Sampled : 05/04/21 14:50 Lab ID : 2102742-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/05/21 18:46mg/kg B1E01011000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 16 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Analytical Report for Samples Center Sampled : 05/04/21 14:50 Lab ID : 2102742-05 Matrix : Solid Sample ID : Sampled by : Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/05/21 18:46mg/kg B1E01011000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )94 %Surrogate: Dibromofluoromethane """( 65 - 128 )95 %Surrogate: Toluene-d8 """( 75 - 121 )88 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 17 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0098 - EPA 7471A Prep[TOC] Batch B1E0098 - EPA 7471A Preparation: EPA 7471A Prep 05/05/21 08:00 Blank (B1E0098-BLK1) [TOC_3]Blank (B1E0098-BLK1)[TOC] Analyzed: 05/05/21 11:40 Mercury mg/kgND0.10 LCS (B1E0098-BS1) [TOC_3]LCS (B1E0098-BS1)[TOC] Analyzed: 05/05/21 11:35 Mercury mg/kg0.802 0.10 0.833 85-11596 LCS Dup (B1E0098-BSD1) [TOC_3]LCS Dup (B1E0098-BSD1)[TOC] Analyzed: 05/05/21 11:37 Mercury mg/kg0.831 0.10 0.833 2085-115100 4 Duplicate (B1E0098-DUP1)Source: 2102717-01 [TOC_3]Duplicate (B1E0098-DUP1)[TOC] Analyzed: 05/05/21 11:44 Mercury mg/kg0.0262 0.10 0.0394 20 QR-0440 Matrix Spike (B1E0098-MS1)Source: 2102717-01 [TOC_3]Matrix Spike (B1E0098-MS1)[TOC] Analyzed: 05/05/21 11:46 Mercury mg/kg0.836 0.097 0.812 0.0394 75-12598 Matrix Spike Dup (B1E0098-MSD1)Source: 2102717-01 [TOC_3]Matrix Spike Dup (B1E0098-MSD1)[TOC] Analyzed: 05/05/21 11:48 Mercury mg/kg0.838 0.098 0.814 0.0394 2075-12598 0.3 Post Spike (B1E0098-PS1)Source: 2102717-01 [TOC_3]Post Spike (B1E0098-PS1)[TOC] Analyzed: 05/05/21 11:50 Mercury ug/L5.22 5.00 0.256 85-11599 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 18 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0102 - EPA 3050B[TOC] Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Blank (B1E0102-BLK1) [TOC_3]Blank (B1E0102-BLK1)[TOC] Analyzed: 05/06/21 13:12 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1E0102-BS1) [TOC_3]LCS (B1E0102-BS1)[TOC] Analyzed: 05/06/21 12:50 Antimony mg/kg99.2 2.5 100 80-12099 Arsenic "99.8 2.0 100 80-120100 Barium "102 1.0 100 80-120102 Beryllium "96.5 0.50 100 80-12096 Cadmium "101 0.25 100 80-120101 Chromium "102 0.50 100 80-120102 Cobalt "102 0.50 100 80-120102 Copper "103 1.0 100 80-120103 Lead "103 0.50 100 80-120103 Molybdenum "98.1 0.50 100 80-12098 Nickel "102 0.50 100 80-120102 Selenium "97.7 2.0 100 80-12098 Silver "4.81 0.50 5.00 80-12096 Thallium "104 1.0 100 80-120104 Vanadium "98.6 2.0 100 80-12099 Zinc "101 2.0 100 80-120101 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 19 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 LCS Dup (B1E0102-BSD1) [TOC_3]LCS Dup (B1E0102-BSD1)[TOC] Analyzed: 05/06/21 12:52 Antimony mg/kg99.8 2.5 100 2080-120100 0.6 Arsenic "102 2.0 100 2080-120102 2 Barium "103 1.0 100 2080-120103 1 Beryllium "97.2 0.50 100 2080-12097 0.8 Cadmium "102 0.25 100 2080-120102 0.9 Chromium "103 0.50 100 2080-120103 0.6 Cobalt "103 0.50 100 2080-120103 0.6 Copper "103 1.0 100 2080-120103 0.6 Lead "103 0.50 100 2080-120103 0.5 Molybdenum "99.6 0.50 100 2080-120100 2 Nickel "103 0.50 100 2080-120103 0.6 Selenium "100 2.0 100 2080-120100 3 Silver "4.89 0.50 5.00 2080-12098 2 Thallium "105 1.0 100 2080-120105 2 Vanadium "98.9 2.0 100 2080-12099 0.4 Zinc "102 2.0 100 2080-120102 0.6 Duplicate (B1E0102-DUP1)Source: 2102717-02 [TOC_3]Duplicate (B1E0102-DUP1)[TOC] Analyzed: 05/06/21 13:17 Antimony mg/kgND2.4 ND 20 Arsenic "7.55 1.9 8.39 2010 Barium "92.7 0.95 97.2 205 Beryllium "0.657 0.48 0.691 205 Cadmium "ND 0.24 ND 20 Chromium "16.8 0.48 16.2 204 Cobalt "7.71 0.48 8.09 205 Copper "18.7 0.95 19.7 205 Lead "11.1 0.48 11.8 206 Molybdenum "1.43 0.48 1.58 2010 Nickel "22.9 0.48 19.7 2015 Selenium "ND 1.9 ND 20 Silver "ND 0.48 ND 20 Thallium "ND 0.95 ND 20 Vanadium "32.2 1.9 32.7 202 Zinc "60.1 1.9 64.4 207 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 20 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Matrix Spike (B1E0102-MS1)Source: 2102717-02 [TOC_3]Matrix Spike (B1E0102-MS1)[TOC] Analyzed: 05/06/21 12:55 Antimony mg/kg26.4 2.5 99.2 ND 10-11627 Arsenic "105 2.0 99.2 8.39 77-12198 Barium "193 0.99 99.2 97.2 30-16997 Beryllium "93.6 0.50 99.2 0.691 86-11194 Cadmium "93.6 0.25 99.2 ND 81-11294 Chromium "118 0.50 99.2 16.2 75-129103 Cobalt "102 0.50 99.2 8.09 71-12194 Copper "119 0.99 99.2 19.7 68-135100 Lead "105 0.50 99.2 11.8 72-12194 Molybdenum "89.4 0.50 99.2 1.58 70-11289 Nickel "114 0.50 99.2 19.7 73-12195 Selenium "89.8 2.0 99.2 ND 76-11691 Silver "4.31 0.50 4.96 ND 54-13287 Thallium "89.0 0.99 99.2 ND 64-12090 Vanadium "130 2.0 99.2 32.7 78-12498 Zinc "158 2.0 99.2 64.4 50-14394 Matrix Spike Dup (B1E0102-MSD1)Source: 2102717-02 [TOC_3]Matrix Spike Dup (B1E0102-MSD1)[TOC] Analyzed: 05/06/21 12:57 Antimony mg/kg29.7 2.4 94.4 ND 2010-11631 12 Arsenic "103 1.9 94.4 8.39 2077-121101 2 Barium "182 0.94 94.4 97.2 2030-16989 6 Beryllium "91.6 0.47 94.4 0.691 2086-11196 2 Cadmium "91.5 0.24 94.4 ND 2081-11297 2 Chromium "113 0.47 94.4 16.2 2075-129103 4 Cobalt "99.2 0.47 94.4 8.09 2071-12196 3 Copper "114 0.94 94.4 19.7 2068-135100 4 Lead "102 0.47 94.4 11.8 2072-12196 3 Molybdenum "88.9 0.47 94.4 1.58 2070-11292 0.6 Nickel "111 0.47 94.4 19.7 2073-12196 3 Selenium "88.7 1.9 94.4 ND 2076-11694 1 Silver "4.23 0.47 4.72 ND 2054-13290 2 Thallium "87.0 0.94 94.4 ND 2064-12092 2 Vanadium "126 1.9 94.4 32.7 2078-12498 4 Zinc "153 1.9 94.4 64.4 2050-14394 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 21 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0102 - EPA 6010B Preparation: EPA 3050B 05/05/21 09:08 Post Spike (B1E0102-PS1)Source: 2102717-02 [TOC_3]Post Spike (B1E0102-PS1)[TOC] Analyzed: 05/06/21 13:00 Antimony mg/L1.95 2.00 -0.0338 75-12598 Arsenic "2.25 2.00 0.171 75-125104 Barium "3.97 2.00 1.98 75-12599 Beryllium "1.97 2.00 0.0141 75-12598 Cadmium "1.97 2.00 -0.0215 75-12599 Chromium "2.42 2.00 0.330 75-125104 Cobalt "2.15 2.00 0.165 75-12599 Copper "2.51 2.00 0.401 75-125105 Lead "2.20 2.00 0.240 75-12598 Molybdenum "2.02 2.00 0.0322 75-12599 Nickel "2.48 2.00 0.403 75-125104 Selenium "1.96 2.00 -0.0744 75-12598 Silver "0.0946 0.100 -0.00744 75-12595 Thallium "1.88 2.00 -0.0732 75-12594 Vanadium "2.71 2.00 0.668 75-125102 Zinc "3.25 2.00 1.31 75-12597 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 22 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0095 - EPA 5035/5030B Solid GC[TOC] Batch B1E0095 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/05/21 06:24 Blank (B1E0095-BLK1) [TOC_3]Blank (B1E0095-BLK1)[TOC] Analyzed: 05/05/21 09:00 TPH Gasoline (C5-C12)mg/kgND0.50 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1080.134 LCS (B1E0095-BS1) [TOC_3]LCS (B1E0095-BS1)[TOC] Analyzed: 05/05/21 08:09 TPH Gasoline (C5-C12)mg/kg0.917 0.50 0.992 68-13992 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1270.158 LCS Dup (B1E0095-BSD1) [TOC_3]LCS Dup (B1E0095-BSD1)[TOC] Analyzed: 05/05/21 08:34 TPH Gasoline (C5-C12)mg/kg1.03 0.50 0.994 2068-139103 11 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1270.157 Duplicate (B1E0095-DUP1)Source: 2102652-01 [TOC_3]Duplicate (B1E0095-DUP1)[TOC] Analyzed: 05/05/21 09:59 TPH Gasoline (C5-C12)mg/kgND5.2 ND 20 "1.30 39-157Surrogate: 4-Bromofluorobenzene 1001.30 Matrix Spike (B1E0095-MS1)Source: 2102652-01 [TOC_3]Matrix Spike (B1E0095-MS1)[TOC] Analyzed: 05/05/21 14:41 TPH Gasoline (C5-C12)mg/kg7.97 4.9 9.80 ND 10-17181 "1.23 39-157Surrogate: 4-Bromofluorobenzene 1151.40 Matrix Spike Dup (B1E0095-MSD1)Source: 2102652-01 [TOC_3]Matrix Spike Dup (B1E0095-MSD1)[TOC] Analyzed: 05/05/21 15:07 TPH Gasoline (C5-C12)mg/kg8.18 5.2 10.4 ND 2010-17178 3 "1.30 39-157Surrogate: 4-Bromofluorobenzene 1071.40 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 23 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0062 - EPA 3550C[TOC] Batch B1E0062 - EPA 8015M Preparation: EPA 3550C 05/05/21 10:31 Blank (B1E0062-BLK1) [TOC_3]Blank (B1E0062-BLK1)[TOC] Analyzed: 05/05/21 17:58 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "49.9 65-136Surrogate: o-Terphenyl 7637.8 LCS (B1E0062-BS1) [TOC_3]LCS (B1E0062-BS1)[TOC] Analyzed: 05/05/21 17:12 TPH Diesel (C13-C22)mg/kg41110 500 72-11582 TPH Motor Oil (C23-C40)"467 50 500 74-12693 "50.0 65-136Surrogate: o-Terphenyl 8040.0 LCS Dup (B1E0062-BSD1) [TOC_3]LCS Dup (B1E0062-BSD1)[TOC] Analyzed: 05/05/21 17:35 TPH Diesel (C13-C22)mg/kg43310 499 2072-11587 5 TPH Motor Oil (C23-C40)"493 50 499 2074-12699 6 "49.9 65-136Surrogate: o-Terphenyl 8241.1 Duplicate (B1E0062-DUP1)Source: 2102648-01 [TOC_3]Duplicate (B1E0062-DUP1)[TOC] Analyzed: 05/05/21 21:27 TPH Diesel (C13-C22)mg/kg35.5 10 34.6 20 D-042 TPH Motor Oil (C23-C40)"71.2 50 65.4 20 D-048 "49.8 65-136Surrogate: o-Terphenyl 10853.6 Matrix Spike (B1E0062-MS1)Source: 2102648-01 [TOC_3]Matrix Spike (B1E0062-MS1)[TOC] Analyzed: 05/05/21 21:51 TPH Diesel (C13-C22)mg/kg73110 499 34.6 46-147140 TPH Motor Oil (C23-C40)"559 50 499 65.4 35-17199 "49.9 65-136Surrogate: o-Terphenyl 8844.1 Matrix Spike Dup (B1E0062-MSD1)Source: 2102648-01 [TOC_3]Matrix Spike Dup (B1E0062-MSD1)[TOC] Analyzed: 05/05/21 22:15 TPH Diesel (C13-C22)mg/kg56210 499 34.6 20 QR-0246-147106 26 TPH Motor Oil (C23-C40)"485 50 499 65.4 2035-17184 14 "49.9 65-136Surrogate: o-Terphenyl 8341.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 24 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0101 - EPA 5035/5030B MEOH[TOC] Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLK1) [TOC_3]Blank (B1E0101-BLK1)[TOC] Analyzed: 05/05/21 13:17 Benzene mg/kgND0.25 Bromobenzene "ND 0.25 Bromochloromethane "ND 0.25 Bromodichloromethane "ND 0.25 Bromoform "ND 0.25 Bromomethane "ND 0.25 n-Butylbenzene "ND 0.25 sec-Butylbenzene "ND 0.25 tert-Butylbenzene "ND 0.25 Carbon tetrachloride "ND 0.25 Chlorobenzene "ND 0.25 Chloroethane "ND 0.25 Chloroform "ND 0.25 Chloromethane "ND 0.25 2-Chlorotoluene "ND 0.25 4-Chlorotoluene "ND 0.25 Dibromochloromethane "ND 0.25 1,2-Dibromo-3-chloropropane "ND 0.25 1,2-Dibromoethane (EDB)"ND 0.25 Dibromomethane "ND 0.25 1,2-Dichlorobenzene "ND 0.25 1,3-Dichlorobenzene "ND 0.25 1,4-Dichlorobenzene "ND 0.25 Dichlorodifluoromethane "ND 0.25 1,1-Dichloroethane "ND 0.25 1,2-Dichloroethane "ND 0.25 1,1-Dichloroethene "ND 0.25 cis-1,2-Dichloroethene "ND 0.25 trans-1,2-Dichloroethene "ND 0.25 1,2-Dichloropropane "ND 0.25 1,3-Dichloropropane "ND 0.25 2,2-Dichloropropane "ND 0.25 1,1-Dichloropropene "ND 0.25 cis-1,3-Dichloropropene "ND 0.25 trans-1,3-Dichloropropene "ND 0.25 Ethylbenzene "ND 0.25 Hexachlorobutadiene "ND 0.25 4-Isopropyl Toluene "ND 0.25 Isopropylbenzene "ND 0.25 Methylene chloride "ND 0.25 Naphthalene "ND 0.25 n-Propylbenzene "ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 25 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Blank (B1E0101-BLK1)Analyzed: 05/05/21 13:17 Styrene mg/kgND0.25 1,1,1,2-Tetrachloroethane "ND 0.25 1,1,2,2-Tetrachloroethane "ND 0.25 Tetrachloroethene (PCE)"ND 0.25 Toluene "ND 0.25 1,2,3-Trichlorobenzene "ND 0.25 1,2,4-Trichlorobenzene "ND 0.25 1,1,1-Trichloroethane "ND 0.25 1,1,2-Trichloroethane "ND 0.25 Trichloroethene (TCE)"ND 0.25 Trichlorofluoromethane "ND 0.25 1,2,3-Trichloropropane "ND 0.25 1,2,4-Trimethylbenzene "ND 0.25 1,3,5-Trimethylbenzene "ND 0.25 Vinyl chloride "ND 0.25 Xylenes (total)"ND 0.25 "0.0496 74-122Surrogate: Dibromofluoromethane 940.0468 "0.0496 65-128Surrogate: Toluene-d8 930.0462 "0.0496 75-121Surrogate: 4-Bromofluorobenzene 870.0431 LCS (B1E0101-BS1) [TOC_3]LCS (B1E0101-BS1)[TOC] Analyzed: 05/05/21 12:22 Benzene mg/kg2.30 0.25 1.99 70-131116 Bromobenzene "1.97 0.25 1.99 74-13099 Bromochloromethane "1.85 0.25 1.99 64-13393 Bromodichloromethane "1.99 0.25 1.99 69-137100 Bromoform "1.74 0.25 1.99 55-13288 Bromomethane "1.64 0.25 1.99 10-14283 n-Butylbenzene "2.58 0.25 1.99 64-156130 sec-Butylbenzene "2.53 0.25 1.99 75-155127 tert-Butylbenzene "2.32 0.25 1.99 74-144117 Carbon tetrachloride "2.18 0.25 1.99 67-135110 Chlorobenzene "2.17 0.25 1.99 73-134109 Chloroethane "1.83 0.25 1.99 10-16792 Chloroform "2.13 0.25 1.99 69-124107 Chloromethane "2.32 0.25 1.99 34-136117 2-Chlorotoluene "2.14 0.25 1.99 75-135107 4-Chlorotoluene "2.14 0.25 1.99 70-138108 Dibromochloromethane "1.99 0.25 1.99 67-135100 1,2-Dibromo-3-chloropropane "1.99 0.25 1.99 41-149100 1,2-Dibromoethane (EDB)"1.92 0.25 1.99 68-13197 Dibromomethane "1.48 0.25 1.99 61-14074 1,2-Dichlorobenzene "2.07 0.25 1.99 76-136104 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 26 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS (B1E0101-BS1)Analyzed: 05/05/21 12:22 1,3-Dichlorobenzene mg/kg2.17 0.25 1.99 76-138109 1,4-Dichlorobenzene "2.14 0.25 1.99 72-132108 Dichlorodifluoromethane "1.31 0.25 1.99 10-15566 1,1-Dichloroethane "2.33 0.25 1.99 63-139117 1,2-Dichloroethane "2.06 0.25 1.99 64-126104 1,1-Dichloroethene "2.77 0.25 1.99 52-167139 cis-1,2-Dichloroethene "2.07 0.25 1.99 70-135104 trans-1,2-Dichloroethene "2.43 0.25 1.99 67-147122 1,2-Dichloropropane "2.05 0.25 1.99 68-131103 1,3-Dichloropropane "2.04 0.25 1.99 64-128103 2,2-Dichloropropane "2.31 0.25 1.99 63-154116 1,1-Dichloropropene "2.22 0.25 1.99 68-138112 cis-1,3-Dichloropropene "2.09 0.25 1.99 72-134105 trans-1,3-Dichloropropene "2.26 0.25 1.99 69-132114 Ethylbenzene "2.46 0.25 1.99 68-136124 Hexachlorobutadiene "2.20 0.25 1.99 72-198111 4-Isopropyl Toluene "2.39 0.25 1.99 74-150120 Isopropylbenzene "2.41 0.25 1.99 71-149121 Methylene chloride "2.57 0.25 1.99 QM-0851-127129 Naphthalene "1.99 0.25 1.99 57-158100 n-Propylbenzene "2.27 0.25 1.99 70-143114 Styrene "2.25 0.25 1.99 68-138113 1,1,1,2-Tetrachloroethane "1.92 0.25 1.99 76-13097 1,1,2,2-Tetrachloroethane "2.09 0.25 1.99 60-136105 Tetrachloroethene (PCE)"2.09 0.25 1.99 73-138105 Toluene "2.18 0.25 1.99 72-128110 1,2,3-Trichlorobenzene "1.74 0.25 1.99 61-16688 1,2,4-Trichlorobenzene "1.85 0.25 1.99 71-15893 1,1,1-Trichloroethane "2.24 0.25 1.99 71-135113 1,1,2-Trichloroethane "2.07 0.25 1.99 64-132104 Trichloroethene (TCE)"1.92 0.25 1.99 74-13997 Trichlorofluoromethane "1.74 0.25 1.99 30-15687 1,2,3-Trichloropropane "2.01 0.25 1.99 67-123101 1,2,4-Trimethylbenzene "2.52 0.25 1.99 68-134127 1,3,5-Trimethylbenzene "2.37 0.25 1.99 71-140119 Vinyl chloride "2.46 0.25 1.99 43-144124 Xylenes (total)"7.54 0.25 5.96 69-138126 "0.0497 74-122Surrogate: Dibromofluoromethane 980.0485 "0.0497 65-128Surrogate: Toluene-d8 950.0471 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 940.0467 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 27 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSD1) [TOC_3]LCS Dup (B1E0101-BSD1)[TOC] Analyzed: 05/05/21 12:49 Benzene mg/kg2.25 0.25 1.99 2070-131113 2 Bromobenzene "1.93 0.25 1.99 2074-13097 2 Bromochloromethane "1.85 0.25 1.99 2064-13393 0 Bromodichloromethane "2.00 0.25 1.99 2069-137101 0.5 Bromoform "1.81 0.25 1.99 2055-13291 3 Bromomethane "1.48 0.25 1.99 2010-14275 10 n-Butylbenzene "2.57 0.25 1.99 2064-156129 0.2 sec-Butylbenzene "2.51 0.25 1.99 2075-155126 0.8 tert-Butylbenzene "2.34 0.25 1.99 2074-144118 1 Carbon tetrachloride "2.12 0.25 1.99 2067-135107 3 Chlorobenzene "2.20 0.25 1.99 2073-134110 1 Chloroethane "1.75 0.25 1.99 2010-16788 4 Chloroform "2.10 0.25 1.99 2069-124106 1 Chloromethane "2.15 0.25 1.99 2034-136108 8 2-Chlorotoluene "2.15 0.25 1.99 2075-135108 0.6 4-Chlorotoluene "2.15 0.25 1.99 2070-138108 0.5 Dibromochloromethane "1.94 0.25 1.99 2067-13598 2 1,2-Dibromo-3-chloropropane "1.89 0.25 1.99 2041-14995 5 1,2-Dibromoethane (EDB)"1.96 0.25 1.99 2068-13199 2 Dibromomethane "1.52 0.25 1.99 2061-14076 3 1,2-Dichlorobenzene "2.12 0.25 1.99 2076-136107 2 1,3-Dichlorobenzene "2.17 0.25 1.99 2076-138109 0 1,4-Dichlorobenzene "2.21 0.25 1.99 2072-132111 3 Dichlorodifluoromethane "1.31 0.25 1.99 2010-15566 0.2 1,1-Dichloroethane "2.30 0.25 1.99 2063-139116 1 1,2-Dichloroethane "2.09 0.25 1.99 2064-126105 2 1,1-Dichloroethene "2.55 0.25 1.99 2052-167128 8 cis-1,2-Dichloroethene "2.01 0.25 1.99 2070-135101 3 trans-1,2-Dichloroethene "2.37 0.25 1.99 2067-147119 2 1,2-Dichloropropane "2.07 0.25 1.99 2068-131104 0.8 1,3-Dichloropropane "2.02 0.25 1.99 2064-128102 1 2,2-Dichloropropane "2.25 0.25 1.99 2063-154113 3 1,1-Dichloropropene "2.20 0.25 1.99 2068-138111 1 cis-1,3-Dichloropropene "2.06 0.25 1.99 2072-134103 2 trans-1,3-Dichloropropene "2.25 0.25 1.99 2069-132113 0.8 Ethylbenzene "2.47 0.25 1.99 2068-136124 0.2 Hexachlorobutadiene "2.25 0.25 1.99 2072-198113 2 4-Isopropyl Toluene "2.42 0.25 1.99 2074-150122 1 Isopropylbenzene "2.36 0.25 1.99 2071-149119 2 Methylene chloride "2.45 0.25 1.99 2051-127123 5 Naphthalene "2.00 0.25 1.99 2057-158101 0.9 n-Propylbenzene "2.29 0.25 1.99 2070-143115 0.9 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 28 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 28 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 LCS Dup (B1E0101-BSD1)Analyzed: 05/05/21 12:49 Styrene mg/kg2.26 0.25 1.99 2068-138114 0.4 1,1,1,2-Tetrachloroethane "1.96 0.25 1.99 2076-13099 2 1,1,2,2-Tetrachloroethane "2.08 0.25 1.99 2060-136105 0.2 Tetrachloroethene (PCE)"2.07 0.25 1.99 2073-138104 1 Toluene "2.21 0.25 1.99 2072-128111 1 1,2,3-Trichlorobenzene "1.87 0.25 1.99 2061-16694 7 1,2,4-Trichlorobenzene "1.89 0.25 1.99 2071-15895 2 1,1,1-Trichloroethane "2.17 0.25 1.99 2071-135109 3 1,1,2-Trichloroethane "2.16 0.25 1.99 2064-132108 4 Trichloroethene (TCE)"1.89 0.25 1.99 2074-13995 1 Trichlorofluoromethane "1.58 0.25 1.99 2030-15679 10 1,2,3-Trichloropropane "1.90 0.25 1.99 2067-12395 6 1,2,4-Trimethylbenzene "2.60 0.25 1.99 2068-134131 3 1,3,5-Trimethylbenzene "2.38 0.25 1.99 2071-140120 0.6 Vinyl chloride "2.27 0.25 1.99 2043-144114 8 Xylenes (total)"7.47 0.25 5.96 2069-138125 0.9 "0.0497 74-122Surrogate: Dibromofluoromethane 980.0486 "0.0497 65-128Surrogate: Toluene-d8 940.0467 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 920.0459 Duplicate (B1E0101-DUP1)Source: 2102742-01RE1 [TOC_3]Duplicate (B1E0101-DUP1)[TOC] Analyzed: 05/05/21 15:07 Benzene mg/kgND1.3 ND 20 Bromobenzene "ND 1.3 ND 20 Bromochloromethane "ND 1.3 ND 20 Bromodichloromethane "ND 1.3 ND 20 Bromoform "ND 1.3 ND 20 Bromomethane "ND 1.3 ND 20 n-Butylbenzene "ND 1.3 ND 20 sec-Butylbenzene "ND 1.3 ND 20 tert-Butylbenzene "ND 1.3 ND 20 Carbon tetrachloride "ND 1.3 ND 20 Chlorobenzene "ND 1.3 ND 20 Chloroethane "ND 1.3 ND 20 Chloroform "ND 1.3 ND 20 Chloromethane "ND 1.3 ND 20 2-Chlorotoluene "ND 1.3 ND 20 4-Chlorotoluene "ND 1.3 ND 20 Dibromochloromethane "ND 1.3 ND 20 1,2-Dibromo-3-chloropropane "ND 1.3 ND 20 1,2-Dibromoethane (EDB)"ND 1.3 ND 20 Dibromomethane "ND 1.3 ND 20 1,2-Dichlorobenzene "ND 1.3 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 29 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 29 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Duplicate (B1E0101-DUP1)Source: 2102742-01RE1 Analyzed: 05/05/21 15:07 1,3-Dichlorobenzene mg/kgND1.3 ND 20 1,4-Dichlorobenzene "ND 1.3 ND 20 Dichlorodifluoromethane "ND 1.3 ND 20 1,1-Dichloroethane "ND 1.3 ND 20 1,2-Dichloroethane "ND 1.3 ND 20 1,1-Dichloroethene "ND 1.3 ND 20 cis-1,2-Dichloroethene "ND 1.3 ND 20 trans-1,2-Dichloroethene "ND 1.3 ND 20 1,2-Dichloropropane "ND 1.3 ND 20 1,3-Dichloropropane "ND 1.3 ND 20 2,2-Dichloropropane "ND 1.3 ND 20 1,1-Dichloropropene "ND 1.3 ND 20 cis-1,3-Dichloropropene "ND 1.3 ND 20 trans-1,3-Dichloropropene "ND 1.3 ND 20 Ethylbenzene "ND 1.3 ND 20 Hexachlorobutadiene "ND 1.3 ND 20 4-Isopropyl Toluene "ND 1.3 ND 20 Isopropylbenzene "ND 1.3 ND 20 Methylene chloride "ND 1.3 ND 20 Naphthalene "ND 1.3 ND 20 n-Propylbenzene "ND 1.3 ND 20 Styrene "ND 1.3 ND 20 1,1,1,2-Tetrachloroethane "ND 1.3 ND 20 1,1,2,2-Tetrachloroethane "ND 1.3 ND 20 Tetrachloroethene (PCE)"ND 1.3 ND 20 Toluene "0.572 1.3 ND 20 A-01 1,2,3-Trichlorobenzene "ND 1.3 ND 20 1,2,4-Trichlorobenzene "ND 1.3 ND 20 1,1,1-Trichloroethane "ND 1.3 ND 20 1,1,2-Trichloroethane "ND 1.3 ND 20 Trichloroethene (TCE)"ND 1.3 ND 20 Trichlorofluoromethane "ND 1.3 ND 20 1,2,3-Trichloropropane "ND 1.3 ND 20 1,2,4-Trimethylbenzene "ND 1.3 ND 20 1,3,5-Trimethylbenzene "ND 1.3 ND 20 Vinyl chloride "ND 1.3 ND 20 Xylenes (total)"ND 1.3 ND 20 "0.0502 74-122Surrogate: Dibromofluoromethane 930.0467 "0.0502 65-128Surrogate: Toluene-d8 950.0475 "0.0502 75-121Surrogate: 4-Bromofluorobenzene 880.0442 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 30 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1)Source: 2102742-02 [TOC_3]Matrix Spike (B1E0101-MS1)[TOC] Analyzed: 05/05/21 20:08 Benzene mg/kg11.1 1.3 10.0 ND 37-145111 Bromobenzene "9.57 1.3 10.0 ND 29-14796 Bromochloromethane "9.29 1.3 10.0 ND 40-14593 Bromodichloromethane "10.2 1.3 10.0 ND 39-153102 Bromoform "9.14 1.3 10.0 ND 32-14391 Bromomethane "12.1 1.3 10.0 ND 10-141121 n-Butylbenzene "12.3 1.3 10.0 ND 10-162123 sec-Butylbenzene "12.5 1.3 10.0 ND 14-168125 tert-Butylbenzene "11.8 1.3 10.0 ND 21-159118 Carbon tetrachloride "10.4 1.3 10.0 ND 28-148104 Chlorobenzene "10.6 1.3 10.0 ND 32-148106 Chloroethane "11.0 1.3 10.0 ND 11-166110 Chloroform "10.3 1.3 10.0 ND 40-139103 Chloromethane "9.86 1.3 10.0 ND 18-13598 2-Chlorotoluene "10.7 1.3 10.0 ND 25-151107 4-Chlorotoluene "10.7 1.3 10.0 ND 22-150106 Dibromochloromethane "9.53 1.3 10.0 ND 40-14795 1,2-Dibromo-3-chloropropane "9.97 1.3 10.0 ND 25-158100 1,2-Dibromoethane (EDB)"9.29 1.3 10.0 ND 38-14793 Dibromomethane "7.54 1.3 10.0 ND 39-15075 1,2-Dichlorobenzene "10.6 1.3 10.0 ND 24-154106 1,3-Dichlorobenzene "10.9 1.3 10.0 ND 21-153108 1,4-Dichlorobenzene "10.6 1.3 10.0 ND 21-146106 Dichlorodifluoromethane "5.88 1.3 10.0 ND 10-14959 1,1-Dichloroethane "11.2 1.3 10.0 ND 34-151112 1,2-Dichloroethane "10.1 1.3 10.0 ND 40-137100 1,1-Dichloroethene "11.8 1.3 10.0 ND 21-172118 cis-1,2-Dichloroethene "9.65 1.3 10.0 ND 38-14796 trans-1,2-Dichloroethene "11.3 1.3 10.0 ND 30-160112 1,2-Dichloropropane "10.4 1.3 10.0 ND 39-146104 1,3-Dichloropropane "10.2 1.3 10.0 ND 39-141102 2,2-Dichloropropane "9.32 1.3 10.0 ND 26-14993 1,1-Dichloropropene "10.7 1.3 10.0 ND 28-150106 cis-1,3-Dichloropropene "9.97 1.3 10.0 ND 34-149100 trans-1,3-Dichloropropene "10.7 1.3 10.0 ND 36-143107 Ethylbenzene "11.5 1.3 10.0 ND 23-150115 Hexachlorobutadiene "11.1 1.3 10.0 ND 10-192111 4-Isopropyl Toluene "11.7 1.3 10.0 ND 11-165117 Isopropylbenzene "11.2 1.3 10.0 ND 17-166112 Methylene chloride "12.0 1.3 10.0 ND 28-135120 Naphthalene "12.0 1.3 10.0 ND 10-174120 n-Propylbenzene "11.3 1.3 10.0 ND 16-156113 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 31 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0101 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/05/21 09:05 Matrix Spike (B1E0101-MS1)Source: 2102742-02 Analyzed: 05/05/21 20:08 Styrene mg/kg10.8 1.3 10.0 ND 24-154108 1,1,1,2-Tetrachloroethane "9.48 1.3 10.0 ND 38-14995 1,1,2,2-Tetrachloroethane "11.0 1.3 10.0 ND 22-164110 Tetrachloroethene (PCE)"9.82 1.3 10.0 ND 25-15398 Toluene "10.7 1.3 10.0 ND 26-149107 1,2,3-Trichlorobenzene "10.2 1.3 10.0 ND 10-163101 1,2,4-Trichlorobenzene "9.87 1.3 10.0 ND 10-16299 1,1,1-Trichloroethane "10.6 1.3 10.0 ND 34-149106 1,1,2-Trichloroethane "9.74 1.3 10.0 ND 25-17597 Trichloroethene (TCE)"9.32 1.3 10.0 ND 25-17093 Trichlorofluoromethane "10.8 1.3 10.0 ND 19-155107 1,2,3-Trichloropropane "10.3 1.3 10.0 ND 32-165103 1,2,4-Trimethylbenzene "12.6 1.3 10.0 ND 15-150126 1,3,5-Trimethylbenzene "11.7 1.3 10.0 ND 10-158117 Vinyl chloride "10.9 1.3 10.0 ND 22-148108 Xylenes (total)"35.6 1.3 30.1 ND 22-153118 "0.0501 74-122Surrogate: Dibromofluoromethane 940.0473 "0.0501 65-128Surrogate: Toluene-d8 940.0469 "0.0501 75-121Surrogate: 4-Bromofluorobenzene 900.0453 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 32 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid Total Metals by CVAA EPA 7471A OEC, CA-ELAPMercury Total EPA 7471A Solid Total Metals by ICP EPA 6010B OEC, CA-ELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP8260B Full List Solid Volatile Organic TPH by GC/FID EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 33 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 33 of 37 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 Natural Healing Center Clarence Reynolds Pacific Petroleum 05/06/2021 17:25Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2102742 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL A-01 Potential carryover from previous high leveled sample. D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. QM-08 The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out-Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 34 of 36 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 34 of 37 File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0511.D Operator : BNT Acquired : 5 May 2021 12:06 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-01@ Misc Info : 1@B1E0095 GRO SO Vial Number: 11 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME0511.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0512.D Operator : BNT Acquired : 5 May 2021 12:32 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-02@ Misc Info : 1@B1E0095 GRO SO Vial Number: 12 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOME0512.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0513.D Operator : BNT Acquired : 5 May 2021 12:58 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-03@ Misc Info : 1@B1E0095 GRO SO Vial Number: 13 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 Time Response_GOME0513.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0514.D Operator : BNT Acquired : 5 May 2021 1:24 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-04@ Misc Info : 1@B1E0095 GRO SO Vial Number: 14 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 Time Response_GOME0514.D\FID1A File : C:\HPCHEM\1\DATA\2021\MAY21\050521\GOME0515.D Operator : BNT Acquired : 5 May 2021 1:49 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2102742-05@ Misc Info : 1@B1E0095 GRO SO Vial Number: 15 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME0515.D\FID1A File : X:\MAY21\050521\B0ME0526.DOperator : RWSAcquired : 5-5-2021 07:52:41 PM using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-01@B1E0062 Misc Info : 1@ Vial Number: 262.00 2.10 2.20 2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20 4.30 4.40 4.50 4.60 4.70 4.80100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07 1.8e+07 1.9e+07 2e+07TimeResponse_Signal: B0ME0526.D\FID1A.CH File : X:\MAY21\050521\B0ME0534.DOperator : RWSAcquired : 5-5-2021 09:27:30 PM using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-02@B1E0062 Misc Info : 1@ Vial Number: 342.10 2.20 2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20 4.30 4.40 4.50 4.60 4.70 4.80 4.90 5.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME0534.D\FID1A.CH File : X:\MAY21\050521\B0ME0536.DOperator : RWSAcquired : 5-5-2021 09:51:16 PM using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-03@B1E0062 Misc Info : 1@ Vial Number: 361.80 2.00 2.20 2.40 2.60 2.80 3.00 3.20 3.40 3.60 3.80 4.00 4.20 4.40 4.60 4.80 5.00 5.20 5.40 5.60100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME0536.D\FID1A.CH File : X:\MAY21\050521\B0ME0538.DOperator : RWSAcquired : 05 May 2021 10:15 pm using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-04@B1E0062 Misc Info : 1@ Vial Number: 381.80 2.00 2.20 2.40 2.60 2.80 3.00 3.20 3.40 3.60 3.80 4.00 4.20 4.40 4.60 4.80 5.00 5.20 5.40 5.60 5.80 6.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME0538.D\FID1A.CH File : X:\MAY21\050521\B0ME0540.DOperator : RWSAcquired : 05 May 2021 10:38 pm using AcqMethod TPH01C1.MInstrument : GC15 Sample Name: 2102742-05@B1E0062 Misc Info : 1@ Vial Number: 402.10 2.20 2.30 2.40 2.50 2.60 2.70 2.80 2.90 3.00 3.10 3.20 3.30 3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20 4.30 4.40 4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME0540.D\FID1A.CH Page 35 of 37 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLD92$elueluieiheluekuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 36 of 37 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)ULGJH6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)ULGJH6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)ULGJH6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)ULGJH6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)ULGJH6ROLG5HFHLSW/RJLQ%\/:&5HFHLSW5HYLHZHG%\-9=Page 37 of 37 [TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2103212 Report Date: June 01, 2021 10:29 NHC SLO, 2640 Broad StreetNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on May 24, 2021 13:05 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com California ELAP Certification # 2438 client.oec.com\reportsClient Connect: Page 1 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix Bottom West Center 2103212-01 05/24/2021 11:20 05/24/2021 13:05Solid Solid Bottom East Center 2103212-02 05/24/2021 11:25 05/24/2021 13:05Solid Solid Bin 20339-A 2103212-03 05/24/2021 11:30 05/24/2021 13:05Solid Solid Bin 20339-B 2103212-04 05/24/2021 11:35 05/24/2021 13:05Solid Solid Bin 20339-C 2103212-05 05/24/2021 11:40 05/24/2021 13:05Solid Solid Bin 20144-A 2103212-06 05/24/2021 11:45 05/24/2021 13:05Solid Solid Bin 20144-B 2103212-07 05/24/2021 11:50 05/24/2021 13:05Solid Solid Bin 20144-C 2103212-08 05/24/2021 11:55 05/24/2021 13:05Solid Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 2 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 05/25/2021 08:55B1E0696 STLC Metals by ICP 6010B STLC 05/28/2021 09:36B1E0829 STLC Metals Extraction STLC Metals Extraction 05/26/2021 08:58B1E0743 TCLP Metals by ICP 6010B TCLP 05/27/2021 10:55B1E0794 TCLP Metals Extraction TCLP Metals Extraction 05/26/2021 09:03B1E0744 Total Metals by CVAA Mercury Total EPA 7471A 05/25/2021 07:50B1E0694 Total Metals by ICP 6010B Total 05/25/2021 07:26B1E0693 Volatile Organic Compounds by GC/MS 8260B Full List 05/25/2021 09:00B1E0697 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 05/26/2021 06:59B1E0737 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 3 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.22 B1E0694 05/25/21 14:04mg/kg 1Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:18mg/kg B1E06931Antimony2.4 "7.0 """"Arsenic 1.9 "560 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "120 """"Chromium 0.48 N-02, N-03 "21 """"Cobalt 0.48 "43 """"Copper 0.96 "7.3 """"Lead 0.48 "0.62 """"Molybdenum 0.48 "160 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "46 """"Vanadium 1.9 "56 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B05/28/21 13:17mg/L B1E08292Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:15mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 4 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M05/26/21 13:56mg/kg B1E07371TPH Gasoline (C5-C12)0.50 """( 39 - 157 )101 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M51B1E069605/25/21 14:26mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )90 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 5 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 15:16mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 6 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom West Center Sampled : 05/24/21 11:20 Lab ID : 2103212-01 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 15:16mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )101 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )97 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 7 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:06mg/kg B1E06941Mercury0.095 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:21mg/kg B1E06931Antimony2.4 "6.6 """"Arsenic 1.9 "220 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "120 """"Chromium 0.48 N-02, N-03 "19 """"Cobalt 0.48 "39 """"Copper 0.96 "8.3 """"Lead 0.48 ND """ ""Molybdenum 0.48 "150 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "51 """"Vanadium 1.9 "62 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B05/28/21 13:24mg/L B1E08292Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:17mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 8 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.2 B1E0737 05/26/21 15:34mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )118 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M330B1E069605/25/21 14:03mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )108 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 9 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 15:43mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 10 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bottom East Center Sampled : 05/24/21 11:25 Lab ID : 2103212-02 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 15:43mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )101 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )96 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 11 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-03 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:08mg/kg B1E06941Mercury0.099 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:24mg/kg B1E06931Antimony2.5 "5.1 """"Arsenic 2.0 "230 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "160 """"Chromium 0.49 N-02, N-03 "21 """"Cobalt 0.49 "47 """"Copper 0.98 "11 """"Lead 0.49 "0.74 """"Molybdenum 0.49 "190 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "62 """"Vanadium 2.0 "72 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B05/28/21 13:34mg/L B1E08292Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:20mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 12 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M4.2 B1E0737 05/26/21 16:26mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )118 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M350B1E069605/25/21 15:12mg/kg 1TPH Diesel (C13-C22)10 "55 """"TPH Motor Oil (C23-C40)50 """( 65 - 136 )112 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 13 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 16:11mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 14 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-A Sampled : 05/24/21 11:30 Lab ID : 2103212-03 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 16:11mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )102 %Surrogate: Dibromofluoromethane """( 65 - 128 )103 %Surrogate: Toluene-d8 """( 75 - 121 )97 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 15 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-04 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:10mg/kg B1E06941Mercury0.090 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:26mg/kg B1E06931Antimony2.4 "10 """"Arsenic 1.9 "290 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "710 """"Chromium 0.48 N-02, N-03 "47 """"Cobalt 0.48 "52 """"Copper 0.96 "13 """"Lead 0.48 "1.2 """"Molybdenum 0.48 "1900 """"Nickel 0.48 N-02 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "77 """"Vanadium 1.9 "83 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.11 B1E0829 05/28/21 13:37mg/L 2Chromium0.10 "0.37 """"Nickel 0.10 B-02 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:23mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 16 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M0.76 B1E0737 05/26/21 17:18mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )101 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M71B1E069605/25/21 13:41mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )106 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 17 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 16:38mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 18 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-B Sampled : 05/24/21 11:35 Lab ID : 2103212-04 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 16:38mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )100 %Surrogate: Dibromofluoromethane """( 65 - 128 )101 %Surrogate: Toluene-d8 """( 75 - 121 )97 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 19 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-05 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A1.4 B1E0694 05/25/21 14:12mg/kg 1Mercury0.092 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:13mg/kg B1E06931Antimony2.5 "6.1 """"Arsenic 2.0 "220 """"Barium 1.0 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "140 """"Chromium 0.50 N-02, N-03 "21 """"Cobalt 0.50 "46 """"Copper 1.0 "19 """"Lead 0.50 "0.57 """"Molybdenum 0.50 "180 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 1.0 "54 """"Vanadium 2.0 "87 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.18 B1E0829 05/28/21 13:39mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:25mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 20 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.3 B1E0737 05/26/21 19:53mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )107 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M390B1E069605/25/21 14:49mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )105 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 21 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 17:05mg/kg B1E06971000Benzene1.3 ND """ ""Bromobenzene 1.3 ND """ ""Bromochloromethane 1.3 ND """ ""Bromodichloromethane 1.3 ND """ ""Bromoform 1.3 ND """ ""Bromomethane 1.3 ND """ ""n-Butylbenzene 1.3 ND """ ""sec-Butylbenzene 1.3 ND """ ""tert-Butylbenzene 1.3 ND """ ""Carbon tetrachloride 1.3 ND """ ""Chlorobenzene 1.3 ND """ ""Chloroethane 1.3 ND """ ""Chloroform 1.3 ND """ ""Chloromethane 1.3 ND """ ""2-Chlorotoluene 1.3 ND """ ""4-Chlorotoluene 1.3 ND """ ""Dibromochloromethane 1.3 ND """ ""1,2-Dibromo-3-chloropropane 1.3 ND """ ""1,2-Dibromoethane (EDB)1.3 ND """ ""Dibromomethane 1.3 ND """ ""1,2-Dichlorobenzene 1.3 ND """ ""1,3-Dichlorobenzene 1.3 ND """ ""1,4-Dichlorobenzene 1.3 ND """ ""Dichlorodifluoromethane 1.3 ND """ ""1,1-Dichloroethane 1.3 ND """ ""1,2-Dichloroethane 1.3 ND """ ""1,1-Dichloroethene 1.3 ND """ ""cis-1,2-Dichloroethene 1.3 ND """ ""trans-1,2-Dichloroethene 1.3 ND """ ""1,2-Dichloropropane 1.3 ND """ ""1,3-Dichloropropane 1.3 ND """ ""2,2-Dichloropropane 1.3 ND """ ""1,1-Dichloropropene 1.3 ND """ ""cis-1,3-Dichloropropene 1.3 ND """ ""trans-1,3-Dichloropropene 1.3 ND """ ""Ethylbenzene 1.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 22 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20339-C Sampled : 05/24/21 11:40 Lab ID : 2103212-05 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 17:05mg/kg B1E06971000Hexachlorobutadiene1.3 ND """ ""4-Isopropyl Toluene 1.3 ND """ ""Isopropylbenzene 1.3 ND """ ""Methylene chloride 1.3 ND """ ""Naphthalene 1.3 ND """ ""n-Propylbenzene 1.3 ND """ ""Styrene 1.3 ND """ ""1,1,1,2-Tetrachloroethane 1.3 ND """ ""1,1,2,2-Tetrachloroethane 1.3 ND """ ""Tetrachloroethene (PCE)1.3 ND """ ""Toluene 1.3 ND """ ""1,2,3-Trichlorobenzene 1.3 ND """ ""1,2,4-Trichlorobenzene 1.3 ND """ ""1,1,1-Trichloroethane 1.3 ND """ ""1,1,2-Trichloroethane 1.3 ND """ ""Trichloroethene (TCE)1.3 ND """ ""Trichlorofluoromethane 1.3 ND """ ""1,2,3-Trichloropropane 1.3 ND """ ""1,2,4-Trimethylbenzene 1.3 ND """ ""1,3,5-Trimethylbenzene 1.3 ND """ ""Vinyl chloride 1.3 ND """ ""Xylenes (total)1.3 """( 74 - 122 )102 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )98 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 23 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-06 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.23 B1E0694 05/25/21 14:14mg/kg 1Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:37mg/kg B1E06931Antimony2.5 "4.9 """"Arsenic 2.0 "230 """"Barium 0.99 ND """ ""Beryllium 0.50 ND """ ""Cadmium 0.25 "150 """"Chromium 0.50 N-02, N-03 "25 """"Cobalt 0.50 "49 """"Copper 0.99 "41 """"Lead 0.50 "0.69 """"Molybdenum 0.50 "190 """"Nickel 0.50 ND """ ""Selenium 2.0 ND """ ""Silver 0.50 ND """ ""Thallium 0.99 "60 """"Vanadium 2.0 "82 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.15 B1E0829 05/28/21 13:42mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:28mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 24 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M1.5 B1E0737 05/26/21 20:45mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )115 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M370B1E069605/25/21 14:49mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )102 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 25 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 17:33mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 26 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-A Sampled : 05/24/21 11:45 Lab ID : 2103212-06 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 17:33mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 "2.8 """"Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )99 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )96 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 27 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-07 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA EPA 7471A0.19 B1E0694 05/25/21 14:16mg/kg 1Mercury0.093 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:40mg/kg B1E06931Antimony2.5 "4.6 """"Arsenic 2.0 "180 """"Barium 0.99 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "150 """"Chromium 0.49 N-02, N-03 "19 """"Cobalt 0.49 "40 """"Copper 0.99 "24 """"Lead 0.49 ND """ ""Molybdenum 0.49 "150 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.99 "50 """"Vanadium 2.0 "77 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.19 B1E0829 05/28/21 13:45mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:30mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 28 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 28 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.2 B1E0737 05/26/21 21:36mg/kg 1TPH Gasoline (C5-C12)0.50 D-04 """( 39 - 157 )108 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M320B1E069605/25/21 15:12mg/kg 1TPH Diesel (C13-C22)9.9 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )95 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 29 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 29 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 18:00mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 30 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 30 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-B Sampled : 05/24/21 11:50 Lab ID : 2103212-07 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 18:00mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 "2.3 """"Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )100 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )98 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 31 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 31 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA [TOC_1]2103212-08 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A05/25/21 14:18mg/kg B1E06941Mercury0.098 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B05/25/21 14:42mg/kg B1E06931Antimony2.5 "5.0 """"Arsenic 2.0 "140 """"Barium 0.98 ND """ ""Beryllium 0.49 ND """ ""Cadmium 0.25 "160 """"Chromium 0.49 N-02, N-03 "23 """"Cobalt 0.49 "45 """"Copper 0.98 "14 """"Lead 0.49 ND """ ""Molybdenum 0.49 "190 """"Nickel 0.49 ND """ ""Selenium 2.0 ND """ ""Silver 0.49 ND """ ""Thallium 0.98 "50 """"Vanadium 2.0 "71 """"Zinc 2.0 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP STLC/EPA 6010B0.17 B1E0829 05/28/21 13:47mg/L 2Chromium0.10 [TOC_2]TCLP Metals by ICP[TOC] TCLP Metals by ICP ND EPA 1311/EPA 6010B05/27/21 19:40mg/L B1E07941Chromium0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 32 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 32 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID EPA 8015M2.1 B1E0737 05/26/21 22:28mg/kg 1TPH Gasoline (C5-C12)0.49 D-04 """( 39 - 157 )119 %Surrogate: 4-Bromofluorobenzene [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID EPA 8015M560B1E069605/25/21 14:26mg/kg 1TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )120 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 33 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 33 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B05/25/21 18:28mg/kg B1E06971000Benzene1.2 ND """ ""Bromobenzene 1.2 ND """ ""Bromochloromethane 1.2 ND """ ""Bromodichloromethane 1.2 ND """ ""Bromoform 1.2 ND """ ""Bromomethane 1.2 ND """ ""n-Butylbenzene 1.2 ND """ ""sec-Butylbenzene 1.2 ND """ ""tert-Butylbenzene 1.2 ND """ ""Carbon tetrachloride 1.2 ND """ ""Chlorobenzene 1.2 ND """ ""Chloroethane 1.2 ND """ ""Chloroform 1.2 ND """ ""Chloromethane 1.2 ND """ ""2-Chlorotoluene 1.2 ND """ ""4-Chlorotoluene 1.2 ND """ ""Dibromochloromethane 1.2 ND """ ""1,2-Dibromo-3-chloropropane 1.2 ND """ ""1,2-Dibromoethane (EDB)1.2 ND """ ""Dibromomethane 1.2 ND """ ""1,2-Dichlorobenzene 1.2 ND """ ""1,3-Dichlorobenzene 1.2 ND """ ""1,4-Dichlorobenzene 1.2 ND """ ""Dichlorodifluoromethane 1.2 ND """ ""1,1-Dichloroethane 1.2 ND """ ""1,2-Dichloroethane 1.2 ND """ ""1,1-Dichloroethene 1.2 ND """ ""cis-1,2-Dichloroethene 1.2 ND """ ""trans-1,2-Dichloroethene 1.2 ND """ ""1,2-Dichloropropane 1.2 ND """ ""1,3-Dichloropropane 1.2 ND """ ""2,2-Dichloropropane 1.2 ND """ ""1,1-Dichloropropene 1.2 ND """ ""cis-1,3-Dichloropropene 1.2 ND """ ""trans-1,3-Dichloropropene 1.2 ND """ ""Ethylbenzene 1.2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 34 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 34 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Analytical Report for Samples Bin 20144-C Sampled : 05/24/21 11:55 Lab ID : 2103212-08 Matrix : Solid Sample ID : Sampled by : Clarence Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B05/25/21 18:28mg/kg B1E06971000Hexachlorobutadiene1.2 ND """ ""4-Isopropyl Toluene 1.2 ND """ ""Isopropylbenzene 1.2 ND """ ""Methylene chloride 1.2 ND """ ""Naphthalene 1.2 ND """ ""n-Propylbenzene 1.2 ND """ ""Styrene 1.2 ND """ ""1,1,1,2-Tetrachloroethane 1.2 ND """ ""1,1,2,2-Tetrachloroethane 1.2 ND """ ""Tetrachloroethene (PCE)1.2 ND """ ""Toluene 1.2 ND """ ""1,2,3-Trichlorobenzene 1.2 ND """ ""1,2,4-Trichlorobenzene 1.2 ND """ ""1,1,1-Trichloroethane 1.2 ND """ ""1,1,2-Trichloroethane 1.2 ND """ ""Trichloroethene (TCE)1.2 ND """ ""Trichlorofluoromethane 1.2 ND """ ""1,2,3-Trichloropropane 1.2 ND """ ""1,2,4-Trimethylbenzene 1.2 ND """ ""1,3,5-Trimethylbenzene 1.2 ND """ ""Vinyl chloride 1.2 ND """ ""Xylenes (total)1.2 """( 74 - 122 )99 %Surrogate: Dibromofluoromethane """( 65 - 128 )101 %Surrogate: Toluene-d8 """( 75 - 121 )96 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 35 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 35 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0694 - EPA 7471A Prep[TOC] Batch B1E0694 - EPA 7471A Preparation: EPA 7471A Prep 05/25/21 07:50 Blank (B1E0694-BLK1) [TOC_3]Blank (B1E0694-BLK1)[TOC] Analyzed: 05/25/21 13:31 Mercury mg/kgND0.10 LCS (B1E0694-BS1) [TOC_3]LCS (B1E0694-BS1)[TOC] Analyzed: 05/25/21 13:27 Mercury mg/kg0.840 0.10 0.833 85-115101 LCS Dup (B1E0694-BSD1) [TOC_3]LCS Dup (B1E0694-BSD1)[TOC] Analyzed: 05/25/21 13:29 Mercury mg/kg0.849 0.10 0.833 2085-115102 1 Duplicate (B1E0694-DUP1)Source: 2103193-05 [TOC_3]Duplicate (B1E0694-DUP1)[TOC] Analyzed: 05/25/21 13:47 Mercury mg/kg0.216 0.18 1.87 20 QR-04159 Matrix Spike (B1E0694-MS1)Source: 2103193-05 [TOC_3]Matrix Spike (B1E0694-MS1)[TOC] Analyzed: 05/25/21 13:51 Mercury mg/kg1.04 0.093 0.776 1.87 QM-0775-125NR Matrix Spike Dup (B1E0694-MSD1)Source: 2103193-05 [TOC_3]Matrix Spike Dup (B1E0694-MSD1)[TOC] Analyzed: 05/25/21 13:53 Mercury mg/kg1.68 0.090 0.751 1.87 20 QM-07, QR-04 75-125NR 47 Post Spike (B1E0694-PS1)Source: 2103193-02 [TOC_3]Post Spike (B1E0694-PS1)[TOC] Analyzed: 05/25/21 15:19 Mercury ug/L5.28 5.00 0.114 85-115103 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 36 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 36 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0693 - EPA 3050B[TOC] Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Blank (B1E0693-BLK1) [TOC_3]Blank (B1E0693-BLK1)[TOC] Analyzed: 05/25/21 14:02 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1E0693-BS1) [TOC_3]LCS (B1E0693-BS1)[TOC] Analyzed: 05/25/21 14:45 Antimony mg/kg99.7 2.5 100 80-120100 Arsenic "99.6 2.0 100 80-120100 Barium "102 1.0 100 80-120102 Beryllium "98.2 0.50 100 80-12098 Cadmium "100 0.25 100 80-120100 Chromium "99.5 0.50 100 80-120100 Cobalt "101 0.50 100 80-120101 Copper "101 1.0 100 80-120101 Lead "102 0.50 100 80-120102 Molybdenum "97.8 0.50 100 80-12098 Nickel "101 0.50 100 80-120101 Selenium "99.0 2.0 100 80-12099 Silver "4.96 0.50 5.00 80-12099 Thallium "102 1.0 100 80-120102 Vanadium "97.6 2.0 100 80-12098 Zinc "100 2.0 100 80-120100 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 37 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 37 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 LCS Dup (B1E0693-BSD1) [TOC_3]LCS Dup (B1E0693-BSD1)[TOC] Analyzed: 05/25/21 14:47 Antimony mg/kg1002.5 100 2080-120100 0.5 Arsenic "99.7 2.0 100 2080-120100 0.1 Barium "101 1.0 100 2080-120101 0.05 Beryllium "98.5 0.50 100 2080-12098 0.3 Cadmium "100 0.25 100 2080-120100 0.2 Chromium "99.4 0.50 100 2080-12099 0.2 Cobalt "101 0.50 100 2080-120101 0.05 Copper "100 1.0 100 2080-120100 0.2 Lead "102 0.50 100 2080-120102 0.1 Molybdenum "98.4 0.50 100 2080-12098 0.6 Nickel "102 0.50 100 2080-120102 0.1 Selenium "100 2.0 100 2080-120100 1 Silver "4.96 0.50 5.00 2080-12099 0 Thallium "102 1.0 100 2080-120102 0.4 Vanadium "97.0 2.0 100 2080-12097 0.7 Zinc "100 2.0 100 2080-120100 0.2 Duplicate (B1E0693-DUP1)Source: 2103212-05 [TOC_3]Duplicate (B1E0693-DUP1)[TOC] Analyzed: 05/25/21 14:15 Antimony mg/kgND2.4 ND 20 Arsenic "5.18 1.9 6.10 2016 Barium "205 0.97 218 206 Beryllium "0.408 0.49 0.435 206 Cadmium "ND 0.24 ND 20 Chromium "154 0.49 144 207 Cobalt "22.3 0.49 20.9 206 Copper "48.8 0.97 46.3 205 Lead "17.9 0.49 19.3 208 Molybdenum "0.510 0.49 0.574 2012 Nickel "196 0.49 179 209 Selenium "ND 1.9 ND 20 Silver "ND 0.49 ND 20 Thallium "ND 0.97 ND 20 Vanadium "52.3 1.9 54.0 203 Zinc "69.6 1.9 87.4 20 QR-0423 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 38 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 38 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Matrix Spike (B1E0693-MS1)Source: 2103212-05 [TOC_3]Matrix Spike (B1E0693-MS1)[TOC] Analyzed: 05/25/21 13:50 Antimony mg/kg13.1 2.4 97.9 ND 10-11613 Arsenic "101 2.0 97.9 6.10 77-12196 Barium "226 0.98 97.9 218 QM-0730-1698 Beryllium "95.2 0.49 97.9 0.435 86-11197 Cadmium "90.0 0.24 97.9 ND 81-11292 Chromium "218 0.49 97.9 144 75-12976 Cobalt "109 0.49 97.9 20.9 71-12190 Copper "146 0.98 97.9 46.3 68-135102 Lead "107 0.49 97.9 19.3 72-12190 Molybdenum "35.0 0.49 97.9 0.574 QM-0770-11235 Nickel "230 0.49 97.9 179 QM-0773-12152 Selenium "85.9 2.0 97.9 ND 76-11688 Silver "4.79 0.49 4.90 ND 54-13298 Thallium "85.9 0.98 97.9 ND 64-12088 Vanadium "138 2.0 97.9 54.0 78-12486 Zinc "162 2.0 97.9 87.4 50-14377 Matrix Spike Dup (B1E0693-MSD1)Source: 2103212-05 [TOC_3]Matrix Spike Dup (B1E0693-MSD1)[TOC] Analyzed: 05/25/21 13:52 Antimony mg/kg9.34 2.4 95.8 ND 20 QR-0210-11610 33 Arsenic "96.6 1.9 95.8 6.10 2077-12195 4 Barium "295 0.96 95.8 218 20 QR-0230-16980 26 Beryllium "91.2 0.48 95.8 0.435 2086-11195 4 Cadmium "85.1 0.24 95.8 ND 2081-11289 6 Chromium "271 0.48 95.8 144 20 QM-07, QR-04 75-129133 22 Cobalt "113 0.48 95.8 20.9 2071-12196 3 Copper "140 0.96 95.8 46.3 2068-13597 4 Lead "104 0.48 95.8 19.3 2072-12188 3 Molybdenum "32.4 0.48 95.8 0.574 20 QM-0770-11233 8 Nickel "319 0.48 95.8 179 20 QM-07, QR-04 73-121146 32 Selenium "79.5 1.9 95.8 ND 2076-11683 8 Silver "4.59 0.48 4.79 ND 2054-13296 4 Thallium "79.5 0.96 95.8 ND 2064-12083 8 Vanadium "147 1.9 95.8 54.0 2078-12497 6 Zinc "158 1.9 95.8 87.4 2050-14374 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 39 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 39 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0693 - EPA 6010B Preparation: EPA 3050B 05/25/21 07:26 Post Spike (B1E0693-PS1)Source: 2103212-05 [TOC_3]Post Spike (B1E0693-PS1)[TOC] Analyzed: 05/25/21 14:08 Antimony mg/L1.98 2.00 0.00347 75-12599 Arsenic "2.07 2.00 0.121 75-12598 Barium "6.39 2.00 4.34 75-125103 Beryllium "1.96 2.00 0.00863 75-12598 Cadmium "1.83 2.00 -0.0417 75-12591 Chromium "4.75 2.00 2.85 75-12595 Cobalt "2.27 2.00 0.414 75-12593 Copper "2.88 2.00 0.919 75-12598 Lead "2.24 2.00 0.384 75-12593 Molybdenum "1.97 2.00 0.0114 75-12598 Nickel "5.42 2.00 3.56 75-12593 Selenium "1.80 2.00 -0.120 75-12590 Silver "0.0954 0.100 -0.00119 75-12595 Thallium "1.78 2.00 -0.0164 75-12589 Vanadium "3.01 2.00 1.07 75-12597 Zinc "3.61 2.00 1.74 75-12594 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 40 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 40 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: STLC Metals by ICP - Quality Control[TOC_1]STLC Metals by IC Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0829 - EPA 3010A Leachate[TOC] Batch B1E0829 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 05/28/21 09:36 Blank (B1E0829-BLK1) [TOC_3]Blank (B1E0829-BLK1)[TOC] Analyzed: 05/28/21 12:56 Chromium mg/LND0.050 Nickel "ND 0.050 LCS (B1E0829-BS1) [TOC_3]LCS (B1E0829-BS1)[TOC] Analyzed: 05/28/21 13:01 Chromium mg/L10.5 0.050 10.0 80-120105 Nickel "10.4 0.050 10.0 80-120104 LCS Dup (B1E0829-BSD1) [TOC_3]LCS Dup (B1E0829-BSD1)[TOC] Analyzed: 05/28/21 13:03 Chromium mg/L10.1 0.050 10.0 2080-120101 4 Nickel "10.1 0.050 10.0 2080-120101 3 Duplicate (B1E0829-DUP1)Source: 2103212-01 [TOC_3]Duplicate (B1E0829-DUP1)[TOC] Analyzed: 05/28/21 13:21 Chromium mg/L0.0790 0.10 0.0810 202 Nickel "0.329 0.10 0.345 205 Leach Fluid Blank (B1E0829-LBK1) [TOC_3]Leach Fluid Blank (B1E0829-LBK1)[TOC] Analyzed: 05/28/21 12:58 Chromium mg/LND0.050 Nickel "0.0385 0.050 B-02 Matrix Spike (B1E0829-MS1)Source: 2103212-01 [TOC_3]Matrix Spike (B1E0829-MS1)[TOC] Analyzed: 05/28/21 13:10 Chromium mg/L10.0 0.10 10.0 0.0810 82-11999 Nickel "10.0 0.10 10.0 0.345 80-11697 Matrix Spike Dup (B1E0829-MSD1)Source: 2103212-01 [TOC_3]Matrix Spike Dup (B1E0829-MSD1)[TOC] Analyzed: 05/28/21 13:12 Chromium mg/L10.3 0.10 10.0 0.0810 2082-119102 3 Nickel "10.3 0.10 10.0 0.345 2080-11699 3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 41 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 41 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: TCLP Metals by ICP - Quality Control[TOC_1]TCL Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0794 - EPA 3010A Leachate[TOC] Batch B1E0794 - EPA 1311/EPA 6010B Preparation: EPA 3010A Leachate 05/27/21 10:55 Blank (B1E0794-BLK1) [TOC_3]Blank (B1E0794-BLK1)[TOC] Analyzed: 05/27/21 18:35 Chromium mg/LND0.050 LCS (B1E0794-BS1) [TOC_3]LCS (B1E0794-BS1)[TOC] Analyzed: 05/27/21 18:20 Chromium mg/L10.0 0.050 10.0 80-120100 LCS Dup (B1E0794-BSD1) [TOC_3]LCS Dup (B1E0794-BSD1)[TOC] Analyzed: 05/27/21 18:22 Chromium mg/L9.84 0.050 10.0 2080-12098 2 Duplicate (B1E0794-DUP1)Source: 2102854-01 [TOC_3]Duplicate (B1E0794-DUP1)[TOC] Analyzed: 05/27/21 18:52 Chromium mg/LND0.050 ND 20 Leach Fluid Blank (B1E0794-LBK1) [TOC_3]Leach Fluid Blank (B1E0794-LBK1)[TOC] Analyzed: 05/27/21 18:37 Chromium mg/LND0.050 Leach Fluid Blank (B1E0794-LBK2)Analyzed: 05/27/21 18:40 Chromium mg/LND0.050 Leach Fluid Blank (B1E0794-LBK3)Analyzed: 05/27/21 18:42 Chromium mg/LND0.050 Matrix Spike (B1E0794-MS1)Source: 2102854-01 [TOC_3]Matrix Spike (B1E0794-MS1)[TOC] Analyzed: 05/27/21 18:25 Chromium mg/L10.2 0.050 10.0 ND 82-119102 Matrix Spike Dup (B1E0794-MSD1)Source: 2102854-01 [TOC_3]Matrix Spike Dup (B1E0794-MSD1)[TOC] Analyzed: 05/27/21 18:45 Chromium mg/L10.2 0.050 10.0 ND 2082-119102 0.6 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 42 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 42 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0737 - EPA 5035/5030B Solid GC[TOC] Batch B1E0737 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 05/26/21 06:59 Blank (B1E0737-BLK1) [TOC_3]Blank (B1E0737-BLK1)[TOC] Analyzed: 05/26/21 10:49 TPH Gasoline (C5-C12)mg/kgND0.50 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1020.128 LCS (B1E0737-BS1) [TOC_3]LCS (B1E0737-BS1)[TOC] Analyzed: 05/26/21 09:57 TPH Gasoline (C5-C12)mg/kg1.08 0.50 0.994 68-139108 "0.124 39-157Surrogate: 4-Bromofluorobenzene 1170.146 LCS Dup (B1E0737-BSD1) [TOC_3]LCS Dup (B1E0737-BSD1)[TOC] Analyzed: 05/26/21 10:23 TPH Gasoline (C5-C12)mg/kg1.20 0.50 0.998 2068-139120 11 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1230.154 Duplicate (B1E0737-DUP1)Source: 2103210-01RE1 [TOC_3]Duplicate (B1E0737-DUP1)[TOC] Analyzed: 05/26/21 13:04 TPH Gasoline (C5-C12)mg/kgND0.49 ND 20 "0.122 39-157Surrogate: 4-Bromofluorobenzene 990.120 Matrix Spike (B1E0737-MS1)Source: 2103210-01RE1 [TOC_3]Matrix Spike (B1E0737-MS1)[TOC] Analyzed: 05/26/21 23:45 TPH Gasoline (C5-C12)mg/kg0.868 0.48 0.967 ND 10-17190 "0.121 39-157Surrogate: 4-Bromofluorobenzene 1170.142 Matrix Spike Dup (B1E0737-MSD1)Source: 2103210-01RE1 [TOC_3]Matrix Spike Dup (B1E0737-MSD1)[TOC] Analyzed: 05/27/21 00:11 TPH Gasoline (C5-C12)mg/kg0.911 0.50 0.998 ND 2010-17191 5 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1190.149 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 43 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 43 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0696 - EPA 3550C[TOC] Batch B1E0696 - EPA 8015M Preparation: EPA 3550C 05/25/21 08:55 Blank (B1E0696-BLK1) [TOC_3]Blank (B1E0696-BLK1)[TOC] Analyzed: 05/25/21 13:41 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "50.0 65-136Surrogate: o-Terphenyl 8743.3 LCS (B1E0696-BS1) [TOC_3]LCS (B1E0696-BS1)[TOC] Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22)mg/kg51210 499 72-115103 TPH Motor Oil (C23-C40)"473 50 499 74-12695 "49.9 65-136Surrogate: o-Terphenyl 10049.9 LCS Dup (B1E0696-BSD1) [TOC_3]LCS Dup (B1E0696-BSD1)[TOC] Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22)mg/kg48710 500 2072-11597 5 TPH Motor Oil (C23-C40)"459 50 500 2074-12692 3 "50.0 65-136Surrogate: o-Terphenyl 9748.7 Duplicate (B1E0696-DUP1)Source: 2103212-01 [TOC_3]Duplicate (B1E0696-DUP1)[TOC] Analyzed: 05/25/21 14:03 TPH Diesel (C13-C22)mg/kg35.5 9.9 50.9 20 QR-0636 TPH Motor Oil (C23-C40)"ND 50 ND 20 "49.7 65-136Surrogate: o-Terphenyl 8642.6 Matrix Spike (B1E0696-MS1)Source: 2103212-01 [TOC_3]Matrix Spike (B1E0696-MS1)[TOC] Analyzed: 05/25/21 12:55 TPH Diesel (C13-C22)mg/kg50010 498 50.9 46-14790 TPH Motor Oil (C23-C40)"432 50 498 ND 35-17187 "49.8 65-136Surrogate: o-Terphenyl 8944.5 Matrix Spike Dup (B1E0696-MSD1)Source: 2103212-01 [TOC_3]Matrix Spike Dup (B1E0696-MSD1)[TOC] Analyzed: 05/25/21 13:18 TPH Diesel (C13-C22)mg/kg4979.9 497 50.9 2046-14790 0.6 TPH Motor Oil (C23-C40)"432 50 497 ND 2035-17187 0.2 "49.7 65-136Surrogate: o-Terphenyl 8944.3 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 44 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 44 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1E0697 - EPA 5035/5030B MEOH[TOC] Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1) [TOC_3]Blank (B1E0697-BLK1)[TOC] Analyzed: 05/25/21 13:26 Benzene mg/kgND0.25 Bromobenzene "ND 0.25 Bromochloromethane "ND 0.25 Bromodichloromethane "ND 0.25 Bromoform "ND 0.25 Bromomethane "ND 0.25 n-Butylbenzene "ND 0.25 sec-Butylbenzene "ND 0.25 tert-Butylbenzene "ND 0.25 Carbon tetrachloride "ND 0.25 Chlorobenzene "ND 0.25 Chloroethane "ND 0.25 Chloroform "ND 0.25 Chloromethane "ND 0.25 2-Chlorotoluene "ND 0.25 4-Chlorotoluene "ND 0.25 Dibromochloromethane "ND 0.25 1,2-Dibromo-3-chloropropane "ND 0.25 1,2-Dibromoethane (EDB)"ND 0.25 Dibromomethane "ND 0.25 1,2-Dichlorobenzene "ND 0.25 1,3-Dichlorobenzene "ND 0.25 1,4-Dichlorobenzene "ND 0.25 Dichlorodifluoromethane "ND 0.25 1,1-Dichloroethane "ND 0.25 1,2-Dichloroethane "ND 0.25 1,1-Dichloroethene "ND 0.25 cis-1,2-Dichloroethene "ND 0.25 trans-1,2-Dichloroethene "ND 0.25 1,2-Dichloropropane "ND 0.25 1,3-Dichloropropane "ND 0.25 2,2-Dichloropropane "ND 0.25 1,1-Dichloropropene "ND 0.25 cis-1,3-Dichloropropene "ND 0.25 trans-1,3-Dichloropropene "ND 0.25 Ethylbenzene "ND 0.25 Hexachlorobutadiene "ND 0.25 4-Isopropyl Toluene "ND 0.25 Isopropylbenzene "ND 0.25 Methylene chloride "ND 0.25 Naphthalene "ND 0.25 n-Propylbenzene "ND 0.25 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 45 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 45 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Blank (B1E0697-BLK1)Analyzed: 05/25/21 13:26 Styrene mg/kgND0.25 1,1,1,2-Tetrachloroethane "ND 0.25 1,1,2,2-Tetrachloroethane "ND 0.25 Tetrachloroethene (PCE)"ND 0.25 Toluene "ND 0.25 1,2,3-Trichlorobenzene "ND 0.25 1,2,4-Trichlorobenzene "ND 0.25 1,1,1-Trichloroethane "ND 0.25 1,1,2-Trichloroethane "ND 0.25 Trichloroethene (TCE)"ND 0.25 Trichlorofluoromethane "ND 0.25 1,2,3-Trichloropropane "ND 0.25 1,2,4-Trimethylbenzene "ND 0.25 1,3,5-Trimethylbenzene "ND 0.25 Vinyl chloride "ND 0.25 Xylenes (total)"ND 0.25 "0.0500 74-122Surrogate: Dibromofluoromethane 990.0496 "0.0500 65-128Surrogate: Toluene-d8 1010.0507 "0.0500 75-121Surrogate: 4-Bromofluorobenzene 960.0482 LCS (B1E0697-BS1) [TOC_3]LCS (B1E0697-BS1)[TOC] Analyzed: 05/25/21 11:37 Benzene mg/kg1.80 0.25 1.98 70-13191 Bromobenzene "2.09 0.25 1.98 74-130105 Bromochloromethane "1.77 0.25 1.98 64-13389 Bromodichloromethane "2.12 0.25 1.98 69-137107 Bromoform "2.09 0.25 1.98 55-132105 Bromomethane "1.51 0.25 1.98 10-14276 n-Butylbenzene "2.47 0.25 1.98 64-156125 sec-Butylbenzene "2.46 0.25 1.98 75-155124 tert-Butylbenzene "2.34 0.25 1.98 74-144118 Carbon tetrachloride "1.70 0.25 1.98 67-13586 Chlorobenzene "2.08 0.25 1.98 73-134105 Chloroethane "1.65 0.25 1.98 10-16783 Chloroform "2.01 0.25 1.98 69-124101 Chloromethane "2.46 0.25 1.98 34-136124 2-Chlorotoluene "2.16 0.25 1.98 75-135109 4-Chlorotoluene "2.30 0.25 1.98 70-138116 Dibromochloromethane "2.01 0.25 1.98 67-135102 1,2-Dibromo-3-chloropropane "2.45 0.25 1.98 41-149124 1,2-Dibromoethane (EDB)"1.98 0.25 1.98 68-131100 Dibromomethane "1.92 0.25 1.98 61-14097 1,2-Dichlorobenzene "2.20 0.25 1.98 76-136111 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 46 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 46 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS (B1E0697-BS1)Analyzed: 05/25/21 11:37 1,3-Dichlorobenzene mg/kg2.30 0.25 1.98 76-138116 1,4-Dichlorobenzene "2.23 0.25 1.98 72-132112 Dichlorodifluoromethane "1.51 0.25 1.98 10-15576 1,1-Dichloroethane "1.90 0.25 1.98 63-13996 1,2-Dichloroethane "2.04 0.25 1.98 64-126103 1,1-Dichloroethene "1.79 0.25 1.98 52-16790 cis-1,2-Dichloroethene "1.84 0.25 1.98 70-13593 trans-1,2-Dichloroethene "1.69 0.25 1.98 67-14785 1,2-Dichloropropane "3.19 0.25 1.98 QM-0868-131161 1,3-Dichloropropane "1.91 0.25 1.98 64-12896 2,2-Dichloropropane "2.11 0.25 1.98 63-154107 1,1-Dichloropropene "1.82 0.25 1.98 68-13892 cis-1,3-Dichloropropene "2.08 0.25 1.98 72-134105 trans-1,3-Dichloropropene "2.16 0.25 1.98 69-132109 Ethylbenzene "1.92 0.25 1.98 68-13697 Hexachlorobutadiene "2.24 0.25 1.98 72-198113 4-Isopropyl Toluene "2.40 0.25 1.98 74-150121 Isopropylbenzene "2.21 0.25 1.98 71-149112 Methylene chloride "1.81 0.25 1.98 51-12791 Naphthalene "2.29 0.25 1.98 57-158116 n-Propylbenzene "2.29 0.25 1.98 70-143116 Styrene "2.47 0.25 1.98 68-138124 1,1,1,2-Tetrachloroethane "2.10 0.25 1.98 76-130106 1,1,2,2-Tetrachloroethane "2.18 0.25 1.98 60-136110 Tetrachloroethene (PCE)"1.79 0.25 1.98 73-13891 Toluene "1.99 0.25 1.98 72-128101 1,2,3-Trichlorobenzene "2.47 0.25 1.98 61-166125 1,2,4-Trichlorobenzene "2.43 0.25 1.98 71-158123 1,1,1-Trichloroethane "1.92 0.25 1.98 71-13597 1,1,2-Trichloroethane "2.23 0.25 1.98 64-132113 Trichloroethene (TCE)"1.87 0.25 1.98 74-13994 Trichlorofluoromethane "2.69 0.25 1.98 30-156136 1,2,3-Trichloropropane "2.05 0.25 1.98 67-123104 1,2,4-Trimethylbenzene "2.31 0.25 1.98 68-134117 1,3,5-Trimethylbenzene "2.27 0.25 1.98 71-140114 Vinyl chloride "2.14 0.25 1.98 43-144108 Xylenes (total)"6.81 0.25 5.94 69-138115 "0.0495 74-122Surrogate: Dibromofluoromethane 1030.0512 "0.0495 65-128Surrogate: Toluene-d8 1040.0516 "0.0495 75-121Surrogate: 4-Bromofluorobenzene 940.0467 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 47 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 47 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSD1) [TOC_3]LCS Dup (B1E0697-BSD1)[TOC] Analyzed: 05/25/21 12:04 Benzene mg/kg1.74 0.25 1.99 2070-13187 3 Bromobenzene "2.08 0.25 1.99 2074-130104 0.4 Bromochloromethane "1.69 0.25 1.99 2064-13385 5 Bromodichloromethane "2.14 0.25 1.99 2069-137107 0.8 Bromoform "2.06 0.25 1.99 2055-132103 1 Bromomethane "1.50 0.25 1.99 2010-14275 1 n-Butylbenzene "2.33 0.25 1.99 2064-156117 6 sec-Butylbenzene "2.25 0.25 1.99 2075-155113 9 tert-Butylbenzene "2.17 0.25 1.99 2074-144109 8 Carbon tetrachloride "1.60 0.25 1.99 2067-13580 6 Chlorobenzene "2.07 0.25 1.99 2073-134104 0.3 Chloroethane "1.70 0.25 1.99 2010-16785 3 Chloroform "1.93 0.25 1.99 2069-12497 4 Chloromethane "2.16 0.25 1.99 2034-136108 13 2-Chlorotoluene "2.05 0.25 1.99 2075-135103 5 4-Chlorotoluene "2.15 0.25 1.99 2070-138108 7 Dibromochloromethane "2.11 0.25 1.99 2067-135106 5 1,2-Dibromo-3-chloropropane "2.68 0.25 1.99 2041-149135 9 1,2-Dibromoethane (EDB)"2.01 0.25 1.99 2068-131101 1 Dibromomethane "1.92 0.25 1.99 2061-14096 0.08 1,2-Dichlorobenzene "2.20 0.25 1.99 2076-136110 0.4 1,3-Dichlorobenzene "2.15 0.25 1.99 2076-138108 7 1,4-Dichlorobenzene "2.13 0.25 1.99 2072-132107 5 Dichlorodifluoromethane "1.50 0.25 1.99 2010-15575 0.5 1,1-Dichloroethane "1.83 0.25 1.99 2063-13992 4 1,2-Dichloroethane "2.01 0.25 1.99 2064-126101 2 1,1-Dichloroethene "1.73 0.25 1.99 2052-16787 4 cis-1,2-Dichloroethene "1.71 0.25 1.99 2070-13586 8 trans-1,2-Dichloroethene "1.64 0.25 1.99 2067-14782 3 1,2-Dichloropropane "1.94 0.25 1.99 20 QR-0468-13197 49 1,3-Dichloropropane "2.05 0.25 1.99 2064-128103 7 2,2-Dichloropropane "2.00 0.25 1.99 2063-154100 5 1,1-Dichloropropene "1.75 0.25 1.99 2068-13888 4 cis-1,3-Dichloropropene "1.98 0.25 1.99 2072-134100 5 trans-1,3-Dichloropropene "2.25 0.25 1.99 2069-132113 4 Ethylbenzene "2.05 0.25 1.99 2068-136103 7 Hexachlorobutadiene "2.12 0.25 1.99 2072-198107 5 4-Isopropyl Toluene "2.23 0.25 1.99 2074-150112 7 Isopropylbenzene "2.24 0.25 1.99 2071-149112 1 Methylene chloride "1.79 0.25 1.99 2051-12790 1 Naphthalene "2.10 0.25 1.99 2057-158106 8 n-Propylbenzene "2.12 0.25 1.99 2070-143106 8 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 48 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 48 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 LCS Dup (B1E0697-BSD1)Analyzed: 05/25/21 12:04 Styrene mg/kg2.23 0.25 1.99 2068-138112 10 1,1,1,2-Tetrachloroethane "2.18 0.25 1.99 2076-130109 3 1,1,2,2-Tetrachloroethane "2.11 0.25 1.99 2060-136106 3 Tetrachloroethene (PCE)"1.81 0.25 1.99 2073-13891 0.8 Toluene "1.83 0.25 1.99 2072-12892 9 1,2,3-Trichlorobenzene "2.32 0.25 1.99 2061-166116 6 1,2,4-Trichlorobenzene "2.35 0.25 1.99 2071-158118 3 1,1,1-Trichloroethane "1.86 0.25 1.99 2071-13593 3 1,1,2-Trichloroethane "2.18 0.25 1.99 2064-132109 2 Trichloroethene (TCE)"1.82 0.25 1.99 2074-13991 3 Trichlorofluoromethane "2.59 0.25 1.99 2030-156130 4 1,2,3-Trichloropropane "1.96 0.25 1.99 2067-12398 5 1,2,4-Trimethylbenzene "2.16 0.25 1.99 2068-134108 7 1,3,5-Trimethylbenzene "2.13 0.25 1.99 2071-140107 6 Vinyl chloride "2.12 0.25 1.99 2043-144107 0.6 Xylenes (total)"6.17 0.25 5.98 2069-138103 10 "0.0498 74-122Surrogate: Dibromofluoromethane 1030.0512 "0.0498 65-128Surrogate: Toluene-d8 1020.0510 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 1000.0499 Duplicate (B1E0697-DUP1)Source: 2103210-01 [TOC_3]Duplicate (B1E0697-DUP1)[TOC] Analyzed: 05/25/21 14:48 Benzene mg/kgND1.2 ND 20 Bromobenzene "ND 1.2 ND 20 Bromochloromethane "ND 1.2 ND 20 Bromodichloromethane "ND 1.2 ND 20 Bromoform "ND 1.2 ND 20 Bromomethane "ND 1.2 ND 20 n-Butylbenzene "ND 1.2 ND 20 sec-Butylbenzene "ND 1.2 ND 20 tert-Butylbenzene "ND 1.2 ND 20 Carbon tetrachloride "ND 1.2 ND 20 Chlorobenzene "ND 1.2 ND 20 Chloroethane "ND 1.2 ND 20 Chloroform "ND 1.2 ND 20 Chloromethane "ND 1.2 ND 20 2-Chlorotoluene "ND 1.2 ND 20 4-Chlorotoluene "ND 1.2 ND 20 Dibromochloromethane "ND 1.2 ND 20 1,2-Dibromo-3-chloropropane "ND 1.2 ND 20 1,2-Dibromoethane (EDB)"ND 1.2 ND 20 Dibromomethane "ND 1.2 ND 20 1,2-Dichlorobenzene "ND 1.2 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 49 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 49 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Duplicate (B1E0697-DUP1)Source: 2103210-01 Analyzed: 05/25/21 14:48 1,3-Dichlorobenzene mg/kgND1.2 ND 20 1,4-Dichlorobenzene "ND 1.2 ND 20 Dichlorodifluoromethane "ND 1.2 ND 20 1,1-Dichloroethane "ND 1.2 ND 20 1,2-Dichloroethane "ND 1.2 ND 20 1,1-Dichloroethene "ND 1.2 ND 20 cis-1,2-Dichloroethene "ND 1.2 ND 20 trans-1,2-Dichloroethene "ND 1.2 ND 20 1,2-Dichloropropane "ND 1.2 ND 20 1,3-Dichloropropane "ND 1.2 ND 20 2,2-Dichloropropane "ND 1.2 ND 20 1,1-Dichloropropene "ND 1.2 ND 20 cis-1,3-Dichloropropene "ND 1.2 ND 20 trans-1,3-Dichloropropene "ND 1.2 ND 20 Ethylbenzene "ND 1.2 ND 20 Hexachlorobutadiene "ND 1.2 ND 20 4-Isopropyl Toluene "ND 1.2 ND 20 Isopropylbenzene "ND 1.2 ND 20 Methylene chloride "ND 1.2 ND 20 Naphthalene "ND 1.2 ND 20 n-Propylbenzene "ND 1.2 ND 20 Styrene "ND 1.2 ND 20 1,1,1,2-Tetrachloroethane "ND 1.2 ND 20 1,1,2,2-Tetrachloroethane "ND 1.2 ND 20 Tetrachloroethene (PCE)"ND 1.2 ND 20 Toluene "ND 1.2 ND 20 1,2,3-Trichlorobenzene "ND 1.2 ND 20 1,2,4-Trichlorobenzene "ND 1.2 ND 20 1,1,1-Trichloroethane "ND 1.2 ND 20 1,1,2-Trichloroethane "ND 1.2 ND 20 Trichloroethene (TCE)"ND 1.2 ND 20 Trichlorofluoromethane "ND 1.2 ND 20 1,2,3-Trichloropropane "ND 1.2 ND 20 1,2,4-Trimethylbenzene "ND 1.2 ND 20 1,3,5-Trimethylbenzene "ND 1.2 ND 20 Vinyl chloride "ND 1.2 ND 20 Xylenes (total)"ND 1.2 ND 20 "0.0494 74-122Surrogate: Dibromofluoromethane 1020.0503 "0.0494 65-128Surrogate: Toluene-d8 1040.0514 "0.0494 75-121Surrogate: 4-Bromofluorobenzene 970.0478 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 50 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 50 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1)Source: 2103212-01 [TOC_3]Matrix Spike (B1E0697-MS1)[TOC] Analyzed: 05/25/21 19:22 Benzene mg/kg8.97 1.2 9.94 ND 37-14590 Bromobenzene "11.0 1.2 9.94 ND 29-147111 Bromochloromethane "9.22 1.2 9.94 ND 40-14593 Bromodichloromethane "10.9 1.2 9.94 ND 39-153110 Bromoform "10.7 1.2 9.94 ND 32-143108 Bromomethane "10.3 1.2 9.94 ND 10-141104 n-Butylbenzene "11.6 1.2 9.94 ND 10-162117 sec-Butylbenzene "12.2 1.2 9.94 ND 14-168123 tert-Butylbenzene "11.8 1.2 9.94 ND 21-159119 Carbon tetrachloride "8.48 1.2 9.94 ND 28-14885 Chlorobenzene "10.9 1.2 9.94 ND 32-148110 Chloroethane "12.6 1.2 9.94 ND 11-166127 Chloroform "9.94 1.2 9.94 ND 40-139100 Chloromethane "10.4 1.2 9.94 ND 18-135105 2-Chlorotoluene "10.8 1.2 9.94 ND 25-151108 4-Chlorotoluene "11.3 1.2 9.94 ND 22-150114 Dibromochloromethane "10.2 1.2 9.94 ND 40-147103 1,2-Dibromo-3-chloropropane "12.4 1.2 9.94 ND 25-158125 1,2-Dibromoethane (EDB)"10.1 1.2 9.94 ND 38-147102 Dibromomethane "9.74 1.2 9.94 ND 39-15098 1,2-Dichlorobenzene "11.4 1.2 9.94 ND 24-154115 1,3-Dichlorobenzene "11.3 1.2 9.94 ND 21-153114 1,4-Dichlorobenzene "10.9 1.2 9.94 ND 21-146110 Dichlorodifluoromethane "6.32 1.2 9.94 ND 10-14964 1,1-Dichloroethane "9.32 1.2 9.94 ND 34-15194 1,2-Dichloroethane "9.93 1.2 9.94 ND 40-137100 1,1-Dichloroethene "7.41 1.2 9.94 ND 21-17274 cis-1,2-Dichloroethene "8.87 1.2 9.94 ND 38-14789 trans-1,2-Dichloroethene "8.06 1.2 9.94 ND 30-16081 1,2-Dichloropropane "10.0 1.2 9.94 ND 39-146101 1,3-Dichloropropane "9.84 1.2 9.94 ND 39-14199 2,2-Dichloropropane "9.05 1.2 9.94 ND 26-14991 1,1-Dichloropropene "9.03 1.2 9.94 ND 28-15091 cis-1,3-Dichloropropene "9.92 1.2 9.94 ND 34-149100 trans-1,3-Dichloropropene "11.0 1.2 9.94 ND 36-143111 Ethylbenzene "10.8 1.2 9.94 ND 23-150109 Hexachlorobutadiene "11.4 1.2 9.94 ND 10-192115 4-Isopropyl Toluene "11.9 1.2 9.94 ND 11-165120 Isopropylbenzene "11.7 1.2 9.94 ND 17-166118 Methylene chloride "8.61 1.2 9.94 ND 28-13587 Naphthalene "12.4 1.2 9.94 ND 10-174124 n-Propylbenzene "11.3 1.2 9.94 ND 16-156114 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 51 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 51 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1E0697 - EPA 8260B Preparation: EPA 5035/5030B MEOH 05/25/21 09:00 Matrix Spike (B1E0697-MS1)Source: 2103212-01 Analyzed: 05/25/21 19:22 Styrene mg/kg11.5 1.2 9.94 ND 24-154116 1,1,1,2-Tetrachloroethane "11.1 1.2 9.94 ND 38-149111 1,1,2,2-Tetrachloroethane "10.7 1.2 9.94 ND 22-164107 Tetrachloroethene (PCE)"9.37 1.2 9.94 ND 25-15394 Toluene "10.4 1.2 9.94 ND 26-149105 1,2,3-Trichlorobenzene "12.7 1.2 9.94 ND 10-163128 1,2,4-Trichlorobenzene "12.4 1.2 9.94 ND 10-162124 1,1,1-Trichloroethane "9.87 1.2 9.94 ND 34-14999 1,1,2-Trichloroethane "11.3 1.2 9.94 ND 25-175113 Trichloroethene (TCE)"9.24 1.2 9.94 ND 25-17093 Trichlorofluoromethane "12.0 1.2 9.94 ND 19-155121 1,2,3-Trichloropropane "9.81 1.2 9.94 ND 32-16599 1,2,4-Trimethylbenzene "11.7 1.2 9.94 ND 15-150118 1,3,5-Trimethylbenzene "11.4 1.2 9.94 ND 10-158114 Vinyl chloride "11.2 1.2 9.94 ND 22-148112 Xylenes (total)"32.3 1.2 29.8 ND 22-153108 "0.0497 74-122Surrogate: Dibromofluoromethane 1020.0508 "0.0497 65-128Surrogate: Toluene-d8 1020.0509 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 1000.0499 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 52 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 52 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid STLC Metals by ICP STLC/EPA 6010B OEC, CA-ELAP6010B STLC Chromium Water STLC/EPA 6010B OEC, CA-ELAP6010B STLC Nickel Water STLC Metals Extraction STLC OEC, InternalSTLC Metals Extraction Solid TCLP Metals by ICP EPA 1311/EPA 6010B OEC, CA-ELAP6010B TCLP Chromium Water TCLP Metals Extraction EPA 1311 OEC, CA-ELAPTCLP Metals Extraction Solid Total Metals by CVAA EPA 7471A OEC, CA-ELAPMercury Total EPA 7471A Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 53 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 53 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Sample Method Summary (Continued) Laboratory & CertificationMethodAnalysisMatrix Total Metals by ICP EPA 6010B OEC, CA-ELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP8260B Full List Solid Volatile Organic TPH by GC/FID EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid EPA 8015M OEC, Internal8015 TPH-Gasoline Solid EPA 8015M OEC, CA-ELAP8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 54 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 54 of 59 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/01/2021 10:29Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103212 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL B-02 The method blank contains analyte at a J-flag concentration. D-04 The sample chromatographic pattern does not resemble the fuel standard used for quantitation. N-02 Analyte concentration below TTLC but above 10x STLC. N-03 Analyte concentration above 20x TCLP. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery and/or RPD values. QM-08 The spike recovery was outside acceptance limits for the LCS. The batch was accepted based on acceptable LCSD recovery. QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data. QR-04 The RPD exceeded the QC control limits. QR-06 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to non-homogenous sample matrix. QC batch accepted based on LCS and/or LCSD recovery and/or RPD values. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. TMP3 Temperature [Out-Acceptable] Direct from Field The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 55 of 58 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:California ELAP Certificate # 2438 Page 55 of 59 File :V:\DATA\MAY21\052521\B0ME2532.DOperator : CMLAcquired : 25 May 2021 2:26 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-01@B1E0696(S) Misc Info : 1@ Vial Number: 300.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2532.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2612.D Operator : RR Acquired : 26 May 2021 1:56 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-01RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 12 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2612.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2529.DOperator : CMLAcquired : 25 May 2021 2:03 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-02@B1E0696(S) Misc Info : 1@ Vial Number: 270.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2529.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2614.D Operator : RR Acquired : 26 May 2021 3:34 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-02RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 14 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 100000 105000 110000 Time Response_GOME2614.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2535.DOperator : CMLAcquired : 25 May 2021 3:12 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-03@B1E0696(S) Misc Info : 1@ Vial Number: 330.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2535.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2616.D Operator : RR Acquired : 26 May 2021 4:26 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-03RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 16 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2616.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2527.DOperator : CMLAcquired : 25 May 2021 1:41 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-04@B1E0696(S) Misc Info : 1@ Vial Number: 250.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07TimeResponse_Signal: B0ME2527.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2618.D Operator : RR Acquired : 26 May 2021 5:18 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-04RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 18 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2618.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2533.DOperator : CMLAcquired : 25 May 2021 2:49 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-05@B1E0696(S) Misc Info : 1@ Vial Number: 310.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0ME2533.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2624.D Operator : RR Acquired : 26 May 2021 7:53 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-05RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 24 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2624.D\FID1A File :V:\DATA\MAY21\052521\B0ME2534.DOperator : CMLAcquired : 25 May 2021 2:49 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-06@B1E0696(S) Misc Info : 1@ Vial Number: 320.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0ME2534.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2626.D Operator : RR Acquired : 26 May 2021 8:45 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-06RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 26 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 Time Response_GOME2626.D\FID1A File :V:\DATA\MAY21\052521\B0ME2536.DOperator : CMLAcquired : 25 May 2021 3:12 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-07@B1E0696(S) Misc Info : 1@ Vial Number: 340.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07TimeResponse_Signal: B0ME2536.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2628.D Operator : RR Acquired : 26 May 2021 9:36 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-07RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 28 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2628.D\FID1A File :V:\DATA\MAY21\052521.SEC\B0ME2531.DOperator : CMLAcquired : 25 May 2021 2:26 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103212-08@B1E0696(S) Misc Info : 1@ Vial Number: 290.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07 1.7e+07TimeResponse_Signal: B0ME2531.D\FID2B.CH File : C:\HPCHEM\1\DATA\2021\MAY21\052621\GOME2630.D Operator : RR Acquired : 26 May 2021 10:28 pm using AcqMethod GASBTEXE.M Instrument : GC7 Sample Name: 2103212-08RE1@ Misc Info : 1@B1E0737 GRO Solid Vial Number: 30 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 Time Response_GOME2630.D\FID1A Page 56 of 59 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLDYRDeluikuieiheluikuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 57 of 59 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG5HFHLSW/RJLQ%\-9=5HFHLSW5HYLHZHG%\’$Page 58 of 59 STLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr & TCLP CrSTLC Cr, Ni & TCLP Crall added at 5/25/21; SPPage 59 of 59 [TOC_1]Cover Page[ Oilfield Environmental & Compliance, Inc. Analytical Report Project: Pacific Petroleum Orcutt, CA 93457 P. O. Box 2646 Pacific Petroleum California Clarence Reynolds OEC Work Order:2103479 Report Date: June 09, 2021 16:44 NHC SLO, 2640 Broad StreetNumber: sparvin@oecusa.com Shahnaz Parvin, Project Manager Enclosed is an analytical report for the above referenced project. The samples included in this report were received on June 04, 2021 12:50 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. If you have any questions regarding this report, please do not hesitate to contact the undersigned. Authorized for release by: This laboratory is accredited in accordance with the recognised International Standard ISO /IEC 17025. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISOILAC-IAF CommuniquØ dated April 2017) 307 Roemer Way, Suite 300 Santa Maria, CA 93454 client.oec.com\reports CA-ELAP 2438, TNI 02666 TNI 2016 & ISO/IEC 17025:2017 www.oecusa.com Fax: Main: (805) 925-3376 (805) 922-4772 Page 1 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Sample ID Laboratory ID Client Matrix Date Sampled Sample Summary Date Received [TOC_1]Sample Summary[TOC] Lab Matrix Bottom East @ 12’2103479-01 06/03/2021 11:50 06/04/2021 12:50Solid Solid Bottom West @ 12’2103479-02 06/03/2021 11:55 06/04/2021 12:50Solid Solid [TOC_1]Sample Batch Preparation Summary[Sample Batch Preparation Summary Analysis Preparation Date/TimeBatch ID OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List 06/04/2021 16:24B1F0145 STLC Metals by ICP 6010B STLC 06/09/2021 08:56B1F0261 STLC Metals Extraction STLC Metals Extraction 06/07/2021 16:29B1F0229 Total Metals by CVAA Mercury Total EPA 7471A 06/07/2021 07:40B1F0194 Total Metals by ICP 6010B Total 06/07/2021 08:26B1F0197 Volatile Organic Compounds by GC/MS 8260B Full List 06/04/2021 12:21B1F0146 Volatile Organic TPH by GC/FID 8015 TPH-Gasoline 06/04/2021 10:34B1F0154 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 2 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 2 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA [TOC_1]2103479-01 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A06/07/21 16:25mg/kg B1F01941Mercury0.087 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B06/07/21 14:12mg/kg B1F01971Antimony2.3 "5.6 """"Arsenic 1.9 "120 """"Barium 0.93 ND """ ""Beryllium 0.47 ND """ ""Cadmium 0.23 "73 """"Chromium 0.47 N-02 "18 """"Cobalt 0.47 "47 """"Copper 0.93 "8.2 """"Lead 0.47 ND """ ""Molybdenum 0.47 "130 """"Nickel 0.47 ND """ ""Selenium 1.9 ND """ ""Silver 0.47 ND """ ""Thallium 0.93 "49 """"Vanadium 1.9 "65 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B06/09/21 14:34mg/L B1F02612Chromium0.020 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M06/04/21 17:01mg/kg B1F01541TPH Gasoline (C5-C12)4.5 """( 39 - 157 )92 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 3 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M06/05/21 12:12mg/kg B1F01451TPH Diesel (C13-C22)10 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )87 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 4 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 4 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B06/04/21 16:16mg/kg B1F01461Benzene0.050 ND """ ""Bromobenzene 0.050 ND """ ""Bromochloromethane 0.050 ND """ ""Bromodichloromethane 0.050 ND """ ""Bromoform 0.050 ND """ ""Bromomethane 0.050 ND """ ""n-Butylbenzene 0.050 ND """ ""sec-Butylbenzene 0.050 ND """ ""tert-Butylbenzene 0.050 ND """ ""Carbon tetrachloride 0.050 ND """ ""Chlorobenzene 0.050 ND """ ""Chloroethane 0.050 ND """ ""Chloroform 0.050 ND """ ""Chloromethane 0.050 ND """ ""2-Chlorotoluene 0.050 ND """ ""4-Chlorotoluene 0.050 ND """ ""Dibromochloromethane 0.050 ND """ ""1,2-Dibromo-3-chloropropane 0.050 ND """ ""1,2-Dibromoethane (EDB)0.050 ND """ ""Dibromomethane 0.050 ND """ ""1,2-Dichlorobenzene 0.050 ND """ ""1,3-Dichlorobenzene 0.050 ND """ ""1,4-Dichlorobenzene 0.050 ND """ ""Dichlorodifluoromethane 0.050 CCHI ND """ ""1,1-Dichloroethane 0.050 ND """ ""1,2-Dichloroethane 0.050 ND """ ""1,1-Dichloroethene 0.050 ND """ ""cis-1,2-Dichloroethene 0.050 ND """ ""trans-1,2-Dichloroethene 0.050 ND """ ""1,2-Dichloropropane 0.050 ND """ ""1,3-Dichloropropane 0.050 ND """ ""2,2-Dichloropropane 0.050 ND """ ""1,1-Dichloropropene 0.050 ND """ ""cis-1,3-Dichloropropene 0.050 ND """ ""trans-1,3-Dichloropropene 0.050 ND """ ""Ethylbenzene 0.050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 5 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 5 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom East @ 12’Sampled : 06/03/21 11:50 Lab ID : 2103479-01 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B06/04/21 16:16mg/kg B1F01461Hexachlorobutadiene0.050 ND """ ""4-Isopropyl Toluene 0.050 ND """ ""Isopropylbenzene 0.050 ND """ ""Methylene chloride 0.050 ND """ ""Naphthalene 0.050 ND """ ""n-Propylbenzene 0.050 ND """ ""Styrene 0.050 ND """ ""1,1,1,2-Tetrachloroethane 0.050 ND """ ""1,1,2,2-Tetrachloroethane 0.050 ND """ ""Tetrachloroethene (PCE)0.050 ND """ ""Toluene 0.050 ND """ ""1,2,3-Trichlorobenzene 0.050 ND """ ""1,2,4-Trichlorobenzene 0.050 ND """ ""1,1,1-Trichloroethane 0.050 ND """ ""1,1,2-Trichloroethane 0.050 ND """ ""Trichloroethene (TCE)0.050 ND """ ""Trichlorofluoromethane 0.050 ND """ ""1,2,3-Trichloropropane 0.050 ND """ ""1,2,4-Trimethylbenzene 0.050 ND """ ""1,3,5-Trimethylbenzene 0.050 ND """ ""Vinyl chloride 0.050 ND """ ""Xylenes (total)0.050 """( 74 - 122 )103 %Surrogate: Dibromofluoromethane """( 65 - 128 )99 %Surrogate: Toluene-d8 """( 75 - 121 )105 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 6 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 6 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA [TOC_1]2103479-02 (Solid)[ Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Total Metals by CVAA[TOC] Total Metals by CVAA ND EPA 7471A06/07/21 16:27mg/kg B1F01941Mercury0.092 [TOC_2]Total Metals by ICP[TOC] Total Metals by ICP ND EPA 6010B06/07/21 14:15mg/kg B1F01971Antimony2.4 "7.4 """"Arsenic 1.9 "160 """"Barium 0.96 ND """ ""Beryllium 0.48 ND """ ""Cadmium 0.24 "51 """"Chromium 0.48 N-02 "14 """"Cobalt 0.48 "63 """"Copper 0.96 "8.9 """"Lead 0.48 "0.57 """"Molybdenum 0.48 "88 """"Nickel 0.48 ND """ ""Selenium 1.9 ND """ ""Silver 0.48 ND """ ""Thallium 0.96 "52 """"Vanadium 1.9 "71 """"Zinc 1.9 [TOC_2]STLC Metals by ICP[TOC] STLC Metals by ICP ND STLC/EPA 6010B06/09/21 14:37mg/L B1F02612Chromium0.020 [TOC_2]Volatile Organic TPH by GC/FID[TOC] Volatile Organic TPH by GC/FID ND EPA 8015M06/04/21 17:29mg/kg B1F01541TPH Gasoline (C5-C12)4.4 """( 39 - 157 )95 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 7 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult [TOC_2]Semi-Volatile Organic TPH by GC/FID[TOC] Semi-Volatile Organic TPH by GC/FID ND EPA 8015M06/05/21 12:34mg/kg B1F01451TPH Diesel (C13-C22)9.9 ND """ ""TPH Motor Oil (C23-C40)50 """( 65 - 136 )90 %Surrogate: o-Terphenyl The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 8 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07 [TOC_2]Volatile Organic Compounds by GC/MS[TOC] Volatile Organic Compounds by GC/MS ND EPA 8260B06/04/21 15:48mg/kg B1F01461Benzene0.048 ND """ ""Bromobenzene 0.048 ND """ ""Bromochloromethane 0.048 ND """ ""Bromodichloromethane 0.048 ND """ ""Bromoform 0.048 ND """ ""Bromomethane 0.048 ND """ ""n-Butylbenzene 0.048 ND """ ""sec-Butylbenzene 0.048 ND """ ""tert-Butylbenzene 0.048 ND """ ""Carbon tetrachloride 0.048 ND """ ""Chlorobenzene 0.048 ND """ ""Chloroethane 0.048 ND """ ""Chloroform 0.048 ND """ ""Chloromethane 0.048 ND """ ""2-Chlorotoluene 0.048 ND """ ""4-Chlorotoluene 0.048 ND """ ""Dibromochloromethane 0.048 ND """ ""1,2-Dibromo-3-chloropropane 0.048 ND """ ""1,2-Dibromoethane (EDB)0.048 ND """ ""Dibromomethane 0.048 ND """ ""1,2-Dichlorobenzene 0.048 ND """ ""1,3-Dichlorobenzene 0.048 ND """ ""1,4-Dichlorobenzene 0.048 ND """ ""Dichlorodifluoromethane 0.048 CCHI ND """ ""1,1-Dichloroethane 0.048 ND """ ""1,2-Dichloroethane 0.048 ND """ ""1,1-Dichloroethene 0.048 ND """ ""cis-1,2-Dichloroethene 0.048 ND """ ""trans-1,2-Dichloroethene 0.048 ND """ ""1,2-Dichloropropane 0.048 ND """ ""1,3-Dichloropropane 0.048 ND """ ""2,2-Dichloropropane 0.048 ND """ ""1,1-Dichloropropene 0.048 ND """ ""cis-1,3-Dichloropropene 0.048 ND """ ""trans-1,3-Dichloropropene 0.048 ND """ ""Ethylbenzene 0.048 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 9 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Analytical Report for Samples Bottom West @ 12’Sampled : 06/03/21 11:55 Lab ID : 2103479-02 Matrix : Solid Sample ID : Sampled by : C Reynolds Field Data : NA Units Dilution Notes MethodAnalyzedRLBatchAnalyteResult R-07Volatile Organic Compounds by GC/MS (Continued) ND EPA 8260B06/04/21 15:48mg/kg B1F01461Hexachlorobutadiene0.048 ND """ ""4-Isopropyl Toluene 0.048 ND """ ""Isopropylbenzene 0.048 ND """ ""Methylene chloride 0.048 ND """ ""Naphthalene 0.048 ND """ ""n-Propylbenzene 0.048 ND """ ""Styrene 0.048 ND """ ""1,1,1,2-Tetrachloroethane 0.048 ND """ ""1,1,2,2-Tetrachloroethane 0.048 ND """ ""Tetrachloroethene (PCE)0.048 ND """ ""Toluene 0.048 ND """ ""1,2,3-Trichlorobenzene 0.048 ND """ ""1,2,4-Trichlorobenzene 0.048 ND """ ""1,1,1-Trichloroethane 0.048 ND """ ""1,1,2-Trichloroethane 0.048 ND """ ""Trichloroethene (TCE)0.048 ND """ ""Trichlorofluoromethane 0.048 ND """ ""1,2,3-Trichloropropane 0.048 ND """ ""1,2,4-Trimethylbenzene 0.048 ND """ ""1,3,5-Trimethylbenzene 0.048 ND """ ""Vinyl chloride 0.048 ND """ ""Xylenes (total)0.048 """( 74 - 122 )104 %Surrogate: Dibromofluoromethane """( 65 - 128 )102 %Surrogate: Toluene-d8 """( 75 - 121 )104 %Surrogate: 4-Bromofluorobenzene The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 10 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by CVAA - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0194 - EPA 7471A Prep[TOC] Batch B1F0194 - EPA 7471A Preparation: EPA 7471A Prep 06/07/21 07:40 Blank (B1F0194-BLK1) [TOC_3]Blank (B1F0194-BLK1)[TOC] Analyzed: 06/07/21 12:49 Mercury mg/kgND0.10 LCS (B1F0194-BS1) [TOC_3]LCS (B1F0194-BS1)[TOC] Analyzed: 06/07/21 12:53 Mercury mg/kg0.782 0.10 0.833 85-11594 LCS Dup (B1F0194-BSD1) [TOC_3]LCS Dup (B1F0194-BSD1)[TOC] Analyzed: 06/07/21 13:30 Mercury mg/kg0.859 0.10 0.833 2085-115103 9 Duplicate (B1F0194-DUP1)Source: 2103489-02 [TOC_3]Duplicate (B1F0194-DUP1)[TOC] Analyzed: 06/07/21 13:34 Mercury mg/kgND0.097 ND 20 Matrix Spike (B1F0194-MS1)Source: 2103489-02 [TOC_3]Matrix Spike (B1F0194-MS1)[TOC] Analyzed: 06/07/21 13:37 Mercury mg/kg0.827 0.091 0.755 ND 75-125110 Matrix Spike Dup (B1F0194-MSD1)Source: 2103489-02 [TOC_3]Matrix Spike Dup (B1F0194-MSD1)[TOC] Analyzed: 06/07/21 13:39 Mercury mg/kg0.839 0.089 0.742 ND 2075-125113 1 Post Spike (B1F0194-PS1)Source: 2103489-02 [TOC_3]Post Spike (B1F0194-PS1)[TOC] Analyzed: 06/07/21 13:41 Mercury ug/L5.52 25.0 0.00199 QL-0285-11522 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 11 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0197 - EPA 3050B[TOC] Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Blank (B1F0197-BLK1) [TOC_3]Blank (B1F0197-BLK1)[TOC] Analyzed: 06/07/21 13:30 Antimony mg/kgND2.5 Arsenic "ND 2.0 Barium "ND 1.0 Beryllium "ND 0.50 Cadmium "ND 0.25 Chromium "ND 0.50 Cobalt "ND 0.50 Copper "ND 1.0 Lead "ND 0.50 Molybdenum "ND 0.50 Nickel "ND 0.50 Selenium "ND 2.0 Silver "ND 0.50 Thallium "ND 1.0 Vanadium "ND 2.0 Zinc "ND 2.0 LCS (B1F0197-BS1) [TOC_3]LCS (B1F0197-BS1)[TOC] Analyzed: 06/07/21 13:35 Antimony mg/kg92.0 2.5 100 80-12092 Arsenic "97.2 2.0 100 80-12097 Barium "99.6 1.0 100 80-120100 Beryllium "95.1 0.50 100 80-12095 Cadmium "98.2 0.25 100 80-12098 Chromium "98.8 0.50 100 80-12099 Cobalt "99.2 0.50 100 80-12099 Copper "98.2 1.0 100 80-12098 Lead "100 0.50 100 80-120100 Molybdenum "96.0 0.50 100 80-12096 Nickel "99.6 0.50 100 80-120100 Selenium "96.4 2.0 100 80-12096 Silver "4.92 0.50 5.00 80-12098 Thallium "100 1.0 100 80-120100 Vanadium "96.6 2.0 100 80-12097 Zinc "98.6 2.0 100 80-12099 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 12 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 12 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 LCS Dup (B1F0197-BSD1) [TOC_3]LCS Dup (B1F0197-BSD1)[TOC] Analyzed: 06/07/21 13:37 Antimony mg/kg94.8 2.5 100 2080-12095 3 Arsenic "98.8 2.0 100 2080-12099 2 Barium "101 1.0 100 2080-120101 1 Beryllium "96.5 0.50 100 2080-12096 1 Cadmium "99.2 0.25 100 2080-12099 1 Chromium "100 0.50 100 2080-120100 1 Cobalt "100 0.50 100 2080-120100 1 Copper "99.8 1.0 100 2080-120100 2 Lead "101 0.50 100 2080-120101 1 Molybdenum "98.2 0.50 100 2080-12098 2 Nickel "101 0.50 100 2080-120101 1 Selenium "97.8 2.0 100 2080-12098 1 Silver "4.93 0.50 5.00 2080-12099 0.1 Thallium "102 1.0 100 2080-120102 1 Vanadium "98.0 2.0 100 2080-12098 1 Zinc "99.8 2.0 100 2080-120100 1 Duplicate (B1F0197-DUP1)Source: 2103489-01 [TOC_3]Duplicate (B1F0197-DUP1)[TOC] Analyzed: 06/07/21 13:52 Antimony mg/kgND2.4 ND 20 Arsenic "1.22 1.9 ND 20 Barium "21.0 0.97 22.9 208 Beryllium "ND 0.49 ND 20 Cadmium "ND 0.24 ND 20 Chromium "1.94 0.49 2.02 204 Cobalt "1.40 0.49 1.78 20 QR-0424 Copper "1.33 0.97 1.40 205 Lead "1.23 0.49 1.40 2013 Molybdenum "ND 0.49 ND 20 Nickel "1.31 0.49 1.34 202 Selenium "ND 1.9 ND 20 Silver "ND 0.49 ND 20 Thallium "ND 0.97 ND 20 Vanadium "3.86 1.9 4.18 208 Zinc "4.32 1.9 4.51 204 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 13 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Matrix Spike (B1F0197-MS1)Source: 2103489-01 [TOC_3]Matrix Spike (B1F0197-MS1)[TOC] Analyzed: 06/07/21 13:40 Antimony mg/kg70.3 2.3 93.4 ND 10-11675 Arsenic "93.3 1.9 93.4 ND 77-121100 Barium "119 0.93 93.4 22.9 30-169102 Beryllium "90.1 0.47 93.4 ND 86-11196 Cadmium "91.8 0.23 93.4 ND 81-11298 Chromium "96.8 0.47 93.4 2.02 75-129102 Cobalt "94.2 0.47 93.4 1.78 71-12199 Copper "96.2 0.93 93.4 1.40 68-135102 Lead "94.4 0.47 93.4 1.40 72-121100 Molybdenum "88.2 0.47 93.4 ND 70-11294 Nickel "95.2 0.47 93.4 1.34 73-121101 Selenium "90.1 1.9 93.4 ND 76-11697 Silver "4.56 0.47 4.67 ND 54-13298 Thallium "92.3 0.93 93.4 ND 64-12099 Vanadium "96.5 1.9 93.4 4.18 78-12499 Zinc "98.0 1.9 93.4 4.51 50-143100 Matrix Spike Dup (B1F0197-MSD1)Source: 2103489-01 [TOC_3]Matrix Spike Dup (B1F0197-MSD1)[TOC] Analyzed: 06/07/21 13:42 Antimony mg/kg70.4 2.4 95.8 ND 2010-11673 0.1 Arsenic "94.3 1.9 95.8 ND 2077-12198 1 Barium "116 0.96 95.8 22.9 2030-16997 3 Beryllium "91.2 0.48 95.8 ND 2086-11195 1 Cadmium "92.3 0.24 95.8 ND 2081-11296 0.6 Chromium "97.6 0.48 95.8 2.02 2075-129100 0.8 Cobalt "94.7 0.48 95.8 1.78 2071-12197 0.6 Copper "96.9 0.96 95.8 1.40 2068-135100 0.7 Lead "94.9 0.48 95.8 1.40 2072-12198 0.6 Molybdenum "88.6 0.48 95.8 ND 2070-11293 0.5 Nickel "95.5 0.48 95.8 1.34 2073-12198 0.3 Selenium "91.2 1.9 95.8 ND 2076-11695 1 Silver "4.64 0.48 4.79 ND 2054-13297 2 Thallium "93.1 0.96 95.8 ND 2064-12097 0.9 Vanadium "97.2 1.9 95.8 4.18 2078-12497 0.7 Zinc "103 1.9 95.8 4.51 2050-143103 5 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 14 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 14 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Total Metals by ICP - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0197 - EPA 6010B Preparation: EPA 3050B 06/07/21 08:26 Post Spike (B1F0197-PS1)Source: 2103489-01 [TOC_3]Post Spike (B1F0197-PS1)[TOC] Analyzed: 06/07/21 13:45 Antimony mg/L2.03 2.00 0.00248 75-125101 Arsenic "2.04 2.00 0.0178 75-125101 Barium "2.50 2.00 0.460 75-125102 Beryllium "1.96 2.00 0.00218 75-12598 Cadmium "2.00 2.00 -0.00308 75-125100 Chromium "2.07 2.00 0.0408 75-125101 Cobalt "2.06 2.00 0.0359 75-125101 Copper "2.06 2.00 0.0283 75-125102 Lead "2.07 2.00 0.0283 75-125102 Molybdenum "2.01 2.00 -0.00109 75-125101 Nickel "2.06 2.00 0.0271 75-125102 Selenium "1.99 2.00 -0.0103 75-12599 Silver "0.0945 0.100 -0.00169 75-12594 Thallium "2.03 2.00 -0.00407 75-125101 Vanadium "2.08 2.00 0.0842 75-125100 Zinc "2.10 2.00 0.0909 75-125101 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 15 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 15 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: STLC Metals by ICP - Quality Control[TOC_1]STLC Metals by IC Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0261 - EPA 3010A Leachate[TOC] Batch B1F0261 - STLC/EPA 6010B Preparation: EPA 3010A Leachate 06/09/21 08:56 Blank (B1F0261-BLK1) [TOC_3]Blank (B1F0261-BLK1)[TOC] Analyzed: 06/09/21 13:50 Chromium mg/LND0.010 LCS (B1F0261-BS1) [TOC_3]LCS (B1F0261-BS1)[TOC] Analyzed: 06/09/21 14:17 Chromium mg/L10.1 0.010 10.0 80-120101 LCS Dup (B1F0261-BSD1) [TOC_3]LCS Dup (B1F0261-BSD1)[TOC] Analyzed: 06/09/21 14:19 Chromium mg/L10.2 0.010 10.0 2080-120102 0.5 Duplicate (B1F0261-DUP1)Source: 2103218-01 [TOC_3]Duplicate (B1F0261-DUP1)[TOC] Analyzed: 06/09/21 14:27 Chromium mg/L1.22 0.020 1.22 200.08 Leach Fluid Blank (B1F0261-LBK1) [TOC_3]Leach Fluid Blank (B1F0261-LBK1)[TOC] Analyzed: 06/09/21 13:52 Chromium mg/LND0.020 Leach Fluid Blank (B1F0261-LBK2)Analyzed: 06/09/21 13:55 Chromium mg/LND0.020 Leach Fluid Blank (B1F0261-LBK3)Analyzed: 06/09/21 13:58 Chromium mg/LND0.020 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 16 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 16 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic TPH by GC/FID - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0154 - EPA 5035/5030B Solid GC[TOC] Batch B1F0154 - EPA 8015M Preparation: EPA 5035/5030B Solid GC 06/04/21 10:34 Blank (B1F0154-BLK1) [TOC_3]Blank (B1F0154-BLK1)[TOC] Analyzed: 06/04/21 12:45 TPH Gasoline (C5-C12)mg/kgND0.49 "0.123 39-157Surrogate: 4-Bromofluorobenzene 870.107 LCS (B1F0154-BS1) [TOC_3]LCS (B1F0154-BS1)[TOC] Analyzed: 06/04/21 11:48 TPH Gasoline (C5-C12)mg/kg1.38 0.50 0.998 68-139138 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1260.158 LCS Dup (B1F0154-BSD1) [TOC_3]LCS Dup (B1F0154-BSD1)[TOC] Analyzed: 06/04/21 12:17 TPH Gasoline (C5-C12)mg/kg1.29 0.50 1.00 2068-139128 7 "0.125 39-157Surrogate: 4-Bromofluorobenzene 1160.146 Duplicate (B1F0154-DUP1)Source: 2103455-02RE1 [TOC_3]Duplicate (B1F0154-DUP1)[TOC] Analyzed: 06/04/21 15:35 TPH Gasoline (C5-C12)mg/kgND0.50 0.113 20 "0.124 39-157Surrogate: 4-Bromofluorobenzene 920.113 Matrix Spike (B1F0154-MS1)Source: 2103429-02 [TOC_3]Matrix Spike (B1F0154-MS1)[TOC] Analyzed: 06/04/21 19:23 TPH Gasoline (C5-C12)mg/kg0.905 0.49 0.973 ND 10-17193 "0.122 39-157Surrogate: 4-Bromofluorobenzene 1090.132 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 17 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 17 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Semi-Volatile Organic TPH by GC/FID - Quality Control[TOC_1]Semi- Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0145 - EPA 3550C[TOC] Batch B1F0145 - EPA 8015M Preparation: EPA 3550C 06/04/21 09:14 Blank (B1F0145-BLK1) [TOC_3]Blank (B1F0145-BLK1)[TOC] Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22)mg/kgND10 TPH Motor Oil (C23-C40)"ND 50 "50.0 65-136Surrogate: o-Terphenyl 8341.5 LCS (B1F0145-BS1) [TOC_3]LCS (B1F0145-BS1)[TOC] Analyzed: 06/04/21 11:45 TPH Diesel (C13-C22)mg/kg43410 499 72-11587 TPH Motor Oil (C23-C40)"420 50 499 74-12684 "49.9 65-136Surrogate: o-Terphenyl 9245.8 LCS Dup (B1F0145-BSD1) [TOC_3]LCS Dup (B1F0145-BSD1)[TOC] Analyzed: 06/04/21 12:07 TPH Diesel (C13-C22)mg/kg44410 499 2072-11589 2 TPH Motor Oil (C23-C40)"441 50 499 2074-12688 5 "49.9 65-136Surrogate: o-Terphenyl 9446.7 Duplicate (B1F0145-DUP1)Source: 2103472-01 [TOC_3]Duplicate (B1F0145-DUP1)[TOC] Analyzed: 06/04/21 16:23 TPH Diesel (C13-C22)mg/kgND10 ND 20 TPH Motor Oil (C23-C40)"ND 50 ND 20 "49.9 65-136Surrogate: o-Terphenyl 8140.5 Matrix Spike (B1F0145-MS1)Source: 2103472-01 [TOC_3]Matrix Spike (B1F0145-MS1)[TOC] Analyzed: 06/04/21 15:37 TPH Diesel (C13-C22)mg/kg45210 498 ND 46-14791 TPH Motor Oil (C23-C40)"500 50 498 ND 35-171100 "49.8 65-136Surrogate: o-Terphenyl 8441.6 Matrix Spike Dup (B1F0145-MSD1)Source: 2103472-01 [TOC_3]Matrix Spike Dup (B1F0145-MSD1)[TOC] Analyzed: 06/04/21 16:00 TPH Diesel (C13-C22)mg/kg49610 498 ND 2046-147100 9 TPH Motor Oil (C23-C40)"517 50 498 ND 2035-171104 3 "49.8 65-136Surrogate: o-Terphenyl 8844.0 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 18 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 18 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control[TOC_1] Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte [TOC_2]Batch B1F0146 - EPA 5035/5030B Solid[TOC] Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1) [TOC_3]Blank (B1F0146-BLK1)[TOC] Analyzed: 06/04/21 11:32 Benzene mg/kgND0.0050 Bromobenzene "ND 0.0050 Bromochloromethane "ND 0.0050 Bromodichloromethane "ND 0.0050 Bromoform "ND 0.0050 Bromomethane "ND 0.0050 n-Butylbenzene "ND 0.0050 sec-Butylbenzene "ND 0.0050 tert-Butylbenzene "ND 0.0050 Carbon tetrachloride "ND 0.0050 Chlorobenzene "ND 0.0050 Chloroethane "ND 0.0050 Chloroform "ND 0.0050 Chloromethane "ND 0.0050 2-Chlorotoluene "ND 0.0050 4-Chlorotoluene "ND 0.0050 Dibromochloromethane "ND 0.0050 1,2-Dibromo-3-chloropropane "ND 0.0050 1,2-Dibromoethane (EDB)"ND 0.0050 Dibromomethane "ND 0.0050 1,2-Dichlorobenzene "ND 0.0050 1,3-Dichlorobenzene "ND 0.0050 1,4-Dichlorobenzene "ND 0.0050 Dichlorodifluoromethane "ND 0.0050 CCHI 1,1-Dichloroethane "ND 0.0050 1,2-Dichloroethane "ND 0.0050 1,1-Dichloroethene "ND 0.0050 cis-1,2-Dichloroethene "ND 0.0050 trans-1,2-Dichloroethene "ND 0.0050 1,2-Dichloropropane "ND 0.0050 1,3-Dichloropropane "ND 0.0050 2,2-Dichloropropane "ND 0.0050 1,1-Dichloropropene "ND 0.0050 cis-1,3-Dichloropropene "ND 0.0050 trans-1,3-Dichloropropene "ND 0.0050 Ethylbenzene "ND 0.0050 Hexachlorobutadiene "ND 0.0050 4-Isopropyl Toluene "ND 0.0050 Isopropylbenzene "ND 0.0050 Methylene chloride "ND 0.0050 Naphthalene "ND 0.0050 n-Propylbenzene "ND 0.0050 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 19 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 19 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Blank (B1F0146-BLK1)Analyzed: 06/04/21 11:32 Styrene mg/kgND0.0050 1,1,1,2-Tetrachloroethane "ND 0.0050 1,1,2,2-Tetrachloroethane "ND 0.0050 Tetrachloroethene (PCE)"ND 0.0050 Toluene "ND 0.0050 1,2,3-Trichlorobenzene "ND 0.0050 1,2,4-Trichlorobenzene "ND 0.0050 1,1,1-Trichloroethane "ND 0.0050 1,1,2-Trichloroethane "ND 0.0050 Trichloroethene (TCE)"ND 0.0050 Trichlorofluoromethane "ND 0.0050 1,2,3-Trichloropropane "ND 0.0050 1,2,4-Trimethylbenzene "ND 0.0050 1,3,5-Trimethylbenzene "ND 0.0050 Vinyl chloride "ND 0.0050 Xylenes (total)"ND 0.0050 "0.0498 74-122Surrogate: Dibromofluoromethane 1040.0516 "0.0498 65-128Surrogate: Toluene-d8 1010.0503 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 1060.0529 LCS (B1F0146-BS1) [TOC_3]LCS (B1F0146-BS1)[TOC] Analyzed: 06/04/21 09:47 Benzene mg/kg0.0406 0.0050 0.0398 70-131102 Bromobenzene "0.0466 0.0050 0.0398 74-130117 Bromochloromethane "0.0399 0.0050 0.0398 64-133100 Bromodichloromethane "0.0445 0.0050 0.0398 69-137112 Bromoform "0.0447 0.0050 0.0398 55-132112 Bromomethane "0.0407 0.0050 0.0398 10-142102 n-Butylbenzene "0.0476 0.0050 0.0398 64-156120 sec-Butylbenzene "0.0493 0.0050 0.0398 75-155124 tert-Butylbenzene "0.0482 0.0050 0.0398 74-144121 Carbon tetrachloride "0.0442 0.0050 0.0398 67-135111 Chlorobenzene "0.0445 0.0050 0.0398 73-134112 Chloroethane "0.0390 0.0050 0.0398 10-16798 Chloroform "0.0412 0.0050 0.0398 69-124104 Chloromethane "0.0297 0.0050 0.0398 34-13675 2-Chlorotoluene "0.0454 0.0050 0.0398 75-135114 4-Chlorotoluene "0.0460 0.0050 0.0398 70-138116 Dibromochloromethane "0.0439 0.0050 0.0398 67-135110 1,2-Dibromo-3-chloropropane "0.0435 0.0050 0.0398 41-149109 1,2-Dibromoethane (EDB)"0.0409 0.0050 0.0398 68-131103 Dibromomethane "0.0433 0.0050 0.0398 61-140109 1,2-Dichlorobenzene "0.0458 0.0050 0.0398 76-136115 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 20 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 20 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS (B1F0146-BS1)Analyzed: 06/04/21 09:47 1,3-Dichlorobenzene mg/kg0.0462 0.0050 0.0398 76-138116 1,4-Dichlorobenzene "0.0457 0.0050 0.0398 72-132115 Dichlorodifluoromethane "0.0210 0.0050 0.0398 CCFH10-15553 1,1-Dichloroethane "0.0389 0.0050 0.0398 63-13998 1,2-Dichloroethane "0.0416 0.0050 0.0398 64-126104 1,1-Dichloroethene "0.0342 0.0050 0.0398 52-16786 cis-1,2-Dichloroethene "0.0401 0.0050 0.0398 70-135101 trans-1,2-Dichloroethene "0.0392 0.0050 0.0398 67-14799 1,2-Dichloropropane "0.0406 0.0050 0.0398 68-131102 1,3-Dichloropropane "0.0405 0.0050 0.0398 64-128102 2,2-Dichloropropane "0.0432 0.0050 0.0398 63-154109 1,1-Dichloropropene "0.0393 0.0050 0.0398 68-13899 cis-1,3-Dichloropropene "0.0416 0.0050 0.0398 72-134105 trans-1,3-Dichloropropene "0.0437 0.0050 0.0398 69-132110 Ethylbenzene "0.0449 0.0050 0.0398 68-136113 Hexachlorobutadiene "0.0546 0.0050 0.0398 72-198137 4-Isopropyl Toluene "0.0504 0.0050 0.0398 74-150127 Isopropylbenzene "0.0473 0.0050 0.0398 71-149119 Methylene chloride "0.0346 0.0050 0.0398 51-12787 Naphthalene "0.0482 0.0050 0.0398 57-158121 n-Propylbenzene "0.0474 0.0050 0.0398 70-143119 Styrene "0.0456 0.0050 0.0398 68-138115 1,1,1,2-Tetrachloroethane "0.0459 0.0050 0.0398 76-130115 1,1,2,2-Tetrachloroethane "0.0399 0.0050 0.0398 60-136100 Tetrachloroethene (PCE)"0.0443 0.0050 0.0398 73-138111 Toluene "0.0430 0.0050 0.0398 72-128108 1,2,3-Trichlorobenzene "0.0507 0.0050 0.0398 61-166127 1,2,4-Trichlorobenzene "0.0502 0.0050 0.0398 71-158126 1,1,1-Trichloroethane "0.0424 0.0050 0.0398 71-135107 1,1,2-Trichloroethane "0.0414 0.0050 0.0398 64-132104 Trichloroethene (TCE)"0.0442 0.0050 0.0398 74-139111 Trichlorofluoromethane "0.0429 0.0050 0.0398 30-156108 1,2,3-Trichloropropane "0.0452 0.0050 0.0398 67-123114 1,2,4-Trimethylbenzene "0.0454 0.0050 0.0398 68-134114 1,3,5-Trimethylbenzene "0.0461 0.0050 0.0398 71-140116 Vinyl chloride "0.0326 0.0050 0.0398 43-14482 Xylenes (total)"0.133 0.0050 0.119 69-138112 "0.0497 74-122Surrogate: Dibromofluoromethane 1060.0525 "0.0497 65-128Surrogate: Toluene-d8 1040.0517 "0.0497 75-121Surrogate: 4-Bromofluorobenzene 1070.0530 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 21 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 21 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1) [TOC_3]LCS Dup (B1F0146-BSD1)[TOC] Analyzed: 06/04/21 10:13 Benzene mg/kg0.0423 0.0050 0.0400 2070-131106 4 Bromobenzene "0.0498 0.0050 0.0400 2074-130124 7 Bromochloromethane "0.0412 0.0050 0.0400 2064-133103 3 Bromodichloromethane "0.0455 0.0050 0.0400 2069-137114 2 Bromoform "0.0458 0.0050 0.0400 2055-132115 2 Bromomethane "0.0391 0.0050 0.0400 2010-14298 4 n-Butylbenzene "0.0476 0.0050 0.0400 2064-156119 0.1 sec-Butylbenzene "0.0508 0.0050 0.0400 2075-155127 3 tert-Butylbenzene "0.0496 0.0050 0.0400 2074-144124 3 Carbon tetrachloride "0.0456 0.0050 0.0400 2067-135114 3 Chlorobenzene "0.0457 0.0050 0.0400 2073-134114 3 Chloroethane "0.0394 0.0050 0.0400 2010-16798 1 Chloroform "0.0421 0.0050 0.0400 2069-124105 2 Chloromethane "0.0308 0.0050 0.0400 2034-13677 4 2-Chlorotoluene "0.0452 0.0050 0.0400 2075-135113 0.4 4-Chlorotoluene "0.0468 0.0050 0.0400 2070-138117 2 Dibromochloromethane "0.0463 0.0050 0.0400 2067-135116 5 1,2-Dibromo-3-chloropropane "0.0461 0.0050 0.0400 2041-149115 6 1,2-Dibromoethane (EDB)"0.0422 0.0050 0.0400 2068-131105 3 Dibromomethane "0.0459 0.0050 0.0400 2061-140115 6 1,2-Dichlorobenzene "0.0472 0.0050 0.0400 2076-136118 3 1,3-Dichlorobenzene "0.0489 0.0050 0.0400 2076-138122 6 1,4-Dichlorobenzene "0.0472 0.0050 0.0400 2072-132118 3 Dichlorodifluoromethane "0.0228 0.0050 0.0400 20 CCFH10-15557 8 1,1-Dichloroethane "0.0405 0.0050 0.0400 2063-139101 4 1,2-Dichloroethane "0.0425 0.0050 0.0400 2064-126106 2 1,1-Dichloroethene "0.0347 0.0050 0.0400 2052-16787 2 cis-1,2-Dichloroethene "0.0420 0.0050 0.0400 2070-135105 5 trans-1,2-Dichloroethene "0.0401 0.0050 0.0400 2067-147100 2 1,2-Dichloropropane "0.0430 0.0050 0.0400 2068-131107 6 1,3-Dichloropropane "0.0426 0.0050 0.0400 2064-128106 5 2,2-Dichloropropane "0.0446 0.0050 0.0400 2063-154111 3 1,1-Dichloropropene "0.0406 0.0050 0.0400 2068-138102 3 cis-1,3-Dichloropropene "0.0434 0.0050 0.0400 2072-134108 4 trans-1,3-Dichloropropene "0.0454 0.0050 0.0400 2069-132114 4 Ethylbenzene "0.0470 0.0050 0.0400 2068-136118 5 Hexachlorobutadiene "0.0549 0.0050 0.0400 2072-198137 0.5 4-Isopropyl Toluene "0.0514 0.0050 0.0400 2074-150128 2 Isopropylbenzene "0.0499 0.0050 0.0400 2071-149125 5 Methylene chloride "0.0360 0.0050 0.0400 2051-12790 4 Naphthalene "0.0511 0.0050 0.0400 2057-158128 6 n-Propylbenzene "0.0466 0.0050 0.0400 2070-143116 2 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 22 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 22 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 LCS Dup (B1F0146-BSD1)Analyzed: 06/04/21 10:13 Styrene mg/kg0.0479 0.0050 0.0400 2068-138120 5 1,1,1,2-Tetrachloroethane "0.0490 0.0050 0.0400 2076-130123 7 1,1,2,2-Tetrachloroethane "0.0417 0.0050 0.0400 2060-136104 5 Tetrachloroethene (PCE)"0.0454 0.0050 0.0400 2073-138114 3 Toluene "0.0439 0.0050 0.0400 2072-128110 2 1,2,3-Trichlorobenzene "0.0520 0.0050 0.0400 2061-166130 3 1,2,4-Trichlorobenzene "0.0512 0.0050 0.0400 2071-158128 2 1,1,1-Trichloroethane "0.0432 0.0050 0.0400 2071-135108 2 1,1,2-Trichloroethane "0.0448 0.0050 0.0400 2064-132112 8 Trichloroethene (TCE)"0.0448 0.0050 0.0400 2074-139112 1 Trichlorofluoromethane "0.0430 0.0050 0.0400 2030-156107 0.1 1,2,3-Trichloropropane "0.0463 0.0050 0.0400 2067-123116 3 1,2,4-Trimethylbenzene "0.0459 0.0050 0.0400 2068-134115 1 1,3,5-Trimethylbenzene "0.0465 0.0050 0.0400 2071-140116 0.9 Vinyl chloride "0.0338 0.0050 0.0400 2043-14484 3 Xylenes (total)"0.139 0.0050 0.120 2069-138116 4 "0.0500 74-122Surrogate: Dibromofluoromethane 1040.0519 "0.0500 65-128Surrogate: Toluene-d8 1020.0510 "0.0500 75-121Surrogate: 4-Bromofluorobenzene 1060.0530 Duplicate (B1F0146-DUP1)ISlowSSource: 2103474-01 [TOC_3]Duplicate (B1F0146-DUP1)[TOC] Analyzed: 06/04/21 15:22 Benzene mg/kgND0.0050 ND 20 Bromobenzene "ND 0.0050 ND 20 Bromochloromethane "ND 0.0050 ND 20 Bromodichloromethane "ND 0.0050 ND 20 Bromoform "ND 0.0050 ND 20 Bromomethane "ND 0.0050 ND 20 n-Butylbenzene "ND 0.0050 ND 20 sec-Butylbenzene "ND 0.0050 ND 20 tert-Butylbenzene "ND 0.0050 ND 20 Carbon tetrachloride "ND 0.0050 ND 20 Chlorobenzene "ND 0.0050 ND 20 Chloroethane "ND 0.0050 ND 20 Chloroform "ND 0.0050 ND 20 Chloromethane "ND 0.0050 ND 20 2-Chlorotoluene "ND 0.0050 ND 20 4-Chlorotoluene "ND 0.0050 ND 20 Dibromochloromethane "ND 0.0050 ND 20 1,2-Dibromo-3-chloropropane "ND 0.0050 ND 20 1,2-Dibromoethane (EDB)"ND 0.0050 ND 20 Dibromomethane "ND 0.0050 ND 20 1,2-Dichlorobenzene "ND 0.0050 ND 20 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 23 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 23 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Batch B1F0146 - EPA 8260B Preparation: EPA 5035/5030B Solid 06/04/21 09:21 Duplicate (B1F0146-DUP1)ISlowSSource: 2103474-01 Analyzed: 06/04/21 15:22 1,3-Dichlorobenzene mg/kgND0.0050 ND 20 1,4-Dichlorobenzene "ND 0.0050 ND 20 Dichlorodifluoromethane "ND 0.0050 ND 20 CCHI 1,1-Dichloroethane "ND 0.0050 ND 20 1,2-Dichloroethane "ND 0.0050 ND 20 1,1-Dichloroethene "ND 0.0050 ND 20 cis-1,2-Dichloroethene "ND 0.0050 ND 20 trans-1,2-Dichloroethene "ND 0.0050 ND 20 1,2-Dichloropropane "ND 0.0050 ND 20 1,3-Dichloropropane "ND 0.0050 ND 20 2,2-Dichloropropane "ND 0.0050 ND 20 1,1-Dichloropropene "ND 0.0050 ND 20 cis-1,3-Dichloropropene "ND 0.0050 ND 20 trans-1,3-Dichloropropene "ND 0.0050 ND 20 Ethylbenzene "ND 0.0050 ND 20 Hexachlorobutadiene "ND 0.0050 ND 20 4-Isopropyl Toluene "ND 0.0050 ND 20 Isopropylbenzene "ND 0.0050 ND 20 Methylene chloride "ND 0.0050 ND 20 Naphthalene "ND 0.0050 ND 20 n-Propylbenzene "ND 0.0050 ND 20 Styrene "ND 0.0050 ND 20 1,1,1,2-Tetrachloroethane "ND 0.0050 ND 20 1,1,2,2-Tetrachloroethane "ND 0.0050 ND 20 Tetrachloroethene (PCE)"ND 0.0050 ND 20 Toluene "ND 0.0050 ND 20 1,2,3-Trichlorobenzene "ND 0.0050 ND 20 1,2,4-Trichlorobenzene "ND 0.0050 ND 20 1,1,1-Trichloroethane "ND 0.0050 ND 20 1,1,2-Trichloroethane "ND 0.0050 ND 20 Trichloroethene (TCE)"ND 0.0050 ND 20 Trichlorofluoromethane "ND 0.0050 ND 20 1,2,3-Trichloropropane "ND 0.0050 ND 20 1,2,4-Trimethylbenzene "ND 0.0050 ND 20 1,3,5-Trimethylbenzene "ND 0.0050 ND 20 Vinyl chloride "ND 0.0050 ND 20 Xylenes (total)"ND 0.0050 ND 20 "0.0498 74-122Surrogate: Dibromofluoromethane 1080.0538 "0.0498 65-128Surrogate: Toluene-d8 1020.0509 "0.0498 75-121Surrogate: 4-Bromofluorobenzene 1020.0506 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 24 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 24 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Sample Method Summary Laboratory & CertificationMethodAnalysisMatrix Semi-Volatile Organic TPH by GC/FID EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP,NELAP8015 Diesel & Motor Oil List Solid EPA 8015M OEC, Internal8015 Diesel & Motor Oil List Solid EPA 8015M OEC, CA-ELAP,NELAP8015 Diesel & Motor Oil List Solid STLC Metals by ICP STLC/EPA 6010B OEC, Internal6010B STLC Chromium Solid STLC Metals Extraction STLC OEC, InternalSTLC Metals Extraction Water Total Metals by CVAA EPA 7471A OEC, InternalMercury Total EPA 7471A Solid Total Metals by ICP EPA 6010B OEC, CA-ELAP,NELAP6010B Total Antimony Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Arsenic Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Barium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Beryllium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Cadmium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Chromium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Cobalt Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Copper Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Lead Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Molybdenum Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Nickel Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Selenium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Silver Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Thallium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Vanadium Solid EPA 6010B OEC, CA-ELAP,NELAP6010B Total Zinc Solid Volatile Organic Compounds by GC/MS EPA 8260B OEC, CA-ELAP,NELAP8260B Full List Solid EPA 8260B OEC, Internal8260B Full List Solid Volatile Organic TPH by GC/FID EPA 8015M OEC, Internal8015 TPH-Gasoline Solid The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 25 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 25 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: Notes and Definitions [TOC_1]Notes and Definitions[TOC] DefinitionQualifier MDL Relative Percent DifferenceRPD Analyte NOT DETECTED at or above the method limit (MDL)ND Method Detection Limit Reporting Limit (Quantitation Limit)RL CCFH The CCV for this analyte failed high. Results for this analyte may be biased high. CCHI The CCV for this analyte failed high. Analyte result is ND. Data is not impacted. ISlowS The internal standard associated with this sample fails the method criteria on the low side. Results may be biased high. N-02 Analyte concentration below TTLC but above 10x STLC. QL-02 The spike recovery is outside the control limits. QR-04 The RPD exceeded the QC control limits. R-07 Reporting limits are at or below state/federal hazardous waste criteria limits. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 26 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 26 of 32 Project: Project Number: Project Manager: Pacific Petroleum California P. O. Box 2646 NHC SLO, 2640 Broad Street Clarence Reynolds Pacific Petroleum 06/09/2021 16:44Orcutt CA, 93457 Oilfield Environmental & Compliance, Inc. 2103479 WO & Reported: [TOC_1]Other Documents[ The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 27 of 31 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 922-4772 FAX: (805) 925-3376www.oecusa.com client.oec.com\reportsClient Connect:CA-ELAP 2438, TNI02666 Page 27 of 32 File : C:\MSDCHEM\1\DATA\JUN21\060521\B0MF0512.DOperator : CMLAcquired : 05 Jun 2021 12:12 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103479-01@B1F0145(S) Misc Info : 1@ Vial Number: 100.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07TimeResponse_Signal: B0MF0512.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\JUN21\060421\DOMF0414.DOperator : RRAcquired : 4 Jun 2021 5:01 pm using AcqMethod GAS-BTEX.MInstrument : GC4Sample Name: 2103479-01@1:10 prep Misc Info : 1@ Vial Number: 140.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50500010000150002000025000300003500040000450005000055000600006500070000750008000085000TimeResponse_DOMF0414.D\FID1A File : C:\MSDCHEM\1\DATA\JUN21\060521\B0MF0514.DOperator : CMLAcquired : 05 Jun 2021 12:34 pm using AcqMethod TPH01CX.MInstrument : GC15 Sample Name: 2103479-02@B1F0145(S) Misc Info : 1@ Vial Number: 120.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50100000020000003000000400000050000006000000700000080000009000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07TimeResponse_Signal: B0MF0514.D\FID1A.CH File : C:\HPCHEM\1\DATA\2021\JUN21\060421\DOMF0415.DOperator : RRAcquired : 4 Jun 2021 5:29 pm using AcqMethod GAS-BTEX.MInstrument : GC4Sample Name: 2103479-02@1:10 prep Misc Info : 1@B1F0154 GRO Solid Vial Number: 150.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.505000100001500020000250003000035000400004500050000550006000065000700007500080000TimeResponse_DOMF0415.D\FID1A Page 28 of 32 BUHFHLSWVDPSOHRHFFRPLQGH[SKS6DPSOH5HFHLSW:RUN2UGHU5HYLHZLV&RPSOHWH:RUN2UGHU5HIUHVK&OLHQW1DPH7HPS&5HIULJHUDWRUV&2&5HFHLYHG/RJLQ3DFLILF3HWUROHXP&DOLIRUQLDemuekuieihemuekuieih5HFRUGHG&RUUHFWHG$FFHSWDEOH5DQJH&WR&6HH([FHSWLRQ1RWHV%HORZ6DPSOH7UDQVSRUW2(&&RXULHU6DPSOHU$IWHU+RXUV’URS2II’HOLYHU\2WKHUWKDQ2(&6KLSPHQW&DUULHU7UDFNLQJ&XVWRG\6HDOV1RQH3UHVHQW&RROHUV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH6DPSOHV3UHVHQW,QWDFW3UHVHQW1RW,QWDFW1RQH&RQGLWLRQ3UHVHUYDWLRQ<HV1R1$5HFHLYHG2Q,FH:LWKLQ5DQJH$FFHSWDEOH&RPSOHWHG&2&V5HFHLYHGZLWK6DPSOHV5HFHLYHG2XWVLGH5DQJH$FFHSWDEOH&RUUHFW&RQWDLQHUV3UHVHUYHIRU$QDO\VLV’LUHFWIURP)LHOGRQ,FH&RQWDLQHUV,QWDFWDQG*RRG&RQGLWLRQ$PELHQW$LURU)LOWHU0DWUL[&RQWDLQHU/DEHOV&RQVLVWHQWZLWK&2&5HFHLYHG$PELHQW3ODFHGRQ,FH2(&3UHVHUYDWLRQ$GGHG6DPSOH7HPSHUDWXUH$FFHWDEOHIRU$QDO\VLV6DPSOH4XDQWLW\6XIILFHQW5HFHLYHG2XWVLGH5DQJH>([FHSWLRQ@,QVXIILFLHQW,FHRU8QNQRZQ([FHVVLYH)UHH/LTXLGPage 29 of 32 BUHFHLSWVDPSOHRHFFRPLQGH[SKS&RQWDLQHUV&2&&KDQJHV$QG2U&RUUHFWLRQV&RWDQLQHU,’&2&&RQWDLQHU’HVFULSWLRQ+RPH0DWUL[3UHVHUYDWLYHS+&KORULQH6XOIXU&RPPHQWV$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG$R]*ODVV:0)ULGJH:DON,Q6ROLG%P/92$)UHH]HU92$6ROLG5HFHLSW/RJLQ%\’$5HFHLSW5HYLHZHG%\$00Page 30 of 32 samples taken and received 6/4/2021 per client confirmation MLSPage 31 of 32 samples taken and received 6/4/2021 per client confirmation MLS01- added STLC Cr02- added STLC Cr; SP 6/7/21Page 32 of 32 1 From:Bliss, Matheson Sent:Tuesday, October 19, 2021 4:57 PM To:Daniel Ringstmeyer; Clarence Reynolds Cc:Maggio, Rodger; John Hochleutner Subject:2600 Broad St SLO Closure Report Dan and Clarence, Please further clarify site investigation activities with a revised closure report with the items listed below. Feel free to call me if I have not made my questions clear. 1. What was the control sample taken 3/25? Where was it collected, describe in the report. 2. SECOND TIME: analyticals state a sample was collected from Soil Pile E of the tank excavation, yet no data has been added to the data table with the rest of the results from same sampling date- describe why? Why was it originally stated that a sample could not be collected from Soil Pile E. 3. “Tk Bot E End @8’” is listed twice on figure- revise for “Tk Bot W End @8’”. 4. Add STLC/TCLP data for samples taken 3/25 including STLC of 56 for lead from “sump Tr W”. 5. Tank excavation on figure 1 still has data points for concrete slab removal including NW, NE, SW, and SE Corners- remove from tank excavation on figure or better clarify where samples were collected from in body of report. 6. Where is tabulated data for “Sump Trench West”/ lab ID 2103032-07 from page 4 of report? Revise if it is supposed to be referencing 2103032-01. I see analyticals for 2103032-01 through -06 in report but not on data tables. Add data table for these soil samples. On the figure there is both a “Sump T. West Wall Sample” and a “Sump Trench W. Side Sample”. It is very hard to determine which sample is from which sampling date and the corresponding analyticals- further clarify with analytical sample number OR sampling date on figure. 7. Add description of asbestos testing of tile and brick to report from analyticals dated 4/23. 8. Page 4 of report states a concrete slab was removed and hydrocarbon impacted soil underneath the slab was most likely from the removed fuel tank- is this the same fuel tank at the south end of the site? If so, there is potentially hydrocarbon impacted soil in the middle of the two excavations remaining? Further explain. Page 5 of the report states “The area to the west and below the tanks..”, was there a second tank that was removed? 9. Do the dashed lines on figure next to the trench excavation represent soil stockpiles? If so, label. What is the dashed line north of the tank excavation on the figure? 10. On page 5 of report it states “two verification samples were taken from excavation floor approximately 4’ east and west of center”. Are these samples the same as “bot east @12’” and Bot west @12’”? Where are they on the figure? I see a “top of concrete, center (-7’)Sample” and a “below concrete (-10)” but no samples labeled at 12’. 11. SECOND TIME: add further detail to data tables explaining area of site samples are from (e.g. pg 29 of report, add title stating “concrete slab” or “extended trench excavation”, etc.; “NW Corner” sample could be confused with tank excavation samples). Revise data tables or add a column for sampling date instead of date when analytical results were received. Add data table numbers to more easily reference. 12. It would be helpful to only attach the analytical results that include the additional testing (STLC/TCLP) instead of both the original report and the additional report unless there is information on the original report that is not also on the additional analytical report. Thank you, Mattie 2 Matheson Bliss Hazardous Materials Coordinator Fire Department Fire Prevention E mbliss@slocity.org T 805.781.7383 C 805.540.4413 slocity.org Stay connected with the City by signing up for e-notifications From: TransferBigFiles <DoNotReply@TransferBigFiles.com> On Behalf Of Ringstmeyer, Daniel Sent: Thursday, October 7, 2021 3:50 PM To: Bliss, Matheson <mbliss@slocity.org> Subject: TransferBigFiles.com - Files have been sent to you! This message is from an External Source. Use caution when deciding to open attachments, click links, or respond. TransferBigFiles.com - Files have been sent to you! You have been sent one or more files through the TransferBigFiles.com service. If you were not expecting to receive any files, please use caution before downloading anything to your computer. Go to Download Page » (link expires 11/6/2021 7:00:00 AM) Message from sender: Attached is the Revised Closure Report for 2600 Broad Street which incorporates the requested information for Matty. Thanks, Dan 2021-10-07 - My Transfer 1 Files - 36 MB 3 2600 Broad St. Closure Rpt Rev. 1.pdf 1 From:Bliss, Matheson Sent:Tuesday, July 13, 2021 8:49 AM To:Clarence Reynolds; Daniel Ringstmeyer Cc:William Sarten; John Hochleutner; Maggio, Rodger Subject:RE: NHC SLO 2600 Broad Street Closure Report Hi Clarence, Thank you for the response. Dan, Could you please incorporate this into the closure report and add some additional information? I still only see one figure with 6 sample locations noted. Please add figures for the Sump and Fire Trench (Originally, samples were taken from the West Wall of the Sump Trench and at the bottom of the South End of the trench (OEC Lab ID#s 2101841-07,08). After data showed further excavation was required and carried out, a sample was taken from the Sump Trench West side (OEC Lab ID# 2103032-01) in the middle of its length because that is where most of the brick was. A sample was also taken from the bottom center of the trench (OEC Lab ID# 21020302-03). This Process was repeated for the Fire Trench with the inclusion of a sample on the East side of the trench were the material seemed to be consistent along the length of both trenches.) Add a figure for the concrete excavation (Five samples were taken from the floor of the excavation. See OEC Lab ID#s 2102742-01 through -05. The sample locations are as follows: NW Corner @ 8’, NE Corner @8’, SW Corner @ 8’, SE Corner @ 8’ and the center of the excavation @ 8’….. Once it was believed that all contaminated material was removed two verification samples were taken from the excavation floor approximately 4’ East and West from the center where the highest amount of petroleum had been present). Add a data table for the tank slurry and coating (The tank had been filled with a concrete slurry. There was also a thin layer of what appeared to be petroleum on the outside of the tank. Both the coating and slurry were sampled. See OEC Lab ID#s 2101909-01 and 2102464-01).Clarify in the data tables which area the samples were collected from (e.g. the bins in the data tables on pg 24, 26, and 27 were excavated from which area of the site; the soil sample “N TK Wall” on pg 28 is referring to which excavation?). Rectify information on the diesel tank soil pile. It was stated only three sides of the soil pile were sampled; however, per table on pg 29, four soil pile samples were collected (A sample was not taken from the East side as it was too close to the mouth of the excavation and unsafe… however there is a “Soil Pile E” sample.) Please confirm site location on all tables. Further clarify contaminants of concern if there was no Phase I performed for the site. In the diesel tank excavation, if groundwater was observed infiltrating the excavation, was a sample collected and what are the results? Thank you, Matheson Bliss Hazardous Materials Coordinator Fire Department Fire Prevention E mbliss@slocity.org T 805.781.7383 C 805.540.4413 slocity.org Stay connected with the City by signing up for e-notifications 2 From: Clarence Reynolds <c.reynolds@ppcinc.biz> Sent: Friday, June 18, 2021 2:56 PM To: Bliss, Matheson <mbliss@slocity.org> Cc: William Sarten <w.sarten@ppcinc.biz>; John Hochleutner <john@ppcinc.biz> Subject: NHC SLO 2600 Broad Street Closure Report This message is from an External Source. Use caution when deciding to open attachments, click links, or respond. Hi Mattie, I hope this gives you a better idea of how the project proceeded. Unfortunately, the Diesel Tank Excavation and Trench area have been backfilled so no pictures are available. Please let me know if you need more detail. 1. Describe the two distinct excavations (diesel tank and concrete structure), the trenches (noted on 4/6 data table), and soil piles and bins that are also noted on the data tables. Add additional figures detailing these areas and specific sampling locations. Diesel Tank Excavation: OEC Lab ID# 2101841-01 through 04 – Tank Wall Samples were taken at depth of 4’ in the center of each wall. 2101841-05 & 06 Tank Bottom Samples were taken at a depth of 8’ at the inlet and outlet ends of the tank. These samples were located at the bottom center of the East and West ends of the excavation approximately 1’ from the East and West walls respectively. The sample locations can be seen on page 9 of the closure report. The soil excavated from the diesel tank removal generated a pile approximately 5’ in height, 8’ in length and 4’ in width. Composite samples were taken from the North, South and West sides of the pile. This was done by taking three equal amounts of material from halfway up each side of the pile at intervals of about 1’5” and a depth of about 6”. These aliquots were mixed into three composite samples representing the three sides of the pile. A sample was not taken from the East side as it was too close to the mouth of the excavation and unsafe. Trenches: A trench was dug approximately 3’ deep to accommodate a water line. A pile of soil and brick was generated. It was approximately 3’ in height, 6’ in length and 4’ in width. A composite sample was taken from the pile by taking six equal amounts of material from half way up the pile (1.5’) at 2’ intervals and a depth of approximately 6”. These aliquots were combined into a single sample. As the excavation continued, the trench was segregated into two sections for sampling. This was done because half the length of the excavated material was composed of soil and the other length contained brick as well as soil. The length containing only soil was dubbed “Fire Trench” and the other “Sump Trench”. Originally, samples were taken from the West Wall of the Sump Trench and at the bottom of the South End of the trench (OEC Lab ID#s 2101841-07,08). After data showed further excavation was required and carried out, a sample was taken from the Sump Trench West side (OEC Lab ID# 2103032-01) in the middle of its length because that is where most of the brick was. A sample was also taken from the bottom center of the trench (OEC Lab ID# 21020302-03). This Process was 3 repeated for the Fire Trench with the inclusion of a sample on the East side of the trench were the material seemed to be consistent along the length of both trenches. Concrete Excavation: During the excavation of the trench, the outline of a brick structure was discovered containing lose bricks and soil. As this material was removed, a concrete slab was uncovered. Brick and soil from this excavation was placed into several twenty cubic yard bins. This material was sampled by taking three samples from each bin. Material was taken from the center of each bin moving left to right at a distance of 3’ apart for each sample (A, B, C). See OEC Lab ID#s 210508-01 to -15. The concrete slab was removed and it was discovered that there was hydrocarbon impacted soil underneath it, most likely from the removed fuel tank. Five samples were taken from the floor of the excavation. See OEC Lab ID#s 2102742-01 through -05. The sample locations are as follows: NW Corner @ 8’, NE Corner @8’, SW Corner @ 8’, SE Corner @ 8’ and the center of the excavation @ 8’. The data for these samples showed the presence of weathered hydrocarbon and that more material needed to be removed. Two twenty cubic yard bins of material were excavated and sampled in the same manner as the other bins. See OEC Lab ID#s 2103212-03 through -08. Once it was believed that all contaminated material was removed two verification samples were taken from the excavation floor approximately 4’ East and West from the center where the highest amount of petroleum had been present. Results from these samples showed that the petroleum had been removed to an acceptable level. 2. Reasoning for contaminants of concern (e.g. why weren’t SVOCs, PAHs, etc. included in testing). These compounds were not considered necessary due to the nature of the site. There was no indication that they would be present for any reason considering the location and types of businesses in the area. 3. History of the site, possible uses of the diesel tank and concrete pit, reason for high lead. Any information on diesel tank closed in place. To the best of our knowledge, there is no available phase one assessment for this site. Apparently somewhere close to the site there was a brick factory. The tank was likely used either for fueling or for waste. The tank had been filled with a concrete slurry. There was also a thin layer of what appeared to be petroleum on the outside of the tank. Both the coating and slurry were sampled. See OEC Lab ID#s 2101909-01 and 2102464-01. The tank was then disposed of at the McKittrick Land Fill. The bricks are possibly left over from a demolished structure, of what kind it is not clear. The concrete may have been a cap for the fuel contamination underneath it. Although the chromatographs for the TPH data show a weathered diesel pattern, it is possible that gasoline range organics may have been present and have degraded. Due to the presumed age of the site, this may have been leaded gasoline explaining the presence of lead. 4. Depth to groundwater in the area. Approximately 15’ to the NE of the Diesel Tank Excavation between the former Quik Mart and the building that will be the NHC SLO, ground water was discovered at a depth of 2’. In the tank excavation, ground water was discovered at a depth of 5’. No ground water intruded into the second excavation were the bricks and concrete slab were found. 4 Best Regards, Clarence Reynolds Compliance – CST P.O. Box 2646 | Orcutt, CA 93457 (805) 925-1947 EXT 352 | Fax: (805) 925-0884 | Cell: (805) 868-9081 Website: www.ppcinc.biz Attention: During the COVID-19 pandemic please anticipate a delay in response time to our emails. Safety being our number one priority requires us to take social distancing measures. We appreciate your patience and understanding during this time and will respond as soon as possible. 1 From:Clarence Reynolds <c.reynolds@ppcinc.biz> Sent:Friday, June 18, 2021 2:56 PM To:Bliss, Matheson Cc:William Sarten; John Hochleutner Subject:NHC SLO 2600 Broad Street Closure Report Attachments:NHC SLO Closure Report pg. 9 mark up.pdf Follow Up Flag:Follow up Flag Status:Completed This message is from an External Source. Use caution when deciding to open attachments, click links, or respond. Hi Mattie, I hope this gives you a better idea of how the project proceeded. Unfortunately, the Diesel Tank Excavation and Trench area have been backfilled so no pictures are available. Please let me know if you need more detail. 1. Describe the two distinct excavations (diesel tank and concrete structure), the trenches (noted on 4/6 data table), and soil piles and bins that are also noted on the data tables. Add additional figures detailing these areas and specific sampling locations. Diesel Tank Excavation: OEC Lab ID# 2101841-01 through 04 – Tank Wall Samples were taken at depth of 4’ in the center of each wall. 2101841-05 & 06 Tank Bottom Samples were taken at a depth of 8’ at the inlet and outlet ends of the tank. These samples were located at the bottom center of the East and West ends of the excavation approximately 1’ from the East and West walls respectively. The sample locations can be seen on page 9 of the closure report. The soil excavated from the diesel tank removal generated a pile approximately 5’ in height, 8’ in length and 4’ in width. Composite samples were taken from the North, South and West sides of the pile. This was done by taking three equal amounts of material from halfway up each side of the pile at intervals of about 1’5” and a depth of about 6”. These aliquots were mixed into three composite samples representing the three sides of the pile. A sample was not taken from the East side as it was too close to the mouth of the excavation and unsafe. Trenches: A trench was dug approximately 3’ deep to accommodate a water line. A pile of soil and brick was generated. It was approximately 3’ in height, 6’ in length and 4’ in width. A composite sample was taken from the pile by taking six equal amounts of material from half way up the pile (1.5’) at 2’ intervals and a depth of approximately 6”. These aliquots were combined into a single sample. As the excavation continued, the trench was segregated into two sections for sampling. This was done because half the length of the excavated material was composed of soil and the other length contained brick as well as soil. The length containing only soil was dubbed “Fire Trench” and the other “Sump Trench”. Originally, samples 2 were taken from the West Wall of the Sump Trench and at the bottom of the South End of the trench (OEC Lab ID#s 2101841-07,08). After data showed further excavation was required and carried out, a sample was taken from the Sump Trench West side (OEC Lab ID# 2103032-01) in the middle of its length because that is where most of the brick was. A sample was also taken from the bottom center of the trench (OEC Lab ID# 21020302-03). This Process was repeated for the Fire Trench with the inclusion of a sample on the East side of the trench were the material seemed to be consistent along the length of both trenches. Concrete Excavation: During the excavation of the trench, the outline of a brick structure was discovered containing lose bricks and soil. As this material was removed, a concrete slab was uncovered. Brick and soil from this excavation was placed into several twenty cubic yard bins. This material was sampled by taking three samples from each bin. Material was taken from the center of each bin moving left to right at a distance of 3’ apart for each sample (A, B, C). See OEC Lab ID#s 210508-01 to -15. The concrete slab was removed and it was discovered that there was hydrocarbon impacted soil underneath it, most likely from the removed fuel tank. Five samples were taken from the floor of the excavation. See OEC Lab ID#s 2102742-01 through -05. The sample locations are as follows: NW Corner @ 8’, NE Corner @8’, SW Corner @ 8’, SE Corner @ 8’ and the center of the excavation @ 8’. The data for these samples showed the presence of weathered hydrocarbon and that more material needed to be removed. Two twenty cubic yard bins of material were excavated and sampled in the same manner as the other bins. See OEC Lab ID#s 2103212-03 through -08. Once it was believed that all contaminated material was removed two verification samples were taken from the excavation floor approximately 4’ East and West from the center where the highest amount of petroleum had been present. Results from these samples showed that the petroleum had been removed to an acceptable level. 2. Reasoning for contaminants of concern (e.g. why weren’t SVOCs, PAHs, etc. included in testing). These compounds were not considered necessary due to the nature of the site. There was no indication that they would be present for any reason considering the location and types of businesses in the area. 3. History of the site, possible uses of the diesel tank and concrete pit, reason for high lead. Any information on diesel tank closed in place. To the best of our knowledge, there is no available phase one assessment for this site. Apparently somewhere close to the site there was a brick factory. The tank was likely used either for fueling or for waste. The tank had been filled with a concrete slurry. There was also a thin layer of what appeared to be petroleum on the outside of the tank. Both the coating and slurry were sampled. See OEC Lab ID#s 2101909-01 and 2102464-01. The tank was then disposed of at the McKittrick Land Fill. The bricks are possibly left over from a demolished structure, of what kind it is not clear. The concrete may have been a cap for the fuel contamination underneath it. Although the chromatographs for the TPH data show a weathered diesel pattern, it is possible that gasoline range organics may have been present and have degraded. Due to the presumed age of the site, this may have been leaded gasoline explaining the presence of lead. 3 4. Depth to groundwater in the area. Approximately 15’ to the NE of the Diesel Tank Excavation between the former Quik Mart and the building that will be the NHC SLO, ground water was discovered at a depth of 2’. In the tank excavation, ground water was discovered at a depth of 5’. No ground water intruded into the second excavation were the bricks and concrete slab were found. Best Regards, Clarence Reynolds Compliance – CST P.O. Box 2646 | Orcutt, CA 93457 (805) 925-1947 EXT 352 | Fax: (805) 925-0884 | Cell: (805) 868-9081 Website: www.ppcinc.biz Attention: During the COVID-19 pandemic please anticipate a delay in response time to our emails. Safety being our number one priority requires us to take social distancing measures. We appreciate your patience and understanding during this time and will respond as soon as possible.