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HomeMy WebLinkAboutSLOUNIFLOW_FS1 Admin iRC3926i Color_2474_001Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 0310l/2021O9:47 Sample Summary Sample ID Laboratory ID Client Matrix Lab Matrir Date Sampled Dste Received NWWall NEWall SE Wall SWWall NW Tank Bottom SE Tank Bottom Soil Pile Composite 2101070-01 2101070-02 2101070-03 2101070-04 2101070-05 2101070-06 2101070-07 Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid 02117/202111:30 02117/202111:32 02/17/2021 tl;34 02/1712021ll:36 02117/2021ll:38 02117/2021ll:40 02117/202111:45 021171202112:30 021171202112:30 02117/202112:30 02117/202112:30 02117/202112:30 02/1712021 12:30 021171202112:30 Sample Batch Preparation Summary Analysis Batch ID Preparation Date/Tine OEC Admin Services Chromatograms Semi-Volatile Organic TPH by GC/FID 8015 Diesel & Motor Oil List STLC Metals by ICP 60108 STLC STLC Metals Extraction STLC Metals Extraction TCLPMetals by ICP 60109 TCLP TCLP Metals Extraction TCLP Metals Extraction Total Metals by CVAA Mercury Tota1EPL747lA Total Metals by ICP 60i0B Total Volatile Organic Compounds by GC/IVIS 82608 Full List Volatile Organic TPII by GC/FID 8015 TPH-Gasoline 8180595 B1B08l7 8180665 81B0796 8180668 BlB0575 8180590 81B0563 B180591 02/18/2021 13:20 02/25/2021 1'l:39 02122/2021 09:22 02/25/2021 09:14 02/22/2021 09:54 02/18/2021 O8:05 02118/2021 09:11 02/1712021 1606 02/18/2021 09:21 The results in this repott apply to the sampla analyzed in accordance with the chain of custody doument. This analytical report must be reprcduced in its entirety. California ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 w\rvw.oecusa.com FAX: (805) 925-3376 Page 2 of 52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 031011202109:47 Analytical Report for Samples Sample ID : NW Walt Mahix: Solid Lab ID : 2101070-01 Sampled : 02117 l2l ll :30 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.091 mC.&C 1 8180575 021t8/21 13:45 EPA74"11A Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zlnc STLC Metals by ICP ND 3.3 140 ND ND 160 1t l4 2,2 ND 340 ND ND ND 35 27 2.4 1.9 0.96 0.48 0.24 0.48 0.48 0.96 0.48 0.48 0.48 t.9 0.48 0.96 1.9 1.9 mC/kC 1 BlB0590 02/19/21 10:01 EPA 60lOB N-02, N-03 N-02 Chromium Nickel TCLP Metals by ICP 0.39 2.2 0.10 0.10 mg[- 2 B180817 02126/21 12:13 STLC/EPA 60108 Chromium ND 0.050 mglL 1 8180796 02125121 19:49 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of custody domment. This analytical rcport must be reproduced in its entirety, California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 3 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2t01070 03/01/202109:47 Analytical Report for Samples Sample ID : NW Wall Matrix: Solid Lab ID : 2101070-01 Sampled : 0211.7 l2l ll :30 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/ITD R-07 TPH Gasoline (C5-C12) Surrogate : 4 - B ro moJluorc benzen e ND 5.0 85% -dkg I (31 - 168) B1B0s91 02/19/21 10:23 EPA 80I5M Semi-Volatile Organic TPH by GCmfO TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate : o-Ter p heny I ND ND l0 mdkC 1 50 102% (65-133) BlB0595 02118/21 17:13 EPA 8015M The rcsults in this report apply to the samples analyzed in accordance with the chain of ffitody doctmenl This analylical rcport must be reproduced in its entirety. Client Connect: client.oec.com\reports TEL: (805) 9224772 (805) 925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oeGusa,com FAX: Page 4 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03/0I/202109:47 Analytical Report for Samplcs SampleID: NWWatt Matrix: Solid Lab ID : 2101070-01 Sampled : 02117 l2l ll :30 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/1US R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene seo-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodi fl uorometlane 1,1 -Dichloroethane 1,2-Dichloroethane 1, i -Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene i,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- I ,3 -Dichloropropene trans- 1,3 -Dichloropropene Ethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 t.2 t.2 1.2 1.2 1.2 1.2 1.2 t1 ta t.2 1.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 1..2 t.2 1..2 1.2 t.2 1a 1.2 1.2 1.2 1.2 1.2 11 1a 11 t.z 1.2 1.2 mdkc 1000 8180563 02/18/21 12:01 EPA 82608 The results in this report apply to the samples analyed in accordance with the chain of custody document. This analytical report m6t be reproduced in its entircty. Client Connect: client.oec.com\reports TELi (805) 9224772California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 FAX: (805) 925-3376www.oecusa,com Page 5 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P.O.Box2646 OrcuttCA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03/01/202109:47 Analytical Report for Samples Sample ID : NWWall Matrix: Solid Lab ID : 2101070-01 Sampled : 02/17 l2l ll :30 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IUS (Continued)R-07 Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene (TCE) Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylberzene Vinyl chloride Xylenes (total) Surro gate : D ibro mofluo romet han e Surrogate: Toluene-d8 Surrogate : 4- B rc m oflu orob ewene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.2 1.2 t.2 t.2 1n 1.2 r.2 t.2 1.2 1.2 t.2 t.2 t.2 t.2 ll 1.2 1..2 1.2 1.2 l,) 11 88% 95% 101 % mg&g 1000 8180563 02118/27 12:01 EPA 82608 (7s-122) (66- 128) (76- r22) The results in this report apply to the samples analyzed in accordance with the chain ofcustody doatment. This analytical report must be reproduced in ils entirety. California ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELI (805) 9224772 www'oecusa'com FAX: (805) 925-3376 Page 6 of52 Oilfield Environmental & Compliance, lnc. Pacific Peholeum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2t0lo70 031011202109:47 Analytical Report for Samples Sample ID : NE Wall Matrix: Solid Lab ID : 2101070-02 Sampled :, 02/17 /21 ll:32 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.097 me/kg 1 8180575 02/18/21 13:51 EPA747IA Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc STLC Metals by ICP ND 4.3 140 ND ND 160 32 20 4.Q ND 400 ND ND ND 3E 36 2.3 t.9 0.93 0.46 0.23 0.46 0.46 0.93 0.46 0.46 0.46 1.9 0.46 0.93 1.9 1.9 mg/kg 1 BlB0590 02119/21 10:03 EPA 601OB N-02, N-03 N-02 Chromium Nickel TCLP Metals by ICP 0.77 3.5 0.10 0.10 mg[-J BlB0817 02/26/2112:40 STLC/EPA60108 Chromium ND 0.050 mg/L I 8180796 02125/21 19:52 EPA 1311/EPA6010B The results in this report apply to the samples analyzed in accordance with the chain of castody document. This analytical rcport must be repmduced in i* entirety. Client Connect: client.oec.com\reports TEL:. (805) 9224772 FAX: (805) 925-3376 Cal ifornia ELAP Certific ale # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com Page 7 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P.O.Box2646 Orcutt CA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2t0t070 03l0ll2021 O9:47 Analytical Report for Samples SampleID: NE Wall Matrix: Solid Lab ID : 21010'10-02 Sampled : 02/17 /21 ll :32 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/F"ID R-07 TPH Gasoline (C5-C12) Surro gate : 4 - B ro mofl uoro b enze ne Semi-Volatile Organic TPH by GC/T'ID ND 5.1 82% mdkC I (3t - 168) BlB0591 02/19/21 10:55 EPA 8015M TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Surrogate : o-Terphenyl ND ND m9lk9 1 8180595 02/18/21 17:28 EPA 8015M (6s-133) l0 50 103 % The results in this report apply to the samples analyzed in accordance with the chain of cwtody docament. This analytical report must be rcproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 8 of 52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum Califomia P. O. Box 2646 orcutr cA, 93457 Project: Pacific Petroleum Project Number: CSI Conskuction Project Manager: Clarence Reynolds WO & Reported: 2101070 031011202109:47 Analytical Report for Samples Sample ID : NE Wall Matrix: Solid Lab ID : 2101070-02 Sampled : 02/17 /21 ll :32 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3 -chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1, I -Dichloropropene cis- 1,3 -Dichloropropene trans- 1,3 -Dichloropropene Ethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1? l.J l.J 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 l.J 1.3 1.3 i.3 l.J 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 mC/kC 1000 8180563 02/18/21' 12:58 EPA 82608 The results in this report apply to the samples analyzed in accordance with the chain of custody docttment. Ihis analytical rcport must be repmduced in its entirety. Client Connect: client.oec.com\reports TELI (8O5) 9224772 FAX: (805) 925-3376 California ELAP Gertificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa-Gom Page 9 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P.O.Box2646 Orcuft CA, 93457 Project: Pacific Petroleum ProjectNumber: CSI Conshuction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109:47 Analytical Report for Samples Sample ID : NE Wall Matrix: Solid Lab ID : 2101070-02 Sampled : 021 l7 127 1l:32 Sampled by : Clarence Reynolds FieldData:NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS (Continued)R-07 Hexachlorobutadiene 4-Isopropyl Toluene Isopropyibenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tekachloroethane 1, I,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3 -Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl ohloride Xylenes (total) Sur ro gdte : D ib ro mofluo romet hane Surrogate: Tbluene-d8 Surrogate : 4 -B ro m of uorob enzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.J 1.3 i.3 1.3 i.3 1.3 1.3 1.3 1.3 I.J 1.3 1.3 1.3 1.3 1.3 1.3 i.3 1.3 l.J 1.3 1.3 1.3 86% 96% 98% mdkc 1000 8180563 02118/21 12:58 EPA82608 (75-r22) (66- 128) (76- 122) The rcsults in this report apply to the samples analyzed in accordance with the chain of ustody doalment. This analytical report must be ,eprcduced in its entire$. Galifornia ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL:. (8O5) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 10 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2l0lo70 03l0ll2021 09:4'l Analytical Report for Samples Sample ID : SE Walt Matrix: Solid Lab ID : 2101070-03 Sampled : 021 17 121 17 :34 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.092 mg/kC 1 BlB0575 02/18/21 13:53 EPA747IA Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc STLC Metals by ICP ND 3.3 150 ND ND 200 t9 t7 2,0 ND 340 ND ND ND 33 26 2.3 1.9 0.93 0.46 0.23 0.46 mC/kg BlB0590 02/19/21 10:14 EPA 60108 0.46 0.93 0.46 0.46 0.46 1.9 0.46 0.93 1.9 1.9 N-02, N-03 N-02 il Chromium Nickel TCLPMetals by ICP 0.59 3.3 0.10 0.10 mg/L 2 BlB0817 02/26/21 12:43 STLC/EPA 60108 Chromium ND 0.050 mslL 1 8180796 0212512t 19:55 EPA 1311/EPA 60108 The resuhs in this report apply to the samples analyzed in accordance with the ehain of custody ilocttment. This analytical report mwt be rcpruduced in its entirety, California ELAP Certificale # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (8QQ 925-3376 Page 1 I of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petoleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2tot070 03/01/202109:47 Analytical Rcport for Samples Sample ID : SE Wall Mahix: Solid Lab ID : 2101070-03 Sampled : 02/17 /21 ll'.34 Sampledby : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/IID R-07 TPH Gasoline (C5-C12) Sur ro gate : 4 - B ro m oJluoro b enz ene ND 4.7 77% -dkg 1 (31 - 168) 8180591 02/l9l2l 11:23 EPA 8Oi5M Semi-Volatile Organic TPH by GC/FID TPH Diesel (C13-C22) TPH Motor Oil {C23-C40) Surrogate : o-Tbrp h eny I ND ND 10 50 102 % mg/kC 1 BlB0595 02/t8/21 17:42 EPA 8015M (6s-133) The resul5 in this repofi apply to the samples analyzed in accordance with the chain of cttstody doanment. This analytical report must be reproduced in its entireA. Client Connect: client.oec.com\reports TEL: (8AQ 9224772California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 FAX: (805) 925-3376www.oecusa.com Page 12 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum Califomia P. O. Box 2646 OrsxtCA,93457 Projecl Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 210t010 03/01-12021 09:47 Analytical Report for Samples Sample ID : SE Wall Matrix: Solid Lab ID : 2101070-03 Sampled : 02ll7l2l ll:34 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GCIIVIS R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifl uoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene f ans- 1,2-Dichloroethene 1,2-Dichloropropane I ,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- 1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 t.2 7.2 1.2 1.2 1.2 1.2 1.2 t.2 1.2 1.2 t.2 1.2 1.2 t.2 1.2 r.2 1.2 t.2 t.2 t.2 1.2 t.2 t.2 1.2 1.2 1.2 t.2 1.2 1.2 1.2 1t t.2 1.2 1.2 mdkC 1000 8180563 02118/21 13:27 EPA 82608 t The rcults in this report apply to the samples analyzed in accordance with the chain of ustody docament. This analytical report must be reptoduced in its enlircA. California ELAP Certificale # 2438 Client Connect: client.oec.com\reports TELi (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 13 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project PacificPetroleum ProjectNumber; CSI Conskuction Project Manager: Clarence Reynolds WO & Reported: 2101070 0310112021 O9:4'l Analytical Report for Samples Sample ID : SE Wall Makix: Solid Lab ID : 2101070-03 Sampled : 02/ l7 /21 ll :34 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS (Continued)R-07 Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1,1, 1-Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3 -Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Surrc gate : Dibromofluo romet hane Surrogate: Toluene-d8 Surrogat e : 4 - Bromofluorob enzen e ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 t.2 t.2 t.2 1.2 t.2 t.2 t.2 t.2 t.2 r.2 1.2 t.2 t.2 1.2 t.2 t.2 t.2 t.2 1.2 t.2 1a 87% 96% 97% mg/kg 1000 8180563 02118/21 13:27 (75-122) (66- 128) (76- 122) EPA 82608 The results in this report apply to the samples analyzed in accordance with the chain of custody doctment. This analytical rcport mut be reprodueed in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page l4 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Projecf Pacific Petroleum Project Number: CSI Conskuction Project Manager: Clarence Reynolds WO & Reported: 2101070 O3/011202109:41 Analytical Report for Samples Sample ID : SW Wall Mahix:Solid Lab ID : 2101070-04 Sampled : 02117 /21 ll'36 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.089 mdkg 1 8180575 02/18121 13:55 EPA,7471A Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc STLC Metals by ICP ND 2.9 130 ND ND 160 18 t6 12 ND 330 ND ND ND 31 33 2.3 1.9 0.93 0.47 0.23 0.47 0.47 0.93 0.47 0.47 0.4'1 1.9 0.47 0.93 1.9 1.9 mC/kC 1 8180590 02119/21 70:17 EPA6OiOB N-02, N-03 N-02 Chromium Nickel TCLPMetals by ICP 0.48 3.4 0.10 0.10 mgll- 2 BIB08I7 02/26121 12:45 STLC/EPA 60108 Chromium ND 0.050 mglL 1 8180796 02/25/2t 19:57 EPA 1311/EPA 60108 The results in this report apply to the samples analyzed in accordance with the chain of custody doatmenl This analytical rcport mwt be reprcduced in its entirety, California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (8OS)9224772 www.o€cusa.com FAX: (805) 925-3376 Page l5 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reyrolds WO & Reported: 2r0to70 0310112021 O9:4'l Analytical Report lbr Samples Sample ID : SW Wall Mahix: Solid Lab ID : 2101070-04 Sampled : 02ll7l2l ll:36 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic TPH by GC/IID R-07 TPH Gasoline (C5-C12) Surro gate : 4-B romofluorc bewene Semi-Volatile Organic TPH by GC/FII) ND 4.8 81 % mdkC 1 ( 3t - 168 ) BlB0591 02/19/21 1l:51 EPA 80I5M TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Sunogate: o-Terphenyl ND ND 10 50 101 % m&&c 1 8180595 02/18/21 17:56 (6s-133) EPA 8015M The ,esults in this report apply to the samples analyzed in accordance with the chain ofcustody doctmenl This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 16 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcr*tCA,93457 Project: PacificPeholeum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2r0to70 03/011202109t47 Analytical Report for Samples Sample ID: SWWall Matrix: Solid Lab ID : 2101070-04 Sampled : 02ll7l2l 11:36 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/MS R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- 1,3 -Dichloropropene trans- 1,3 -Dichloropropene Ethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 1) t.2 1.2 ta 11 1.2 LZ t.2 t1 'l) la 1) t1 1') 1.2 1A 1.2 t.z 1.2 1.2 1.2 t.2 1.2 t.2 t.2 1.2 t.2 1.2 t.2 t.2 t.2 t.2 11 1) mc&c 1000 8180563 02/18/21 13:55 EPA 82608 The results in this report apply to the samples analyzed in accordance with the chain ofcutody doctment. This analytical report mwt be rcproduced in its entirety. California ELAP Certiflcale # 2438 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 9224772 FAX: (805) 925-3376 Client Connect: client.oec.com\reportg www.oecusa.com Page l7 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 031011202109:47 Analytical Report for Samples SampleID: SWWall Matrix: Solid Lab ID : 2101070-04 Sampled : 02117 /21 ll :36 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Anilyzed Method Notes Volatile Organic Compounds by GC/IVIS (Continued)R-07 Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroeihene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1,1, l-Trichioroethane 1, I,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Surrogate : DibromoJluo rome t hane Surrogate: Toluene-d8 Surrogate : 4- Bromo fluo rob e nze ne ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ta 1.2 1.2 1.2 t.2 t.2 1.2 1.2 t.2 t.2 1.2 1.2 t.2 t.2 t.2 t.2 t.2 1.2 t.2 1.2 1.2 1.2 87% 95% 97% mdkc 1000 8180563 02118/21 13:55 EPA 82608 ,r, -,14 (66- 128) (76- 122) The rcsults in this report apply to the samples analyzed in accordance with the chain ofcustod.y docttment. This analytical rcport must be reprtdueed in its mtirety. Cal ifornia ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 9224772 FAX: (805) 925-3376 Client Gonnect: client.oec.com\reports www.oecusa.com Page I8 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03l0ll202l O9:47 Analytical Report for Samples Sample ID : NW Tank Bottom Matrix: Solid Lab ID : 2101070-05 Sampled : 02117 /21 11 :38 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP 0.15 0.099 mC/kC 1 BlB0575 02118/21 13:57 EPA7471A Antimony Arrenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc ND 2.0 12 ND ND 27 2.9 8.0 7.4 ND 36 ND ND ND 23 s00 2.3 1.9 0.94 0.47 o.23 0.4'1 0.4't 0.94 0.47 0.4'7 0.4'7 t.9 0.47 0.94 1.9 1.9 mc/kg 1 BlB0590 02/19/21 10:19 EPA 60108 Volatile Organic TPH by GC/T'ID R-07 TPH Garoline (C5-C12) Surrogate : 4 - B romofluorob enzen e Semi-Volatile Organic TPH by GC/TID 52 4.6 94% mgkc 1 (31 - 168) BlB0591 02119/21 13:17 EPA 8015M E TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surrogate: o-krphenyl 2500 ND 20 100 103 % mg/kg J BlB059s 02/l9l2l 09:1t EPA 8OI5M D-07 (6s - 133) The results in this report apply to the samples analyzed in accordance with the chain of custody ilocament. Ihis analytical rcport must be reprcduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL:. (805) 9224772 FAX: (805) 925-3376ww,w.oecusa.com Page 19 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project Pacific Petroleum Prqiect Number: CSI Construction Project Manager: Clarence Reynolds WO & Repoded: 2tot070 03/Ol/202109:47 Analytical Report for Samples Sample ID : NW Tank Bottom Matrix : Solid Lab ID : 2101070-05 Sampled : O2ll7 121 ll :38 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomet}tane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chioroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromodthane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- 1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 t.2 t.2 t.2 1.2 t.2 r.2 t.2 t.2 t.2 t.2 t.2 1.2 t.2 t.2 t.2 t.2 1.2 1.2 1.2 1.2 1.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 1t l1 1.2 L.Z t.2 t.2 ms.&c 1000 8180563 02/18/21 14:24 EPA 82608 fi il The results in this report apply to the samples analyzed in accordance with the chain of custody domment. This analytical report mut be reproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 9224772 FAX: (805) 925-3376 Client Connect: client.oec.com\reports www.oecusa.com Page 20 of 52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 QrctrttCA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 031011202109:47 Analytical Report for Samples Sample ID : NW Tank Bottom Matrix : Solid Lab ID : 2101070-05 Sampled : 02/17 /21 ll :38 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS (Continued)R-07 Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1, l, 1,2-Tetrachloroethane 1, i,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene i,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1,1, 1-Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Suno gate : D ibro mofluo rome thane Surrogate: Toluene-d8 Surrogate : 4 - B romofluorob enzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1J 1.2 1.2 t.2 1.2 1.2 11 tt 11 t.2 It t.z 1.2 1.2 1.2 1.2 1.2 1.2 t.2 87% 95% 98% mdkg 1000 8180563 02/18/21 14:24 EPA 82608 (7s - t22) (66- 128) (76-122) The resuhs in this report apply to the samplu analyzed in accordance with the chain of crcto$t domment. This analytical report m6t be rcprodueed in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\reports TEL: (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 2l of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 OrcuttCA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109:47 Analytical Report for Samples Sample ID : SE Tank Bottom Matrix: Solid Lab ID : 2101070-06 Sampled : 02/17 /21 7l:40 Sampled by : Clarence Reynolds Field Data : NA Analyte Result RI Units Dilution Batch Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP 0.13 0.092 -dkg 1 B1B0575 02/18/21 13:59 EPA,7471A Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Volatile Organic TPII by GC/IID 2.5 2.0 0.98 0.49 0.25 0.49 0.49 0.98 0.49 0.49 0.49 2.0 0.49 0.98 2.0 2.0 ND 3.4 88 0.49 2.3 47 3.9 t4 6.1 ND 67 ND ND ND 23 820 mC/kC I BlB0590 02/l9l2l 10:22 EPA 60lOB R-07 TPH Gasoline (C5-C12) Surro gate : 4- B ro mofluorob enzene ND 5.1 8t% mdkc 1 (31 - 168) B1B0591 02119/21 12:20 EPA 8015M Semi-Volatile Organic TPH by GCIFID TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surro gate : o -Terp heny I t5 ND 10 50 102 % mClkC 1 B1B0595 02/18/21 18:70 EPA 80i5M (6s-13s) The results in this report apply to the samples analyzed in accordance with the chain of custody doumenL This analylical report mwt be reprcduced in its entirety. Client Connect: client.oec.com\reports TELI (805) 9224772 FAX: (805) 925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa,com Page 22 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 QrcuttCA,93457 Project Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO &Reported: 2101070 031011202109:47 Analytical Report for Samples Sample ID : SE Tank Bottom Matrix: Solid Lab ID : 2101070-06 Sampled : 02/17 l2l ll :40 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butyibenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane i,2-Dibromoethane (EDB) Dibromomethane I,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane I ,1 -Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1 ,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane I , 1 -Dichloropropene cis- 1,3 -Dichloropropene trans- 1,3 -Dichloropropene Ethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1a ta t.2 1.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 1.2 1.2 11 t.2 t.2 t.2 t.2 1.2 t.2 1.2 t.2 t.2 t.2 t.2 t.2 1.2 1.2 11 1.2 1..2 1a 1'' 1.2 1t 1.2 mg/kg 1000 8180563 02/18/21 14:52 EPA 82608 The rcsults in this report apply to the samples analyzed in accordance with the chain of custody iloument. Ihis analytical report must be reprcduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 $rv'w.oecusa.com FAX: (805) 925-3376 Page 23 of 52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 orcutt cA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Repoted: 2tot070 03/01/202109:47 Analytical Report for Samples Sample ID : SE Tank Bottom Matrix: Solid Lab ID : 2101070-06 Sampled : 02117 /21 1l :40 Sampled by : Clarence Reynolds Field Data: NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/IVIS (Continued)R-07 Hexachlorobutadiene 4-IsopropyI Toluene Isopropylbenzene Mothylene chloride Naphthalene n-Propylbenzene Styrene l, 1, 1,2-Tetrachloroethane 7,1,2,2 -Tetr achloroethane Tetrachloroethene (PCE) Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1, l-Triohloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3-Trichloropropane 1,2,4-Trii, ethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Surro g ate : D ib romofluo rome t hane Surrogate: Tbluene-d8 Surrogate : 4-B rcmofluo rob enzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 1.2 1t la 1.2 t.2 1.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 1.2 t.2 t.2 1.2 1.2 1.2 t1 87% 96% 99% mclks 1000 8180563 02/18/21 14:52 EPA 82608 i,, - ,,,, (66- t28) (76- 122) The results in this report apply to the samples analyzed in accordance with the chain of custody dodmenL This analylical report must be rcproduced in its entiret!. Client Connect: client.oec.com\reports TEL: (805) 9224772 (805)925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: Page 24 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109:47 Analytical Rcport for Samples Sample ID : Soil Pile Composite Matrix : Solid Lab ID : 2101070-07 Sampled : 02117 /21 lll45 Sampled by : Clarence Reynolds FieldData: NA Analyte Result RL Units Dilution Batoh Analyzed Method Notes Total Metals by CVAA Mercury Total Metals by ICP ND 0.096 mdkg i 8180575 02/18/21 14:01 EPA7471A Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum NickeI Selenium Silver Thallium Vanadium Zinc ND 3.1 95 ND ND 7t 13 t4 10 ND 180 ND ND ND 2l t20 2.3 1.8 0.91 0.46 0.23 0.46 0.46 0.91 0.46 0.46 0.46 1.8 0.46 0.91 1.8 1.8 mClkC 1 B1B0590 02/19/21 10:25 EPA 601OB N-02 STLC Metals by ICP Chromium Volatile Organic TPH by GC/FID 0.40 0.10 mglL 2 BlB0817 02/26121 12:48 STLC/EPA6010B R-07 TPH Gasoline (C5-C12) Sur ro gate : 4- B ro mofluoro b enzene ND 4.5 86% mC/kC I (31 - 168) BlB0591 02/t9/21 12:48 EPA 8015M The results in this report apply to the samples analyzed in accordance with the chain of custod), doumenl This analytical rcport must be rcpmduced in its atirety' Client Connect: client.oec.com\reports TEL: (BAQ 9224772 (80s)925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: Page 25 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcuft CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 o3l0ll202109:47 Analytical Rcport for Samples sample ID : Soil PiIe Composite Matrix: Solid Lab ID : 2101070-07 Sampled : 02/17 /27 ll :45 Sarrpled by : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batch Analyzed Method Notes Semi-Volatile Organic TPH by GC/T'ID TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surrogate: o-krphenyl ND ND t0 50 r03 % mdkC 1 B1B0595 02/18/21 18:38 EPA 8OI5M (6s-1s3) The resul* in this report apply to the samples analyzed in accordance with the chain ofcustody doument. This analytieal report must be repmduced in its entitety. Client Connect: client.oec.com\reports TEL: (8A$ 9224772 FAX: (805) 925-3376 California ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com Page 26 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2t01070 031011202109:47 Analytical Report for Samples Sample ID : Soil PiIe Composite Matrix: Solid Lab ID : 2101070-07 Sampled : O2/17 l2l ll :45 Sampled by : Clarence Reynolds FieldData : NA Analye Result RL Units Dilution Batch Analyzed Method Notes Volatile Organic Compounds by GC/1VIS R-07 Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene D ichlorodifl uoromeflane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1, l -Dichloropropene cis- 1,3-Dichloropropene trans- 1,3-Dichloropropene Ethyibenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND t.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 1.2 t.2 t.2 1.2 t.2 t.2 1.2 t.2 t.2 t.2 t.2 7.2 t.2 1.2 t.2 1.2 t') 11 1.2 1.2 t.2 t.2 t.2 t.2 mdkg 1000 8180563 02/18/21 15:21 EPA 82608 The rcsults in this report apply to the samples analyzed in accordance with ,he chain of custody doctment. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELI (805) 9224772 wwwoecusa.com FAX: (805) 925-3376 Page 27 of52 Oilfield Environmental & Compliance, lnc. Pacific Peholeum Califomia P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 210t070 03/01/202109:47 Analytical Report for Samplcs Sample ID : Soil Pile Composite Matrix: Solid Lab ID : 2101070-07 Sampled : 02117 l2l ll :45 Sampledby : Clarence Reynolds Field Data : NA Analyte Result RL Units Dilution Batoh Analyzed Method Notes Volatile Organic Compounds by GC/IUS (Continued)R-07 Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene l, 1, 1,2-Tekaohloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3 -Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Surrogate : Dibro moJluoromet han e Surrogate: Toluene-d8 Suno gate : 4- B ro moJluo rob enzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1a 1a 1' t.2 t.2 t.2 1.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 t.2 1.2 1.2 1.2 t.2 1a tt 1.2 88% 96% 98% mdkC 1000 8180563 A2/l8l2l 15:21 EPA 82608 (7s-122) (66- 128) (76- 122) The results in this report apply to the samples analyzed in accordance with the chain of cutody doament. This analytical report must be reprcduced in its entireA. Client Connect: client.oec.com\reports TELi (805) 922'4772 FAX: (805) 925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa,com Page 28 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 orcutt cA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109:47 Total Metals by CVAA - Quality Control Analyte Result RL Units Spike Level Source Result %REC ToREC Limits RPD RPD Limit Notes Batch B180575 - EPA 7471A Preparation: EPA 74714 Prep 021 18/21 08:05 Blank @180575-BLKI) Mercury LCS (B1B0s7s-BS1) Mercury LCS Dup (B1B0575-BSD1) Mercury Dupltcate (B1B0575-DUP1) Mercury Matrix Spike (8180575-MSl) Mercury Matrix Spike Dup (8r80575-MSDl) Mercury Post Spike (81B0575-PS1) Mercury 0.845 0.8s7 Source: 2101084-05 0.0290 Source: 21010E4-05 0.804 Source: 2101084-05 0.808 Source: 21010E4-05 s.32 Analyzed: 02/ 18 l2l 13 :33 0.10 mg/kg Analyzed: 021 I 8 /21 13 :29 0.10 mC/kC 0.833 Analyzed: 02/ | 8 l2l 13 :3 I 0.10 mg/kg 0.833 Analyzed: 021 18/21 13:37 0.097 mC/kC 0.0229 Analyzed: 02/ 18/21 13:39 0.090 rng/kC 0.751 0.0229 Analyzed: 021 18121 13:41 0.093 mc/ks 0379 4.0229 Analyzed: 02/ 18/21 13 :43 ug/l- 5.00 ND 10i 85-115 103 85-115 104 '75-t25 24 20 QR-04 120 0.5 20l0l '15-125 0.157 103 85-115 The results in this report apply to the samples analyzed in accordance with the chain of custody dorument. This analytical report mwt be reproduced in its entirety. California ELAP Certiflcate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client,oec.com\reports TELI (8O5) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 29 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 210L070 031011202109:47 Total Metals by ICP - Quality Control Analyte Result RL Units Spike Level Source Result %REC ToREC Limits RPD RPD Limit Notes Batch B1B0590 - EPA 60108 Preparation: EPA 30508 02/1.8/21 09:ll LCS @rB0s90-BS1) Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc LCS Dup (8180590-BSDI) Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Analyzed: 02/ 19 /21 09:25 2.5 mg/kg 100 2.0 ' 100 1.0 ' 100 0.50 u 100 0.2s " 100 0.s0 ' 100 0.50 u 100 1.0 " 100 0.50 ' 100 0.50 u 100 0.50 u 100 2.0 ' 100 0.50 ' 5.00 1.0 . 100 2.0 ' 100 2.0 ' 100 Analyzed: 021 19 /21 09:27 2.5 mdkg 100 2.0 ' 100 1.0 " i00 0.s0 ' 100 0.25 ' 100 0.50 n 100 0.s0 ' 100 1.0 " 100 0.50 ' 100 0.s0 " 100 0.50 u 100 2.0 ' 100 0,50 ' 5.00 1.0 u 100 2.0 ' 100 2.0 . 100 95.8 95.4 103 99.9 98.0 100 99.2 99.0 99.4 9s.7 96.3 94.s 4.80 100 93.8 98.2 1 0.2 2 2 1 , 1 I 1 o.7 0.05 0.5 t 0.9 0.9 I 4.',72 96 95 103 100 98 100 99 99 99 96 96 94 96 100 94 98 95 95 101 98 97 98 98 98 98 95 96 94 94 99 93 97 80-i20 80-120 80-120 80-120 80-i20 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-i20 80-120 80-120 80-120 94.8 9s.2 101 98.2 97.0 98.4 97.9 97.6 98.1 95.0 96.2 94.0 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 99.4 93.0 97.0 The results in this report apply to the samples dnalyzed in accordance with the chain of cltstody doatment. This analytical report must be rcproduced in its enlireA. Galifornia ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 922-4772 www.oecusa.com FAX: (805) 925-3376 Page 30 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project Pacific Petroleum Projoct Number: CSI Constuction Project Manager: Clarence Reynolds WO & Reported: 2t0lo70 0310112021 09:4'l Total Metals by ICP - Quality Control Analyte Result RL Units Spike Level Sowce Result %REC ToREC Limits RPD RJD Notes Limit Batch BlB0590 - EPA60108 Preparation: EPA30508 02ll8l2l 09:ll Matrix Spike @1B0590-MS1) Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Matrix Spike Dup @180590-MSDI) Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Source: 2101085-04 Source: 2101085-04 39.5 92.7 1J / 92.7 89.8 104 95.2 101 94.4 87.0 101 85.1 4.38 90.2 110 111 Analyzed: 02/ 19 l2l 09:29 98.0 98.0 98.0 98.0 98.0 98.0 98.0 98.0 98.0 98.0 98.0 98.0 4.90 98.0 98.0 98.0 2.5 2.0 0.98 0.49 0.25 0.49 0.49 0.98 0.49 0.49 0.49 2.4 0.49 0.98 2.0 2.0 4t.9 97.7 t4s 91.9 94.2 108 99.0 106 99.5 90.7 103 ot t 4.s5 94.2 112 115 mgikC ND 3.78 38.6 0.302 ND 8.93 3.73 5.75 3.36 0.641 7.90 ND ND ND 17.6 18.1 ND 3.78 3 8.6 0.302 NT' 8.93 3.73 5.75 3.36 0.641 7.90 ND ND ND 17.6 18.1 43 96 108 100 96 101 97 103 98 92 97 93 93 96 96 99 43 96 107 100 9',1 102 99 103 99 93 100 92 95 98 t00 101 l 0-l 16 7'7-t21 30-169 86-111 81-trz 75-129 '11-t2r 68-1 35 '12-r2r 70-tt2 '73-tzt 76-116 54-t32 64-120 '78-t24 50-143 10-116 77-tzl 30-169 86-1 1 1 81- 112 75-129 71-l2t 68-135 72-t2t 70-t12 '73-t2r 76-tL6 s4-132 64-t20 '78-t24 50-143 Analyzed: 021 19/21 09:45 2.3 mC/kC 92.4 1.8 " 92.4 o.92 u 92.4 0.46 u 92.4 0.23 " 92.4 0.46 ', 92.4 0.46 ' 92.4 0.92 " 92.4 0.46 ', 92.4 0.46 ' 92.4 0.46 " 92.4 1.8 " 92.4 0.46 " 4.62 0.92 " 92.4 1.8 " 92.4 1.8 " 92.4 6 5 5 6 5 4 4 5 5 4 J 7 4 ) J 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 The results in this report apply to the samples analyzed in accordance with the chain of cwtody docamenl. This analytical report must be reprcduced in its entirety. California ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 3l of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 orcutt cA, 93457 Projecl Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2l0l07a 03101/202109:4'l Total Metals by ICP - Quality Control Analyte Result RL Units Spike Level Source Result %REC ToREC Limits RPD RPD Limit Notes Batch 8180590 - EPA 60108 Preparation: EPA 30508 02118/21 09:ll Post Spike (8180590-PS1) Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Source: 2101085-04 1.88 L99 2.80 l.96 t.92 2.t5 2.01 2.t3 2.01 1.92 2.tl 1.88 0.0924 1.93 2.28 114 Analyzed: 021 19 /21 09 :48 mglL 2.00 -0.00109 ' 2.00 0.0796 " 2.00 0.813il 2.00 0.00635 " 2.00 -0.0120 ' 2.00 0.188u 2.00 0.0785 ' 2.00 0.121. 2.00 0.0707u 2.00 0.0135 ' 2.00 0.166 ' 2.00 -0.041su 0.100 -0.00288 " 2.00 -0.0262u 2.00 0.371n , 2.00 0382 94 96 100 97 96 98 97 100 97 96 97 94 92 96 96 9',1 75-t25 75-125 75-t25 75-125 75-t25 7s-125 75-125 75-125 '15-125 75-125 75-125 75-t25 '15-125 7s-t25 75-125 '15-125 The rcults in this report apply to the samples analyzed in accordance with the chain of custody domment. This analytical reporl must be reprcduced in its entirety, California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Glient Connect: client.oec.com\repoils TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 32 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum ProjectNumber: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03l0ll202l09:47 STLC Metals by ICP - Quality Control Result RL Units Spike Level Source ToREC Result %REC Limits RPD RPD Limit Notes Batch 8180817 - STLC/EPA60108 Preparation: EPA30l0ALeachate 0212512L I'l:39 Blank (B1B0E17-BLK1) Chromium Nickel LCS (B1BO8U-BSr) Chromium Nickel LCS Dup (8180817-BSDI) Chromium Nickel Iluplicate @180817-DUP1) Chromium Nickel Leach Fluld Blank (8180817-LBK1) Chromium Nickel Leach Fluid Blank @180t17-LBK2) Chromium Nickel Leach Fluid Blank @180817-LBK3) Chromium Nickel 10.1 t0.2 Source: 2101070-01 0.434 2.62 Analy zed: 02 / 26 / 2l 12:08 mE/L Analy zed: 02 I 26 I 2l | 2:24 mglL Analyzed: 02126121 ll :57 mgll- Analyzed: 02/26121 L2:59 ND ND 9.94 9.98 ND ND ND ND ND ND 0.050 0.0s0 0.050 0.050 0.050 0.050 80-120 80-120 Analyzed: 02126121 ll :54 mglL Analy zed: 02 I 26 I 2l 12:06 mg[,i0.0 10.0 10.0 10.0 99 100 101 102 80-120 80-120 0.386 2 2 12 76 20 20 20 20 0.10 0.10 0.10 0.10 0.10 0.10 2.24 melL Ana$zed: 02/26121 13 :02 0.10 mg/|, 0.10 The results in this report apply to the samples analyzed in accordance with the chain of cltstody doatmenL This analytical report must be reprcduced in iE utire$. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 33 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2t01070 03l0ll202109:47 TCLP Metals by ICP - Quality Control Analyte Result RL Units Spike Level Source %REC Result %REC Limits RPD RPD Limit Notes Batch 8180796 - EPA 1311/EPA 60108 Preparation: EPA 3010A Leachate 02/25/21 09:L4 Blank (B1B0796-BLK1) Chromium LCS (8180796-851) Chromium LCS Dup (B180796-BSD1) Chromium Duplicate @180796-DUP1) Chromium Leach f,'luid Blank (81B0796-LBK1) Chromium Leach Fluid Blank (B180795-LBK2) Chromium Leach Fluid Blank @180796-LBK3) Chromium Matrix Spike (81B0796-MS1) Chromium Matrix Spike Dup @180796-MSDI) Chromium t0.2 10.3 Source: 2100781-02 ND ND Source: 2100781-02 10.3 Source: 2100781-02 10.0 Analyzed: 02/25/21 19:15 0.050 mglL Analyzed: 02/25 /21 18:57 0.050 mg/L 10.0 Ana$zed: 02/25 /2L 19:.00 0.050 mglL 10.0 Analy zed:. 02 / 25 / 2 I | 9 :3 I 0.050 mgT Analyzed: 02/25 121 L9:20 0.050 melL Analyzed: 02/25 I 2l 19 :02 0.050 mglL Analyzed: 02/25 I 2l 19 :23 0.050 mglL Analyzed: 02/25 l2l 19''26 0.050 mg[- 10.0 Analyzed: 02/25/21 19:28 0.050 mglL 1.0.0 ND 103 89-115 ND ND ND 102 80-120 103 80-120 100 89-1 15 0.7 20 320 20 ND ND The results in this report apply to the samples analyzed in accordance with the choin of ustody doument. This analytical tcport must be reproduced in its entirety. California ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (8OS) 9224772 wrrw.oecusa.com FAX: (805) 925-3376 Page 34 of52 Oilfield Environmental & Compliance, lnc. Pacific Peffoleum California P.O.Box2646 OrcnttCA,93457 Project: Pacific Petroleum Projeot Number: CSI Constuction Project Manager: Clarence Reynolds WO & Reported: 2t0to70 03l0ll202l09:47 Volatile Organic TPH by GC/FID - Quality Control Result RL Units Spike Level Source o/oREC Result ToREC Limits RPD RPD Limit Notes Batch B1B0591 - EPA 8015M Preparation: EPA 5035/50308 Solid GC 02ll8l2l 09.,21 Blank @180591-BLKI) TPH Gasoline (C5-Cl2) Sul ro gate : 4 - B ro mofl uom b enzene LCS (818059r-BSl) TPH Gasoline (C5-Cl2) Surro gate : 4 - B ro mofl uoro b enzene LCS Dup (8180591-BSDI) TPH Gasoline (C5-C12) Sur ro ga t e : 4 - B ro m ofl u o ro b e nz e n e Duplicate (8180591-DUPI) TPH Gasoline (C5-C12) Surrogate : 4- B ro motluo ro be nze n e Matrix Spike (81B0591-MS1) TPH Gasoline (C5-Cl2) Sur ro gat e : 4-B ro mofluorc b e nzene Matrix Spike Dup (81B0591-MSD1) TPH Gasoline (C5-C12) Sur ro gate : 4 - B romofl uoro b enzene 1.01 Source: 2101083-01 ND Source: 2101084-05 0.944 Source: 21010E4-05 1.10 Analyzed: 02/ 19 /21 10:23 0.50 mg/kg 0.106 ' 0.125 Analyzed: 02/ 19 l2l 08:52 0.50 nClkg 0.994 0.143 ', 0.124 Analyzed: 02/ 19 /21 09:20 0.50 mS&C 0.996 0.142 ', 0.12s Analyzed: 02/l9l2l l7 :15 0.50 ms/kg 0.0801 " 0.12s Analyzed: 02/20/21 00:18 0.50 mgkc 0.998 0.117 ', 0.125 Analyzed: 02120/21 00:46 0,50 mglkC 0.998 0.134 ', 0.125 ND 85 31-t68 1.13 113 ll5 62-l5l 3 1-168 102 114 64 95 94 62-t5t 31-168 10 20 15 20 ND ND ND 20 110 107 31- 168 10-166 31-I68 10-166 3 t- 168 The reults in this report apply to the samples analyzed in accordance with the chain of custody doument. This analytical report must be reproduced in its entirety. Client Connect: client.oec.com\reports TELI (805) 9224772 FAX: (805) 925-3376 California ELAP Gertificate # 2438 307 RoemerWay, Santa Maria, CA93454 www.oecusa.com Page 35 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109:47 Semi-Volatile Organic TPH by GC/FID - Quality Control Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes BatchBlB0595 -EPA8015M Preparation: EPA3550C 02/l8l2l 10:12 Blank (81B0595-BLKI) T?H Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surro gate : o-Te rp heny I LCS (B1B0s9s-BS1) TPH Diesel (C13-C22) TPH Motor Oil (C23-C4O) Surro gate : o-Terp heny I LCS Dup (8180595-BSD1) TPH Diesel (C13-C22) TPH Motor Oil (C23-C40) Sur ro gate : o-Tbrp heny I Duplicate (8180595-DUP1) TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surro gate : o -Terp heny I Matrlx Spike (8180595-MS1) TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surrogate : o -Terp he ny I Matrix Spike Dup (8180595-MSDI) TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) Surro gate : o-Terp heny I Source: 2101084-04 ND ND Source: 2101084-04 462 522 Source: 2101084-04 439 500 Analyzed: 02/ l8l2l 13 :58 10 mg/kg 50 51.0 ' s0.0 Analyzed: 02/ I 8 I 2l ll :05 10 mdke 499 50 " 499 50.1 ', 49.9 Analyzed: 021 I 8 /21 ll :20 9.9 mgkc 497 50 " 497 49.0 ' 49.7 Analyzed: 02/ I 8/ 2l l4:I3 10 mglkC 50n 50.0 " 49.9 Analy zed: 02 I I 9 I 21 09 : 5 0 9.9 mC/kC 497 50 " 497 51 .4 u 49.7 Analyzed: 02/ 18 I 2l 13 :43 10 mgkg il 50.6 85 93 r00 86 97 99 ND ND 422 46s 429 484 88 100 101 ND ND ND ND ND ND 500 500 50.0 50 102 65-133 77-lr4 '16-128 65-133 '77-tt4 76-128 6s-133 100 65-1 33 2 4 20 20 20 20 93 105 103 45-149 34-t7s 6s-133 4s-149 34-t7s 65-1 33 5 4 20 20 The results in this report apply to the samples analyed in accordance with the chain of custody docament. This analytical report mwt be rcpruduced in its enlirety. Cal ifornia ELAP Certificale # 2438 307 RoemerWay, Santa Maria, CA93454 Client Connect: client.oec.com\reports TEL. (805)9224772 www.oecusa.com FAX: (805) 925-3376 Page 36 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 031011202109:47 Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Spike Level Source Result o/oREC ToREC Limits RPD RPD Notes Limit Batch B180563 - EPA 82608 Preparation: EPA 5035/50308 MEOH O2/17 121 16:06 Blank @180563-BLKI) Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- I ,3 -Diohloropropene trans- 1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Analy zed: 02 I I 8 / 2l | 0 :03 mg&gND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.25 0.25 o.25 0,25 0.25 0.2s 0.25 0.25 0.25 o.25 0.2s 0.25 0.25 0.2s o.25 0.2s 0.25 0.2s 0.25 o.25 0.2s 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.2s 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.2s The results in this rcpofl apply lo the samples analyzed in accordance with the chain of cwtody doument. This analytical report must be rcproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\repods TEL: (805)9224772 www.oecusa.com FAX: (805) 925-3376 Page 37 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 OrcuItCA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2t0t070 031011202109:47 Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Batch 8180563 - EPA 8260B Preparation: EPA 5035/50308 MEOH 02ll7l2l 16:06 Blank (B1B0563-BLK1) Styrene l, 1, 1,2-Tetrachloroethane 1,1,2,2 -Tet achloroethane Tetrachloroethene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Surro gate : D ibru mofluoro m eth ane Surrogate: Toluene-d8 Sur ro gate : 4-B ro mofluo rc b e nzen e LCS (8180s63-BS1) Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane i,2-Dibromo-3 -chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.2s 0.25 0.25 0.2s 0.25 0.2s Analy zed; 02 / | I I 2l I 0 :03 mg/kg 0.0498 0.0498 0.0498 Analyzed: 021 | 8 l2l 09 :06 mC/kg 4.0431 0.0478 0.0484 87 96 97 '18 82 '77 't6 '75 22 95 99 93 '76 83 25 't5 80 8'l 8'7 79 't6 78 74 85 7s,122 66-128 76-1 22 75-t3t 75-r36 70-135 76-t37 55-139 10-t57 62-166 72-167 69-158 70-t40 '76-137 10-t64 7s-123 26-r46 73-t4s 6'1-tst 68-144 45-r48 '73-t34 70-t40 78-142 1.56 1.63 1.s3 t.52 r.49 0.441 1.89 i.98 1.8s t<t 1.65 0.499 t.49 1.60 r.73 t;14 1.57 1.51 i.55 1.47 1.70 0.25 0.2s 0.25 0.25 o.25 0.25 4.25 0.2s 0.25 0.25 0.2s 0.25 0.25 0.25 0.2s 0.2s 0.25 0.2s 0.2s 0.25 0.25 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 The resuhs in this report apply to the samples analyzed in accordance with the chain ofcustoily iloument. This analytical rcport must be reprodueed in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 38 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orcutt CA,93457 Projecf PacificPetroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Repoded: 2t01070 03101/2021 09l.47 Volatile Organic Compounds by GC/iVIS - Quality Control Analyte Result RL Units Spike Level Source Result %REC ToREC Limits RPD RPD Limit Notes Batch 8180563 - EPA 8260B Prqraration: EPA 5035/50308 MEOH 02/17/21 16:06 LCS (8180s63-BS1) 1 ,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifl uoromethane 1, I -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene trans' 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- 1 ,3 -Dichloropropene hans- 1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 4-Isopropyl Toluene . Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1,1,2,2 -Tetr achloroethane Tetrachloroethene (PCE) Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofluoromethane 1,2,3 -Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xyienes (total) Sur rogate : D i b ro nofluo rc me th ane Surrogate: Toluene-d8 Surrogqte : 4 -B romofluorobenzene Analyzed: 02/ 18 I 21 09:06 0.25 mg/kE 2.00 0.2s ' 2.00 0.25 " 2.00 0.25 " 2.00 0.2s ' 2.00 0.25 " 2.00 0.25 " 2.00 0.2s ' 2.00 o.25 ', 2.00 0.25 il 2.00 0.25 ' 2.00 0.2s ' 2.00 0.25 ' 2.00 0.25 " 2.00 0.2s " 2.00 0.25 " 2.00 0.2s " 2.00 0.25 ', 2.00 0.25 " 2.00 0.2s " 2.00 0.25 ', 2.00 0.25 ', 2.00 0.25 ' 2.00 0.2s " 2.00 0.25 u 2.00 0.25 " 2.00 0.2s " 2.00 0.25 u 2.00 0.25 " 2.00 0.2s . 2.00 0.25 n 2.00 0.25 " 2.00 0.25 ' 2.00 0.25 u 2.00 0.25 " 2.00 0.25 " 2.00 0.25 " 5.99 0.04s1 ' 0.0499 0.0477 ' 0.0499 0.051 5 ', 0.a499 1.75 1.68 t.76 1.61 t.52 1.66 1.s8 1.65 t.57 t.57 t.70 i.59 1.58 1.66 1.68 ) ?t 1.89 t.69 t.49 1.65 1.81 .t.57 1.65 1.5'7 r.69 1.53 1.83 1.86 1.56 1.57 1.60 1.81 1.61 1.68 t.76 l.5l 5,06 88 84 88 8l '76 83 '79 83 79 79 85 80 79 83 84 116 95 85 75 83 90 79 83 79 85 9l 93 78 78 80 91 81 84 88 76 85 90 96 103 76-r46 '72-t40 10-166 65-t39 67-125 54-168 74-135 68-149 74-130 68-130 33-187 7t-140 78-135 70-t37 69-143 69-203 74-t54 72-157 49-129 61-158 69-147 71-144 78-132 64-138 74-t48 76-t31 63-r70 7t-165 '14-t37 68-134 '19-t39 32-1s4 69-r25 6',1-144 66-r54 39-150 71-147 75-1 22 66-r 28 76-122 The results in this report apply to the samples analyzed in accordance with the chain of custody docttment. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Connect: client.oec.com\repons TELi (805) 9224772 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 Page 39 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Penoleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2l0to70 031011202109:47 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Level Source %REC Result ToREC Limits RPD RPD Limit Notes Batch 81B0563 - EPA82608 Preparation: EPA 5035/50308 MEOH 02117121 16:06 LCS Dup (8180563-BSDI) Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3 -chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane I ,1 -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene hans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1 ,1 -Dichloropropene cis- I ,3 -Dichloropropene trans- 1,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Analy zed: 02 / | 8 / 21 09 :3 5 mC/kg 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 77 81 76 75 74 )i 91 96 90 't4 81 25 IJ 82 85 86 78 '73 7'7 t3 83 86 83 87 79 76 80 '78 80 79 77 82 77 79 82 8l t12 92 82 74 84 88 1.s3 r.62 1.52 1.50 t.47 0.441 1.82 1.91 1.80 1.48 1.61 0.503 t.46 1.63 1.69 1.71 1.57 1.46 i.54 1.45 1.66 t.72 1.65 1.74 t.57 1.51 1.s9 1.56 1.60 1.57 1.55 1.63 1.s3 1.58 t.64 t.62 2.23 1.84 1.64 t.47 1.68 1.75 0.25 0.25 o.25 0.25 0.25 0.2s 0.25 0.25 0.25 o.25 0.2s 0.25 0,25 0.2s 0.25 0.25 0.25 0.2s 0.25 0.25 0.2s 0.25 o.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.2s 0.25 0.25 0.2s 0.25 0.25 0.2s 0.25 0.25 o.25 75-131 75-136 70-i35 76-137 s5-139 10-157 62-t66 72-t67 69-158 70-r40 76-t37 10-t64 75-123 26-t46 73-t45 67-l5l 68-144 45-t48 73-1,34 70-t40 78-t42 76-t46 72-t40 l0-166 65-139 6'7-t25 54-168 74-135 68-149 74-t30 68-130 33-187 7t-t40 78-135 70-t37 69-t43 69-203 74-ls4 72-r57 49-129 61-158 69-147 220 0.9 20 120 t20 t20 020 420 320 320 ?20 320 0.8 20 220 220 320 220 0.1 20 320 0.9 20 120 220 220 220 0.9 20 320 0.8 20 420 220 320 0.3 20 120 420 420 020 120 420 320 320 320 120 220 320 QM-09 QM-09 The results in this report apply to the samples analyzed in accordance with the chain of custody doilment. This analytical rcport mut be reprcduced in its entirety. California ELAP Gertificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TELi (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 40 of52 Oilfield Environmental & Compliance, lnc. Pacifi c Petroleum California P. O. Box 2646 Orctfi|CA,93457 Project: Pacific Petoleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2l0lo70 031011202109:47 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC Result ToREC Limits RPD RPD Limit Notes Level Batch 8180563 - EPA 82608 Preparation: EPA 5035/50308 MEOH 02/17121 16:06 LCS Dup (8180563-BSDI) St''!ene l, 1, 1,2-Tetrachloroethane 1,1,2,2 -Tetr achloroethane Tetrachloroethene (PCE) Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1 , 1 , 1 -Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3 -Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xyienes (total) Sur ro gate : D ib ro mofluo romethane Surrogate: Toluene-d8 . Surrogate: 4-Bromofluorobenzene Duplicate (81B0563-DUP1) Benzsne Firomobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Source: 2101070-01 Analyzed: 02 I 18 /21 09 :35 mg/kC 2.00 2.00 2.00 2.00 2.00 2.04 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 s.99 0.0499 0.0499 0.0499 Analyzed: 02/ 1 8 I 2l 12:29 mClkg 1.54 1.63 1.55 1.63 1.49 1.85 1.84 1<t 1.55 i.5s 1.85 1.60 1.64 1.70 1.53 4.92 0.25 0.25 0.25 0.25 0.25 0.25 0.25 0.2s 0.25 0.25 0.25 0.2s 0.25 0.25 0.2s 0.25 0.0449 0.0478 0.0514 220 t20 120 420 320 r20 120 220 120 320 220 0.9 20 320 320 220 320 '7',| 82 "t8 82 75 92 92 76 77 78 93 80 82 85 77 82 90 96 10i 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 7t-t44 '18-t32 64-138 74-148 76-l3t 63-t70 71-165 74-t37 68-r34 79-139 32-154 69-l2s 67-144 66-154 39-1s0 71-147 7s-1 22 66-128 76-122 QM-09 QM-09 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.2 1.2 1.2 1.2 1) 11 1.2 1.2 t', 1) t.2 It 1.2 1.2 1.2 1.2 1.2 t.2 1.2 1.2 1.2 The results in this report apply to the samples analyzed in accordance wilh the chain ofeustody document. This analytical rcport must be reproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 4l of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 OrcuftCA,93457 Project: Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109:47 Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Spike Sowce %REC Result %REC Limits RPD RPD Limit Notes Level Batch 8180563 - EPA E260B Preparation: EPA 5035/50308 MEOH 02/17/2L 16:06 Duplicate @1B0563-DUPI) 1 ,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis- 1,2-Dichloroethene trans- 1,2-Dichloroetlene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- 1,3-Dichloropropene trans- 1,3 -Dichloropropene Ethylbenzene Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Styrene 1, 1, 1,2-Tetrachloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3'Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Sur ro gate : D ib ro nofluorc methane Surrogate: Toluene-d8 Surrogate : 4- B romofluorobenzene Source: 2101070-01 Analyzed: 021 18 I 2l 12:29 mClkgND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.2 1.2 1.2 11 r.2 1.2 7.2 1.2 1.2 1.2 1.2 1.2 1.2 r.2 1.2 1.2 1.2 1.2 1.2 t.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 t', l') 1.2 1.2 1.2 t.2 r.2 t.2 1.2 t.2 0.0437 0.0477 0.0485 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 0.0498 0.0498 0.0498 88 96 97 75- I 22 66-128 76-122 The results in this repoft apply to the samples analyzed in accordance with the chain of custody docament. This analytical ,eport m6t be ,epruduced in its entirety. Client Connect: client.oec.com\reports TELi (805) 9224772 FAX: (805) 925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.eom Page 42 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petroleum Project Number: CSI Conskuction Project Manager: Clarence Reynolds WO & Reported: 2l0to70 03101/202109:47 Volatile Organic Compounds by GC/MS - Quality Control Analyte Result RL Units Spike Source %REC Result T.REC Limits RPD RPD Limit Notes Level Batch 8180563 - EPA 82608 Preparation: EPA 5035/50308 MEOH 02117121 16:06 Matrix Spike (Br80563-MS1) Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene Dibromochloromethane 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifl uoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis- 1,2-Dichloroethene trans- i,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1 -Dichloropropene cis- 1,3 -Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Hexachlorobutadiene 4-Isopropyl Toluene Isopropylbenzene Methylene chloride Naphthalene n-Propylbenzene Source: 2101070-04 8.33 8.63 8.54 8.69 8.82 8.3'7 8.47 9.46 9.r'7 8.01 8.6',7 8.67 8.14 8.31 8.66 8.s6 9.08 8.92 8.71 8.18 8.79 8.'12 8.36 6.70 8.60 8.34 8.07 8.52 8.55 8.76 8.65 8.47 8.04 8.67 9.t7 8.54 9.86 8.84 8.46 7.92 9.24 8.73 Analyzed: 02/18121 15:49 1.3 mg/kC 10.0 ND 1.3 " 10.0 ND 1.3 ' 10.0 ND 1.3 u 10.0 ND 1.3 ' 10.0 ND 1.3 - 10.0 ND 1.3 n 10.0 ND 1.3 " 10.0 ND 1.3 . 10.0 ND 1.3 ' 10.0 ND 1.3 ' 10.0 ND 1.3 ' 10.0 ND 1.3 ' 10.0 ND 1.3 " i0.0 ND i.3 u 10.0 ND 1.3 n 10.0 ND 1.3 ' 10.0 ND 1.3 ' 10.0 ND 1.3 u 10.0 ND 1.3 ' 10.0 ND 1.3 " 10.0 ND 1.3 " lq.o ND 1.3 u 10.0 ND 1.3 ' i0.0 ND 1.3 u 10.0 ND i.3 . 10.0 ND 1.3 ' 10.0 ND 1.3 " 10.0 ND r.3 " 10.0 ND 1.3 . 10.0 ND 1.3 n i0.0 ND 1.3 " i0.0 ND 1.3 ' r0.0 ND 1.3 n 10.0 ND 1.3 " 10.0 ND 1.3 " 10.0 ND 1.3 ', 10.0 ND 1.3 " 10.0 ND 1.3 " 10.0 ND 1.3 u 10.0 ND 1.3 " 10.0 ND 1.3 " 10.0 ND 83 86 85 87 88 84 85 94 92 80 86 86 81 83 86 85 9l 89 87 82 88 8',1 83 6'.1 86 83 81 85 85 87 86 85 80 86 92 85 98 88 84 79 92 87 36-t46 28-ts2 43-t46 43-t53 26-tst 10-158 10-171 t0-t76 19-i68 29-r51 3 1-15 I 13-160 M-137 10-144 24-t58 t9-160 40-1s3 21,-r64 41-r48 45-158 24-ts8 i9-r60 20-152 10-1s3 35-148 42-t32 18-t74 41-146 2'7-16l 42-l4s 42-t4t 10-166 28-isl 38-148 36-144 16-162 10-193 tl-167 13-174 30-13 I l0-178 12-160 The tcsults in this report apply to the samples analyzed in accordance with the chain of custody docament. This analytieal report must be reproduced in its entirety. California ELAP Certificate # 2438 Client Gonnect: client.oec.com\reports TELi (805) 9224772 925-3376307 Roemer Santa cA 93454 www.oecusa.com FAX: Page 43 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 93457 Project: Pacific Petoleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2loto70 O3l0l/202109:47 Volatile Organic Compounds by GC/MS - Quality Control Result RL Units Spike Level Source Result o/oREC %REC Limits RPD RPD Notes Limit Batch 8180563 - EPA 82608 Preparation: EPA 5035/50308 MEOH 02/l'll2l 16:06 Matrix Spike (B180563-MS1) Sryrene l, 1, 1,2-Tetrachloroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene (PCE) Toluene 1,2,3 -Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1, 1-Trichloroethane 1, 1,2-Trichloroethane Trichloroethene (TCE) Trichlorofl uoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride Xylenes (total) Surrogate : Dibromofluoromethane Surrogate: Toluene-d8 Sur ro gate : 4-B ro mofluo ro b e nzen e Source: 2101070-04 8.24 9.17 9.03 8.47 8.03 9.16 8.99 8,32 8.80 8.41 7.66 9.4r 8.26 8.61 8.07 25.7 Analyzed: 02/ 18 /2L 15 :49 1.3 mC/kC 10.0 1.3 ' 10.0 r.3 " 10.0 1.3 ' 10.0 1.3 " 10.0 1.3 u 10.0 1.3 u 10.0 1.3 ' i 0.0 1.3 ' 10.0 1.3 u 10.0 1.3 u 10.0 1.3 ', 10.0 1.3 ' 10.0 1.3 ', 10.0 1.3 ' 10.0 1.3 " 30.1 0.04s3 ' 0.0s01 0.0481 ' 0.0501 0,0518 ' 0.0501 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 23-160 36-1s2 19,175 23-162 26-ls2 10-168 10-170 36-150 25-r79 29-167 15-156 26-177 1,4-15'1 10-167 l4-154 21-162 7s-122 66-128 76-122 82 92 90 85 80 91 90 83 88 84 76 94 82 86 81 85 90 96 10i The rcsults in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 Client Connect: client.oec.com\reports TEL: (805) 9224772 www.oecusa.com FAX: (805) 925-3376 Page 44 of 52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 9345? Project Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2tot070 03l0ll2021O9:47 Sample Method Summary Analysis Method Matrix Lrborator? & Certifi cation Semi-Volatile Organic TPH by GC/I'ID 8015 Diesel & Motor Oi1 List EPA 8015M 8015 Diesel & Motor Oi1 List EPA 8015M 8015 Diesel & Motor Oil List EPA 8015M 8015 Dieset & Motor Oil List EPA 8015M 8015 Diesel & Motor Oi1 List EPA 8015M 8015 Diesel & Motor Oii List EPA 8015M 8015 Diesel & Motor Oil List EPA 8015M 8015 Diesel & Motor Oil List EPA 8015M Solid Solid Solid Solid Solid Solid Solid Solid OEC, Intemal OEC, CA-ELAP OEC, Intemal OEC, CA-ELAP OEC, Internal OEC, CA-ELAP OEC, Intemal OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP OEC, Internal OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP STLC Metals by ICP 60108 STLC Chromium 60108 STLC Nickel STLC Metals Extraction STLC Metals Extraction TCLPMetals by tCP 60108 TCLP Ckomium TCLP Metals Extraction TCLP Metals Exhaction Total Metals by CVAA Mercury Total EPA 7471A STLC/EPA60IOB STLC/EPA60IOB STLC EPA 131I/EPA60108 EPA 13II Water Water Solid Water Solid SolidEPA7477A. The results in this report apply to the samples analyzed in accordance wilh the chain of custody doc,umenL This analytical report must be repruduced in its entirety' Client Connect: client.oec.com\reports TELi (805) 9224772 FAX: (805) 925-3376 California ELAP Certificale # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com Page 45 of52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum Califomia P. O. Box 2646 Orcutt CA, 93457 Project PacificPetroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 031011202109:47 Sample Method Summary (Continued) lnalysis Method Matrix Laboratory & Certilication Total Metals by ICP 6010B Total Antimony 6010B TotalArsenic 60108 Total Barium 6010B Total Beryllium 6010B Total Cadmium 60108 Total Chromium 6010B Total Cobalt 60108 Total Copper 60108 Total Lead 60108 Total Molybdenum 60108 Total Nickel 60108 Total Selenium 60108 Total Silver 6010B Total Thallium 60108 Total Vanadium 60i0B Total Zinc Volatile Organic TPH by GC/T'ID 8015 TPH-Gasoline 8015 TPH-Gasoline 80i5 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline 8015 TPH-Gasoline EPA 601OB EPA 60108 EPA 60108 EPA 60lOB EPA60lOB EPA 60108 EPA 6010B EPA60108 EPA60108 EPA 60108 EPA 601OB EPA60lOB EPA 60lOB EPA 60lOB EPA 60108 EPA60lOB OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP OEC, CA.ELAP OEC, CA.ELAP OEC, CA-ELAP OEC, CA-ELA? OEC, CA.ELAP OEC, CA-ELAP OEC, CA.ELAP OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP OEC, CA-ELAP Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Volatile Organic Compounds by GCIIVIS 82608 Full List EPA8260B Solid EPA 8015M EPA 8015M EPA 8015M EPA 8015M EPA 8015M EPA 8015M EPA 8015M EPA 8015M Solid Solid Solid Solid Solid Solid Solid Solid OEC, CA.ELAP OEC, Intemal OEC, CA-ELAP OEC, Internal OEC, CA.ELAP OEC, Intemal OEC, CA-ELAP OEC, Intemal OEC, CA.ELAP The results in this report apply to the samples analyzed in nccordance with lhe chain of custody domment. This analyticdl report must be reprcdueed in its atirety. California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 TEL: (805) 9224772 FAX: (805) 925-3376 Client Connect: client.oec.com\reports www.oecusa.com Page 46 of 52 Oilfield Environmental & Compliance, lnc. Pacific Petroleum California P. O. Box 2646 Orcutt CA, 93457 Project Pacific Petroleum Project Number: CSI Construction Project Manager: Clarence Reynolds WO & Reported: 2101070 03101/202109.47 Notes and Definitions Quallller Definition Method Detection Limit Reponing Limit (Quantitation Limit) Analyte NOT DETECTED at or above the method limit (MDL) Relative Percent Difference The heavy oil range organics present are due to hydrocarbons eluting primarily in the diesel range. The concenfation indicated for this analyte is an estimated value above the calibration range ofthe instrument. This value is considered an estimate (CLP E-flag). Analyte concentration below TTLC but above 10x STLC. Analyte concentration above 20x TCLP. The spike recovery was outside acceptance limits for the LCSD. The batch was accepted based on acceptable LCS recovery. The RPD exceeded t}te QC control limits. Reporting limits are at or below state/federal hazardous waste criteria limits, Temperatffe [Out-Acceptable] Direct from Field MDL RL ND RPD D-07 E N-02 N-03 QM-09 QR-04 R-07 TMP3 The resuhs in this report apply to the samples analyzed in accordancewith the chain ofcustoily dommeni Ihis analytical report mwt be reprcduced in its entirety. Client Connect: client.oec.com\reports TEL:' (805) 9224772 FAX: (805) 925-3376 California ELAP Certificate # 2438 307 Roemer Way, Santa Maria, CA 93454 www.oecusa.com Page 47 of52 -E ale :Operator :Acquired :Instrment : Sample Name: Misc Info : Via]- Nunber: C : \HPCHBM\1\DATA\FEB2 L\02 1I2 1\A0MB1I34. D ,f,rH 18 Feb 2021- 5:13 pm using AcqMethod MACH1-2.M GC #1 2l-01070-01GB1B059s (S) 1A 31 AOMB1E34.D\FID1A File : C:\HPCHEM\1\DArA\2021\FEB21\021921\DOMB1906.DOperator : RWSAcquired : 19 Eeb 2021" 10:23 am usingt AcqMethod GAS-BTEX.M Instrument i GC4 Sample Nane: 2L01070-01@ Misc lnfo : 1@8180591 GRO SOLIDViaf Number: 6 Fife : c:\HPCHEM\1\DATA\FEB21\02r821\A0MB1835.DOperator : JJHAcquired | 18 Eeb 2021 5:28 pm using AcqMethod MACH1-2.M Instrument ; GC #1 Sample Name : 2101070-02@B1B0595 (S) Misc lnfo : 1@Vial Number: 32 AOMB,I835.O\FID1A Fil-e : C:\HPCHEM\1\DATA\2021\FEB21\021921\DoMB1907.DOperator : RWSAcquired : L9 Eeb 2021 10:55 am using AcqMethod GAS-BTEX.M Instrument : GC4 Sample Name: 2101070-02@1:10 PREP Misc fnfo : 1GB1B0591 GRo SoLIDvial- Nunber: 7 11 File Operator Acquired Instrument C : \EPCHEM\ 1 \DATA\FEB2 1.\02 1 82 1 \AOMB1 8 3 6. D J'JH LB Feb 2021 5:42 pm using AcqMethod MACH1-2.M GC #1 Sample Name: 2101070-0308180595 (S) Misc Info : 1GVial Number: 33 - notttslsS6-D\Fto-1A - File : c:\HPCHEM\1\DATA\2021\FEB21\02192L\DOMB1908.D Operator : RWS Acquired z L9 Eeb 2021 1l:23 am using AcqMethod GAS-BTEX.M Instniment : GC4 Sampl-e Name: 2101070-03@L:10 PREP Misc Info : 1GB1B0591" GRO SOIID ViaL Nunber: 8 DOMBI9OS.D\FIDlA 11 Time Fi]-e : c:\HpcHEM\1\DATA\FEB21\021"821\AOMBI837.DOperato! : ,J,tH Acquired : 18 Feb 2021 5:56 pm using AcqMethod MACHL-2.M Instrument : GC #L Sample Name : 2101-070-040B1B0595 (S) Misc Info : 1GVial Number: 34 - __ Aotr,lelgaz.otrtotA File : C:\r{pcHEM\l\DATA\2021\FEB21\021921\DOMBL909.DOperator : RWSAcquired '. L9 Eeb 2021 11:51- am using AcqMethod GAS-BTEX.MInstrment : GCA sample Name: 2101-070-04G1:10 PREP Misc Info : 1@8180591 GRO SOLIDVial Nunber: 9 File Operator Acquired fnstniment Samp.le Name Misc Info Via]- Nunber : \HPCHEM\ 1\DATA\FEB2 ].\02 192 1\AOMB19O8 . D ,fH 9 Eeb 202L 9:11 am using AcqMethod MActl1-2.M cc #L L0L070-05RE1@B180595 (S) G c 'J 1 ) 6 Fil-e : c:\IIPCHEM\1\DATA\2021\FEB21\021921\DoMB1912.DOperator : RwSAcquired I 19 Eeb 202L L:17 pm using AcqMethod GAS-BTEX.M Instrument : GC4 Sample Name: 2101-070-05@1:10 PREP Misc Info : 1@8180591 GRO SOLIDViaI Nurnber: 12 DOMB19.I2.D\FID.IA Ibe FilE : C:\HPCHEM\].\DATA\FEB21\021821\AOMB1838.DOperator : ,J'JH Acquired : 18 Feb 2021 6:10 pm using AcqMethod MACH1-2.M Instnment : GC #1 Sampl-e Name : 2101070-06e8180595 (S) Misc Info : 10Vial Nuftdcer: 35 AOMBl 838.D\FIDlA FiIe : C:\HPCHEM\1\DATA\2021\FEB21\021921\DOMB1910.DOperator : RWSAcquired : 19 Feb 2021- 12:20 pm using AcqMethod GAS-BTEX.M Instrument : GC4 Sample Name: 2101070-06G1:10 PREP Misc Info : 1@8180591 GRO soLID Vial- Number: 10 File : c:\HPCHEM\1\DATA\FEB21\021821\A0MBI840.DOperator : JJHAcquired : 18 Feb 2021- 6:38 pm using AcqMethod MACH1-2.M Instrument : GC *1 Sample Name : 2101070-07@8180595 (S) Misc Info : 1@ Via-I Number: 37 A0MB184o.D\AD1A -- File : C:\HPCHEM\1\DATA\2021\FEB21\02L921\DOMB1911.DOperator : RWSAcquired : 19 Feb 2021 12:48 pm using AcqMethod GAS-BTBX.M fnstrument : GC4 Sample Name: 2101070-07G1 : 10 PREP Misc rnfo : 1@8180591 GRO sollD Vial- Nunlcer: 11 Company: Pacific Petroleum Californla, Inc.Name: Street Address: PO Box 2646 Sile:,-a Citv:Orcutl Strt€: CA citv.strre: Se-fJ,1:r4 7sl 4S Tclelhone: (E05)925-194?Fax: (805) 925-0884 OC Datn Level: Report To: Chrcncc Reynolds Authorized By: 1 Emril To:C.ReYnoHe@oocinc.biz CC:John@oocinc-bi!R€au€sted Anrlv3es Tumaround flme ITATI D slsnd..d [-l 5 wo.k D.ys O t wor.oaya l-l 2 work Davr E 2-8 liouc n ASAP !!. ! F J E o 3c 6E ao a t otoo 4!F o qo a o! o 8i:< t: !oo !:9€ OEa' F :ommenta: Run Blo!r!.y ITTPH > 1% 3?LC'TCLP Ar nod.d to. {rzdoui ChirlllcrtlonLeb Samplo lO DatetTlme Sampled Matrix Numbor ot Contaln6ra Cllent Sampls lD o\2.tz.rtln2n s.ilN ttntt X x X o?"c.tt.tl ltt 27 '\hly' t^l-.t/x V Y hZ 111^2t ll!2u (S tr l^\^l(x Y Y c\uvl a.r7.1lli|^L s I SIJ t^J,.lt x X V ab 1.t1-?1 I tl ?.\I A.,hl L-L Sdko""t x (K 2.t1,at liluA l {3F t^l,LRal(,:*t \/Y X o:Lt->-tt I u4S \S^il P: le /o,n.^s.te x X X Rocolvsd Deto Tlme:23v Recelved Date Date:Data:Tlme: lv6,e samplos r€caived in good condition? Yes on 16?Yos No Pacific ;nr-* fftitgF#T P.0. Box 2646 Santa Maria, CA 93454 Phone: (805) 925-1947 Fax: {805) 925-0884 &lc10l o SPECIAL INSTRUCTIONS: omNil coc copy to e.rynoldr@ppcinc'biz CHAIN.OF-CUSTODY li b Rcvis, Page .18 of 52 a@ Sample Receipt w6qtuR6tu{&a@ Work Ordgr Clisnt Name Tomp'C R€frig€Etor(s) Pacific Potrol6um Callfonia 11.€8,voai Rdd M,@. @.dcb!'c(tua*ld{ Sample Transport C oECcourler/S6mpler n After Houm Drcp Ofi gDeliv€ry (Othsr lhan OEC) O Shipment Cari6r Custody Seals g None Pres€nt 2117t2021 Coole(s) Sampls(s) C Pr€ssnt, lntact D Pressnt, Not lntact D Presenl lntact a Pressnt, Not htact C None I None Complet€d COCS Received with Sample(s) conect Conlainsr(s) Pr€soruo for Analysis Container(s) lntact and Good Condiiion Contalner Label(s) Conslstsnt with COC OEC Preservation Add€d"' Sample Quantity Sufiicont 2101070_rec6ipt COC Rsc€ived Login Yes No N/A galguqU VJ l]g ?{l Tg Condition/Pr€servatlon Received On lce Wilhln Range (Accepiabls) Rscsived Outside Rangs(Acc6ptable) Dlrsct from Fiold on lco Amblent: Alr or Filter Matrix R€csivsd Ambisnt, Placed on lce Samp16 Tompsraturg AcGtable for Analysis Recelved Outside Range lExceptlonl' lnsufriclsnt lcs or Unknown Excsssivg Frse Liquid g C f ir =C x Page 49 of 52 sample,osc.com/indox.php a2l9 /2A2a / 2o2a 2t't7t202'l Gontainers, COC Changes, And/Or Corrections 2l01o7o_recsipt D (COCI Contain6r Description llHo'"llrtratrix Prsservalive pH/Chlorin€ /Sulfur Commenls 1A 'l602 Glass WM llFridoe8-Walkln llsolid c1B J2A 1602 Glass WM llFridqe6-walk-ln llsolid t2B 20mL VOA llFr€szsr-VOA1 llsolid l602 Glass WM llFrido€8-walk-ln llsolid 13B l0mL VOA llFreszor-VOAI llSolid t4A l602 Glass WM llFridoe8-walk-ln llsolid 4B l0mL VOA llFreezer-VOAI llSolid l5A l602 Glass WM llFridseS-Walk-ln llsolid t5B l0mL VOA llFreezer-VoA1 llSolid t6A l602 Glass WM llsolid B lomL VOA llFreszsr-VOA1 llSolid ,74 l602 Glass WM llFridsoS-walkln llsolld '78 ZomL VoA llFre€z€r-voA1 llSolid Rec€ipt Login By: FaollrzrlrAA L Pqge 50 of52 sampla.oec.com/index.php Company: Pscitic Petroleum Californir, lnc. Street Address: PO Box 2646 Site:,./. city:OrcItt Stste: CA Citv.statei s<-o , c-A 73?os Telephone: (805)925-1947 Fox: (805) 9210884 OC Dala Level: Report To: Clrrencc Reynolds Aulhorircd Bv: 1 omail To: C.Rsvnolds@oocinc.biz CC:John@oocine.biz Reouestcd Anrlvses fumaround Ilme fiAn n suncert fl 5 Wort Dey!R 1 Wor* Days 2 Wo.* Day3 ll z+ souo fl ASAP !t I ! F o t.6E 3a G : otoo 4:F o oo ! oSiE tsoo 2 6Ei' F Comments: 'Run Blorlley ITTPH > 1% '9TLC'TCLP Ar n..drd tor ,lrzrrdour Claralllcrtlon Ac.l( foL YA-t' Lab Sample lO Dats/Tlms Samplod Matrlx l,lumber of ContalneF Cliont Sample lD o\).tz,rtln2n s.ilu.] w., tt X X X 48hr TAT per (>?.c,tz.:lltraQ \hly' t^l-.tt x V )( emalt AStt z/1 hz .ta^2tlt!2u (I S tr l^\^l{x Y 0.-t t.n.tllrtu^s I SIJ t^J, lt x x v a5 1.t1-i\ l tl *\I Ai d T;-f B"lto'"t x (X 0[t.t-t..rtlttuz \I SF -f:^h*Ralta,*t v v X l 1.t1-^t Lt45 a,)S^i{ P: Ie l^,"r-ns.le k X X Recelvod 23'l Rocelved Data:Tlm.; Rellnqubhad By:Drto:Tlmo:Rocelvod By Lab:Date:llm6: on lm? [] Yes No T6mp' :.:.: De€.: r: :::.:: _i:.: : Pacific ilrru HlftgF#T P.0. Box 2646 Santa Mada, CA 93454 Phone: (805) 925-1947 Fax (805) 925-0884 &t0101 o a CHAIN.OF.CUSTODY li b Rdi!' Page 5l of 52 ient SPECIAL INSTRUCTIONS: small coc copy to c.rcynold!@ppcinc.bl2 Pacific nlls* *lftgr#r P.O. Box 2646 Santa Maria, CA 93454 Phone: (805) 925-1947 Fax: (805) 925-0884 101 o CHAIN.OF.CUSTODY ll t Rcvis, Page 52 of52 nt t21 SPECIAL INSTRUCTIONS: 6meil coc copy to c.roynolds@ppcinc.bit , Comnlnv: Prcific Petroleum Crlifornir, Inc,Namc: Street Address: PO Box 2646 site: 7t> F F-^&l Citv:Orcutt Strt€: CA citv.State: Sac , z:tr 7Slof Teleohone: {80S)925-1947 Frx:1805) 925-0884 0C Dals L€vel: AulhoriredRcDorl To: Clerence Revnolds X erlrlerl tltll)it1 l\nl SEmail To: e8lyrgtsE@ppsrr1s.biz CC:John@DDcinc.biz R€ouesl€d AnNlvses Hou6 ASAP nx Dfl 2-ATumaround Tims ITAT) D shndard ll 5 work Day3 I Work Oayt 2 Work Deyg !t T EF J o s oi z6 G * oIoo L tF 0 oo g I!cI oSRi)< : ts O 2 6ft' 3omments: Run Blo.r!.y lflPH > l% SILCnCLPAT nxded tot Lab Sampls lD Date/Time Samplod Matrix l{umbor of Contaln6rs Cllent Sample lD r]rf (CJ\).t-z ctltt2A \t AIN ul., tt X X X X S'I ;LP C STI lNi 48hr TAT per arft(Y XS-;LP (.. STI cNi email ADtrr z/ Io7-t-t-7.>llti22 "\I ^lF til,J/ LC/T )LP (r, ST cNi()'1 .t72llll24 q I S F' l^t--tt X Y X XS' LC/Te.n.t lltt;r s SIJ r^J-. lt x X Y XS )LP (r, ST cNinu iltl T^^L Bnlfna Y {Xa5t.t't,tll tl *,\ XVht2 t1.il I |.tA ,)SF- T,^L'RnlJo,*',\/Y 'r.t1.1, l,)4,i \I S^:I P, l. ln-^ns te X X X XS LCC rme,\y'39 Time:Dete:Tlma: Dats: Date: Recoived Rocelvsd Rellnoulshad Av:Dato:Tlme:Data:Tlme: rB€ivod in on lm?Yes Nomndilion? Yes D No T6rnp" l 4, Wrrlo Tracklng Number ,rllr-.rf-,'i--rir ' 2 Page 1 ol 3. Emergency Response Phone .,.: ir ._,,.{ l,jl NON.HAZARDOUS WASTE MANIFEST 1 Ganeralor l0 Number 5 Gensralofr Name and Marl:ng Add.ess Gensralor's Sile Addrssg {il diftsrenl lhsn msilh! addrs$s} 6, lraflsporlor 'l Crrnpany Name L ..ilg':, 1 1'J,4.: i .i 7 Transpoder 2 Company Nems g.0o6ignated Facilily Namr and Sile Addrgss f :.it)::i : r: Numb6r Fii,iR,' tr"!fr:,.11,i!i rj.i tll. l0 Numbor liii'iftI r] 1:ti. li,ji; ,: , 'ij,i'taf\r.r i,.lti..lil"i Il 1.,.:lt'l;)ir,f) 1,,; lirl,}l'; | '.; :,r,,,1r.:t-rr,,,,t1. " .) " . i.t i;,dt,tii i':'.ir,iij ri4tli.f,, ( !. 'l'.:r',,1i ,,''.-. 1'.,,;i|:i :-ii','l , jri :l.,liti 'illlri'0, a-. i]-l,i[r{:: { l';. '10. ConlahorS 't1. Total ,oqanllty 12, Unil wt,rvol.No.rypa L Waste Shipping NaDe and D6scripti0& iill':]i1. I I a-'il'll , -'.,:.fi:i):ri:-.i ,,:. .]i;: lt -'i,it ,;til-:;il ,r.\,f:ii ,../il!-i i1,;1ilii..i- ," r -1, ,ll 2 3 4. t3. Spscial Handllng hslnclions and Addllion€l hlormalion 'rr,r;.,. i? r,i i. ,11:;:Jii,fft1.f[ r,Fi : t.i,.)t. ,::1r;ra.:!'itlr't,r'-,:'l:-qGf'\r\l:';f: l{ !i1'- . .l;1. 1,rd 14, GENERAToR'8/oFFERo8'S CERfIRCATIoN: I h0r6by dscla,e that ths contsnls 0l mark8d and labrledplacadod, and srg in all rsspecls ln pr0p6r condlllon l0r transport nam€, ard aro cl&soilisd, packag6d, -t(".t--:. -( Monlh Day Ysa, r,,'ll)r-.--r i*I i.,\,r g, oF tlrlz UIg Lz I tmpon ro u,s."II lExoortfromUs.\Porl ol Bntry/irll: lrnnsnorlar Slonelure ffor erDods onlvl:Dat€ l6avlno U.S.r ItS. lntorhattonal 16. Transportor Acknolrlsdgrnonl 0t Hsc€ipl ol Matorlals 9ay it, Month YgarNams r:-"Jt*' e ru Goo- ah2 trt- T.snsportsr 2 Firled/fyped Nams Month Day Y6gt 17.oiscrepaficy X nesioue Manlloil Relsronca Numbsr: t7a. Oimrepancy indicalior Spaca Full RsleclionPadlal Rol€clionnt0usnlilyType U.S. EPA l0 Numbsr'17b. All6mal0 facllily {or Gsneralor) Fecilily's Phons l7s. Sig0stur€ 0f Allernat6 Facilily {0r Ge'l€ralor} 't f\4 { Monlh 9ay Yoar Ff,6f E 2 fi t Yost .i lh6 msnilgsl18,Facilily Ownor or a8 n0t6d io llsm 17aCortiflcalion ol rocaipl of mei6dale c0vsr6d Pinlodffyp€d Ncmo f[ll.\i\f.ri!]r )t:.1 i:.: . I169'BLC-O 5 11977 {Fev.9/09) i&'orld 0il Rccvcline f{J0(} N Alar,ieda Street Compton. CA90222 I{auler: PACIFIC PETROLEUM CO Truck: 480 Trailer: Driver: RENE Customer: PACIFIC PETROLEUM CORP - PAC004 Product: OILYWATER Load Gallons: 1,550 Lnh lnnh,tit 'l'icket: 336ti52 l)ate. 2,'i 1 i2021 Time: l6:32:05 - 20:09:04 Barrels: Gross: 475?A Tare: 28580 Net: I8940 Tons: 9.47 54.14 Wash Out: Cold Gallons; 150 Minutes: 45 lb In Scale DK S( lb Out Scale DK S( lb 2274 t 23 PC) Tank: Tank 2: Category: Profile: W/P: 2A02 NA c-l 478850 Yes BS&W: Cravity: pH: 98.00 10.00 7.00 API Temp: Sedirnent: Flash Point: 60.00 Halides: <100 1.00 Actual llalides: 00.00 Comment: HOTWASHOKPERCLARENCE Deputy Weighmasler In: Daniel Pool Deputy Weighmaster Out: John Santiago Manifest/BOL n7 NHPPC2O2IOOO WEIGHMASTER CERTIFICATE rer:rtgnizert authority of accumey, as prcscribed hy Chapter 7 (cnmmencing witlr Seclion 12700) of Division 5 of the Calilbmia Busincss and Pmf essions Cude. adtninisleretl h1, the Division of Measuremenl Standaftls of lhe Crlilbnia Dcparlrn('rrl rl'ltood and Agriculturc. I DeMenno Kerdoon dba World Oil Recycling 9302 Garfield Avenue South Gate CA 90280 il\wOICE PACIFIC PETROLEUM CORP. PACOO4 ATTN: ACCOUNT MANAGER P. O. BOX 2e$ oRcuTT cA s3457 E*nail lnv.: r-vrrqag@pnclnc.bh Filt I lil lnvoice f: Datsl PO *: lorms: Due Dala: Quotc # ; Order # : Salospe'3on i B.lch : t400-00080713 v2312A21 Net 30 3t2512021 s40&0008073& Jerry Ratajesak Qurntity unif Pricc AmountUOI\,,l Dr:rcrt;:tron $0.35 t7e5,s02,274 GAL C1 WATER NON HAZARDOUS 338852 2t17t2Q21 23 GAL SOLIDSSURCHARGE-NONHAZ $1.65 $37.S5 8:}3.85 FA 16% ENVIRONMENTAL SURCHARGE s0.16 $133.42 ,I EA COLD TRUCK WASHOUT FEE 336852 2t17t2A2'l $300.00 t300.00 Subrot l TaxTotal 81,267.27 s0.00 llantfast #: I oate NH-PPC20210'0117 CSI CONSTRUOTION 2117t20?1 REMIT PAYMENT TO: P.O. BOX 843912, LOS ANGELES, CA 90084-3012 Tola $1.2.67.27 For your convenience, we now accept Visa, MasterCard, American Express and Discover! To make credit card payments please contact the Credit Department at (562) 231-1550. Far all other billing questians please call (310) 886-3400. THANKYOU FOR YOUR BUSINESS Page'1 ol 1 ":l Rq tttu /Csf 7 rt',lh, ricket#9J211 SLe/ Bedford Enterprises, lnc P,O. Box 5875 Santa Maria CA, 93456 {805) 922-4e77 RC/PR15183S.001 .JYEIGH'M45IER CER TiFITNI€ tHts lS i{l qtRlFr f$ lhe folls$n{l (ierrll:-{l 4nrnodl'.' da', ve$|K,. f 4ei$/ed. dr ( ru'{gl ft l wa0tr'.i6ter. *lu,e dr.d1'}rt 't {({u&y. 4 trt:mx4 by c,1&{e, 7 'f r)r'rnftrr,rt irh strDtr, llTqs} .rl thrtr)'r 5 ., tE ad{tr*r EurlEs .ttill,trletars Cc,tlt -sLlrlrCe rsrj ijt tlr lli4sar ul lv{E dilir08'! :lld LldrJ! .'t dleI llrqri6 Depitriqrt of Frld llrl,l4llrdk,t glt-i.C,FlAtE iadratlll{Iarirtt€hitrr i} wIrI ,rErrrsff,t;{r!p,0ltlrernal€il.{ '.tsbLnL,H,l.ere'rr r"lr'fr€ll;,rdlb7il, lscq!.rl urLt|ttrfidl(ltli<4 l0rt&ilrfi't lvt+lj/' tt. t' E\t I r€i .a iJ, c' r,hr' tde l0 BF f or J Er'le4nrrej ln( li0f0 HttFlrtLEiS AcfiE€hf€ilt |, (il!rrri:,.b!'r ls S€ lRris'lrrl u it.*' Afitfii €rdErlrlsri, lft !rnrfl,$e!, I lEtt:'y relp-se nnJ irreer d,{lh$ Beals{l er'tap$rr. lr{ ,19 4r€rnlEr, sldrelltlrldr!. 6if,{essr3. asgrr! -r"I.lotaE$, rur .dfildl*i fd "dl clflr'r. d3r,{eB, .l6nail! ar,lll,aarlrlx dlh ,nfdl lr} rry' l€r}ln.+ 1ri!. rlh,hJ Jtdh qr u.)!cfy dln.Ue U' rt l r' !y irdlff . r r.tl! O r'd,0L4 lrnnl Jly rrlrlle .,3',irp ,..ilifcl .lrri q Utctdq irul ur{Ml{,rJ 'hle Fe'erlt.)n BeillTrl L rErl,r,€r ,ri F,ir,.,r j :..,' |,cL..llrtgi+,,ird"et,6',-rIP*'.lutJE 'e'yarc,,r ' tLltl .r rq Er t) r) f'rrrly' ar,J Lla d 8e{{U(t E,'tfrf,rbei. lr,. Idrr ni] ig.tillt dl lrlr:,(l.irn,i,,g!. Ilelrdrrdt.drLlrdl.ltEghrIrIb{)fttlD lr Jt'9crutrrluy ll,ts5 ,.iei*, u Fops:ty dalage E t € crEI c#a(l o, r'y rEglgetre As hrrcr ' :ntrl4rdt6n ol the racJrc l€rFrr I lgpuy crtlsgly dl€ dl r{rl,; Lrd' tellsrt 154? d UreClrlCo{b taCdaarila{hth Fosdet ctuL c(nE oF cAl]Fo*lllA. 5Ec rlcfi I !rl?. i. if Ea,'elease dcee (lDr erhhl lD {h|tr {l4h lhd lr€{ilu ihes tDl t'a$, o. .esot.L i ) P'rt n h6 rdol a lt€ llne d a\xr.lq llle r€aedle slith rl lutur, b/ hrt r"n!l !lt ttrlStidl/.rltgla{l nt! ;elltDrgr{ wrli orc.leltfr Purchas€d From: Pacif c Pstroleum Co. (PFC} Carrier: Pscific Petroleum Co. (PPC) ln Date: U7|2AU 1:07:21 PM Contractr 30S- Scrap metalPd 1030 Vehicle lD:48798X1 lrailer. Tniler: Shpmnt matlrial YiMS *1 Uhprepared BuYet: Bedford Enterprices, lnc Orgin: Ean Luis Obispo Out Dat6: 211712Q21 l:20:36 PM Blt*: Sealf: Markf: Weight: - Pounds 24420 27729 700 Totals 700 &*+ Deputy Slgnature Adrian t.l*utrJ"'lS liaitrty Driver $ignalure iitr {)r;rl1'' [t.10 Juan Baz 'a