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HomeMy WebLinkAbout539 Marsh Docs_RedactedI I I I I I I county of {)n Luis obispo crtv.a san uts oB,tspo reEnvironmental Health Services (805) 781-5544 P.O. Box 1489 2156 Sierra Way San Luis Obispo, CA 93406 Fire Department (805) 781-7380 2160 Santa Barbara Avenue San Luis Obispo OA 93401'5240 CERTIFIED UNIFIED PROGRAM AGENCY (CUPA) i HAZARDOUS MATERIALS INSPECTION FORM BPOl BPO2 BPO3 TROl TRO2 EROl ATOl ATO2 EFW data entry by: IEi\Date: COMMENTS NOn cos N/A trtr BUSINESS PIAN Business plan is complete, current, & available during inspection (IISC 25503.5, Tide 19 CCR2729) Inventory of hazardous materials is complete (HSC 25504' Title 19 CCR2729) Site layout/facility maps are accurate (HSC 25504' Title 19 CCR2729) TRAININGPLAN Facility has appropriate training program (Titte 19 CCR2732 &22 CCR66265.16) Training documentation is maintained on site for current personnel (Titte 19 CCR2732 & 22 CCR 6626s.16) EMERGENCY RESPONSE PLAN Contingency plan is complete, updated, and maintained on site (HSC 25504, Title 19 CCR273I & 22 CCR S 6626s.s3ts4) /' Facility is operated and maintained to prevent/minimize/mitigate {ire, explosion, or release of hazardous materials/waste constituents to the environment. Maintains all required or appropriate equipment including an alarm and communications system (Title 19 CCR 2731 & 22 CCR 66265.31' , .43) ABOVEGROUND PETROLEUM STORAGE TANK ACT SPCC PIan is reviewed and certified by a registered engineer within last 5 yrs. (40 CFR f 12.5(b)) SPCC Ptan is maintained on site or nearest field office. (HSC 25270) to obtain forms to)l comply with BP01-8P03,I andEROI GPS Coordinates: Latitude: -deg min-decimal min Longitude: INSPECTOR:F'ACILITYREP: trnu nuI n n"-ntr E tr u nn httpGo to I FACILITY ,yAD t, Action Gode: 32 37 _33 -31 Routine Complaint Result Gode: _70 PHONE:f AGENCY ! EHS !.AG DEPr F crrY FIRE n Hw Generafor I usr n rer ncnunnpI Business PlanPROGRAMS INSPECTED: J Llcnunp rI Business Plan E xw Generator ! usr E ecrREINSPECTION REQUIRED;! YESE(o PERMISSION TO INSPECT: tnspections may involve obtaining photographs, reviewing and copying records, and Cetermininq compliance with adopted codes. GRANTED BY (NAME/TITLE): 4,try"f lil,fif bf S /rw'r mln County of San Luis ObisPo oI lur s oBtspo rlClty saJlEnvironmental Health Services (805) 781-5544 P.O. Box'1489 2156 Sierra Way San Luis Obispo, CA 93406 CERTIFIED UNIFIED PROGRAM AGENCY (CUPA) HAZARDOUS MATERIALS INSPECTION FORM Fire Department (805) 781-7380 2160 Santa Barbara Avenue San Luis Obispo CA 93401-5240 FACILITY REP: EFW data entry by: D,.u"i,: ' I.ir,i Time: YES INSPECTOR: ,t i. ,'t' ,.' : i... NOtrtrn T!n nn ! n tr n !n N/Ann costrtrn nn BPOl BPO2 BPO3 TROl TRO2 EROI ERO2 ATOl ATO2 BUSINESS PLAN Business plan is complete, current, & available during inspection (HSC 25503.5, Title 19 CCR2729) Inventory of hazardous materials is complete (HSC 25504, Title 19 CCR2729) Site layout/facility maps are accurate (HSC 25504' Title 19 CCR2729) TRAINING PLAN Facilify has appropriate training program (Title 19 ccR2732 &22 CCF{66265.16) Training documentation is maintained on site for current personnel (Title 19 CCR2732 & 22 CCR 6626s.16\ EMERGENCY RESPONSE PLAN Contingency plan is complete, updated, and maintained on site (HSC 25504, Title 19 CCR273L &22 ccR s 6626s.s31s4') Facility is operated and maintained to prevent/minimize/mitigate fire, explosion, or release of hazardous materials/waste constituents to the environment. Maintains all required or appropriate equipment including an alarm and communications system (Title 19 CCR273I & 22 CCR 6626531- .43) ABO\'EGROUND PETROLEUM STORAGE TANK ACT SpCC Plan is reviewed and certified by a registered engineer within last 5 yrs. (40 CFR 112'5(b)) SPCC Plan is maintained on site or nearest field office. (HSC 25270) to obtain forms comply with BP01-BP03, TR01 and ER01 decimal min Longitude:-deg -min-decimal min nn Go to http GPS Coordinates Latitude: _deg !,f ' / :. :..', i,i,r,.:!,,1' ,,,tii , ,','' ,,ii '.,".' ..1'',,' FACIL AME:!i ADDRESS:i..l Reinspe on ri: 31 Routine AGENCYn EHS T NC DEPT N C|TY FIRE PHONE: Icnmnen usr n ncrE Business Plan I HW GeneratorPROGRAMS INSPEGTED: n ncr Icnmae! HW Generator [] usrI Business Plann NO IYESREINSPECTION REQUIRED: ISSION TO INSPECT: lnspections may involve obtaining photographs'reviewing and copying records, and codes. GRANTED BYiance withnln Re Fire Department 21 60 Santa Barbara Avenue, San Luis 0bispo, CA 93401 -5240 805.781.7380 $tooity.,Jrq January L2,20L8 Mr. Dennis Rademacher Commercial Property Located at 539 Marsh Street, San Luis Obispo, CA. Closure Letter for Abatement of Lead Contaminated Soil. Dear Mr. Rademacher: Thank you for your assistance during the characterization and abatement of Lead contaminated soil. Your consultant, Earth Systems, has provided me with work plans, soil analytical w/chain of custody, and hazardous waste manifests relevant to the site clean-up. Based on all of this data San Luis Obispo City Fire is issuing this closure letter with no further requirements. Please let me know if you have any questions or concerns, if I can be of further assistance please contact me at (805) 781-7383. Sincerely, Hazardous M rials nator San Luis Obispo City Fire Department kbovle@slocitv.ors cc Mr. Tim Conroy, Earth Systems SLO City Building Division Address File Ea rth Systems 4378 old santa Fe Road | San Luis obispo, cA 93401 | Phr805.544.3276 I www.earthsystems.com January LI,ZOLB FILE NO.: SL-L7522-EA Mr. Dennis Rademacher PROJECT:RADEMACHER PROPERW 539 MARSH STREET SAN LUIS OBISPO, CALIFORNIA SUBJECT; Results of Supplemental Confirmation Sampling for Site Cleanup Dear Mr. Rademacher: This report presents the results of supplemental confirmation soil sampling and analysis at the above-referenced site. The purpose of the work was to collect and analyze soil samples from a remedial excavation at the rear of the property, per the request of the San Luis Obispo Fire Department (SLOFD). Our work has consisted of collecting soil samples from four locations in the excavated area, laboratory analysis for soluble lead, and preparation of this report. lncluded with this report are a vicinity map, a sample location map, a SLOFD field inspection form, and laboratory reports. Site Description/Project Background The site consists of a 50- by 135-foot commercial lot on the east side of Marsh Street, approximately 45 feet north of Beach Street, in San Luis Obispo, California (for purposes of description in this document, Marsh Street is assumed to run north-south). The site contains a one-story commercial building occupying the central part of the loU the area west of the building isusedforparking,andtherearofthelotcontainsasmall patio/backyardarea. Therearedge of the lot contains a small slope that ascends approximately 5 feet to the adjacent lot to the east. The site location and layout are shown on the Vicinity Map and Sample Location Map attached with this letter. The building on-site is presently used for professional offices. Based on information obtained from historical maps and the property owner, the site was originally developed as an automobile repair business in the mid-1950s. This use lasted until sometime in the 1970's, after which it was used for commercial offices and retail purposes. ln February 2OL5, four shallow borings were excavated at the site to collect soil samples in the rear part of the site. The intent of the sampling was to evaluate lead and hydrocarbon concentrations in soil at the rear of the former repair building, as the repair business operated at a time when typicalwaste disposal practices were not in accordance with current environmental standards. Laboratory analysis determined that low levels of oil-range hydrocarbons were present in shallow soils, as well as total and soluble lead at concentrations above health-based Rademacher Propefty San Luis Obispo, California January L1,,20L8 [aboratory Analysis The four soil samples were submitted to a State-certified laboratory for analysis. Each sample was analyzed for soluble lead by the California Waste Extraction Test (WET) and EPA Test Method 60108. Lead was detected in each of the four samples, at concentrations rangingfrom 0.50to 3.1 milligrams per liter (mg/L). Laboratory reports and chain-of-custody documents are attached with this letter. Results for the January 2015 (total lead) and January 2OL8 (soluble lead) confirmation sampling events are summarized below in Table 1. TABIE 1 RESULTS OF LABORATORY ANALYSIS 5.0200Target Cleanup Level 3.1160c-6@24" 2.6L20c-5@18" L.71.20c-4@t6" 0.s0110c-3@ts" L2c-2@3', 4.4c-l@3', 5efrtbb L?C.llniru, lon'tDitreffgtl lhntd, jlilrt igj6Sirrah F, Conclusions and Recommendations Results of the January 2018 soil sampling indicate that soluble lead concentrations in the four samples with total lead greater than 50 mg/kg are below the 5.0 mg/L Soluble Threshold Limit Concentration (STLC). Consequently, the soils are not considered a hazardous waste. Based on the results of the January 2016 and January 2018 sampling events, it is our opinion that the remedial excavation has satisfactorily removed the lead-affected soil, and we request that the SLOFD issue a closure letter for the site, [imitation This report has been prepared for the exclusive use of Mr. Dennis Rademacher, regarding the property at 539 Marsh Street in San Luis Obispo, California. Use ol or reliance on the information and opinions contained in this report by other parties, without first consulting this office, is at those parties' own risk. The findings and conclusions in this report are based on the results of Jaboratory analysis of soil samples. lt is possible that variations exist beyond or between points explored during the course oftheproject. Changesinconditionscouldalsooccurduetocontaminantmigration,variations in rainfall, temperature, or other factors not apparent at the time of field work. 3 VICINITY MAP Rademacher Property 539 Marsh Street San Luis Obispo, California f-t230 fr ftl}; I : qfm lbbil 142 IH@ W(XS{ ) a TI € Earth Svstems Pacific L Project No. SL-1 7522-EA January 2018 County of San Luis Obispo ( ot lrils cffy san oBtspo Date:dr TNTT "/ il4il7 //t4/ Environ mental Health Services (805) 781-5544 P.O. Box 1489 2156 Sierra Way San Luis Obispo, CA 93406 BPOl BPO2 BPO3 TROl TR()2 EROl Fire Department (805) 781-7380 2160 Santa Barbara Avenue San Luis Obispo CA 93401-5240 EFW data entry by: CERTIFIED I]NIFIED PROGRAM AGENCY (CUPA) HAZARDOUS MATERIALS INSPECTION FORM N/Atrun cosITn NOnnn NINI T n nnnn !n ATOI AT02 BUSINESS PLAN Business plan is complete, current, & available during inspection (HSC 25503.5, Title 19 CCR2729) Inventory of hazardous materials is complete (HSC 25504, Title 19 CCR 2729) Site layout/facility maps are accurate (HSC 25504, Title 19 CCR2729) TRAINING PLAN Facility has appropriate training program (Title 19 CCR2132 &22 CCR66265.L6) Training documentation is maintained on site for current personnel (Titlc 19 CCx.2732 & 22 CCR 66265.16) EMERGENCY RESPONSE PLAN Contingency plan is complete, updated, and maintained on site (HSC 25504, Title 19 CCR273L &22 ccR s 6626s.53/s4) Facility is operated and maintained to prevent/minimize/mitigate fire, explosion, or release of hazardous materials/waste constituents to the environment, Maintains all required or appropriate equipment including an llarm and communications system (Title 19 CCR 2731 & 22 CCR 66265.31- .43) ABOVEGROUND PETROLEUM STORAGE TANK ACT SPCC Plan is reviewed and certilied by a registered engineer within last 5 yrs. (40 CFR 112.5(bD SPCC Plan is maintained on site or nearest field office. (HSC 25270) to oltain forms f comply with BPO1-8P03,and ER01COMMENTS Go to GPS Coordinates: Latitude: _deg __min_decimal min INSPECTOR: lnspections may involve obtaining photographs, reviewing and copying records, andSION nce BYcodes flcnr-nnefl ncrn usrI HW Generatorf] Business PlanN YESg{oREINSPECTION REQUIRED !cnunen ncrE usrI HW Generatorn Business PlanED:PROGRAMS 1ilsnecr PH MTITNflADDRESS: (?{ Result Code: Action Code: I 32 37 33 31 Routine Complaint _70 _80 AGENCYEJFn ,ac oepr 1ffow nnr t-til]ilfnFACILITY NAilE: ,? lilin IA .,ttt|. 0+t @ FACILITY REP: mIn Oilfield Environmental & Cornpliance, lnc. Earth Systems Pacific 43?8 Old Santa Fe Rd. San Luis Obispo CA,93401 Projeot Earth Systerns Pacific Project Number: SL-17522-8A539 Marsh, SLO Project Manager: Tim Conroy Rcportcd: 0lll0l20l814:26 SAMPLE SUMMARY ID ID Client Mrlrix Lrb Matrix Drte Drte c-3A@r5 c-44@t6 c-5A@18 c-6L@24 180025 l-01 180025 t-02 r 80025 I -03 1800251-04 Solid Solid Solid Solid Solid Solid Solid Solid 0l/0211815204 AUA2/815:21 0l/02/18 t4:53 0l/02/1814:47 0l/03/18 l4:43 0l/03/18 14:43 01103/1814:43 0l/03/18 14:43 1'he resuhs in this reporl apply to lhe samples analy:ed in accotdance wilh rhe ehain of cwtody doament This analylical rcport m6t ba reprcduced in its enti?ety Client Connect: cli€nt.oec.com\reports TEL; (805) 9224772 FAX: (805) 925-3370307 RoemerWay, Suite 300, Santa Maria, CA 934 www.oecusa.com Page 2 ofs Oilfield Environmental & Compliance, lnc. STLC Metals by 6000/7000 Series Methods - Quality Control Batch 88A0176 - $Tf,CrcPA 60108 Preparation: EPA 30104 Leachate 01/09/18 13:56 Blrnk (B8A0l?6-BLKI ) Lead LCS (884,0176-85r) Lead LCS Dup (88A0176-BSDI) Lead Duplicate (BEAOl76-DUPl) Lead Leach Fluid Blank (88A0176-LBKI) Lead Matrix Spike (88A0176-MS1) Lead 2.16 2.18 Source: l7047EE-01 0.141 ND Sourcc: 17047t&01 9.62 Sourcc: l7047EE-01 9.68 lul,alyzedl. 0 I /091 I 8 I 5:20 0-010 mgll- Analyzed: 0 l/09/l 8 14:53 0"010 mglL 2.00 Analyzed; 01109i18 14:56 0.010 mgL 2.0A Analyzed: 0 l/09/1 8 15:31 0.050 mg/L ND Analyzed: 0 | /09t 1& 15:24 0.050 mglL Analyzed: 0 l/09/l 8 15:00 0.050 mg& 10.0 ND Anatyzed: 0 l/09/1 8 I 5:03 0-050 mg& 10.0 ND 108 80-120 109 80-120 t-01 96.2 80-116 ND zv 20 Ma(rix Spike Dup (88A0I76-MSDI) Lead 96.8 80-n6 0.673 2Q The results in tl?is rcport apply to the samples analyzed in accotdance with the chqin ofcustody doeument This analytic^! tepoil nul be reproduced in iti entirety Client Connect: client.oec.com\reports TEL: (805) 9224772 FA)(: (805) 92s-3376 Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA" 93401 Projec* Earth Systems Pacific Pncject Number: SL-17522-EA 539 Marsh, SLO Project Manager; Tim Conroy Reported: 01ll0D0l814:26 Anall.te Result RL Units Spike Sotuce Level Result %R.EC %REC Limits RPD RPD Limit Notes 307 RoemerWay, Suite 300, Santa Maria, CA 934 www.oecusa.com Page I of5 Oilfield Environmental and Compliance 307 Roemer lfay Suits 300, Santa llarla, CA $454 Phone: (805J 912*{772 Fax. {805) 925,3376 rlrw.oecusa.cdm 101 Adtlsson Way, Taft, CA 93268 Phone: CHAIN OF CUSTODY of Timel e3 I t*' /Q(45 t'3'r t2 :sz-sommgilaJFo*$.trix Ksfri A = air./ v€9or AQ = aqu6B DIV - ddnKng w€lar F i ffller 9VU =.grdr_rd wEtea P. product / oil P\{ = productml€r I = slid l$diment SW = *rfa6.wtea Xr.-Lft e. )-41IJt4q1q XL-S* a- 1.3'Ist.rl{eh 2\c-Ll* (>, lL'"l-tl.fr Itl XC-sae, I{'I5l-"t:8 Claent S8mple lD ASAP- Conl.(€* key) *otoltdTime llOTE; Smpbs EcelYed afte. d:o0Fll 5 Days (6td} be considecd as reeived ths trilt buslmss 1 Day-3 Dayilimer 10 Days- EDF.(std)-REport Foms(s): FAX-L N\\ e Fd;.,n*. Sl4qrtl Enall: Sp€cirl lnstruc{ons:rdnalyrh Raquested City of San Luis Obispo Fire Department 2160 Santa Barbara Avenue, San Luis Obispo, CA 94301'5240 Phone 805-781 -7380, Fax 805-543-801 9 REQUEST FOR PUBLIC RECORDS The California Public Records Act (Government Code 6250. et seq.) was enacted to ensure public access to public . -;eco;ds. Ttlis form will enable us to accurately and efficiently fill your request. 'Gopies are $0.35 per page-- -"- NAME:|.,\ea.zLoy s DATE OF REQUEST ld- 7-/ 7 FIRM:6-4 *te-'r ADDRESS:/tf /+ 'Trab^-co s ?)t . PHONE:tru { bb3 b4o2'PHOTO ID INFORMATION REQUESTED: For each record, list street address and subject matter s'bq \No-n 5 =+3^n-' L,-ct 06*C)c YOUR REQUEST WILL BE PROCESSED IN COMPLIANCE WITH THE PUBLIC RECORDS ACT. @lifomia Ganemment @de S€,c{.ion esg ( c). Eadt agency, upon reguest for a apy of rwds slr€ll, withil lo &ys hom r*eipt ol the request' detemine whelher the reauest, in whole oiin' ptt, seeis qipiei ot disileabte publb rwrds h &e possession of the agency and shal Pvtlptly naify A* Wo* n*ing ihe iquest of the diteminatim aid he reasqts thereforc. ln unusua! circumstances, lhe time limit presaibed in this s""iim m"y Oe extend6d by written notice by the head ol the agency or hls or her destgnee to the percon making the request setting forth the reasons for the ertension and the date on which a determinatio-n is expected to be dispatched. No notice shall specify a date that would result in an extensiott for more than 14 days.l Please contact Kerry Boyle of San Luis Obispo City Fire to schedule a File Review. He can be reached at (805) 781-7383. FOR OFFICIAL USE ONLY Researched bf Time Spent: Date Gompleted: Charge (if any): Mail:Pickup: 05-29-02 Irt" *rd h llils sedim, 'Untsual dmnnlrjtatlrxts, m&t:F', but mly lo the ertenl reasatabty neessary to the pttP€r P1rr/,sslng of lhe pttlanlar ro$resg t)Ttn need to eea'rilt lor aN dled trc requered rcoordt lmn lield ladlltles or other aslaillshments tlls't are se!€nte^frcfn AB offi6 proessli fre rpquest 2)The need to seardt lu, tileA and apgqrhtely exatnlne a wlmthow anount of-Eer€tr,te aN dlsllnd reands 'wn4r uiAena/aeA h abhgte reqwsL q'f}ls ;od tq-crnsdiittoit, wlttih slrr.ll be @d(r;ted wnh .all po.dlcr.ble ffnedt wlth g$lyl agency havhg etbtanltal hlerest |fr.'the aircrntmlUon d tho rcquest or anq:U two or morc @nponents ol he agency lpvlry eu0s/lanilal suble(' naildrhlet€6,tll7F/eln. Re: Fire Department 2lbil fliji'la t,ittfii.\ttt A\)eilt.te 5t11 I irrs i;bis1jo. lA ( '/l _11 -,1r'i{l ?,,0i 7fr1 7:,8(J slucily orri February 5,20L6 Mr. Dennis Rademacher, Owner Commercial Property 539 Marsh Street San Luis Obispo, CA 93401 539 Marsh St., San Luis Obispo, CA. Report From Earth Systems Pacific Dated February 3, 2Ot6 - "Results of Confirmation Sampling for site Cleanup". Dear Mr. Rademacher: I have had an opportunity to review the lab analysis for the Confirmation Soil Samples collected following the removal of lead contaminated soil from the property mentioned above. At this point in time there are a couple of options for you to consider. All of the confirmation samples are below the initial target for lead to be considered a hazardous waste. However, the confirmation samples were not tested for solubility potential with the test being called Soluble Threshold Limit Concentration (STLC). ln order to issue a full Case Closure letter from SLO City Fire Dept. we would need to run that test on 4 of the 6 samples tested. The laboratory has a modest holding time for the samples should you choose to run the additional test (STLC), so it is important to act in the next week or two. lf the 4 samples pass the test San Luis Obispo City Fire Department would issue you an unconditiona I site closure letter. lf we will leave the soil in place without running the additional analytical test, there would still be restrictions on your use of the land. A change in zoning, building occupancy, or site grading would trigger our oversight. lf the property were to be listed for sale the lead would need to be disclosed to potential buyers. Please evaluate your long term goals for this parcel and advise me of your intentions. I will prepare a guidance document or case closure letter based on your feedback. lt was a pleasure to work with your consultant and contractor. lf you would like to discuss this further please contact me at (805) 78L-7383. Sincerely, \,k D. Kerry Boyle Hazardous Materia Coordin r San Luis Obispo City Fire Department kbovle@slocitv.ors Mr. Tim Conroy, Earth Systems Pacific SLO City Building Division, Address File cc Earth Systd-,s Pacific 4378 Old Santa Fe Road San Luis Obispo, CA 93t101 Ph: 805.544.3276 esp@earthsystems.com www.earthsystems.com February 3,2016 FILE NO.: SL-L7522-EA Mr. Dennis Rademacher PROJECT:RADEMACHER PROPERTY 539 MARSH STREET SAN LUIS OBISPO, CALIFORNIA SUBJECT: Results of Confirmation Sampling for Site Cleanup Dear Mr. Rademacher: This report presents the results of confirmation soil sampling and analysis at the above- referenced site. The purpose of the work was to collect and analyze soil samples from a remedial excavation at the rear of the property, which was formerly occupied by an auto repair business. Our work has consisted of collecting soil samples from six locations in the excavated area, laboratory analysis for total lead, compiling disposal documents, and preparation of this report. lncluded with this report are a vicinity map, a sample location map, a City inspection report, disposal manifests/weight tickets, and laboratory reports. Site Description/Project Background The site consists of a 50- by 135-foot commercial lot on the east side of Marsh Street, approximately 45 feet north of Beach Street, in San Luis Obispo, California (for purposes of description in this document, Marsh Street is assumed to run north-south). The site contains a one-story commercial building occupying the central part of the lot; the area west of the building is used for parking, and the rear of the lot contains a small patio/back yard area. The rear edge of the lot contains a small slope that ascends approximately 6 feet to the adjacent lot to the east. The site location and layout are shown on the Vicinity Map and Sample Location Map attached with this report. The building on-site is presently used for professional offices. Based on information obtained from historical maps and the property owner, the site was originally developed as an automobile repair business in the mid-1950s. This use lasted until sometime in the 1-970's, after which it was used for commercial offices and retail purposes. ln February 20L5, four shallow borings were excavated at the site to collect soil samples in the rear part of the site. The intent of the sampling was to evaluate lead and hydrocarbon concentrations in soil at the rear of the former repair building, as the repair business operated at a time when typical waste disposal practices were not in accordance with current environmental standards. Laboratory arfVsis fttermined that low levels of oil-range hydrocarbons were Rademacher Property San Luis Obispo, California February 3,2OtG present in shallow soils, as well as total and soluble lead at concentrations above health-based screening levels and hazardous waste criteria established by the State of California. Due to the initial nature of the work, the vertical and lateral extent of lead contamination were not defined by the sampling. ln April 2015, six additional borings were drilled in the rearyard, with 15 soil samples submitted for analysis. The results of the analysis identified an area of elevated lead concentrations in the southeast corner of the property, extending from near the lower part of the rear slope to a former roll-up door on the back wall of the building. The vertical and lateral extent of contamination was determined by the sampling. After reviewing the concentrations and distribution of lead in the borings, and considering the site's commercial zoning, a target cleanup threshold of 200 mg/kg total lead was proposed; the cleanup threshold was approved by the San Luis Obispo Fire Department (SLOFD) in a letter dated May 19, 2015. On January !6-L7, 20L6, the affected soil was excavated and removed from the site by RTS Construction Services, lnc., a State-licensed hazardous substances contractor. The excavation removed the lower 2to 3 feet of the slope in the southeast corner of the site, and t2to 18 inches of soil in the level area between the base of the slope and the site building. Due to a lack of equipment access to the rear of the property, the soil was excavated by hand and moved to the front of the site in 55-gallon drums, which were then emptied into covered roll-off containers. A total of approximately 17 loose cubic yards (18.9 tons total weight) of soil was excavated and transported to the Chemical Waste Management, lnc. facility in Kettleman City, California, a licensed hazardous waste disposal site. Copies of the signed hazardous waste manifests and weight tickets for the soil are attached with this letter. Soil Sampling and Laboratory Analysis On January 20,20'1.6, six confirmation samples, labeled C-1- through C-6 , were collected from the bottom and sidewalls of the excavation as shown on the Sample Location Map. The samples were collected into laboratory-provided glass jars with Teflon-lined lids. Upon retrieval, sample containers were capped, labeled, sealed and placed on ice for transport to the testing laboratory. Sample collection was conducted under the observation of SLOFD personnel. A copy of the SLOFD inspection report is attached with this letter. Laboratory Analysis The confirmation samples were submitted to a State-certified laboratory for analysis. Each sample was analyzed for total lead by EPA Test Method 60L0. Lead was detected in each of the six samples at concentrations ranging from 4.4 to 160 milligrams per kilogram (mg/kg). Laboratory reports and chain-of-custody documents are attached with this letter. Results for the January 2016 confirmation sampling are summarized in Table 1. 2 Rademacher Property San Luis Obispo, California February 3,20L6 TABLE 1 RESULTS OF TABORATORY ANALYSIS- Jan 20,2OL6 Conclusions and Recommendations Approximately 19 tons of lead-affected soil were removed from the rear of the site in January 2OL6, and was legally disposed of at a licensed hazardous waste disposal facility. Six confirmation samples were collected from the bottom and sidewalls of the excavation underthe observation of the SLOFD, and analyzed for lead at a State-certified laboratory. Analytical results indicate that residual concentrations in the samples of lead are below the target cleanup threshold of 200 me/ke. Confirmation sample results indicate that the excavation was successful in removing the lead- affected soils to levels below the target cleanup threshold, and the site is suitable for use for commercial (i.e., non-residential) purposes. lt is possible that the remaining soil could contain lead at levels unsuitable for residential use, or requiring special disposal/handling measures if removed from the site. lf the zoning of the property is changed to a more sensitive use category, or if grading/excavation of the site is anticipated, the issue of lead in soil must be considered to ensure that these soils are properly managed. Limitation This report has been prepared for the use of Mr. Dennis Rademacher, regarding the property at 539 Marsh Street in San Luis Obispo, California. Use of, or reliance on the information and opinions contained in this report by other parties, without first consulting this office, is at those parties'own risk. The findings and conclusions in this report are based on the results of laboratory analysis of soil samples. lt is possible that variations exist beyond or between points explored during the course of the project. Changes in conditions could also occur due to contaminant migration, variations in rainfall, temperature, or other factors not apparent at the time of field work. 3 Target Cleanup level 200 160c-6@24" c-s@18"t20 L20c-4@16" L10c-3@r.s" c-2@3'12 4.4c-r@3' Total lead (mg/kg]Sample lD Rademacher Property San Luis Obispo, California February 3,ZOLG The services provided by Earth Systems Pacific have been conducted in a manner consistent with the level of care and skill ordinarily exercised by members of our profession currently practicing under similar conditions in this area of California. No other warranty is expressed or implied. Should you have any questions or comments regarding this document, please contact the undersigned at your convenience Sincerely, Earth Systems Pacific 4 T, Timothy Conroy, CEG Associate Geologist Attachments Copy to Doc. No 1602-008.1TR/sr Vicinity Map Sample Location Map SLOFD lnspection Report Hazardous Waste Manifests/Weight Tickets Laboratory Reports San Luis Obispo City Fire Department, Attn.: Mr. Kerry Boyle RTS Construction Services, lnc., Attn: Mr. Jared Spann b No.1698 CERTIFIED ENGINESRING a \F cluo o C4rEdo t0!4DcImY'mIdb VICINITY MAP Rademacher Property 539 Marsh Street San Luis Obispo, California F__l 2C)ft Sffh: l:9,flI| IlGtdL 142 hlw W6$d Earth Svstems PacificIIvProject No. SL-17 522-EA January 201 6 oc om @ noNo IFUUtFa Iat oIn Confirmation Sample Location (Appr Edge of Remedial Excavation Property Boundary "u+ LEGEND Addition to 3tructure fN MAP Earth Systems Pacific@ February 1,2016 a ET Gounty of San Luis Obispo clt}/ san s o6'tspo #oI lurEnvironmental Health Services (805) 781-5544 P.O. Box 1489 2156 Sierra Way San Luis Obispo, CA 93406 Fire Department (805) 781-7380 21 60 Santa Barbara Avenue San Luis Obispo CA 93401-5240 CERTIFIED UNIF'IED PROGRAM AGENCY (CUPA) HAZARDOUS MATERIALS INSPECTION FORM BPOl BPO2 BPO3 TROI TRO2 EROl ERO2 ATOl ATO2 Latitude: _deg EFW data entry by: Date: GPS INSPECTOR: YES NO COS!n ntrn nun n nn trn untrn N/A trtr BUSINESS PLAN Business plan is complete, current, & available during inspection (HSC 25503.5, Title 19 CCR2729, Inventory of hazardous materials is complete (HSC 25504, Title 19 CCR2729) Site layout/facility maps are accurate (HSC 25504' Title 19 CCR2729) TRAINING PLAN Facility has appropriate training program (Title 19 CCR2732 & 22 CCR 66265.L6) Training documentation is maintained on site for current personnel (Title 19 CCR2732 & 22 CCR 66265.16\ EMERGENCY RESPONSE PLAN Contingency plan is complete, updated, and maintained on site (HSC 25504, Title 19 CCR273I & 22 ccR $ 6626s.s3ts4) Facility is operated and maintained to preventiminimizeimitigate fire, explosion, or release of hazardous materials/waste constituents to the environment. Maintains all required or appropriate equipment including an alarm and communications system (Title 19 CCR 2731 & 22 CCR 66265.31' .43) ABOVEGROUND PETROLEUM STORAGE TANK ACT SPCC Plan is reviewed and certified by a registered engineer within last 5 yrs. (40 CFR 112.5(b)) SPCC Plan is maintained on site or nearest field office. (HSC 25270) to obtain forms with BP01-BP03, TR01 and ER01 min Longitude:-tteg -min-decimal min FACILITY REP: Go to J PERMISSION TO INSPECT: tnspections may involve obtaining photographs, reviewing and determining compliance with adopted codes. GRANTED BY {NAME/TITLE): copying records, and n No IYESREINSPECTION REQUIRED n eerE usr! HW Generatorf] Business Plan !calnne PROGRAMS INSPECTED:n usrn Hw Generatorf] Business Plan Icnlnne! aer FACI PH ADDRESS AGENCYn EHS A,G DEPT CITY FIRE INSPECTION TYPEn Routine n Action Code:37 33 31 Reins Other 0,r1/, tun+rrn 4 o U/4//4/qa,f"A fi ?s '#"utj tor uss on elile Form oMB N0.2050.003e Please Facility Ovnsr or Cortifrcallon of of hazardouE materlals covsred by lhe manifsst exc€pt as ndsd ln tt€m ,8a o\rq 20. Manageme{t l'lelhod Code619. HazardousWaste codes for hazardous wast€ treairnonl, Faclllty (or tRestrtu, Phono: u.s. n.r* 18. €r,F lsa.BhuepancylndicationSpaca n OmnW Iru,rirlR.l.dion trrulRoJeolion ctlltk (, u,tttcr F Jc) d Exportftom U.S, kafk#CA60'079 J 4 U,S,;Dato lho lnastg minlmlzatlon statementcorf! lhal a40CFRldenliliedlnl?m am aquantily snallllft ls ku6. edlf lhattha contenlsExpoder,oflhe attachedconformto the lsrarBof thls oonslgnmenl Consent. alo properallrespaolsandmailed tocondltonlnandlabolod/placardod,for applicabletrans@rl ac$rding lfoxport he ftlmaryshlpmentandlamherebydedateaIodassifled,name, ad Pna t 7. TransporlerAcknowlsdgment ol Recelptof Matorials lmportto U.S. ,.Pod ofenlry/exih 4, g;'tea \o(a 3. , Solid (""t\ 'lleB6'ltCM0ff1 fll t I TypeNo. 9a. HM Sb, U,S, DOT Dasalplion (lndudlng Ptop€t ShipPing Namo, Hazatd Class, lD Numbor' and Pa*lns Gmup (if any)) 11, Total quantjty 10. Contalners 12. Unlt Wt,/Vol, 13. Waste Codes 5. G6nsrabfs Name and Malllng Address' DclrccRndomac&sr JJ} MadlEtrtlr Gen6relofs Phone: addr€ss)sll6 Addross (lf dillerGnt than UNdORM HAZARDOU$ WASTE MANIFEST 1. GineratoilD Number fA,gOB}8J?J9J (66rJ 746-l r32 Rosponsd2. Page I of aclring NumberI A37 856 JJK 8700-22 (Rsv. $05)DHSIGNATEO FACILITYTO DESTINATIOhI STATE (!F REQUiRED) TARE: NET: GRoqd$.l54 ti{J(J .Jr 0v1e/'16 5?5,0 rb ttJ.?6 tnn a0!iQ01hr :i. . .,,L8 LIQTJID i ' '' ! SOTID H farEnrn:(. . it TAM.POTBNTTAL NBG N.SCRBEN NEG ::s'cnsnN' NnG. })flDIZERSCREJN NBG .JD;SCRBBN BKGD NALYST "F soL PPM PPM PAINT:FILTER TEST..NIA VISBLEOIL NSC: '. ' PERCENTSOLID DENSITY CALCIJLATED QTY LWCr PASS. .FAIL POS AT-"F I. I I I I I I I I I I I POS. Pos ' POS POS. POS. !sm l> so%nBsrus >60mm < 6.75 ft. l Af YES YES YES oFwAsTE ltsS 'F NO NO No' NoCANMAJOBTTY BBCPATBDON SIDBS? AI.L,'. IMT t ee ()50 1 t<!_1* Tiaz .:t065 ------ '1ooo 1o,47 1044 1030:.:_ 103.1 1:!31il,{ o8 B"-n S'oll 1;@ a^aluial. DESORIPTION' 1154\11]s .--\123110F --.-t10€:1094 1063 r rzb LT€'A .'tt\oo .;E 1:IZFK53 22,e :1o15 I 11062 1046 1045 .1o44 1o29 1o2.a 1.OzV 4152 gaqsIrzooItzz>. 1 1.o4.4 1S..e21o2€, .1 013I \oar 1 Ogl 1060 1o43 1o42lozs 26 1'to4 1l03 '.1201 :1 151 1 150 1o..t12 'tto24 1011 1479 \to". o ,robd 1.O591041 10401.023 \ou ;.X1.125 1124 1.1 41 1.1174 1173 tlo22l()10 '.1147iAn' 1009 .197q 1077to{, idI.1039 4034:1o.21 1'146' 4oi761020i'ooeI\= 19591o.37 1145 -\ -- 'l007 lozE1036 rr\ 1 170 :looo \rooq 'loo2I 1o74 1()54 1('531 035 1 019 101A .1121\-:1+82 _--} ..t120 1:119.1'143 22e 1005 1cB4 741A 'tu'to 1017 1073 '1o721 051 1062 1o,94 1 095-1 11:42 .t14111j7 1i16 1140 :_i. TIMEQUT ..1. ssps 3C.uNn \ MANIFEST 2 3'4(cTRcLBONB)$IAP.# !i Please or for use elife Form OMB N0.2050.0039 DI n ovJnor or Cedlllcadon of recelpt of hazaldous nal€rlals clvered manllost oxcepl aE nded h ltom 10a20. 19. HazardousWagte cod6s lor hazardous wast€ lreatmont,Molhod Codes and recycling FaclliVs Phone: 18b, Altomate Fadllty (or Generotor)U,S. EPA lD Number n ouanttty IResluuel8a, Dlscrepancy lndlcation Space IExporrfromU.S, Typs I 17 u.s,:Dab Poi of enhy/exil:16. I Pal,rl*r1rdlo,,fl ruttR lectton of Receipt ot Materials lmporlloU,$, ^. Ed()s t F.z Etut-itoo. CDz &F &L2 17r-tp is lrue, Frofile$C460907S gov€nmenhl smalllhatthowasteidentifiedln40mlnlmizafolslatomenlaamgemrator) conform to6!ntantsIExpono(lhathoc€rUfy tho temsof thls cnllslgnment ol lhe attached arolabelod/placsrded,maded and alllnend applloable of lhis are and 0m thEshipmontandlfexport frimary ereshipping 4. Ig l,'* dogq -rrdleg Llt tvqkt 'Tr'uE 3. I CM001 EOUiF (3olr-611 T00010 TypeNo. 9a. HM gb. U,S, 0OT Doicdpilon (ndudirqg Proper Shipring Name, Haz6'Id Glass, lD Number, and Packng Group (lfany)) 12, Unit W.lvol. 11. Total Qusntlty .l0. ContalnerE 13. Wasle Godes Goneratols Phone: (lf dllferent than malllng address) EA .5100 Gonoratofs DruirRadearachnr J39 Mar&$trrt UNIFORM HAZARDOUS WASTEMANIFEST 2. Page 1 olTffiGllDliumbersAc08tc37J95 t3r JJK70 are DESTGNATED FAeltmVTO DESTINATION STAT€ (lF BEAUIRED) ,i. T'IME ,,i. .. .. . i' ...... .. c.FqsptI t-6U340 Llr iiPPM TARE: 10".[7' tqn ' ..,t.. 400s01br .. :..r:.j .' t L5:04',' it,:.- .I i' yanpAcn: N/A : PASS ': 'FAIL .NEG .' POS. LB/G H .'. SOLID. *peARiNop.: ViTBRMIX AT TAMPOTBNTIAL NEq '_i.' ; -1: ' N:,SCREBN NEG :.SiRBBN NEc }XIDIZERSCREEN NEG :AD;'SCREBN . BKGD NALYST lphnrnnrenresr I ivIs,BLJgIL I PERCBNT SOTID lopNrr* l"aiewettoqtv llwcr ! srr li so%oBsRls .l ;. lt 69'o. l<6.75'ft; Pop Poq POS POS POS AT Af YES YES YES PPM oF. OF ,NO NO NO NO'CAN-MAJORTTY OFWASTE. IESBBCoATEDoNAtL ,-, -sorist I}IIT GALLONSUSBD \. \ 11067'1o32 ( I O4a roait \ \ 1q47 I1egs_ ro6o \1'154 i\ 10'64 1063 '1A46 :1.O45 4r.'hor _ _\_ 1"fu1 t ot'st .1qAaloaz1944 '1o29 ,1024 1030 1031 {23() 1 11152 153 \ '1()14 I rr\(258 1013 rlO60---:;- 1 061{943 :1O42 1o2ei 1025 111.O',4 1 103\or:t zciz1 151 1,15u.\r)ee 1229 \:ii.'.. . \ 1042 10591041 '11o.2 1 101 1 .rosdno4o '1o.24 1o23 11.24 7'.425 rrh Io8o .1O79 1 1174 1173. \' ros'oo1074 1147{o39 1034 r\'zz--_\ 1.1t23, vo991O77 70 11. '1.1146 'ro9a't&a\1 008 .1009 1010 {o55, --:2ro{e !9az' '1o22 1o.21 1o20 '1.121 Y.198 1'146 1\,rociz r oo'o10o2 oo3 lo53 '1036 1035 1919 1014 1096 .4n,q7 1o74 lOVQ 1143 112(J ,i'r.1s 1o,34 .1o951 005'1 1o17. 1 tJ3:5 1052 1051 1072 1o94 :1,1.1a .111.7 1142 1141 i_- T1 1071 1093 1144 _I:t \ RM#RT/tiru B1s PHiasBlA, Oilfield Environmental and Compliance, INC Tim Conroy Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo, CA 93401 27 January2016 RE: 539 Marsh St, SLO Work Order: 1600350 Dear Client Enclosed is an analytical report for the above referenced project. The samples included in this report were received on 21-Jan-1610:40 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. lf you have any questions regarding this report, please do not hesitate to contact the'undersigned Sincerely, 1: .. iI Meredith Sprister Project Manager TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Numbe r : SL- 17 522-EB Project Manager: Tim Conroy Reported: 27-Ian-16 13:07 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received c-l@3', c-2@3' c-3@1s' c-4@16 c-5@18" c-6@24" 1600350-01 1600350-02 1600350-03 1600350-04 1600350-05 1600350-06 Solid Solid Solid Solid Solid Solid 20-Jan-16 12:15 20-Ian-76 12:20 20-Jan-16 72:26 20-Ian-16 12:35 20-lan-16 12:40 20-Jan-16 12:44 2l-Ian-16 10:40 2l-Ian-16 10:40 2l-Jan-I6 10:40 2l-Ian-16 10:40 2l-Jan-16 10:40 2l-Ian-16 10:40 Oilfield Environmental and Compliance The results in this report apply to the samples analyed in accordance with the chain of custody document. This analytical report must be reproduced in its entiretJ). TEL: (805) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 2 of 6 Oilfield Environmental and Compliance, lNC. c-t@3' 16003s0-01 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Totnl Mefnls hv EPA 6000/7000 Series Methods Lead 4.4 0.49 mg/kg I 8640590 25-Ian-16 25-Jan-16 EPA60I0B c-2@s' 1600350-02 (Solid) Analyte Result Reporting Units Dilution Batch Prepared Analyzed Method Notes l,rmlt Oilfield Environmental and Compliance Tofal Mefels hv F,PA 6000/7000 Series Methods Lead 12 0.46 mglkg I B6A0s90 25-Jan-16 25-Jan-16 EPA6010B c-3@ts" 16003s0-03 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tnfnl Mefcls hv tr',PA 6000/7000 Series Method.s Lead 110 0.48 mg/kg I 86A0590 25-Ian-16 25-lan-16 EPA60108 N-02, N-03 Oilfield Environmental and Compliance The results in this report apply to the samples analyed in accordance vith the chain of custody document. This dndlytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX: (805) 925-3376 Earth Systems Pacific 4378 Old, Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Numbe r : SL- 17 522-EB Project Manager: Tim Conroy Reported: 27-Jan-16 13:07 307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 3 of 6 Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EB Project Manager: Tim Conroy Reported: 27-Ian-16 13:07 Oilfield Environmental and Compliance, lNC. c-4@16,, 16003s0-04 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhnds Lead 120 0.50 mClke I 86A0590 25-Ian-16 25-Ian-16 EPA6010B N-02,N-03 c-5@18" 16003s0-0s (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofcl Mefels hv EPA 6000/7000 Mcfhnds Lead t20 0.49 mg/kg 1 86A0590 25-Jan-16 25-Jan-16 EPA60l0B N-02,N-03 c-6@24" 16003s0-06 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhods Lead 160 0.46 melke I 86A0590 25-Jan-16 25-Ian-16 EPA 6010B N-02, N-03 Oilfi eld Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 4 of 6 Earth Systems Pacifio 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St SLO Project Number: SL- I 7522-EB Project Manager: Tim Conroy Reported: 27-Ian-16 13:07 Oilfield Environmental and Compliance, INC Batch 86A0590 - EPA 30508 Total Metals by EPA 6000/7000 Series Methods - Quality Control Blank (86A0590-BLKI)Prepared & Analyzed: 25-Jan-16 Lead LCS (86,{0590,851) ND 0.50 mdkC Prepared: 25-Jan-16 Analyzed: 26-Jan-16 Lead LCS Dup G6A0590-BSDr) 104 0.50 mClk9 100 104 80-120 Preoared: 25-l an-16 Analvzed: 26-J atl6 Lead Duplicate (8640590-DUPI) 103 0.50 mglkg Source: 1600377-01 100 103 80-120 Prepared & Analy zed:. 25 -J an-l 6 0.677 20 Lead Matrix Spike (86A0590-MS1) 2.23 0.50 mgkC Source: 1600377-01 1.97 12.1 Prepared: 25 -I an-76 Analyzed: 26-Jan-16 20 Lead Matrix Spike Dup (86A0590-MSD1) 88.9 0.49 mdkc Source: 1600377-01 98.0 1.97 88.7 7t-111 Prepared & Analyzed: 25-Jan-16 Lead 48.9 0.49 mdkg 98.9 1.97 47.5 7l-111 58.0 20 QM-07, QR-04 Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Oilfield Environmental and Compliance The results in this report apply to the samples dnaly:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL:(805) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 5 of6 ,' Oilfield Environmental and Compliance, INC Notes and Definitions The RPD exceeded the QC control limits. The spike recovery was outside acceptance limits for the MS andior MSD. The batch was accepted based on acceptable LCS and/or LCSD recovery and/or RPD values. Analyte concentration above 20x TCLP. Analyte concentration below TTLC but above lOx STLC. Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference QR-04 QM-07 N-03 N-02 DET ND NR dry RPD Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-l7522-EB Project Manager: Tim Conroy Reported: 27-Ian-16 13:07 Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chdin of custody document. This analytica! report must be rcproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 6 of 6 Oilfield Environmental and Gompliance 307 Roemerlllay Suite 300, Santa illaria,.CA 93454 . ' Phone: (805)9224772 Fax: (805) 925-3376 www;oecusa.com .\ 101 Adkisson Way, Taft, CA 93268 1 CHAIN OF CUSTODY Phone:l.762-s143 Page 0f l-?D"ltlTrtt kF+blni\ /,/*).8 2i( rta'tilt>zl t->o-b/mo s-z*r$*$ (\) s ( t / I / I Date: e D a CI { /a Date: Date: L Time: Time: Time; Time: C4 e >,f{ C-€ g. l8'' (--+ @ lLu (.'3 e /''4 e-T@3' C-l @- 3' NOTE: Samples rcceived after 4:00PM will be considered as received the next business To W ASAP- (see xey)Glient Sample lD 1 Day-3 Days'2 Days-5 Days (std)- .CoIULUFT EDF-FDF EDD. #of Cont. Date/Time Sampled Tims 10 DaYs- Format(s): FAX- Phone, {44-Znb Fax:E-mall: e* Xx )\ Y K K d + s MatrkKey*: A = airlvapor AG= aqueous D-llU = drinking water F = filbr GW = ground.water P = product/oil PliV = product water S E soliJ /sedrnent $W = slrtiace water WP= wipe lVl,lt = waste water gommenlslPCXI; -l $pecial lnstructiors:Analysis Requested t* Receiired Received Date: Received Date:Tlme: CLIENT:ga'rlh COC RECEIVED DAIEMI|E 0l-p.t *t b /0 4a LOGII{ DATETBtrE: WORKORDER;tbooTST o{-&/ - [h /05 q TEMPERATUNE: 5 'c Aeeptable Rsng€: 0'C lo 6.C [see e(csption noiBs belowl SABIPLERECEIPT REFRFERAT0R(S), g TRANSPORT Counierlsampler E De[very (Other than OEC) fl Af,er-llours Outside Dropotr lgroughl lnsidel lnitialsiDab/Time: fl Shipment Tracking #: SEALS Present cooler{s): nPresent, lntact ffpresent,Notlntaci I None Sample(s): lPresent, lnhc't EPresent,Nolhlact I trfne LE RECEIPT, CONDTTIOH, PRESERVATTON il Samples Received Outside Temperature REnge lAcceptsblel tr Ambient Ak or Filier M€trk n ReceiveU Ambjent, Placed onlc€forTransporl f1 Sample Tempemture Acreplabte for Analysis Requested f] Samples Received Outside Temperature Range JExceptionl n See Problem ChEin * I lnsuffrcient lce or Unknown Cause E Expedited PM Nolificaticn COC Document(s) Rec€ived Wth Samptes Conect Containeds) br Analysis Requested Containe(s) lntact and in Good Condition ConEiner Lsbel(s) Consistent with COC Pmper Preselatiott on Sample Label(s) OEC Preseruative Added e VOA Containers Free sf Headspace Tedler Beg(s) Free of Condensa$on YES NO N'A Ffr*nBtr-tr E il*il FD.iltrn&trn(tr n..Btr n*# (*) oEc PREri. tD r) PROBLEM CHATN FORfi REQUTRED hA l'9'ft oEc CONTAINER ID I +-r*H. l'8 oz ala-fs €a..eA CONTAINER DESCRIPTION PRESERVAT1VE GHECKS: Cf, S'&/or pH s 5 MATRIX COMMENTS INITIALS coc R RECEIPT LOGIN BY:u{RECEIPT REVIEVUED BY:6'aL ':page-f. ", I .Ha rth System s Facific May L4, 2015 FILE NO.: SL-17522-EA Mr. Dennis Rademacher PROJECT RADEMACHER PROPERW 539 MARSH STREET SAN LUIS OBISPO, CALIFORNIA SUBJECT: Results of Supplemental Soil Sampling and Analysis REFERENCE:Change Order No, 1, Rademacher Property, 539 Marsh Street, San Luis Obispo, for Supplemental Soil Sampling and Analysis, by Earth Systems Pacific, Doc. No. 1503.198.PRP.CO1, dated March 30, 2015 Dear Mr. Rademacher: This report presents the results of additional soil sampling and analysis at the above-referenced site. The purpose of the work was to evaluate the environmental condition of soils in the rear yard of the property, which was formerly occupied by an auto repair business. Our work has consisted of collecting soil samples from six borings, laboratory analysis of 16 samples for total and/or soluble lead, data analysis, and preparation of this report. lncluded with this report are a vicinity map, a boring location map, lead concentration maps and laboratory reports/chain-of- custody documents. Site Description/Project Background The study area consists of a 50- by 135-foot commercial lot on the east side of Marsh Street, approximately 45 feet north of Beach Street, in San Luis Obispo, California (for purposes of description in this document, Marsh Street is assumed to run north-south), The site contains a one-story commercial building occupyingthe central part of the lo| the area west of the building is used for parking, and the rear of the lot contains a small patio/back yard area, The rear edge of the lot contains a small slope that ascends approximately 6 feet to the adjacent lot to the east. The site location and layout are shown on the Vicinity Map and Boring Location Map attached with this report. The building on-site is presently used for professional offices. Based on information obtained from historical maps and the property owner, the site was originally developed as an automobile repair business in the mid-1950s. This use lasted until sometime in the 1970's, after which the property was used for offices and retail purposes. 4378 Old Santa Fe Road San Luls Obispo, CA 93401 Ph: 805.544.3276 esp@earthsystems.com www.earthsystems.com 539 Marsh Street San Luis Obispo, California May 14, 2015 Laboratory Analysis Sixteen soil samples (14 from the current sampling event and two archived samples from the previous event) were submitted to a State-certified laboratory for analysis. Each sample was analyzed for total concentrations of lead by EPA Test Method 6010; based on total lead results, three of these samples were analyzed for soluble lead by the California Waste Extraction Test (WET), and one forthe FederalToxicity Characteristic Leaching Procedure (TCLP) methods. Results of Laboratory Analysis- February/April 2015 Total concentrations of lead were detected in all of the soil samples submitted for analysis. Total lead concentration5 ranged from 9.1to 1,000 milligrams per kilogram (me/kg). Soluble lead was detected by the WET Method in each of 6 samples analyzed, at concentrations ranging from 1.5 to 27 milligrams per liter (mg/L). Soluble lead was detected by the TCLP Method in one of three samples analyzed, at a concentration of 0.087 mg/l. TCLP lead was not detected in the remaining two samples, with a reporting limit of 0.05 mS/1. Laboratory reports and chain-of-custody documents are attached with this letter. Lead results for the February and April 2015 sampling events are summarized in Table 1, 2 539 Marsh Street San Luis Obispo, California May L4, 2015 Discussion of Analytical Results For purposes of evaluating remedial actions, we compared the detected concentrations of target compounds to environmental screening levels (ESLs) for commercial/industrial propertiesl, based on the site's commercial zoning. ESLs are health-based screening levels used to evaluate health risks to site occupants, using very conservative exposure assumptions based on a property's current or expected use. Total concentrations of lead were detected above its commercial ESL of 320 mg/kg in boring HA-9 to a depth of 2 feet bgs, and in Borings HA-2 and HA-3 to a depth of l-foot bgs. With the exception of the lZ-inch sample from HA-9, total lead was below its Total Threshold Limit Concentration (TTLC) of 1,000 mg/kg, which is used to determine whether a waste is hazardous under California law. Soluble lead exceeded its Soluble Threshold Limit Concentration (STLC) of 5.0 mg/t in the l2-inch sample from HA-5, but was below the STLC in shallow samples from borings HA-B and HA-10. The STLC was also exceeded in the L2-inch samples from previous borings HA-L, HA-2 and HA-3. The Federal hazardous waste threshold (TCLP)for soluble lead was not exceeded or approached in any of the three samples analyzed for this parameter. Conclusions and Recommendations Ten borings were drilled at the rear of the site in February and April 2015, with a total of 22 soil samples submitted for laboratory analysis of hydrocarbons and metals. Diesel- and motor oil- range hydrocarbons were found in two of the borings at concentrations slightly above the City action level of 100 mg/kg. However, the concentrations detected are localized, and are below commercial site use ESLs established by the CRWQCB. They also occur in conjunction with lead, and consequently mitigation of elevated lead will concurrently resolve potential concerns related to hydrocarbons. Slightly elevated concentrations of zinc, nickel and chromium were detected in several samples collected during the February 2015 sampling event. As discussed in the March 20L5 sampling report, nickel and chromium are interpreted to be normal background concentrations resulting from the presence of ultramafic rocks of the Franciscan Formation in the area. Zinc concentrations are probably the result of past site activities; however, they occur in conjunction with elevated lead levels, and consequently mitigation of elevated lead willconcurrently resolve potential concerns related to zinc. Lead was detected above its ESL in borings HA-2, HA-3, and HA-9, indicating that some form of mitigation is needed. The concentrations of total or soluble lead in these borings indicate that once excavated, the resulting soil may be classified as a hazardous waste under California regulations. The vertical and lateral extent of contamination were sufficiently defined during the current work to establish a basis for remedial action. I User's Guide: Derivotion and Apptication of Environmental Screening Levels, lnterim Finol 2073, California Regional Water Quality Control Board, 5an Francisco Bay Region. 5 539 Marsh Street San Luis Obispo, California May L4, 2015 The findings and conclusions in this report are based on the results of laboratory analysis of soil samples. lt is possible that variations exist beyond or between points explored duringthe course of the project. Changes in conditions could also occur due to contaminant migration, variations in rainfall, temperature, or other factors not apparent at the time of field work. The services provided by Earth Systems Pacific have been conducted in a manner consistent with the level of care and skill ordinarily exercised by members of our profession currently practicing under similar conditions in this area of California. No other warranty is expressed or implied. Should you have any questions or comments regarding this document, please contact the undersigned at your convenience. Sincerely, Earth Systems Pacific 7 4*) (/ -Timothy Conroy, CEG Associate Geologist Attachments: Copy to: Doc. No: Vicinity Map Boring Location Map Lead Concentration Maps: L-, 2- and 3-Foot Depths Laboratory Reports San Luis Obispo City Fire Department, Attn.: Mr. Kerry Boyle 1505-068.1TR/sr e q €N0.1 4 G Or Interlocking Brick Patio EXISTING STRUCTURE Oid Roller Door Wndow IHA-t+ *o-u+ to-u+ *o-t+ Addition to Structure HA_2+ *o-u+ u'e-to + Boring Location (Approx-) ..+ Fenceline ProPerty Boundary *o-+Ho"+ no-t+ HA-10+ Earth SYstems Pacific 0 SCALE (FEE|) 4378 Old Santa Fe R@d San Luis ObisPo' CA 93401€116 54+3276 . FAx (805)544-17A6 E{ait €P@€arthsyslec-ffi BORING LOCATION MAP 539 MARSH S TREET @ ar^! a n15 QF (805) sL-1752-EA /-+- /San Luis Obispo, Califomia .9 I g EXISTING STRUCTURE Old Roller Door Window Window Slab i*'+%;i+ lnterlocking Brick Patio Addition to Structure Tff+ %i+ LEGEND:HA-10+ Boring Location (Approx.) Fenceline Property Boundary (200) Total Lead, mg/kg - Estimated ExtentofTotal Lead in soilz 200 mg/kg " No data at this depth "o-1F ?fr'+ /tl;i+*ott+-i;ii+ ,-,o+ /Y. /05 SCALE (FEET)LEAD CONCENTRATIONS, 2-FOOT DEPTHEarth Systems Pacific 4378 Old Santa Fe Road San Luis Obispo. CA 9340'l€116 539 MARSH STREET San Luis Obispo, California (805)544-3276 . FAX (805)s44-1786 E-mail: esp@earths)6tems.@m sL-17522-EA c May 14, 2015 RW Oilfield Environmental and Compliance, INC Tim Conroy Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo, CA 93401 30 April 2015 RE: 539 Marsh St, SLO Work Order: 1501538 Dear Client: Enclosed is an analytical report for the above referenced project. The samples included in this report were received on 09-Apr-15 16:25 and analyzed in accordance with the attached chain-of-custody. Unless othenrrise noted, alt analyticaltesting was accomplished in accordance with the guidelines established in our Quality Assurance Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. lf you have any questions regarding this report, please do not hesitate to contact the undersigned. Sincerely, @^g;+* Ankita Kashyap Project Manager TEL: (805) 9224772 307 Roemer Way, Suite 300, Santa Maria, CA 93454 \,vww.oecusa.com FAX: (805) 925-3376. Earth Systerns Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SI-- I 7522-EA Project N4anager: Tim Conroy Rcportcdi 30-Apr-15 12:30 Oilfield Environmental and Compliance, lNC. H"A-z @33-36" 150I538-01 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed tvlethod Notes Oilfield Environmental and Compliance Total Metnls bv EP.A.0/7000 Seripc fuIefhorls Lead ll 0.46 mdkg I 85D0359 l3-Apr-15 lS-Apr-15 EPA60l0B HA-3 @ 33-36" 1501538-02 (Solid) Analyte Result Urrits Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Gompliance 6000/7000 Series Methods Lead I90 0.4'1 mg/kg I 85D0359 l3-Apr-15 lS-Apr-15 EPA60l0B N'02,N-03 HA-s @ 9-12" 1501538-03 (Solid) Analyie Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tnfql Mpfqls hv l?.PA 60n0/7000 orips Mefhnrls Lcad 89 0.49 mdkg I 85D0359 l3-Apr-15 l5-Apr-15 EPA60I0B N-02 STLC Metals bv Spries Mefhods Lead 6.9 0,050 mg/L I 85D0820 27-Apr-15 29-Apr-15 STLC/EPA 60r08 N-07 Oilfield Environmental and Compliance The rcsuhs in this rcport appl\, to the sanrples analy:ed in accoilance v'ith the chain of cuslody docunent. This anal!ical report nl.ult be rcproduced in ils eillitvty. TEL: (805) 9224772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 3 of l2 Earth Systems Pacific 4378 Old Santa Fe Rd. Project: 539 Marsh St, SLO Project Nunrber: SL-17522-EA Project Manager: 'finr Conroy Iieported i 30-Apr-15 l2:30San Luis cA,93401 Totnl Metals bv EPA Oilfield Environmental and Compliance, lNC. HA,-1 @21-24" I501538-08 (Solid) Analyte Result Uuits Dilution Batch Prepared Analyzed Mcthod Notss Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhnds Lend 28 0.47 rng/kg I 85D0398 l4-r\pr-15 l5-Apr-15 EPA60l0B }J^L-9 @9-12',1 I501538-09 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Series Methorls Lead 51 0.49 mdkg I 85D0398 l4-Apr-15 l5-Apr-15 EPA60l0B N'02 STLC Metals bv Series Methods Lcad 1.5 0.050 mg/l- I 85D0820 27-Apr-15 29-Apr-15 STLC/EPA 60108 HA-8 @ 2t-24" 1501538-10 (Solitl) Analyte Result Units Dilution Batch Prepared Analyzed Mcthod Notes Oilfield Environmental and Compliance Tnfnl Mefrls hv IIPA 6000/?000 rios Mpfhodc Lcntl 9.1 0.46 mC/kC I 85D0398 l4-Apr-15 l5-Apr-15 EPA60l0B Oilfield Environmental and Compliance The results in this rcport appll'to the sanples anal1,:ed in accordance vilh lhe chain of custod)'doaunenl, 'l'his analylical t'eporl ntust be reproduced iu ils enliretr-. TEt: (805) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page5ofl2 Iiartlr Systems Pacific 4378 Old Santa Fe lld. San Luis Obispo CA,93401 Project: 539 Marsh St, SLO Projeet Nurnber: SL- 17 522-E A Project Manager: Tim Conroy Reported: l5 l2:30 Oilfield Environmental and Compliance, INC HA-l0 @21-24'l 1501s38-14 (Solid) Analyte Rcsult Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Totel Metnls bv EPA 6000/7000 Mafhods Lead 54 0.49 m/kg I 85D0436 I 5-Apr- I 5 I S-Apr- 15 EPA 60108 N-02 Oilfield Environmental and Compliance The results in this rcport apply to llrc santples anal;ced in accordance tvith lhe chain of cttstody doctonent, This analytical reporl Must be rcp'oduced in ils enti,ely. TEL: (805) 922-4772www.oecusa.com Ftrf,:(805)925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 7 of 12 Earth Systerns Pacific 4378 Old Santa Fe Rd. Project: 539 Marsh St, SLO Project Number: SL-l 7522-EA Pro.ject Manager: Tim Conroy Reported: 30-Apr-15 l2:30San Luis cA,93401 Oilfield Environmental and Compliance, lNC, Total Metals by EPA 6000/7000 Series Methods - Quality Control Batch 85D0398 - EPA 30508 Duplicatc (85D0398-DLtP r)Source: 1501530-0I Prepared: l4-Apr-15 Analyzed: lS-Apr-15 Lead Matrix Spil<e (85D0398-MSl 2.93 0,50 tng/kg Source: 1501530-01 7.28 Plcpared: l4-Apr-15 Analyzed: lS-Apr-15 85.3 20 QR-04 Lcad Nlatrix Snikc Dup (l]5D0398-lvlSD t) 93.6 0.46 mg/kg Sourcc:1501530-01 92.4 7.28 93.4 65- l 19 Preoared: l4-Apr-15 Analvzed: l5-Apr-15 Lead Batch 85D0436 - EPA 30508 9q.7 0.49 mg/kg 97.2 7.28 95.1 65- l 19 6.30 20 Blank (85D0436-BLKI)Prepared & Analyzed: l5-Apr-15 I-cad ND 0.50 tndkg LCS (85D0436-BSl)Prepared & Analyzed: l5-Apr-15 l,cad ll3 0.50 n{ks 100 I 13 80-120 Prenared & Analyzed: lS-Apr-15LCS Dun (85D0436-IlSDl Lead I l0 0.50 mgkg Source:1501582-01 r00 I l0 80- 120 z.5I 20 Duplicatc (8SD0436-DUP l)Prepared & Analyzed: l5-Apr-15 Lead Nlntrix Spike (85D0436-VIS I ) 2.95 0.46 mdkg Sourcc: 1501582-01 3.00 Prepared & Analyzed: 15-Apr-15 1.69 20 Lead Nlatrix Spikc Dun (85D0436-IWSDl 104 0.49 mdkC Source:1501582-01 98,5 3.00 102 65-l l9 Prepared & Analyzed: lS-Apr-15 Lead 99. r 0.47 nrg/kg 94.5 3.00 102 65-119 448 20 Oilfield Environmental and Compliance Thc resuhs in this rcporl ttppl)t lo the sanrples analy:ed in accordance'tvilh the chain of custod)'docun ent. This analytical t'eport 'raust be reproduced in its enlirely' TEL: (805) 922-4772www.oecusa.com FAX: (805)925-3376 Reporting Spike Levcl Sourcc Rcsult %nEc Lirnits RPD LimitnalyteResultLimit tjnils %REC RPD Notes 307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page9ofl2 Oilfield Environmental and Compliance, INC TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 85D0732 - EPA 30508 Leachate Blank (85D0732-BLKI)Prepared & Analyzed: 23-Apr-15 Lead ND 0.050 mgll. LCS (85D0732-BSl)Prepared ct Analyzed: 23-Apr- l 5 Lcad 9.80 0.050 nglL r0.0 98.0 80-120 Prepared & Analyzed: 23-Apr-15LCS Dup (85D0732-BSDI) Lead Duplicutc (85D0?32-DUPI ) 9.55 0.050 litrglL Source: 1501538-11 r0.0 95.5 80-120 Prepared & Analyzed: 23-Apr-15 2,63 20 Lead iVlatrix Spilie (85D0732-MS I) 0.0760 0.050 mg/L Source:1501538-ll 0.0870 Prepared & Analyzed: 23-Apr-l 5 t3.5 20 Lead 9.94 0.050 mglL Source:150I538-11 10.0 0.0870 98.6 '75-125 lVlatrix Spike Dup Prepared & Analyzed: 23-Apr-15 Lead 9.38 0.050 rngil 10.0 0.0870 92.9 15-125 5.8J 20 Earth Systenrs Pacific 4378 Old Santa Ire Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-l 7522-EA Project Manager: Tim Conroy Reportcd: 30-Apr-15 l2:30 Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPI) Limit Notes Oilfield Environmental and Compliance The rcsuks in this rcport apply ro rhe samples anallrecl in accordance vith the chain of custody docunent. This onalytical t'eport musl be rcprnduced in irs e,rtircly. TEL: (805) 922-4772 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com Fe{ (80!)_9!5-3376 Pagellof12 Oilfield Environmental and Compliance 307 RoemerWay, Santa Maria CA 93454 phone: (S05) 9224772 fax:. (805) 92S3376 www.oecusa.com ' Rev062012 ' 101 Adkisson UYay, Taft, CA 93268 phone: CHAIN OF CUSTODY prg. I or L SirS irfT LDW iod& b4b a4,l'1. ate/Time Sampled L\t4 tbil t\*{ I.L\L Ln1 s Matrix$ (see key) f s a\) s e:\ S g s (t .5 -{ I I I I I I f I I #of Conl I I I Date:Time: Glient Sample lD 72hr- EDD- Tumaround Time 10 via- FAX- 5 Days- PDF. 24 hr-48 hr- Geodracker EDF- To: Fax: Sampler: E<nail: L+A 4 P,4- t7" t*A4re-8- l.>'' ItA -b (D. 2-l *)'+v #h'Le 4a>' pf{r -.fra- S''7144tt P H&-€p- 9- ttu H*4@e3-,Lu H*-La 33- M' l+A 4 LVl-X*rv IrlA.-1 & s-tTq [ttA -ft p, >1->+Lt r+A *7 @- ?4 tyr' X Y X X xX Y x { -oA-. *\{- tbt- X X X Date:Time: LZKI Time:Date: [rate: Date: Tlme: Tlme: * Matrix Key A.=wpor/ air S=solid/sdiment F=produciloil Hy|, = haz wasts (Liq.) WATERTypes: DW= ddnking 61i9= grcund p161= podtrcad SVI = surface WW = Msta lrcrQ,lte.4 .{3d Analysis Requested site: SL- t?$|?-L *e*'luar<L if s/-D $peciaI lnstructions: Comments/Po# RECEIPT cLIENT:?).?:l-*oEC rD *: tS$\ K3E- remP:Ll oc Acceptable Rangc: ooC to 5oC Rav,0U540 COCRECETYED DATE/TIME:lt.4.\sAtaS RECEIPTLOGIN DATE/TTME:5 @,,, REFRIGERATOR(s): ( SAMPLE TRANSPORT, RECETPT, CONDffiON & PRESERVATION: E[ofC Courier/Sampler CoC document6) receivedwith sainples E_Oelivery(Other than OEC Courier) Corect containers folanalysis requested ' $ samptes Received on Ice Container(s) intact and in good condition I gamples Reoeived outside Temp. Range* Container label($ consistent with CoC fl Sarnptes Direct from field (Outside Temp) OEC preservative added (**no!e std ID) il Afier-Horns Outside Drop-off[Brought Inside] Proper presen'atioa on sample label(s) (InitialslDate/Time): VOA containers fiee of headspace N/A n tr n n fl F. E< Yes No E[x H, fl+K[*EK !* E** trnntr fl*n rE* (*) PROBLEM CHAIN FORM NEEDED Custody Seals (circle): Present rOd Samples / Coolers Intact / Broken* Method of Shipment & Tracking #6rapplicable): Tedlar free of ($*) OEC Preservative ID: Dissolved Metals Filtratio* (oatenniu*esene ID) l> /7 12 OECID CoNTArI{ERS, COC CHANGES AND/OR CORRECTIONS CIIANGES AUTHORAED BY: Client ID ***If bladq referto cac t' ?-u ..vi-E----ywT-FE 1'Tr*$". EA Container Description Preservative ResCl /pE )-- Matrix Date/Time SamDled *** Commenfs I Remarks / Etc. RECEIPT I,OGIN BY:RECEIPT RE\TWED BY:4 Page of Oilfield Environmental and Compliance 307 Roemer Way, Santa Maria CA 93454 phone: (S05) 9224772 fax (805)925-3376 www.oecusa,com Rev 062012 101 Adkisson Way, Taft, CA 93268 phone: {661) 762-9143 CHAIN OF CUSTODY ofPage Tlme: Date:Time: \lg'lt1.t Date: Date:Time: ffi&#.nffij ffiffi- l efu.ffi"qffi- ffi*Kq-+$sw ffiAsW{ffi| ffiqffi $ffi{{qkkr- Sampled Turnaround Tlme 10 5 Days-72hr-48 hr-24hr-ASAP- reportvia- FAX-PDF.Geotracker EDF-EDD. lo:L L Phone:Fax:E*nail: Citv/State/ZlP: b Address: { .t Matrlxr (see key) I I #of Gont. l+t*to {4 u->+' HA, -{D e T-nr Client Sample lD X X -se" \rt{- tJ Analysis Requested 6t-- t7.r7?'€*Slt€: a Proiect Name/#: I A _sa- QCln '* Matrix Key A = vspot/ air 3=solid/sedlmsnt P = Fodu6{/oil HW = hazursste (L'q.) WATERTypes: DW = drinkins 61iy = ground PW = produced SiW = surfu€ WW = €i{B 7n ufcr, *) Comments/PO#: Special lnstructlons: Det€:Tlme: Received Received leceived Data:Tlme: Oilfield Environmental and Compliance, INC Earth Systenrs Pacitic 4378 Old Santa Fe Rd, San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO ProjectNunber: SL-17522-EA Reported Project r: Tim 15 16:26 ANALYTTCAL REPORT FOR SAMPLES ID ID IHatrix Dnte Dnte Received HA-g @ 33-36"I 501742-01 Solid 08-Apr-15 l3:31 22-Apr-i5 l5:54 Oilfield Environmental and Compliance I'he rcsults in thit tuport apply to the sanples analy:ed in accordance t'lth rhe chain of c,tstody docunrent. This anolytical repotl musl be rcproduced i,t lls entirery'' TEL: (805) 9224772 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925'3376 t r I |ll I tlt - Page 2 of 5 Oilfield Environmental and Compliance, INC Total Metals by EPA 6000/7000 Series Methods - Quality Control Batch B5D0720 - EPA 30508 Blank G5D0720-BLKt)Prepared & Aualyzed: 23-Apr-15 Lead LCS (85D0720-rlSl) ND 0.25 rng/kg Prepared & Analyzedl 23-Apr-15 Lead 97.0 0.25 nrg/kg 100 97 0 80-120 Prepared & Analyzed: 23-Apr- I 5LCS Dun (8SD0720-llSDI) Lead Duplicatc (85D0720-DUPI ) 98.8 0.25 mdkC Sourcc: 150 I 740-01 100 98.8 80-120 Prepared & Analyzed: 23-Apr" I 5 1.79 20 Lead Nlatrix Spilce (l]5D0720-NISI ) 4.39 0.25 nrg/kg Sourcc:1501740-01 4.04 Prepared & Analyzed: 23-Apr. I 5 8.34 20 Lead 86. r 0.23 me,/kC 92.2 4.04 89. I 65- l 19 Earth Systems Pacifio 4378 Old Santa Fe Rd. Project: 539 Marsh St, SLO Project Number: SL-17 522-E A I{eported: 29-Apr-13 l626San l-uis cA,9340r Project Manager: Tim Reporting Linit Spike Sourcs l{esult %REC Limits RPD LimitResultUnits Lcvel %I{EC I{PD Notcs Oilfield Environmental and Compliance The resdts in this rcport apply to lhe sanryles analy:ed in accotdance vilh the chain of arstor$,document. This anal/ical t"porl nu$l be ,"ptoduced in ils enlirely. TEL: (805) 9224772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 4 of 5 Oilfield Environmental and Compliance 307 RoemerWay, Santa Maria CA 93454 phone: {80519224772 fax: (805) 925'3376 'w!trw.oecusa.com ' R*062012 101 Adkisson Way, Taft, CA 93268 phone: (661)?62:91/A GHAIN OF CUSTODY of t.Page Turnaround Time Date/Tlme Sampled via- FAX- s Matrix* (see key) #of Cont, I Fax:E-mail: #*-?ref64bn Client Sample lD 10 Days-72hr-48 hr-24 hr- Geotracker EDF-EDD- ASAP. X FP \)+ Fs .4) Lsite:JJ \ss( Date: .f-&)1sl*"- lS oate: V, Date:q.?Z-( ts Time: I Date:q.?jL'tS oate: t.-t S rime: ltLcbC0 * Matrix Key. . A=vapo'r/air 5=sofdis€dimeflt P=F{oduct/oil $W=tEwste(Lh.) WATER Types: Dw=dlnkirE. 619=gpurd PW = produc€d 3W = surfac€ l lW = wast€ 1(-ba,3{K bk Analysis Requested , Special lnstruc-trons: l"D ProlectName/#:-sL - t7.{>2 -ES- GommentslPO#: Oilfield Environmental and Compliance, INC Tim Conroy Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo, CA 93401 19 February 2015 RE: 539 Marsh St, SLO Work Order: 1500466 Dear Client: Enclosed is an analytical report for the above referenced project. The samples included in this report were received on 03-Feb-1515:10 and analyzed in accordancewith the attached chain-of-custody. Unless otherwise noted, all analyticaltesting was accomplished in accordance with the guidelines established in our Quality Assurance Manual, applicabte standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety, lf you have any questions regarding this report, please do not hesitate to contact the undersigned. Sincerely, ' /' ; "/;,.,. .: ,''t ,. r. t..l;;/:i1-..', ,'! --..* Meredith Sprister Project Manager TEL: (805) 927-4772 FAXI (80s) 925"3376307 Roemer Way,Suire 300, sanra Maria, cA 93454 www.oecusa,Gom Earth Systems Pacific 4378 Otd Sanra Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Nurnbcr SL-17522-EA Rcportcd: l9-Feb-15 16:0?Project Managcr: Tim Oi{field Environmental and Compliance, INC HA-1/9-12" 1500466-01 (Solld) Analyte Result **?ll:*H Units Dilution Batch Prepared Analyzcd Method Notes Oilfield Environmental and Compliance Totnl Metals hv EPA 6000/7000 Serles Mcthods 1.4 99 B9 130 130 STI,(] Mafnlc hv 60ll0/70fl0 Series Mefhnds Lead 7.0 0.050 melL t 8580488 l?-Feb-15 l7-Feb-15 STLCIEPA 60IOB N-07 TEPII hv (]C nID Cndmium Chromiunr Lcad Nickel Zirrc 0.23 mg/kg t BsB0l47 05-Feb-15 05-Feb-15 EPA60tOB 0.46 r' I 0.46 " x 0.23 0.91 N-02 N-02 TPH Diesel (Ct3-C22) TPI{ Motor Oil (C23-C40) ND ND l0 50 mgkC I B5B0l40 05-Feb-15 05-Feb-15 El'A80l5M Surrogate : o -Tbrphe nyl t04% 6t-r42 IIA-1/30-36" 1500466-02 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed hlethod Notes Oilfield Environmental and Compliance Ttr'.PI{ hv G(l I?In TPFi Dicsel (Cl3-C22) TPH Motor Oil (C23-C40) ND ND l0 50 mdkg I B5B0t40 05-Feb.ls os.Feb-I5 EPA80t5M Surmgate: o-Terphenyl r}t % 61-t42 Oilfield Environmental and Compliance The rexilts in this report apply to the sanrples analy:ed in accordance *ith the chain of custody document.'I'hls analytical rcpofl nrust be reprcdtced in its entirety, TEL; (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 3 of 12 Earth Systems Pacific 4378 Old Sanu Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL- I 7522-fiA Reported: l9-Feb-15 l6:07ProjectTim Oilfield Environmental and Compliance, INC HA-3t9-L2" r500466-0a (Solid) Analyte Result R"plrllffr Units Dilution Batch Prepared Analyzed Mcthod Notes Oilfield Environmental and Compliance Total Metals hv EPA 6000/7000 Series Methods 0.23 0.46 0.46 0.23 0.92 STLC Metals bv 6000/7000 Series Methods Lead 27 0.050 mglL I 8580488 l7-FeUI5 l7-Feb-15 STLC/EPA 601 0B N-07 TCLP Metals bv 6000/7000 Serics Methods Lead ND 0.050 rng/l, t 8580566 t9-Fcb-15 t9-Fcb.l5 EPA l3l t/EPA 601 0B TE.PH hv (]C IIID Cadmium Chronrium Lead Nickcl Zlnc 5.O I40 5I0 150 3r0 mdkc I 85B0l47 05-Fcb-t5 0S-Feb-15 EPA60l0B N-02, N.03 N-02, N-03 TPH Diescl (Cl3-C22) TPH Motor Oil (C23-C40) ND t70 10 50 ng/lg t B5B0t40 05-Fcb-15 05-Feb-15 EPA80l5M Surrogale : o-Terphe nyl 106% 6t-t42 Oilfield Environmental and Compliance The resillrs ln thir report apply to the santples anoly:ed in occordance villt the clwirt ot custody doctmenl Thls analytlcal reporl muil be repraduced fu ils entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 5 of l2 Ealth Systems Pacific 4378 Old Santa Fe Rd, San Luis Obispo CA, 93401 Project: 539 Marsh St" SLO Project Number: SI--l 7522-EA Projcct Manager: 'lirn Conroy Rcportcd: l9-Feb-15 l6:07 Oilfield Environmental and Compliance. INC Batch 8580147 - EPA 30508 Total Metals by EPA 6000/7000 Series Methotts - Qualify Control Blsnk (8580147-ItLKl)Prepared & Analyzed: 05-Feb-15 Cadnrium Chromium Lcad Nickcl Zinc LCS (8580r47-BSl) ND ND ND ND ND 0.?s 0.50 0.50 0.25 1.0 mdks Prepared & Analvzed: 05-Feb-15 Cadmium Chromium Lead Nickel Zinc LCS Dun (8580147-BSDI) 97.3 103 97. I 100 98.0 0.25 0.s0 0.50 0.25 t.0 mc/kg 100 t00 t00 100 100 97.3 103 97. I t00 98.0 80-120 80.120 80-120 80-l 20 80-120 Prenarcd & Analvzcd: 05-Fcb-15 Cadmium Chromium Lead Nickel Zinc Durrlicate (8500147-DUP l) 98.0 105 98.1 l0l 98,4 0.25 0.s0 0.50 0.25 t.0 mdkc 100 t00 100 100 100 98.0 105 98. I l0l 98.4 80-120 80- 120 80- 120 80-120 80-120 0.717 t.68 1.02 0.748 0.509 20 20 20 20 20 Source: 1500387-07 Prepared & Analvzed: 05-ltcb-15 Cadmium Chromium Lcad Nicket Zinc Mrtrix Snilre (8580f d7-MSl) 0.389 9.51 t0.9 8.62 41.3 0.23 0.47 0.47 0,23 0.94 nrg/kg 0.484 10.6 8.90 8.98 43. I 21.8 t 1.2 19.9 4.05 4.22 QR4420 20 20 20 20 Sourccl1500387-07 Prepared&Analyzcd:054rcb-15 Cadmiurn Chromium Lead Nickel Zinc 91.3 ul 96.4 t00 t32 0.2s 0.49 0,49 0.25 0.98 98.0 98.0 98,0 98.0 98.0 92,6 r03 89.3 93.3 9l-l mgks 0.484 10.6 8.90 8.98 43. I 82-ut 73-t24 s6. t 37 1 t -t25 59-l 36 Oilfield Environmental and Cornpliance The results in this report apply to tln santples anoly:ed in accodonce with the chain o! custod|t docunent, This andlytical repoil must be rcproduced in lls eniltely, TELr (805) 922-4772www.oecusa.com FAX:(805) 925.3376 Reporting Limit Units Spike Levcl Source Result %REC %REC Limits RPD Rqsult RPD Limit Notcs 307 Roemer Way, Suite 300, Santa Maria, CA 93454 Pagc 7 of l2 Oilfield Environmental and Compliance. INC Bstch 8580488 - EPA30508 Lerchate STLC Metals by 6000/7000 Series Methods - Quality Control Bla nlr (13580488-BLI(r)Prepared & Analyzed: l?-Feb-15 Lead LCS (r!5804B8-BSl) ND 0.050 tnglL Prepared & Analyzed: l7-Feb-15 Lerd LCS Dup (8580488-BSDI) 9.75 0.050 ms/L 10.0 97.5 80- 120 Prepared & Analyzed: 17-Feb-15 Lead Duplicate (85804B8-DUP I ) 9.81 0.050 mg/L Source: 1500466-01 10.0 98.1 80.120 Prepared & Analyzed: l?-Feb-15 0.614 20 Leod Matrix Spikc (8S80488-MSl) 7.21 0.050 mg/I. Source: 1500466-01 7.02 Prcpared & Analyzed: l7-Feb-15 2.74 20 Lcad Matrix Spikc Dup (8580488-MSDl) 17.I 0.050 mg/L Source: 1500466-01 10.0 7.02 l0l 7s-125 ?rerrared & Analyzed: 17'Feb-t5 Lead r6.8 0.050 ms/L 10.0 7.02 97.9 75-125 L68 20 Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project: 539 Marsh St, SLO Project Number: SL"17522-EA Project. Manager: Tim Conroy Reportcd: l9-Feb-15 l6:07 Reporting Limit Spike Sourcc Result "/oREC Limits RPD LimitAnalyteResultUnits Level %REC RPD Notes Oilfield Environmental and Compliance Tle results itr this repoil apply to the sauples onaly.ed in accordonce with the chain ol cuslody document. This analytical report must be reproduced in its entircty. TEL:(805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer way, suite 300, santa Maria, cA 93454 Poge 9 of l? Earth Systems Pttcific 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project: 539 Marsh St, Sl.O Project Number: SL-17522-EA Project Manager: Tim Conroy Re portcd: l9-Feb-15 l6:07 Oilfield Environmental and Compliance, INC Batch 8580140 - EPA 35508 TEPH by GC FID - Qualify Control Blank (8580140-BLl(1)Prepared & Analyzed: 05-Feb-15 TPH Diescl (Cl3-C22) TPH Motor Oil (c23-C40) ND NP t0 50 mdkc S ur roga t e : o -Te r p h e nyl LCS TPH Diesel (Cl3-C22) 52,0 50.0 l0 m/ks 50o 104 6t-142 05-Feb- I 5 100 83-l 14 &A 502 Surrogate: o-krphenyl LCS Dun {8S80140-BSDI) t2.4 s0.0 t05 6t-t42 Prepared & Analyzed: 05-Feb-15 TPtl Diesel (Cl3-C22)510 l0 mgkg 500 102 83-l t4 t.55 20 Surroga le : o.Te rpheny I Duplicatc (B5B0I 40-DUPI ) 5 2,7 Source: 1500466-02 50.0 105 6t-142 Prepared & Analyzed: 05-Feb-15 TPH Diescl (Cl3-C22) TPI{ Motor Oil (C23-Ca0) ND ND l0 50 rng/kg ND ND 20 20 Surrogate : o-Te rphenyl Matrix Soike (BSB()t 40-MSr) 5 1,2 Sourre: f500466-02 50.0 102 6t-t42 Preoared & Analvzcd: 05-Fcb-15 TPH Diescl (Cl3-C22)500 l0 mg/kg 500 ND 99,9 7l-128 Svrcgale: o-Terphenyl Mntrix Spikc Dup (8580r4O-lt{SDl) 50.0 IA2 6t-142 Sourcc: 1500466-02 Prepared&Analyzed:05-Feb-15 5 t.2 TPH Diesel (Cl3-C22)5t3 t0 ms/ks 500 ND t03 7l-128 2.56 20 &rrogate: o-Terphenyl 5 t.8 50.0 r04 6t-142 Oilfield Environmental and Compliance The resnlts in this report apply to the sanples analy:ed in acconlance with the chain ol custody docanent. Thls analytical reporl rrausl I)e reproduced h its entil"ry. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376 Reporting Spikc Sourcc Result %REC Limits RPD Analyte Rcsult Limit Units Level %REC RPD Linrit Notes 307 Roemer Way, Suite 300, Santa Maria, CA 93454 Pagc tl of12 Oilfield' Environrnental and Gompliance 307 RoemerWaY, Santa Maria GA 93454 phone: (805)9n-4n2 fa* {805} 92$'3376 rlrww.oecusa.com ' "- R4082012. 101 Adkisson l'tJay,Taft, CA 932S8 phone: (661) 762-9143 CHAIN OF CUSTODY Page of radress: Ll 6@ Fax:E.mall::hone: lo:tr(-l- iend via- FA)(- Turnaround Tlme ecelied ecelved >lNK-nt1 t-ljlttnp >{z/ti- a3a Hblt{- pt1 V-hl6-wr 7{7Lt{'44i 6 s s s t I t I I I q - I|-q-i{ t+& -3 / 4-L>q t** ->/ 1'lvu .36tt "FFP '10 Days- ,ftfrt 5 (see ilatrlxr #of 48 hr 24ht-ASAP.72hr- Cllent Sarnple lD Geotracker EDF-EDD. X X X X o'tN;r =*'tv SFC\FF X X X X f,s \ -!tt 3 nme: I sf Tim6: o '( \) rime: Date: Dat6: -3'/ * Matrlx Key A= vaps/€h P=ploducl/oil 5W=l@msb(Uq) WATERTyp6 tw=drhkiog !1y=gound PW = OroduEd $W = sudace ,VW=v/"ste Comments/Pof$: Analysis Requested Sp€cial lnstructions: eceived tsI,EMCHA.tr}{CLIENT: €a*2,4 1'zSr*tv1 OEC iD #: /€Oo ISSUF,S RBCORDED BY {DATE/TIME/IMTIALS;:6 UTIONS:- Client Authori2ation Contact - Date/TindlnitialsINFO:- Contact b-ja"(t (t (rl 6 @.., -L{ S**Pue I -/z //*s Ha-tq(7 ? t\ tr XO COC document(s) received with samples SContainer label(s) NOT consistent rvitb COC I Containe4s) NOT intact or in 6jood condition E Custody Seals Broken PLEASE PROVIDE DETAILS OF ISSUE(S) BELOW-Samples/Containers Affected' as necessary' E Somples Received Outside Temp" Range (see below) rssuE(s) I lncorect containers foranalysis requcsted E OtHnn, {ifmultiplc, identiff withoumbers) FINAL RESOLUTION OF ISSUES BY (DATE/TIMEnNTTIALS): z*zPasc of 0tr0t/os RECEIPT GLIENT: €tBa-fl *vrta's a@D oEC ID #: / 5;oCIttb b Temp:o d't AcccptnbleRnnge: ooc to 6oC (? REFRIGERATOR(s): d - R*.0lilstlo COC RNCEIVED DATEfTIME: ffioec CourierlsamPler [l oelivery(Other than OEC Courier) Fsamples Received on lce D Samples Received Outside femp' Range* I Samples Direot from heid (Outside Temp) COC document(s) received with samples Correst containers for analysis requested Container{s) intaet and in good condition Container ldbel(s) consistent with COC OEC preservative added (**note std lD) '. Yes NoE fl'r'I -!*-ffi-w.' 4kt'El"'* fl* Eo* nntr n[+n fl'* N/A n tr tr n B m mI D nfter-Hours outside Drop-off[Brought Inside] Proper preservation on sample labe(s) lel's & PRESERVATION:RECEIPT, CONDITTONSAMPLETRANSPORT, Samples / of(In itials/Date/Time):VO,{ containers free of headsPace (s*) OEC Preservative ID: Dissolved Metals Filtration: (Datcl'lnlt/Prescra'€ lD) lntact / Brokent Method of Shipment & lacking #(if applicablc): Custody Seals (circle): Present/ 0) pnonr,rM CHAIN OEC ID ClientclD il*If blank rcfer to coC lxa, fdber I Coirtainer Description ll <-- Preservgtive li lvH ResCl .s Mafrix Dnte/fime Samnled ***Comrnents / Rernarks / Condition Notes, Etc' CI{ANGES AIruHORIZED BY:AND/OR CORRECTIONSCONTAINERS, COC CHANGES RECEIPT LOGIN BY:/-cr*RECEIPT REVIEWED BY;6,M Pagc 4--ol- Oilfield Environrnental and Compliance 307 RoemerWay, Santa Maria CA 93454 phone: (80515224772 fax: {805)925-3376. **.oecusa.com ' .Rsv0620:12. 101 Adkisson $Iay,Taft, CA 93268 phone: {661} 762-9143 CHAI$'I OF CUSTOIIY Page of lecelv€d locelved l€celved L(^d4(Jn W OLtL'v* PJ,-ltsQgP-sa- \ .Jr A A I l* wtatrlx Key lA=u"potr"i,lS=$lftllsedlmBnt p-p.arciloit l.tw = haz rvssra (UqJ HTATER T)treBl DW =dff dng GW = g@und PW= lroduced SlV: surfacq lYW. waste _s a- ag ,J A A A X \r:s t) -1*, L.i. : X ^X X X J( Special lnstructlons:Anatysis Requested Namsl#: 6*X: -3'ru F- X th*-t l3g-A6o Client Sample lD l+k-t /1-tzF{ ,l* ->/ q -tyu r+4 -3 / 4-L>' t{-A^ 1'/ r-,r', bl^i+- * / sg:;/-u -'',4z i'TY Gf' 21*\" \- - #of Cont I I t I l t Date:t57 24hr-48 hr-72ht-10 Days-ASAP.5 Matrbf' (see key) 5 s s s 5 .s Tlme: Daie: '/{1w". ,,*;'/-Qo ftDTIme: Dats: Date: Datemms Sampled tlTttS"q4t HtlS-wt Hbhf- ptl >lb/ti- rda Yl}l6^p.v zdNK-**1 pr,o',"' -fl14 -nXL E*nall:Fax: fftlo: Geotracker EDF-vla- FAX-EDD.PDF. Tumaround Tlme :'l Ea rth Syste m s Pacific 4378 Old Santa Fe Road San Luis Obispo, CA 93401 Ph: 805.544.3275 esp@earthsystems.com www.earthsystems.com May 3.4,2075 FILE NO.: SL-77522-EA Mr. Dennis Rademacher PROJECT:RADEMACHER PROPERTY 539 MARSH STREET SAN LUIS OBISPO, CALIFORNIA SUBJECT: Results of Supplemental Soil Sampling and Analysis REFERENCE:Change Order No. 1, Rademacher Property, 539 Marsh Street, San Luis Obispo, for Supplemental Soil Sampling and Analysis, by Earth Systems Pacific, Doc. No. 1503.198.PRP.CO1, dated March 30, 20L5 Dear Mr. Rademacher: This report presents the results of additional soil sampling and analysis at the above-referenced site. The purpose of the work was to evaluate the environmental condition of soils in the rear yard of the property, which was formerly occupied by an auto repair business. Our work has consisted of collecting soil samples from six borings, laboratory analysis of 16 samples for total and/orsolublelead,dataanalysis,andpreparationofthisreport. lncludedwiththisreportarea vicinity map, a boring location map, lead concentration maps and laboratory reports/chain-of- custody documents. Site Description/Project Background The study area consists of a 50- by L35-foot commercial lot on the east side of Marsh Street, approximately 45 feet north of Beach Street, in San Luis Obispo, California (for purposes of description in this document, Marsh Street is assumed to run north-south). The site contains a one-story commercial building occupying the central part of the lo| the area west of the building is used for parking, and the rear of the lot contains a small patio/back yard area. The rear edge of the lot contains a small slope that ascends approximately 6 feet to the adjacent lot to the east. The site location and layout are shown on the Vicinity Map and Boring Location Map attached with this report. The building on-site is presently used for professional offices. Based on information obtained from historical maps and the property owner, the site was originally developed as an automobile repair business in the mid-1950s. This use lasted until sometime in the 1970's, after which the property was used for offices and retail purposes. t 539 Marsh Street San Luis Obispo, California May t4,2OL5 ln February 2015, four soil borings were excavated at the site to collect soil samples in the rear part of the site. The intent of the sampling was to evaluate metals and hydrocarbon concentrations in soil at the rear of the former repair building, as the repair business operated at a time when typicalwaste disposal practices were not in accordance with current environmental standards. Laboratory analysis determined that low levels of hydrocarbons were present in shallow soils, as well as total and soluble lead at concentrations above health-based screening levels observed by the City of San Luis Obispo and hazardous waste criteria enforced by the State of California. Due to the initial nature of the work, the vertical and lateral extent of lead contamination were not defined by the sampling. ln March 20L5, a site meeting was held with representatives from the property owners, Earth Systems Pacific, and Mr. Kerry Boyle, Hazardous Materials Coordinator for the San Luis Obispo City Fire Department (SLOFD). The SLOFD is the local lead agency for soil contamination cases in the city of San Luis Obispo. After discussing the results of the initial sampling, it was agreed that the target contaminant driving cleanup decisions for the site is lead, in either its total or soluble form. Earth Systems Pacific proposed to collect samples from several additional locations to better define the vertical and lateral extent of contamination; this approach was verbally approved by Mr. Boyle at the meeting. Soil Sampling and Laboratory Analysis On April 8,20L5, six additional soil borings, labeled HA-5 through HA-10, were drilled in the rear yard of the property as shown on the Boring Location Map. The borings were drilled to a depth of 3 feet below ground surface (bgs) using a 4-inch diameter manual soil auger; soil samples were collected from the borings at depths of 6-!2 inches, t8-24 inches and 30-36 inches with a manually driven spoon-type sampler lined with stainless steel sleeves to retain soil. Upon retrieval, sample sleeves were capped with Teflon, labeled and placed on ice for transport to the testing laboratory. Sampling equipment was cleaned between samples by washing with a non-phosphate detergent, rinsing in clear water and a final rinse with deionized water. After sampling, the borings were filled with bentonite and hydrated. Soil cuttings generated from the borings were stored in sealed 5-gallon plastic containers, labeled, and secured on-site pending identification of appropriate disposal measures. Field Observations Soils beneath the site consist of light brown to brown sandy fat clay with scattered gravel. These soils were in a moist and medium stiff condition. Groundwater was not encountered in any of the borings, to the maximum depth explored of 3 feet bgs. Depth to groundwater in the area of the site is 15 to 20 feet bgs, based on previous work at nearby properties. 2 No hydrocarbon odors or soil discoloration were noted in any of the borings 539 Marsh Street San Luis Obispo, California May i.4, 20L5 Laboratory Analysis Sixteen soil samples (14 from the current sampling event and two archived samples from the previous event) were submitted to a State-certified laboratory for analysis. Each sample was analyzed for total concentrations of lead by EPA Test Method 6010; based on total lead results, three of these samples were analyzed for soluble lead by the California Waste Extraction Test (WET), and one for the Federal Toxicity Characteristic Leaching Procedure (TCLP) methods. Resu lts of Laboratory Ana lysis- Februa rV I April 2Ot5 Totalconcentrations of lead were detected in allof the soil samples submitted for analysis. Total lead concentrations ranged from 9.1to 1-,000 milligrams per kilogram (mg/kg). Soluble lead was detected by the WET Method in each of 6 samples analyzed, at concentrations ranging from L.5 to 27 milligrams per liter (me/L). Soluble lead was detected by the TCLP Method in one of three samples analyzed, at a concentration of 0.087 mg/1. TCLP lead was not detected in the remaining two samples, with a reporting limit of 0.05 mg/1. Laboratory reports and chain-of-custody documents are attached with this letter. Lead results for the February and April 2015 sampling events are summarized in Table L. 3 539 Marsh Street 5an Luis Obispo, California TABTE 1 RESULTS OF LABORATORY ANALYSIS. LEAD Februa 3 and 8,2015 Total lead expressed in mg/kg, WET/TCLP in mg/L ESL Environmental Screening Level, commercial/industrial site use, <1O-foot depth, California Regional Water Quality Control Board, December 2013 (Table K-2), in mg/kg TTLC TotalThreshold Limit Concentration (CA hazardous waste threshold), in mg/kg STLC Soluble Threshold Limit Concentration (CA hazardous waste threshold), in mg/L TCLP Toxicity Characteristic Leaching Procedure (Federal hazardous waste threshold), in mg/L Concentrations exceeding regulatory thresholds shown in bold text 4 May L4,2AI5 Soluble tead {TCtPlTotal Lead Soluble tead {WET} HA-tl9-12"89 7.O HA-219-L2"380 t6 <0.05 LLHA-2133-36" ,tHA-3le-tz 510 27 <0.05 HA-3133-35"190 31HA-419-L2" HA-s19-L2"89 6.9 3LHA-'12L-24" HA-019-12"200 HA-612t-24"t7 HA-719-t2"200 HA-712'-24"20 HA-819-L2"51 1.5 HA-812t-24"9.1 HA-g19-L2"1,000 0.087 HA-912L-24 640 90HA-9/33-36" HA-LOl9-L2"57 2.0 HA-tO-21-24"54 320ESL TTLC 1,000 srtc 5.0 5.0TCtP 539 Marsh Street San Luis Obispo, California May L4,203.5 Discussion of Analytical Results For purposes of evaluating remedial actions, we compared the detected concentrations of target compounds to environmental screening levels (ESLs) for commercial/industrial propertiesl, based on the site's commercial zoning. ESLs are health-based screening levels used to evaluate health risks to site occupants, using very conservative exposure assumptions based on a property's current or expected use. Total concentrations of lead were detected above its commercial ESL of 320 mg/kg in boring HA-9 to a depth of 2 feet bgs, and in Borings HA-2 and HA-3 to a depth of L-foot bgs. With the exception of the L2-inch sample from HA-9, total lead was below its Total Threshold Limit Concentration (TTLC) of L,000 mg/kg, which is used to determine whether a waste is hazardous under California law. Soluble lead exceeded its Soluble Threshold Limit Concentration (STLC) of 5.0 mg/L in the 12-inch sample from HA-5, but was below the STLC in shallow samples from borings HA-8 and HA-10. The STLC was also exceeded in the 12-inch samples from previous borings HA-1, HA-2 and HA-3. The Federal hazardous waste threshold (TCLP)for soluble lead was not exceeded or approached in any of the three samples analyzed for this parameter. Conclusions and Recommendations Ten borings were drilled at the rear of the site in February and April 20t5, with a total of 22 soil samples submitted for laboratory analysis of hydrocarbons and metals. Diesel- and motor oil- range hydrocarbons were found in two of the borings at concentrations slightly above the City action level of 100 mg/kg. However, the concentrations detected are localized, and are below commercial site use ESLs established by the CRWQCB. They also occur in conjunction with lead, and consequently mitigation of elevated lead will concurrently resolve potential concerns related to hydrocarbons. Slightly elevated concentrations of zinc, nickel and chromium were detected in several samples collected during the February 2015 sampling event. As discussed in the March 201-5 sampling report, nickel and chromium are interpreted to be normal background concentrations resulting from the presence of ultramafic rocks of the Franciscan Formation in the area. Zinc concentrations are probably the result of past site activities; however, they occur in conjunction with elevated lead levels, and consequently mitigation of elevated lead will concurrently resolve potential concerns related to zinc. Lead was detected above its ESL in borings HA-z, HA-3, and HA-9, indicatingthat some form of mitigation is needed. The concentrations of total or soluble lead in these borings indicate that once excavated, the resulting soil may be classified as a hazardous waste under California regulations. The vertical and lateral extent of contamination were sufficiently defined during the current work to establish a basis for remedial action. r User's Guide: Derivation and Applicotion of Environmental Screening Levels, tnterim Finol 2013, California Regional Water Quality Control Board, San Francisco Bay Region. 5 539 Marsh Street San Luis Obispo, California May L4, 201"5 ln determining an appropriate target cleanup concentration for a site, it is necessary to consider the physical nature of the contaminant, the existing and proposed use of the site, and the likelihood of site occupants being exposed to the contaminant. Use of a hazardous waste threshold, in this case the STLC via the Waste Extraction Test (WET), does not consider health risks and is therefore not appropriate to use as a cleanup threshold. The WET extraction fluid is an acidic solution with a pH of 5, and is intended to simulate conditions in a landfill leachate to evaluate whether a substance is likely to leach into groundwater. Landfill leachate is not present at the site, and thus the WET result does not realistically represent the solubility of lead for in- situ site soils. lt is, however, appropriate to apply WET results to any excovoted soil for determining disposal options. Various health-based screening levels exist for soil contaminated with lead at commercial/industrial sites. These include the California Department of Toxic Substances Control Human Health Screening Level (320 mg/kg), the USEPA Regional Screening Level (800 mg/kg), and the RegionalWater Quality Control Board Environmental Screening Level (320 mg/kg). After reviewing the concentrations and distribution of lead in the borings, we propose a target cleanup threshold of 200 mg/kg for this site. ln our opinion, this will provide an adequate level of protection related to human health and the environment. Once excavation is complete, any remaining soil containing lead at 200 mg/kg or less will be covered with clean soil, thus further limiting the potential for exposure. As shown on the figures accompanying this report, lead concentrations display a fairly well- defined hot spot in the southeastern corner of the property, with the highest concentrations found on the slope at the rear property line. This distribution is consistent with dumping of used oil on the slope when the site was used as a repair garage. The figures show the estimated extent of soilcontainingtotal lead above 200 mg/kg at depths of I,2 and 3 feet below grade. ln total, we estimate that 22lo 28 cubic yards of soil will need to be excavated from the affected area to reduce lead levels to less than 200 mg/kg. A lack of equipment access to the patio from the front of the property complicates the excavation process, and will probably require cooperation with the adjacent property owner to the east, to allow access for equipment to excavate the soil. Before beginning any remedial action, a removal work plan should be submitted to the SLOFD for approval. A copy of this report should also be submitted to the SLOFD for review and comment prior to finalizing any plans for remedial action. Limitation This report has been prepared for the use of Mr. Dennis Rademacher, regarding the property at 539 Marsh Street in San Luis Obispo, California. Use of, or reliance on the information and opinions contained in this report by other parties, without first consulting this office, is at those parties'own risk. 6 539 Marsh Street San Luis Obispo, California May 14, 20L5 The findings and conclusions in this report are based on the results of laboratory analysis of soil samples. lt is possible that variations exist beyond or between points explored during the course of the project. Changes in conditions could also occur due to contaminant migration, variations in rainfall, temperature, or other factors not apparent at the time of field work. The services provided by Earth Systems Pacific have been conducted in a manner consistent with the level of care and skill ordinarily exercised by members of our profession currently practicing under similar conditions in this area of California. No other warranty is expressed or implied. Should you have any questions or comments regarding this document, please contact the undersigned at your convenience. Sincerely, Earth Systems Pacific 7 tr_ Timothy Conroy, CEG Associate Geologist Attachments Copy to Doc. No Vicinity Map Boring Location Map Lead Concentration Maps: 1-,2- and 3-Foot Depths Laboratory Reports San Luis Obispo City Fire Department, Attn.: Mr. Kerry Boyle 1505-068.1TR/sr No.1698 CEHTIFIED ST oo o rr FcR VICINITY MAP Rademacher Property 539 Marsh Street San Luis Obispo, California D.Im Ymtd\ lm 0{C0 sunc Dn: US$ f__l S0 n Srh: I : C,m Dd} l,t! hG WCS4 Earth SvstemeProject No. SL-17 522-EA s Pacific May 201 5 HA-10 + Addition to Structure LEGEND Boring Location (APProx') Fenceline PropertY Boundary ATI ON MAP STREET Earth SYstems Pac +*- oc'c (Do N ()o IFUUttsa xav o e MaY 7, 2015 po, California o 39 co 4)o coocoo!ooit 6O I Uuu a TaG or) 6 Addition to Structure LEGEND HA-10 +Boring Location (ApProx.) Property Boundary (200) Total Lead, mg/kg - Estimated Extent of Total Lead in soil > 200 mg/kg NS 1.FOOT DEPTH Earth Systems Pacific STREETe May 14,2O15 California o =9 co't o co Coooo9 o nO ItsUUMF U) IaM on Addition to Structure LEGEND HA-10 +Boring Location (Approx.) --_..--_o- Fenceline Property Boundary (200) Total Lead, mg/kg - fstirylated Extent of Total Lead in soil z 200 mg/kg * No data at this dePth )NS,2.FOOT DEPTH Earth Systems Pacific STREET May 14,2015 r, California o =c co o coocoo oo lr) no IFUUuts LA Ta( o ts) 6 Addition to Structure HA-10 + Boring Location (Approx.) -+-..._o--..- Fenceline Property Boundary (200) Total Lead, mg/kg )NS 3-FOOT DEPTH Earth Systems Pacific STREET May 14,2O15 t, California Oilfield Environmental and Compliance, lNC. Tim Conroy Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo, CA 93401 30 April 2015 RE: 539 Marsh St, SLO Work Order: 1501538 Dear Client: Enclosed is an analytical report for the above referenced project. The samples included in this report were received on 09-Apr-1516:25 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analyticaltesting was accomplished in accordance with the guidelines established in our Quality Assurance Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. lf you have any questions regarding this report, please do not hesitate to contact the undersigned. Sincerely, @ 14 ;+ Ankita Kashyap Project Manager TEL: (805) 922-4772 FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com Oiffield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 l2:30 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received HA-2 @33-36" HA-3 @ 33-36" HA-s @9-12" HA-5 @2t-24" HA-6 @9-12" HA-6 @21-24" HA-7 @9-12" HA-7 @21-24" HA-& @9-t2" HA-g @21-24" HA-9 @9-12" HA-9 @2r-24" HA-10 @9-t2" HA-10 @21-24" I 50 I 538-01 I 50 I 538-02 l 501 538-03 1 50 I 538-04 I 501 538-05 r 50 I 538-06 I 50 I 538-07 1 501 538-08 l 50 I 538-09 I 50 I 538-10 1501538-11 1501538-12 1501538-13 l s0 1 538- l4 Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid Solid 03-Feb-15 ll:00 03-Feb-15 12:11 08-Apr-15 09:17 08-Apr-15 09:26 08-Apr-15 10:08 08-Apr-15 l0:20 08-Apr-15 1l:07 08-Apr-15 11:29 08-Apr-15 l2:36 08-Apr-15 12:45 08-Apr-15 13:ll 08-Apr-15 13:19 08-Apr-15 l4:03 08-Apr-15 l4:18 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 l6:25 09-Apr-15 16:25 09-Apr-15 16:25 09-Apr-15 l6:25 09-Apr-15 l6:25 09-Apr-15 16:25 09-Apr-15 l6:25 Oilfield Environmental and Compliance The results in this report dpply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page2 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number : SL-17 522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 12:30 HA-z @33-36" 1501s38-01 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofcl Mefnls hv EPA 6000/7000 Series Mefhods Lead 11 0.46 mg/kg I 85D0359 l3-Apr-15 l5-Apr-15 EPA60I0B HA-3 @ 33-36" 1s01s38-02 (Solid) Analyte Result Reporting l,rmrt Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofel Mefels hv FI,PA 6000/7000 Series Mefhods Lead r90 0.47 mg/kg I 85D0359 13-Apr-15 l5-Apr-15 EPA60l0B N-02, N-03 HA-s @9-12" 1501s38-03 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofnl Mefels hv EPA 6000/7000 Series Methods Lead STLC Mefels hv 6000/7000 Series Methotls 0.49 mg/kg I B5D0359 l3-Apr-15 15-Apr-15 EPA60I0B N-0289 Lead 6.9 0.050 mg/L I 85D0820 27-Apr-15 29-Apr-15 STLC/EPA 60108 N-07 Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL:(805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 3 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number : SL-77 522-E A Project Manager: Tim Conroy Reported: 30-Apr-15 12:30 HA-s @ 2r-24" 1501s38-04 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofal Mefals hv tr]PA 6000/7000 Mpfhnds Lead 31 0.46 mg/kg I BsD0359 13-Apr-15 15-Apr-15 EPA60I0B HL-6 @9-12" 1501538-05 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofnl Mefcls hv T',PA 6000/7000 Mslhndc Lead 200 0.48 mg/kg 1 B5D0398 l4-Apr-15 15-Apr-15 EPA 60108 N-02, N-03 IJL-6 @21-24" 1s01s38-06 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhods Lead 17 0.48 mg/kg I 85D0398 l4-Apr-15 l5-Apr-15 EPA60l0B H.A-7 @9-t2" 1501s38-07 (Solid) Analyte Result Renortins'Limii Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofel Metals hv EPA 6000/7000 Mefhods Lead 200 0.48 mg/kg I B5D0398 14-Apr-15 l5-Apr-15 EPA60l0B N-02, N-03 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 4 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Numbe r : SL- 17 522-EA Pro_ject Manager: Tim Conroy Reported: 30-Apr-15 l2:30 IJA-1 @21-24" 1s01538-08 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofal Mefals hv EPA 6000/7000 ries Mefhnds Lead 20 0.47 mg/kg I B5D0398 l4-Apr-15 l5-Apr-15 EPA60I0B }JA-g @9-12" 1s01s38-09 (Solid) Analyte Result Reoortins'Limii Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tnfnl Mefels hv ['.PA 6000/7000 Series Mefhods Lead 5l 0.49 mg/kg 1 85D0398 l4-Apr-15 l5-Apr-15 EPA60I0B N-02 STLC Mefnls hv 6000/7000 Se Mpfhnds Lead 1.5 0.050 mg/L I 85D0820 27-Apr-15 29-Apr-15 STLC/EPA 6010B HA-8 @ 2t-24" 1s01s38-10 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhnds Lead 9.1 0.46 mg/kg I 85D0398 l4-Apr-15 15-Apr-15 EPA60l0B Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical reporl must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 5 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project: 539 Marsh St, SLO Project Number : SL-17 522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 l2:30 H.A-9 @9-t2" rs01538-11 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhods Lead 1000 0.47 mg/kg I BsD0436 15-Apr-15 l5-Apr-15 EPA6010B N-01,N-03 T(-LP Mefrls hv 6O00/7000 Mathndc Lead 0.087 0.050 mglL I BsD0732 23-Apr-15 23-Apr-15 IJA-9 @21-24" 1501538-12 (Solid) EPA I3IUEPA 60i08 Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 es Mefhnds Lead 640 0.50 mg/kg I B5D0436 l5-Apr-15 l5-Apr-15 EPA60l0B N-02,N-03 HA-10 @9-12" 1s01s38-13 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Tofal Metals bv EPA 6000i7000 es Mefhnds Lead 57 0.48 mg/kg I B5D0436 15-Apr-15 l5-Apr-15 EPA 6010B N-02 STLC Metals hv 6000/7000 Mpfhods Lead 2.0 0.050 mglL 1 85D0820 27-Apr-15 29-Apr-15 STLC/EPA 60108 Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its enlirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 6 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 12:30 HA-10 @2t-24" 1s01538-14 (Solid) Analyte Result *"O"fliil$ Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA 6000/7000 Mefhnds Lead 54 0.49 mC/kC t 85D0436 l5-Apr-15 l5-Apr-15 EPA60I0B N-02 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirely. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 PageT of12 Oilfield Environmental and Compliance, lNC. Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 12:30 Total Metals by EPA 6000/7000 Series Methods - Quality Control Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Batch B5D0359 - EPA 30508 Blank (85D0359-BLK1)Prepared: l3-Apr-l 5 Analyzed:15-Apr-15 Lead ND 0.50 mdkg LCS (85D0359-BSl)Prepared: 13-Apr-l 5 Analyzed:15-Apr-15 Lead ll4 0.50 mclkq 100 114 80-120 LCS Dup (85D0359-BSDI)Prepared: l3-Apr-15 Analyzed:I 5-Apr- 15 Lead Duplicate (B5D0359-DUPI) lll 0.50 mdkC Source:1501536-01 100 lll 80-120 2.40 Prepared: l3-Apr-15 Analyzed: I 5-Apr-15 20 Lead Matrix Spike (85D0359-MS1) 1.96 0.46 mdkC Source:1501536-01 2.55 26.2 Prepared: l3-Apr-l 5 Analyzed: l5-Apr-15 20 QR-04 Lead Matrix Spike Dup (85D0359-MSDl) 90.9 0.47 mdkc Source: 1501536-01 94.3 2.55 93.7 65-119 Prepared: l3-Apr-15 Analyzed: l5-Apr-15 Lead Batch 85D0398 - EPA 30508 84.9 0.46 mdkC 91.3 2.s5 90.2 6s-ll9 6.80 20 Blank (85D0398-BLKI)Prepared: l4-Apr- 15 Analyzed:l5-Apr- l5 Lead ND 0.50 mdkg LCS (85D0398-BSl)Prepared: l4-Apr-15 Analyzed:l5-Apr-15 Lead LCS Dup (85D0398-BSDI) 102 0.50 m9lk9 100 102 80-120 Prepared: l4-Apr-15 Analyzed: l5-Apr-15 Lead 108 0.50 mdkg 100 108 80-120 5.23 20 Oilfield Environmental and Compliance The results in this report apply to lhe sd,nples analyzed in accordance with the chain of custody document. This andlytical report must be reproduced in its entirety. TEL:(805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 8 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-l7 522-E A Project Manager: Tim Conroy Reported: 30-Apr-15 l2:30 Total Metals by EPA 6000/7000 Series Methods - Quality Control Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Batch 85D0398 - EPA 30508 Duplicate (85D0398-DUPI)Source: 1501530-01 Prepared: 14-Apr-l5Analyzed:15-Apr-15 Lead Matrix Spike (B5D0398-MS1) 2.93 0.50 mdkg Source: 1501530-01 Prepared: l4-Apr-15 Analyzed:15-Apr-15 7.28 85.3 20 QR-04 Lead 93.6 0.46 mdkg Source: 1501530-01 92.4 '1 .28 93,4 65-119 Matrix Spike Dup (85D0398-MSDI Prepared: l4-Apr-15 Analyzed:I 5-Apr- I 5 Lead Batch 85D0436 - EPA 30508 99.7 0.49 mdkC 97.2 7.28 9s.l 65-119 6.30 20 Blank (85D0436-BLKI)Prepared & Analyzed: 15-Apr-15 Lead LCS (85D0436-BS1) ND 0.50 mdkg Prepared & Analyzed: 15-Apr-15 Lead LCS Dup (B5D0436-BSD1) ll3 0,50 mdkc 100 113 80-120 Prepared & Analyzed: 15-Apr-15 Lead Duplicate (85D0436-DUPI) I l0 0.50 mg/kC Source:1501582-01 100 ll0 80-120 Prepared & Analyzed: 15-Apr-15 2.51 20 Lead Matrix Spike (85D0436-MSl) 2.95 0.46 ms/kg Source: 1501582-01 3.00 Prepared & Analyzed: l5-Apr-15 1.69 20 Lead 104 0.49 mdkg Source: 150f582-01 98.5 3.00 102 65-l 19 Matrix Spike Dup (B5D0436-MSDI Prepared & Analyzed: l5-Apr-15 Lead 99.1 0.47 mg/kC 94.5 3.00 102 65-119 4.48 20 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 9 of 12 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number : SL-l7 522-EA Pro-lect Manager: Tim Conroy Reported: 30-Apr-15 l2:30 STLC Metals by 6000/7000 Series Methods - Quality Control Result Reporting Limit Units Spike Level Source Result %REC %REC l,imits RPD RPD Limit Notes Batch 85D0820 - EPA 3050B Leachate Blank (85D0820-BLKI)Prepared: 27 - Apr-l 5 Analyzed:29-Apr-15 Lead LCS (85D0820-BS1) ND 0.050 mslL Prepared: 27 - Apr-l 5 Analyzed:29-Apr-15 Lead LCS Dup (B5D0820-BSDr) 960 0.050 mglL 10.0 96.0 80-120 Prepared: 27 -Apr-15 Analyzed: 29-Apr- I 5 Lead Duplicate (85D0820-DUP1) 10.0 0.050 mglL Source: 150f538-03 10.0 100 80-120 4.38 20 Prepared: 27 - Apr-l 5 Analyzed:29-Aor-15 Lead Matrix Spike (85D0820-MSf ) 7.01 0.050 mE/L Source: 1501538-03 Prepared: 27 - Apr-15 Analyzed:29-Aor-15 6.90 1.51 20 Lead 16.6 0.050 mgfl- Source: 1501538-03 10.0 6.90 96.9 7s-125 Matrix Soike Dup G5D0820-MSD Prepared: 27 - Apr-l 5 Analyzed:29-Aor-15 Lead 16.2 0.050 mslL l0.0 6.90 92.8 7s-125 2.47 20 Oilfield Environmental and Compliance The results in this report apply to the samples dnaly:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page l0 of 12 Oilfield Environmental and Compliance, lNC. Ea(h Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 12:30 TCLP Metals by 6000/7000 Series Methods - Quality Control Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Batch 85D0732 - EPA 3050B Leachate Blank (85D0732-BLK1)Prepared & Analyzed: 23-Apr- I 5 Lead LCS (85D0732-BS1) ND 0.050 mgI, Prepared & Analyzed: 23-Apr-15 Lead LCS Dup (85D0732-BSDI) 9.80 0.050 mg/L 10.0 98.0 80-120 Prepared & Analyzed: 23-Apr-15 Lead 9.55 0.050 mgtL Source: 1501538-11 10.0 95.s 80-120 Prepared & Analyzed: 23-Apr-15 2.63 20 Duplicate (85D0732-DUPl Lead Matrix Spike (85D0732-MSI 0.0760 0.0s0 mslL Source:1501538-11 0.0870 Prepared & Analyzed: 23-Apr-15 13.5 20 Lead Matrix Spike Dup (85D0732-MSD 1) 9.94 0.050 mglL Source:1501538-11 10.0 0.0870 98.6 '15-125 Prepared & Analyzed: 23-Apr-15 Lead 9.38 0.0s0 mC/L 10.0 0.0870 92.9 75-125 5.85 20 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL:(805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page ll of12 Oilfield Environmental and Compliance, INC QR-04 N-07 N-03 N-02 N-01 DET ND NR dry RPD Notes and Definitions The RPD exceeded the QC control limits. STLC analyte concentration exceeds STLC limit. Analyte concentration above 20x TCLP. Analyte concentration below TTLC but above 10x STLC Analyte concentration exceeds TTLC. Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: Tim Conroy Reported: 30-Apr-15 12:30 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety' TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 12 of 12 Oilfield Environmental and Compliance Revo6201z 307 RoemerWay, Santa Maria CA. 93454 101 Adkisson UYay, Tafi, GA 93268 phone: (S05) 9224772 fax (805) 92+3376 $t{w.oecusa.com ' phbne: {001} 762;914i} CHAIN OF CUSTODY Page i of La.rlo,u, Jrcs f..3q fufiKL Jt flD sire: SL-J ?S >{^eft' Speciat Instruciions: Comments/P0* Analysis Requested * Matrix Key A= vapor/ air S=solid/ssdiment P=product/oil HW = hz r.raste tuq) WATERTypes: DW= drinking 9161 = ground p51= poduced SW = surface WW=wasb Proiec.t Namef#: I Date:Time: Time: Date: Date:I Date: Date:Time: [czs -s€\ rl tbtr'v X Y Xxx X X X K XY 3 Fax:E-mail: To:Sampler: via- FAX-PDF-Geotracker EDF-EDD- 10 5 Days-72 hr-48 hr-24er-ASAP- Glient Sample lD H*-L A 33- 3A" t]*4@fi*,Lo l-l,h-€ra, 4- tzu r**- Sp- ft zt+:+tt \> # h' L e. 4 -tl-' l*A-bo,, ?A *+v uA -7 re- 4.- l.>" Fn -7 @- 7t -y7u U-A -E Q.4- l7o t'+A .f, p, >t ->'{u lrlA*1 @ 4-tT'l t+A 4 &V14*rv #of Cont. / I I I I I I I I I I I Matrix* (see key) s _{ c\) s a\) c\) 4s s f Date/Time Sampled ILLI bq,I'7 b4b icoP. Lo?P itnl. I.LL1 tLlb IALT{ lJ tl ttitl fslrS { Y Tumaround Time Oilfield Environmental and Gompliance 307 RoemerWay, Santa Maria GA 93454 phone: (8051922-4772 fax (80$ 925'3376 www.oecusa.com ' Rev062012 ' 101 Adkisson Way, Taft, GA 93268 phone: (661)762-9,143 CHAIN OF GUSTODY a a Page of Special lnstructions: Gomments/PG: sLb',p-{ - {at lhhRh, s Matrix Key A= vapor/ air S =sofrd /sediment P = prsduc{/ oil HW = hazwaste (Liq.) WATERTyp6: DW= ddnkins 651=gound PW = prcduced sl,!= suqce WW=waste 774 X Proieet Namel#: / * 6t-- l7.T 7?"e4Site: Analysis Requested \>(s \ A rb [+) X-[t* -tD e f^i>o Client Sample lD \I-A-LD O U-7't" #ot Cont. I I Turnaround Time 10 Days-72ht-Vlhr-ASAP.48 hr-5 Date: Matri:C* (see key) .s s Time:Date: tftT- tro-} \tr2<1-t Time: Time: Time:Date: f,late: Tirne:Date:By: Gitv/State/ZP: eoo- D E+nail:Fax: PDF. ILTo: Geotacker EDF- Samplen reportvia- FAX- AMPLE RECEIPT CLIENT: eO"r}l\' 8f tt* F*-c-.r s- RECEIPTLOGIN .4.rsq l6 5ZDATE/TIME:.{ OECID*: t:-d.rtK3F Temp:q oc AcceptableRange ooc to 6oC x Rex 0U5n0 COCRECETYEI) DATE/TIME:Lt -a.r<€!.tY){REFRIGERATOR(s): irfq Yes No El fl*E[*K[* &[+ E** trtrtrtr[xtr rE* N/A tr tr tr tr fl R EK (*) PROBLEM CHAIN FORM NEEIEI) Custody Seals (circle): Present/ Ot'tl \r-rl Samples / Coolers Intact / Broken* Method of Shipment & Tracking #(ifapplicable): Samples Received Outside Temp. Range* Container label(s) consistent\rith COC El Samples Direct from fibld (Outside Temp) OEC preservative added (**note std ID) E After-Ho1rs Outside Drop-off[Brought Inside] Proper preservation on sample label(s) PRESERVATION:SAMPLE TRANSPORT, RECETPT, CONDmON & Samples Received on IceFtr VOA containers fiee of headsPace(Initials/Dateffime): tee of 1+*; OEC Preservative ID: Dissolved Metals Filtration: (Date/Inil/&esena ID) COC docunnent(s) received wittr samples Correct containers foranalysis requested Containe(s) intact and in good condition Elonc Courier/sampler Q OefiverylOther than OEC Cornier) CoNTArI\ERS, COC CTTANGES AllD/OR CORRECTIONS CHANGES AUTIIORIZED BY: Comments /Remarks / Condition Notes. Etc. Date/Time Sampled ***Mafrix .)- ResCl /nH PreservativeContainer Description 1-Tt*6e- EA Client ID ***If blanh referto cocOEC ID /- t7 t2 RJECEIPT I-OGIN BY:RECEIPT RE\IE\ilED BY:d p"e" f or f Oilfield Environmental and Gompliance 307 Roemer Way, Santa Maria GA 93454 phone: (80519224772 laxz (S05) 92$3376 wv/w.oecusa.com Rev062012 101 Adkisson Way, Taft, CA 93268 phone: (661) 762-9143 CHAIN OF CUSTODY e"s.l*L Special lnstructions AaaA on q(zz-[6 Yrd.tent @ Gomments/PO#:* Matrix Key A= vapor/ air S=solid/sedlment P=prcduc{/oil HW = hazwasG (Llq.) WATER Types: DW = drinkirE cW =gromd pW = produced SW = surfac€ llltw=mste A _o+q ,QF- A A A GY Cu X >( X X X X V >2^ Name/#: 7 Analysis Requested -aG\ atIt "br- x Y X Xx Za.tl B;+1* TseRzr-v+uP hA1e,9-1.>" tH-7 @ Lt -yf Lt-A -6 P,4- 17" >t ->'+"lrA 4 ,o, /4A-1 @ 4-ttt vl+A 4 &74+t 5 Days-10 Days- Client Sample lD hr- Dateflime SamPled EDD.Geotracker EDF- 48 hr-ASAP-24 hr- #of Gont. Matrlx* (see key) Il.ft-L e 3J- Ab" tt*4@a3-TLo l-/^ ,h-€ e. I - tzu ilh-Le.4a>" t*A-be- ?A 2+v I I I I I / I I I I I I 2-KtI Date: Date: S o$ 4 i'! fS s a\) f oxl'7 bfib luLl 'bD8: Date:Time: Time: loZP ttrt I.n-1 tL7L taLl{ lb tl r t\l1v ,lais .l Time:Date: Time:Date:By: E-rnail:Fax= via- FA)(-PDF. Turnaround Time Oilfield Environmental and Compliance 307 Roemer Way, Santa Maria CA 93454 phone: (S05) 922-4772 tax: (S05) 925-3376 www,oecusa.com . Rev 062012 ,l01 Adkisson Way, Tafi, CA 93268 phone: (66r) 762-9143 CHAIN OF CUSTODY ofPage ,e.r - d\q funsb. f* SLb Site:6l-- l?.T *^'€* Special lnstructionsr Comments/Po#: Analysis Requested i* Matrix Key A = vapor/ air S=solid/sedlment P=product/oil HW = hazu/aste (Liq.) WATERTYpeS; DW = drinking GW = ground PW = produced SW = surface Ywl/=mite t, Proiect Name/#: I Date:Time: Date: Date:Time: Daie:Time:q \L?'?-< _sq- CJ -Fu) A -s(\ \rl rI X X (- Gity/StatelZlP: Fax:E-mail: To: report via- FAX-PDF.Geotracker EDF-EDD. N Turnaround Tlme 10 Days-5 Days-72ht-48 hr-24hr-ASAP. Client Sample lD tf{. -D e t^i>' l+A*LD A u->+" #of Gont. I I Matrix* (see key) t s Date/Tlme Sampled 4k{r- ms vlxl'(- t+tR Time: Time: Date: Received By: Received leceived Date: Oilfield Environmental and Compliance, INC Tim Conroy Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo, CA 93401 29 April 2015 RE: 539 Marsh St, SLO Work Order: 1501742 Dear Client: Enclosed is an analytical report for the above referenced project. The samples included in this report were received on 22-Apr-15 15:54 and analyzed in accordance with the attached chain-of-custody. Unless othenarise noted, all analyticaltesting was accomplished in accordance with the guidelines established in our Quality Assurance Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. lf you have any questions regarding this report, please do not hesitate to contact the undersigned. Sincerely, Meredith Sprister Project Manager TEL: (805) 922-4772 FAX: (805)925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.Gom Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-77 522-EA Project Manager: Tim Conroy Reported: 29-Apr-15 16:26 ANALYTICAL REPORT FOR SAMPLES ID ID Matrix Date Sampled Date Received HA-9 @33-36 l50t'742-01 Solid 08-Apr-15 13:31 22-Apr-15 15:54 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance wilh the chain of custady document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 2 of 5 Oilfield Environmental and Compliance, INC Earth Systems Pacifrc 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: Tim Conroy Reported: 29-Apr-75 16:26 IJA-9 @33-36" ls0l7 42-01(Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Metals bv EPA Series Mefhods Lead 90 0.25 mg/kg I B5D0720 23-Apr-15 23-Apr-15 EPA60I0B N-02 Oilfield Environmental and Compliance The results in this report apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 3 of 5 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Numbe r : SL-17 522-E A Project Manager: Tim Conroy Reported: 29-Apr-15 16:26 Total Metals by EPA 6000/7000 Series Methods - Quality Control Reporting Spike Level Source Result %REC %REC Limits RPD LimitAnalyteResultLimit Units RPD Notes Batch 85D0720 - EPA 30508 Blank (85D0720-BLKI)Prepared & Analyzed: 23-Apr- I 5 Lead ND 0.25 mdkC LCS (B5D0720-BSI)Prepared & Analyzed: 23-Apr-15 Lead LCS Dup (85D0720-BSDI) 97.0 0.25 mC/kC 100 97.0 80-120 Prepared & Analyzed: 23-Apr-l 5 Lead Duplicate (85D0720-DUPI) 98.8 0.25 mdkC Source: 1501740-0f 100 98.8 80-120 Prepared & Analyzed: 23-Apr-15 L'19 20 Lead Matrix Spike (85D0720-MS1) 4.39 0.25 mC/kg Source: 1501740-01 4.04 Prepared & Analyzed: 23-Apr-15 8.34 20 Lead 86. I 0.23 mdkC 92.2 4.04 89.1 65-119 Oilfield Environmental and Compliance The results in this report apply to the sdmples analy=ed in accordance with the chaih of custody document. This analytical report must be reproduced in its entirety. TEL: (805) 922-4772 805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 ww\ t.oecusa.com FAX:( Page 4 of 5 Oilfield Environmental and Compliance, INC N-02 DET ND NR dry RPD Notes and Definitions Analyte concentration below TTLC but above l0x STLC. Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: Tim Conroy Reported: 29-Apr-15 16:26 Oilfield Environmental and Compliance The results in this reporl apply to the samples analy:ed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. TEL:(805) 922-4772www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 5 of5 Oilfield Environmental and Compliance ' Rdv0620l2 . 101 Adkisson Way, Taft; CA 93268 phone: (66{}762:914} CHAIN OF CUSTODY 307 RoemerWay, $anta Maria CA 93454 phone: (805)9224772 fax (805)925.3376 wwllv.oecusa,com 'f Page Special lnstructions: Gommenis/PO#: tt-. Sw *MatrixKey.. A= vapor / air S=Eolid/sediment P = producti ofl HW =hazwasle (Uq.) WATER Types: DW = drinking . Glff=ground pW = produced SW= surface WW=$asle X '6L -tV,{>Z -a#Proiect ttame/ih' QLSite:\ )-) Analysis Requested Ffl $t *tY- FeGlient Sample lD il+-?e{a&bo #of Gont. Is Matrix"* (see key) +a*lr*t Dateffime Sampled L tRs rime: lLLqbC0oate:1. .?-2- t<' Tirne: \Date: Time: \ssL Date: Date:k.?Z-( ts rime: I Oate: V +t-*-fsoo,", lS tt-PCity/StatelZlP: 72hr- E-mail:Fax: 510 Days- flTurharound Time EDO. ASAP- Geotracker EDF- 48 hr-24hr- To: report via- FAX- RECEIPT CLIENT: trAr+h gfirnsggg RECEIPTLOGIN DATE/TIME:4.L2-tse-tG.i,) rD #: l50 ' f "tL Temp:39 "c Acceptable Rmge:OoC to 6oC COCRECETYEI) Rsv.0vr5n0 r{A2-ts.Q t sYY REFRIGERAToR(s):XDATE/TIME: Comments / Ramarks / Coudition Notes, Etc. DatelTime Samoled ***Matrix \ ResC[. /pH 'PreservativeContain€r Description 4=l^-o C[ent ID ***ffblank refer to CoC E Samples Received Outside Temp. Range* Container labe(s) consistent with COC EI Samples Direct from field (Outside Temp) OEC preservative added (**note std ID) E After-Hours Outside Drop.off[Brought kside] Proper preservation on sample labe(s) Yes E E R ET EI** n tr tr No fl* ll*'['r fl* n tr N/A n tr tr tr FF El-E PRESERVATIOFT:SAMPLE IRAI{SPORT, RECEIPT, COFIDmON & freeTedlar Samples / (*)PROBLEMCHArN VOA containers free of headspace(Initials/Dateffime): (**) OEC Preservative ID: . Dissolved Metals Filtation {DaterlniD?resenc ID) Intact I Broken* Method of Shipment & Tracking #.lif applicable): Custo{v Seals (bircle): PresentCOC docurnen(s) received with samples Correct containers for analysis reqpested Container(s) intact aad in good condition Kosc Courier/Sampler EI De[very(Otler than oEC Courier) lsamples Received on Ice C0NTATNERS, COC CTTaNGES AND/0R BY:CHANGESCORRECTIONS OEC ID )b" RECEIPT LOGIN BY:RECEIPT REVIEWED BY:@ Pags -of Oilfield Environmental and Compliance, INC Tim Conroy Earth Systems Pacific 4378 Old Santa Fe Rd, San Luis Obispo, CA 93401 19 February 2015 RE: 539 Marsh St, SLO Work Order: 1500466 Dear Client: Enclosed is an analytical report for the above referenced project. The samples included in this report were received on 03-Feb-15 1 5:10 and analyzed in accordance with the attached chain-of-custody. Unless otherwise noted, all analyticaltesting was accomplished in accordance with the guidelines established in our Quality Assurance Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety. lf you have any questions regarding this report, please do not hesitate to contact the undersigned. Sincerely, ' /' l " /.:,..,. t,t,... r,,t,J::l:;\.,,1.,..:r i1 :. c- Meredith Sprister Project Manager TEL:(805) 922.4772 FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.Gom Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Projecil 539 Marsh St, SLO Project Number: SL-17522-EA Project Manager: Tim Conroy Rcported: l9-Feb-15 l6:07 ANALYTICAL REPORT FOR SAMPLES ID Laboratory ID Matrix Datc Datc Received HA-l/9-12' HA-l/30-36" HA-2/9-12" HA-3i9-12" FIA-4/9-12" HA-4/33-36" I 500466-01 I 500466-02 I 500466-03 I 500466-04 I 500466-05 I 500466-06 Solid Sotid Solid Solid Solid Solid 03-Feb-15 09:42 03-Feb-15 l0:01 03-Feb-15 l0:19 03-Feb-15 lt:30 03-Feb-15 l2:20 03-Feb-15 l2:41 03-Feb-15 l5:10 03-Feb-15 l5:10 03-Feb-15 l5:10 03-Feb-15 l5:10 03-Feb-15 15:10 03-Feb-15 l5:10 Oilfi eld Environmental and Compliance The results in this report apply to the satnples atnlyzed in accordance with the chain of custody docunreil. This analytical repofi m{sl be reproduced in its entircly, TEL: (805) 922-4772wwrrv.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page2 of 12 Oitfield Environmental and Compliance, INC Earth Systerns Pacific 4378 Otd Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17522-EA Project Manager: Tim Conroy Reported: l9-Feb-I5 l6:0? HA-1/9-12" rs00466-01 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance Total Mefnls trv EPA 6000/7000 Saries Methods Cadmium Chromium Lcad Nickel Zinc STLC Metals bv 6000/7000 Series Methods 1,4 99 B9 130 130 0.23 0.46 0.46 0.23 0.91 mg/kg It lt B5B0l47 05-Feb-15 05-Feb-t5 EPA60l0B N-02 N-02 Lcad TEPH hv (l(l FID 7.0 0.050 m{L I BiBo488 l7-Feb-15 l?-Feb-I5 STLC/EPA 60IOB N-07 TPI-I Diesel (Cl3-C22) TPH Motor Oil (C23-C40) ND ND l0 meikg 50n B5B0l40 05-Feb-15 05-Feb-t5 EPA80l5M Surrogate : o -Terpheny I t04% 6t-t42 IIA-1/30-36" 1500466-02 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance TEPH bv GC FTD TPFI Diesel (Cl3-C22) TPH Motor Oil(c23-C40) ND IO ND 50 mgkg I B5B0l40 05-Feb-15 05-Feb-15 EPA80l.sM Su rroga te : o -TbrP he nY I t0t % 6l-142 Oilfield Environmental and Compliance The results in thit rcpo,'t apply to ilte samples analy:ed in accordance with the chain of ctrstody document, This analytical repofi must be reproduced in its entirety. TEL: (805) 922-4772wwur.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, santa Maria, cA 93454 Page 3 of 12 Oilfield Environmental and Compliance, INC Earth Systens Pacific 4378 Old Santa Fe i{d. San Luis Obispo CA, 93401 Project: 5i9 Marsh St, SLO Project Number: SL-17522-EA Project Manager: Tim Conroy Rcported: 19-Feb-15 16:07 tr&-?t9-L2" 1500466-03 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Gompliance Tnfel Mcfals hv E.PA Knn0l7n0n Scrias Mefhnds Cadmiunr Chromium Lcad Nickel Zinc STLC Mafels hv 6OOO/7IIOO Soripc Mafhndc 3.0 140 380 150 700 0.24 0.48 0.48 0.24 0.96 mdkc il I B5B0l47 05-Feb-15 05-Feb-15 EPA60108 N-02, N-03 N-02, N-03 Lead TCLP Mntqls hv 6OOO/7OOO Sarins Mcfhods 0.050 mg/L I B5Bo488 l7-Feb-1516 l?-Feb-15 STLC/EPA 60108 N-07 Lead TEPH bv GC FID ND 0.050 mg/L I B5B0s66 t9-Feb-15 l9-Feb-ls EPA l3l l/EPA 60r0B TPH Diesel (C13.C22) TPII Motor Oil (C23-C40) 46 330 l0 mg/kg 50tr I B5B0l40 05-Feb-15 05-Feb-15 EPAS0lsM Snrrogale : o-Terphenyl ra4% 6r-t42 Oilfield Environmental and Compliance The resilts itt this report apply to the samples analy:ed in accotdance vilh the chain af custody document, This analytical t'eport must be rcproduced in its entircty, TEL: (805) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Pagc 4 of 12 Oilfield Environmentat and Compliance, INC Earth Systenrs Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project 539 Marsh St, SLO Project Number: SL-17 522-EA Project Manager: f im Conroy Reported: l9-Feb-15 l6:07 HA-319-t2'l 1500466-04 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Gompliance Tofrl Mofclc hw f,'.PA 600O/7O00 Snricc Mafhnds Cadmium Chromium Lead Nickel Zinc STLC Mctals bv 6000/7000 Series Methods 5.0 140 st0 150 310 0.23 a.46 0.46 0.23 0.92 mc/kg tr I B5B0l47 05-Feb-15 0S-Feb-15 EPA60l0B N-02, N-03 N-02, N-03 Lcad TCLP Metals bv 6000/7000 Series Methods 27 0.050 mg/L I 8580488 l7-Feb-15 l7-Feb-15 STLC/EPA 60108 N-07 kad TEPH bv GC FTD ND 0.050 mg/L r 8580566 t9-Feb-15 l9-Fcb-15 EPA r3r tiEPA 60108 TPH Diesel (Cl3-C22) TPII Motor Oil (C23-C40) ND 170 l0 mg/kg 50n I B5B0l40 05-Feb-15 05-Feb-15 EPA80l5M Surrogate : o-Terphe nyl t06% 6r-t42 Oilfield Environmental and Compliance The results in this report apply to the sanplas analy:ed in accordance with the chain o! custody document, This analytical report rlaus! be reproduced in its entirety. TEL:(805) 922-4772www.oecusa.com FAXr (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 5 of l2 Oilfield Environmental and Compliance, INC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project; 539 Marsh St, SLO Project Nunrber: SL-17522-EA Project Manager: Tim Conroy Reported: l9-Feb-15 16:07 HA-4t9-r?t' 1s00466-05 (Solid) Analyte Result O"O"flififr Units Dilution Batch Prepared Analyzed lv{ethod Notes Oilfield Environmental and Compliance Total Metals bv 8P.4.6000/7000 Series Methods Cadmium Chromiunr Lcad Nickel Zlnc TEPI{ hv GC FII) 0.97 160 31 r50 57 a.23 0.47 0.47 4.23 0.94 mg/kC 0 B5B0l47 Os-Feb-I5 05-Feb-15 EPA60l0B N-02, N-03 TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) ND ND l0 rng/kg 50il I B5B0l40 05-Feb-15 05-Feb-t5 EPA80l5M Surrogate : o-Terphe nyl r02% 6t-r42 IIA-4/33-36" 1500466-06 (Solid) Analyte Result Units Dilution Batch Prepared Analyzed Method Notes Oilfield Environmental and Compliance TF,PH hv GC FII) TPH Diesel (Cl3-C22) TPH Motor Oil (C23-C40) ND ND l0 mgks 50 '|, I B5B0l40 05-Feb-15 05-Feb-15 EPAS0lslvl Surrogate : o -Terphe nyl 104 % 6l-142 Oilfietd Environmental and Compliance The results in thit report apply to the sauples analy:ed in accordance with the chain of custody dontmenl'l'his analytical report ntust be reproduced in its ehlircty. TEL: (80s) 922-4712www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 6 of 12 t- Oilfield Environmental and Compliance. INC Earth Systerns Pacific 4378 Otd Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL-17522-EA Project Manager: 'firn Conroy Reported: 19-Feb-15 l6;07 Total Metals by EPA 6000/7000 Series Methods - Qualify Control Reporting Spike Level Source Result %REC Limits RPD LimitAnatyteResultLimit Units %REC RPD Notes Batch 8580147 - EPA 30508 Blank (B5It0l47-BLKI)Prepared & Analyzed: 05-Feb-15 Cadmium Chromium Lead Nickel Zinc ND ND ND ND ND 0.25 0.50 0.50 0.25 1,0 mS/kg Prepared & Analvzed: 05-Feb-15LCS (BsBol47-BS1) Cadmium Chromium Lead Nickel Zinc 97.3 103 97.1 100 98.0 0.2s 0.50 0.50 0.25 1.0 mS/kg 100 100 100 t00 100 97.3 103 97.1 t00 98.0 80-120 80-120 80-120 80-120 80-t20 LCS Dup (8580147-BSDr)Prepared & Analyzed: 05-Feb-15 Cadmium Chromium Lead Nickel Zinc 98.0 t0s 98.1 l0l 98.4 0.2s 0.s0 0.50 0.25 1.0 mg/kg 100 100 100 100 100 98.0 105 98, I l0l 98.4 80-120 80-120 80-120 80- I 20 80- 120 0.7 t7 1.68 1.02 0.748 0.509 20 20 20 20 20 Dunlicatc (8580 147-DUPI)Source: 1500387-07 Prepared & Analyzed: 05-Fcb-15 Cadmium Chromium Lead Nickel Ziac 0.389 9.51 10.9 8.62 41.3 0.23 0.4'l 0.47 0.23 0.94 nrg/kg 0.484 8.90 8.98 43.1 21.8 ll.2 19.9 4.05 4.22 QR-042A 20 20 20 20 10.6 Matrix Spikc (l]580147-MS1)Sourccr1500387-07 Prepared&Analvzed:05-Feb'15 Cadmium Chromium Lead Nickel Zinc 9 t.3 llt 96.4 100 t32 0.25 0.49 0.49 o.25 0.98 men(g 98.0 98.0 98,0 98.0 98.0 0.484 10.6 8.90 8.98 43.1 92.6 103 89.3 93.3 91. I 82-l t I 73-124 56-137 7 t-t25 s9- I 36 Oilfi eld Environmental and Cornpliance The resuhs itr this report apply to the sanples analy:ed in accordance wilh the chain of custody docpment. This analylical ,eport must be reproduced i,1 its entirety, TEL: (805) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 7 of l2 Oilfield Environmental and Compliance, INC Earth Systems Pacilic 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project 539 Marsh St, SLO Froject Nurnber: SL-17522-EA Reporfed: 19-Feb-t5 16:07Project Manager: Tim Total Metals by EPA 6000/7000 Series Methods - Quality Control I{eporting Spike Level Source Result %REc %REC Limits RPD LimitResultLimit Units RPD Notes Batch 8580147 - EPA 30508 Matrix Spikc Dup (8580147-MSD1 Sourcc: 1500387-07 Prepared & Analyzed: 05-Feb-15 Cadmium Chromium Lead Nickel Zinc 85.3 104 90.7 94.6 125 0.23 0.45 0.45 0.23 0.91 mg/kg 91.0 9l.0 91.0 91.0 9l .0 0.484 10.6 8.90 8.98 43,1 93.2 103 89.9 94.1 90.4 82-lll 73-124 s6- I 37 71-125 59-136 6.76 6.45 6.09 5.96 5.52 20 20 20 20 20 Oilfield Environmental and Compliance The results in this report apply to the sanples analy:ed in accordance with tle chain of crtstody doctrment. This analytical report must be reprcduced in its entirety. TEL: (805) 922-4772www.oecusa.com FAX: (805) 925_3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page I of 12 Oilfield Environmental and Compliance, tNC Earth Systeurs Pacilic 4378 Otd Santa Fe Rd. San Luis Obispo CA,93401 Projece 539 Marsh St, SLO Project Number: SL-17522-EA Project Manager: Tim Conroy Rcportetl: 19-Feb-15 l6:07 STLC lVletals by 6000/7000 Series Methods - Quality Control Reporting Limit Units Spike Lcvel Source Result %REC Limits RPD Result %I{EC RPD Limit Notes Batch B580488 - EPA 30508 Leachate Blnnl< (8580d88-BLI( l)Prepared & Analyzed: l?-Feb-I5 Lead LCS (B5B04B8-BSr) ND 0.050 mglL Prepared & Analyzed: 17-Feb-15 Lead LCS Duo (8580488-8SDl) 9.75 0.050 mg/L 10.0 97.5 80-120 Prepared & Analvzed: l?-Feb-l5 Lead Dunlicate (8580488-DUPI) 9.81 0.050 mgll- Source: 1500466-01 10.0 98.t 80-120 Prepared & Analvzed: l7-Feb-I5 0.614 20 Lead Matrix Soilcc 0580488-MSl) 7 -21 0.050 mg/L 7.Q2 Source: 1500466-01 Prepared & Analyzed: l?-Feb-I5 2.74 20 Lead Matrix Spike Duo G580488-MSD 1) l7.l 0.050 mg/L Sourcc: 1500466-0f 10.0 7.02 l0l 75-125 Prepared & Analyzed: l?-Feb-t5 Lead 16.8 0.050 mc/L 10.0 7.02 97.9 75-125 1.68 20 Oilfield Environmental and Compliance The resulls in this ,eport apply to the samples analy-"ed in accotdance with the chain of cttstody document, This analytical report mftst be reprodtoed in i(s entirety. TEL:(805) 922-4712www.oecusa.com FAX:(805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Page 9 of 12 Oilfield Environmental and Compliance. INC Earth Systems Pacific 4378 OId Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Nunrber: SL-l'l 522-EA Reported: l9-Feb-15 l6:07N,lanager: Tim Conroy TCLP Metals by 6000/7000 Series Methods - Quality Control Analyte I{esult Reporting Limit Units Spike Levcl Source Result %REC %REC Limits RPD RPD Limit Notcs Batch 8580566 - EPA 30508 Leachate Blank (8580566-BLK1)Prepared & Analy'zed: 19-Feb-15 Lead LCS (BsB0s66-BS1) ND 0.050 mg/L Prepared & Analyzed: l9-Feb-15 Lead LCS Dup (8580566-BSD1) 9.70 0.050 mgil 10.0 97.0 80-120 Prepated & Analyzed: l9-Feb-15 Lead Duplicate (8580566-DUPI ) 9.94 0.050 mg/L Source: f500455-05 10.0 99.4 80-120 2.39 20 Prepared & Analyzed: l9-Feb-15 Lead Matrix Spilce (8580566-MSf ) Ll8 0.050 mg/L Source: 1500455-05 1.08 Prepared & Analyzed: 19-Feb-15 8.48 20 Lead Matrix Spilte Dup (8580566-MSDI) I 1.4 0.050 mg/L Source: 1500455-05 10.0 1.08 103 7s-125 Prepared & Analyzed: I9.Feb-15 Lead I 1.1 0.050 mg/L 10.0 1.08 100 75-125 2.31 20 Oilfield Environmental and Compliance The results in this reporl apply lo the samples analy:etl in accordance ntith the chain ol custody docun,ent. This analytical report must be reproduced inits entircly. TEL: (80s) 922-4772www.oecusa.com FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA93454 Page l0 of 12 Oilfield Environmental and Compliance, INC Earth Systems Paciflrc 4378 Old Santa Fe Rd. San Luis Obispo CA,93401 Project: 539 Marsh St, SLO Project Number: SL-l 7522-EA Project Manager: Tim Conroy Reported: l9-Feb-15 l6:07 TEPII by GC FID - Quality Control Reporting Spike Source Result %REC Limits RPD LimitResultLimit Units Level %REC RPD Notes Batch 858014 O - EPA 35508 Blank (B5B0l40-BLKI)Prepared & Analyzed: 05-Feb-15 TPH Diesel (C l3-C22) TPH Motor Oil (C23-C40) ND ND l0 50 mg/tC Surrogate : o-Te rphenyl LCS (BsB0l40-rlsr) 52.0 50.0 104 6t-t42 Prepared & Analyzed: 05-Feb-15 TPH Diesel (Cl3-C22)502 I0 mC/kS 500 r00 83-l 14 Surroga t e : o -Te rphe ny I LCS Duo G5B0l40-BSDI) s2.4 50.0 t05 6t-t42 Prepared & Analyzed: 05-Feb-15 TPH Diescl (C l3-C22)sl0 l0 rng/kg 500 102 83-l 14 r.55 20 Strrogate : o -Te rphenyl Durrlicatc (BSB0l 40-DUPI ) 52.7 x Source: 1500466-02 s0.0 t|s 6t-t42 Prepared & Analyzed: 05-Feb-15 TPH Diesel (C l3-C22) TPH Motor Oil (C23-C40) ND ND l0 50 mg/kg ND ND 20 20 Svr rogale : o -Te r phe nyl Matrix Spilre (l]5801 40-MS l) 5 1.2 102 6r-t42 Source:1500466-02 Prepared&Analyzed:05-Feb-15 50.0 TPH Diesel (Cl3-C22)500 l0 mg/kg 500 ND 99.9 71-128 Surrogale : o-Terphe nyl Matrix Spihc Dup (8580140-MSDI)Sourcc: 1500466-02 50.0 102 6t-t42 Prepared & Analyzed: 05-Feb-15 51.2 TPtt Diesel (Cl3-C22)513 t0 mc/ke s00 ND 103 1l-128 2.56 20 Sur roga le : o-Te rphe nyl 5/.8 50,0 104 6t-t42 Oilfield Environmental and Compliance The rasults in this report apply to the santples analy:ed in accordonce vith the chainol custody docnnent. This analytical report nn$t be rcproduced in its eiltituty. TEL: (805) 922-4112www.oecusa.Gom FAX: (805) 925-3376307 Roemer Way, Suite 300, Santa Maria, CA 93454 Pagc ll of12 Oilfield Environmental and Compliance, tNC Earth Systems Pacific 4378 Old Santa Fe Rd. San Luis Obispo CA, 93401 Project: 539 Marsh St, SLO Project Number: SL- 17522-EA Project Manager: Tinr Conroy Rcported: 19-Feb-15 l6:07 Notes and Definitions QR-04 N-07 N-03 N-02 DET ND NR dry RPD The RPD exceeded the QC conirol limits. STLC analyte concentration exceeds STLC limit. Analyte concentration above 20x TCLP. Analyte concentration below TTLC but above I 0x STLC. Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Oilfield Environmental and Compliance The results irt this report apply to the santples analy=ed in accordqnce with the chain o! cnstody doctorent. This analytical report t tust be reproduced in its entirety. TEL: (805) 922-4712ww\A/.oecusa.com FAX: (905) 925-3376307 Roemer Way, Suite 300, Santa Maria. CA 93454 Page t2 of 12 Rw 082012. 101 ,Adkisson Way,Taft, CA 932$8 phone: {661) 762-9143 CHAIN OF G.U$TODY of Oilfield' Environrnental and Gornpliance 307 RoemerWaY, Santa Maria CA 93454 phone:$a51922-4TT2 tax: (805) 92$3376 wwwoeGusa,Gom Page uaress: Ll Bp ):lL Fax:E.mall:rhone: lo: iend via- FAX. Turnaround Time eceited .etelved $pecial lnstructions: Comments/P0#:* Matrlx Key A = vapor,l ait s: solld / sedlment p = proO*il on Hw=hsmsto (Uq.) WATERTypS: ?w= drinkins GW = gFur|d Pl,Y= prpdued SW=suriace ... l/VW=vrEste X 3 X )( xKX Analysis Requested X Xx 'fu'{ '10 tfr 5 Matrixo Client Sample lD EDD.Geotracker EDF- ASAP.24hr-48 hr-72hr- (sae #of Gont- l*,4- I /1-n-r? ti-* ->/ I -lyu #e-3 / 4-LTu'/ n-tL"t*A^ 1 b/^A- + / ag*eu I I t I I t ji/Dl'lme:Dale: s s s s O Tlme: Time: '{ \) Ttme: -3-/Tlme: Date: Datea Date: ztVLt{"44t T[3[$-mr Hbltf- yotJ >{bltGr€a ,-lj I t{^ py >lblK-*41 eceived COCRECEIVED b @D,A.TE/TIME: REcEmr cLIENT: €nPTll ,uee^'s -3"/S @- N?{ oEC rD #: t Foaqb b Temp of1 ,dcceptable Rnnge: 0oC to 6oC G REFRXGERATOR(s)' 4 ,4 Rw- 0t/15,/10 D 6/* ffioec Courierlsampler E Oelivery(Other than OEC Courier) Fs-rpl*, Received on lce fl Samples Received Outside Temp. Range* I Samples Direct from field (Outside Temp) COC document(s) received with samples Correct containers for analysis requested Container(s) intact and in good condition Container label(s) consistent with COC OEC preservative added (**note std ID) Yes No F fl+Fd r--''r*M-w._ .*trr.ax fl*o nntrn!*tr fl* N/A u tr n n m & K h/i1AJ (*) PR0BLEM cHArN roRM ryE*R Custocly Seats (circle): Presettt lffTp Samples / Coolers Intact l Broken* Method of Shipment & ltracking #iirapplioable): D After-Hours Outside Drop'off iBrought Insidel Proper preservation on sample label(s) CONDITtrON & PRESERVAfiON:RECEtrPT,TRANSPORT,SAMPLE VOA conbiners free of headsPace(Initials/DatdTime): (**) OEC Preservative ID: Dissolved Metals Filtration: ( Datc/l ninPreserve I D 1 Commenb / Remarks / Condition Notes, Efc, Date/Time Sampled ***Matrix *( ResCl /pH Preservative :..' e#Ej- duegj Container DescriPtion I It CIient.IE tlf*Ifblank, rcfer to Coc GES AND/OR CORRECTIONS CHANGES AI]'f,HORTZED EY:CHANCONTAINERS, COC OECID RECEIPT LOGIN BY:lpxt RSCETPT BEVIEWED BY:of 4/ CtsLEM CI{ATN CLIENT: ISSUES RECORDED BV (DATE/TIMENNITIALS):6 4 1'ttr#OEC ID #: /€oo q65 ISSUE(S): PLEASE PROVIDE DETAILS EI Samples Received Outsitle Temp. Range (see H Incorrect containers foianalysis requested E OfffEn: (ifmultiplc, idenriswittr numbers) fl Container($ NOT intact or in good condition H Custody Seals Broken document(s) necessarya5 coc samples with with Affecte4 consistent received NOTIabel(s) Samples/Containers COC Container NO BELOW tr H rssrJE(s) Iow) OF be il a-t/2-fS**Pv€ I (2 ?1 Me<Cou ',4*s /2 3o'ju"f,su'3 rl (f @ -tl,, 4n MINIMUM INFO:- Contact uthorization Contact - Date/lime/Initials- ClientA F"INAL RES0LUTION OF ISSIIES BY (DATE/TIME/INITIAIf): z_2Page- ol' ott0g/os Oilfield Environ,rnental and Compliance 307 Roemer l/Yay, Santa Maria GA. 93454 phone: {S05) s224772 fax (805) 925'3376 . ' Rav 062012 ' 101 Adkisson WaY,Taff, CA 93268 phone: {66{} 762-9143 cr-lAlhr 0F GN..,ST'ODY wY'/v/.oecusa.c.om Page of aaaress: Lk 8p E-mall: Phone: To:t& Send rePort vla- FAX. Turnaround Timo Recelved Received Fax: PDF. Special lnstructions: Comments/PO#:* Matrix Key {=vapor/air 3=solid/sodlmert p=produci/oll HW = haz wastQ (Liq.) WATER TYp6s; DW = drinking 6itY = ground P\,\, = produed WV = surface UYW = w6ta X s \) -rEi t-L 3 Name/#: A.nalysis Requested 9-"-F X X - d6'l t-f t Matrlxn 510 Days- Client SamPle lD EDD-cEotracker EDF- ASAP-48 hr-24hr-72hr- (seeDate/Tlme Sampled #ol Cont xf ** ->/ g -lyu t+fr-3 /4-L 9- lLq/LTA- 1 q (az3 -rA \ l I t I I I .ir.6T[me:Date: 5 s s s 6 s I Date: -3-/ -rtTime: /{/oTime: TIme: Tlme: Date: Date: ).l3ltd-;lz til$-ntt il?Lt{-44, vtslS-w I tllfi{- yatl >/+lti- ato Recelved COCRECEIVED Rq,0li!5/10 {e S;/ LE RECEIPT GLIENT; €*pfrfl flve€^s oEC t (4 /s2{D RECEIPTLOGIN DATE/TIME ID #: l yooUb b Temp: AccePtablcRange: l}oc to 6oC I{EFRTGERATOR{s), { 4-' 4 oc DATE/TIME: KOpC Courier/Sampler COC document(s) received with samples D Oelivery(Other than OEC Courier) Correct containers for analysis requested Fsun,pt.. n"ceived on Ice Containe(s) intact and in good condition il samples Received outside Temp. Range* container label(s) consistent with coc fl Samples Direct from field (Outside Temp) OEC preservative added (+*note std ID) I after-Hours outside Drop-off [Brought Inside] Proper preservation on sample label(s) ', Yes No N/Am fl* D E{ Fl'r. n -@,rg. n E"rJ, -f]* tr f]*n [ trtrtrKn[*m'n[*E & PRESERVATION:CONDITIONRECEIPT,TR.ANSPORT,SAMPLE Present /Custodl' Seals (ci rcle): Samples VOA containers free ofheadsPace (In itials/Date/Time) : 1*+; OEC Preservative ID: Dissolved Metals Filtration: (Date/lilt/Prescive ID) Intact / Brokentr Method of Shipment & Tracking #(ifaltplicsble): , f) PRoBLEM CHAIN Commenb / Remarks / Condition Notes. Etc' Dateffime SamDIed ***Mstrix -s lsH ResCl < Presen'ative li k!- vUerI DescriptionCohtainer t) CoCCtien6ID it*If blank reftr to CI{ANGES AI.ruI{ORIZED BY:CORRECTIONSAND/ORCOC CHANGESCONTAINERS, OEC ID RECEIPT LOGIN BY:/cr*'RECEIPT ITEVIEWED BY;6/#Pasc of i ROtsfrEM CE{AIN CLIENT: €**-rr f.,trrE**'S -. oEC ID #:/€oo q'b 6 z ISSUES RECORIIED BY (DArE/TIME/INITIALS) :3 - Ciient Authorization Contact - I)ate/Time/Initials- ContactMINIMUM N.{FORESOLI]TIONS:etc- rt-rC' c- \J*S<- {+t+-4 ca I Samples Received Outside Temp. Range.(see below) E lncorrect containers for analysis requestbd fl OTHBR: (if multiple; identiff rvitlr numbcrs) tr XO COC document(s) received with samples frContainer label(s) NOT consistent with COC fl Container(s) NOT intact or in good condition E Custody Seals Eroken BELOW - Samples/Containers Affected as necessaryPLEASE PROVIDE DETAILS OF ISSUE(S)ISSUE(S): Ha-rHns- /z'o?M*<S*nPv€ | /z rt -Jb" rfn-q4al FINAL RESOLUTION oF ISsUEs BY parnruME/I'NITIALS):Page. / of 09/09,'08 Oilfield Environrnental and Comptriance 307 Roemer WaY, $anta Maria CA 93454 phone: (805) 9224772 tax: {805) 925-3376 www.oecusa.com ' .R€v0620j12. 101 Adkisson Way, Taft, CA 93268 phone: (661) 762-9143 CFIAIN OF C{.'STCIFV Page of tecelved tocelved L6d4 ov1 Wt oLtr'v* tJ,-lls€gi i:.t :- CommentsrPO#: _sA- o-J P A A * Matrlx Key A,= vepor / air s = $lid lsediment P = producii oil !lw= hazws6la (Llq) WATERType8: Dw = driEkhg G-W = gpund pW=pmdud SW = surfaca IVW=mslo _s a- c)J6 A A A s \) q( I i,- 3 X X XK Special lnstructlons: Name/#: Analysis Requested 7 T X x X X i( Dart I Fri'{{" 10 Days-5 ASAP.24hr- #ofMatrix** Cont.(ses key) Client Sample lD EDD.Geotracker EDF- 48 hr-72hr- -t Et.bL**-t /1-t th*4 i7&-&v ** ->/ q -lyu I+A -3 / 4-LTu t+A^ 4'/ ,-,r' bfh,- + / s*-\L't aa-,^itY Gpo, ^\,J\\' -\/r I I I I I I F/oTlme:Date: 5 s S s 5 s '/ 4 Trme rtn;1/-Qo3-/ Tlme: Date: Date: Datel Tlme: I 7l7hS.44i vlsl$-wt Hbl,{- ptf >{blti- l6a YIVIt{nv >lbtK-n41 E-mall:Fax: via- FAX-PDF. Tumaround Tlme lecelved