HomeMy WebLinkAboutSLOUNIFLOW_FS1 Admin iRC3926i Color_0153_001UNDERGROUND STORAGE TAI\K REMOVAL AND SITE ASSESSMENT
UPS FACILITY
3601 SACRAMENTO DRTVE
sAN LUIS OBISPO, CALIFORIIIA
January 28, 1994
Job Number: 40065-002{1
TABLE OF CONTENTS
Section
1.0 EXECUTIVE SUMMARY
2.0 INTRODUCTION
2.1 SITE DESCRIPTION
3.0 REGIONAL GEOLOGIC AND HYDROGEOLOGIC SETTING
4.0 UST EXCAVATION AND SAMPLING
5.0 FOLLOW UP SITE ASSESSMENT 5-1
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DRILLING AND SOIL SAMPLING
GROUNDWATER MONMORING WELL INSTALLATION
5.3 GROUNDWATER SAMPLING
5.4 WELL SURVEYING
5.5 USED OIL UST SAMPLING INVESTIGATION
5.6 DOMESTIC WELL SAMPLING
6.0 SUBSUF.FACE CONDITIONS
7.0 ANALYTICAL TEST METHODS
8.0 SOIL ANALYTICAL RESULTS
9.0 GROUNDWATER ANALYTICAL RESULTS . . . .
1O.O SUMMARY AND CONCLUSIONS
11.0 LIMITATIONS
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TABLE I
TABLE 2
TABLE 3
TABLE 4
TABLE 5
TABLE 6
LIST OF TABLES
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Soil Boring Sample Analytical Results
Groundwater Analytical Results
LIST OF FTGI]RES
Vicinity
Site
LIST OF APPET..{DICFS
Rinse Water Hazardous Waste Manife.st
. Non-Hazardous Soil Manifest
Tank Disposal Certifi cate
il,;;'n.po* *."ffii:l3"ilSX;t,lfrHfi
FIGURE 1
FIGURE 2
APPENDIX A
APPENDX B
APPENDIX C
APPENDIX D
APPENDTX E
Map
Map
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1.0 EXECUTIVE SI.]MMARY
On October 13, 1993, Science & Engineering Analysis Corporation (SE4COR) conducted soil
sampling beneath a former 10,000 gallon gasoline and a 550 gallon used oil underground storage
tank (UST) at the UPS facility in San Luis Obispo, California. Total petroleum hydrocarbons (TPH)
and benzene, toluene, ethylbenzene and total xylenes (BTE&E constituents were identified in the
capillary fringe soils beneath the gasoline UST. Low levels of TPH and BTE&X constituents were
identified in the vadose zone soil beneath the used oil UST. A water sample obtained from the
gasoline UST excavation contained TPH characterized as gasoline and BTE&X constituents. The
integrity of the water sample appears to have been jeopardized by a sheen of free product floating
on the water.
Between October 14 and November 17,1993, SEACOR drilled seven soil borings and installed three
groundwater monitoring wells at the site to evaluate the potential impact of TPH and BTE&X
constituents to the soil and groundwater around the USTs.
Presented below is a summary of the results:
Approximately 250 cubic yards of TPH and BTE&X impacted soil was excavated
from around and beneath the gasoline UST and transported to a recycling facility.
Free product and water from the gasoline UST excavation was removed with a
vacuum truck after obtaining the previously mentioned water sample. The free
product and water was transported to a recycling facility.
Only one soil sample from the seven borings indicated the presence of TPH
characterized as gasoline and BTE&X constituents.
Groundwater samples obtained from the three groundwater monitoring wells did not
indicate the presence of TPH characterized as gasoline and BTE&X constituents.
A groundwater sample obtained from an on site domestic well owned and operated
by UPS did not indicate the presence of TPH characterized as gasoline and BTE&X
constituents.
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I 2.0 INTRODUCTION
On behalf of United Parcel Service (UPS), SEACOR has prepared the following report describing
the results of the removal of two underground storage tanks (UST), soil and water sampling beneath
the former USTs and a follow up site assessment conducted at the UPS facility located at 3601
Sacramento Drive in San Luis Obispo, California (Figure 1). The purpose of the UST removals was
to replace a former single-walled gasoline UST with a new double-walled gasoline UST and to take
a used oil UST out of service. The purpose for soil and water sampling beneath the USTs was to
evaluate the potential impact to soil and groundwater beneath the USTs. The purpose of the follow
up site assessment was to evaluate the vertical and lateral extent of petroleum hydrocarbons
encountered in soil and groundwater beneath the USTs. The site assessment activities were
conducted per the approval of the Regional Water Quality Control Board - Central Coast Region
(RWQCB) in a telephone conversation with SEACOR on October 14, 1993.
The scope of work conducted by SEACOR to date has included the following
Soil and water sampling from beneath the former USTsa
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Sampling of three soil stockpiles generated during UST removal and sampling of trvo
soil stockpiles associated with UST installation.
Drilling and sampling of seven soil borings.
Installation and sampling of three groundwater monitoring wells
Wellhead surveying.
Laboratory analysis
Report preparation
2.I SITE DESCRIPTION
The UPS facility is located in an industrial area within the City of San Luis Obispo. A parcel
distribution facility is located in the central portion of the facility. A large parking lot and several
planters surround the central building. The northeastern boundary of the property is Sacramento
Drive. Northwest of the site is a vacant lot. Southwest and southeast of the site is the Plumbers and
Steamfitters Union Office and an industrial building, respectively.
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The surface topography on and adjacent to the site slopes gently toward the south and southwest.
Surface drainage on the site is directed into a retention basin on the southern portion of the UPS
properly.
A single-walled 10,000 gallon gasoline UST and single-walled 550 gallon used oil UST, which are
the subject of this report, were located on the east side of the UPS building. The age of the USTs
are unknown. A dispenser island with one gasoline dispenser was located directly above the gasoline
UST.
A domestic well owned by UPS is located on the southern edge of the site, approximately 170 feet
southwest of the former USTs. The domestic well water is used for washing the UPS delivery trucks
and wash water in the facility. The domestic well water is not used for drinking. Figure 2 presents
the site configuration and the location of the former USTs and domestic well.
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3.0 REGIONAL GEOLOGIC AND IIYDROGEOLOGIC SETTING
The site is located in the Southern Coast Ranges geomorphic province of California. The Coast
Ranges extend from the San Francisco Bay in the north to the Santa Ynez River in the south. The
eastern boundary of the Coast Ranges is the Central Valley and the western boundary extends
offshore into the Pacific Ocean. The Coast Ranges are characterized by northwest-southeast trending
mountain ranges and intervening valleys which are generally separated by faults.
The site is further located in the northwestern end of the Edna Valley which is a northwest-southeast
trending valley. In the vicinity of the site, several streams within the Edna Valley have eroded the
underlying bedrock and subsequently filled the low lying areas with a shallow veneer of alluvial
sediments. The alluvial sediments include sand, gravel and clay. Beneath the alluvium is bedrock
of the Franciscan Formation. Dominant rock types within the Franciscan Formation include
serpentinite, metavolcanic rocks, chert and greywacke sandstone. Outcrops of bedrock are located
in the hills approximately ll2 mile northeast and northwest of the site and on the southern corner of
the site.
Surface drainage in the vicinity of the site is generally toward the south and southwest. Several
small streams flow from the hills northeast of the site and into San Luis Obispo Creek southwest of
the site (Figure 1).
Several potentially active faults, with a characteristic northwesterly trend, flank the Edna Valley.
The Edna Fault is considered a potentially active fault and trends northwesterly along the southern
boundary of the Edna Valley and is located approximately 2 miles south of the site. Near the Cuesta
Ridge area approximately 3 miles north of the site is a series of subparallel faults including the
potentially active West Huasna/Cambria Fault.
Groundwater in the vicinity of the site occurs within the unconsolidated alluvium and in deeper
fractures within the bedrock. Depth to uppermost groundwater beneath the site varies. Shallow
groundwater normally occurs where the alluvium is thickest and is absent where the alluvium thins
or is nonexistent. The regional groundwater flow direction beneath the site is most likely
south/southwesterly toward San Luis Obispo Creek. Groundwater quality in the San Luis Obispo
area is variable, however, the uppermost groundwater zone commonly contains elevated levels of
total dissolved solids and nitrates. Groundwater in deeper aquifers within the alluvial sediments and
bedrock is used for domestic and agricultural uses.
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4.0 UST EXCAVATION AND SAMPLING
On October 13, 1993, personnel from SEACOR arrived on site to observe triple rinsing and the
removal of the 10,000 gallon gasoline UST and 500 gallon used oil UST and obtain verification soil
samples. Petro Builders, Inc. of Santa Fe Springs, California was contracted by UPS to remove and
dispose of the USTs and transport excavated soil and rinsate water to the appropriate disposal
facility. SEACOR was contracted by Petro Builders, Inc. to obtain the verification soil samples and
conduct the assessment work. The UST and verification soil sampling was conducted under the
guidance of Mr. Spencer Meyer of the City of San Luis Obispo Fire Department (SLOFD).
Prior to UST removal, the overburden and surrounding soil was excavated and stockpiled adjacent
to each UST excavation. Soil from the gasoline UST excavation was stockpiled in Stockpiles 1 and
2 (Figure2). Soil from the used oil UST excavation was placed in Stockpile A.
Following excavation of the overburden and surrounding soil, the USTs were triple rinsed. The
rinsate was collected in a vacuum truck. The rinse water from the USTs was vacuumed into a
vacuum truck.
During the gasoline UST removal, strong hydrocarbon odors and grayish brown stained soil were
observed beneath the UST. No holes were observed in the gasoline UST. Following removal of
the gasoline UST, groundwater was noted in the bottom of the excavation. A sheen of free product
was observed on the water surface. The dimensions of the excavation were approximately 35 feet
long by 15 feet wide by 15 feet deep.
Three grab soil samples (S-5, 5-6 and S-7) and one grab water sample (W-1) were obtained from
the gasoline UST excavation. Figure 2 presents the approximate locations of the soil and water
samples. Soil samples S-5 and S-7 were obtained from a depth of approximately 15 feet below grade
in the gasoline UST excavation. Soil sample 5-6 was obtained from the northern sidewall of the
UST excavation at a depth of approximately 14 feet below grade. All three soil samples were
obtained from the capillary fringe soils. Visual observations of the gasoline UST excavation
sidewalls did not indicate the presence of petroleum hydrocarbons in the vadose zone soil.
Following soil and water sampling from the gasoline UST excavation, the water with a sheen of free
product was vacuumed from the pit. The water was transported under hazardous waste manifest to
DeMenno Kerdoon in Compton, California, a hazardous waste recycling facility. Appendix A
presents a copy of the hazardous waste manifest.
The volume of soil removed from the gasoline UST excavation and stockpiled in Stockpiles 1 and
2 equalled approximately 250 cubic yards. Two grab soil samples (S-10 and S-11) were obtained
from Stockpile 1 and one grab soil sample (S-9) was obtained from Stockpile 2. The soil in
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Stockpiles I and2 was transported as non-hazardous waste to TPS Technologies, Inc. in Adelanto,
California. Copies of the non-hazardous soil manifest are included in Appendix B.
Following soil and water sampling, the gasoline UST excavation was backfilled with clean imported
gravel from approximately 15 to 8 feet below grade. The remainder of the excavation was backfilled
with clean imported sand. The surface was paved with asphalt.
During the used oil UST removal, no hydrocarbon odors or stained soil was observed. Numerous
holes were observed in the used oil UST. A concrete hold down slab was encountered in the
excavation at approximately 8.5 feet below grade. No water was encountered in the excavation.
The dimensions of the excavation were approximately 10 feet long by 8 feet wide by 8.5 feet deep.
Three grab soil samples (S-1, S-2 and S-3) were obtained from three sidewalls of the used oil UST
excavation at a depth of 7.5 feetbelow grade. Based on the analytical results for soil sample S-1,
the excavation was deepened and another soil sample (S-8) was obtained at a depth of approximately
8.5 feet below grade, just above the concrete slab (Figure 2).
Approximately 20 cubic yards of soil was removed from the used oil UST excavation, stockpiled
(Stockpile A) and sampled (S-4). Based on the results of the sample analysis, the used oil UST
excavation was backfilled with the soil in Stockpile A. The surface was paved with asphalt.
On October 22,1993, six soil samples (Stockpile 3A, 38, 3C,4A,48 and 4C) were obtained from
excavated soils for the new USTs (Stockpiles 3 and 4). Figure 2 presents the locations of the
stockpiles. The purpose for sampling was to evaluate whether the soil was impacted with petroleum
hydrocarbons from the former gasoline UST. Based on the analytical results of the soil samples, the
soil from the new gasoline UST excavation was transported to a Class III landfill.
Grab soil samples from the UST excavations were obtained from a backhoe and placed in laboratory
supplied containers. The water sample from the gasoline UST excavation was obtained by lowering
a Teflon* bailer in the excavation. The water sample was decanted from the bailer into laboratory
supplied containers.
The grab soil samples from the stockpiles were obtained by pushing a laboratory supplied container
into the soil. The soil and water samples obtained from the gasoline and used oil UST excavations
and from Stockpiles 1,2 and, A were transported to an on-site mobile laboratory immediately after
sampling.
The former gasoline and used oil USTs were transported to M&M Salvage in Nipomo, California.
A copy of the tank disposal certificate is presented in Appendix C.
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5.0 FOLLOW UP SITE ASSESSMENT
5.I. DRILLING AND SOIL SAMPLING
Based on the analytical results of soil and water samples collected from the gasoline UST excavation,
soil borings were drilled and sampled on October 14 and 15, 1993. The purpose of the soil borings
was to evaluate the lateral extent of the hydrocarbon impacted soil and the potential for hydrocarbon
impacted groundwater. Prior to drilling at the site, well construction permits were obtained from
the San Luis Obispo County Division of Environmental Health. Seven exploratory soil borings
labelled as B-1, MW-l (B-2), B-3, B-4, B-5, MW-z and MW-3 were drilled and sampled in the site
area using a truck-mounted drill rig equipped with eight-inch diameter hollow-stem augers. Boring
locations are shown on Figure 2. Prior to drilling each boring, the augers were steam cleaned to
prevent cross-contamination. Drilling was directed by a qualified SEACOR geologist working under
the direct supervision of a California Registered Geologist.
The purpose of borings B-1, MW-l (B-2) and B-3 was to evaluate the lateral extent of the
hydrocarbon impacted soil and potentially impacted groundwater southwest of the former gasoline
UST and facilitate installation of a groundwater monitoring well. In addition, these three borings
were drilled to evaluate the depth to bedrock beneath the site. UPS intended to install a new gasoline
UST in an area not impacted by petroleum hydrocarbons and underlain by alluvium rather than
bedrock, so as to not hinder excavation with a backhoe. Following drilling and sampling of borings
B-1, MW-l (B-2) and B-3, the new gasoline UST location was excavated. Soil from the new
gasoline UST excavation was stockpiled in Stockpiles 3 and 4. Figure 2 presents the location of the
new gasoline UST and Stockpiles 3 and 4.
The purpose for drilling borings B-4, B-5, MW-2 and MW-3 was to evaluate the lateral extent of
hydrocarbon impacted soil and groundwater west and north of the gasoline UST and facilitate well
installation. Borings B-4 and B-5 were originally drilled to facilitate installation of a groundwater
monitoring well. However, no groundwater was encountered during drilling and a monitoring well
was installed in boring MW-2, closer to the gasoline UST excavation.
Soil samples for chemical analysis and logging purposes were collected in the soil borings at 2.5-foot
intervals using a split-spoon sampler containing brass sleeves for sample retention. Soil samples
retained for chemical analysis were immediately sealed with Teflonru film, capped, labelled and
placed on ice in a cooler. Remaining soils were visually classified in accordance with the Unified
Soil Classification System and monitored for volatile organic vapors using a flame-ionization detector
(FrD).
All sampling equipment was cleaned in an aqueous solution of non-phosphate cleanser, rinsed with
tap water and rinsed a second time with distilled water to prevent cross-contamination between
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borings and sample intervals. Soil cuttings generated during drilling activities were stockpiled in
Stockpiles I and 2. Boring logs are presented in Appendix D.
5.2 GROT]NDWATER MOMTORING WELL INSTALLATION
Immediately after soil sampling, groundwater monitoring wells were constructed in soil borings MW-
1 (B-2), MW-2 and MW-3. The wells were constructed by lowering PVC casing inside the hollow
stem augers. Filter pack sand and a bentonite seal was tremied through the augers as they were
slowly pulled from the ground. The casing string consisted of flush-threaded, 2-inch diameter,
Schedule 40 PVC. The screened portion was factory slotted with 0.020-inch slots. The base of the
casing string was sealed with a PVC, flush-threaded, bottom plug and the top was covered with a
locking water-tight cap.
The screened interval extended from 10 to 30 feet below grade in well MW-l and 8 to 28 feet below
grade in wells MW-2 and MW-3. The annular space between the well casing and borehole was
packed with clean, #3 Monterey sand to approximately 2 f*t above the top of the screened section.
A two-foot-thick bentonite seal was placed above the filter sand, and the remainder of the annulus
was grouted with a bentonite-cement slurry. Each well head was completed with a locking, flush
mounted well cover.
Following installation, the new wells were developed by surging and bailing to clear sediment from
the formation and filter pack. Development was considered complete when the well produced water
that was relatively free of sediment.
5.3 GROI]I\DWATER SAMPLING
Groundwater sampling was conducted from monitoring wells MW-l, MW-2 and MW-3 on
November 11, 1993. Prior to sampling, the depth to groundwater was measured in all three wells
using a Solinst* electronic water level meter. Following water depth measurements, the wells were
purged to produce groundwater representative of the aquifer. Water quality parameters (temperature,
pH, and conductivity) were measured during purging. Approximately three well volumes of
groundwater were removed from groundwater monitoring wells MW-l and MW-3 during purging.
Groundwater monitoring well MW-2 was bailed dry after approximately 2 well volumes.
Groundwater samples were collected after the water level in wells MW-l and MW-3 recovered to
within 80 percent of the level measured prior to purging. A groundwater sample was obtained from
well MW-2 approximately 2 hours after being purged dry the second time. Groundwater samples
were collected using a Teflon* bailer fitted with a bottom-emptying device and decanted into
laboratory prepared sample containers. Samples were sealed, labeled, entered on a chain-of-custody
form and placed in a chilled cooler for delivery to the analytical laboratory.
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All purging and sampling equipment was cleaned in an aqueous solution of non-phosphate cleanser,
rinsed in tap water and rinsed a second time in distilled water to prevent cross-contamination.
Development and purged well fluids were contained in labeled DOT-approved 55-gallon drums. The
drums are currently stored on-site.
5.4 WELL SI]RVEYING
On November 17,1993 groundwater monitoring wells MW-l, MW-2, MW-3 and the domestic well
were surveyed to a common site datum @enchmark) to determine their relative vertical elevations
and horizontal positions. Additional groundwater depth measurements were obtained from wells
MW-l, MW-2, MW-3 and the domestic well during surveying. Each well was permanently marked
with a survey point upon which subsequent water level measurements will be obtained. Survey
points were determined to an accuracy of 0.01 feet. The horizontal distances of each well were
located in reference to several permanent site features (i.e., curbs, utility poles). Table l presents
the groundwater elevations for the groundwater depth measurements obtained on November 1.1 and
November 17, L993.
5.5 USED OIL UST SAMPLING INVESTIGATION
On October 29 md November l, 1993, personnel from SEACOR attempted to hand auger several
soil borings around the former used oil UST excavation to obtain soil samples from beneath the hold-
down slab. Borings were attempted within the used oil UST excavation boundaries and outside the
excavation boundaries. However, obstructions such as pieces of asphalt, rock, the hold-down slab
and irrigation pipes were encountered, thus no soil samples were collected.
5.6 DOMESTIC WELL SAMPLING
On December 16, 1993, a groundwater sample was obtained from the domestic well at the UPS
facility. The domestic well sample was obtained from a sampling port at the wellhead by personnel
from Coast to Coast Analytical Services, Inc.
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6.0 SUBSURFACE CONDITIONS
Soil and unconsolidated sediments (alluvial sediments) encountered during drilling included clay,
sandy clay, clayey sand, silty sand and gravelly sand. Bedrock was encountered in all borings drilled
except borings B-1 and MW-3. The approximate thickness of the alluvial sediments varied across
the site and appeared to be deepest in the vicinity of soil boring MW-3. Bedrock was encountered
in boring MW-l (B-2) at approximately 23 feet below site grade, in boring B-3 at approximately 12
feet, in B-4 at approximately 5 feet, in boring B-5 at approximately 7 .5 feet and in boring MW-2
at approximately 6.5 feet of depth. A surface outcrop of bedrock is located on the southern corner
of the site. The bedrock surface beneath the site appflrs to dip toward the central portion of the
facility (i.e. toward boring MW-3).
The bedrock, where encountered in the borings, was weathered and appeared to be predominantly
claystone, sandstone and serpentinite indicative of the Franciscan Formation. The bedrock outcrop
on the southern corner of the site is composed of serpentinite.
Very low organic vapor concentrations (OVA) ranging from less than 1 to 20 parts per million (ppm)
were observed in the vadose zone soil samples from all seven borings except boring B-1. In boring
B-1, the OVA readings increased from 5 ppm to greater than 1,000 ppm from 5 to 14 feet below
grade, respectively. A moderate hydrocarbon odor was observed in the soil sample from 12.5 feet
below grade in boring B-1. No hydrocarbon odors were observed in the remaining borings.
During drilling, saturated soil was encountered at 20 feet below grade in boring MW-l (B-2) and
22.5 feet in boring MW-3. Groundwater or saturated soil was not encountered in the remaining
borings. Borings B-4 and B-5 were left open for approximately 4 and 2 hours, respectively, to
observe for groundwater. Originally, boring B-4 was to be converted to a groundwater monitoring
well, however, no groundwater was encountered. Boring B-5 was drilled after B-4 to determine the
presence of groundwater in the borehole. After no groundwater was encountered in borings B-4 and
B-5, boring MW-2 was drilled closer to the gasoline UST excavation and a monitoring well was
installed. Groundwater was not observed in groundwater monitoring well MW-2 immediately after
construction.
Based on the hydrogeologic conditions at the site, the groundwater elevations in the three
groundwater monitoring wells are not representative of a uniform, water table aquifer. Groundwater
monitoring wells MW-1 and MW-3 were screened within an alluvial aquifer, whereas, well MW-2
is screened within fractured bedrock. The groundwater elevations in well MW-l on November 11
and 17, 1993 were approximately one foot lower than the elevations in well MW-3. However, the
elevations in well MW-2 on November 11 and 17,1993 were approximately 10.5 feet lower than
the elevations in well MW-3. The groundwater elevations in wells MW-l and MW-3 appear to be
representative of the observed alluvial aquifer conditions, whereas, well MW-2 reflects water
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conditions in the fractured Franciscan Formation. Therefore, a representative groundwater flow
direction could not be established.
The well construction details for the UPS domestic well include 320 feet of PVC casing screened
from 220 to 320 feet below grade. A filter pack extends from 50 to 320 feet below grade. A
surface seal extends from the surface to 50 feet below grade. The depth to groundwater in the
domestic well on November 17, 1993 was 23.22 feet.
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7.0 AI\ALYTICAL TEST METHODS
The three soil samples (S-5, 5-6 and S-7) and water sample (W-1) obtained from the gasoline UST
excavation and the three soil samples (S-9, S-10 and S-11) obtained from Stockpiles I and 2 were
analyzed for total petroleum hydrocarbons (TPH) characterized as gasoline by Environmental
Protection Agency (EPA) Test Method 8015, and benzene, toluene, ethylbenzene and total xylene
(BTE&X) by EPA Test Method 8020. Soil samples S-5, 5-6, S-7, S-9, S-10 and S-11 were analyzed
for organic lead by EPA Test Method 6010. Table 2 presents a summary of the analytical results
from the samples obtained from the gasoline UST excavation and Stockpiles 1, and2.
The four soil samples (S-1, S-2, S-3 and S-8) obtained from the used oil excavation and soil sample
(S-4) obtained from Stockpile A were analyzed for total recoverable petroleum hydrocarbons (TRPH)
by EPA Test Method 418.1, BTE&X by EPA Test Method 8020, total chromium by EPA Test
Method 6010 and organic lead by EPA Test Method 6010. Table 3 presents a surnmary of the
analytical results from the samples obtained from the waste oil excavation and Stockpile A.
The six soil samples obtained from stockpiles 3 and 4 (stockpile 3A', 38, 3C,4A,48 and 4C) were
analyzed for TPH as gasoline and BTE&X constituents by EPA Test Method 8260. Table 4 presents
a surnmary of the soil samples analytical results from stockpiles 3 and 4.
The five soil samples obtained from borings B-1, MW-1 (B-2), B-3, B-5 and MW-3 and the three
groundwater samples obtained from monitoring wells MW-l., MW-2 and MW-3 were analyzed for
TPH as gasoline and BTE&X constituents by EPA Test Method 8260. Table 5 presents a summary
of the soil sample analytical results from the borings. Table 6 presents a summary of the
groundwater sample analytical results from wells MW-l, MW-2 and MW-3.
The domestic well sample obtained on December 16,1993 was analyzed for TPH and BTE&X by
EPA Test Methods 8015/8020. Table 7 presents a summary of the analytical results from the
domestic well.
Copies of laboratory results and chain-of-custody documents for the soil and groundwater samples
are presented in Appendix E.
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8.0 SOIL ANALYTICAL RESULTS
The analytical results of two of the three soil samples (S-5 and 5-6) obtained from the gasoline UST
excavation indicated TPH characterized as gasoline at 72 and 1,500 milligrams per kilogram
(mg/kg). Benzene was also detected in soil samples S-5 and 5-6 at 7.0 and 2.5 mglkg, respectively.
The third soil sample (S-7) collected from the gasoline UST excavation did not indicate the presence
of TPH as gasoline and benzene at detection limits of 10 and 0.025 mg/kg. Organic lead was not
detected in the soil samples obtained from beneath the gasoline UST at a detection limit of 0.3
mg/kg.
The analytical result of the three soil samples (S-9, S-10 and S-11) collected from stockpiles 1. and
2 indicated concentrations of TPH chuactefized as gasoline ranging from 28 to 1,300 mg/kg and
benzene concentrations ranging from less than 0.25 mglkg to 2.3 mg/kg. Organic lead was not
detected inthe soil samples obtained from stockpiles 1 and 2 ata detection limit of 0.3 mg/kg.
The analytical results from soil sample S-L obtained from the eastern edge of the used oil UST
excavation and at a depth of 7.5 feet below grade indicated 250 mglkg of TRPH and 0.025 mg/kg
of benzene. Soil sample S-8 obtained approximately one foot below sample S-1 did not indicate the
presence of TRPH or benzene at detection limits of 10 and 0.025 mglkg, respectively. The
analytical results from soil sample S-2 obtained from the southern corner of the used oil UST
excavation indicated benzene at 0.27 mg/kg. However, TRPH was not detected at a detection limit
of 10 mg/kg. Soil sample S-3 did not indicate the presence of TRPH or BTE&X constituents. The
analytical results of soil sample S-4 obtained from stockpile A indicated low levels of BTE&X
constituents, well below the RWQCB Action l,evels. TRPH was not detected in soil sample S-4.
Organic lead was not detected in any of the five soil samples associated with the former used oil
UST excavation (S-1, S-2, S-3, S-4 and S-8). Total chromium was detected in all ftve samples
associated with the former used oil excavation at concentrations ranging from 7.1 to 18.1 mg/kg.
These concentrations are less than the Title 22 Total Threshold Limit Concentration (TTLC) and
Soluble Threshold Limit Concentration (STLC) for total and soluble chromium, respectively. The
TTLC and STLC for total and soluble chromium are 2,500 mg/kg and 560 milligrams per liter
(mglt), respectively.
TPH characterized as gasoline and BTE&X constituents were not detected in the six soil samples
obtained from stockpiles 3 and 4. The detection limits for TPH characterized as gasoline and
BTE&X constituents were 0.5 and 0.005 mg/kg, respectively.
TPH characterized as gasoline and benzene were detected in soil sample B-1 @ 12.5' , obtained from
the capillary fringe zone, at concentrations of 6.0 and 0.26 mglkg, respectively.
8-1
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TPH characterized as gasoline and BTE&X constituents were not detected in soil samples MW-l (B-
2) @ 12.5' ,B-3 @ 10.0', B-5 @ 12.5' and MW-3 @ I2.5' at detection limits of 0.5 mg/kg for TPH
and 0.005 mg/kg for BTE&X constituents.
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9.0 GROUI\DWATER ANALYTICAL RESULTS
TPH characterized as gasoline was detected in water sample W-l at a concentration of 390,000
micrograms per liter Qrg/t). BTE&X constituents were also detected at concentrations of 6,600,
1.3,000, 26,000 and 130,000 p.gll, rcspectively. The integrity of this sample may have been
impacted by the sheen of free product which may be a result of the UST removal activities.
TPH charactefized as gasoline and BTE&X constituents were not detected in the groundwater
samples obtained from groundwater monitoring wells MW-l, MW-2 and MW-3. The detection
limits for groundwater samples MW-l, MW-2 and MW-3 were 50 p.glt fot TPH characterized as
gasoline and 0.5 y.gll for the BTE&X constituents.
TPH charactefiznA as gasoline and BTE&X constituents were not detected in the groundwater sample
obtained from the domestic well on December 16,1993. The detection limit for TPH was 500 pgl/
and the detection limit for BTE&X compounds ranged from 0.3 to 0.6 Llgll.
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9-1,
1O.O SI.IMMARY AND CONCLUSIONS
During removal of the 10,000 gallon gasoline UST, approximately 250 cubic yards of soil was
excavated from above and around the former UST. A dispenser island located directly above the
UST was removed along with the UST. No holes were observed in the gasoline UST. The
excavated soil was recycled at TPS Technologies, Inc. in Adelanto, California. The gasoline UST
excavation was backfilted with clean imported sand and gravel.
Three soil samples and one water sample were collected from the gasoline UST excavation. One
soil sample was obtained from the capillary fringe. One soil sample (5-6) was obtained from the
capillary fringe and trvo soil samples (S-5 and S-7) were obtained from the bottom of the gasoline
UST excavation.
Visual observations of the gasoline UST excavation indicates that the soil impacted with petroleum
hydrocarbons appear to be located within the capillary fringe soils. Petroleum hydrocarbon impacted
soil was not observed within the vadose zone soils on the sidewalls of the UST excavation.
The integrity of the water sample from the gasoline UST excavation appears to have been jeopardized
by the sheen of free product. Following water sampling, water with a sheen of free product was
skimmed from the gasoline UST excavation with a vacuum truck and transported to a recycling
facility.
During removal of the 550 gallon used oil UST, approximately 20 cubic yard of soil was excavated
and stockpiled on site in Stockpile A. Numerous holes were observed in the UST upon removal.
A concrete hold down slab remains in the UST excavation. No groundwater was encountered and
four soil samples were obtained from the used oil excavation.
Following UST removal and soil sampling, the used oil excavation was backfilled with the soil in
Stockpile A.
The former gasoline and used oil USTs were transported to M&M Salvage in Nipomo, California.
Subsurface conditions are characterizedby weathered bedrock of the Franciscan Formation which
is overlain by alluvial sediments. The thickness of the alluvial sediments ranges from approximately
5 feet in boring B-4 (north of the gasoline UST excavation) to more than 28 feet in boring MW-3,
southwest of the former gasoline UST excavation. An outcrop of bedrock is exposed on the southern
corner of the site, southwest of the former gasoline UST excavation.
Water was encountered in the former gasoline UST excavation at a depth of approximately 15 feet
below grade. Groundwater was encountered during drilling of borings MW-1 and MW-3 at a depth
l0-1
of approximately 14 feet below grade in the alluvial sediments. No groundwater was encountered
during drilling of boring MW-2 in the bedrock. Stabilized groundwater levels occur at a depth of
approximately L2.5 feet in the alluvium (wells MW-l and MW-3) and 23 feet in the bedrock (well
MW-2 and the domestic well). Groundwater elevations in groundwater monitoring wells MW-l and
MW-3 do not appear to correlate with the relative groundwater elevation in groundwater monitoring
well MW-2 and the domestic well.
The lateral extent of the TPH and BTE&X constituents has been defined toward the southwest of the
former gasoline UST excavation by boring MW-l, toward the west by boring MW-3 and toward the
northeast by boring B-5.
Although TPH characterized as gasoline and BTE&X constituents were identified in a water sample
(W-1) collected from the former gasoline UST excavation, groundwater samples collected from the
rhree monitoring wells on-site (MW-l, MW-2 and MW-3) and the domestic well did not indicate the
presence of TPH characterized as gasoline or BTE&X constituents-
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11.0 LIMITATIONS
This report has been prepared for the exclusive use of the United Parcel Service as it pertains to the
property located at 3601 Sacramento Drive in San Luis Obispo, California. The findings and
conclusions presented in this report are based primarily on the chemical analysis of soil and
groundwater samples obtained during this investigation. All work has been performed in a manner
consistent with that level of care and skill normally exercised by members of the environmental
science profession currently practicing under similar conditions in the area. No other warranty,
either expressed or implied, is made.
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ssaflvI
Domqstic Well NANA100.00 76.7{23.22-
96.27MW-3 84.0312.2483.8212.45
MW-2 73.O323.6t96.64 73.4723.17
95.64MW-1 83.0612.5882.7r12.93
to'
NA - Not available.
'Domestic well not pumping during groundwater depth measurcment.
NA130 mglt26 mglt6.6 mglt 13 mg/t39O mgllW-l (15 feet)
< 0.35.5<o.25<0.25<0.25210S-ll (Stockpile l)
<0.34.20.860.510.2428S-10 (Stockpile 1)
<0.3ll022l52.31300S-9 (Stockpile 2)
< 0.3o.970.055<0.025< 0.025<10S-7 (15 feet)
< 0.396l83.12.515005-6 (15 feet)
<0.32'to83287.O72S-5 (15 feet)
Organic Lead
(by 6010)
Total Xylenes
(by 8020)
Ethylbenzene
(by 8020)
Toluene
(by s020)
Benzene
(by 8020)
TPH as Ga^soline
(by 8015)
Sample ID and
Depth
Table 2 - Gasoline UST Excavation and Stockpiles I and 2 Analytical Results
(alt results in milligrams per kilogram' except sample W-l)
Note:
NA
mg/t
Not analyzed.
Milligrams per liter
<0.318. I0.520.0290.028< 0.025<10S-8 (8.5 feet)
< 0.39.51.10.2r0.120.053<10S-4 (Stockpile A)
<0.311.0< 0.050< 0.025< 0.025<0.025<10S-3 (7.5 feet)
< 0.38.0o.620.22o.220.2't<10S-2 (7.5 feet)
< 0.37.1o.2t0.0400.0430.025250S-1 (7.5 feeO
Organic Lead
(by 6010)
Total Chronriuin
(by 6010)
Total Xylenes
(by 8020)
Ethylbenzene
(by 8020)
Toluehe
(bv 8020)
Benzene
(by 8020)
TRPH
fty 4r8;r) :
Sample ID and
Depth
Table 3 - Waste Oil UST Excavation and Stockpile A Analytical Results
(all results in Inilligranrs per kilograrn)
< 0.005< 0.005< 0,005< 0.005< 0.5srockpile 4c
< 0.005< 0.005< 0.005< 0.005< 0.5Stockpile 4B
< 0.005< 0.005< 0.005< 0.005<0.5Stockpile 4,A'
<0.005< 0.005< 0.005< 0.005<0.5Stockpile 3C
<0.005< 0.005< 0.005< 0.005<0.5Stockpile 38
< 0.005< 0.005< 0.005< 0.005< 0.5Stockpile 3A
Total Xylenes
(by 8020)
Ethyltlenzene
(by 8020)
Toluene
(by 8020)
Benzene
(by 8020)
TPI{ as Gasoline
(by 8015)
Sample ID
Table 4 - Stockpile 3 and 4 Analytical Results
(all result-s in rnilligrarns per kilograrn)
t
t
< 0.005 <0.005< 0.005< 0.005<0.5MW-3 @ t2.5',
<0.005< 0.005< 0.005<0.005<0.5B-5 @ 12.5'
<0.005< 0.005< 0.005<0.005<0.5B-3 @ lo.0'
<0.005< 0.005< 0,005<0.005<0.5MW-l (B-2) @ r2.s',
0.600.150.02o.266.0B-r @ 12.5',
Total Xylenes
(by 8260)
Ethylbenzene
(by 8260)
Toluene
(by 8260)
Benzene
(by 8260)
TPH as Gasoline
(by 8260)
Sample ID and
Depth
Table 5 - Soil Boring Sarnple Analytical Resutts
(all rasults in milligrams per kilogram)
<0.5<0.5< 0.5<0.5<50MW-3 (tLnug3)
<0.5<0.5< 0.5<0.5<50MW-2 (rur'/93)
<0.5<0.5< 0.5<0.5<50MW-l (ntnt%)
Total Xylenes
(by S260)
Ethylbenzene
(by 8260)
Toluene
(by 8260)
Benzene
(by,82oo)
TPH:as Gasoline
(by E260)
Sample ID
Table 6 - Groundwater Analytical Results
(all results in micrograms per liter)
<500Domestic Well <0.6<0.6< 0.3< 0.3
Sample ID Toluene
(by 8020)
Benzene
(by 8020)
TPH as Gasoline
(by 8015)
Ethylbenzene
(by 8020)
Table 7 - Domestic, Well Analytical Results
(all results in micrograms per liter)
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FIGLIREDATE:
NOVEMBER I993
PROJECT #A0065-002-otCAD F]LE:lB-6502VM
UPS SAN LUIS OBISPO FACILITY
3601 SACRAMENTO DRIVE
SAN LUIS OBISPO, CALIFORNIA
SOURSE: USGS 7.5 minuLe topographic map.
San Luis Obispo quadrangle,
SEACOR
Science & Engineering Analysis Corporation
3485 SaclarnenLo Dr. San Luis Obisrro, CA 93401 (805) 546-0455
VICINITY N4AP
l\
,
I
rll 4tane(
Park
4 .,.,)
Disposal
Trailer
Park
221
\1,
t"n @ I
20
Jli %,:-__.,'%2-'io r--
I
a 1/ "c
Trailer
Park
BM
i
B
,'lt\
I9
%
,oo
;;\ o,a
mpl 8.
'Pu
'---.-_Pio. o
Tta iler
'Gr
SITE
Pa rk
Si nshe
.Meadori Parkadio Tower
<.-J
R
,,r80
SEACOR
Science & Engineering Analysis Corporation
3485 Sacramento Drive, Suite A, San Luis Obispo, California g3401
(805) 544-0455 Fax (805) 546-0583
UPS SAN LUIS OBISPO FACILITY
3601 SACRAMENTO DRIVE
SAN LUIS OBISPO, CALIFORNIA
SITE L4AP
DRAWN BY DON PRATT
CAD FILE:
18-6502SM
PROJECT # aooos-ooz-or
DATE: NovEMBER 1993
Stockpile
s-10o
O s-rt
SCALE IN FEETr---------r
02040
PARKING LOT
UPS BUILDING
o
MW-3
New UST
Excavation
o
Cur Mrv-l (B-2)B-1
B-3 PLANTER
e
UPS Domestic lYell
ESTIMATED PROPERTY LINE
F
rI]
&a
HFiz
tstAForrner
Used OiI
UST
Excavation
s-4
Stockpile
PLANTER
B-4
Former
Gasoline
s-z;o
PLANTER
{
UST Exca S-DBf{t'1N}'i
o
B-5
O
o w-l s-5 MW-2
J!t
Stockpile
#t
Stockpile
LEGEND
O Soil Boring
B-3
O Groundwater Monitoring Well
MW-1
e Domestic Well
O Grab Soil Sample
s-7
O Grab WaLer Sample
w-1
FIGURE:
2
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APPENDIX A
Rinse Water Hazardous Waste Manifest
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15. Spccicl Hondfing lBrnrlior md Addiriml lnlomotion
li"tls$Jsney rssprylgel t3101 e4€-a{33
tuirb f27 - tri&frf, qfi;ifqprletre pl.oeactLrc
19 Urcropqnry- !_ndrcorbn
bock of Pale 6: :t).poffirtr o{ Tork Svbrtwa
:t :, Sdrffito.Coli{on*r'
Cqrtlol
Mornh,
Modfi "'DcY Y,aor
ildrh Ddy Ymr
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a{ro
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orsc 8O22A (12191)
ePA a7@-22
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d.
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trwro of fre'L
Sacts LlqukjftazafCauo
sb wltlro.
(irrluding PrcPor Tbrv'cf r6ii"a
I I us DOT Dcrriprim ShippttS Clc,ond
Sin Addra
Ef;a!{3000 Alai*rlq,
|/+5d 1lgr4 14 K#*S9F*ility 1.lfi.Dcigmicd did
,+
CorponY i*ir*
'l .'it.l. ,"i'
7, TsrPortrr
8. US EPA
\.'
6. US EPA ID
@se4
5.TrmsPort!r l,
h.fi.Acdcd,
Spce
DO THIS
Grccnr HAULER REIAINS
APPENDIX B
Non-Hazardous Soil Manifest
Date
#
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a
a
ao
-ot
a
o
$\o
q)(t
and date:Print or Type Name:
Dar.r*en R Bart I ett / Car-I a {loa I
Rerycling Facility ccrtifies the rcceipt ol thc soil coocrcd by tltis tnanifcst exccpt as noted abooe:
\E
o
E
Crtc
IJ\oc)E
Month
I
Print
-c
Typ"
sttcharryuayordclayingtrttractinglrunto,subaddiugoff-Ioadingtpitlrottt thcbeingdirectlytssoiltlnttltis4Sfrrthetcntifyreceiocd.IlWeuhcncmrdititm so iIsucltccrtifythntandabooesoiltlcsc'ribedtofthereceipIlWeacknouledgecertificatim:Transporter's bcing rleliaerad it aactly the sanrc
Sitc tn tlrc Desigtntcd Facility
(D
!oa.a^q(!\ts
Signature and date:YearDuyMonth
Print or Type Name:Consultant f,lGenerator Cl
cnfirely
arty uay.it tflalter zlouldorthatsuchsoiItoadoncaddedbccttItasutltrothixgaboacSitcsltounttheGencratiottfmttteluscetfifiedbyconpletcdandteShectDassortheSoildesctibedtntlnsefrontakanIterein,ssoilrefcreaccdthethatIlWecertifyconsultnnt's ceftification:Generntor's andlm
List any exception to items listed above
o
o
o
Gas
Diesel
Other
o
o
o
0-10%
10 -20v"
2(P/o - over
o
oOther
OrganicSand 0'
Clay O
o
o
o
Gas
Diesel
Other
o
o
a
0-70%
10.-20%
20/" - over
o
o
o
o
Sand
Clay.
Organic
Other
Customer Account Nunber with TltS:FAX #
(
Perc<>n to Cont.lct:
Transgrrter's US EPz\ ID Nc.Tran-sporter's I)hone #:
FAX #
4
Facility Pernrif NumbersFacility Phe'ne #:Desigpated Facility (fransport to): (nanc & atltlress)
TFS'fechnoiogi.ps Inc.
1 ;l3iig H i l: i st:Lt s 6lv en r.re
Ade
FAX #:(' t
Percon to Contact:
BETX
Levels.
Site Phone #:Cenerahrx Site (Transport ftom): (nnnt & aLldress)
u, p. s.
36IZI T SRCRAf4EFITI] DR.
CAN LUIS OPISFI]
Customcr Account Nurnber rvith TPS:
6--5.f Cst
Fr\ X #:
Consultant's Name and Billing Address:
F'E-TRN BUII-I]HRS INC.
I.fi6CIg PfIIN'TER ilUE.
withAccountNumber
36
U SE
.t
RUICE
DR-
_ll
Truck #: :
TRANSPORTER'S
.:Yt,
\;-:::- *
r
a 'Dab:of ShiPmecrb
.''i 'j-+ : :1'
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Prlnt or Type Name
I).:rl-r-en F. H.rr- b i ett ,/ Car- 1 a Cua l.,,/ghg('
and date:
Tmnspottt's catifcation: IlWe acknouledgc receipt ol the sllil ilesoibed abooe and catify that such soil is being itelioered in uactly the same
cottdidott as athen teeioed. IlWe frther cetify that this soil is being directly fianspmted ftom the Geteratior Site to thc Designatttt Facility
tttitlwut off-loading, adding b, srbfiactiagltom or in atry uay ilelaying ilelioery to such site. . .
Reqcling Fecillty catifies tlu receipt of tle soil cooeredby this manifest acept as noted abooe:
Discrepancieo:
t\'Cc
{;
',1
;:.1
..r.
?lL-uil)
q)
r:
Signarure and date:Printor Type Nane Monthi, !3y YearConsultant OGenerator O
thAt
any atay.it tnelta
of to toouldiloneaddctlbeentesuchhasandaothingshotottabooestdtcGenqatimtfmbVmelusccrtifedcotttplcEdandDabSttrrtsoil,
SoiIsoilsdesqibedlro-thoseentirelyt thetakenhacintssoilref*encedthecertiflthlIlWccatifcatlon:andlor coasultant'sGataatot's
o
o
o
o
o
o
o ?7Other
Organic
I ''i
Sand
Clay
List any exception to iEms li6d above
C,ag
Di€td
Other
0-1096 cI
70-2001" o
200/"-c;w O
1tn
o
o
o
Cag
Die8€l
Other
o
o
o
0-10%
10-20%
20lo-g,vel
o
o
Sand'
aay
Organic O
Other O
l,id.l Dccriflion ol Oclivny r :.hiror.q*i:d.Gffidrye:'.q,Ffien$@'E$
- i. r;'li l:..
'.::r: -ji :iii- i
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D;rrr*l:n E,;rr^i; l. .: i:'i:
( {]rr.1[t ) tltr ;,i*i]',1'fi 1.
ar]sc{iri1.i .l ia r il.,; ; i- i r:, I ::; i.: : i i .,\,1i:a{' !,
li,-.::tr::::.:Ci i::C:ir: ' i - ri l".,;:..rl :.
F'$ Techrro1oni-:r.,,
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rJ e 1 ,alr t rl , il;t I i. i:ct r'ti i a
.:,.!.1::i j
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itji 5{-1CRAl'1Et'lTO DFi.
f-r (:
r, orrsrril;rrrt's fl,:rrle antJ ifi;!:l^;1 A.li!r;:ss:
ETRO BUII-DER5 1N[.
r,6tArl Pll tl{TEP AUE.
;iNil'fi i:E :it-'f{ lf.ltr=? []A 9Ei.;'rA i :i I ra ) 9.i6 -:j:j95
Bi.IF G l RT{RD
i31O) 94tu'*i!:;:rfi5
. rr:. il:'r' .tr,, ' r;jrl \i,rii. .: r,ltlr .l l-tl;
I ti:rsr:n ici {]^:: :i :.1 :
N l.-t,JIS 0SISrrt], CA
ftCEI-t?SE (,ct:IFi)FIR
ltliriancl ..1dd:cs:,:It i;ii\i:rrr.:
e.q'1 , sACRrlmEFl'T't) IlR. ,
TianSporter Tmck #:
I .t .. ...: : : t
. r' .:rl. 1 ": , -,, .AhITDFISLJL-T
o frir l';r1-tnl,'rt:
. -J r r. ..i ij. . : . ...,;r.:,-.,Plarl typc..TMNSPORTER'S COPY
r r,J. recnnorogres borl Kecyclmg
Non-Hazardous Soils
i*\:r+5
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;:tr:ri i'riiliii r'' i';, ;r,r rr-::rr'fechnologt'e:;1.;;i\", i .,t-,rt :r,::..jyt,-.; l
f nc.I( EAAr ) Sir e-Aul';t 1
fa,::l:i . :;:::.1'ri:,:\i,i.,.r-::
3ii:S Hi bi 5r,Lis dlverit.rg iJ.arr.'t:n F*r i: I et b
delantu, ll,-il i f nr-n i.r (];:i lkl t i 6 ;. t) ) ,:i4h -l3lz|la4
.:'rl::i: 'i l';i:lf Ti'1-:
I8t*W€ighf
Sand
CIuy
O Organic Q,
O Other O
0-10% o70-2M O
2Wo-ov€l O
Gag
Diesel
Other
o
a
o SD
Sand
Clay
o
o
Organic Q
Other O
0-10%
10 -?01"
2Mo-svq
o
o
o
C,as.
Dieael
other
o
o
tr 642 43
List any exception to itsra lisH above
Ganerato/s andl or consultant's ccrtifcation: IlWc
Datc Shet cotnplcted aad certifedby melwfm thc
elta it in any rDay.
clttifV thtt tlE soil tefaenced hcrein is taken entirely lrom thosc soils desctibed in the SoiIGenaatiott Sitc shotot abooe and nothing hasbem idded or done to such soil that uonlit
Print or Name:o o Signarure and date:Month Day
Transp orter's c ertlf c a ti otr :IlWe acknouledge reccipt of the soil des.ribcd abooe and c*tify that strch soil ts being delioesed trt dactly thecondition49athertweioed.IlWe fi*her ceftify thtt this soil ,s being tlirectly safle
toithout of-loading adding
transpottcd ftom the Genera tiort Sitc ta thz Designatcd Facilityto,*bhacting lrom ot tt afly @4y delaying dclioey to sttch site-
Print or Name
Y7',n ,
Dirrepanciee:
te/
Recycling Facility certilies thc receipt of thc soil coored by this manifest aceVt as notcd abooe:
Print or Type Name
Oar*r'en R
date:
Bartlett / [ar-la Coa.i e
I 3
'zr
l
t:Qhi t_t.1i 5 [rE ] $p(]. cA
$tr-iftttflt4Er I i':l Dfi _
Siti:,,1r-'r.lt. ll ii,;yn,. ,"r-:::,. ll :,..:.ii
CIh'ag PAIFI ER AVE.
.;:.:AFI'If] [:E sF,R I NGS, t*lF] gl:16 7[1
,,.{ l ili,.^ ^.1f,-..- ..ER|; INII^i ;ll'o'l"br+g-e ,:g:i
F, "&?Fi'ffsd'
i:-r1o) 9r+6*539iI
. LIS
.,:' "' el i1:
i;FAtplNo
: i',. s.
.-:r-:r n l(l C{)rlt.ict:.SACRAf,IENTO DR.
TffiRBEI-"'.HTKIJTEE
LIJI $ OF rspflr CA
''b'i'iis'iiil -tliiN r' ""Transporter Tnrck #lDate of Shipment:
ah8g #
I
TMNSPORTER'S COPY
Print or Type Name:
[)ai'r"en R Bat'tlett / CarIa Coalr lqs ,
date:
3l/
Rccycling Fncility ccrtifics the reccipt of the soit ctwcred by tltis nanifcst cxccttt fls trotcd abooe:
{
\
o€lI
Arr
()
Iq
Discrepancies:I
I
q)to
a_(rt
rqf
rF
t this soil is beiug dircctly transportctltotn
in any way delayiugjcttuAyto suph sftc'zuithotrt off-loading, ailtlitrg to, subtracfittg ftmtt or
condititm as when receioctl. IlWe firther ccttify tha the Gcnetation Site to tlte Designted Facility
tltot sllrh soil is being delioeted ir exnctly the sameTransp or ter's c er tifi c a ti tm : II W e acku oul ed ge receipt of tlte soil dcsctibed abooc aud cntify
Print or Type Name:Coroultant qCenerator O Signature and date:Month YearDry
Gancrato/s andl ot consul
.Date SIrcet cotnpletcd and
alter it itt artY.uaY'
taflt's ccrtification: IlWe ccrtifu tlnt the soil refaranced hetefu is tnkcn cntirely from thos€ soils desctibed in the'Soil
certifed by nelus for thc Gcnaratiott Sitc shotott abooc and nothhtg lns bcut adilcd ot donc to suclt soil that
.zaould
List any exception to item$listed above
o
o,
Sand
Clay
Organic tr
Other O
o
a
o
Gas
Dicel
Other
0- 10v. o,10-20% o'7H6-over O ffiq
Customer r\ccount Number rvith T1€:
Transporter's DOT No.:
o
o
o
o
o
o
o
o
Organic
Transpr>rter Name and l"{ailing Address:
Other
)
to
'iransporter's [)hone #:
0-70%
10-20%
209; - over
Gas
Diesel
Other
Sand'- O.
Clay O
FAX #:
(
Transp'orter's US EPi\ ID No.:
"IAX *: '
/A i 4r \ i:'A*-.''fltitlt
n -.-.L 1 -- l- !
Ir6rSY{'S tortPR f'-- - o'."c' r-
Desigrated Facility (Transport to): (nane €t addrcss)
TFS 'fechtro l r:q i e5 Inc.
1P3-:8 Hihi e{*'Lts Avent-te
L1,{a I nn{-n f',,r 1 i fnrti: qiLiil.;11
Facility Phone #:Facility Permit Numbers
)
F.,\X #
t
AVC.
Levels
I)ercon t0 Contact TPH
Lcvcls
Site l]hotre #:BETX
Levt,ls
r\J
FAX #:
(
"1fi)
t1^4+ti-5.;;qi
Customer Accorrnt Number with TPS:?
p[SrlYS/cntitF :':E 13 J
t-.
rr Y nn ntl
Corurrltant's Nanre and Billing Address:
l
PETRO BI.'ILDERS INC.
11160'9 PflI[\ITER ffUE.
Ceneration Site (TransPort froml': (namc & aildressi
u. F]" 5"
"3hfi I SiilcRf:rME:hlTO DR.
IALIJ I S NF'
Consultant's.Phone #:
Person to Coritact:
FAX #;
Trartsporter Truck #:for Pavment:
I
'.,ii,
:rj{ [
Load,#
jfiji,t lij:'
Given by TIrS:Facility #:
TPS fechnologies Soil RecYcling
. Non-Hazardous Stlils
,!iPment:
q) ' ,rerikrr's Nanre and
UNITED F'AREEL
36AT SNCRRMEFITCI DR.
'j
1:,,r;,1:ili!!. -i.''ir.,iti. \t - .:;.,. ti.r 'i;l '
,,i_j:. :.:,,
1 ,-::
,,Ji'' r ,;i'l.
. a .-
N
qqoo
.ot
G
o
G
q)
o(I
I
I
{
t
\
t
t l. t '-".-.t ,..- I
t
I
t
'l:
r,
.dnerah)t'; Nlame and Biliing Address:
f;..,
UNIT€T}.: F'ARCEL SERU ICE
3e'OT $ACRAFIENTO DR.
BAN t_t.t I EiF,N
(!
thqoo
ot
(!
(t
TRANSPORTER'
Print or Type Name:
Darretr R Bar"t lett / Cat'la Crralt ti 3
re date:
Rccyclfug Facility ccrtifics the reccipt of tltc soil coocred by this nnnifest exccpt is notetl abottc:
\
Eo<t\
cttc
(v\Ic
'i..
*ratType Name:
Discrepancies:
DayMonth
o!oa-latr(E
l--
Sitc to tlw Designted FacilltY
sueh soit is bciug deliancd in aactly the sante
Print or Type Name
'
-i2;!" :
Generator O Consrrltant O,Io"' ll"1Signature and date:Month
Gareratm,s afidlot consultant's,c*tifcntion: IlWe ccrtifu that the soil referenceil heteit is takcn cntirely fton tlnse soils described in
Datc Slcet conplctcd and certified by melus fm the Gaieiatiott Sitc shozurt abooe and nothing has beor added or donc to such soil tlnt
altt it irt auy uay,
the Soil
uould
List any excePtion to items Iisted above:
24'70
F_o
o
o
0- 10%
r0-20%
2V/o - over
o
o
Sand
Clay
o
OOther
Organic o
o
o
Gas
Diesel
other /
Customet Account Nurnber with TPS:'
0
Transporter's DOT No,
o
o
o
Transporter's l)honc #
,
Name and Mailing Address:
to ContacL
0-10% o
10-20% o'
2(f/o-over O
Gas.
Diesel
Other
Sancl Q Organic O
Clay O Other O
FAX #
(
TransFrrrterls US EPA iD No.:
FAX #:
dA t q ) ::,/+f1,_Rultalr
l;ErEfrIb'co'S&t:--L)VJEr tr
t1n.....-+dr- trtrsr-* l o* I
De'sigrated Facility (Transport loJ: hanr {t ad,Iress)
TFS Techrlologi.eri Inc-
1:.388 l-l iili !icr-(5 fiven'-te
6'lrJe1anttr, llal. if nr.n { -r c}i3.1tl 1
Facility Phone #:Facilitv Permit Numbers
)
FAX #:
t
AVC.
Levels
I)erson to Contact:TPH
Levels
Cent'ration Site (Transprrrt from): (natne {t adircss)
u. p. s.
3601 SACRAIYIEFITII DR-
CASAN LUTS CIPISBI]
Site Phone #:BETX
Levels
FAX tr:
t :l !. ra ) ')4t1.-1.195
Ctrstomer Accottnt Nurnber with "[?S:
.......-:lg/-.JtLl
Pcrson to Contact:
n('rI: a: T c)a\tff\
$onsrrltant's Name and Billing Ad&ess:
F,ETRCI BIJILDERS INC.
1'A609 pAINTER llUF-.
aATn(1:iAFtl-A F E eiF f? tN i:r: Tll
Consultant's Phone #:
FAX #:Cugtomer Account Number rvith TP.S:,i.. : r
.:. 't : ,
Pe,rson trc Contact:
6enerator's Phone #:" ''f
' ;!:
Transporter Truc\l!_,, .'
,1 , ',,;_ .. ' 1i.,,
for, Pavment:
.TPS Technologies.,soil Re-qygllqg'
.,',,, Non-Hhzard6usSoilsi:*.',,'"r:.:'i, 1i
I
t
a .re of Shipmenh..,. ,r
'-'.l Jr' ' .r; .. .'
Cenerabols Namd ald Bilhng Ad -
ess, ,'
UNITED FiASCEL SERUICE.
36Ar S'jICRHMEFITU DR"
G
tn
oo
rot
G
TMNSPORTER'S COPY
Print or Type Name:
D;lrren R tsartletb / t-lat'la Cc.rlt tt'k lq3
date:re
\
oGtt
Crt
TJxooc
as noted abouc:Recycling Facitity cotifics thc receipt of tlrc soil cooercd by this nanifest
Dirrepancies:
Type Name:nt or L
YearMonth
o!oa-taq
G
tiut: IlWe ackttouledge receiPt of the soil desctilnd abooc antl cntify tln ing delioetad in exactly tlcsame
Sitc tu tltc Designted FacilitYfrthet certify,tlnt this soil isbeing directly transportcd fton
to,. sabtracting fron or in any way delayitg dclioery to such sitc.uitlrortt off-I o ailiu g aild ittg
tlrccmtdition as railtctr receiocd. IlWe
Transpmter's cntifica t sttch soil is be
Print or Type Name:C€nerator O Consultant O l,t"-Signature and date:Month D"y
atty 7udy,it tnalt*
usDateSheet ,roccrtiliedbycmtpletedand otSitcGetcratiotrfornelthaltas-beattltingandsltotr'r,t abtwe todonededad such tlnt zuouldsoil
on:Generotot's consul tant'sandlm 5etllWecertifycertifcatitnkcnertihereittssoilrefcrenccdthetha soilsthorelylrn*tn therlesc-ribed Soil
List any exception to items listed above
o
oOther
Organic 0- 10% o10-20% o
2tlo-over O
Sand O
CIay O
0
o
o
Ga*
Desel
Other
L'/-{ks
_\
qD
Customer Account Number with TllS:
0
Tians?orter's DOT No.
o
o
o
0
o
D
o
O
u
o
Transporter Name and Mailing Address:
Other
Organic
)
Sand
Clay
to
Other
Tran-sporter's Phone #:
0 - i0')/"
10-20%
20plo - over
FAX #
(
. Gas
, Diesel
Transpr'lrter's US EPz\ ID No.:
(
Designated Facility (Transportlo): (none [t rtddress)
TFg Te.:hrtol.r:qi e:i Int:.
tP;;:B Fl il:isrrr-tE Avetrrte
^ y^n i e q::r ilTl 1C\dp1:r'hn- {--nli
Facility Phone #:Facil-ity Permit Numbers
)
FAX #
(
AVC.
I-evels
Person ttt Contact:TPH
Levels
Gerreration Site (TransPort from): (nane & address)
U. Fr; S.
.3601 SACRAIYIENTO DR.
CA5AN LUlS OF'TSBO
Site' Phorre #:BETX
Levels
FAX F:
( .i r cl ) 946*5:iC5
Customcr Accottnt Number with TPS:
P.-'l'"iit t.;iilF
Ift1f1 rlYtr){flftl
Consuitant's Name and.Billing Address:
PETRO BIJILNERS INC,
106r49 pfl I N'rER AVE.
STTITA F.E SPRI c/-1 9trr'
Consultant's Phone #:
FAX #Customer Account Number with TPS;
Person to Contact '.
Gencrator's USEPA
6
by TPS: '.,;.;. ri;..
' . 1' l:t'', t1i'a]
l 4I+5 it:: ': " \ :;:'
#
Technologies So
, Non'Hazardous
il
Soils
PT S Re cycling
1
/ V{-tt''::'
t'
(J ment:.'r'1'
,rtor's N:une
J Il'ED PA ERU I CE
j6o1 SACRAtt{EFlTo DR.
r.]
(E
o
oo
ot
a
o
IE
o
o(5
; . ;L-d 1f1111:1r1:l:' ;:iY. 4i f ,:COPY
Print or Type Name:
. Dat'ren R Bartlett / Cat^1"r CoaIe t,lzlqz
and date:
0
Recycling Fncility ccrtifies tlrc recciltt of tlrc soil coocrerl by tltis nanilest cxccpt ns noted aboac:
\
=o,i
Orc
o\IJoq
Month
(
or
Day Year
atpitltout 4ily TDayoftltlittgto,ocrytt,tfictirtg Itottrsnb tocleliilclaying suclr sitc.
ort asconditi receiocd.uthcn llWe tracntifytlntfrrtherdircctlylsbeitgthissoil nsportccl ftonTransporter's llWe tcntificatim:ackttourl rcceipcdge tlrc anddcsaibedabozse"f soil tlncntify
Signature and date:
t srtclt soil is beingdelioncd in aactly tiie samd.' '
tlrc Gateration Sitc ttt tlu Dcsigntcd Facility'o1ioa-
UT
at
F
Print or Type Name:Generator O Constrltant Cl I '"lrSignature and date:Month D"y
Carctato/s andlor consultant's certificafiott: llWe certify that tlrc soil tefetanced
Date SIrcet cotttplcted and certifcil by trclus for tlrc Gurctatiott sitc shount obotse
Itnein is takat entirely fron those soils desc:ribetl in thc Soil
and nothing has beu addctl or dottc to srtch soil that uould'
alta it in atty uaY,
List any exc€ption to itemi listed above:
Sand
Clay
o
o,
o
oOther
fl
o
o
Cas
Dsel
Other
o
o
o
0 - 10"/"
10 - 20'1"
2Wo - over
,l
Customer Account Number with TllS:
400
Transporter's DOT No.:
o
o
o
o
o
o
o
o
l0%
-20%
Transporter Name and Marling Address:
)
over
l0
ztr/"
Sand
Clay
ire*<>n to Contact:
Transporter's l)hone #:
Gas
Diesel
Oth€r
Organic O
Other O
FAX #:
(
Transporter's US EPr\ ID No.:
F.AX #:
{ t! l. g ) e4e'*8lZlfir}
i;'co'iAci-
1*r.rr.r*c.ri Fi"er''L .l e i, t
Desigrated Facility (Transport la): (nane {t ail'lres;)
TFS Techitt:lcJgSies Inc,
1e:1i18 Hi l--i:i sr:.'r-l 3 Avent-te
ficlelantcl .California 9i:r:i[tt
Facility Phone #:
/ ^,adr \ ,1 i- r_, d inrn I
Facility Perrnit Numbers
)
FAX #:
I
AVC.
Level-s
Person to Contact:TPH
Levels
Cene'ration Site (TransFnrt ftom): (natnt & aidress)
lJ. F. S.
36rAt SACRAIVIEFITCI DR.
sRN LUIS OPISBO. C'1
Site Phone #:I]ETX
Levels
FAX *:
{ 31C') 946*5..:i95
Ctrstomer Accottnt Nurnber wiih TPS:
Person to Contact:
BT'T4 G I RARN
SAFITA FE gPRINGS cFl 91/J67&
IT DERS
rNrEntr0fr69
R oPET I r'lc"
AVE.
'and Billing Address:
1,? 11(h\
Consultant's Phone #:
FAX *Customer Account Number with TPS'I
Pt'rson to Contact;
n1lTr**t*:ir,ii"
TPS Technologies Soil RecYclingt' r, Non-Hazardous g;ilg '; I ':i
>
1
l.
.Pment: :
-"
- ' l".':.
ct
atr)r's Name dnd Billing Addres: ,
. ...,,.,.. .- : t,..:JI-TED PARCEL SERUICH
Ji6|a1 sAcRAmgf\t:ro DR.
(E
f,ta
oo
rot
G
o
G
Q)co(5
TRANSPORTER'S
Z€/ot- //414
SignaturePrint or Type Name:
Dar.r.pir R Barb1ett / Carla CoaIe
Rccyclittg Fncility certilics thc reccipt of the soil coocrert by tltis nnnifest exccpt as notul abooe:
\
o(utL
Crt
tJ\tq
Transporter's cntificatim: llWe acknoutledge rcceipt of the soil t stralr soil isbeiug delioeted.in,_aaetly the santc,
tlrc Gdrcration Sitc to tle Designted Facility. :- .: ... .
curtlition as ailrcn receioed, llWe fitrther cntify that'tlis soil is
utitltout off-Ioadfug adding to, stbtractingftorn or hr auy uay to srtch
beiug tlirectly ttansporttd lrom
rlcsc:ribed abooe and ccrtify tltaoEoo-
a4c(tr
li
I
Signature and date:YearD"yMmthPrint or Type Name;Consuitant OCenemtor O
Geterator's atdlw consultant's certif catiott: IlWe certify that the soil refcrenccrl hetein is taken entirelq ltom those soils desc,ribed in ttrc SoiIDate SIrcct conpleted and ccrtified by nelus for the Gurcratiott Sitc shoun abooe aud notlthry has b"c1ifra"a or d.one to.sucl soil that zoouldalter it itt a,ty rDay, l
List any exception to items listed above
77 .n(
a
o
o
Gas
Diesel
Other
0- 10% o10-20% o
209o - over O
Sand O Organic O
Clay O Other 0
Customer Account Number with TIISi
tluwoz67Coalv/b
Transporter's DOT No.:
Transporter's US EP:\ ID No.:
o
o
o
o
O
o
o
o
o
o
Transpr>rter Name and Mailing Address:
Other
Organic
)
Sand
Clay
Contact:to
Tran-sporter's I)hone #:
Gas
Diesel
Other
0- 10%
10 - 20v"
20oh - over
FAX #:
I
FAX #:
(61.9) Er+6*8t4tl4
Peiftii loConTatti'
'O=r*nan Et:v't I..1'*
FaciJ.ity Permit NumbemFacility Phone #:Dt'si6natt'd Facility (Transport to): (nanrc {t address)
TF|S TerltrnoloEies Inc.
leieB Hihi si:Lr5 flvenne
r'n i €l tiE;i0 lArJelanto" [a l i f'rr
AVC.
Levels)
FAX #:(
TPH
Levcls
Person to Contact:
tsETX
Levels
Sitt' Phone #:()
Ceneration Site (Transport from): (natne a uildress)
L.J. F'.5"
360T SACRAMEN'TO NR"
sAN LUIS 0FISE|O! CA
Customer Account Number with TPS:FAX #:
( -1 i. k]) q46 *5.i9 5
i'crilii lo'Con-taiti
Ff']R G T t?f.lt?n
Consultant's Phone #:Consultant's Name and Billing Ad&ess:
F'ETRO T\IJILDERS INC,
f06'49 ITRIFITER AtJE.
CR 9rzlr_.7rzlTFI FE $trRl
FNX#
' Person to Contact: r
TPS Technologies Soil Recyclingr, Non-Hazardous fuils
ry:.-._: .'- -.-:- -_=_-:::::- __=_:_:. -.,: -
o
I
and\(iate:
Print or Type Name:
Dar.r-en R IfartietI .r' iar. la rloai
Rccycling Facility ccrtifies thc rcccipt of the soil coocrcd by this uranifcst exccpt ns noted above:
dSignatu
1.r
Print
-p
Typu
thc soil referenccd hcrcin is tnkcn uttirely /ron those soirs desc-ribcd in thc soilSitc slrount abotc nnd nothiug has beou iiaoa or dortc to sucrr soil that zpottrd
Signature and date:
o
o
0
o
o
o
o
o
YearMonth
o8
D"yConsultant OGenerator O
Sand
Clay
ru4y delayinganyortrtftotrtto,subftactingadilingo//-t oadingtDitttortt tltcdircctlytsbeingsoiltthisccrfifytlnasIIWefrthctreceioed.wlmncotttli tiott t sttclttltn soilandccttifydcsctibedaboocsoiltltcreccilttofacknoutledgecertificatitm:IlWeTrausporter's
Gateratot's anrllw consultatt,s cerfificntiott: IlWe ccrtifu that
Ddtc Shcct cotttpleted and ccrtilicd by urclus for thc Ceucratiortaltn it in arty way,
List any exception to items listecl above:
nt or Type Name:
bcing dclioetcd in aactly the sanrc
Cas
Diesel
Other
0-10%
70 -20,/.
2ff/" - over
Organic O
Other 0
Sitc to tlrc Designtcd Facitity
tuJl^Qi.e3017:8tlo
o
0
a
Cas
Diesel
Other
o
o
o
0-n%
10-20%
70t% - over
tr
a
o
o
Sand
Clay Other
Organic
Customer Account Nurnber with T[)S:
Transporter's DOT No.
'iransgrrter's US EI)A lD No.:
Transpr:rter Name and lv{ailing Address:
irerson to Contact:
Transporter's Phone #:
FAX #
I
FAX $:
ii l'+i ;;t4ri-gtijr34
i'}di.ihriib Coffilli *i {'rs-'l r.
Ilrrv.': ti iJa,r.t'[ or: ::
Facij-ity Ptrmit
i ,rra,a 1 -r,- r-.
Facility Phone #:
Desigpated Facility (Transportta): (nanrc fi address)
TF15'TecnnttI0gies Iirc-.
1E -:jl:jg i-i i ir i st:r-r s i-l v L- rr r-r q
Arl eic.ni:o, llar. i. Fr:r-r-ri a !;::trll.
!
FAX #:AVC.
Levr'.ls
TPH
Lt:vels
I)ersorr tt"l Contact:
I]ETX
Leveis
Site Phone #:
l'
Cenc'ration Site (Transport ftom): (nant & atiLlress)
u. r.:,. s.
JbU 1 SRf,Ti']MEhITCI DR"
u.i{sAN I*U15 DF'ISF{]
Customer Account Nutnber r.vith TpS:F..\X *:
i:J d) 146--;1it1 ";
t'(.rsun to LOtrtact:
RTiII ii i FA RN
.. ntr i} \ - r)j,.1.-,-:r.:,()t-
Consultant's Phone #:
Corrsrrltant's Name and Billing Adclress:
F'E.fI?f] BIJILDERS INC"
ltzr5rztg t:,ftINTER FiuE.
sl:R I5tq A 91116 ?fic:
Customer l\ccount Number with TpS:FAX #:
Person to Contact:
Cenerator's US EPA ID No.Cenerator's Phone #:
UN I TED F'ARNEI. SERU I CE
36At'ii-'tcRAtYtEhtTo DR.
I
r's Nirme and ISilling Addrq;s:Cenerato
Load #
A*A
Civen bv TPS:Facility #:
I
Transporter Truck #:
-hqrAt t! TnLtf
Resporsible for Pavmcnt:Date of Shipment:
N
tn
oo
st
a
o
G
o
q)(t
TPS Technologies Soil Recycling
Non-Hazardous Soils
\
,o
,qt\
CD
R COPY
APPENDIX C
Tank Disposal Certificate
T
t
[:-;
t-
t
M&IIT SALVAGE
2105 OTIVERA ROAD
NTPOMO, CA. 93444(80s) 349-031 4(B0s) 680-07ss
TANK DISPOSAL CERTIFTCATION
t'
I
This is to certify that M&M salvage has in accordance with
applicable local, state and federal rules and requlations
properly disposed of the following.
CUSTO}IER PETRO BUILDERS
EXCAVATION LOCA TION N/A
TANK IDENTIFICATION
IDENTTFICATION NUIIIBER U/A
SIZE ONE 1 O OOO GALLON AND ONE 550 GALLON
CONSTRUCTION STEEL
PRODUCT N/A--S HIPPED TO US RINSED NON HAZARDOUS
OTHER
r certify that this document and all attachments were pre-
pared .,.r&er my d5-rection and supervi-sion to assure that
iualified perionel properly disposed of the above noted
fanks. Baled on my inquiry of the person or persons who
managed the progran asJignments, the above information is
truel accurale ind compl-te to the best of my knowledge.
'fil (rC o-/< t3
L
I,TIKE MCCOR}TICK DATE
APPENDIX D
Boring Logs and Well Permits
I'
)
- Cement
Total depth at 14'
2-
4-
6_
B-
10-
tz-
t{-
16-
18-
20-
21
-
28-
2a_
5
100
>1000
tB/2i/
2A
r7/2i/
30
20/
30/
50
t5/
20/
40
lllltry)
,ll//z)
lZZfu)
t /t ll:
t/441t
t /'4 /4:
tll/lt
tllllt
tlll,tt
dTzlql 2
4llllt
t//llt
///v4t
tr%/4t
t%74t
Mottled green and yellov-brovn SANDY CLAY, tret, low plasticity, moderate hydrearbon
odor, hardCL
Mottled yellor/ yellor brorn SANDY CLAY, moist, lov Plasticity' hard
slight hJrdrocarbon odor
cL/
SCI
Yellor
clayey
brorn and black CRAVELY SAND, motst, flne-to coarse-gralned, subrounded
sand, very denseSW
Yellow brorn CLAYEY SAND, moist, fine grained, trace caliche, vert denseSC
Dark brorn/black to Srey CLAY, molst, medlum high plssticity' hardCH
Bro*n SANDY GRAVEL, molst, fioe-to coarse-Sralned (base)cw
BORING ABANDONMENT/
rELL CONSTRUCTION DE'TAILSLITHOLOGIC DESCRIPTION
(color, solt clas€ificatlon, molsture, grrln elze/ plastictty, density, other)
3
6
aFAa
o
r
q
o
ts
ia
J
&
Fz
J
.ST ACOR
STABILIZED I{ATER LEVEL (BGS): NAFIRST VATER (bgs)r None
FINISH DATE/TIME: octot'er 14, 1903START DATE/ TIME: october 14,1003
MONITORINC DEVICE: OVA l2BSAMPLING METHoD: Hollor Stem Augeri Split Spoon
LOG OF BORING:PC.l OFI
B-1
LOGGED BY: BOB wILSONSUBCONTRACTOR AND EqUIPMENT: West Hazmat Drilling Co.: B-57
FILE NAME: 1B-B502B[BORTNG LOCATIoN: South Vest of former UST
PROJECT l: A0065-002-01PRoJECT: UPS San Luls Oblspo. Ca
r
r
t
t
I
t
I
t
I
lYell cover
Cement
PVC Blank
Bentonite grout
l3 Sand
PVC
0.02"
Scren
glotg
Total depLh of rell at 30 feel-
Groundrater encountered st ?0 feet
4.-
6-
8-
10-
t+-
16-
18-
20-
21
-
26-
zB_
32-
5
I
I
t4/.6/
25
t2/.ts/
2E
ts/
35
L7/
z5
ro/.
20/
15
20/
35'/
15
t5/
30/
35
25/.
35/
50
20/
30'/
30
Bronn to yellor brown CLAYEY SANDSTONE (b€drock), moist to tet, very dense
Yellowish brown to brown SANDY CLAY, moist, low Plasticit,v' trace black sPeckE hard
trace clay films on fractures
Reddish brown to brown CRAVELY CLAY, moist-to wet, lot plasticity! sme sand,
subrounded grovels and aand, some black specks (reathered bedrock), hard
becomes harder and drier, trace cobbles up to l diameter
CL
Brorn to greylsh broFn CLAYEY SAND, moist, flne grained, sllght eptlc odor, very densesc
Dark brorn/black CLAY, moist, medium-to high Plasticity, hardCH
Brown SANDY GRAVEL, moist, fine-to coar6e-gtained (base)
BORTNC ABANDONMENT/
WELL CONSTRUCTTON DETAII,sLITHOLOGIC DESCRIPTION
(color, soll clssslficatlon, molsture, grait elze/ plastictty, density, other)
Eg
o
o
F
E
a
Fa
t
J
@
J
&
tsz
E
q
h
"SgACORSTABILIZED WATER LEVEL (AGS): 13'FTRST VATER (bgs): 20'
fINlsH DATE/TIME: 0ctober 14, 1993START DATE/ TIME: October 14, 1993
MONIToRINC DBVICB: oVA l2BSAMPLING METHOD: None
I-OG OF BORING: PC. I 0F IMw-1(B-z)
LOGGED BY: BRUCE CUTTINCSUBCONTRAC'TOR AND EQUIPMENT: West Hazmot Drilling Co; B-57
FII.F NAME: l8-65O2MWlBORING LOCATION: South lfest of B-l
PRoJECT #: A0065{)02-01PROJECT: UPS San Luls Oblspo. Ca
r'
L
t'
t
Bentonite grout
Total depth at 15 feet
4-
6-
8-
l0-
14-
16-
18-
20-
21
-
2g-
30-
.\2
-
3
l0
I
I
Lt/t2/
l3
rc/ih/
T/
20/
30'/
50/
25/
l,.0/
80/
6"'
t/z2r*t
/ll 2'.1 ,
t l/// rry,
(llltt
t//l 4lt
t/1 r'/4/
r/lllt
t rrl /t/,
'fll/4t
tlllzt
t//lll ,
tllllt
tl4//t
tryl/2,
t//tllt
tVl/lv
Yellor and red CLAYEY SAND,/ SANDY CLAY, moist, hsrd' fine grained (weathered bedrek)
crey snd reddleh bro*n clayey dandatone, molst, (bedr@k) very dense
Becom€a drier and denser
cL/
sc'I
I
Yellow and greylsh brown mottled CLAY, moist' hard' lotr plssticityCL
Reddish brown GRAVELY SAND, Eoist, fine- [o cmrse-grained, trace cobbles up to
l" i[ diameter
sw
Reddlsb brown GRAVELY CLAY tlth cobbl€d, Eoist, lov- to medtum ptaatlcltJCL
BORING ABANDONMENT/
f,ELL CONSTRUCIION DE-TAII,SLITHOLOGIC DESCRIPTION
(color, eoll classlfication, molsture, gtsjn elze/ pla6ticlty, dendity, other)
3
s
o
@)
Fo
e
ar
Foo
hFoJq
J
Fz
J&
=
.SgACOR
STABILIZED WATER LEVEL (BGS): NAFIRST f,ATER (bgs): None
FINISH DATE/TIME: 6:00pm October 14' 1993START DATE/ TIME:4:30Pm October 14, 1003
MONITORING DEVICE: OVA l?BSAMPLING MtrIHOD: Hollor Stem Auger: SPlit SPoon
LOG OF BORING:PG.I OFT
B-3
LOCGED BY: BOB wltSONSUBCoNTRACTOR AND EQUIPMENT: west llazmat Drilliog Co.; B-57
FII-E NAME:1n450283BoRING LOCATIoN: South vest of B-z
PROJECT l: A0065-002-01PRoJECT: UPS Son Luls obispo, Ca
L
If-
_ Cement
/2/z 4z
ll tvl
//& ll
ll Z/t
/t zl
/2 trZ
ll lt
ll 4z
ll 4l
//l ll
/ry ll
lz /4
,/l zl
ll lt
,trl lZ
72 ll
lry ll
//t/ ll
/,/ lz
/// r'/l
fz 44
ll,{z
lZ /r'l
// /4
zz lz
/4 rll
// /4
lt //
lz //z
//z z'z
fu //l
?v4 lZ
Total depth at 30 feet
No croundrater was encountered during drilling
borlng ras left open for apProxlmately-4 hours-to observe for groundtater
1-
8-
l0-
14-
l6
18-
20-
24-
28-
30-
0
0
0
0
0
s/t6/
tB/
35/
35
857
6'
30/
75'/
10/
75'/
8"'
35/
,30t
60/
6"
60/
a"'
roo /
2"
ao/
6"'
Greenish prev (eathered CLAYSTONE lbedrrck), abundant caliche, trace char'odl,
some l/2-eulrounded gravels (chorcoal end serPentined)
Color change to greyish brotn
Some green caliche, some l" subrounded gravels
color chaD(e to dsrk 8r€y, trec€ lron oride stalning
Color change to dark grey to black, some l" diameter subrounded gravels (serpentine),
molst to slightly moist
Mostly dry
Mottled black and green weathered serpentine and claystone, dry
CL Bluish grey CLAY. molst, moderately plastic, hlgb)y
coheivE, abundant iron oxide staining
Greylab brown SANDY CLAY, moist, sltghtly cohesive. sliShtlt pl6stlc' 102
Reddish brown SILTY SAND, moiat, abundaut l/2'' diameter subangular gravele (base)SM
4" of Asphsltic Concrete (AC)
BORINC ABANDONMENT/
fr ELL CONSTRUCTION DETAIT.SLITHOLOGIC DESCRIPTION
(color, soil classification, mol6ture, gtaln elze/ Ptssticity, deneity, other)
2
o
5
o
tsea
E
a
&
I
o
tsoJa
J
Fz
aJ
@
"9gACORSTABILIZED l{ATER LEVEL (BCS): NAFIRST {ATBR (bgs): None
FINtsH DATE/TIME: october 15, 1993START DATE/ TIME: october 15, 1093
MONITORING DEVICE: OVA 128SAMPLING METHoD: Hollow Stem Auger; SPlit SP@n
LOG OF AORING:PC.t OFIB-4
LoccED BYr BRUCE CUT'IINGSUBCONTRACTOR AND EqUIPMENT: lYest Hazmat Drilling Co.: B-57
FII E NA ME: l8-650284BORING LOCATI0N: Northeast Esd of Tsnk Pit
PROJECT #: 40065-00?-01PRoJECT: UPS San Luls Oblspo, Ca
r
t
i
i
1
t
l
t
- Cement
Total depth at 30 feet
No groundwater encountered during drilling
boring was lefL open approximateltz hourtto observe lor groundlater
4_
6_
B-
14+
16-
18-
21
-
28,
-
32-
0
0
0
0
0
o
i{/
t5/
35/
35
ze/
70/
6"
60/
6"'
60/6''
N/
a"'
{ y'4 /2,
,ltztt
, /4 zt,
tllz/t?
t/414t,
t///41 ?
t //z tlz 1tllll/1
t/4ltl
t/4/24
t7lrzlI
,42 4l 4
tlry2,/l
trryltI
tltltl
tztl*p
t//4Zl 4
,llzllt
t//r'/42
t//tltt
ttrzt74 I
,lzltl
tl4lt/
t // f4l
z y'zZ 4l
t/tltt
tztr'r'4z
t ll l,rt I
t t/l //l I
t//tlzl
llllt
7q /4 I
/4?ry4
Dark
oxid€
grey to brovn teathered bedrock (serpentine), dry abundant caliche, some iron
staining
Mottled gren and black, abundsnt iron oxide staining
Mottled black and gren teathered serpentine and claystone, dry
creen and black CLAY, moldt, moderately plastlc, moderately mheslve, sme @ar&
sand, trace iron oxide rtainint
c.i." "r,."r" i. ".""i'i"n b;;;",';;i"i; ;;;;;;;i';h;t;;;i' ;;t;;;;t l' ai"*"t".
""urnluiir"grouEls (chert and serpertlne), abundant callche at 5'
Some l/2" subtounded graeels abundant caliche
CL
AbundAnt L/2" to l" dlameter subrounded gravels,Reddi6h brotn SILTY SAND, motst,
f ine-to coar*-grained (Base)SM
t" of Asphaltic Concrete (AC)
BORING ABANDONMENT/
f, ELL CONSTRUCTION DE-TAII,sLITHOLOGIC DESCRIPTION
(color, eoll classification, molsture, greln aize/ plasticlty, deneity, other)
o
ts
o)
Fq
A
d
e
a
a
t
o
F
Ja
I
&eFz
a
A
q
"Sg ACOR
STADILIZED WATER LEVEL (BGS): NAFIRST f,ATER (ugs): None
FINISH DATE,/TIME: october 15, l9g3START DATE/ TIME: October 15, l0B3
M0NTTORING DEVICE: OVA 128SAMPLrNG METHOD: lloltow Stem Auger; Split SPoon
LOG OF BORINC:PC.r OFIB-5
t.OcGED BYr BRUCE CUI'TINGSUBCONTRACTOR AND EQUIPIENT: west Hazmst Drilling Co.; B-57
FU.E NAME: 18-O5O2B5BoRING LocATtON: East of Tank Pit
PROJECT l: A0065--002-01PROJECT: UPS San Luls Oblspo, Ca
t.
I
I
r-
l
t
I
t
t
t
t
t
I
I
I
t
t
I
t
t
t
t
t_
IL-
\ tYell covet
-
Concrete
-
PVC Blank
- Bentonite grout
-
#3 Sanal
-
PVC Scree!
0.02" ilots
Total depth of rell at 26 feet
No groundf,ater was encountered during drilling
2
1
a
B_
10-
t2-
L4-
16-
1B_
20-
21 _
28,
-
3O-
Grey to greenlsh grey serPentlne bedrmk, dry
YelloFish bronn to brovn SANDY CLAYSToNE moist' loi plasticity, trace black sPecks
creenish broin to green SILTSToNE/CLAYSTONE moist, teather€d erlEotine Hr@k
Dark brotn to black CLAY, moi6t medium plasticitj.
Mottled dark brown and grey aandy clay, molst loi plastlclty
CL
BORING ABANDONMENT/
'ELL
CONSTRUCTION DTTAILSLITHOLOGIC DESCRIPTION
(color, eoll classification, molstur€, gtai^ Elre/ Pta€tlclty' density' other)
3
a
)
F
o
o
a
&
a
a
o
F
J
d
Fz
HJq
"9gACORSTABILIZED WATER LBVEL (BGS): NAFIRST f,ATER (bgs): None
FINISH DATE/TIME: october 15, 1993START DATE/ TIME: october 15, lg93
MONITORINC DEVICE OVA T2BSAMPLTNG METH0D: None
PC-t OFILOG OF BORING:
MW_2
LOCGED BY: BRUCB CUTTINGSUBCONTRACTOR AND EQUIPMENT: West Hazmat Drilling Co.; B-57
FILE NAME 1B-65O2YIY2BORING LOCATIoN: North East of UST Excaystion
PROJECT #: 40065-00?-01PROJETT: UPS San Luis Oblspo, Ca
t
i
L-
t
t_
\ werl eovcr
-
Concrete
-Concrete
slurry
-
PVC Blank
- Bentonite grout
-
#3 Sand
PVC
o.o2"
Scren
slots
Total depth of welt at 28 feet
Groundwaler encountered aL 22.5 leel
1-
6-
t0-
L4-
t6-
1A_
20-
?1
-
2A-
30-
32-
0
0
0
o
o
o
0
0
tt/ti/
zo
t3/
t7'/
zo
t2/.
25
to/
18'/
25
t5/
25/
35
t5/t7/
to/
t6'/
?o
8/t2/
20
35/60/z"
Brorn CLAYEY SAND, saturated, abundant l" diameter subrounded gravels, medium- to
cosrse-gralned sand
Dark grey to blsck SANDY CLAY, very mol8t, fine-Srained sDd fraetlon. dllghtly
plastic, slightly 6hesive
i".","n *"*" "io;, ;;':i, -;.;;;"i, 't""i,.,
ii.iit..n*,".' i;"". -"d;;;-;*;;.;sAnd
lncrease in sand to 1OZ (sandy clay), color change to reddish brown, abundant iron
oxtde and charcoal stalnlng, trace r@tles
Increase in coarse-grained Band, highly Plastic
color chanse to brovn. verY moist, increase in fine grained sand to 20%, slightly
coheslve, slightly plastlc, abundant charcoal. trace irbn oxide staining
Increase in sand to 3OZ, very moist
Decrease in sand to 5%
Trace coarse sand
Increase iD sand to 5%, very molst, @lor change to light brorn
Saturated, abundant gravels to l" diarneter
CL
neddish browE SILTY SAND, moist, abundant l/2' diamele. subrounded gravels (base)'
tints to coarse-graln€d
SM
3" Asphaltlc Concrete (AC)
BORTNG ABANDONMENT/
f, ELL CONSTRUCTION DETAII,SLITHOLOGIC DESCRIPTION
(color,60ll classificatlon, moisture, gtain alze/ pla6ticlty, density' other)
E
o
o
F
a
B
q
c
a
Ja
I
&
Fz
Iq
"SgACORSTABILIZED YATER LDVEL (BGS): t3'FIRST ITATER (bgs): 22.5'
FINTSH DATE/TIME: October 15, 1993START DATE,/ TIME: October 15, lg03
M0NITORING DEVICE: OvA l2BSAMPLING MBTHOD: None
LOG OF BORING:PG.I OFI
MW_3
l.occED BY: BRUCE CUTTINGSUBCONTRACTOR AND EQUIPMENT: WesL llszlnat Drilling Co; B-57
FlLn NAME: ln-650Mlt3BORINO L0CATION: South East of Tank Pit Next to Duildins
PROJECT T: A0065-002-01PROJ8CT: UPS Son Luis Oblspo, Ca
l.
I
.TO: COUNTY HEALTH DEPARTMENT
APPLICATION FOR WATER WELL PERMIT
;
Date
PermitNo. )'" t ' :-
hereby apply for a permit to.:/
- construcl ['1, repair I L or abandon [ ] a well located on AP# i
Section Township
=,C1r''
Range
t-rrai.14 1'0,':',:.'.' l
(St et Address or C ounty Road)
AddfeSS '-:, *:) ,' ,, 1i',-.7., ,-
'I
Owner/Agent
Contractor's Bond Cash Deposit
Well Driller
ACREAGE
/.
../ l"
/' '' ,/ /'-.tContractor's License Number
." r'- Jtr' -t.-)j, '': 4/ ','' / ,r
I hereby agree to comply with all laws and regulations of the San Luis Obispo County Health Department
and the State of California pertaining to, or regulating well construction. Within fifteen days after
completion of the well, I will furnish the County Health Department a log of the well and notify them
before putting the well in use.
_:: ! "6 S
Applicant
INTENDED USE
lndustrial
Domestic, Private
Domestic, Public
f rrigation ,
Othetftt . ," 7/,1v ,
Fee Paid Date
lt" tt't - /
Comments
" Site lnspection
Final Letter
Site Letter
Abandonment
- Approved_ Not Approved_ Specialist
Permit Expires 6 Months After lssue Date
X-Conn Letter
Date
-To: COUNTY HEALTH DEPARTMENT
APPLICATION FOR WATER WELL PERMIT
Date
Permit No.l, : .:/
n-->.,..t i4 ,'l',..r'I ! {'1.,, hereby apply for a permit to
-construct ['J* repair [ ], or abandon [] a well located on AP# '' '=i / ''l'i" i' ,t' 5-
Section t Township
j. ltl) I ..Range
(" 1 / .- '1_ r .r. i
t!n'.1, -a' .,- !' ;
(Street Address or County Roa
Owner/Ag ent
.lt :
/:- ,,, ,-.,...,,, , ''r.(
7;., .:t''Address
Contractor's Bond
Well Driller
Cash Depo sit
/,r'i . /
,..... €7,lt,t
Contractor's License Number ,"" - $ 7 5 ;'-r'q 7q
I hereby agree to comply with all laws and regulations of the San Luis Obispo County Health Department
and the State of California pertaining to, or regulating well construction. Within fifteen days after
completion of the well, I will furnish the County Health Department a log of the well and notify them
before putting the well in use
ACREAGE Signed
Applicant
INTENDED USE
lndustrial
Domestic, Private
Domestic, Public
lrrigation
Other ,l|f '.',,. '/t,' n'? fr *''' j'
Comments
1-' R r"
. .t," 1
, '-,' y' ; 1, i',1.'
Fee Paid ,' i ' , :'ir Date i- /'' :',,,. r .
I
t
t
I
t_
Site lnspection_
Final Letter
Site Letter
Abandonment
Approved NotApproved_ Specialist
Permit Expires 6 Months After lssue Date
X-Conn Letter
Date
t
t
To: COUNTY HEALTH DEPARTMENT
APPLICATION FOR WATER WELL PERMIT
Date
Permit No
, hereby apply f
.'/ 7
i',.' .rl(or a permit to
-construct F}, repair [ ], or abandon Il a well located on AP#/:.;'7 {- 1 'T/ ,,i;z 5
Section Township IRange
,,. ,. .! t.' !.t4 (:: 4a
(Street'Address or CountY Ro d)
( a:./ S' t'
."1
Owner/Agent
(. ,,_. I a., (.;. /).1 !. a; .' //t L,. {
'i'z:1t tAddress
Contractor's Bond Cash Deposit
Well Driller
Contractor's License Number
v
l''7 '''j'
I hereby agree to comply with all laws and regulations of the San Luis Obispo County Health Department
and the State of California pertaining to, or regulating well construction. Within fifteen days after
completion of the well, I will furnish the County Health Department a log of the well and notify them
before putting the well in use
ACREAGE
--t' ;.2 {Signed
Applicant
INTENDED USE
lndustrial
Domestic, Private
Domestic, Public
lrrioation
Orfi". )i..t.,. .,"; i . , . /1 tr, ;,
t: i;
'1
t
,' ? ,"', ,/ 4 7
Fee Paid Date I t i'. -t '/,,',1.,
Comments:
- Site lnspection
Final Letter
Site Letter
Abandonment
- Approved_ Not APProved
Permit Expires 6 Months After lssue Date
Specialist
X-Conn Letter
Date
r
l"
t-
I
t-
I
t
APPENDIX E
Laboratory Reports and Chain of Custody Documents
I
It,
I
l,-
L
t"
r
t
Ano lytico lTechnolog ies, I nc
t-.
I
Corporote Offices: 5550 Morehouse Drive Son Diego, CA 9212\ (619) 45e-9l4l
SECOND COPY
ATI I.D. ! 310164
october 29, 1993
, PETRO-BUILDERS
10609 PAIITTER A\rENT'E
5ANTA FE SPRTNGS, CA 90570
Project Name: IIPS SAN LUIS OBISPO
Project # : (NoNE)
Attention: JtlE GIRIIRD
Aaalytical Technologies, Iuc. has received the following sanple(s):
Date Received Quantitv Matrix
october 13, 1993
October 13, 1993
11 SOIL
WATER1
The sample(E) were anaLyzed with EPA oethodology or equivalent methods as specified in tbe
elclosed aualytical schedule. Ihe synbol for "less than" indicates a value below the reportable
detectiotx liuit.
The results of tbese analyses and tbe quality control data are enclosed.
The eamples were aaalyzed by Analytical Technologies' Inc. Mobile Lab (MO4O1).
{fr_8.rMs
M. E.
I"ABORATORY MANAGER
,CARY STEWAR:I
PROJECI
t.
I
t
1t nno Vtico I Tech nolo g ies, I nc.
SA.I.{PLE CROSS REFERENCE
CIiENt : PETRO-BUILDERS
Project # : (No$E)
Project lilame: I'PS SAII LUIS OBISPo
Page 1
Report Date: October 29, 1993
ATI I.D. : 310164
Date CollectedMatrix-ATr # client Description
t
t
1
2
3
4
5
6
7
8
9
10
11
L2
s-1
s-2
s-3
s-4
w-1
s-5
s-6
s-7
s-8
s-9
s-10
s-11
SOIL
SOIL
SOIL
SOIL
WATER
sorL
SOIL
SOIL
SOIL
SOIL
SOIIJ
SOIL
13-ocr-93
13-ocI-93
13-OCT-93
13-OCT-93
13-oCT-93
13-OCT-93
13-OCT-93
13-OCT-93
13-OCr-93
13-OCT-93
13-OCT-93
13-OCT-93
---TOTAIS---
Matrix
SOIL
WATER
# Samples
11
1
ATI STANDARD DISPOSAI PRACTICE
Abe sample(s) fron tbis project will be disposed of iu twenty-one (21) days
thi,s report. If, an extended storag€ period ls required, please contact
departmeot before the scheduled disposal date.
from tbe date of
our sanple control
t
t_
L
ft nno VticoITechnologies, I nc
ANAI,YTICAL SCEEDT'LE
CIiENt : PETRO-BUILDERS
Project # ! (NoNE)
Project Name: ttPS SAtl LUIS OBISPO
Page 2
ATr I.D.: 310164
Aualysia Iecbnique I De s c riptiou
t EPA
EPA
6010 (CEROMTUM)
6010 (LEAD, ORCANTC)
8O2O (BENZENE, TOLT'ENE, ETFTLBENZENE.
EpA 418. 1 (PErROLsUll EYDROCARBONS)
EPA 80ls-CDOES (IrttEL EYDROCARBONS)
INDUCTIVELY COT'PLED ARGON PI.ASMA
INDUC:nI\/ELY COI'PLED AROOIT PLASITA
cc/PEoro roNrzATroN DErEcroR
INFRARED SPECTROMETER
cclELAME TONTZATTON DETECTOR
. EPA
MOD
MOD
xvLENEs)
t.
t
L
L
ft n no Vtico lrec h nolog ies, I nc
GENERAI. CEEMISTRY RESI'LTS
Client : PETRO-EUILDERS
Project # t (NoNE)
Project NaEe! ttPS SAN LUIS OBfsPo
Pagre 3
ATI I.D.: 310164
Sample Clieat ID
#
Matrix Date
Sanpled
Date
Receivod
1
2
3
4
9
s-1
s-2
s-3
s-4
s-8
SOIL
SOIL
SOIL
SOIL
SOIL
13-OCT-93
13-OCT-93
13-OCT-93
13-ocr-93
13-ocr-93
13-OCT-93
13-OCT-93
13-ocT-93
13-OCT-93
13-OCT-93
Parameter Units 1 2 3 4 9
PEIROLST'M EYDROCARAONS MC/Ke 2so <10 <10 <10 <10
A A no lytico lTech nolog ies, I nc.
GENERAL CEEMTSTRT - gUArrBY COMTROL
DnP/MS
I PEIrRO-BUILDERSClient
Page 4
ATI r.D. : 310164t -Proj
I rroJ
ocl # ! (NoNE)
ect Name: I,PS SAII LUIS OBISPO
Parameters REF I.D. Units SamPIe
Result
DuP
Result
RPD Spiked
SampIe
Spike
Conc
t
Rec
PETROLET'}{ EYDROCARBONS 310164-02 MG/KG <1O 100 o N/A N/A N/A
[-* n..orrery = (Spike Sample Result - Sample Result)*loO/spike Concentration
I npO 1n"l"lin" t Differeaca) - (sanple Result - Duplicate Result)*l0O/Average Result
t-
I
t
L
L
I
I ft n no rvlco lTech nolog ies, I n c
METAIS REST'LTS
CIiENt : PETRO-BUILDERS
Project # s ($oNE)
Project Name: ttPs sAN LUIS oBIsPo
Page 5
AII I.D.: 310164
r"
t
Sample Clieut ID
#
Matrix Date
Sampled
Date
Received
-1
2
3
_4
6
s-1
s-2
s-3
s-4
s-5
SOIL
SOIL
SOIL
SOIL
sort
13-OCT-93
13-OCT-93
13'ocr-93
13-OCT-93
13-ocr-93
13-ocI-93
13 -OCI- 9 3
13-OCT-93
13 -OCT-93
13-OCT-93
Parameter Units 1 2 3 4 6
CEROMII'M
ORGANIC LEAI)
MG/KG 7.1
MG/KC <0.3
8.O
<0
11 .0
<0 .3
9.s
<o .3 3<03
ft n no Vtico lrec h nolo g ies, I nc.
METALS RESI'LTS
CIiEDt : PEIRO-BUILDERS
Project # : (NONE)
Project Name: I'PS sAlI LuIs oBIsPo
Page 6
ATI I.D.: 310164
Sanple Client ID
#
Matrix Date
Sampled
Date
Received
7
8
9
10
11
s-6
s-7
s-8
s-9
s-10
SOIL
SOIIJ
SOIL
SOIL
SOIL
13-ocf-93
L3-ocr-93
13-OCT-93
13-OCT-93
13-ocr-93
13-ocr-93
13-OCT-9 3
13-OCT-93
13-OCT-93
13-OCT-93
Para&eter Units 7 I 9 10 11
CEROMII I.I
ORGANIC LEAI'
Mc/KG 18. 1
<o .3 3<o<07l'rc/KG o 3 <o.3
ft nno tvtcc lTech nologies, I n c
METALS RESI'LTS
Clietrt I PETRO-BUILDERS
Project # s (NoNE)
Project Naae: ttPS SAN LUIS oBISPo
Page 7
AII I.D.s 310164
Sample Client ID
#
Matrix Date
Sampled
Date
Received
- t2 s-11 SOIL 13-OCT-93 13-ocT-93
ParaEet€r Uaits 12
[- onnmrrc r.ueo I'tc/Kc <o.3
r
ft onotu,icolliechnologies,l nc
MEEASS - QUALTTY COMIROL
DrrP/MS
Client : PETRO-BUILDERS
roject # : (NoNE)
Project NaBe! I'PS sAlI LUIS oBIsPo
Page 8
ATI I.D. : 310164
Paraueters REF f.D. Units SanPIe
Result
DuP
Result
RPD Spiked
Sample
spike
Corlc
t
Rec
CEROMII'M
ORGAI{IC LEAI)
31O230-O4 I'lC/Ke 7.4
310231-01 MGIKG <0.3
7.L
<0 .3
4
0
88
89
50.8
4.7
49,4
5.3
t Recovery = lSpike Sample Result - Sample Result)*lOo/Spike Concentration
RpD (Relalin" t Difference) = (Sanple Result - Duplicate Result)*lOO/Average Result
l,-
I
{t-
ft nno tv,ico I Tec h nolog ies, I nc
METAIS - QUAlrrY coNrRoL
BLANK SPIKE
Client : PETRO-BUILDERS
-Project # : (NONE)
Project Name: L'PS SAN LUIS OBISPo
Page 9
ATI I.D. : 310164
-ParaDetera Blank Units
spike ID#
Blank
ResuIt
spikedg6nple
spike
Cot1c.
t
Rec
CFROMIT'M
ORCANIC LEAD
40990
409 13
45.7
4.3
so.o
5.3
Mc/Kc <0.5
Mc/Kc <0.3
91
81
t Recovery = (Spike Sample Result - Sample Result)*loo/Spike Concentration
_RpD (Relalir" t Differetlce) = (Sample Result - Duplicate Result)*lOo/Average Result
L
ft nno tvticolTech nologies, I nc.
Test 3
Blank I.D. :
Client :
Project # :
Project Name:
GAS CAROMATOGRAPEY - gUAI,ITY COMTROL
REAGENT BLANK
MOD EPA 8015-CDOES (rUEr, EYDROCARBONS)
272L9
PETRO-BUILDERS
(NoNE)
I'PS SA}I LUIS OBISPO
ATI T.D.
Date Extracted
Date Analyzed
Di1. Factor
Page 22
310154
13-ocT-93
13-OCT-93
1 .00
Paraoeters Units Results
rUEL TTDROCAREONS
AYDROCARBON RANGE
EYDROCARBONS QUAIIIIITATED USING
SI'RROGATES
Br s ( 2-ETAYLEEXrIT ) PEIEAT,ATE
Mc/Kc <10
93t
ft nno rvticolTechnologies, I nc
CAS CSROMATOGRAPEY REST'LTS
test : EPA 8O2O (BENZENE, TOLI'ENE, ETETLBENZENE, XTLENES)
Client : PETRO-BUILDERS
Project # : (NONE)
Project NaE€: tPS sAll Lufs OBISPO
Page 10
ATI I.D. : 310164
Samplo Clj-ent ID
#
Matrix Date
Sanpled
Date
Extracted
Date
AnaLyzed
Dil.
Factor
5 w-1 WATER 13-OCT-g3 13-OCT-g3 13-OCT-g3 500.00
Parameter Units 5
t uclL
ue/L
uclL
uc/L
6 600
13000
2 6000
130000
BEI|ZENE
:tolt ttrE
- ET Y:LIIENZENE
XYLENES (TOTAr,)
SI'RROGATES
_ TRIFLUOROTOLIJENE t 182 *E
*B RESULT OIIISIDE OF LIMITS DI'E TO SAI'{PLE MATRIX INAERFERENCE
1t n no rvtico I Tec h nolo g ies, I n c
GAS CEROMATOGRAPEY REST'LTS
Test : EPA 8O2O (BENZEI{E, TOLI'ENE, ETEyLBENZEI{E. XTLENES)
Clieut : PETRO-BUILDERS
Project # ! (NoNE)
Project Name: I'PS SAN LUIS oBIsPo
Page 11
ATI T.D :310154
Sample Client ID
#
Matrix Date
Sampled
Date
Extracted
Date
Analyzed
Dil.
Factor
1
2
3
s-1
s-2
s-3
SOIL
SOIL
SOIL
1 .00
1 .00
1 .00
13-OCT-93
13-OCT-93
13-OCT-93
13-OCT-93
13-OCT-93
13-OCT-93
13-OCT-93
13-OCT-93
13-oCA-93
Units 1 2 3Param6ter
" BENZENE
TOLI'ENE
ETE:TLBENZE$E
XYLEI{ES (TOTAL)
SIJRROGATES
TRIT{LUOROTOLI'ENE
Mc/KG
MG/KG
MG/KG
MG/KG
0 .025
o .043
0 .040
101
o.27
o.22
o.22
o.62
<o.025
<o.025
<o .025
<o .050
106
o.2L
t 165
I
I An olyticolTechnologies,
I nc.GAS CEROMATOGRAPEY RESI,LTS
r:ff:". ; Hl.::;3rlffXl"*' ToLUENE, ErErIBENzErrE, XYIENES)
lProject# :(NoNE)' Project Namer UpS SalJ f,UfS OBfSpO
Page 12
ATI I.D. : 31O164
I Sauple Client ID
#Matrix Date
:::::::__
13-ocr-93
13-ocT-93
l3-ocT-93
4
6
7
Date Date Dil.Extracted A.nalyzed Factor
13-ocT-g3 13_ocT_93 1.OO13-ocT-93 14_ocr,93 10.0013-oc!-93 14-ocr_93 50.oo
s-4
s-5
s-6
SOIL
sorL
sorLt
I
-Parameter Uoits 4 6 7
I
BENZEITg
IOT.UTNE
EIEYLBETTZENE
XYLENES (toTAL)
MclKc
Ms/Ka
MclKc
Mc/Ke
0.053
o .12
0.21
1.1
7.O
28
83
270
305 *'t
2,5
3.1
18
96
114
SI'RROGA.rES
I-I TRrnLuoRoTOLnEt{E
I
t 131
**DUPLICETE ANALYSTS NOT WITETN CONAROL LTMTTS
fk n no Vtico lrec h no lo g ies, I nc.
GAS CEROMAIOGRAPEY RESI'LTS
Test : EPA 8O2O (BENZENE, TOLLIENE, ETEYLAENZENE' XYLEIIES)
Client s PETRO-BUILDERS
Project # : (NoME)
Project Names ttPS SAlf LUIS OBfSPo
Page 13
ATT I.D :31O164
Saople Client ID
!It
Matrix Date
Sampled
Date
Extracted
Date
Analyzed
Dil.
Factor
I
9
10
s-7
s-8
s-9
SOIL
sorL
SOIL
l3-ocr-93
13-oCT-93
13-OCT-93
13-OCT-93
13-ocT-93
13-OCT-93
14-OCT-93
14-OCT-9 3
14-ocr-93
1.00
1. OO
so.oo
t Uoits I 9 10Parameter
BEI{ZEI{E
TOLI'ENE
ETflYLBENZEI{E
XTLENES (TOTAL)
SI'RROGATES
TRITLUOROAOLI'E$E
Mc/Kc
Mc/Ke
Ma/Kc
MC/KC
<0. o25
<o .025
o.055
o.97
LO2
<o .025
o.o28
o.o29
o.52
103
2.3
1s
22
110
t LL2
ft ono tu,icolTechnologies, I nc.
GAS CEROMATOGRAPEY RESI'LTS
Test : EPA 8O2O (BENZENE, TOLLTENE' ETEYLBENZENE' XYLENES)
Client : PETRO-BUILDERS
Project # ! (NoNE)
Project Namer ttPS SAIII LUIS OBISPO
Page 14
ATI I.D. : 310164
Sample Clieat ID
#
Matrix Date
Sanpled
Date
Extracted
Date
Analyzed
Dil.
Factor
11
L2
s-10
s- 11
SOIL
SOIL
13-OCT-93
13-OCT-93
13-ocr-93
13-ocr-93
14-Ocr-93
14-ocr-9 3
4 .00
10.o0
Parameter Uaits 11 L2
BENZE!{E
TOLIJENE
ETBrI,BENZENE
xrl.ElrEs (ToTAL)
SI'RROGAEES
TRIELUOROTOLI'ENE
MG/KG
Mc/Kc
Mc/KG
MG/KG
o.24
o.s1
o.85
4.2
<0.25
<o.25
<o.25
5.5
10st118
ft nnoVticolrechnologies, I nc.
GAS CEROMATOGRAPEY - QUALTTY COtflfROL
REAGENT BLANK
Test s EPA 8O2O (BENZEI{E, ToLITENE, ETBTLBENZENE' xfLENEs)
Blank r.D. z 272t7
C1ient : PETRO-BUfLDERS
Project # s (NoFE)
-Project Namer ttPS SAN LuIs oBIsPo
ATI I.D. :
Date Extracted:
Date Analyzed :
Dil. Factor !
Page 15
310154
13-OCT-93
14-OCT-93
1.OO
Paraoeters UnitE Results
I BBNZENE
TOLT'ENE
ETEYLBEI{ZENE
"XYLENES (ToTAI.)
ST'RR,OGATES
- TRIT'LUOROTOLT'ENE
MG/Kc
MG/KG
MclKc
MG/KG
<o.025
<0 .025
<0.025
<o. o50
96*
r
I
t-
r-
ft nnorvticolTechnologies,l nc
GAS CEROMATOGRAPEY - QUAIITY COlirlRoL
REAGENT BLANK
rest r EPA 8O2O (BENZEI{E, TOLIIENE, EIEI-LBENZENE, XyLENES)
Blank I.D. z 272L8
CliErrt : PETRO-BUILDERS
Project # : (NONE)
_ Project Name: ttPs sAIiI LuIs oBISPO
ATI I.D. !
Date Extracted:
Date Analyzed :
Dil. Factor :
Page 16
3 10 164
13-ocr-93
14-ocr-93
1. OO
Parameters Uaits Results
l'
i
BENZET{E
TOLT'ENE
E] TYT.BENZENE
'XTLENES (TOTAT)
SI'RROGATES
TRIELUOROAOLI'E$E
uelL
uclL
uc/L
uclL
<o.50
<0 .50
<0.50
<1. O
111t
A Anolyticolrechnologiet'18!" caRoMATocRApEy - euAlrry coNrRoL
MSMSD
ETEYLBENZENE,
Psge 17
xrLENEs) ATI I.D. : 310164
Date Extracted: 13-OCf-93
Date Aaalyzed : 14-OCT-93
Sanple Matrix s SOIL
REF I.D. : REAGE$T SOIL
Test
l'{sMsD #
Client
: EPA 8O20 (BENZEI{E, TOLIENE,
: 55465
: PETRO-BUILDERS
Project # : (NoNE)
Project Name: ttPS SAll LUIS OBfSPO
Parnmeters Units SanpIe
ResuIt
Conc
Spike
spiked
Samp).e
Dup
spike
DUP RPD
t Rec
t
Rec
_ BEIIZE}IE
IOLt'ENE
r'rc/Kc
MG/KG
<o . o25
<o .025
o. s0
o. so
0.48
o .47
96
94
0.48
o.47
96
94 0
o
- t Recove-" = lSpike Sample Result - Sanple Result)*lOO/Spike Conceatration
RPD (Relative t Difference) = (Spiked Saople Result - Duplicate Spike Result)*lOo/Average Result
I
t
t
ft nno tvticolrechnotogies, I nc.
GAS CEROMATOGRAPEY - QUAITTY COlflfRoL
MSMSD
ETEYLBENZENE, XTLENES)fest
MsMsD #
Clieat
r EPA 8O2O (BENZENE, ToLI'ENE,
:55466
: PETRO-BUIIDERS
(lroNE)
UPS SAN LUIS OBISPO
ATI I.D. t
Date Extracted:
Date Analyzed :
Sample Matrix :
REF I.D. :
Paga 18
310164
13-OCT-93
19-OCT-93
WA:lER
REAGEITT WATER-Project # t
Project Name:
Parameters Units Cotlc
Spike
t
Rec
Dup
spike
SampIe
Result
Spiked
Saople
DUP RPD
t Rec
BENZEI{E
TOLTIEI{E
ua/L
uelL
<0 .50
<0.50
10
10
9.6
9.8
96
98
96
94
9.6
49
o
4
t Recovery = (Spike Sample Resu1t - Samp1e Result)*100/Spike Concentratioa
.RpD (Relaline t Differetrce) = (Spiked Sample Result - Duplicate Spike Result)*l00/Average Result
ft nnorvtico lrechnologies,l nc.
GAS CEROMATOGRAPBY RESI'LTS
Test : MoD EPA 8015-cDoEs (rUEL AYDROCARBoNS)
Client : PETRO-BUILDERS
Project # : (NoNE)
Project Name: ttPS sAlI LUIS oBIsPo
Page 19
ATr r.D. : 310154
Saople Client ID
4tt
Matrix Date
Sampled
Date
Extractod
Date
Aoalyzed
Dil.
Factor
5 lr-1 WATER 13-ocr-g3 13-OCT-93 13-OCT-93 100.00
Paraueter Units 5
t-F"T'E.L ETDROCARAONS
BYDROCARBON RANGE
InTDROCARBONS gUAlfrrrATED USrNC
t'lclL 390
c6-c14
GASOLINE
ST'RROCATES
- B r s ( 2 -ETErLEEXyr. ) PEEEALATE $N/A*S
*E REST'LT OTIISTDE OF I,IMITS DI'E TO SAI'IPLE MATRIX IIflIERFERENCE
t
t
L
L
L
t
r f,t n no ryricolTechnologies,lnc
[-ru".CIient
GAS CEROMATOGRAPEY REST,I,TS
: MOD EpA gOlS_cDoEs (FtEL EYDROCARBONS)! PETRo.BUTLDERS
r (NolrE)
: T'PS SAN LUIS OBTSPO
Page 20
t-
Project #Project llaue
Atr r.D. I 3tOl64
Data Date Dit.acted Analyzed Factor
Sample Client fD
#Matrix
sorL
sorL
Date
6
7
-8
s-5
s-6
s-7
SamFled Extr
13-ocT-93 13_ocr-93 13-oct_93 10.oo
SOIL 13-ocE-g3 13_ocT_93 13-ocT_93 1 oo .00
Parameter
13-ocT-93 13 -ocI-93 14_ocE_93 1 .00
Uuits 6 7 8FUEL EYDROCARBONS
EYDRoCARBoN RJIIiIGE
EYDROCARAONS QUANTTTATED UsINc
MclKc 72
c6-c14
GASOLTNE
1so0
c6-c14
GASOLTNE
a I s ( 2 -ETEYLSEXTL ) PEIEALAIE
*E
t 94 N/A*s
<10
113REST'LT OUISTDE OF LTMIIS DI,'E TO SAMPLE T{ATRTX TNTERFERENCE
r-
; ftnnorvticolliechnolosies,lnc
GAS CSROMATOGRAPEY REST'LTS
r-I rest : MoD EPA 8ols-cDoEs (FUEL EYDRoCARBoNS).Client 3 PETRO-BUILDERS
Project #: (NoNE)
: UPS SAN LUIS OBISPOProject Nane
Page 21
ATr r.D. : 310164
Sauple Client ID
-#
Matrix Date
Sanpled
Date
Extracted
Date
Analyzed
Dil.
Factor
10
11
s-9
s-10
s-11
SOIL
SOIL
SOIIr
1.OO
1. O0
1 .00
13-Ocr-93
13-ocr-93
13-OCT-93
13-OCT-g3
13-OcA-93
13-OCT-93
111-OCT-93
13-oCT-93
13-OCT-932
Unitg 10 11 t2Parameter
-FT'EL EYDROCARBONS
EYDROCARBON RANGE
EYDROCARBONS QUAIIIITATED USINe
ST'RROGATES
Brs ( 2-ETEYLEE XYT, ) PBTEAI,ATE
Mc/KC
t
1300
c6-c14
GASOLTNE
105
28
c6-c13
GASOLINE
89
2to
c6-c14
GASOLINE
83
t
t
I
L
L
ft n no rvtico I Tech nolo g ies, I nc.
Iest :-Blank I.D. :
Clieut :
Project # :
-Project Name:
GAS CEROMATOGRAPEY - QUAIITY COMTROL
REAGENA BLANK
MOD EPA 8O1s-CDOES (FttEL EYDROCARBONS)
27220
PETRO-BUILDERS
(rroNE)
IIPS SAN LUTS OBISPO
ATI I.D.
Date Extractad
Date Analyzed
Dil. Factor
Page 23
310164
13-ocT-93
14-ocr-93
I .00
Paraaetera Units Results
F'T'TIJ ETDROCARBONS
E']TDROCARBON RAIIGE
F:TDROCARBONS gUAIIIITATED USING
SI'RROGATES
B r s ( 2 -EEEYLEEXYL ) PETEAT.ATE
t{c/L <0.50
98t
ft ono,u,icolTech nolog ies, I nc.
Test
f-ususo *
I crient
GAS CEROMATOGRAPEY - QUALTTY COIflTROL
MSMSD
: UoD EPA 8015-cDOEs (r'uEL EYDRoCARBoNS)
z 55467
s PETRO-BUILDERS
ATI I.D.
Date Extracted
Date Analyzed
Sample Matrix
REF I.D.
Page 24
310164
13-ocr-93
13-OCT-g3 ..
SOIL
REAGEIflT SOILroject f (No!{E)
Project NaDe: I'PS SAII LUIS OBISPo
Parameters Units Sample Conc Spiked t Dup DuP RPD
Result Spike SamPle Rec SPike * Rec
FUEL EYDROCARAONS MCIKG <10 100 118 118 ].2O L2O 2
t Recovery = (Spike Samplo Result - Sample Result)*100/Spike Concentratiou
RpD (Relaiive t Difference) = (spiked Sanple Result - Duplicate spike Result)*lOO/Average Result
ft nnotvticclTechnotogies,l nc
GAS CHROMATOGRAPEy - QUALITy COTflIROL
MSMSD
Tast : MOD EPA 8015-cDoES (r'ItEL EYDROCARBONS)
r-rsr.rso # : 55469
Client : PETRO-BUILDERS
-Project # : (Nol{E)
Project Naae: IIPS SAII LUIS OBISPo
ATI I.D. :
Date Extracted:
Date Analyzed :
Sample Matrix :
R-EF I.D. :
Page 25
310164
13-ocT-93
14-ocr-93
WATER
REAGEI{T WATER
Paraneters Units Sample
ResuLt
Conc
Spike
Spiked
SampIe
t
Rec
DUP
Spike
Dup RPD
t Rec
FI,'EL EYDROCARBONS MelL <o.50 10 10 100 9.8 982
t Recovery = (Spike Sample Result - Sample Result)*lo0/Spike Concentration
RpD (Relative t Diffarence) = (Spiked Sample Result - Duplicate Spike Result)*l0O/Average ltesult
A Anolytico lTechnologiesrl nc., phoenix, Arizono
San Diego . Phoenix . Seattle . Pensacola. Ft. Collins . Portland
MOBILE LABORATORY
GHAIII OF GUSTODY
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Time:Signature:t{C)
Signature:
mmenlJ:
SAMPLE ID DATE TIME MATRIX LAB ID
RECEIVED tsY:BECEIVED 2.
Zy^q(envirotechnology REPORT OF ANALYTICAL RESULTS
Client:Bob Wilson
SEACOR
3485 Sacramento Drive, Suite A
San Luis Obispo, CA 93401
Lab Number:
Collected:
Received:
Matrix:
2749-1
10114193
10120193
Soil
Sample Description:
B_1 @ 12.5
Analyzed: 10122193
Method: EPA 8260
Project uPs (slo)
Project Number:A0065-OO2-01
Bob WilsonCollected
CONSTITUENT POL*
mg/ks
RESULT *
ms/ks
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
o.26
o.o2
0.1 5
0.60
101
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 6.0
15
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc
9L lt*t^-/-/
MSD #1
2749-1.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
Accounting/Soles: 319 La Paloma
Shell Beach, California 93449
hx 805177 3 -0795 tel 805/773-5402
Lob Services: 7l Zaca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4'4696
, Zv^q(envirotechnologY REPORT OF ANALYTICAL RESULTS
Client Bob Wilson
SEACOR
3485 Sacramento Drive, Suite A
San Luis Obis o, CA 93401
Lab Number:
Collected:
Received:
Matrix:
2749-2
10114193
10120193
Soil
Sample Description:
B-3 @ 10.0
Anafyzed: 10122193
Method: EPA 8260
Project:UPS (SLO)
Project Number A0065-002-01
Bob WilsonCollected
CONSTITUENT P RESULT* II
mg/kgmg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate RecoverY
0.005
0.005
0.005
0.005
ND
ND
ND
ND
91
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
*xResults listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.
qA /4a*^*h
MSD #1
2749-2.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
Accounting/Soles: 319 La Paloma
Shell Beach, California 93449
tax 805177 3-0795 tel 805/773-5402
Lob Services: 7l Taca Lane, Suite I l0
San Luis ObisPo, California 93401
fax 805/544-8226 tel 805/54 4-4696
i Zv^q(envirotechnology REPORT OF ANALYTICAL RESULTS
1'Client: Bob Wilson
SEACOR
3485 SaCramento Drive, Suite A
San Luis Obispo, CA 93401
Lab Number:
Collected;
Received:
Matrix:
2749-3
10114193
10120193
Soil
Sample Description:
(MW-1) B-2 @ 12.5
Analyzed: 10122193
Merhod: EPA 8260
Project UPS (SLO)
Project Number
Collected by:
A0065-002-01
Bob Wilson
CONSTITUENT POL*
mg/kg
RESULT**
mg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
89
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.
qA l-l<--.t^,fl-N
MSD #1
2749-3.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
AccountinglSales: 319 La Paloma
Shell Beach, California 93449
fax 805 177 3 -0795 tel 805/773-5402
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4696
I Zv^"I envirotechnology REPORT OF ANALYTICAL RESULTS
Client Bob Wilson
SEACOR
3485 Sacramento Drive, Suite A
San Luis Obispo, CA 93401
Lab Number:
Collected:
Received:
Matrix:
2749-4
10/15/93
10t20t93
Soil
Project uPs (sLo)
Project Number
Collected by:
A0065-002-01
Bob Wilson
Sample Description
Analyzed
Method:
B-5 @ 12.5
10t22193
EPA 8260
CONSTITUENT RESULT* *
mg/kgmg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
BB
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.
%MSD #1
2749-4.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
I
t
Accounting/Soles: 319 La Paloma
Shell Beach, Calilornia 93449
fax 805 1773-0795 tel 805/773-5402
Lob Services: 7 I Zaca Lane, Suite I I 0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4596
, ZV^q(envirotechnology REPORT OF ANALYTICAL RESULTS
Client:Bob Wilson
SEACOR
3485 Sacramento Drive, Suite A
San Luis Obispo, CA 93401
Lab Number:
Collected:
Received:
Matrix:
2749-5
10/15/93
10t20t93
Soil
Sample Description:
MW-3 @ 12-5
Analyzed: 10122193
Method: EPA 8260
Project:UPS (SLO)
Project Number
Collected by:
A0065-002-01
Bob Wilson
CONSTITUENT POL*RESULT'+
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
o.oo5
ND
ND
ND
ND
B9
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
{'POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
Zy maX envirotechnology, inc
gAl"*ffi
MSD #1
2749-5.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
I
I
I
AccountiiglSoles: 319 La Paloma
Shell Beach, California 93449
hx 805 177 3 -0795 tel 805/773-5402
Lob Services: 7l ZacaLane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 8OSlS44-4696
r Zv^q(envi rotechnology OUAL,T' ASSURANCE RE'ORT - SptKE RESULTS
Client:
Zy maX envirotechnology, inc
71 Zaca Lane, Suite 110
San Luis cA 93401
Project
Project Number:
Collected
Lab Number:
Collected:
Received:
Matrix:
os 10/22193
Soil
Sample Description
Analyzed
Method:
Ouality Assurance Spike
10t22t93
EPA 8260
CONSTITUENT Amount piked Amount Recovered
mg/kg
Percent
Recovery
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.057
0.155
0.029
o.174
0.052
0.1 46
0.026
0.1 49
91
94
90
B6
104
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.90
43%
0.86
40%
96
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
NS - Not Spiked
Submitted by,
Zy maX envirotechnology, inc.
MSD #1
qs1022.xls
JMM/smc/jmm/mas John MacMurphey
Laboratory Director
{
I
t
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
, fax 805/773-0795 tel 8051773-5402
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 8051544-4696
Zv^^I envirotechnology OUALITY ASSURANCE REPORT-
SPIKE DUPLICATE RESULTS
Client
ZymaX envirotechnology, inc.
71 Zaca Lane, Suite 110
San Luis O cA 93401
Project
Project Number:
Collected
Lab Number
Collected:
Received:
Matrix:
osD 10122193
Soil
Sample Description:
Ouality Assurance Spike Duplicate
Analyzed: 10122193
Method: EPA 8260
CONSTITUENT Amount Spiked
mg/kg
Amount Recovered Percent Relative Percent
Difference*m Recovery
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.057
0.1 55
0.029
o.174
o.o47
0.1 31
0.026
o.147
82
B5
90
84
94
10
11
0
1
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.90
43%
0.81
40o/"
90 6
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*Relative Percent Difference of the spike and spike duplicate
NS - Not Spiked
Submitted by,
Zv maX envirotechnology, inc.
W/-14--*hMSD #1
qs 1022.x|s
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
I
I
t
AccountinglSales: 319 La Paloma
Shell Beach, California 93449
lax 805 177 3 -0795 tel 805/773-5 402
Lob Services: 7l ZacaLane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/544'4696
i Zy^q(envirotechnology ouAlrry AssuRANcE REpoRT - BLANK RESULTS
Client
ZymaX envirotechnology, inc.
71 Zaca Lane, Suite 110
San Luis Obispo, CA 93401
Project
Project Number:
Collected by:
Lab Number
Collected:
Received:
Matrix:
BLK 10t22t93
Aqueous
Sample Description
Analyzed
Method:
lnstrument Blank
10t22t93
EPA 8260
CONSTITUENT POL*
ug/L
RESULT**
ug/L
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0,00s
0.005
0.00s
0,005
ND
ND
ND
ND
88
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
r'POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc
#u4.WMSD #1
b1O22g.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
fax 805 177 3 -0795 tel 805/773-5402
Lob Services: 7l Zaca Lane, Suite I l0
San Luis Obispo, California 93401
iax8051544-8726 tel 805/54 4-4595
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Sampler's Signature:
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Laboratory
Project Manager
Project #
Special Instructions/ Comments :
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Total no. of containers
Chain of custody seals:
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Date,/, ) / ; c / zlpue, / "r1_
Zv^q(envirotechnology REPORT OF ANALYTICAL RESULTS
Client: Bob Wilson
Seacor Environmental Engineering
3485 Sairamento Drive, Suite A
San Luis O , cA 93401
Lab Number:
Collected:
Received:
Matrix:
2759-1
10t22t93
10122193
Soil
Project:UPS
Project Number
Collected by:
40065-002-01
Don Pratt
Sample Description
Analyzed
Method:
Stockpile 3A
10t27193
EPA 8260
CONSTITUENT *RESULT**
mg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
89
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.
W//1&-**1MSD #2
2759-1.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
t
Accounung/Soles: 319 La Paloma
Shell Beach, California 93449
fax 805 1773 -0795 tel 805/773-5402
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4696
r ZV^^I envirotechnology REPORT OF ANALYTICAL RESULTS
Client:Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Obispo, CA 93401
Sample Description:
Stockpile 3B
Analyzed: 10127193
Method: EPA 8260
Lab Number:
Collected:
Received:
Matrix:
2759-2
10122t93
10122193
Soil
Project UPS
Project Number:
Collected by:
A0065-002-01
Don Pratt
CONSTITUENT POL*
mg/kg
RESULTI'*
mg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
88
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
TymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
Zymil( envirotechnology, inc.
q"LP'^"ffi
MSD #2
2759-2.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
t
I
t
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
fax 805177 3 -0795 tel 805/773-5402
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
fax8051544-8226 tel 805/54 4-4696
|.-
i Zv^q(envirotechnology REPORT OF ANALYTICAL RESULTS
Client: Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Obis o cA 93401I
I
l
Sample Description:
Stockpile 3C
Analyzed: 10127193
Method: EPA 8260
Lab Number:
Collected:
Received:
Matrix:
2759-3
10t22t93
10t22t93
Soil
Project:UPS
Project Number
Collected by:
A0065-002-01
Don Pratt
CONSTITUENT POL*
mg/kg
RESULT**
mg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.00s
0.005
0.005
ND
ND
ND
ND
87
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.
Qr+*--*HMSD #2
2759-3.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
I
1
t
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
fax 805 177 3 -07 95 tel 805/773-5402
Lob Services: 7 I Taca Lane, Suite I I 0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4696
Zvmq(envirotechnology REPORT OF ANALYTICAL RESULTS
Client:Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Ob cA 93401
Lab Number
Collected:
Received:
Matrix:
2759-4
10122193
10t22t93
Soil
Sample Description:
Stockpile 44
Analyzed: 10127193
Method: EPA 8260
Project:UPS
Project Number:A0065-002-01
Don PrattCollected
CONSTITUENT POL*
mg/kg
RESULT* *
mg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
87
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc
WA4^-^t/--{MSD #2
27594.x|s
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
Accounting/Soles: 319 La Paloma
Shell Beach, California 93449
fax 805 177 3 -0795 tel 805/773-5402
Lob Services: 7 I Zaca Lane, Suite I I 0
San Luis Obispo, California 93401
lax 8OS 1544-8226 tel 805/54 4'469 6
Zv^q{envirotechnology REPORT OF ANALYTICAL RESULTS
Client Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Obispo, CA 93401
Lab Number
Collected:
Received:
Matrix:
2759-5
10122t93
10t22t93
Soil
Sample Description:
Stockpile 48
Analyzed: 10127193
Method: EPA 8260
Project:UPS
Project Number
Collected by:
40065-OO2-O1
Don Pratt
CONSTITUENT POLI'RESULT*
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
BB
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.
wP*^hMSD #2
2759-5.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
Accounting/Soles: 3 19 La Paloma
Shell Beach, California 93449
fax 8051773 -0795 tel 805/773-5 402
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
tax 805t544-8226 tel 805/54 4'4696
i Zy^"I envirotechnology REPORT OF ANALYTICAL RESULTS
Client:Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Obispo, CA 93401
Lab Number:
Collected:
Received:
Matrix:
2759-6
'tol22l93
10t22193
Soil
Sample Description:
Stockpile 4C
Analyzed: 10.127193
Method: EPA 8260
Project:uPs
Project Number A0065-OO2-O1
Don PrattCollected
CONSTITUENT POL*
mg/kg
RESULT**
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.005
0.005
0.005
0.005
ND
ND
ND
ND
87
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.5 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
ITPOL - Practical Ouantitation Limit
**Resutts listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc.q*,**tr4
MSD #2
2759-6.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
AccountinglSoles: 3 l9 La Paloma
Shell Beach, California 93449
lax B0S 177 3 -0795 tel 805/773-5 402
Lob Services: 7l7aca Lane, Suite ll0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4696
i Zv^"I envirotechnology OUALITY ASSURANCE REPORT - SPIKE RESULTS
I Client:
ZvmaX envirotechnology, inc
71 Zaca Lane, Suite 11O
San Luis Obis , cA 93401
Project:
Project Number:
Collected
Lab Number:
Collected:
Received:
Matrix:
os 10/27193
Soil
Sample Description:
Ouality Assurance Spike
Analyzed: 10127193
Method: EPA 8260
CONSTITUENT Amount ked Amount Recovered Percent
Recoverymg/kg
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.054
0.1 34
o.o22
o.137
0.046
o.117
o.o21
o.122
B5
87
95
B9
92
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
o.90
36%
0.76
3B%
B4
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
NS - Not Spiked
Submitted by,
ZymaX envirotechnology, inc
MSD #2
qs1027.xls
JMM/smc/jmm/mas
wA4'-+'l
John MacMurphey
Laboratory Director
Accounting/Solis; 319 La Paloma
Shell Beach, California 93449
fax 8051773-0795 tel 805/773-5402
Lob Services: 7 I Zaca Lane, Suite I I 0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4696
t Zv^^I envirotechnology OUALITY ASSURANCE REPORT.
SPIKE DUPLICATE RESULTS
t Client
ZymaX envirotechnology, inc
71 Zaca Lane, Suite 11O
San Luis Obis cA 93401
Project
Project Number
Collected
Lab Number:
Collected:
Received:
Matrix:
osD 10t27t93
Soil
Sample Description:
Ouality Assurance Spike Duplicate
Analyzed: 10127193
Method: EPA 8260
CONSTITUENT Amount Spiked
mg/kg
Amount Recovered Percent Relative Percent
DifferencermRecovery
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.054
0.1 34
o.o22
0.1 37
0.046
0.113
o.o21
o.121
85
84
95
BB
B9
0
3
0
1
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
0.90
36o/o
o.72
39%
BO 5
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*Relative Percent Difference of the spike and spike duplicate
NS - Not Spiked
Submitted by,
ZymaX envirotechnology, inc
g"L Arq'-MSD #2
qs1027.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
hx 805 177 3-07 95 tel 805/773-5402
I
I
t
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/544-4696
i Zy^^I envi rotechnology ouALrry AssuRANcE REpoRT - BLANK RESULTS
Client:
ZymaX envirotechnology, inc.
71 Zaca Lane, Suite 11O
San Luis Obis cA 93401
Project:
Project Number
Collected by:
Lab Number:
Collected:
Received:
Matrix:
BLK 10127193
Aqueous
Sample Description:
lnstrument Blank
Analyzed: 10127193
Method: EPA 8260
CONSTITUENT POL*
ug/L
R
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.5
0.5
0.5
0.5
ND
ND
ND
ND
90
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
50.ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
{tPOL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnology, inc
a'*
John MacMurphey
Laboratory Director
MSD #2
b1027gs.xls
JMM/smc/jmm/sc
I
t
AccountinglSoles; 319 La Paloma
Shell Beach, California 93449
tax 805 177 3 -0795 tel 805/773-5402
Lob Services; 7l Zaca Lane, Suite I l0
San Luis Obispo, California 93401
fax B0 5/544-8226 rel 80 S IS 4 4- 469 6
Chain-of-CustodyNumb..,A g6U 1
Special Instructions,/ Comments :
I
\ro,r'rii- 4 A
a+n,ko,'t, Ll g
\l*k d;,1( 4 a
\)rt, l(s, t< 3 C -
\I"ur.^nitz 3 g
-1'hark:lt' 3 n
Sample ID
Sampler's Name:
Sampler's Signature:
Project #ho(,5- rn} -o/Task #,+
Project Manager
Laboratory {Jor^.. /Ti:rn-around time:
C)ts
"O dt
<o, ^/ .,r, \ ()C. <un r ) ?'?fO t
\",2rQ4 -,pf \i)or lH \\--,/ \ --,
SEACOR Chain -of -Custody Record
*
b-2)
Date
2: fD
2 :so
l,'tc
,;4c
D:10
?r qo
Time
{
so;l
Matrix
Relinquished by:
Sign
Print
Company
Time
-
Date
Relinquished
Sign
Print ?r
n->/-n col(Companyr,
Time 'J 3o La)Date la-s?fr
/\
X
X
X
X
K
N
@
XE
hE\trd<,
F€
Analysis Request
o
!o
FA
di
$
AF
o
d
o
oo'5Ndoc€
9N<e
6rE
E9dv
9e
-e a.l
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o
b0
d
€
I
\hpb>
6^
ATYNia
EhONca6
ta
Oq
9ro
.Ja @
o€
SPai6
Received by:
Sign
Print
Company
Time Date
by
Sign
Print
Company
Time lGr'io out la'72'1:
doJ
?*! c.l
rr
O^
.J
LZ
=
O
-.]UF
._1\_r/
:6 -r
-t I
I
2
-L
) 11'--I *\
Comments,/
Instructions
Client
Client Contact
Client Phone Number:
Total no. of containers
Chain of custody seals:
Rec'd good condition,/cold :
Conforms to record:
Sample Receipt
t\
ri/i\
{,
I
i
l
i
l
I
I
I
'e
o
O
o
!
E
z
oate/O /22/?Zpage /of i
i Zv^q(envirotechnology REPORT OF ANALYTICAL RESULTS
Client: Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis , cA 93401
Lab Number
Collected:
Received:
Matrix:
2439-1
11t11193
11t11193
Sample Description:
MW-1
Analyzed: 1 1/16/93
Method: EPA 8260
Project:UPS - SLO
Project Number:40065-OO2-01
Don PrattCollected
CONSTITUENT POL*RESULT*"
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate Recovery
0.5
0.5
0.5
0.5
ND
ND
ND
ND
95
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
50 ND
N/A
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #171 7
'tPOL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed PoL
Submitted by,
ZymaX envirotechnology, inc.
^t ^D-
MSD #2
2839-1.xls
JMM/smc/jmm/mas
Wl^,.-John MacMurp
.-r
hey
I
Laboratory Director
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
hx 805177 3-0795 tel 805/773-5402
Lob Services: 7l Zaca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4-4696
i Zv^q(envirotechnology REPORT OF ANALYTICAL RESULTS
Client:Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Obis o cA 93401
Lab Number:
Collected:
Received:
Matrix:
2439-2
11111193
1',111193
Sample Description:
MW-2
Analyzed: 11/16/93
Method: EPA 8260
Project UPS - SLO
Project Number:
Collected by:
A0065-002-01
Don Pratt
CONSTITUENT POL*RESULTI' II
u IL
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate RecoverY
0.5
0.5
o.5
o.5
ND
ND
ND
ND
92
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
50 ND
N/A
ZymaX envirotechnology, inc. is ceftified by CA Department of Health Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnol , lnc
qJ-
John MacMurphey
Laboratory Director
MSD #2
2839-2.xls
JMM/smc/jmm/mas
Accounting/Soles: 319 La Paloma
Shell Beach, California 93449
fax 805 17 7 3-0795 tel 805/773-5402
Lob Services: 7l Zaca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/544'4696
Zv^^I envirotechnology REPORT OF ANALYTICAL RESULTS
t-Client Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Ob , cA 93401
Lab Number:
Collected:
Received:
Matrixr
2839-3
11111193
11t11193
ueous
Project:UPS - SLO
Project Number A0065-002-01
Don PrattCollected
Sample Description
Analyzed:
Method:
MW-3
1 1/16/93
EPA 8260
CONSTITUENT POL*RESULT**
ug/Lu
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate RecoverY
0.5
0.5
0.5
0.5
ND
ND
ND
ND
9B
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
50 ND
N/A
ZymaX envirotechnology, inc' is certified by CA Department of Hea Ith Services: Laboratory #1717
*POL - Practical Ouantitation Limit
**Results listed as ND would have been reported if present at or above the listed POL
Submitted by,
ZymaX envirotechnolo gy, inc.ffiMSD #2
2839-3.xls
JMM/smc/jmm/mas
John MacMurphey
Laboratory Director
AccountinglSoles: 319 La Paloma
Shell Beach, California 93449
lax 805 177 3-0795 tel 805/773-5402t.
Lob Seruices: 7 I Zaca Lane, Suite I I 0
San Luis Obispo, California 93401
fax 805/544-8226 tel 8051544-4596
Zv^^I envi rotechnology ouAlrry AssuRANcE REpoRT - sptKE REsuLTs
l'
I
I
L
l
I
I
Client: Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Ob cA 93401
Project:UPS- SLO
Project Number:40065-OO2-01
Don PrattCollected
Lab Number:
Collected:
Received:
Matrix:
2839-2 Spike
11111193
11111193
eous
Sample Description:
MW-2
Analyzed: 11/16/93
Method: EPA 8260
STITUENT Amount Spiked Amount Recovered
ug/L
Percent
RecoveryIL
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate RecoverY
10.2
26.8
4.6
26.2
10.4
28.6
5.2
29.O
102
107
113
111
96
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
180
35o/o
182.
37%
101
ZymaX envirotechnology, inc. is certified by CA Department of Health Services:Laboratory #1717
NS - Not Spiked
Submitted by,
ZymaX envirotechnology, inc.
MSD #2
2839-2s.xls
JMM/smc/jmm/mas John MacMurphey
Laboratory Director
9"t- W
Accounting/Soles: 319 La Paloma
Shell Beach, California 93449
fax 8051773-07 95 tel 805/773-5402
Lob Services: 7l Taca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/544-4696
r
I
I
r
I
i
Air, Water & Hazardou
Certified Hazardous Waste,
s Waste Sampling, Analysis & Consultation
Chemistry, Bacteriology & Bioassay Laboratories
San Luis Obispo, CA . Benicia, CA . Camarillo, CA . San Jose, CA . Coleta, CA
Anaheim, CA . Tempe, AZ . Yalparaiso, IN . Westbrook, ME . Indianapolis, IN
ScCal Diirisicr-r (Carnarillo Laboratory) (BO5) 389-1353
4765 Cal1e Qtetzal , Canrari_I1o, Californ_i-a 930a2 FAX (805) 389-1438
CLID{f : Fted Castillo
tldted Parcel Services, le.jrtenance Departnent
1501 Randro Ccurcjo Blvd.
Nevtbury Park, CA 91320
REPORT OF A}ALYTIEAL RESULTS
SAI4PI,E DESCR]PTTCbT ICrRX(S.pI{PLED BY
ralc l{urnlcer
Project
Analyzed
lnalyzed by
le$rod
c,J- 5890 - 1
San Lu-is dcispo UPS PO
#8257388
t2h7 /e3
IG.
8502/80!5M
Pagre 1 of 1
SA}4PI,JED DATE RECEIVED
DrJllcing Water frcrn Well Head hefore
R.O. 3501 Sasanento
Drinking Water Brj-an pabst 1_2t/16/93 L2/15/93
CONSTTTT'ENI (CAS RN)RESULT
Pg/ t'
*PQL
lJg/ L.
IScrIE
H[EX( + TPFI (Gasolirre)
Benzene
Toluene
Ethylbenzerie
Xylenes (total)
Total Petroletrn fffdrocarbcrrs (Gasoline)
.Arnrunt Surrcgate Spiked
Percent Sr:rr. Recovery
pH of preserved sanpLe
1
0.6
s00.
10000 .
l{D
.ND
ND
ND
llD
10400
104
.)
0.3
0.3
0.5
1
This rryort. shia-l1 rrot be rryrod.rced except in ful1 wittrout prior writter-r:trprcnral frcrn CCA.S, Inc. r:b
CerEifications: CAH,AP #1598 & #rZg:; UTEI.AP #E-t+Z; AruIAp #M,O:'62; A2LA #0136-01; L.A-Co.CS #10187*RESULTS listed as rl{Dr were not detected at or abqve the listed PQL (practical O:antitaLicn Linait)(1) EcIRACIED kl/ EPA 5030 (purge-and-trap)
L2/22/e3
GC3/r€Cas038
MH/gps/]<hr
cJs9s323stz
Respectfully suhnitted,
-COAST
Ph.D
sEmrlcEs, INc
t
I
t
Air, Water & Hazardous Waste Sampling, Analysis & Consultation
Certified Hazardous Waste, Chemistry, Bacteriology & Bioassa y Laboratories
San Luis Obispo, CA . Benicia, CA . Camarillo, CA . San Jose, CA . Goleta, CA
Anaheim, CA . Tempe, AZ . Valparaiso, IN . Westbrook, ME . Indianapolis, IN
socal Dirrisicn (canrarillo raboratory) (805) 389-1353
4755 call-e Quetzal, Canarillo, california 93012 FAX (905)389-1438
QC Barch ID: CJ595323512
CI,IETT: Coast-to-Coast Analytical Services, Inc
Analyzed : t2/1"6/93
Analyzed LV: KR
lernod : E502l8015M
METTrcD BI,ANK
REPORr OF AIGLYITCAL RESULTS Page L of 1
SAI.{PLED DATE RECErVEDSA}4PLE DESCRIPTTO{IATRTX SA{PI.ED BY
MHIH@ BIANK Aqueous
CONSTITUENI (CAS RN)RESUI,T
tts/L
*PQL
IJg/ J'
IqcnE
HfH( + rPIl (Gasoline).
Benzene
Toluene
Ethylbenzene
Xylenes (tota1)
Tota] Petroler.rn t{a*:ocarbcns (Gasoline)
Arcullt Surrogate gpiked
Percent Surr. Recovery
1
0.3
0.3
0.3
ND
ND
m
ND
ND
11500
l_15
0.6
s00.
10000
This rryort sha11 r:ot be rryrodrced except in ful-1 witlrout prior written afproval frcrn CCA.S, Inc. rab Cer*RESULTS listed as rNDr were not detected at or above ctre listed pQL (practical Srantitaticn Ljrrdt)(1) EfIRACTD by EPA 5030 (purge-and-rrap)
L2/22/e3
GC3/r(3Cas02
MH/gps/khr
Gls9s3 -2
Respectfully sulcnr:ltted,
Pres
cek, Ph.D
INC
t
Air, Water & Hazardous Waste Sampling, Analysis & Consultaiion
Certifieo Hazardous Waste, Chemistry, Bacteriolo y & Bioassay Laboratories
San Luis Obispo, CA . Benicia, CA . Camarillo, CA . San Jose, CA . Coleta, CA
Anaheim, CA . Tempe, AZ . Valparaiso, IN . Westbrook, ME . Indianapolis, IN
SoCal Oivisicn (Carrarillo Iaboratory) (805) 389-1353
4765 Cal1e Quetzal , Carnarillo, Californ-ia 930L2 Fl,X (805)389-1438
QC BatcLi ID: Gf59532351-Z
CLISII: Coa-st-to-Coast Ar:alytical Services, Inc
I
l nnalyzed :
^imalyzed Llf:
fvlethod :
12/a7 /93
KR
E602l80L5M
SAT{PLE DESCRTPIIICN
QC PATRD( SPIKE
REPORT OF AqLYTICAL RESULTS
I@IITTTX SEMPLED BY
Page 1 of 1
SA{PI,ED DATE RECETVED
}ATRD( SPIKE Aqueous
@NSTITUENT ORTG]]qL
RESULT
SPIKE
.OM:UNT
RESUI.JT ?REC I\UIE
ps/L
BTH( + TPH (C"asoljle)
Benzene
Toluerie
EttryJ-benzene
Xylenes (tota1)
Total Petroleun tlproca:Ccors (Gasoljne)
23.
150.
31.'
230.
2000.
100
106
100
100
100
1
m
ND
liD
$rD
l{D
23.
170.
lJ- _
230.
2000.
Ttris report sha-U not be rryrr:d:ced elccept in ful1 without prior written atrp::ora.t frcrn CCA.S, Inc. Iab Cer
*RESULTS lj-sted as 'NDr rvrere not detected at or above the listed FQL (Practical Quantitaticrr LinLit)
(1) E(TRACTED h'L EPA 5030 (purge-ar:d-trap)
12/22/93
GC3/rGC3s040
MH/gps/khr
oJs953 -2
Respectfully sutraltted,
t_
L
, Ph.D
sEFncrs INC
t
Air, Water & Hazardous W
Certified Hazardous Waste, Che
aste Sampling, Analysis
mistry, Bacteriology & B
& Consultation
ioassay Laboratories
5an Luis Obispo, CA . Benicia. CA . Camarillo, CA . San Jose, CA . Goleta, CA
Anaheim, CA . Tempe, AZ . Valparaiso, IN . Westbrook, ME . Indianapolis, IN
Socal Dj.v-isicn (Canlarillo l€boratory) (805) 389-1353
4765 Ca11e Q:etzal , Carnarillo, Ca'liforrria 930L2 FAX (805)389-1438
QC Batdr ID: C,J5953235t2
Cf,IHr{I: Coa-st-to-Coast Analytical Services, Inc
analyzed
Analyzed by
l4ethod
L2/a7 /93
KR
E602l801sM
SAI4PI,E DES@TSIICN
QC IATRI( SPIKE
REPOM OF ATqLYTICAL RESULTS
lgrRrx SAT4PLM BY
Page 1 of 1
SA{PI,ED DATE RECEIVED
ICCRD( SPIKE DUPLICATE Aqueous
@Ngrr:IUEI{I Og1GIIq\L SpIKE RESULT ?REC ?DrFF t6rrE
RESULT TIVXSUNT IIS/L
HfD( + TPH (Gasolirre)
Benzene
Toluene
Ethrylbenzene
Xylenes (toral)
Total Petroler-rn f{drocarbo"rs (Gasolite)
23.
150.
31.
230 _
2000 -
24.
,170-
33.
240.
2100.
104
106
r-06
104
105
4-3
U.
6.2
4.3
4_9
t_
ND
ND
ND
ND
ND
ltris report, sha-ll not be reprod:ced except in ful-l witliout prior written a{pnoval frcrn CCA.S, fnq. rah Cer*RESULTS listed as rNDr were not detected at or above tlte listed pe], (practj-cal e:antitaticn Limit)(1) EfIRACIED by EPA 5030 (purge-and-rrap)
l
i
L2/22/e3
GC3/r(3Cas041
MH/gps/khr
cJ5953 -2
Respectfully suhnitted,
coAsT-TO-COA.SI
Ph.D
SETMICES, n\C
r Zy^^I envirotechnology OUALITY ASSURANCE REPORT-
SPIKE DUPLICATE RESULTS
Client: Bob Wilson
Seacor Environmental Engineering
3485 Sacramento Drive, Suite A
San Luis Obis cA 93401
Lab Number:
Collected:
Received:
Matrix:
2439-2 Spike Duplicate
11111t93
11111193
eous
Sample Description:
MW-2
Analyzed: 1 1/16/93
Method: EPA 8260
Project UPS- SLO
Proiect Number:A0065-002-01
Don PrattCollected
coN T Amount Spiked
ug/L
Amount Recovered
us/L
Percent
Recovery
Relative Percent
Diflerence*
Benzene
Toluene
Ethylbenzene
Xylenes
Percent Surrogate RecoverY
10.2
26.8
4.6
26.2
10.0
27.6
4.7
26.6
9B
103
102
102
4
4
10
I
99
TOTAL PETROLEUM HYDROCARBONS
Gasoline
BTX as a Percent of Fuel
180
35o/o
183
35%
102 1
ZymaX envirotechnology, inc. is certified by CA Department of Health Services: Laboratory #1717
*Relative Percent Difference of the spike and spike duplicate
NS - Not Spiked
Submitted by,
ZymaX envirotechnology, inc
MSD #2
2839-2s.xls
JMM/smc/jmm/mas Laboratory Director
Accounting/Soles: 3 l9 La Paloma
Shell Beach, California 93449
Lob Services; 7l Zaca Lane, Suite I l0
San Luis Obispo, California 93401
fax 805/544-8226 tel 805/54 4'4696; fax 805/773-0795 tel 8051773-5402
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Benzene
Toluene
Ethylbenzene
Xylenes
envirotechnology
OUALITY ASSURANCE REPORT -
Client
ZymaX envirotechnology, inc.
71 Zaca Lane, Suite I 10
San Luis Obis cA 93401
Project:
Project Number:
Collected
0.5
0.5
0.5
0.5
Percent Surrogate Recovery
TOTAL PETROLEUM HYDROCARBONS
Gasoline
50
BTX as a percent of Fuel
ZymaX envirotech nology, inc. is certifie dbyCAD*POL - Practical Ouantitation Limit
epartment of H ealth Services:Labo
*Results listed as ND would have been reported if present at or above the risted pol
Submitted by,
ZymaX envirotechnology, inc.
BLANK RESULTS
ND
ND
ND
ND
95
ND
N/A
I
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ratory #1717*
MSD #2
b11169.xls
JMM/smc/jmm/sc John MacMurphey
Laboratory Director
Lob Seryices: 7 I Zaca Lane, Suite I I 0
- San Luis Obispo, California 93401
tax 805/544-8226 tet 80S/54 4-4696
Lab Number:
Collected:
Received:
Matrix:
BLK 11t16t93
eous
s ample Description:
Analyzed:
Method:
lnstrument Blank
11t16t93
EPA 8260
POL*
ug/L
T
*ULT
ug/L
Accounting/Soles: 319 La paloma
Shell Beach, California 93449
fax 805t7t 3 -0795 tet 805/773-5402
)Chain-of-Custody Number: A 9589 \
AY
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Sample ID
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Time Matrix
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Project Manager
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DateTime
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Chain of custody seals:
Rec'd good condition/cold:
Confor#s to record:1
Comments,/
Instructions
Request
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